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HomeMy WebLinkAboutWI0700012_Monitoring (Report)_19980511GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C, 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Depth To Water Level Measuring point is Tank Farm CWW-1 4 inch 7.28 2.25 Water pumped/bailed before sampling Field Analysis: pH 6.3 Date Sample Collected 4/13/98 Laboratory Name Well Depth Sample (Screened) Interval 33.27 PERMIT NUMBER: Permit Type: System: Disposal Type: W10700012 Non Discharge Tank Farm Remedial System Other 55.0 Ft. Ft To 52.68 Ft ft. below measuring point (before Water Level ft. above land surface MSL CONTINUOUS Purge Measurement Specific Conductance 2297 uMhos Temp Date Lab Sample Analyzed 4/13/98 To PCS Phosphate Env. Lab Certification No(s) 330 GALS oC 18.9 4/21/98 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED 3.32 Ft. MSL COD Coliform:MF Fecal Coliform:MF Total N/A N/A N/A Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 1984 6.5 10.8 81.5 N/A N/A N/A N/A 700.3 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/1 mg/I mg/I mg/I uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium N/A N/A 3.430 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A NIA Yes mg/I mg/I mg/I ug/I ug/I ug/I ug/I ug/I ug/I ug/l ug/I ug/I ug/I ug/I ug/I Odor NONE Appearance VERY LT YELLOW Ni - Nickel Ph - Lead Zn - Zinc N/A ug/I N/A ug/I N/A L7 .'1 C:) Pesticides/Herbicides(Specify) N/A '_ iV -< Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC Fri T. .. -; 0.2t4; N/A �g/I N/A ug/I N/A ug/I I CERTIFY THAT THIS R a?ORT IS TRUE AND ACCURATE SIGNATURE OF PERMITTEE R AUTHORIZED AGENT) GW-59 Rev. 8/96 11'/71 Date Note: Values should reflect dissolved and colloidal concentrations. (See #3 on bad() See back for instructions Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or cal[: DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C. 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Tank Farm CWW-2 4 inch Depth To Water Level 7.00 Measuring point is 3.00 Water pumped/bailed before sampling Field Analysis: pH 6.2 Well Depth Sample (Screened) Interval 30.57 ft. below measuring point (before ft. above land surface CONTINUOUS Purge Measurement Specific Conductance 2606 uMhos Temp Date Sample Collected 4/13/98 Date Lab Sample Analyzed 4/13/98 Laboratory Name PCS Phosphate Env. Lab Certification No(s) PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other 52.15 Ft. Ft To 49.82 Water Level 3.23 MSL GALS oC 19.6 To 4/21/98 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Ft. MSL Yes Ft Odor NONE Appearance CLEAR COD Coliform:MF Fecal Coliform:MF Total N/A N/A N/A Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 2236 6.4 12.0 119.1 N/A N/A N/A N/A 759.4 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I mg/I uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium N/A N/A 5.100 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A mg/I mg/I mg/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/l Ni - Nickel Ph - Lead Zn - Zinc Pesticides/Herbicides(Specify) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC NfAij N/At N/A IV N/A 0.20 N/A N/A N/A .ug/l ggf. ram. mg/I ug/I ug/I ug/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERMITTEE(dR AUTHORIZED AGENT) GW-59 Rev 8/96 Date Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) ' See back for instructions '" Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: DIVISION OF WATER QUALITY GROUNDWATER P.O. SOX 29578 RALEIGH, N.C, 27626-0578 (919) 733-3221 ECTION Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Depth To Water Level Tank Farm CWW-3 4 inch 7.99 Measuring point is 3.08 Water pumped/bailed before sampling Field Analysis: pH Date Sample Collected Laboratory Name 6.4 4/13/98 PCS Phosphate Env. Lab Well Depth Sample (Screened) Interval 36.42 ft. below measuring point (before ft. above land surface CONTINUOUS Purge Measurement Specific Conductance 2711 uMhos Temp Date Lab Sample Analyzed 4/13/98 To Certification No(s) 330 PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other 53.00 Ft. Ft To 50.67 Ft Water Level 1.96 MSL GALS oC 26.5 4/21/98 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Ft. MSL Yes Odor NONE Appearance CLEAR COD N/A mg/I Coliform:MF Fecal N/A /100m1 Coliform:MF Total N/A /100m1 Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 2060 6.6 9.9 114.7 N/A N/A N/A N/A 669.7 N/A N/A N/A I CERTIFY THAT THIS REPO SIGNATURE OF PERMI GW-59 Rev. 8/96 EE(OR mg/I units mg/I mg/I mg/I mg/I mg/I mg/I mg/1 uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium S TRUE AND ACCURATE THORIZED AGENT) N/A N/A 6.100 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A mg/I mg/I mg/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I Date Ni - Nickel Ph - Lead Zn - Zinc Pesticides/Herbicides(Specify) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC N/A N/A N/A 0, N/A —< ug/I ug/I I ll 'T1 0.20 rig'(I N/A u6li N/A ug/I N/A ug/I Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) See back for instructions " Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O, BOX 29578 RALEIGH, N,C. 