WI0700012_Monitoring (Report) May - July 1999_19990823

GROUNDWATER QUALITY MONITORING:
'COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 7.39 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2607 uMhos
Temp. 18.5 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4,0
t_D
7/15/99
7/15/99 to 8/5/99 (7)
PCS PHOSPHATE
330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1588
pH (when analyzed) 6.5
TOC 9.8
Chloride 43.2
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
771.4
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
129.500 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
.1
NjA"'-' ug/I
t14A ug/I
ugfl
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
0.73
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/l VOC : method#
method#
: method#
N/A ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
66
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of A fir• a t) Name and Title - Please type or print
Sign2fure of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from
Well Depth: 23.00 ft.
Screened Interval: 18.80 ft.
Depth to Water Level: 7.42 ft.
Permit):
Well Diamter:
to 21.63 ft.
SWW-2
4 inch
below measuring point.
Measuring Point is 3.42 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2162 uMhos
Temp. 18.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
w
7/15/99
ci
7/15/99 to 8/5/99 iNa
PCS PHOSPHATE rn
Certification No(s) 330
I
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1456
6.6
8.6
44.7
N/A
N/A
N/A
611.5
N/A
N/A
N/A
mg/I
units
mg/I Ca - Calcium
mg/I
mg/I
mg/I
mg/I Fe - Iron
Yes n/a No and field acidified Yes n/a No
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
mg/I Hg - Mercury
uMhos
mg/I
mg/I
71.500 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N9A
`ia N31
NiA
N/A mg/I Ammonia Nitrogen
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A ug/l
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Se- Selenium
Sodium
0.19
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC
N/A ug/I
: method#
: method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of th ized ent) Name and Title - Please type or print
Sig ature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 24.50 ft. Well Diamter:
SWW-3
Screened Interval: 20.17 ft. to 23.00 ft.
4 inch
Depth to Water Level: 7.02 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1738 uMhos
Temp. 23.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/15/99
Date sample analyzed: 7/15/99 to 8/5/99
lD
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
Yes n/a No and field acidified Yes n/a No
N/A mg/I
N/A mg/1
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1240 mg/I Al - Aluminum
pH (when analyzed) 6.2 units Ba - Barium
TOC 7.8 mg/I Ca - Calcium
Chloride 35.6 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I Fe - Iron
Sulfate 550.8 mg/I Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
91.500 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.13
N/A
N/A
N/A
N/A
N/A ug/l Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC
N/A ug/I
method#
method#
method#
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of jythorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
o-nw
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter:
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.02 ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2078 uMhos
Temp. 29.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/15/99
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
7/15/99 to 8/5/99
Certification No(s) 330 �.
l
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified Yes n/a No
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead taN/Act ug/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 105.500 mg/I Zn - Zinc N/A` ug/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/1 Ammonia Nitrogen mg/I
Dissolved Solids: Total 1628 mg/1 Al - Aluminum N/A ug/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) 6.3 units Ba - Barium N/A ug/l Fluoride 0.11 mg/1
TOC 9.2 mg/I Ca - Calcium N/A ug/I MIBK N/A ug/I
Chloride 45.7 mg/I Cd- Cadmium N/A ug/I Ag - Silver N/A ug/I
Arsenic N/A mg/I Chromium: Total N/A ug/I Se- Selenium N/A ug/I
Grease and Oils N/A mg/1 Cu - Copper N/A ug/I Sodium N/A ug/l
Phenol N/A mg/1 Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC)
Sulfate 699.1 mg/I Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A ug/I Report attached? Yes (1) No X (2)
N/A mg/I Mg - Magnesium N/A ug/I VOC
N/A mg/I Mn - Manganese N/A ug/I
Specific Conductance
Total Ammonia
TKN as N
: method#
: method#
: method#
4--f\1/Acl ug/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
_608£'66
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of{pthor*d Agent) me and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 6.86 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.2 , Specific Conductance 2035 uMhos
For Groundwater Treatment
Sys erns Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Temp. 28.9 oC, Odor NONE
Appearance: LT YELLOW CLDY
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/15/99 to
Date sample analyzed: 7/15/99 to 8/5/99c
Laboratory Name: PCS PHOSPHATE `..
