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HomeMy WebLinkAboutWI0600055_Monitoring (Report)_20100201ACOM Environment Prepared for: Abbott Laboratories Abbott Park, II Prepared by: AECOM Raleigh, NC 60135880.400 February 2010 Progress Report for 3rd and 4t" Quarters 2009: Groundwater Monitoring and Annual Remediation Effectiveness Evaluation Former Abbott Facility Solvent Release Remediation NCDENR ID No. NCD-000-0040 Laurinburg, Scotland County, North Carolina /"' coftll Environment Prepared for: Abbott Laboratories Abbott Park, II Prepared by: AECOM Raleigh, INC 60136880.400 February 2010 Progress Report for 3rd and 4t" Quarters 2009: Groundwater Monitoring and Annual Remediation Effectiveness Evaluation Former Abbott Facility Solvent Release Remediation NCDENR ID No. NCD-000-0040 Laurinburg, Scotland County, North Carolina Prepared gy Matt Allen, P.G. Senior Project Geologist Reviewed By S. Grant Watkins, P.G., RSM Senior Program Manager $14 1035 AECOM Environment i Contents 1.0 Introduction...................................................................................................................... 1-1 1.1 Site Description and Background........................................................................................1-1 1.2 Regulatory Status and Remedial Investigations.................................................................1-1 1.2.1 Historical Remedial Actions..................................................................................1-2 1.3 RAP Groundwater Monitoring Programs............................................................................1-3 2.0 Groundwater Sampling Methods.................................................................................. 2-1 2.1 Groundwater Monitoring Program Summary ......................................................................2-1 2.2 Sampling Procedures..........................................................................................................2-1 2.2.1 Decontamination and Containment Procedures..................................................2-2 2.2.2 Quality Control/Quality Assurance Procedures...................................................2-2 2.3 Free Phase Product Measurements...................................................................................2-2 3.0 Sampling Results............................................................................................................ 3-1 3.1 Groundwater Flow and Hydrology.......................................................................................3-1 3.2 Groundwater VOC Analytical Results.................................................................................3-1 3.2.1 Extent and Distribution of VOCs in Groundwater................................................3-1 3.2.2 Trends in VOC Concentrations............................................................................3-2 3.3 Groundwater Geochemistry ................................................................................................3-2 3.3.1 pH..........................................................................................................................3-3 3.3.2 Dissolved Oxygen.................................................................................................3-3 3.3.3 Oxidation -Reduction Potential..............................................................................3-3 3.3.4 Ferrous Iron...........................................................................................................3-3 3.3.5 Methane-Ethane-Ethene......................................................................................3-3 3.3.6 Alkalinity................................................................................................................3-4 3.3.7 Total Organic Carbon...........................................................................................3-4 3.4 Groundwater Microbial Results...........................................................................................3-4 3.5 Free Phase Product Inspection...........................................................................................3-5 4.0 Remediation Effectiveness Evaluation......................................................................... 4-1 4.1 VOC Degradation Trends....................................................................................................4-1 4.1.1 Tricholorethene and Daughter Compounds........................................................4-1 4.1.2 Methylene Chloride...............................................................................................4-2 4.1.3 Freon 113..............................................................................................................4-2 4.2 TOC Availability...................................................................................................................4-2 60135880 February 2010 AECOM Environment 4.3 Microbial Profiles..................................................................................................................4-3 4.3.1 Summary of Biodegradation Potential.................................................................4-4 5.0 Conclusions.....................................................................................................................5-1 6.0 References....................................................................................................................... 6-1 60135880 February 2010 AECOM Environment List of Appendices Appendix A Semi -Annual Groundwater Sampling Records Appendix B Laboratory Analytical Reports (November 2009 Groundwater Samples) Appendix C Historical VOC Analytical Results at Solvent Plume Wells (Table C.1) Appendix D TCE and cis-1,2-DCE Trend Plots for Selected Wells Appendix E Historical Cumulative Trend Plots for TCE, cis-1,2-DCE, Freon 113 and Methylene Chloride List of Tables Table 1-1 Monitoring Well Construction Details Table 1-2 Summary of Groundwater Sampling Program: November 2009 Table 2-1 Groundwater Level Gauging and Elevation Data: November 2009 Table 2-2 Geochemical Parameters in Monitoring Wells: November 2009 Table 2-3 Volatile Organic Compound Analytical Results in Groundwater: November 2009 Table 3-1 Dehalogenating Bacteria Analytical Results: December 2009 Table 3-2 Historical Free Phase Product Observations List of Figures Figure 1-1 Figure 1-2 Figure 3-1 Figure 3-2 Figure 3-3 Figure 3-4 Site Location Map Site Plan Shallow Groundwater Potentiometric Surface Map: November 2009 Deep Groundwater Potentiometric Surface Map: November 2009 TCE in Groundwater: Shallow Aquifer Zone November 2009 TCE in Groundwater: Deep Aquifer Zone November 2009 60135880 February 2010 AECOM Environment 1-1 1.0 Introduction This Progress Report is for the 3rd and 4th quarters 2009 and presents the results of the November 2009 semi-annual groundwater monitoring event and the findings of the annual remediation effectiveness evaluation conducted by AECOM North Carolina, Inc. (AECOM) on behalf of Abbott Laboratories (Abbott) at the Former Abbott Laboratories facility located at 16000 Joy Street in Laurinburg, Scotland County, North Carolina (the "Site"). The Site is located at the intersection of NC Highway 15-501 and NC Highway 401 in Laurinburg. Figure 1-1 shows the Site location on a regional topographic map. Figure 1-2 is a Site plan that shows the Site property boundaries, Site features (including groundwater monitoring wells), and boundaries of surrounding properties. The November 2009 semi-annual groundwater sampling activities summarized in this report were performed as part of a groundwater monitoring program that supports the ongoing Phase II in -situ bioremediation program being conducted by Abbott under an approved Remedial Action Plan (RAP) Addendum. The comprehensive groundwater monitoring event performed by Abbott in November 2009 included the sampling and analysis of groundwater from 23 (twenty-three) of the 26 (twenty-six) existing Site monitoring wells using to monitor the solvent plume. 