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Tank Farm CWW-4 4 inch Depth To Water Level 6.78 Measuring point is 2.75 Water pumped/bailed before sampling Field Analysis: pH Date Sample Collected Laboratory Name 6.3 4/13/98 Date Lab Sample Analyzed PCS Phosphate Env. Lab Certification No(s) Well Depth Sample (Screened) Interval ft. below measuring point (before ft. above land surface CONTINUOUS Purge Measurement 41.67 Specific Conductance 2695 uMhos Temp 4/13/98 To 330 PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other 53.00 Ft. Ft To 50.92 Ft Water Level MSL GALS oC 28.6 4/21/98 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED 3.95 Ft. MSL COD Coliform:MF Fecal Coliform:MF Total N/A N/A N/A Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 1928 6.6 10.1 120.8 N/A N/A N/A N/A 651.1 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I mg/I uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium N/A N/A 5.500 N/A N/A N/A N/A N/A N/A N/A NIA N/A N/A N/A N/A Yes mg/I mg/I mg/I ug/I ug/I ug/I ug/l ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I Odor NONE Appearance CLEAR Ni - Nickel Ph - Lead Zn - Zinc N/A N/A ) N/A u(, Pesticides/Herbicides(Specify) N/A , .) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC 0.14 N/A N/A N/A ugil ug/( uglt ':11 u mg/I ug/I ug/I ug/I I CERTIFY THAT THIS REPO 'T1S TRUE AND ACCURATE SIGNATURE OF PERMIT EE(OR THORIZED AGENT) GW-59 Rev. 8/96 -11/1/776" Date Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) " See back for instructions Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forrns please write or call: DIVISION OF. WATER QUALITY GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C. 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Depth To Water Level Measuring point is Water pumped/bailed before sampling Field Analysis: pH Date Sample Collected Laboratory Name Tank Farm CWW-5 Well Depth 4 inch Sample (Screened) Interval 41.75 7.76 ft. below measuring point (before 2.58 ft. above land surface CONTINUOUS Purge Measurement 6.4 Specific Conductance 2253 uMhos Temp 4/13/98 Date Lab Sample Analyzed 4/13/98 To PCS Phosphate Env. Lab Certification No(s) 330 PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other 53.17 Ft. Ft To 51.08 Ft Water Level MSL GALS oC 31.3 4/21/98 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED COD N/A Coliform:MF Fecal N/A Coliform:MF Total N/A Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 1488 7.1 8.8 108.4 N/A N/A N/A N/A 419.6 N/A N/A N/A I CERTIFY THAT THIS REPORT 2.98 Ft. MSL Odor NONE Yes Appearance LT YELLOW mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/1 mg/I mg/I mg/I uMHos mg/I mg/I NO2 As N N/A mg/I NO3 as N N/A mg/I Phosphorous: Total as P 9.050 mg/I Al - Aluminum N/A ug/I Ba - Barium N/A ug/I Ca - Calcium N/A ug/I Cd - Cadmium N/A ug/I Chromium: Total N/A ug/I Cu - Copper N/A ug/I Fe - Iron N/A ug/I Hg - Mercury N/A ug/I K - Potassium N/A ug/I Mg - Magnesium N/A ug/I Mn - Manganese N/A ug/I Sodium N/A ug/I TRUE AND ACCURATE SIGNATURE OF PERMITTEE(OR AUTHORIZED AGENT) GW-59 Rev. 8/96 Date Ni - Nickel Ph - Lead Zn - Zinc N/A N/A N/A t 3 Pesticides/Herbicides(Specify) N/A - .v Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC 0.15 N/A N/A N/A ugll ugSl ugjl • rn _1 S ,) my/b ug/I ug/I ug/I Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) " See back for instructions "" Submit blue and yellow copies only to address ab ove GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Tank Farm Well ID Number CWW-6 Well Diameter 4 inch Depth To Water Level 6.85 Measuring point is 2.92 Water pumped/bailed before sampling Field Analysis: pH 6.8 Date Sample Collected Laboratory Name Well Depth Sample (Screened) Interval 36.62 ft. below measuring point (before ft. above land surface CONTINUOUS Purge Measurement Specific Conductance 1677 uMhos Temp 4/13/98 Date Lab Sample Analyzed 4/13/98 To PCS Phosphate Env. Lab Certification No(s) 330 53.00 Water Level MSL GALS oC 28.8 4/21/98 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED DIVISION OF WATER QUALITY -GROUNDWATER SECTION P.O. F30X 29578 RALEIGH, N.C. 27626-0578 (919) 733-3221 PERMIT NUMBER: Permit Type: System: Disposal Type: W10700012 Non_Discharge Tank Farm Remedial System Other Ft. Ft To 50.88 3.07 Ft. MSL Yes Ft Odor NONE Appearance LT RST BROWN COD Coliform:MF Fecal Coliform:MF Total Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N N/A mg/I NO2 As N N/A mg/I N/A /100m1 NO3 as N N/A mg/I N/A /100m1 Phosphorous: Total as P 3.250 mg/I Al - Aluminum N/A ug/I 1068 mg/I Ba - Barium N/A ug/I 7.1 units Ca - Calcium N/A ug/I 8.6 mg/I Cd - Cadmium N/A ug/I 117.6 mg/I Chromium: Total N/A ug/I N/A mg/I Cu - Copper N/A ug/I NIA mg/I Fe - Iron N/A ug/I N/A mg/I Hg - Mercury N/A ug/I N/A mg/I K - Potassium N/A ug/I 220.0 mg/l Mg - Magnesium N/A ug/I N/A uMHos Mn - Manganese N/A ug/I N/A mg/I Sodium N/A ug/I N/A mg/I Ni - Nickel Ph - Lead Zn - Zinc Pesticides/Herbicides(Specify) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC I CERTIFY THAT THIS REPe�-T IS TRUE AND ACCURATE SIGNATURE OF PERMITTEE(O GW-59 Rev. 8/96 AUTHORIZED AGENT) Date N/A ug/I N/A ug/I N/A :fig/I LJ7 N/A-4 f iJ _girt • • T) 0.26 rng/I c-) N/A ug/I N/A ug/I N/A ug/I Note: Values should reflect dissolve• d and colloidal concentrations. (See #3 on bade) * See back for instructions Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or calk DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.G. 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Depth To Water Level Measuring point is Tank Farm CWW-7 4 inch 7.07 1.25 Water pumped/bailed before sampling Field Analysis: pH 6.6 Date Sample Collected 4/13/98 Well Depth Sample (Screened) Interval 36.58 ft. below measuring point (before ft. above land surface CONTINUOUS Purge Measurement Specific Conductance 1278 uMhos Temp Date Lab Sample Analyzed 4/13/98 To PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other 53.00 Ft. Ft To 50.83 Ft Water Level 2.88 MSL GALS oC 24.5 4/21/98 Ft. MSL Laboratory Name PCS Phosphate Env. Lab Certification No(s) 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Yes COD Coliform:MF Fecal Coliform:MF Total Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N I CERTIFY THAT THIS R N/A mg/I NO2 As N N/A mg/I N/A /100m1 NO3 as N N/A mg/I N/A /100m1 Phosphorous: Total as P 5.250 mg/I Al - Aluminum N/A ug/I 924 mg/I Ba - Barium N/A ug/I 7.0 units Ca - Calcium N/A ug/I 8.2 mg/I Cd - Cadmium N/A ug/I 89.2 mg/I Chromium: Total N/A ug/I N/A mg/I Cu - Copper N/A ug/I N/A mg/I Fe - Iron N/A ug/I N/A mg/l Hg - Mercury N/A ug/I N/A mg/I K - Potassium N/A ug/I 186.8 mg/I Mg - Magnesium N/A ug/I N/A uMHos Mn - Manganese N/A ug/I N/A mg/I Sodium N/A ug/I N/A mg/I TRUE AND ACCURATE .'