fv
Certification No(s) 330 al
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1544
pH (when analyzed) 6.7
TOC 12.2
Chloride 65.3
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate 651.9
N/A
N/A
N/A
Specific Conductance
Total Ammonia
TKN as N
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Yes n/a
No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 53.500 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium N/A ug/I
Chromium: Total N/A ug/I
Cu - Copper N/A ug/I
Fe - Iron N/A ug/I
N/A ug/I
K- Potassium N/A ug/I
Mg - Magnesium N/A ug/I
Mn - Manganese N/A ug/I
Hg - Mercury
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
rn
N/At± ug/I
N :71 ug/I
141.A1 ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.26
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS,
(Specify test method #.
Report attached? Yes
VOC
HPLC)
Attach lab report.)
(1) No X
method#
method#
method#
mg/I
mg/I
ug/I
ug/I
ug/I
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
OCOoCZ66
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of AytkyrizeQ Agent) game and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter: 4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.35 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 1657 uMhos
Temp. 28.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1268
pH (when analyzed) 6.5
TOC 14.1
Chloride 108.8
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate 303.4
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I Ca - Calcium
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
7/15/99
7115/99 to 8/5/997a
PCS PHOSPHATE
330 —'
No and field acidified Yes n/a No
N/A mg/I
N/A mg/I
73.000 mg/I
N/A mg/I
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
Ni - Nickel
Pb - Lead
k c�
N/A
N/A
Zn - Zinc N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.06
N/A
N/A
N/A
N/A
N/A ug/l VOC : method#
method#
method#
N/A ug/I
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of orized Agenjl.Name and Title - Please type or print
Signature of Permittee (or Authorized Agent)
e-
(Date)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 29.50 ft. Well Diamter:
SWW-7
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.31 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.7 , Specific Conductance 1252 uMhos
Temp. 26 oC, Odor NONE Appearance:
CLEAR
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
N/A mg/I
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 986
pH (when analyzed) 6.0
TOC 12.3
Chloride 86.1
Arsenic N/A
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
288.8
N/A
N/A
N/A
mg/I
units
mg/1
mg/I
mg/1
mg/I
mg/1
mg/I
uMhos
mg/I
mg/I
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and '4.1.J
colloidal concentrations >'
Date sample collected: 7/15/99 cam-)
Date sample analyzed: 7/15/99 to 8/5/99 N
Laboratory Name: PCS PHOSPHATE "'
Certification No(s) 330
No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A mgll
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 74.500 mg/I
Orthophosphate N/A mg/1
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium N/A ug/I
Chromium: Total N/A ug/I
Cu - Copper N/A ug/I
Fe - Iron N/A ug/I
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/l
Ni - Nickel
Pb - Lead
Zn - Zinc
NiA'
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.10
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/l
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
C0 Z66
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authygzed Agent Narrpand Title - Please type or print
f-25
(Date)
Signature of Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
(fool pernn
Well Identification Number (from Permit):
Well Depth: 6.40 ft. Well Diamter:
MWTF1-A
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level:
Measuring Point is
2 inch
3.75 ft. below measuring point.
3.86 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 7.0 , Specific Conductance 639 uMhos
Temp. 28.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
t0
tt�
7/19/99 x.
7/19/99 to 8/15/994o—j
PCS PHOSPHATE ry
330 caz
�•ro
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal
Coliform: MF Total
mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
Yes nla No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 410
pH (when analyzed)
TOC
Orthophosphate
mg/I Al - Aluminum
7.3 units Ba - Barium
5.0 mg/I Ca - Calcium
Chloride
Arsenic
10.1 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
18.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.562 mg/I
NJA ug/I
N/A mg/I Pb - Lead c n N/9 ug/I
Zn - Zinc Nf ug/I
N/A mg/I Ammonia Nitrogen mg/I
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
2.00
N/A
N/A
N/A
N/A
N/A ug/I VOC : method#
method#
method#
N/A ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Auth d A ent) Nam nd Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter:
2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 4.54 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 5.5 , Specific Conductance 476 uMhos
Temp. 25.9 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
7/19/99
7/19/99 to 8/5/99 N
PCS PHOSPHATE is
CZ: rn
`.