1.1 Site Description and Background The Former Abbott facility is located on approximately 51 acres of land at the northeast intersection of U.S. Highway 401 and U.S. Highway 15-501 in Laurinburg, Scotland County, North Carolina. The property is currently developed with a main plant building, parking lots, adjacent warehouse and several smaller support buildings. The facility was constructed by Abbott on agricultural land in 1969 (Radian, 1993). Figure 1-2 shows a site plan with locations of existing monitoring wells and other Site features. Beginning in 1970, Abbott used the facility to manufacture medical support devices for their Hospital Products Division. Medical devices manufactured at the facility included polyvinyl chloride (PVC) tubing and adapters that were used for intravenous drug administration and health maintenance equipment. The manufacturing process included injection molding of PVC and other plastics, parts washing, parts assembly, packaging, and ethylene oxide sterilization. Chemicals used in the manufacturing process included cyclohexanone, methyl ethyl ketone (MEK); toluene; acetone; 1,1,2- trichloro-1,2,2-trifluoroethane (Freon 113); phthalates; and various chlorinated volatile organic compounds (CVOCs) such as trichloroethene (TCE) and methylene chloride (Radian, 1993). Abbott donated the Site property and facility to Scotland County in 2002 and ceased manufacturing operations that same year. Scotland County then transferred the facility to its current property owner Marketta, LLC. QualPak, a business division of GOJO, Inc., is the current tenant and operator of the Site facility. QualPak uses the facility to manufacture and package Purell° brand alcohol -based hand sanitizer products. Since Abbott's departure from the Site, additional infrastructure has been added to the facility to support QualPak's operations. 1.2 Regulatory Status and Remedial Investigations During their ownership of the Laurinburg facility, Abbott operated a solvent evaporation pit at the Site from 1970 through 1976. Solvents including TCE were disposed of in the pit. Abbott informed the 60135880 February 2010 AECOM Environment 1-2 North Carolina Department of Environment and Natural Resources (NCDENR)-Division of Waste Management (DWM) Superfund Section of the existence of the solvent disposal pit in 1989 and subsequently began to investigate Site soil and groundwater quality. Contaminants detected in soil and groundwater around the pit included TCE, acetone, MEK, methylene chloride, toluene, 1, 2- dichloroethene (DCE), Freon 113, 1,1,1-trichloroethane (TCA), and bis-(2-ethylhexyl) phthalate (Radian, 1993). In 1991 Abbott entered into an Administrative Order on Consent (AOC) with the NCDENR. The AOC required Abbott to complete a remedial investigation (RI), develop a Remedial Action Plan (RAP) for meeting site soil and groundwater cleanup criteria, and implement the RAP. Abbott conducted the RI process from 1989-1992 and submitted the RI report to NCDENR in August 1993. The RI conducted at the Site identified groundwater impacted with volatile organic compounds (VOCs) extending from the solvent pit area to the downgradient (i.e., southern) portion of the facility. Concentrations of dissolved TCE and other VOCs indicated the presence residual dense non - aqueous phase liquid (DNAPL) in the aquifer. A DNAPL layer consisting of TCE and methylene chloride was found at a depth of 18 feet bgs during the initial RI work. A layer of floating light non - aqueous phase liquid (LNAPL) was also observed in one well downgradient of the source area during past phases of investigations. Soils impacted by VOCs were identified in an area surrounding the former evaporation waste pit (Radian, 1993). 1.2.1 Historical Remedial Actions Abbott has developed and implemented several phases of site remediation and cleanup strategies that have been ongoing since 1994. Several different technologies have been applied to remediate soils and groundwater during this period. Plans and results of the historical remedial actions are described in past reports submitted to the NCDENR. Results are also summarized in the Work Plan for Supplemental Subsurface Investigation and Remedial Actions (AECOM, 2009). The major phases of remedial actions and their results are summarized in the following sections. Remedial Action Plan 0994 Radian Corporation developed an initial RAP and submitted the Remedial Action Plan report to NCDENR in August 1994. The RAP specified use of an innovative in -situ mixing and volatilization tool (i.e. the MecToolTM) for the pit source area soil and shallow groundwater, combined with two-phase vacuum extraction (TPVE) technology for the shallow groundwater plume and conventional groundwater extraction and treatment for the deeper groundwater plume. Implementation of the initial RAP occurred as follows: • The MecToolTM in -situ mixing/volatilization process was used at the waste pit source area from August 1995 to January 1996. • The south yard groundwater recovery system was installed and began operating in November 1993 and operated until 2006. • The north yard groundwater recovery system began operations in August 1996. The shallow TPVE component of the north yard recovery system was shut down in 1999 and the deeper groundwater recovery wells were shut down in October 2002. (Phoenix, 2007). 60135880 February 2010 AECOM Environment 1-3 Abbott also began separate free product removal efforts at wells MW-10OA and MW-101A using a mobile multi -phase extraction (MMPE) system. Free product removal with MMPE occurred in 2004 (two events) and again in 2006. Remedial Action Plan Amendment (2002) Matrix Environmental Southeast, Inc. (Matrix), on behalf of Abbott, submitted a Remedial Action Plan Amendment report to NCDENR in June 2002. The RAP Amendment proposed an alternate groundwater treatment approach using in -situ anaerobic bioremediation via reductive dechlorination processes. The RAP Amendment also proposed to discontinue groundwater extraction and treatment in the north yard source area, and to continue operating the south yard groundwater extraction system. Hydrogen Release Compound° (HRC°) was identified in the RAP Amendment as the organic substrate selected for the bioremediation program (Matrix, 2002). Implementation of the RAP Amendment occurred as follows: • Phase I of the HRC° injections began in November 2002 with 133 injection borings in and around the solvent waste pit source area (Matrix, 2008). • Phase 11 of the bioremediation program was subsequently conducted in June 2004 by injecting Hydrogen Release Compound -Extended Release (HRC-XTm an extended release, longer lasting version of HRC°) at 123 locations in the northern end of the dissolved VOC plume. Additional injections of HRC-XTM were also performed in the waste pit source area. • In September 2006 the south yard groundwater pumping system was shut down and was replaced by an HRC° in -situ biological treatment system. During this injection event, HRC° was injected at 73 locations in the southern plume area. This part of the remedial action was referred to as the Phase II Supplemental bioremediation program (Matrix, 2008). Remedial Acton Plan Amendment No. 2 (2008) In April 2008, Phoenix Environmental Associates, Inc. (Phoenix) submitted the Remedial Action Plan Amendment 2: Solvent Release Remediation report to NCDENR on behalf of Abbott. The RAP Amendment 2 report provided a summary of the effectiveness of the ongoing bioremediation program, contaminant fate and transport modeling analysis of the remaining TCE plume, and a modified plan for continued bioremediation and monitored natural attenuation (MNA) of VOCs in groundwater. As a result of these evaluations, MNA was selected as the preferred technology to treat VOC- impacted groundwater. The preferred MNA alternative in RAP Amendment 2 included a contingency remedy that specifies additional HRC°enhanced bioremediation should the progress of the MNA remediation deviate significantly from the plume model predictions (Phoenix, 2008). This remedial action contingency allows additional engineered bioremediation to be initiated on an as -needed basis. 1.3 RAP Groundwater Monitoring Programs Two semi-annual groundwater monitoring events are currently performed per year in accordance with the approved sampling plan in the Phase 11 Preconstruction Report Addendum (Phoenix, 2006) and as modified in the RAP Amendment 2 (Phoenix, 2008). The RAP Amendment 2 sampling plan specifies that groundwater samples will be analyzed on a semi semi-annual basis for volatile organic compounds (VOCs) and for Total Organic Carbon (TOC). Once per year, during the April sampling event, the additional parameters of methane/ethane/ethene gases, metabolic acids, and alkalinity are monitored in groundwater at select wells. 