*2) SIGNATURE OF PERMITTEE(OR & JTHORIZED AGENT) GW-59 Rev. 8/96 iq Date Odor NONE Ni - Nickel Ph - Lead Zn - Zinc Appearance LT RST BROWN Pesticides/Herbicides(Specify) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC N/A ug/I N/A ug/I N/A ue/I 0a N/A 3 0.18 -- rYt /1 N/A ug/l N/A ug/I N/A ug/I Note: Values should reflect dissolved and colloidal concentrations. (See #3 on bads) See back for instructions ** Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C. 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Depth To Water Level Measuring point is Tank Farm SWW-1 4 inch 6.49 1.52 Water pumped/bailed before sampling Field Analysis: pH 6.0 Date Sample Collected 4/13/98 Laboratory Name PCS Phosphate Env. Lab Certification No(s) Well Depth Sample (Screened) Interval 18.3 ft. below measuring point (before ft. above land surface CONTINUOUS Purge Measurement Specific Conductance 2408 uMhos Temp Date Lab Sample Analyzed 4/13/98 To 330 PERMIT NUMBER: Permit Type: System: Disposal Type: W10700012 Non Discharge Tank Farm Remedial System Other 22.5 Ft Water Level MSL GALS oC 17.8 4/21/98 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED 4.21 COD Coliform:MF Fecal Coliform:MF Total N/A N/A N/A Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 1908 6.0 12.2 93.3 N/A N/A N/A NIA 798.0 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I mg/I uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium N/A N/A 158.500 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Ft. To 21.12 Ft. MSL Yes mg/l mg/I mg/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I Ft Odor NONE Appearance CLEAR Ni - Nickel Ph - Lead Zn - Zinc NIA N/A N/A pry Pesticides/Herbicides(Specify) N/A .- r ) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC ug/I ug/I ug/I -3 rr1 0.45 : mg/l N/A" ug>4fi NIA , ,yg/I N/A : ug/l I CERTIFY THAT THIS REPOT,`)S TRUE AND ACCURATE SIGNATURE OF PERMITTEE(OR T HORIZED AGENT) GW-59 Rev. 8/96 Date Note: Values should reflect dissolved and colloidal concentrations. (See #3 on bade) " See back for instructions "" Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF WATER QUALITY - GROUNDWATER SECTION For additional forms please write or call: P.O. BOX 29578 RALEIGH, N.C. 27626-0578 (919) 733-3221 Facility Name Address: Well Location Well ID Number Well Diameter PCS PHOSPHATE CO., INC - Aurora Division P.O. Box 48 AURORA, N.C. 27806 County Beaufort Tank Farm SWW-2 4 inch Depth To Water Level 7.75 Measuring point is 3.42 Water pumped/bailed before sampling Field Analysis: pH 6.3 Date Sample Collected 4/13/98 Laboratory Name PCS Phosphate Env. Lab Well Depth Sample (Screened) Interval ft. below measuring point (before ft. above land surface CONTINUOUS Purge Measurement Specific Conductance 2184 uMhos Temp Date Lab Sample Analyzed 4/13/98 To Certification No(s) 330 PERMIT NUMBER: Permit Type: System: Disposal Type: W10700012 Non Discharge Tank Farm Remedial System Other 23.0 Ft. 18.8 Ft To 21.63 Ft Water Level 2.24 Ft. MSL MSL GALS oC 18.6 4/21/98 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED COD Coliform:MF Fecal Coliform:MF Total Odor NONE Yes Appearance CLEAR N/A N/A N/A Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 1592 6.6 10.4 68.9 N/A N/A N/A N/A 655.2 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I mg/I uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium N/A N/A 58.000 N/A N/A N/A N/A N/A N/A N/A N/A N/A NIA NIA N/A mg/I mg/1 mg/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I Ni - Nickel Ph - Lead Zn - Zinc N/A N/A N/A i_! C:O Pesticides/Herbicides(Specify) NIA t iV Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC 0.19L± N/A r. N/A N/A ug/I ug/I 49/I ,7i • rT1 rTj mg/I r", t dc�+l ug/l ug/I I CERTIFY THAT THIS REPO TRUE AND ACCURATE SIGNATURE OF PPPERMI7"(•EE(OR i JTHORIZED AGENT) GW-59 Rev. 8/96 Date Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) • See back for instructions • Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional foams please write or call: DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C. 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Depth To Water Level Measuring point is Tank Farm SWW-3 Well Depth 4 inch Sample (Screened) Interval 5.70 ft. below measuring point (before 3.17 ft. above land surface Water pumped/bailed before sampling Field Analysis: pH 6.0 Specific Conductance 1756 uMhos Temp Date Sample Collected 4/13/98 Date Lab Sample Analyzed 4/13/98 Laboratory Name PCS Phosphate Env. Lab Certification No(s) 20.17 24.5 Ft. Ft To Water Level 4.27 MSL CONTINUOUS Purge Measurement GALS oC 23.8 To 4/21/98 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED COD Coliform:MF Fecal Coliform:MF Total N/A N/A NIA Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 1184 6.4 8.4 45.4 N/A N/A NIA N/A 498.8 N/A N/A N/A I CERTIFY THAT THIS REPORT mg/1 /100m1 /100m1 mg/I mg/I mg/1 mg/I uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium E AND ACCURATE SIGNATURE OF PERMITTEE(OR AUTIi4RIZED AGENT) GW-59 Rev. 8/96 N/A NIA 83.500 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other 23 Ft Ft. MSL Odor NONE Yes mg/I mg/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I Date Appearance CLEAR Ni - Nickel Ph - Lead Zn - Zinc