WI0700012_Monitoring (Report) May - July 2000_20000828

raft
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
m%
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
CIW-7
Well Depth: 48.00 ft. Well Diamter:
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level:
Measuring Point is
4 inch
N/A ft. below measuring point.
N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.4 , Specific Conductance 597 uMhos
Temp. 24.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/24/00
Date sample analyzed: 7/24/00 to 8/14/00
Laboratory Name: PCS PHOSPHATE and
Certification No(s) 330 10
:z;
.;
ENVIRONMENT 1
(":-
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total <1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 438
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
7.8
6.3
9.1
N/A
N/A
N/A
20.0
N/A
N/A
NIA
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/1
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified X
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
Zn - Zinc
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
0.049 mg/I
N/A mg/1
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A ug/I
N/A ug/I
<0.001 mg/I
<0.010 mg/I
N/A ugll
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
<0.010 mg/I
Yes No
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report)
Report attached? Yes (1) No X (2)
VOC method#
N/A ug/I
N/A ug/I
N/A tg/I
yng/I
0.49
N/A fng/l
N/A trig/I
N/A t rng/l
method#
method#
N/A ug/l
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) Nafhe and Title - Please type or print
Siiggnnaatur f Permittee (or Authorized Agent) (Da
6U

ti
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO.. INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
MWTF1-CR
Well Depth: 42.00 ft. Well Diamter:
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 11.58 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
2 inch
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.6 , Specific Conductance 568 uMhos
Temp. 23.6 oC, Odor NONE
Appearance: CLEEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/24/00
Date sample analyzed: 7/24/00 to 8/14/00
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10 -. 3
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A mg/I
N/A /100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
<1.0 /100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 384
pH (when analyzed) 7.8
TOC
5.4 mg/I Ca - Calcium
Chloride
Arsenic
8.9 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
No and field acidified X Yes No
N/A mg/I
N/A mg/l
0.200 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
<0.001 mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1 Fe - Iron
34.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
<0.010 mg/I
N/A ug/l
N/A ug/I
N/A ug/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
N/A ug/I
0.028 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
w --r
J <�
N/A :zug/I
N/A oug/I
N/A tvug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
0.53C ng/I
N/A Ung/I
N/A —T1g/I
N/A mg/I
VOC
method#
method#
method#
N/A ug/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Perrytee (of Authorized Age Na - and Title - Please type or pri t
gnature oygrermittee (or Authorized Agent) '" (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 7.83 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2742 uMhos
Temp. 18.8 oC, Odor NONE Appearance:
CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/25/00
Date sample analyzed: 7/25/00 to 8/14/00'
Laboratory Name: PCS PHOSPHATE
c)
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 135.500 mg/1
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen
Dissolved Solids: Total 1680 mg/I Al - Aluminum N/A ug/I
pH (when analyzed) 6.4 units Ba - Barium N/A ug/I
TOC 11,7 mg/I Ca - Calcium N/A ug/I
Chloride 70.9 mg/I Cd- Cadmium NIA ug/l
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Arsenic N/A mg/I Chromium: Total N/A ug/I Se- Selenium
0.63
N/A
N/A
N/A
Grease and Oils N/A mg/I Cu - Copper N/A ug/I Sodium N/A
Phenol N/A mg/I Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC)
Sulfate 690.4 mg/1 Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.)
Specific Conductance N/A uMhos K- Potassium N/A ug/I Report attached? Yes (1) No X
Total Ammonia N/A mg/l Mg - Magnesium N/A ug/I VOC : method#
TKN as N N/A mg/I Mn - Manganese N/A ug/I : method#
: method#
ug/I
ug/I
ug/I
mg/I
mg/1
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) Namepnd Title - Please type or print
Za? ate
gnature ofPrmittee (or Authorized Agent)
(Da