60135880 February 2010 AECOM Environment 1-4 Figure 1-2 presents the location of the existing Abbott monitoring well network. Groundwater sampling is conducted at twenty-three of these wells to fulfill the amended RAP requirements and to demonstrate the progress of historical and ongoing corrective actions for the former waste pit solvent release plume. An additional three monitoring wells are currently used only for water level gauging but are not sampled for water quality analyses as specified under the RAP Amendment 2 sampling plan. Table 1-1 lists the twenty-six existing solvent plume monitoring wells and summarizes their well construction information. It is noted that well MW-27D is abandoned and was not accessible. The November 2009 sampling event represents the third semi-annual groundwater sampling event that has occurred since submittal of the RAP Amendment 2. During the November 2009 sampling event, alkalinity and methane/ethane/ethene gases were analyzed at six wells to further evaluate the current bioremediation processes and effectiveness. Table 1-2 summarizes the semi-annual groundwater monitoring program sampling and analysis plan for the November 2009 event. In addition to the routine RAP semi-annual groundwater monitoring event, a supplemental site assessment was also conducted at the site in November through December 2009. Groundwater from three existing site monitoring wells (MW-10013, MW-101A, and MW-102C) and two direct push technology (DPT) borings (GW09N-10 and GW09N-12) was sampled in December 2009 and analyzed by Census assays for Dehalococcoides spp. (DHC) and Dehalobacter spp. (DHB) dehalorespiring bacteria as a component of the supplemental investigation. Results of the DHC and DHB analyses of groundwater from these wells and DPT borings are presented herein due to their potential relevance to the effectiveness of the ongoing bioremediation remedy for groundwater. 60135880 February 2010 AECOM Environment 2-1 2.0 Groundwater Sampling Methods The following section describes the sampling methods used during the semi-annual groundwater monitoring event conducted in November 2009. A summary of the November 2009 sampling and monitoring program is provided in Table 1-2. Groundwater sampling results are discussed in Section 3.0 and are summarized in Table 2-1, Table 2-2, and Table 2-3. 2.1 Groundwater Monitoring Program Summary The Second 2009 (3rd and 4tb Quarters 2009) semi-annual groundwater monitoring event was conducted on November 3-5, 2009 by AECOM. Groundwater was sampled at twenty-three of the twenty-six active solvent plume Site monitoring wells. Each of the samples was analyzed for VOCs by EPA Method 8260B and for TOC by EPA Method SM5310B. In addition to the analyses specified in the RAP sampling plan, a select set of samples were analyzed for methane, ethane, and ethene by EPA Method RSK-175 and for alkalinity by EPA Method SM232013. A library search for Tentatively Identified Compounds (TICs) was also performed on seven of the source area wells (Table 1-2). The VOC analyses were performed by Abbott Laboratories, a North Carolina certified analytical laboratory based in Abbott Park, Illinois. All other analyses were performed by Pace Analytical Laboratories, Inc., (Pace) a North Carolina certified analytical laboratory based in Huntersville, North Carolina. Groundwater levels were gauged at each of the twenty-six active Site solvent plume wells during the first day of groundwater monitoring (November 3, 2009). Table 2-1 summarizes the depth to water measurements and groundwater elevations in Site monitoring wells. The field water quality (geochemical) indicator parameters of temperature, pH, specific conductance, dissolved oxygen (DO), oxidation-reduction potential (ORP), and turbidity were measured in each well during the purging process. Table 2-2 summarizes these measurements. Table 2-2 also summarizes the geochemical parameters of ferrous iron, TOC, and alkalinity, and the dissolved gases carbon dioxide, methane, ethane, and ethene that were analyzed on select groundwater samples. Ferrous iron and carbon dioxide concentrations were analyzed in the field using a HACH° portable field colorimeter test kit. The remaining geochemical analyses for TOC, alkalinity and methane/ethene/ethane were conducted at the Pace laboratory. The field generated sample collection records are included in Appendix A. The laboratory analytical reports are presented in Appendix B. 2.2 Sampling Procedures Groundwater sampling procedures were performed in accordance with the U.S. Environmental Protection Agency (USEPA) Region IV Science and Ecosystem Support Division Field Branches Quality System and Technical Procedures protocols. These general protocols and the sampling program from the RAP Addendum 2 were followed. Each well was purged and sampled using low -flow techniques. A peristaltic pump and new polyethylene tubing were used to purge and sample each well. The wells were considered sufficiently purged when measurements of groundwater temperature, pH, specific conductance, DO, and ORP were stable and the turbidity was below 10 Nephelometric Turbidity Units (NTUs) (or when the well 60135880 February 2010 AECOM Environment 2-2 was pumped dry due to inadequate recharge). For this sampling event, field parameters were considered stable if consecutive measurements were within 10% of the previous well volume measurements. Groundwater samples were collected in a sequence from locations with the lowest to highest VOC concentrations, as determined from past analytical data. A groundwater sample collection record was prepared for each well sampled. Sampling records are included in Appendix A of this report. Sample containers were labeled in the field and a chain -of -custody form was completed. Samples were stored on ice in laboratory supplied coolers pending delivery to Abbott Laboratories and Pace. 2.2.1 Decontamination and Containment Procedures Non -disposable sampling equipment was thoroughly decontaminated with a dilute, phosphate -free soap/water solution prior to fieldwork and between monitoring wells to prevent cross -contamination. Decontamination water and water generated during the purging of monitoring wells were temporarily contained in 5-gallon buckets and transferred to 55-gallon drums, which were appropriately labeled and staged on -Site pending analysis for subsequent disposal. 2.2.2 Quality Control/Quality Assurance Procedures Field sampling activities were documented on individual groundwater sampling records and in a field log book. The samples collected on November 3-5, 2009 were appropriately labeled, stored in sample containers on ice, and delivered to Abbott Laboratories and Pace in good condition and properly preserved. Abbott Laboratories processed the VOC samples and reported the results under lab project number 301917. Pace Analytical Laboratories processed the remaining samples and reported the results under lab project number 9257024. A trip blank (TB-0023) was submitted with the cooler containing VOCs. Blind field duplicates (DUP-1 and DUP-2) were collected for primary sample MW-10B and MW-103C, respectively, and analyzed for VOCs by EPA Method 8260B for quality assurance and field precision. Additionally, two equipment blanks (EB-1 and EB-2) were collected using deionized water and were analyzed for VOCs. Water quality meters were calibrated in the field each day before collecting samples. 