Pesticides/Herbicides(Specify) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC N/A N/A � NJAO r^,� N/A ,J 0.10 N/A N/A N/A ug/I ru/I �,'tg re ug/I ug/I ug/I Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) L See back for instructions * Submit blue and yellow copies only to address bove GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Depth To Water Level 7.91 Measuring point is 3.42 Water pumped/bailed before sampling Field Analysis: pH 6.0 Tank Farm SWW-4 Well Depth 4 inch Sample (Screened) Interval 20.5 ft. below measuring point (before ft. above land surface CONTINUOUS Purge Measurement Specific Conductance 2487 uMhos Temp Date Sample Collected 4/13/98 Date Lab Sample Analyzed 4/13/98 Laboratory Name PCS Phosphate Env. Lab Certification DIVISION OF WATER QUALITY GROUNDWATER SEC P,O. BOX 29578 RALEIGH, N.C. 27626-0578 (919) 733.3221 25.0 ION PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other Ft. Ft To 23.3 Water Level MSL GALS oC 32.9 To 4/21/98 No(s) 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED 2.82 Ft. MSL COD Coliform:MF Fecal Coliform:MF Total N/A N/A N/A Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 1536 6.3 9.3 68.1 N/A N/A N/A N/A 632.5 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I mg/I uMHos mg/i mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium N/A N/A 109.000 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Yes mg/I mg/I mgll ug/I ug/I ug/I ug/I ug/I ug/I ug/l ug/I ug/I ug/I ug/I ug/I Ft Odor NONE Appearance CLEAR Ni - Nickel Ph - Lead Zn - Zinc Pesticides/Herbicides(Specify) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC N/A N/A N/A <: j 2. N/A ug/I u/1 uw/I '` 0.09 m /( N/A ug/I N/A ug/I N/A ug/I I CERTIFY THAT THIS REPOT IS,T lkE AND ACCURATE SIGNATURE OF PERMITTEE(c R AUTHIZED AGENT) GW-59 Rev. 8/96 1,--/fibe Date Note: Values should reflect dissolved and colloidal concentrations. (See #3 on bade) * See back for instructions "" Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C. 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Depth To Water Level Measuring point is Tank Farm SWW-5 4 inch 6.68 2.96 Well Depth Sample (Screened) Interval ft. below measuring point (before ft. above land surface 24.83 28.21 Ft Water Level 4.12 MSL Water pumped/bailed before sampling CONTINUOUS Purge Measurement Field Analysis: pH 6.2 Specific Conductance 2362 uMhos Temp Date Sample Collected 4/13/98 Date Lab Sample Analyzed 4/13/98 To Laboratory Name PCS Phosphate Env. Lab Certification No(s) 330 GALS oC 29.4 4/21/98 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED PERMIT NUMBER: Permit Type: System: Disposal Type: W10700012 Non Discharge Tank Farm Remedial System Other Ft. To 24.83 Ft. MSL Yes Ft Odor NONE Appearance CLEAR COD Coliform:MF Fecal Coliform:MF Total N/A N/A N/A Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 1492 6.5 11.2 83.5 N/A N/A N/A N/A 610.8 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I mg/I uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium N/A mg/I N/A mg/I 44.000 mg/I N/A ug/I NIA ug/I N/A ug/I NIA ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I Ni - Nickel Ph - Lead Zn - Zinc Pesticides/Herbicides(Specify) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC N/A N/A1 N/A CI) -r NIA ' 0.28 N/A N/A NIA cgg/l 4/1 rt rr -:r (.;) rn mg/I ug/I ug/I ug/I I CERTIFY THAT THIS REPO TRUE AND ACCURATE SIGNATURE OF PERMITTEE(OR A GW-59 Rev. 8/96 THORIZED AGENT) "—////c4 Date Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) See back for instructions " Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C. 27626-0578 For additional forms (919) 733-3221 please write or call: Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Tank Farm Well ID Number SWW-6 Well Depth 26.00 Ft. Well Diameter 4 inch Sample (Screened) Interval 22.25 Ft To 24.62 Depth To Water Level 7.29 ft. below measuring point (before Water Level 3.37 Ft. MSL Measuring point is 2.58 ft. above land surface MSL Water pumped/bailed before sampling CONTINUOUS Purge Measurement GALS Field Analysis: pH 6.2 Specific Conductance 2085 uMhos Temp oC 32.2 Date Sample Collected 4/13/98 Date Lab Sample Analyzed 4/13/98 To 4/21/98 Laboratory Name PCS Phosphate Env. Lab Certification No(s) 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Yes PERMIT NUMBER: WI0700012 Permit Type: Non Discharge System: Tank Farm Remedial System Disposal Type: Other Ft Odor NONE Appearance CLEAR Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N COD N/A mg/I NO2 As N N/A mg/I Coliform:MF Fecal N/A /100m1 NO3 as N N/A mg/I Coliform:MF Total N/A /100m1 Phosphorous: Total as P 31.000 mg/I Note: Use MPN method for highly turbid samples Al - Aluminum N/A ugll 1336 mg/I Ba - Barium N/A ug/I 6.5 units Ca - Calcium N/A ug/I 11.5 mg/I Cd - Cadmium N/A ug/I 117.1 mg/I Chromium: Total N/A ug/I N/A mg/I Cu - Copper N/A ug/I N/A mg/I Fe - Iron N/A ug/I N/A mg/I Hg - Mercury N/A ug/I N/A mg/I K - Potassium N/A ug/I 343.1 mg/I Mg - Magnesium N/A ug/I N/A uMHos Mn - Manganese N/A ug/I N/A mg/I Sodium N/A ug/I N/A mg/1 Ni - Nickel N/A Ph - Lead N/A Zn - Zinc N/A r'3 Pesticides/Herbicides(Specify) N/A •3 111 r71 n Other FLUORIDE 0.07 mg/t Other MIBK N/A ugll Other Ag - Silver N/A ug/I Other Se - Selenium N/A ugll ug/I ug/l �g(I VOC I CERTIFY THAT THIS REPOR I . TRUE AND ACCURATE 41 (q2 SIGNATURE OF PERMITTEE(OR AOTHORIZED AGENT) Date GW-59 Rev. 8/96 Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) LSee back for instructions ubmit blue and yellow copies only to address ve GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C. 