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
(keen ye ,S)
Well Identification Number (from Permit):
SWW-2
Weil Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 7.31 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.3 , Specific Conductance 2260 uMhos
Temp. 18.4 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Appearance: CLEAR
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Q
7/25/00
7/25/00 to 8/14/00'a
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1504
pH (when analyzed) 6.7
TOC 9.9
Chloride 46.1
Arsenic N/A
Grease and Oils N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
608.3
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/1
mg/1
mg/I
mg/I
uMhos
mg/l
mg/I
Yes
n/a
No and field acidified
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/1
Phosphorus: Total as P 50.500 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/1
N/A ug/I
N/A ug/I
ug/1
ug/1
ug/I
N/A ug/I
N/A ug/i
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No
NIA ug/I
NiA ug/I
N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.25 mg/I
MIBK N/A mg/I
Ag - Silver N/A mg/I
Se- Selenium N/A mg/I
N/A Sodium N/A ug/I
N/A Organics: (GC, GC/MS, HPLC)
N/A (Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) nd Title - Please type or print
zAr
gnature o e mittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter:
4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.09 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2021 uMhos
Temp. 20.9 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/25/00
Date sample analyzed: 7/25/00 to
Laboratory Name:
G7
(„
8/14/00 T
PCS PHOSPHATE
ry
Certification No(s) 330
c1.
t V
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/l Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Orthophosphate
1396 mg/I Al - Aluminum
6.5 units Ba - Barium
9.5 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
36.4
N/A
N/A
N/A
539.4
N/A
N/A
N/A
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A mg/I Pb - Lead
42.000 mg/I Zn - Zinc
Yes n/a No
WI
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
0.14
N/A
N/A
N/A
N/A
N/A ug/I VOC
N/A ug/I
(1) No
method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per tteejofAuthorized Agent am and Title - Please type or print
S nature of mittee (or Authorized Agent) " (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
drom
Well Identification Number (from Permit):
Well Depth: 25.00 ft. Well Diamter:
SWW-4
4 inch
Screened Interval: 20,50 ft. to 23.30 ft.
Depth to Water Level: 7.70 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.1 , Specific Conductance
Temp. 31.6 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2127 uMhos
Appearance: LT RST ORANGE
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration GalleiQ '
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
J.
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/25/00
Date sample analyzed:
Laboratory Name:
C7
C)
]s.
7/25/00 to 8/14/00
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1604
pH (when analyzed) 6.4
TOC 9.4
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
38.5
N/A
N/A
N/A
735.4
N/A
N/A
N/A
mg/l
/100m1
/100m1
mg/I
units
mg/I
mg/1
mg/l
mg/I
mg/I
mg/I
uMhos
mg/I
mg/l
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
No and field acidified Yes n/a No
N/A
N/A
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/l
mg/I
102.500 mg/I
N/A mg/I
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ugfl
N/A ug/I
N/A ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
NIA
NiA
NIA
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.09
N/A
N/A
Se- Selenium N/A
N/A ug/I Sodium N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
N/A ug/I
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/1
mg/I
mg/l
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name aTitle - Please type or print
4at/
ittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
om {ro,
Well Identification Number (from Permit):
SWW-5
Well Depth: 28.21 ft. Well Diamter:
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.93 ft. below measuring point.
2.96 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2152 uMhos
Temp. 28.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation : ,..,
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor Land Application of Sludge
Other
C3
4'
Note: Values should reflect dissolved and 1a,
colloidal concentrations C7 �c rr,
Date sample collected: 7/25/00 W c:. rn
Date sample analyzed: ni
Laboratory Name: --1
Certification No(s) 330
7/25/00 to 8/14/00 —
PCS PHOSPHATE
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1688
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.6
12.5
57.3
N/A
N/A
N/A
726.8
N/A
N/A
N/A
Yes n/a No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
52.000 mg/I Zn - Zinc
Yes n/a No
ca
N/A:
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
mg/1 Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I VOC
N/A ug/I
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.23
N/A
N/A
N/A
N/A
: method#
method#
method#
ug/I
u g/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permi '.-e (of uthorized Agent) me nd Title - Please type or print
Signature o
er
ttee (or Authorized Agent)
(Dafe)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 26.00 ft. Well Diamter:
SWW-6
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.32 ft. below measuring point.
2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.3 , Specific Conductance
Temp. 29.1 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1791 uMhos
Appearance: CLEAR
PERMIT #: W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration GallerAj
Spray Field X Remediation : .c-
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor
Other
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
0
0
7/25/00
7/25/00 to 8114/00
PCS PHOSPHATE
c, r";
.r rra
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
N/A mg/I
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1424 mg/I
pH (when analyzed) 6.6 units
TOC 13.7 mg/I
Chloride 100.1 mg/I
Arsenic N/A mg/1
Grease and Oils N/A mg/I
Phenol N/A mg/I
Sulfate 399.3 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified
N/A mg/l Ni - Nickel
N/A mg/I Pb - Lead
49.000 mg/I Zn - Zinc
Yes n/a No
• NfA
— Nt/,A
NtA
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/l
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/l VOC
N/A ug/l
0.03
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/l
ug/I
(2)
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permitt-e of Authorized Agent) jiagie end Title - Please type or print
Si. ature of r?ttttee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 29.50 ft. Well Diamter:
SWW-7
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.13 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
_ Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.3 , Specific Conductance 1187 uMhos
Temp. 25.6 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X
09/30/01
Remediation: Infiltration Gali p6
Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/26/00
Date sample analyzed: 7/26/00 to 8/14/00 r 4)
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
G)
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 988
pH (when analyzed) 5.4
TOC 12.7
Chloride 163.6
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
237.1
N/A
N/A
N/A
mg/I
/100m1
/100mI
mg/I
units
mg/I
mg/l
mg/l
mg/l
mg/I
mg/I
uMhos
mg/I
mg/I
n/a
No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 59.000 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/l
Cd- Cadmium N/A ug/l
Chromium: Total N/A ug/I
Cu - Copper N/A ug/I
Fe - Iron N/A ug/I
Hg - Mercury N/A ug/I
K- Potassium N/A ug/I
Mg - Magnesium N/A ug/I
Mn - Manganese N/A ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.15
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/l
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) ame =nd Title - Please type or print
ignature odrmittee (or Authorized Agent)
(Date)