2.3 Free Phase Product Measurements A free phase product inspection of six monitoring wells (MW-100A, MW-100B, MW-101A, MW-101 B, MW-102A, and MW-102B) was conducted during the November 2009 sampling event in accordance with the Free Phase Inspection Plan. An electronic oil -water interface probe was used to gauge the liquid levels and presence of free phase product in each of the six designated wells. The interface probe was used to determine if a floating layer of NAPL product was present at the groundwater surface in each well, and then the probe was lowered through the water column to the bottom of the well to determine if a sinking NAPL layer was present. AECOM noted upon opening well MW-101A that it contained an oil absorbent sock, which was removed prior to gauging and sampling the well. In December 2009, during the supplemental groundwater investigation, the potential presence of separate phase product was again checked at well MW-101A using a clear, Teflon bailer. The bailer was first lowered into the well to the groundwater interface and was then retrieved to visually inspect for a separate, oily phase product layer. Subsequently, the bailer was then lowered to the bottom of the well and lowered up and down to collect a liquid sample from the bottom of the well. Results of the free phase product inspection are included in Section 3.5. 60135880 February 2010 AECOM Environment 3-1 3.0 Sampling Results 3.1 Groundwater Flow and Hydrology Water level measurements collected on November 3, 2009 are listed in Table 2-1. Groundwater potentiometric elevations and equipotential contours for the shallow aquifer unit on that date are presented in Figure 3-1. This map indicates that in November 2009, shallow groundwater flow in the upper 30 feet of the water table aquifer was predominantly toward the south-southeast. This groundwater flow map primarily represents data from the shallow "A" labeled monitoring wells. Figure 3-2 shows a potentiometric map that represents groundwater levels in wells screened in the deeper aquifer zones, at depths greater than 30 feet bgs but less than 78 feet bgs. These data include the "B", "C" and "M labeled monitoring wells. Groundwater in these deeper zones flows predominantly toward the south, with radial flow patterns also toward the southeast and the southwest. Based on groundwater elevations measured on November 3, 2009 downward vertical gradients were present at the majority of the multilevel well clusters. 3.2 Groundwater VOC Analytical Results Groundwater samples were collected from twenty-three Site monitoring wells on November 3-5, 2009. Analytical results for this sampling event are summarized in Table 2-2 and Table 2-3. The laboratory analytical report is included as Appendix B. 3.2.1 Extent and Distribution of VOCs in Groundwater Groundwater analytical results for VOCs were compared with the current 15A NCAC 2L Groundwater Standards (revised standards effective January 1, 2010). The following fourteen compounds were detected in groundwater: trichloroethene (TCE), 1,1-dichloroethene (DCE) cis-1,2-DCE, trans-1,2- DCE, vinyl chloride (VC), 1,1,1-trichloroethane (1,1,1-TCA), 1,1-dichloroethane (1,1-DCA), 1,2-DCA, chloroform, methyl ethyl ketone (MEK), methyl tert butyl ether (MTBE), methylene chloride, toluene, and trichlorotrifluoroethane (Freon 113) as listed in Table 2-3. Historic concentrations of target VOCs in groundwater are tabulated in Appendix C. TCE was detected at concentrations above its 2L Groundwater Standard of 3.0 micrograms per liter (pg/L) in groundwater samples collected from thirteen wells sampled during this event (Table 2-3). Concentrations of TCE in groundwater collected from shallow "A" wells screened <30 feet bgs are shown on Figure 3-3 as a TCE isoconcentration plume map. This map illustrates that the shallow TCE plume in groundwater migrates approximately 750 feet south from the waste pit source area and does not extend off -site at detectable concentrations. The shallow TCE plume dimensions have not changed significantly in the past few years. TCE concentrations in groundwater collected from intermediate and deep wells (>30 feet bgs) are shown on Figure 3-4. The deeper TCE plume migrates south from the waste pit source area, in the general direction of deep groundwater flow, and then appears to turn toward the southwest on the southern portion of the Site property. The apparent non -linear shape of the deep plume migration pathway may have several causes, including subsurface lithologic features and preferential flow paths. Current interpretations of the deeper TCE plume dimension are likely influenced by the 60135880 February 2010 AECOM Environment 3-2 screened intervals of the existing deeper wells. The actual distribution of the deeper TCE plume may have a more complex pattern within distinct lithologic strata than is depicted in Figure 3-5. Current data from well MW-18D confirms that TCE has migrated off -site in groundwater to the south but the concentrations are below the 2L Groundwater Standard. The TCE biodegradation daughter products cis-1,2-DCE and vinyl chloride were also detected in groundwater samples above their respective 2L Groundwater Standards. The compound 1,1-DCE was detected above the 2L limit in groundwater at eleven wells. 1,1-DCE is formed by either halorespiration (biological dechlorination) of TCE or by abiotic degradation of trichloroethane (TCA). During the November 2009 sampling event, the following additional VOCs were detected at concentrations above their respective 2L Groundwater Standard in the listed wells: • Toluene: MW-100A, MW-100B, MW-101A, and MW-101B. • Methylene chloride: MW-100A and MW-10013. • MEK: MW-100B. • 1,1,1-TCA: MW-100A, MW-100B, MW-101A, and MW-101B. • 1,2-DCA: MW-104A. The VOCs 1,1-DCA, chloroform, MTBE, trans-1,2-DCE, and Freon 113 were detected above the laboratory detection limits at one or more wells, but the concentrations were below their respective 2L Groundwater Standards. Additionally, the compound cyclohexanone was identified as a TIC in well MW-10013 at an estimated concentration of 1.2 milligrams per liter (mg/L). No other VOC compounds were detected in groundwater samples collected during the November 2009 sampling event. 3.2.2 Trends in VOC Concentrations In comparison with the previous April 2009 sampling event, TCE concentrations in November 2009 decreased in the majority of the on -Site monitoring wells. The laboratory results from November 2009 indicate a slight increase in TCE concentrations at monitoring wells MW-100A, MW-101A, MW-102A, MW-102B, MW-103A, and MW-104C, since April 2009. Overall, TCE concentrations in site monitoring wells have decreased since monitoring began in June of 1993. The historical concentrations of all the VOCs detected in site groundwater are included in the tables provided in Appendix C. Appendix D depicts graphs of TCE and cis-1,2-DCE concentrations over time in selected monitoring wells since September 2002. These graphs represent the TCE reduction trends observed during the time period that enhanced anaerobic bioremediation has been used as a remedy for groundwater remediation. 3.3 Groundwater Geochemistry Field parameters, including temperature, DO, pH, conductivity, oxidation-reduction potential (ORP), and turbidity were recorded during the November 2009 sampling event. Field measurements of ferrous iron and carbon dioxide were also collected using HACH° field test kits. Laboratory analyses of total organic carbon (TOC), methane/ethene/ethane, and alkalinity were also performed on various groundwater samples. Geochemistry parameters are presented in Table 2-2 and discussed below. 60135880 February 2010 AECOM Environment 3-3 3.3.1 pH Field measurements of groundwater pH were collected from monitoring wells during the November 2009 sampling event, which ranged from 4.08 standard units (SU) in MW-16B to 11.40 SU in MW- 16D. A pH value between 5.0 and 9.0 is generally conducive to biologically enhanced reductive dechlorination. The pH values observed at the site appear to be on the low end of the optimal range for optimal reductive dechlorination of target constituents. 3.3.2 Dissolved Oxygen Reductive dechlorination requires an anaerobic environment. Most anaerobic bacteria do not function at DO concentrations greater than approximately 0.5 mg/L. The target DO concentration for reductive dechlorination to occur is less than 1.0 mg/L (AFCEE, 2004). DO concentrations measured in groundwater at the site were less than 1.0 mg/L in all of the source area wells. Concentrations of DO greater than 1.0 mg/L were measured in five downgradient monitoring wells outside of the source area: MW-18B, MW-18D, MW-19D, MW-20B, and MW-20D. Because DO is the preferred electron acceptor used by aerobic microbes to biodegrade organic carbon, areas of higher DO in groundwater typically occur where the carbon source is lowered or depleted. 