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Well ID Number Well Diameter Depth To Water Level Measuring point is Tank Farm SWW-7 Well Depth 4 inch Sample (Screened) Interval 7.31 ft. below measuring point (before 3.00 ft. above land surface Water pumped/bailed before sampling Field Analysis: pH 5.8 Specific Conductance 1503 uMhos Temp Date Sample Collected 4/13/98 Date Lab Sample Analyzed 4/13/98 Laboratory Name PCS Phosphate Env. Lab Certification No(s) PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other 29.50 Ft. 25.17 Ft To 27.50 Ft Water Level 3.39 Ft. MSL MSL CONTINUOUS Purge Measurement GALS oC 27.0 To 4/21/98 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED COD Coliform:MF Fecal Coliform:MF Total N/A N/A N/A Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 1132 6.0 15.4 111.6 N/A N/A N/A N/A 304.7 N/A N/A N/A I CERTIFY THAT THIS REPO mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I mg/I uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium TRUE AND ACCURATE SIGNATURE OF PERMITTEE(OR AIfl HORIZED AGENT) GW-59 Rev. 8/96 N/A N/A 78.000 N/A N/A N/A N/A N/A N/A N/A N/A NIA N/A N/A N/A Yes mg/I mg/I mg/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I 411 icd Date Odor NONE Appearance CLEAR Ni - Nickel Ph - Lead Zn - Zinc Pesticides/Herbicides(Specify) Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC N/A ug/I N/A ug/I N/A rug/I n •�� ,..j N/A • rTi C ,o 0.11 . h1 /I I N/A N/A ug/I N/A ug/I • ug11 Note: Values should reflect dissolved and colloidal concentrations. (See #3 on bade) See back for instructions " Submit blue and yellow copies only to address above Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C.27626-0578 For additional fors (919) 733-3221 please write or call: Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort PERMIT NUMBER: W10700012 Permit Type: Non Discharge System: Tank Farm Remedial System Disposal Type: Other Well Location Tank Farm Well ID Number MWTF1-A Well Depth 6.40 Ft, Well Diameter 2 inch Sample (Screened) Interval 3.40 Ft To 5.40 Ft Depth To Water Level 3.38 ft. below measuring point (before Water Level 10.97 Ft. MSL Measuring point is 3.86 ft. above land surface MSL Water pumped/bailed before sampling 2100 Purge Measurement MLS Field Analysis: pH 7.3 Specific Conductance 508 uMhos Temp oC 18.4 Odor NONE Appearance LT YELLOW Date Sample Collected 4/14/98 Date Lab Sample Analyzed 4/14/98 To 4/21/98 Laboratory Name PCS Phosphate Env. Lab Certification No(s) 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Yes COD N/A mg/I NO2 As N N/A mg/I Ni - Nickel N/A ug/I Coliform:MF Fecal N/A /100m1 NO3 as N N/A mg/I Ph - Lead N/A ug/I Coliform:MF Total N/A /l00ml Phosphorous: Total as P 0.510 mg/1 Zn -Zinc N/A ug/I Note: Use MPN method for highly turbid samples Al - Aluminum N/A ug/I 352 mg/I Ba - Barium N/A ug/I In 7.5 units Ca - Calcium N/A ug/I Pesticides/Herbicides(Specify) N/A ') , _ 4.9 mg/I Cd - Cadmium N/A ug/I tt 13.3 mg/I Chromium: Total N/A ug/I - r N/A mg/I Cu - Copper N/A ug/I t J < N/A mg/I Fe - Iron NIA ug/l N/A mg/I Hg - Mercury N/A ug/I Other FLUORIDE 2.12 - . MO N/A mg/I K - Potassium N/A ug/I Other MIBK N/A " u /P.) <10.0 mg/I Mg - Magnesium N/A ug/I Other Ag - Silver N/A — lI N/A uMHos Mn - Manganese N/A ug/I Other Se - Selenium N/A ug/I N/A mg/I Sodium N/A ug/I VOC N/A mg/I I CERTIFY THAT THIS REPORTRUE AND ACCURATE \sl SIGNATURE OF PERMITTEE(OR AUTHORIZED AGENT) GW-59 Rev. 8/96 d»Ive Date Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) See back for instructions ** Submit blue and yellow copies only to address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, N.C. 27626-0578 For additional forms (919) 733-3221 please write or call: Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other Well Location Tank Farm Well ID Number MWTF1-B Well Depth 13.50 Ft. Well Diameter 2 inch Sample (Screened) Interval 10.60 Ft To 12.60 Depth To Water Level 4.29 ft. below measuring point (before Water Level 10.07 Ft. MSL Measuring point is 3.86 ft. above land surface MSL Water pumped/bailed before sampling 2600 Purge Measurement MLS Field Analysis: pH 5.8 Specific Conductance 593 uMhos Temp oC 19.5 Odor NONE Appearance CLEAR Date Sample Collected 4/14/98 Date Lab Sample Analyzed 4/14/98 To 4/21/98 Laboratory Name PCS Phosphate Env. Lab Certification No(s) 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Yes Ft COD NIA mg/I NO2 As N N/A mg/I Ni - Nickel N/A ug/I Coliform:MF Fecal N/A /100m1 NO3 as N N/A mg/I Ph - Lead N/A ug/I Coliform:MF Total N/A /100m1 Phosphorous: Total as P 8.800 mg/I Zn - Zinc N/A qb/I Note: Use MPN method for highly turbid samples Al - Aluminum N/A ug/I i 1_7 Dissolved Solids: Total 428 mg/I Ba - Barium N/A ug/I : pH (when analyzed) 6.0 units Ca - Calcium N/A ug/I Pesticides/Herbicides(Specify) N/A < TOC 4.9 mg/I Cd - Cadmium N/A ug/I f'J -,1-ii Chloride 93.2 mg/I Chromium: Total N/A ug/I -., Arsenic N/A mg/I Cu - Copper NIA ug/I _ Grease and Oils N/A mg/I Fe - Iron N/A ug/I .c- vn Hardness: Total N/A mg/I Hg - Mercury NIA ug/l Other FLUORIDE 0.25.