WI0700012_Monitoring (Report) Nov - Jan 2003_20130225

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.36 ft. below measuring point.
1.52 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2213 uMhos
Temp. 19.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
'PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONIIED
Lagoon Remediation: Infiltrgtion S,agery
Spray Field X Remediation
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor
Other
Land Application of Sludge,"
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
r31
1/22/03
1/22/03 to 2/7/03
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1696
6.6
8.7
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
71.3
N/A
N/A
N/A
638.4
N/A
N/A
N/A
mg/1 Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
N/A mg/I
N/A mg/I
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/I
units
mg/I
mg/1
mg/I
mg/I
mg/1
mg/I
uMhos
mg/I
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
134.500 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/1 Sodium
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
0.64
N/A
N/A
N/A
N/A
N/A mg/I VOC
N/A mg/I
: method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Aenty Name and Title - Please type or print
V"
GW-59 Rev 4/98
ignature
er-mittee (or Authorized Agent) ( )
Da e

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name:
Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter:
Screened Interval: 18.80 ft. to 21.63 ft.
4 inch
Depth to Water Level: 7.59 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
For Groundwater Treatrnent
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2251 uMhos
Temp. 20.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
EXPIRATION DATE:
UIC X
01/15/08
NPDES
TYPE OF PERMITTED OPERATION BEING MONITCiR D
Lagoon Remediation: Infiltratibn Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of *udge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
1/22/03
1/22/03 to 2/7/03
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1120 mg/I Al - Aluminum
pH (when analyzed) 7.0 units Ba - Barium
TOC 9.5 mg/I Ca - Calcium
Chloride 40.4 mg/I Cd- Cadmium
Arsenic N/A mgll Chromium: Total
Grease and Oils N/A mg/I Cu - Copper
Phenol N/A mg/I Fe - Iron
Sulfate
Specific Conductance
Total Ammonia
TKN as N
738.6 mg/I Hg - Mercury
N/A uMhos
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
N/A mg/I
N/A mg/I
53.250 mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
ug/I
ug/I
ug/I
mg/I
0.20-0 mg/I
N/A mg/I
N/A mg/1 Ag - Silver N/A ' mg/I
N/A mg/I Se- Selenium N/A 1 mg/I
N/A mg/I Sodium N/A ug/I
N/A mg/1 Organics: (GC, GC/MS, HPLC) _.-y
N/A mg/I (Specify test method #. Attach lab report.) 4
N/A mg/1 Report attached? Yes (1) No X (2)
N/A mg/I
N/A mg/1
VOC
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
PermitiEaJ,QfAuthorized Agent)f�Na Ieyand Title - Please type or print
�rZ"" ' j 7�1 z/2 3ture o ermittee (or Authorized Agent) Da e
Signa g ) ( )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 24.50 ft. Well Diamter:
SWW-3
4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 6.13 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 1490 uMhos
Temp. 21.1 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH NC 27626-0578 Phone. [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01 /15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation : ITT)
Land Application ofludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/22/03
Date sample analyzed: 1/22/03 to
Laboratory Name:
Certification No(s) 330 10
2/7/03 0
PCS PHOSPHATE afci? ENVIRONMENT 1
PARAMETERS:
COD
Coliform: MF Fecal
Coliform: MF Total
(Note
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
(Samples for metals were collected unfiltered Yes n/a
N/A
N/A
N/A
Use MPN method for highly turbid samples)
1184
6.7
6.7
35.0
N/A
N/A
N/A
453.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
76.500 mg/I Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/1 Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
N/A mg/1 Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/l Report attached? Yes (1) No X (2)
ug/I
ug/I
ug/I
mg/I
0.09 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A ug/I
N/A mg/I VOC
N/A mg/l
method#
method#
method#
I certify that, to the best of my knowledge and belief. the information submitted in this report is true. accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per tee (of Authorized A e ) Name and Title - Please type or print
�CJt�Z J"C
flee (or Authorized Agent) (Da
Signatur
Permi g ) ( )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter:
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.94 ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 2663 uMhos
Temp. 29.7 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONI40REV,
Lagoon Remediation: InfitgtioriC Gallery
Spray Field X Remediation : a
Rotary Distributor Land Application 4-Sludge....