3.3.3 Oxidation -Reduction Potential The ORP of groundwater is a measure of electron activity and indicates the relative tendency of a solution to accept or transfer electrons. Oxidation-reduction reactions in groundwater containing organic compounds are typically biologically mediated. Therefore, the ORP of groundwater in an aquifer often depends upon the rate of biodegradation. Monitoring ORP can help determine which terminal electron accepting processes (TEAPs) are occurring (AFCEE, 2004). Optimal ORP conditions for promotion of reductive dechlorination are -200 millivolts (mV) or less, although biodegradation can occur along multiple pathways at higher ORP values. No monitoring wells had groundwater ORP values less than -200 mV. And only one monitoring well, MW-103B, had groundwater with an ORP value less than 0.0 mV. Groundwater in the remaining monitoring wells had positive ORP values greater than 0.0 mV. The highest ORP value measured in groundwater was +310.7mV at well MW-104B. 3.3.4 Ferrous Iron Ferric iron is an alternate electron acceptor for microbial respiration, and produces ferrous iron, when oxygen and nitrate are absent or depleted. The presence of ferrous (reduced) iron at concentrations greater than 1 mg/L indicates a reducing environment that can support reductive dechlorination. Groundwater from nineteen of the wells had field geochemical testing of ferrous iron during the November 2009 sampling event. Nine of the wells analyzed for ferrous iron reported concentrations greater than 1.0 mg/L. Wells MW-100B and MW-102B both had the highest concentrations of ferrous iron measured in groundwater (4.0 mg/L) during the November 2009 sampling event. 3.3.5 Methane-Ethane-Ethene Methanogenesis is the production of methane when carbon dioxide is used as terminal electron acceptor and is biologically reduced, or when acetate is split to form carbon dioxide and methane. In addition, methane can form as a final daughter product of reduction of chloroform. The presence of ethane and ethene indicate completion of the TCE reductive dechlorination pathway. Although the fastest rates of anaerobic dechlorination typically occur under strong methanogenic conditions, 60135880 February 2010 AECOM Environment 3-4 methane concentrations greater than 10 mg/L (equivalent to 10,000 pg/L) may indicate that the carbon substrate is being consumed preferentially by methanogenic microorganisms rather than dechlorinating organisms. Methane levels between 1.0-5.0 mg/L (1,000-5,000 pg/L) are desirable, but not required, for reductive dechlorination to occur (AFCEE, 2004). Methane was detected in groundwater at five of the six monitoring wells analyzed for this dissolved gas. Detected concentrations of methane ranged from 52 pg/L at well MW-104B to 4,210 pg/L at MW- 100B. Ethane was detected in was detected in one of the six monitoring wells sampled at a concentration of 27.2 pg/L (MW-103B). Ethene was detected in one of the six monitoring wells sampled at a concentration of 14.4 pg/L (MW-100B). 3.3.6 Alkalinity Increased microbial activity usually will increase the alkalinity of groundwater. This occurs when carbon dioxide is created by the increased biological activity and subsequently causes dissolution of carbonate minerals in the aquifer. Alkalinity is important in maintaining aquifer pH because it buffers the groundwater against metabolic acids that are produced during biodegradation of organic compounds. Alkalinity concentrations that remain at or below background levels, combined with groundwater pH less than 5, will slow biodegradation rates and may require a buffering agent. Alkalinity was measured in groundwater at six wells during the November 2009 sampling event. Values ranged from <5 mg/L at MW-104B to 67.1 mg/L at MW-101A. As shown in Table 2-2, wells with the lower alkalinity concentrations also had the lowest pH levels. A more comprehensive sampling of alkalinity to include background locations will occur in April 2010. 3.3.7 Total Organic Carbon Total Organic Carbon (TOC) is an indicator of the natural organic carbon present in the aquifer that is available as an electron donor substrate necessary for reductive dechlorination reactions. Concentrations of TOC greater than 20 mg/L are generally necessary to sustain biological metabolism. Low TOC levels (less than 20 mg/L) combined with elevated levels of VOCs and alternate electron acceptors indicate that additional carbon substrate is required to sustain biodegradation. TOC was detected at twenty-two of the twenty-three wells sampled during the November 2009 event. Concentrations ranged from 1.2 mg/L at MW-16D to 329 mg/L at MW-100A. TOC concentrations remained greater than 20 mg/L at just three of the source area wells. 3.4 Groundwater Microbial Results Results of the DHC and DHB microbial Census assay analyses conducted on five groundwater samples collected in December 2009 are summarized in Table 3-1. The results show that DHC bacteria are generally absent in groundwater at the locations sampled. Groundwater at MW-101A showed a sparse DHC population of 0.5 cells/mL and DHC bacteria were below detection limits at the other four groundwater sampling locations. DHB bacteria were detected in three of the five groundwater samples analyzed for dehalogenating microbes. Concentrations of DHC in groundwater ranged from 2.70 cells/mL at GW09N-12 (a GeoprobeTm direct push boring) to 1,280 cells/mL at well MW-101A. Based on this limited data set, shallow groundwater appears to have higher DHB concentrations compared to the deeper groundwater. 60135880 February 2010 AECOM Environment 3-5 3.5 Free Phase Product Inspection Free phase product inspection of six monitoring wells (MW-100A, MW-100B, MW-101A, MW-101 B, MW-102A, and MW-102B) is required under the Free Phase Inspection Plan. The free phase product inspections were performed using an oil/water interface probe as described in Section 2.4. A bailer was also used to inspect for floating and sinking free phase product in well MW-101A, which has historically contained small quantities of LNAPL floating on the top of the water column in the well. The November 2009 and historic free phase product observations are presented in Table 3-2. No free phase product was detected in any of the monitoring wells using an electronic oil -water interface probe for the product inspection. Additionally, the bailer inspection method did not show a distinct, measurable separate NAPL layer in the liquids retrieved from the upper and lower water column in MW-101A. However, the bailer had a coalesced oily coating on it, indicating that the water column in well MW-101A contains NAPL product as an emulsion and/or as small droplets. Because the top of the well screen for MW-101A is positioned at least fifteen feet below the water table, the free product likely resides in a deeper interval of the aquifer and it is not an LNAPL that exists in the aquifer solely at or near the water table surface. It is possible that the chemical composition of the NAPL, which is known to be dynamic based on historical chemical analyses, creates a free product density similar to water. In this case, the NAPL mass would neither preferentially sink nor float as a distinct product layer in the water column of the well. 60135880 February 2010 AECOM Environment 4-1 4.0 Remediation Effectiveness Evaluation To evaluate the effectiveness of in situ bioremediation at the Site, TEAPs and other biodegradation indicator parameters were collected and analyzed in groundwater from selected wells during the November 2009 sampling event. Additionally, a review of concentration trends, changes in the extent of the groundwater plume, changes in molar mass, and occurrence of daughter products was conducted. Microbial analyses of several groundwater samples also provide insight into the biodegradation processes and limitations that may be occurring at the Site. Reductive dechlorination of TCE can result in the formation of daughter products cis-1,2-DCE, trans 1,2-DCE, 1,1-DCE, and vinyl chloride. The compounds cis-1,2-DCE, 1,1-DCE, trans-1,2-DCE, and vinyl chloride were detected during the November 2009 groundwater sampling event and have been detected historically at the Site. These daughter products indicate that reductive dechlorination, and possible aerobic co -metabolic biodegradation, is active throughout the VOC plume. Abiotic reductions are also likely but have not been quantified to date. Several lines of evidence indicate the continued occurrence of biodegradation at the site. These include the predominant decrease in parent contaminant concentrations in the main plume, the presence of TCE daughter products, changes in groundwater geochemistry, and the historic detections of methane, ethane, and ethene. 