COD
Coliform: MF Fecal
Coliform: MF Total
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 6.40 ft. Well Diamter:
MWTF1-A
2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 3.80 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
[Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.2 , Specific Conductance 583 uMhos
Temp. 25.8 oC, Odor
NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/24/00
Date sample analyzed: 7/24/00 to
Laboratory Name:
PCS PHOSPHATE
Certification No(s) 330
'>7
.G"
PARAMETERS: (Samples for metals were collected unfiltered
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 360 mg/I
pH (when analyzed) 7.6 units
TOC 4.9 mg/1
Chloride
Arsenic
4.7 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
39.8 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Yes
n/a
No and field acidified
N/A
N/A
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/I
mg/I
0.496 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No
N/A mg/I Ammonia Nitrogen
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/l
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
r
:^) N/A ug/I
NIA ug/I
N/A ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
2.35
N/A
N/A
N/A
N/A
N/A ug/I VOC : method#
method#
method#
mg/I
mg/I
mg/1
mg/1
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent
am and Title - Please type or print
mittee (or Authorized Agent)

•
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 13.50 ft. Well Diamter:
MWTF1-B
2 inch
Screened Interval: 10.60 ft. to 12.60 ft,
Depth to Water Level: 4.94 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys erns Check One:
Influent (98)
Effluent (99)
2600
Field Analysis: pH 6.0 , Specific Conductance 409 uMhos
Temp. 25.2 oC, Odor NONE Appearance: LT CLOUDY
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
1
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/24/00
Date sample analyzed:
Laboratory Name:
7/24/00 to 8/14/00
PCS PHOSPHATE
Certification No(s) 330
a
PARAMETERS: (Samples for metals were collected unfiltered Yes nla
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 288
pH (when analyzed) 4.6
TOC 4.3
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
39.0
N/A
N/A
N/A
30.3
N/A
N/A
N/A
mg/l Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
mg/l
units
mg/l
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified Yes nla No
N/A
N/A
6.500
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
u g/I
ug/I
ug/I
Ni - Nickel
Pb - Lead
API/A -ug/1
N/A Pug/1
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/1
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.34
N/A
N/A
N/A
N/A
VOC : method#
method#
method#
mg/1
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permee (of _ uthorized Agent ame nd Title - Please type or prin
(or Authorized Agent)
E/zS) GTO
(Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
(from per. )
Well Identification Number (from Permit):
WLCT
Well Depth: N/A ft. Well Diamter:
Screened Interval: N/A ft. to N/A ft.
N/A
Depth to Water Level: NIA ft. below measuring point.
Measuring Point is N/A ft above land surface.
For Groundwater Treatmen
Systems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.6 , Specific Conductance 622 uMhos
Temp. 23.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallef7