• r11/I Phenol N/A mg/I K - Potassium N/A ug/I Other MIBK N/A ug/I Sulfate 61.5 mg/I Mg - Magnesium N/A ug/I Other Ag - Silver N/A ug/I Specific Conductance N/A uMHos Mn - Manganese NIA ug/I Other Se - Selenium NIA ug/I Total Ammonia(NH4+NH3) N/A mg/I Sodium N/A ug/I VOC TKN as N N/A mg/I I CERTIFY THAT THIS REPORT I 1TUE AND ACCURATE SIGNATURE OF PERMITTEE(OR AU I ORIZED AGENT) Date GW-59 Rev. 8/96 Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) * See back for instructions ** Submit blue and yellow copies only to address above Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF WATER QUALITY - GROUNDWATER SECTION P,O; BOX 29578 RALEIGH, N.C. 27626-0578 For additional fortes �'� (91 9) 733-3221�;; please write or call: Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other Well Location Tank Farm Well ID Number MWTF1-C Well Depth 42.00 Ft. Well Diameter 2 inch Sample (Screened) Interval 38.70 Ft To 40.70 Ft Depth To Water Level 7.30 ft. below measuring point (before Water Level 7.14 Ft. MSL Measuring point is 3.95 ft. above land surface MSL Water pumped/bailed before sampling 2100 Purge Measurement MLS Field Analysis: pH 7.5 Specific Conductance 497 uMhos Temp oC 19.5 Odor NONE Appearance CLEAR Date Sample Collected 4/14/98 Date Lab Sample Analyzed 4/14/98 To 4/21/98 Laboratory Name PCS Phosphate Env. Lab Certification No(s) 330 10 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Yes COD N/A mg/I NO2 As N N/A mg/I Ni - Nickel N/A ug/I Coliform:MF Fecal N/A /100m1 NO3 as N N/A mg/I Ph - Lead N/A ug/I Coliform:MF Total <1.0 /100m1 Phosphorous: Total as P 0.210 mg/I Zn - Zinc N/A ug/I Note: Use MPN method for highly turbid samples Al -Aluminum N/A ug/I r 384 mgll Ba -Barium N/A ug/I o0 . 7.6 units Ca - Calcium N/A ug/I Pesticides/Herbicides(Specify) N/k2..; `=;_ i r1 4.1 mg/I Cd - Cadmium <1.0 ug/I ___� :=� rr 12.9 mg/I Chromium: Total <5.0 ug/I N.) - �` r'tl N/A mg/I Cu Copper N/A ug/I :"- Tr NIA mg/1 Fe Iron NIA ug/I . J —. m N/A mg/I Hg - Mercury N/A ug/I Other FLUORIDE 0.56 " m6lta .s:' c N/A mg/I K - Potassium N/A ug/I Other MIBK N/A dc671 18.5 mg/I Mg - Magnesium N/A ug/I Other Ag - Silver N/A tig/I N/A uMHos Mn - Manganese 73.0 ug/I Other Se - Selenium N/A ug/I N/A mg/I Sodium N/A ug/I VOC N/A mg/I I CERTIFY THAT THIS REPORT l;.S TRUE AND ACCURATE SIGNATURE OF PERMITTEE(OR AHORIZED AGENT) Date GW-59 Rev. 8/96 Note: Values should reflect dissolved and colloidal concentrations. (See #3 on bade) * See back for instructions ** Submit blue and yellow copies onlyto address above GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: DIVISION OF WATER QUALITY - GROUNDWATER SECTION: P.O. BOX 29578 RALEIGH,N.C, 27626-0578 (919) 733-3221 Facility Name PCS PHOSPHATE CO., INC - Aurora Division Address: P.O. Box 48 AURORA, N.C. 27806 County Beaufort Well Location Tank Farm Well ID Number WLCT Well Diameter N/A Depth To Water Level N/A Measuring point is N/A Water pumped/bailed before sampling Field Analysis: pH Date Sample Collected Laboratory Name 7.6 4/14/98 Date Lab Sample Analyzed 4/14/98 PCS Phosphate Env. Lab Certification No(s) 330 Well Depth Sample (Screened) Interval N/A ft. below measuring point (before ft. above land surface CONTINUOUS Purge Measurement Specific Conductance 471 uMhos Temp N/A Ft. Ft To Water Level MSL GALS oC 18.2 To 4/21/98 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED 10 Ft. MSL Yes PERMIT NUMBER: Permit Type: System: Disposal Type: WI0700012 Non Discharge Tank Farm Remedial System Other Ft Odor NONE Appearance CLEAR COD Coliform:MF Fecal Coliform:MF Total N/A N/A <1.0 Note: Use MPN method for highly turbid samples Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH4+NH3) TKN as N 312 7.8 4.6 9.7 N/A N/A N/A N/A <10.0 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I mg/I uMHos mg/I mg/I NO2 As N NO3 as N Phosphorous: Total as Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Sodium N/A mg/I N/A mg/I P 0.025 mg/I N/A ug/l N/A ug/l N/A ug/I <1.0 ug/I <5.0 ug/1 N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I <10.0 ug/I N/A ug/I Ni - Nickel Ph - Lead Zn - Zinc N/A N/A N/A Pesticides/Herbicides(Specify) N/A iJ Other FLUORIDE Other MIBK Other Ag - Silver Other Se - Selenium VOC 0.69— N/A N/A N/A ug/I ug/I :11 rri moll Ug/I ug/I ug/I I CERTIFY THAT THIS REPORT,I TRUE AND ACCURATE SIGNATURE OF PERMITTEE(OR AUHHORIZED AGENT) GW-59 Rev. 8/96 Date Note: Values should reflect dissolved and colloidal concentrations. (See #3 on back) * See back for instructions ** Submit blue and yellow copies only to address above MY S/('. leve/5 X27-98 77/o; PCS Phosphate Co., Inc. - Tank Farm Remediation System Monitoring Date: 2-13- 9 8 Time: gin Tech: Le System Gauge Pressures SHW-1 O- 3o n swwa //- /4; CW W-1 ios 44 ..n/73,• CWW-7 ///-.?3,as : File:15-03-003-02 pc TLB Level (msl Ditch Level Jam. /O' Barge Slip B 2.2 Water Level 9 90 f Control Tank ,/ 771 % a MSL /y Sand Layer Pelzometers Level Indicators Well ID TOC Elevation MSL' TOC Ste Wtr Level' Level Relative To MSL Ft. Well ID TOC Elevation MSL' TOC Ste WV Level' Level Relative To MSL Ft. Spz-1 10.47 J2 /p./ ' Cpz-1 10.51 a, 83 .168 Spz-2 , 11.21 7 5 Z 3. G 9 Cpz-2 1025 9. gle D // . Spz-3 11.87 Sy/p //,!%/ Cpz-3 11.12 7, 9r[ fir Spz-4 11.45 (o,/,Z 5..33 CPW 9.65 8.73 0.92 Spz-5 11.45 8 62 2, 93 MWTF-1A- 14.35 2, 8/a //, 99 Spz-6 11.23 ' B,rg X. 9.5 MWIF-1B• 14.36 3♦ l4. /0.70 Spz-7 11.59 /Q, ,O'/ /.Spr MWTF-1C• 14.44 a, 90 /..S'/ Spz-8 11.57 _ o. 2 _ SO7_ _ _MWTF-2A 14.05 AQt 7 97 Spz-9 11.01 7 90 .3 // MWFF-2B 14.02 /t, 7S 1.27 Spz-10 12.16 7. 60 735 0 MWTF-2C 14.08 /pfp, ijf / G5- SPW 9.95 '7:34/ 26 / MWFF-3A 1221 .3, d'O B.9/ MWTF-3B 12.18 9.66 ce..5.2 MWTF-3C 12.19 //. ...cal Q 63 Sand Layer And Croatan Formation Withdrawal Wells Well ID TOC Elevation MSL' Max Ste Wtr Level Ft. Max Level Relative To MSL Ft. Control Point MSL' Is Well Pumping (ylea/(Mo Comments SWW-1 10.70 l,L/2 872 +1 • to+2' %ii CWW-1 lose '7 ,7 -/ 93 -2'to-1' S4 �/ ,�! fa',947 AP a1/['q. SW W-2 9.99 7 y3 /. VS +1 • to +2' 4 CWW-2 10.23 ,2p7, /% * -7'90 -2'to1 -0' Y��/ n /hffedie/lerLt%//G. ,4d77/77 /e dir/. W SW-3 9.97 7. 74' / 7 +1'tc+2' rJ['l. CWW-3 925 //, 38 2 $8 -2't0-V /' 4 Avel /l:r47e ,�/J'aw9 ( SWW-4 10.73 9, 57 / ,�// +1• to +2' 9 / �- CWW-4 10.73 a, 98 7..o.2 -2'to -1' TO 4' SAW-5 10.80 0 /, a6 +1'to+2' }"Qh / /ea/ L.'it. Alai. CWW-5 10.74 /p 95~ :2.tS -2'to-1'r[ 4 SWW-6 10.08 7 /f ///p +1 'to+2' f�/(j CWW-0 gin 340 -/. 