4.1 VOC Degradation Trends Reduction of the parent compounds and product of intermediate daughter products is one line of evidence that degradation processes are occurring in Site groundwater. Long-term concentrations trends of several VOCs of concern in Site groundwater are discussed in this section. 4.1.1 Tricholorethene and Daughter Compounds TCE reductions have ranged from 85.8 percent to 99.9 percent in the primary source area groundwater since 2002 when the in -situ bioremediation program began. Molar concentrations for TCE and its daughter products have also continued to decrease based on calculations from previous sampling events, indicating a net loss of the compounds due to sequential reductive dechlorination (Excel, 2009). Individual trend graphs for TCE and cis-1,2-DCE at various wells are provided in Appendix D. Cumulative trend graphs for TCE at all of the primary monitoring wells and cumulative trend graphs for cis-1,2-DCE and other VOCs including Freon 113 and methylene chloride at the source area wells are provided in Appendix E. TCE Treatment in the Primary Source Area TCE concentrations measured in groundwater from wells located in and near the waste pit source area (MW-100A, MW-10013, MW-101A, MW-101 B, MW-102A, and MW-102B) continue to decline following the HRC° and HRC-X° injections performed in November 2002 and June 2004, respectively. Trend graphs of TCE concentrations from November 2002 to present in treatment area monitoring wells are provided in Appendix D. These graphs show the sequential increase in cis-1,2-DCE production, presumably from first order decay via biodegradation of TCE. November 2009 data 60135880 February 2010 AECOM Environment 4-2 indicate the presence of cis-1,2-DCE and 1,1-DCE in most of the source area wells. Source area wells have not historically contained high concentrations of vinyl chloride. TCE Treatment in the Southern Boundary Treatment Area TCE concentrations in groundwater at the Southern Boundary Treatment Area monitoring wells (i.e., the vicinity of MW-10B, MW-1OD, MW-16B, and MW-16D) remain relatively stable following the HRC° injections performed on that part of the property in September 2006. Trend graphs of TCE and cis- 1,2-DCE concentrations from November 2002 to present in the Southern Boundary Treatment Area monitoring wells (Appendix D) indicate an increase in cis-1,2-DCE following the September 2006 injections. TCE was not significantly reduced in this area during this same time period. November 2009 data indicate the presence of cis-1,2-DCE, 1,1-DCE, and vinyl chloride in several of the Southern Boundary wells. TOC concentrations in this treatment area have decreased during the past year to near background levels. 4.1.2 Methylene Chloride Methylene chloride is a known Site contaminant that currently exceeds its 2L Standard at two wells in the source area. This compound was historically present at elevated concentrations >200 mg/L in groundwater beneath the former waste pit prior to starting the bioremediation program in 2002. Long- term monitoring since 2002 shows significant biodegradation of methylene chloride, with reductions up to 99.6 percent in source area groundwater occurring between 2002 and 2009. Appendix E includes a cumulative trend graph of methylene chloride concentrations measured during the past seven-year treatment period. This graph shows that the rate of methylene chloride biodegradation was greatest during the first three years of treatment (2002-2005). Methylene chloride has several possible degradation pathways. It can degrade to methane via reductive halorespiration, and it can also degrade directly to carbon dioxide via aerobic and/or anaerobic oxidation pathways. Methylene chloride can also biodegrade via aerobic cometabolism to intermediate products and then carbon dioxide. Biodegradation of methylene chloride is one possible source of the methane detected in groundwater. 4.1.3 Freon 113 The compound Freon 113 is a known Site contaminant that currently does not exceed its 2L Standard in groundwater. Appendix E includes a cumulative trend graph for this compound. Degradation of Freon 113 has been slower than the other VOCs and appears to be limited in groundwater. Reductions of this compound in the source area groundwater have varied from 28.5 percent to 80.7 percent during the treatment period 2002-2009. Additional treatment is not necessary for Freon 113 in order to meet its current 2L cleanup standard. However, its widespread presence in Site groundwater is an important factor due to its potential interference with efficient biodegradation of the remaining target VOCs. 4.2 TOC Availability An adequate supply of organic carbon is required to sustain continued biodegradation of the remaining chlorinated VOCs in groundwater. Current data indicate that TOC concentrations have declined throughout most of the plume to below levels that are optimal for maintaining efficient biodegradation. Depleting TOC in the source area is of particular importance because of the larger mass of TCE and degradation daughter products that remain in groundwater in this area. 60135880 February 2010 AECOM Environment 4-3 A rapid decline of TOC in groundwater was observed during the past year, concurrent with an increased rate of TCE biodegradation that was also seen during this time frame, particularly in the intermediate depth groundwater. The following table summarizes the TOC concentrations and changes seen during the past three years at several key monitoring wells in and near the source area: Well No. TOC (mg/L) 10/2007 TOC (mg/L) 10/2008 TOC (mg/L) 11 /2009 % Change* (2007-2008) % Change* (2008-2009) Overall Change %* (2007-2009) MW-100A 340 420 329 +23.5% -21.6% -3.2% MW-10013 400 440 18.7 +10% -95.7% -95.3% MW-101A 19 52 23.5 +173.6% -54.8% +23.7% MW-101 B 310 210 8.6 -32.2% -95.9% -97 2% MW-102A 0.99 1.1 95.3 +11 % +85.6% +95.2% MW-102B 7.7 9.0 5.3 +16.8% -41.1 % -31.1 % MW-102C 160 65 1.7 -59.3% -97.4% -98.9% * Percent changes as increases in TOC shown with (+); Percent changes as decreases shown with (). Data in the table above show that the greatest reductions of TOC occurred in the intermediate and deeper zones of the aquifer where the highest dissolved concentrations of VOCs are located. In several wells the TOC concentrations increased during the past two to three years, but this condition was observed primarily in the shallow "A" wells. The shallow aquifer zones outside of the immediate waste pit source area have much lower TCE and total VOC concentrations and thus a lower metabolic consumption of organic carbon likely occurs in these areas. With the exception of well MW-102A, the TOC reduction rates were higher in the more recent monitoring period 2008-2009 than in the comparative monitoring period in 2007-2008. 4.3 Microbial Profiles Anaerobic reductive dechlorination can be facilitated by several classifications of microbes, including methanogenes, sulfate -reducing bacteria, and dechlorinating (dehalorespiring) bacteria. Bacterial cultures containing Desulfitobacterium, Desulfuromonas, Dehalobacterrestrictus, Dehalospirillum multivorans, and Dehalococcoides spp. are all capable of dechlorinating the higher chlorinated ethene compounds such as Tetrachloroethene (PCE) and TCE to the intermediate product of cis-1,2-DCE (AFCEE, 2004). Dehalobacter microbes can also dechlorinate 1,1,1-TCA, another VOC contaminant in Site groundwater, but not cis-1,2-DCE or vinyl chloride. Methanogenes and sulfate -reducing microbes are generally present in all subsurface environments. Research demonstrates that many of these bacteria can exist even in aerobic environments and then flourish when more suitable anaerobic conditions are established (Chapelle, 1993; Hollinger et al., 1998). 