Certification No(s) 330 sm•
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 390
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.2
4.2
61.0
N/A
N/A
N/A
62.0
N/A
N/A
N/A
Yes n/a
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/1
mg/I
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified Yes n/a No
N/A mg/1 Ni - Nickel
N/A mg/I Pb - Lead
7.600 mg/I Zn - Zinc
CA N/A'
N/Z JC
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.24
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
N/A ug/l
method#
: method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
° c Z66
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authoriz Age t) Name d Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): MWTF1-C R
Well Depth: 42.50 ft. Well Diamter:
Screened Interval: 40.50 ft. to 42.50 ft.
Depth to Water Level:
Measuring Point is
2 inch
9.75 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling: 33
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
Field Analysis: pH 7.2 , Specific Conductance 632 uMhos
Temp. 22.8 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and n
colloidal concentrations to c3
Date sample collected: 7/20/99 3a• 27-
Date sample analyzed: 7/20/99 to 8/5/99c= or?
Laboratory Name: PCS PHOSPHATE and EINROWIINENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total <1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
/100m1 Phosphorus: Total as P
Orthophosphate
480 mg/I Al - Aluminum
7.5 units Ba - Barium
5.0 mg/I Ca - Calcium
Chloride
Arsenic
49.0 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
0.265 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Nf4i ug/I
u1 NcA ug/I
WA ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
<1.0 ug/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
47.1 mg/! Hg - Mercury
<5.0 ug/I
N/A ug/I
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
38.0 ug/I
Se- Selenium
Sodium
0.57
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
method#
method#
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
0 C Z 66
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Author d AgenJNae and Title - Please type or print
a'- ZV -97
Signature of Permitfee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jimmy Hardy
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter:
Screened Interval: 31.00 ft. to 45.25 ft.
4 inch
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
For Groundwater Treatrnent
Sys ems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.4 , Specific Conductance 533 uMhos
Temp. 23.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/20/99
Date sample analyzed: 7/20/99
Laboratory Name:
c.,
on
>o
PCS PHOSPHATE and ENtVIIROM1ENT 1
r
0)
N
crk
to 8/5/99
Certification No(s) 330 10 r.^
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
mg/I Nitrite (NO2 as N)
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 410 mg/I
pH (when analyzed) 7.8 units Ba - Barium
TOC 5.0 mg/I Ca - Calcium
Chloride 9.0 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I
Sulfate 21.4 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
0.205 mg/I
N/A mg/I
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
<10.0 ug/I
N/A ug/I
N/A ug/I
<1.0 ug/I
<5.0 ug/I
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
method#
method#
Yes n/a No
N�?4 ug/I
N/A ug/I
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/1
Other (Specify Compounds and Concentration Units)
Fluoride 0.58 mg/I
MIBK N/A ug/I
Ag - Silver N/A ug/I
Se- Selenium N/A ug/I
N/A ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
? 66
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authorized gent) l hne and Title - Please type or print
4P-2J -9r
Signature of Pernlittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
WLCT
Well Depth: N/A ft. Well Diamter:
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level:
Measuring Point is
N/A
N/A ft. below measuring point.