41 -2'to-1' f (j // fri+.7l�Jny JEo d: /e/7. SWW-7 10.70 7 .23 /23 +1'to+2' IU4 CW W-7 9.95 6, '72 -fig -2 • to -1' / P4 *,C«e/s S to .2' 7- 98/ Revised 8/12/97 • Riser length addea ._ . _.. -.unseen 124/97 O% ar 4 Date: Time: Tech: PCS Phosphate Co., Inc. - Tank Farm Remediation System Monitoring 3-//- 19B System Gauge Pressures SWW-1 Q-2• SWW-7 /8,ao %. .•/4, `3 CWW-1 D-.e/a 1-i, CWW-7 5 0 -a72vs: File:15-03-003-02 pa TLB Ditch Level ,;oly Barge Slip 9, 00 Water Level 91/ G --_ Control Tank %. MSL p' /j6S' 7 Sand Layer Peizometers Level Indicators Well ID TOC Elevation MSL' TOC Ste Wtr Level' Level Relative To MSL Ft. Well ID TOC Elevation MSL' TOC Ste WV Level' Level Relative To MSL Ft. Spz-1 10.47 7478 6, / 9 Cpz-1 10.51 a 90 ,. 14/ / 0/ Spz-2 11.21 R. /9 3 tl 7 Cpz-2 10.25 9?4/ Spz-3 .11.87 G.06 56/ Cpz-3 11.12 Spz4 11.45 4 612 -1<D.7 CPW 9.65 8l/Z /0.3 Spz-5 11.45 B. 9f' 2 1/7 MWTF-1A • 14.35 5. /Q, 99 Spz-6 11.23 ' B.6B 2//3,,s MWrF-,B• 14.36 S6 7•.7Y 7,,5,5 - /D.C2 9y09 Spz-7 11.59 /0./6p /Y/ MWTF-1C• 14.44 _ _ _Spz-8__ 11 57 4. /0--•�i 7 �/ -MWTF-2A 14.05 &to S5 Spz-9 11.01 8 289 MWTF-2B 14.02 N./0 /, J. 9,2 Spz-10 12.16 "/�4, .5 75 b.%3 MWTF-2C 14.08 /A/4, 0.92 SPW 9.95 7%pZ _ A.33 MWrF-3A 1221 :f 9 ' J8.3/ „e,,79 4e„Qi MWTF-3B 12.18 9 en MWTF-3C 12.19 //. 9/ Sand Layer And Croatan Formation Withdrawal Wells Well ID TOC Elevation MSL' Max Ste 9 Wh Level Ft. Max Level Relative To MSL Ft. Control Point MSL' Is Well Pumping (Y)es/(N)o Comments W SW-1 10.70 6J+. 4/7 8 4/7�/ 7 +1'to«2' e Cww, 10.60 G•�� -iZ,Gy 2'to-1' 4S ire Awn £mo:t.at0fl ni%/ swW-2 9.99 /_.4/9 +1'to+2' / )ej CWW-2 10.23 �7y7 /./0 -/t'y -2'to-1' ve_j Sww-3 9.97 9/ / 9/l +1 ' m «2• h D /um�/n9 /0 &/c•/r CWW-3 9.95 ��'%yy 7q O3q -/ $7 -2'to-1' �j/P T 5 ... SWW4 10.73 7 7 / a9 +1.to+2' re5 CWW4 10.73 708 -/, 9j -2•to-1' SWW-5 10.80 %yry / i .9 +1 ' to+2' iV/ei 7 e% CWW-5 10.74 7, 93 -/ 07 ' -2 'to-1' yes »e 4 sww� 10.66 ?ryy /, ?9 «1'ta+2 �ei .Cove/4s ,l/oaf "/ut//eelle«1,C:i7e/, CWW-0 9.92 r7.. /.a/ /73 -2'to-,' ��g 19.95 ' d9:J D,1re fare Cww-7 7 02 / 98 -2' to 1' v on ,/%,3^/l 10 _1 1 -. Revised 8/12/97 • Riser length added to TOC elevation 1/24/97 PCS095XLS File: 15-03-003-02 pa TLB v. • ..v�tIIIa L6 vVy un.. - I clin I Mill InCIIICVIaLIVII cySLC11i iVIUIIILVIIfly Date: 4/- - q8 Time: Tech: System Gauge Presaures s-1 9-a 9AS.' SW W-7 e -,S/os,' cWW-1 e-ye`s S -4's ,di,' cww-7 Level (mei Ditch Level .T /o q ' Barge slip 9 7'.9' Wafer Level 961, 4 � Control Tank %MSL " DIPS Sand Layer Pelzometers Level Indicators Well ID TOC . Elevation MSL' TOC Ste Wtr LLevel' Level Relative To MSL FL Well ID TOC Elevation MSL' TOC Ste Wtr Level' Level Relative To MSL Ft. Spz-1 10.47 7••.90? I .,& Cpz-1 10.51 7078 .J.Z_' Spz-2 11.21 8. /S .f04' Cpz-2 10.25 9 63 6.12 Ogg Spz-3 11.87 e.o7'y 5r0.5 Cpx-3 11.12 .7 741 Spzi 11.45 6..5-61 ,i 87 CPW 9.85 8.8.2 I. tee Spz-5 11.45 B81 160 / MWFF-1A• 14.35 Jae J D. /97 Spz-8 11.23 ' 9.Oe of/3- MWrF-18• 14.38 4 all /Q 07 Spz-7 11.59 /et t0-01 /no MWTF-1C• 14.44 7220 t.fe17 tarsi 7/9' 9✓,/V Spz-8 11.57 o./B SinMWFF-2A 14.05 Spz-9 11.01 _ G'''J . 00 S. IM ME-2B 14.02 Spz-10 12.18 5: 07 70 9 MWTF-2C 14.08 /,'J.c4 act. SPW 9.95 Z3.Z . 63 MWrF-3A 1221 y.l'V 9,G0 797 or- sea MWIF-3B 12.18 MWTF-3C 12.19 /�. OD a/9 Sand Layer And Croatan Formation Withdrawal Wells Well ID TOC Elevation MSL' Max Ste Wtr Level FI. Max Level Relative To MSL Ft. Control Point MSL' Is Well Pumping (Y)esr(N)o Comments SWW--1 10.70 G.'99 0 419 +1'to+2' 14-9 c -1 10.80 7.18 '/• 72. -2'to-1' SWW-2 9.99 7 73- /.'73- +1 ' to+2' �Ye, //G9 ...-. CWW-2 1023 700 '0Z00 -2'to -1' �1 fes SwW-3 9.97 670 -&3O +1'to+2' CWW-3 9.95 2 99 -/ O/ -2'to-1' 1✓,Qy rc3 SWW-4 10.73 79/ / 9/ +1'to+2' rGs CVWV-4 10.73 1p,%8 ..?,Z -2'to -1' IVe-j '- SWW-5 10.80 /.6e8 e G8 +1'to+2' CVVW-5 10.74 77l' -/.iy -2'to-l' IY/e9 SWW-8 10.68 9a9 /i 9 +1' to+2' YQ�3 CWW-8 9.92 Jigs ^o%/s -2'to-1' V IB SVVW-7 10.70 7$/ //8/ +1'ta+2' Ye5 CWW-7 9.95 7D7 /r 9_5 -2'to-1' r e3 q / .'1rvtlir,9J-Jac „Lei. Revised 8l12/97 • Riser length added to TOC elevation 1/24)97 PCS095.XLS PCS \\\ Phosphate memo Date May 6, 1998 To L. M. Montgomery Location From T. L. Baker Location Subject TANK FARM REMEDIAL ACTION PLAN QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR FEBRUARY, 1998 - APRIL, 1998 The attached subject report, with required operational and maintenance data, is provided for submittal to the DEHNR- Ground Water Section, Underground Injection Control Program. This report should be submitted along with the laboratory sampling and water level monitoring data. If you have any questions concerning this information, please contact me. T. L. Baker, Superintendent Operations Environmental Attachment pc: W. K. Thornton S. A. Beckle/W. H. Paulson/G. Coghill Randy Allen Tommy Lewis T. W. Davis/OE-00-01-00-08 C:\Mydata\OEDept\TFRAP\OPDATA998.doc 1 PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR THE INJECTION AND WITHDRAWAL WATER WELLS FEBRUARY, 1998 - APRIL 1998 The Tank Farm Remediation System consists of a series of seven injection water wells located on the south side of the Tank Farm Area and a series of fourteen (14) water withdrawal wells located on the north side of the Tank Farm Area. Injection Water Well System The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light (ASF/UV) disinfection system throughout the period. Short periods of planned downtime were experienced for preventative maintenance and inlet DPW Water strainer cleaning. Daily operational data are collected by the Shipping Department and reported to the Operations Environmental Department. The total monthly and quarterly volumes of water injected as well as the month end water level in the Water Level Control Tank are: INJECTED WATER TOTALS; 2 1998 DPW WATER