.v rri
DC
=-{
EXPIRATION DATE:
UIC X
01/15/08
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/22/03
Date sample analyzed: 1/22/03 to 2/7/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1940
pH (when analyzed) 6.6
TOC 8.5
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
39.8
N/A
N/A
N/A
797.7
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/1
units
mg/I
mg/I
mg/I
mg/I
mg/1
mg/1
uMhos
mg/I
mg/I
unfiltered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
Zn - Zinc
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
149.000 mg/1
(3)
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A _ mg/I
N/A mg/I
N/A mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
0.09
N/A
N/A
N/A
N/A
N/A mg/I VOC
N/A mg/I
method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/1
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ttee (of Authorized A ent) ame and Title - Please type or print
eVr-
Signature (fiermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
(nom Wm.)
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 9.52 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 3044 uMhos
Temp. 29.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
C=
CAI
c ..
2s r'
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/22/03
Date sample analyzed:
Laboratory Name:
Certification No(s)
is
r-i
0
1/22/03 to 2/7/03 �'t
PCS PHOSPHATE ail ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2168
pH (when analyzed) 6.9
TOC 13.7
Chloride 64.2
Arsenic N/A
Grease and Oils N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
987.5
N/A
N/A
N/A
/100m1 Nitrate (NO3 as N)
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
uMhos
mg/I
mg/I
Yes n/a No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
77.250 mg/I
N/A mg/I
N/A mg/I
Yes n/a No )
N/A ug/I
N/A ug/I
N/A ug/I
Ammonia Nitrogen mg/1
Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride 0.28 mg/I
N/A mg/I MIBK N/A mg/I
N/A mg/1 Ag - Silver N/A mg/I
N/A mg/I Se- Selenium N/A mg/1
N/A mg/I Sodium N/A ug/I
N/A mg/1 Organics: (GC, GC/MS, HPLC) N?
N/A mg/1 (Specify test method #. Attach lab report.) C
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC method#
N/A mg/l
: method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) and Title - Please type or print
i
gnature,fjt'"Permittee (or Authorized Agent)
-L/ZJ ,:3
(Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
013111 per.'
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.95 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 2657 uMhos
Temp. 27.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC Xf7.1
01/15/08
TYPE OF PERMITTED OPERATION BEING MONITOREI =?
Lagoon Remediation: Infiltration ;Gallery
Spray Field X Remediation : 1
Rotary Distributor Land Application of Sludge,.
0 rn
W cn t
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/22/03
Date sample analyzed: 1/22/03 to 2/7/03
C_J
cs)
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Use
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
for metals were collected
N/A
N/A
N/A
MPN method for highly turbid samples)
1880
6.6
13.3
97.8
N/A
N/A
N/A
825.4
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/1
units
mg/I
mg/I
mg/I
mg/1
mg/1
mg/I
uMhos
mg/I
mg/I
unfiltered Yes n/a
No and field acidified
Nitrite (NO2 as N) N/A
Nitrate (NO3 as N) N/A
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
66.000
N/A
N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mgll
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.04
N/A
N/A
N/A
N/A
VOC method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/1
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and impnsionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Signatur
Terry L. Baker - Manager, Environmental Affairs
Per 'trr ttee (of Authorizted Agent) ame and Title - Please type or print
d.4
7..:0 3
Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-7
Well Depth:
29.50 ft. Well Diamter: 4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level: 7.20 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.8 , Specific Conductance 927 uMhos
Temp. 22.7 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P O. BOX 29578
RALEIGH, NC 27626-0578 Phone. [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
1/28/03 fir-
1/28/03 to 2/7/03-u 71'=
PCS PHOSPHATE an'd EONMENT 1
C
CA)
t
Certification No(s) 330 10 �, R
Date sample collected:
Date sample analyzed:
Laboratory Name:
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 664
pH (when analyzed) 6.4
TOC 7.1
Yes n/a
No and field acidified
Nitrite (NO2 as N) N/A
Nitrate (NO3 as N) N/A
Phosphorus: Total as P 50.250
Orthophosphate N/A
mg/1 Al - Aluminum N/A
units Ba - Barium N/A
mg/I Ca - Calcium N/A
mg/I Ni - Nickel
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I VOC
Yes n/a No )
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/l
0.12 fng/I
N/A r yng/I
Chloride 65.0 mg/I Cd- Cadmium N/A Ag - Silver
Arsenic N/A mg/I Chromium: Total N/A Se- Selenium
Grease and Oils N/A mg/I Cu - Copper N/A Sodium
Phenol N/A mg/I Fe - Iron
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
150.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
N/A
N/A
mg/I
N/A 1-mg/I
N/A 'mg/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
method#
method#
method#
(2)