N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.5 , Specific Conductance 545 uMhos
Temp. 24.7 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge co
tb :r
to
Xi, E2-�
N r3.Z
CII 3E rn
7/20/99 T„ —�-t�'
7/20/99 to 8/5/99:-= of
PCS PHOSPHATE and EtiIRCifii_ifiNT 1
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10 01
—i
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
mg/I
/100m1
/100m1
(Note Use MPN method for highly turbid samp es)
Dissolved Solids: Total 420 mg/I
pH (when analyzed)
TOC
Chloride
7.8 units
4.9 mg/I
7.8 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/1
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
17.1 mg/I
N/A uMhos
N/A mg/I
N/A mg/1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
0.022 mg/I Zn - Zinc
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
<10.0 ug/I
N/A ug/l
N/A ug/I
<1.0 ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
<5.0 ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.58
N/A
N/A
N/A
N/A
N/A ug/I VOC : method#
method#
method#
ug/l
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Author and Title - Please type or print
rf'L,�-�jj
Signature of Permittee (or Authorized Agent) (Date)

Date:
Time:
Tech:
PCS Phosphate Co., Inc. - Tank Farm Remediation System Monitoring
S/&5799
,4m
System Gauge Pressures
SWW-1
. -al 67"111
swW-7
O-&Sts:
®-/?% GUi
Cww.,
CWW7
O -/S st11
File: 15-03-003 02
pc: TLB
Ditch Level
S a4 r
Barge sop
9 GO
Water Level
9 t
9 /�
Control Tank_
$eMSL
/5i49/
Sand Layer Pelzometers Level Indicators
Weil ID
TOC
Elevation
MSL'
TOC
Stc WV
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc WIr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
.5 OV/
�f/3
Cpz-1
10.51
7 V3 ,
c7. le e
Spz-2
11.21
(ef
a 5-4
Cpz-2
10.25
9; %Y
O. 57
Spz-3
11.87
6.71
09
Cpz-3
11.12
t W
cp. sir
ail/
AO qs'
Spz-4
11.45
X/•,
.9S/
CPW
9.65
9. 3/
Spz-5
11.45
94 9
, Do.
MWTF-1A •
14.35
//, DD
Spz-6
11.23 •
9. go
/. (l
MWTF-1B •
14.36
g, Qy
9 3.2
Spz-7
11.59
/f%..0 p
I. 57
MWTF-1C •
14.44
,s,
MWTF-2A MTF-2A
14.05
4.6 6
p 7 y
Spz-8
11.57
G
Spz-9
11.01
�7f
p. 42
p'/.3?
MWIF-2B
14.02
/, /pO
0tea
0•2? .
gp9
l 0'9
spz-10
12.16
5'. 4/9
G./2.
MWrF-2c
14.08
/3. fly/
SPW
9.95 _
7 90
A'.es"
MWIF-3A
12.21
y,/�
/O29
MWTF-3B
12.15
MWTF-3C
12.19
/2-.19
• D AO
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wir
Level Ft.
Max Level
Relative To
MSL FL
Control
Point
MSL'
Is Well
Pumping
(Y)es/(MO
Comments
5ww-,
10.70
/p.9S
a•/S
+1'to+2'
"j/�
CWw-,
10.60
7S5
-/S5
-2'to-1'
Vtv
SWW-2
9.99
7.37
/.63
+1'to+2'
Vei
CWW4
1o.23
7 77
/ 79
•2'to-l'
re
SWW-3
9.97
4.57
o 4'?
+1'to+2'
CVVW-3
9.95
7 ff/
-ZJ/
-2'to4'
rife
G:
SWW�
10.73
75:2
/. y�
+1' to +2'
e ]
CWW-4
ion
r
/•/V
-/ /V
-2'to-1'
/P
SwWs
to.80
7; 26
/Oo
+1'to +2'
CWW-5
10.74
%76,
-'7 7l
-2'to-1'
SWW.B
10.68
6. p_9
2.//
+1'to+7
.�rf-5
•'�( E�i
W CWB
9.92
7,//J
••/ 4/9
-1
-2'to'
SWW-7
10.70
r7gO
_EO
+1•to+2'
1{�j
{ e-5
CWW-7
9.95
G.os
-tot
-2'to-1'
1(B5
.