60135880 February 2010 AECOM Environment 4-4 Current research indicates that the types of bacteria that can further reduce cis-1,2-DCE to vinyl chloride and ethene are much more limited and are not ubiquitous to all subsurface environments (He et al., 2003). Some researchers conclude that the capability of complete dechlorination sequence of PCE and TCE to ethene is limited to only a few species of dechlorinating bacteria within the Deha/ococcoides group, specifically the species Deha/ococcoides ethenogenes (Maymo-Gatell et al., 1999). Other researchers (Flynn et al., 2000) have demonstrated complete dechlorination of PCE to ethene using mixed cultures of bacteria that did not contain any Dehalococcoides species. Under aerobic conditions, several types of bacteria including methanotrophs (methane -oxidizing bacteria) can co -metabolize TCE, cis-1,2-DCE and vinyl chloride. 4.3.1 Summary of Biodegradation Potential Results of microbial and VOC analyses performed on groundwater samples from the Site and potential correlations are summarized below: • DHC bacteria were generally absent in Site groundwater at the locations sampled; • DHB bacteria are present in Site groundwater at low to moderate concentrations, and the highest DHB concentrations were detected in shallow groundwater; • Methanogenic conditions remain in portions of the impacted aquifer, even though groundwater within the plume boundary has become more oxic. Methane concentrations have declined in most of the source area wells during the past year and are near the lower end of the range considered optimal for reductive dechlorination; • Methane generation began when the groundwater ORP was highly reduced from fermentation of the injected organic substrate (i.e, HRC°). Methane concentrations increased significantly in most of the wells between 2006 and 2007 and concentrations peaked in the source area wells in 2008; • A large percentage of the TCE has been dechlorinated to cis-1,2-DCE and to a lesser extent 1,1-DCE throughout the VOC plume. There appears to be an historical "stalling" effect of the dechlorination sequence at cis-1,2-DCE in many of the source area Site wells during the 2005-2008 monitoring period; • Vinyl chloride and ethene are being generated at low concentrations in groundwater at several of the wells, demonstrating that complete dechlorination of TCE is occurring in some portions of the dissolved VOC plume; • Beginning in late 2008, the rate of TCE degradation increased and cis-1,2-DCE production increased at several source area wells. During this same time period, the concentration of cis-1,2-DCE increased at several wells downgradient of the source area without a concurrent change in the TCE concentration; • Other VOCs present in groundwater such as 1,1,1-TCA, Freon 113 and methylene chloride have also been reduced through biological and/or abiotic processes. The cumulative conditions described above suggest that the existing suite of microbes in Site groundwater have a limited ability to completely dechlorinate the TCE to ethene, as well as the ability to biodegrade many of the other primary VOCs present in groundwater. Metabolic reductions of TCE to cis-1,2-DCE have been consistent, but at a slow rate, within the groundwater plume. The initial reductions were likely dominated by DHB bacteria in early phases of the bioremediation program and to a lesser extent by methanogenic bacteria. 60135880 February 2010 AECOM Environment 4-5 The general absence of Dehalococcoides spp. bacteria in Site groundwater combined with the inability of the detected Dehalobacter bacteria to further dechlorinate the remaining cis-1,2-DCE leaves the possibility that other types of anaerobic microbes and/or abiotic reduction pathways are responsible for the low concentrations of vinyl chloride and ethene in Site groundwater. Because the VOC plume still contains low to moderate concentrations of methane and groundwater has become more oxic during the past year, these pathways may include aerobic and anaerobic co -metabolic dechlorination by methanotrophic bacteria. It can not be ruled out that DHC bacteria also exist in other zones of the aquifer that were not represented by the limited sampling data for this group of microbes. 60135880 February 2010 AECOM Environment 5-1 5.0 Conclusions Abbott conducted semi-annual bioremediation performance monitoring in November 2009 as required by the approved RAP. The following conclusions and recommendations are based on results of the sampling event as well as the remediation effectiveness evaluation: • During the monitoring period, shallow groundwater at the Site was determined to be flowing to the south-southeast, which is consistent with previous findings. Deep groundwater at the Site was determined to be flowing to the south, with radial flow components to the southeast and southwest, which is consistent with previous findings. Potentiometric values at multilevel Site monitoring well pairs indicate vertically downward hydraulic flow. • TCE, cis-1,2-DCE and 1,1-DCE were detected at concentrations above the 2L Groundwater Standard in most of the Site monitoring wells. Groundwater at one off -site well (MW-18D) contained these same three VOCs and Freon 113, but the concentrations of each compound were below their respective 2L Standards in the off -site well. • Vinyl chloride was also detected in groundwater at one or more Site wells. Concentrations exceed the 2L Groundwater Standard in several of the wells. • The compound 1,1,1-TCA was detected in groundwater at six Site wells located in the primary (Northern) source area. Concentrations of 1,1,1,TCA exceeded its 2L Groundwater Standard in four of the wells. Groundwater in the southern boundary plume area did not contain 1,1,1- TCA. • Toluene was detected at concentrations above the 2L Groundwater Standard in source area monitoring wells MW-100A, MW-100B, MW-101A, and MW-101B. • Methylene chloride was also detected above its 2L Groundwater Standard in source area monitoring wells MW-100A and MW-100B. MEK was detected a concentration above the 2L Groundwater Standard in monitoring well MW-100B. Neither of these compounds was detected in groundwater samples collected from the southern boundary plume area. • Freon 113 was detected at concentrations above the laboratory reporting limits in twenty-one of the Site monitoring wells, and its concentrations were >20 mg/L at several of the source area wells. However, it was not detected at concentrations above the 2L Groundwater Standard in any Site monitoring wells. These data confirm the widespread distribution of Freon 113 in groundwater throughout the shallow and deeper aquifer zones. • Historical trends show that TCE concentrations in the source area (Primary Treatment Area) wells have decreased since initial HRCO injections began in November 2002. Historical trends in the Southern Plume Area show relatively stable TCE concentrations with an increase in cis-1,2-DCE as a result of electron donor substrate injections. 60135880 February 2010 AECOM Environment 5-2 • Current groundwater geochemical data indicate that TOC is nearing depletion in the aquifer zones undergoing bioremediation, groundwater in the VOC plume is becoming more aerobic, and methanogenic conditions are being lost. These changes in geochemistry have been most pronounced during the past one year of monitoring, and suggest that additional electron donor is required to sustain the ongoing bioremediation treatment. In accordance with the RAP, the next semi-annual bioremediation performance monitoring event will be conducted in May 2010. 