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurateand complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent Na e and Title - Please type or print
GW-59 Rev 4/98
ignature tdf,Permittee (or Authorized Agent) (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter:
2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.18 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.4 , Specific Conductance 518 uMhos
Temp. 11.6 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P O. BOX 29578
RALEIGH, NC 27626-0578 Phone. [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
01/15/08
r-�
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/21/03
Date sample analyzed: 1/21/03 to 2/7/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified
Yes n/a No )
N/A mg/1 Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
452 mg/I Al - Aluminum
8.3 units Ba - Barium
4.5 mg/I Ca - Calcium
12.6 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
0.260 mg/I Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen mg/1
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/1 Fluoride 1.89 mg/I
N/A mg/I MIBK N/A mg/I
N/A mg/I Ag - Silver N/A mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
33.9 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Se- Selenium N/A mg/I
N/A mg/I Sodium N/A ug/I
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Mg - Magnesium
N/A mg/1 Mn - Manganese
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
N/A mg/I method#
: method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurateand complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per(of Authorize�t) Name and Title - Please type or print
ignatureermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter:
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level:
Measuring Point is
2 inch
4.96 ft. below measuring point.
3.86 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: 2200
Field Analysis: pH 6.0 , Specific Conductance 297 uMhos
Temp. 13.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application tiftludge
q , r
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed: 1/21/03 to 2/7/0
Laboratory Name: PCS PHOSPHATE dad ENVIRONMENT 1
Certification No(s) 330 10
1/21/03
fri
r,1
c-)
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No )
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 260 mg/I Al - Aluminum
pH (when analyzed) 5.8 units Ba - Barium
TOC 4.1 mg/I Ca - Calcium
Chloride 30.0 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I Fe - Iron
Sulfate 21.2 mg/I Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
3.475
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.29
N/A
N/A
N/A
N/A
VOC : method#
method#
method#
ug/I
ug/I
ug/I
mg/1
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and impnsionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent)
me and Title - Please type or print
(Dat)
ignatur iff Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter:
2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 10.22 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.6 , Specific Conductance 579 uMhos
Temp. 16.6 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X
EXPIRATION DATE:
01/15/08
Rotary Distributor
Other
UIC
Remediation: Infiltration _Gallery
Remediation : c
[.o
Land Application of eludOi :x?
t '
Note: Values should reflect dissolved and
colloidal concentrations
<n
Date sample collected: 1/21/03 ct) r^^•
Date sample analyzed: 1/21/03 to 2/7/03O
Laboratory Name: PCS PHOSPHATE an? ENYfJRONMENT 1
Certification No(s) 330 10
—t7
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 550
pH (when analyzed) 7.8
TOC 6.5
Chloride 13.7
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I Nitrite (NO2 as N)
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/1
mg/I
Nitrate (NO3 as N)
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
mg/I Fe - Iron
34.7 mg/I Hg - Mercury
0.556 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
<0.001 mg/I Ag - Silver
<0.005 mg/I
N/A mg/I
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Se- Selenium
Sodium
0.44
N/A
N/A
N/A
N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/I VOC
0.060 mg/I
method#
method#
method#
ug/I
u g/I
ug/I
mg/l
mg/l
mg/I
mg/I
mg/I
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Perr»i4te -.(of Authorized Agt) Naq'ie and Title - Please type or print
3 /e%
Da e
ignature �fq �ermittee (or Authorized Agent) ( )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well LocationslSite Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter:
4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
NIA of water pumped/bailed before sampling:
Field Analysis: pH 7.4 , Specific Conductance 552
Temp. 16.5 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
N/A
uMhos
Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
425*
7.7
4.6
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
16.0
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/l
units
mg/I
mg/I
mg/I
mg/1
mg/l
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
TYPE OF PERMITTED
Lagoon
Spray Field
Rotary Distributor
Other
01/15/08
OPERATION BEING MONITORED
Remediation: Infi tr tion Gallery
X Remediation :
Land Application ofludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
us
..