Da.,.aw RJI IOT
• Di ar Iannll. n.1Aael In Witt elnuellnn 4111107
prsa9.5.xi S

7/s/99
,PCS Phosphate Co., Inc. - Tank Farm Remediation System Monitoring
Date: 6//s/99
Time: y/rj
Tech: - ,5".43 sec;i
System Gaugo Pressures
SWW-1
D-; .3
SWW-7
D - /.-
cww-,
e - /4/
CWW-7
O -/r7
Fde: 15-03-003-02
pa TLB
Level Imei
Ditch Level
</. 79 I
Barge Slip
9.89
Water Level
9 y) t
Control Tank
_
•�=MSL
/J .O/
Sand Layer Peizometers Level Indicators
Web ID
TOC
Elevation
MSL'
TOC
Stc WIr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
5.-tc.Z
.. yr
Cpz-1
10.51
7Be9
07.4,
Spz-2
11.21
B 4/6
a 7..<
Cpz-2
10.25
8„39
Q
Spz-3
11.87
6. %�
j . /S
Cpz-3
11.12
�96O
9
d . 78
0,787
Spz-4
11.45
7. /6'
y. 33
CPW
9.65
9. se
.0.ra�%7
Spz-5
11.45
9.36
, w..o 9
MWTF-1A •
14.35
"- Y
/t /3
Spz-6
11.23
9 2/9
/ 77
MWTF-1B •
14.36
a/. 90
9 y/p
Spz-7
11.59
/O. 48
45.1
MWIF-1C •
14.44
9r 9 J 0D
4/, er
Spz-8
11.57
_ - th._6-9-
/
7 ill -
MWIF-2A.
14.05
6 pa
7B3-
Spz-9
11.01
B..�0
,..Q /
MWTF-2B
14.02
// .4/f
459
C.Jy
Spz-10
12.16
.S 6 .
6.S/
MWrF-2C
14.08
/9 574
SPW
9.95
7 7(0
of./9
MWTF-3A
1221
3, f(4
8.3 7
MWTF-3B
12.18
/0 /p
7 99
MWTF-3C
12.19
/a.o 0
-Q, 3/
Sand Layer And Croatan Fonnadon Withdrawal Wells
Web ID
TOC
Elevation
MSL'
Max Stc
Wtr
Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)esl(N)o
Comments
SWW -1
10.70
rLeevel
/. 56
/.56
+1.to+2'
7f5
CWW-1
10.60
7,CS
-/ / 7
-2'to-1'
SWW-2
9.99
6.96
O 96
+1'to+2'
fey
CWW-2
10.23
7 %Q
- / --
-2'to-1'
lei
/�/,
SWW-3
9.97
7S0
/ BO
+1' to+2'
/-3Ls
CWW-3
9.95
74i,
r/Jr0o
-2'to-1'
�`
1/
SWW-4
10.73
7'99
/'99
+1'to+2'
r
CWW-4
1on
7
ol.26
-2'to-V
//j5
SWW-5 .
10.80
goy.
/�'�i
/
+1'to+2'
7,5
!/j
lea#%�i!/6' pJ t•tc)
�"
CWW-5
10.74
6.99
198
-o?, 0/
-2'to-1'
SWW-8
10.66
%</y
/ y4/
+1'' to+2'
fee/el Lam Leo'.