Spray Field X Remediation :
09/30/01
Rotary Distributor Land Application of Sludge
Other
Fig
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/24/00
Date sample analyzed: 7/24/00
Laboratory Name:
Certification No(s) 330 10
ss
to 8/14/00
PCS PHOSPHATE
and EIVIIIONMENT 1
PARAMETERS: (Samples for
COD
Coliform: MF Fecal
metals were collected unfiltered X Yes
N/A mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total <1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 424 mg/I
pH (when analyzed) 7.9 units
TOC 6.6 mg/I
Chloride 9.2 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
19.6 mg/I
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/l Mn - Manganese
<0.010 mg/I
No and field acidified X Yes No ee
N/A mg/I Ni - Nickel re.) Ni ug/I
N/A mg/1 Pb - Lead NA ug/I
0.049 mg/I Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen mg/I
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride 0.49 mg/I
N/A ug/I MIBK N/A mg/I
<0.001 mg/I Ag - Silver N/A mg/I
<0.010 mg/I Se- Selenium N/A mg/I
N/A ug/I Sodium N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/l VOC method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agents Namand Title - Please type or print
rmittee (or Authorized Agent)
(Date

Date:
PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
7/o/S4o 0
Time:
Tech:
System Gauge Pressures
SWW-1
173E
0-/`%s/
�iYo/i.
Svvwa
0-//P6
CWW-1 .
%%-// ,tk5:
CWW-7
0 -/0.as
File: 15-03-003-02
pc: TLB
Level (msl
Ditch Level
1/45:6-0 '
Barge Slip
e, Bo: '
Water Level
38/O
Control Tank
=MSL
e /// // /
(Le
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
yo'f/e3
//MSL
`p.2/
Cpz-1
10.51
A70
/B/
Spz-2
11.21
gee
,,83
Cpz-2
10.25
/Q, OD
, 45-
Spz-3
11.87
6.c%B
s,s9'
Cpz-3
11.12
9.80
/3z
Spz-4
11.45
6. 70
7/
75
CPW
9.65
9- 78
C./ 9
Spz-5
11.45
9.a&
�',//
MWTF-1A•
14.35
�? 80
/4,53-
9 //2-
Spz-6
11.23
9. 'le
/ /5
MWTF-1 B •
14.36
.1/ 99
Spz-7
11.59
/Q OR,
/57
MWTF-1C•
14.44
/use
6 4/0
�,,,9�
7o,5-
Spz-8
11.57
e. 68
ry. p 9
MWTF-2A
14.05
Spz•9
11.01
B 38
Ote 5
MWTF-2B
14.02
/70/0
07 r . �
Spz-10
12.16
75/
‘ 9.2
MWTF-2C
14.08
/y ago
- ,//2.
SPW
9.95
778
07,/7
MWTF-3A
12.21
74/0
g//
2 02-
MWTF-3B
12.18
/a/6
MWTF-3C
12.19
/A 94/
-0: 75
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o
Comments
sWW-1
.10.70
78.6
+1 ' to+2'
745
CM-1
10.60
B.RO
ar D7l1
-2'to-1'
SWW-2
9.99
7. 3/
/ q/
+1. to +2'
785
45
CWW-2
10.23
7, 73
-'/, 27
-2'to-1'
-771/Pl
//OG//Z , f/L 9iJ
SWW-3
9.97
'7 09
/Q9
+1'to+2'
Apr
CWW-3
9.95
739
-/6r%
-2'to-1'
e5
SWW-4
10.73
770
/, 70
+1'to+2'
/"e1
CWW-4
10.73
!/J.SS
�,4
-2 ' to -1'
/itos
SWW-5
10.80
l,9.3
/2 9$
+1'to+2'
yef
J,g/z ,e oi�99el.
CWW-5
10.74
4.6Z
-a38
-2'to-1'
O1
SWW-6
10.66
7 J.z'
/JZ
+1' to+2'
�e1
CWW-6
9.92
G. 9ia
^.?, Oil
-2'to-1'
?85
SWW-7
10.70
'7./3
/ / 7
+1'to+2'
G7/5
CVVW-7
9.95
6.90
c./O •
-2'to-1'
/.lf/5
Revised 8/12/97
• Riser length added to TOC elevation 1/24/97
PCS095.XLS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
May 2000 — July 2000
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
2000
DPW WATER
GALLONS
CONDENSATE
GALLONS .
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
May
401,590
0
401,590
9.0
13.8
June
400,610
0
400,610
9.0
3.6
July
147,790
0
147,790
3.3
13.8
TOTALS
949,990
0
949,990
2