1/21/03
1/21/03 to 2/7/03CO
PCS PHOSPHATE and ENVIRONMENT 1
330 10
(.J
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/1 Fluoride
N/A mg/1 MIBK
Ag - Silver
Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
method#
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
0.031 mg/I
<0.001 mg/I
<0.005 mg/I
N/A
N/A
N/A
u g/I
ug/I
ug/I
mg/I
0.53 mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A ug/I
N/A mg/I VOC
<0.010 mg/I
method#
method#
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*ORIGINAL WAS 510 (RESAMPLED ON 2/25/03)
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authoxizeden j>l Name and Title - Please type or print
'L`z 7/DL'
SignaturPermittee (or Authorized Agent)
(Date)
GW-59 Rev 4/98

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): WLCT
Well Depth: N/A ft. Well Diamter: N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.5 , Specific Conductance 552 uMhos
Temp. 16.6 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Badge
c;
Note: Values should reflect dissolved and .c-
colloidal concentrations
—10
Date sample collected: 1/21/03 ^'-�
Date sample analyzed: 1/21/03 to 2/7/03 W cr7;..7.
Laboratory Name: PCS PHOSPHATE ar ENVIRbNMENT 1
Certification No(s) 330 10 CO
PARAMETERS: (Samples for
COD
Coliform: MF Fecal
Coliform: MF Total
metals were collected unfiltered X Yes
N/A
N/A
<1.0
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
438*
7.7
5.0
15.3
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I
mg/I
m g/I
mg/I
mg/I
uMhos
mg/I
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
0.034 mg/l Zn - Zinc
N/A mg/I
N/A mg/1
N/A mg/1
N/A mg/I
<0.001 mg/I
<0.005 mg/1
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
N/A mg/I Sodium
N/A mgll Organics: (GC. GC/MS. HPLC)
N/A mg/1 (Specify test method #. Attach lab report.)
N/A mg/1 Report attached? Yes (1) No X
N/A mg/l VOC : method#
0.53
N/A
N/A
N/A
N/A
<0.010 mg/1
method#
method#
ug/I
ug/I
ug/I
mg/l
mg/I
mg/I
mg/1
mg/I
ug/I
(2)
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*ORIGNAL WAS 530 (RESAMPLED ON 2/25/03)
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
)tee (of Authorized Ag t) N e and Title - Please type or print
ermittee (or Authorized Agent)
(Date)

PCS
PhosphatecV AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
February 27, 2003
EVAN O. KANE
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
November 2002 — January 2003
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Evan:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/ attachments)
T. L. Baker/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)

PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
Date:
Time:
Tech:
O/- as-03
�DL
System Gauge Pressures
sww-1
0-26 PSZ
sww-7
0 - / 9 Psi
cww-t
0 -B Psi"
CWW-7
.r/ - /0 Piz'
File: 12-07-02
pc: TLB
Relennce
Point MSL
Level Rel
to MSL
Ditch
12.91
'7,30
Barge Slip
10.59
0.54
Water Level
Control Tank
= MSL
80z
/3,92
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
y oa
(O.'/5
Cpz-1
10.51
Q. 90
/• //
Spz-2
11.21
A. 33
a. ge
Cpz-2
10.25
/0. / 6
0.0 9
Spz-3
11.87
, /O
S. 7'7
Cpz-3
11.12
/0.36
6. '76
Spz-4
11.45
4.702
y, 93
CPW
9.65
/0. /.Z
- 0. V/%
Spz-5
11.45
9.59
a o
W MTF-1A•
14.35
.{/8
/0./7
Spz-6
11.23
p
/.9(,
/-c2z]
MWTF-1B•
14.36
'y.96
9,4/0
Spz-7
11.59
/0.02
"57
MWTF-lC•
14.44
/O.aa
V.aa
- Spz-8 _
_ _ 11.57 _
9.. F/Q_
_-_171._L r/
_ _MWTF.-2A-
14.05 -
_ _ 6. B9
_ - % QV
Spz-9
11.01
B.3e
07.63
MWTF-28
14.02
//,//
&. f?