CAWS
0.92
1p, 6�3
-d.7 7
-2'to-1'
J�,(/e
4V5
SWW-7
10.70
'7//0/
/ 0/
+1'to+2'
j/�
CWW-7
9.95
!O 5-a,
-or 4141 -2'to-1'
-en
'on we Sp9ee. 'enf.7.' eiptiyns- /emit/.d 7cV/o// �!!/1llsJ4s4/ /!/�//.S�i
Revised 8/12/97 • Riser length added to TOC elevation 124197 PCS095XLS

PCS Phosphate Co., Inc. - Tank Farm Remediation System Monitoring Fla: 15-03403.02
Date: %//S/99 pc TLe
Time: /2/I2
Tech: 1,(3.t«
System Gauge Prsano',
swW-1
0-39
sww-7
0 -/8
cww-1
D -/S
CWW-7
0 a6
Laval Irtul
Dlt h Laval
y 5 a '
Barge sop
B. 9s'
Water Laval
969
Control Tank
%s la
/4169
Sand Layer Pelzometem Level Indicators
Well ID
TOC
Elevation
MSL•
TOC
Ste Wtr
Level'
,Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Ste WIT
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
W. 7
5 9a
Cpz-1
10.51
7. 4$
a 810
Spz-2
11.21
6.0
0283
Cpz-z
10.25
9 or
0•6'0
ot%.•`/y/
OaZ
Spz-3
11.87
6.4/9
.5.,3Q
Cpz-3
11.12
8 de
Spz-4
11.45
10. 95
4/. 5O
CPW
9.65
9461
Spz-5
11.45
9. 34
a?o 9
MWrF-1A •
14.35
3. 75
/D. /00
Spz-6
11.23 '
9. 3y
/ 89
MWrF-19 •
14.36
• 1:6-4/
9 ea
Spz-7
11.59
/D.Os
/S`/
MWTFAC•
14.44
9.75---f/.69
Spz-8
11.57
6..S 3
SO`%
MWtF-2A
14.05
6. /8
7 B7
Spz-e
11.01
B.4S
02,56
MWIF-2e
14.02
// 414.
& Sip
Spz-10
12.16
.57 44g-
6. 74/
.M1MrF-2C.
14.08
/3. 419'
O•S?
84/4
SPIN
g.os
7. 9a
c?.o3
MWIF.9A '
12.21
3.75
MWTF-38
12.113
/0.30
/ O ]I
MWWF3C
12.19
/a.yY
-to.&c-
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Ste
WIT
_Level Ft.
Max Level
Relative To
MSL FI.
Control
Point
MSL•
Is We/
Pumping
(YIesl(Nio
Carmelite
SWW-1
10.70
7..59
/39
+1•to+2'
.5
CWW-1
1o.so
7rV
-//6
-2'to-1'
S1NW-2
9.99
7 •/a
/ 4/oZ
+1• to+2'
7/3
CYVW2
1021
/,'Glo
-/34
-z•to-l'
7/5
G(Cr
liartrly jn' dblurt.
sww-3
9.97
70a
/. Gan
.r 1'to.
.� o's
-- -.
CMWW-3
9.95
77a
-la
-2'to-l'
/r/,f
Swy 4
10.73
1 01
+1 • to .r
,IrJ
CWW-4
10.73
/7.0:2_
rp.87
-,1.a
-2'to -1'
SwW-5
10.a0
4., 86
0.8�i6C
+1 'to .r
7-1
�J/5
GIMP/410.74
76.5
-/JJ
-2'to-1'
/!
slims
loss
7 as-/
3S
+1'to+r
/101/1
CWWA
9.92
4.{
-/ 98
-2'to-1'
(re.,
SWW-7
10.70
7 2/
/.3/
+1 • to.r
///f
CWW-7
9.95
6.9/'
-2.oy
-2'to-1'
‘615
'
Revised 5112197
• Riser length added to TOC elevation 1124197
PC3095.xIS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER S
May, 1999 — July, 1999 -
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period. Short periods of planned downtime were
experienced for preventative maintenance and inlet DPW Water strainer cleaning. The system was
shutdown two additional times for regular maintenance. On 6/30 the system was shutdown for
approximately five hours to replace a conductivity -sensing probe. On 7/19 the #1 UV Sterilizer was
consistently reading lower than normal intensity. The #2 UV bulb of this Sterilizer was replaced and the
intensity returned to 100%.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
INJECTED WATER TOTALS
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
May-99
390,890
0
390,890
8.8
15.0
Jun-99
406,320
0
406,320
9.4
13.3
Jul-99
478,050
0
478,050
10.7
14.9
TOTALS
1,275,260
0
1,275,260
Withdrawal Well System
The Withdrawal Well System operated the entire period. The withdrawal water well pumps are monitored
daily by the area Maintenance Department and preventative maintenance work is performed is needed.