Withdrawal Well System
The Withdrawal Well System was down for a total of 7.7 hours during the period. The system was down
on 5-9-00 for 1 hour to clean air compressor cooler. The system was down on 6-27-00 for 40 minutes for
compressor maintenance. The system was down 6 hours on 7-12-00 for compressor service. The
withdrawal water well pumps are monitored daily by the area Maintenance Department and preventative
maintenance work is performed as needed. The total monthly and quarterly withdrawal water volumes for
the period are:
2000
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
May
526,766
378,467
905,233
20.3
June
490,787
238,267
729,054
16.3
July
502,725
188,570
691,295
15.5
TOTALS
1,520,278
805,304
2,325,582
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: Pump operated without incident.
SWW-2: Pump operated without incident. -
SWW-3: Pump operated without incident.
SWW-4: On 5/31, 6/5, 6/9, 6/12, 6/13, 6/15, 6/19, 6/20, 6/21 the pump was shaken to start. On 6/21 the
pump was changed.
SWW-5: On 5/16 had to shake pump to start. On 5/19 acid washed the pump. On 5/24, 5/30, 6/8 and 6/12
the pump was shaken to start. On 6/12 the pump was replaced. On 6/13 the pump was shaken to start and
then replaced. On 6/19 and 6/20 the pump was shaken to start.
SWW-6: On 6/6 the pump was shaken to start. On 6/23 the pump was replaced. On 7/20 the pump was
shaken to start.
3

SWW-7: Pump operated without incident.
Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 6/9 the pump was replaced. On 7/19 the pump was shaken to start.
CWW-2: On 6/16 the pump was replaced.
CWW-3: On 6/7 and 6/8 the pump was shaken to start.
CWW-4: Pump operated without incident.
CWW-5: On 6/28 the pump was shaken to start.
CWW-6: On 5/31 the pump was replaced. On 7/25 the pump was shaken to start. On 7/26 the pump was
cleaned.
CWW-7: On 6/27 the pump was shaken to start. On 7/13 the pump was acid cleaned. On 7/19 the pump
was pulled and cleaned.
4

•
August 28, 2000
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
PCS
Phosphatece AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
w
Subject: Underground Injection Control Program
Second Quarter Groundwater Monitoring Report
May 2000 — July 2000
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
/0, &J/Lla, 1/34.,--kA2-CLeA ITT
D. Daniel Winstead III
Environmental Engineer
Environmental Affairs
Attachments
pc: Willie Hardison / Keith Starner — DWQ- GWS, WaRO (w/attch)

bpc: T. L. Baker / 12-01-008-03-002 (w/ attch)
J. A. Hardy / R. B. Lee / T. W. Davis (w/ attch)
R. A. Allen / T. Lewis (w/attch)
D. D. Winstead / 00-24-000 (w/o attch)
W. A. Schinuning (w/o attch)
2