GALLONS •CONDENSATE GALLONS TOTAL-- GALLONS AVERAGE--- GPM TANK LEVEL FEET, MSL Feb 564,680 0 564,680 14.0 14.8 Mar 614,010 0 614,010 13.8 14.8 Apr 605,080 0 605,080 14.0 14.7 TOTALS 1,783,770 0 1,783,770 Withdrawal Well System The Withdrawal Well System operated the entire peri withdrawal water well pumps are monitored daily by Maintenance Department and preventative maintenance performed is needed. The total monthly and withdrawal water volumes for the period are: od. The the area work is quarterly WITHDRAWAL WATER. TOTALS - 1998 SAND FORMATION GALLONS CROATAN FORMATION GALLONS TOTAL GALLONS AVERAGE GPM Feb 477,373 355,806 833,179 20.7 Mar 492,195 274,453 766,648 17.2 Apr 451,636 273,720 725,356 _ 16.8 TOTALS 1,421,204 903,979 2,325,183 Some additional short periods of planned downtime for preventative maintenance, -pipe header cleaning, and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these activities are: Confined Sand Formation Withdrawal Wells (SWW) SWW-1; On 2/9/98 it was determined that the pump and well were scaled up. The system was cleaned with HC1 and placed back in operation. On 4/1 a leaking airline was found and repaired. SWW-2; On 2/12-17 mechanical problems were experienced. On 2/17 the internal float & cam assembly were replaced, the system was cleaned with HC1 and placed back in operation. SWW-3; On 2/23, 3/2, 4/1 and 4/15 the pump stopped and had to be shaken to start. On 3/23 the pump stopped and the air filter regulator was found plugged. This was repaired and the system was placed back in operation. SWW-4; On 2/3 the pump stopped and had to be shaken to start. On 2/18 the pump stopped and it was determined that the pump cam assembly magnet had deteriorated. On 2/19 the cam was replaced, the system was cleaned with HC1. On 2/20 it was place back in operation. On 2/23 the pump totalizer indicator was replaced with a new type. SWW-5; On 3/16-17 the pump experienced mechanical problems. The system was cleaned with HC1 and the cam assembly hook was found broken. This was repaired and the pump was placed back in operation on 3/17. On 4/7 the pump stopped and the discharge line was found plugged. This was cleaned and the system was placed back in operation. SWW-6; On 2/23-3/6 the pump experienced mechanical problems. On 3/3 the pump inlet check valve was found to be leaking and the cam assembly & float were replaced. The pump was cleaned with HC1 and placed back in operation but still was not working normally. On 3/6 the system was cleaned again and the SS float was replace with an original epoxy type float and the system began normal operation. SWW-7; Normal operation with no problems. 3 Croatan Formation Withdrawal Wells (CWW) CWW-1; On 2/19 the pum; stopped and had to be shaken to start. On 3/6-11 the pump experienced mechanical problems. On 3/7 it was cleaned with HC1. On 3/10 the pump vent valve was adjusted. On 3/11 the pump SS float was replaced with an epoxy float and the system began operating normally. CWW-2; Normal operation with no problems. CWW-3; On 2/23 the pump stopped. and it was determined to be scaled up. On 2/24-25 the pump float & air check valve were replaced, the system was cleaned with HC1 and placed back in operation. CWW-4; On 3/30-31 the system was determined to be scaled up, was cleaned with HC1 and placed back in operation. CWW-5; Normal operation with no problems. CWW-6i On 2/6-9 problems were encountered with the pump totalizer indicator and it was replaced on 2/9. On 2/12 mechanical problems were experienced. The pump float was replaced, the system was cleaned with HC1 and placed back in operation. On 2/25-3/2 the pump experienced mechanical problems. The pump float rod connection to the cam assembly -was reversed—and—the—pump—sta-r-ted—pumping- normally ._ On 3-/20_ the pump stopped and had to be shaken to start. On 4/14-15 the pump stopped and the air filter regulator was found plugged. This was repaired and the system placed back in operation. CWW-7; On 2/12-13 mechanical problems were experienced. On 2/13 the pump cam assembly was replaced, the system was cleaned with HC1 and placed back in operation. On 2/18 the pump stopped and it was determined that the air filter regulator was plugged and holes were found in the pump. These were repaired and the system was placed back in operation. On 2/23 and 3/7 the totalizer malfunctioned, was adjusted and returned to operation. On 3/10 the pump stopped and the air filter regulator was found plugged. This was repaired and the system placed back in operation. 4 PCS Phosphate AURORA DIVISION P.O. BOX 48, AURORA, NC 27806 May 8,1998 Underground Injection Control Program Division of Water Quality, Groundwater Section North Carolina DENR P. O. Box 29578 Raleigh, North Carolina 27626-0578 Attention of Mark Milligan Subject Second Quarterly Groundwater Monitoring Report for 1998 Injection Well Permit #WI0700012 PCS Phosphate Co., Inc. Tank Farm Remedial Action System Beaufort Co. Dear Mark: 0 Please find enclosed, the 2m Quarterly Tank Farm Remedial Action System groundwater monitoring report-for-1998,rper-the-requirements-of-the-above. referenced. _permit Additional _ Compliance Monitoring Report Forms for well CIW-7 and the WLCT are included in this report along with the monthly piezometer level monitoring field sheets and a summary performance report of the individual wells. Month In'ected (: al) Withdrawn (• al) February March April 564,680 614,010 605,080 833,179 766,648 725,356 Totals 1,783,770 2,325,183 Please contact me at (919) 322-8193 if you have any questions regarding this information. Sincerely, Leon M. Montgomery Environmental Engineer Attachments pc: Willie Hardison - DWQ WaRO (w/attch)