The total monthly and quarterly withdrawal water volumes for the period are:
WITHDRAWAL WATER TOTALS
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
May-99
484,895
301,580
766,475
17.6
Jun-99
453,269
307,582
760,851
17.6
Jul-99
399,358
319,025
718,383
16.1
1 OTALS
1,337,522
928,18/
2,266,709
3

Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Air Compressor for the Withdrawal Well Pumps
Operation of the air compressor system was normal during most of the period. On 7/1 a valve on the air
dryer malfunctioned causing the compressor to overheat and shutdown. The I&E Maintenance group was
notified to repair the valve. The system was down for approximately 12 hours.
Confined Sand Formation Withdrawal Well (SWW) Pumps
S W W-1: On 6/28 the pump was cleaned with HC1 and returned to service.
SWW-2: On 6/28 the pump was cleaned with HCI and returned to service. On 7/27 the cycle counter
malfunctioned. It was cleaned/repaired and retumed to service.
SWW-3: On 5/20 the pump stopped and was shaken to start. On 6/28 the pump was cleaned with HC1 and
returned to service. On 7/12 the pump stopped and was shaken to start.
SWW-4: On 6/28 the pump stopped due to pluggage. It was replaced with a rebuilt pump. On 7/6 the
cycle counter malfunctioned and was repaired.
SWW-5: No problems.
SWW-6: No problems.
SWW-7: No problems.
Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 6/28 the pump was cleaned with HCI and returned to service.
CWW-2: On 6/28 the pump was cleaned with HCI and returned to service. On 7/20 the pump was replaced
due to a malfunctioning check valve at the bottom of the pump.
CWW-3: On 6/26 the pump stopped and was blowing air due to a malfunctioning cam assembly. It was
cleaned and the pump was placed back in service. On 6/28 the pump was cleaned with HCl and returned to
service.
CWW-4: On 5/28 the pump stopped due to pluggage. It was replaced with a rebuilt pump.
CWW-5: On 7/6 the cycle counter malfunctioned due to an air leak. This was repaired and the pump was
placed back in service.
CWW-6: No problems.
CWW-7: No problems.
4

PCS
PhosphatM AURORA DIVISION
P.O. BOX 48, AURORA, NC 27806
August 23, 1999
Underground Injection Control Program
Division of Water Quality, Groundwater Section
North Carolina DENR
P. O. Box 29578
Raleigh, North Carolina 27626-0578
Attention: Mark Milligan
Subject: Third Quarter Groundwater Monitoring Report
May -July, 1999
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
c-)
.flFps
Please find enclosed, the third quarter Tank Farm Remedial Action System groundwater monitoring report
for 1999. This includes the sampling and reporting requirements of the above referenced permit, Part V,
Section B 1 as well as the reporting requirements of the overall Tank Farm Remedial Action Plan.
Enclosed are: a) Form GW-59 for injection well CIW7 and monitor well MWTFICR (R — This monitor
well is a replacement well. The original well was damaged beyond repair.), b) Form GW-59 for each of
the fourteen withdrawal wells, b) Form GW-59 for monitor wells MWTF1A and MWTFIB, c) Form GW-
59 for the WLCT, d) piezometer level monitoring field sheets, and e) the summary operational and
maintenance report.
On May 13, 1999 PCS submitted a request for approval to reduced water level monitoring from monthly to
quarterly. On August 4, 1999 Mr. Keith Starner of the Washington Regional Office, Groundwater Section
approved this request in a telephone conversation with Mr. Terry L. Baker. This report contains the
monthly water levels, but future reports will have quarterly water level data to coincide with the frequency
of this report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
Terry L. Baker, P.E.
Superintendent, Environmental Affairs
Attachments
pc: Willie Hardison / Keith Starner — DWQ- GWS, WaRO (w/attch)