Spz-10
12.16
(p „sd'
6:6, V
MWTF-2C
14.08
/'9'//. 57
- O. y3
SPW
9.95
7. 7B
&./ 7
W
MTF-3A
12.21
•y.,24
7 95
MWTF-3B
12.18
/0.20
/. 9
MWTF-3C
12.19
/5 4/,„ l
-/013
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wlr
Level Ft.
Pump
Activation Depth
Rel MSL
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping?
(Y)es/(N)o
Comments
SWW-1
10.70
736
6'
/ 3/
+1'to+2'
yes
CWW-1
10.60
756
9'
-/, yy
-2'to-1'
re
SWW-2
9.99
7 59
6'
/.59
+1' to+2'
ye5
CWW-2
10.23
6. 7/
9'
'o(n . a
-2'to-1'
Yes
SWW-3
9.97
6. /3
6'
0.15
+1. to+2'
%IS
CWW-3
9.95
7./O
9'
-/ 90
-2'to-1'
_05
SWW-4
10.73
4. 91/
6'
e.99
+1'to+2'
ej
CWW-4
10.73
7.07
9'
- /9,9
-2'to-1'
Veil
SWW-5
10.80
9.s-t
6'
35,2-
+1. to+2'
Veil
CVVW-5
10.74
6.91
9'
-.2,06
-2'to-l'
SWW-6
10.66
796-
6'
/. 9Sr/
+1' to+2'
,43
e/
CWW-6
9.92
7,37
9'
- /.603
-2'to-l'
yes
SWW-7
10.70
9.20
6'
/. 020
+1 'to+2'
yef
CWW-7
9.95
6.67
9'
-033
-2'to-1'
yes
Revised 7/29/02
• Riser length added to TOC elevation 1/24/97
D:1DatalForms\Weil Form\Tank Farrn Remed Wells.xls

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
OUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
November 2002 — January 2003
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Nov
536,750
0
536,750
12.4
13.5
Dec
583,980
0
583,980
13.1
13.5
Jan
548,610
0
548,610
12.3
12.6
TOTALS
1,669,340
0
1,669,340
• C:\MyData\Reports\2003\Quarterly\TFRAS Report Fourth Quarter 2002.doc
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
zinaL
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Nov
348,436
98,624
447,060
10.3
Dec
412,343
127,763
540,107
12.1
Jan
417,770
139,407
557,177
12.5
TOTALS
1,178,550
365,794
1,544,344
- Some -additional -short -periods -of -planned -downtime -for -preventative -maintenance; pipe -header- cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 11/26 washed well. On 12/30 shook pump to start. On 1/8 changed counter.
SWW-2:
SWW-3: On 12/12 shook pump to start.
SWW-4: On 11/5 shook pump to start. On 11/6 repaired counter. On 11/14 shook pump to start. On
11/20 changed counter. On 11/26 shook pump to start. On 12/3 changed pump.
SWW-5:
SWW-6: On 1/17 washed well.
S W W-7: On 12/23 changed pump.
C:\MyData\Reports\2003\Quarterly\TFRAS Report Fourth Quarter 2002.doc
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 11/14 changed counter. On 12/30 shook pump to start.
CWW-2: On 12/10 changed pump. On 12/30 washed well.
CWW-3: On 11/19 shook pump to start
CWW-4: On 11/19 shook pump to start. On 1/15 shook pump to start.
CWW-5:. On 11/11 change counter. On 11/14 repaired counter.
CWW-6: On 12/10 washed well. On 12/18 shook pump to start.
CWW-7: On 12/27 changed pump
• C:\MyData\Reports\2003\Quarterly\TFRAS Report Fourth Quarter 2002.doc