60135880 February 2010 AECOM Environment 6-1 6.0 References Chapelle, F.H. 1993. Groundwater Microbiology and Geochemistry. New York: John Wily & Sons. Radian, 1993. Remedial Investigation Report, Abbott Laboratories, Laurinburg, NC. Radian Corporation. RUST, 1994. Remedial Action Plan, Abbott Laboratories, Laurinburg, North Carolina. RUST Environment & Infrastructure and Radian Engineering, Inc., August 1994. Hollinger et al, 1998. Dehalobacter restrictus gen. nov. and sp. nov., a Strictly Anaerobic Bacterium that Reductively Dechlorinates Tetra- and Trichloroethene in an Anaerobic Respiration. Archives of Microbiology, Vol. 169(4): 313-321. Maymo-Gatell, et al., 1999. "Reductive dechlorination of chlorinated ethenes and 1,2-dichloroethane by Dehalococcoides ethenogenes 195." Applied and Environmental Microbiology, Vol. 65(7): 3108-3113. Flynn et al., 2000. Microbial Community Changes Associated with a Shift from Reductive Dechlorination of PCE to Reductive Dechlorination of cis-DCE and VC. Environmental Science and Technology, Vol. 34(6): 1056-1061. Matrix, 2002. Remedial Action Plan Amendment, Abbott Laboratories, Laurinburg, North Carolina. Matrix Environmental, Inc. June 2002. He et al., 2003. Detoxification of Vinyl Chloride to Ethene Coupled to Growth of an Anaerobic Bacterium. Nature, Vol. 424:62-65. AFCEE, 2004. Principles and Practices of Enhanced Anaerobic Bioremediation of Chlorinated Solvents. Final -August, 2004. Matrix, 2004. Phase 11 In Situ Bioremediation Preconstruction Letter Report, Abbott Laboratories, Laurinburg, North Carolina. Matrix Environmental Southeast, February 2004. Phoenix, 2006. Phase 11 Preconstruction Report Addendum-HRC Treatment of Southern Boundary Plume Area, Former Abbott Facility, Laurinburg, North Carolina. Phoenix Environmental Associates, Inc., 2006. Phoenix, 2008. Remedial Action Plan Amendment 2-Solvent Release Remediation, Former Abbott Facility, Laurinburg, North Carolina. Phoenix Environmental Associates, Inc. April 2008. Excel, 2009. 1st and 2 d Quarters 2009 Progress Report -Solvent Release Remediation, Former Abbott Facility, Laurinburg, Scotland County, North Carolina. Excel Civil & Environmental Associates, PLLC. June 10, 2009. 60135880 February 2010 AECOM Environment 6.2 AECOM, 2009. Work Plan for Supplemental Subsurface Investigation and Remedial Actions, Solvent Release Remediation, Former Abbott Facility. AECOM North Carolina, Inc., August 2009. 60135880 February 2010 AECOM Environment Tables 60135880 February 2010 Table 1-1 Monitoring Well Construction Details Former Abbott Facility Laurinburg, Scotland County, North Carolina WELL CONSTRUCTION DATA Well Number Date Installed Well Construction Top of Casing MP Elevation (ft, msl) Screened Interval (ft, bgs) Total Well Depth A bgs) Total Well Depth (ft, msl) MW-100A 10/8/2002 2 in Sch 40 PVC 228.86 20 - 30 30.0 198.86 ...................................... MW-100B 10/7/2002 2 in Sch 40 PVC 228.92 35 - 45 45.0 183.92 ...................................... MW-101A 10/11/2002 2 in Sch 40 PVC 228.18 20 - 30 30.0 198.18 ...................................... MW-101B 10/11/2002 2 in Sch 40 PVC 228.17 35 - 45 45.0 183.17 ...................................... MW-102A 10/11/2002 2 in Sch 40 PVC 229.56 20 - 30 30.0 199.56 ...................................... MW-102B 10/10/2002 2 in Sch 40 PVC 229.47 35 - 45 45.0 184.47 ...................................... MW-102C 10/10/2002 2 in Sch 40 PVC 229.54 55 - 65 65.0 164.54 ...................................... MW-103A 10/9/2002 2 in Sch 40 PVC 230.58 20 - 30 30.0 200.58 ...................................... MW-103B 10/8/2002 2 in Sch 40 PVC 230.58 35 - 45 45.0 185.58 ...................................... MW-103C 10/9/2002 2 in Sch 40 PVC 230.60 55 - 65 65.0 165.60 ...................................... MW-104A 6/5/2004 2 in Sch 40 PVC 230.58 2 - 12 12.0 218.58 ...................................... MW-104B 6/5/2004 2 in Sch 40 PVC 230.59 35 - 45 45.0 185.59 ...................................... MW-104C 6/5/2004 2 in Sch 40 PVC 230.56 63.5 - 73.5 73.5 157.06 ...................................... MW-613 7/25/1990 2 in Sch 40 PVC 230.30 14.0 - 19.0 19.0 211.30 ...................................... MW-10B 7/24/1990 2 in Sch 40 PVC 229.10 16.5 - 26.5 26.5 202.60 ...................................... MW-10D 1/17/1996 2 in Sch 40 PVC 228.70 30 - 40 40.0 188.70 ...................................... MW-13B 7/18/1991 2 in Sch 40 PVC 230.30 9.3 - 18 18.0 212.30 ...................................... MW-16B 1/17/1991 2 in Sch 40 PVC 227.90 15.25 - 24.25 24.3 203.65 MW-16D 1/18/1991 2 in Sch 40 PVC 228.90 62.5 - 71.5 71.5 157.40 MW-18B 2/5/1992 2 in Sch 40 PVC 228.70 5.5 - 14.5 14.5 214.20 MW-18D 2/7/1992 2 in Sch 40 PVC 228.70 48.1 - 57.1 57.1 171.60 MW-19B 4/24/1992 2 in Sch 40 PVC 228.70 15 - 25 25.0 203.70 MW-19D 4/27/1992 2 in Sch 40 PVC 228.70 63.8 - 73.8 73.8 154.90 MW-20B 4/28/1992 2 in Sch 40 PVC 227.90 17 - 27 27.0 200.90 MW-20D 4/27/1992 2 in Sch 40 PVC 228.10 68 - 78 78.0 150.10 MW-21 B' 1996 2 in Sch 40 PVC 227.00 15 - 25 25.0 202.00 MW-27D2 1/11/1996 2 in Sch 40 PVC 231.10 30 - 40 40.0 191.10 Notes: 'Well construction logs are not available for MW-21 B. Screened intervals are estimates. 2Well MW-27D could not be located and is recorded as abandoned. ft = feet bgs = below ground surface msl = mean sea level PVC=Polyvinyl chloride Table 1-2 Summary of Groundwater Monitoring Program: November -December 2009 Former Abbott Facility Laurinburg, Scotland County, North Carolina Fixed -Base Laboratory Analyses' Field -Measured Geochemistry and ParameterS2 Well No. VOCs (Method 8260B) VOC TICS (Method 8260) Total Organic Carbon (Method 5310B) Alkalinity (Method 2320B) Methane/Ethane/Ethene (Method RSK-175) DHC &DHB Microbes (CENSUS Assay) Ferrous Iron (Colorimetric)3 Carbon Dioxide (Colorimetric)° Water Quality Indicators5 Water Level Free Product Gauging6 MW-100A X X X X X X X X MW-100B X X X X X X X X X X MW-101A X X X X X X X X X X X MW-101B X X X X X X X X X X MW-102A X X X X X X X X MW-102B X X X X X X X X X X MW-102C X X X X X X X X MW-103A X X X X X X MW-103B X X X X X X X MW-103C X X X X X X MW-104A X X X X X X MW-104B X X X X X X X X MW-104C X X X X X X MW-6B X MW-10B X X X X MW-10D X X X X MW-13B X MW-16B X X X X X X X MW-16D X X X X X X X MW-18B X X X X X X MW-18D X X X X X X MW-19B X X X X X X MW-19D X X X X X X MW-20B X X X X MW-20D X X X X MW-21 B X Notes: I Fixed -base laboratories include Pace Analytical and Abbott Laboratories 2 Field measurements made with HACH colorimetric field test kits and portable field meters a HACH colorimetric test methods HACH colorimetric test methods a Water quality indicators include pH, temperature, dissolved oxygen, oxidation-reduction potential, turbidity, and specific conductance 6 Free product gauging performed with electronic oil -water interface probe in each well shown, and with a bailer in MW-101A. VOCs = volatile organic compounds DHC = Dehalococcoides spp. DHB = Dehalobacterspp. TICs = Tentatively Identified Compounds Table 2-1 Groundwater Level Gauging and Elevation Data: November 2009 Former Abbott Facility Laurinburg, Scotland County, North Carolina Well Identication TOC Elevation ft msl Depth to Water ft btoc Groundwater Elevation ft msl MW-100A 228.86 8.00 220.86 MW-100B 228.92 9.99 218.93 MW-101 A 228.18 8.97 219.21 MW-101 B 228.17 9.70 218.47 MW-102A 229.56 12.43 217.13 MW-102B 229.47 11.45 218.02 MW-102C 229.54 8.18 221.36 MW-103A 230.58 9.89 220.69 MW-103B 230.58 12.13 218.45 MW-103C 230.60 13.10 217.50 MW-104A 230.58 10.23 220.35 MW-104B 230.59 11.57 219.02 MW-104C 230.56 13.25 217.31 MW-6B 230.30 8.00 222.30 MW-10B 229.10 9.48 219.62 MW-10D 228.70 11.98 216.72 MW-13B 230.30 10.91 219.39 MW-16B 227.90 9.20 218.70 MW-16D 228.90 11.85 217.05 MW-18B 228.70 10.62 218.08 MW-18D 228.70 12.50 216.20 MW-19B 228.70 8.80 219.90 MW-19D 228.70 12.60 216.10 MW-20B 227.90 9.35 218.55 MW-20D 228.10 11.67 216.43 MW-21 B 227.00 6.35 220.65 Notes: Water levels were measured on November 3, 2009 TOC: Top of Casing ft: Feet ft btoc: feet below the top of casing msl: mean sea level Table 2-2 Geochemicial Parameters in Monitoring Wells: November 2009 Former Abbott Facility Laurinburg, Scotland County, North Carolina Chemical Name Sample ID Sample Date Units MW-100A 11/5/2009 MW-100B 11/5/2009 MW-101A 11/5/2009 MW-101B 11/5/2009 MW-102A 11/4/2009 MW-102B 11/4/2009 MW-102C 11/4/2009 MW-103A 11/4/2009 MW-103B 11/4/2009 MW-103C 11/4/2009 Duplicate MW-103C 11/4/2009 MW-104A 11/4/2009 MW-104B 11/4/2009 Field Parameters Temperature °C 19.71 22.75 19.65 19.81 19.25 20.60 21.60 20.65 20.63 NM 20.55 20.87 20.81 H SU 5.03 5.90 5.77 5.41 4.93 5.49 4.30 5.62 6.40 NM 6.12 5.60 4.71 Specific Conductivity PS/cm 391 951 418 180 168 84 48 130 204 NM 168 146 81 Dissolved Oxygen m /L 0.25 0.69 0.31 0.31 0.43 0.31 0.28 0.40 0.46 NM 0.42 0.98 0.26 ORP my 52.1 0.5 35.2 49.2 43.5 61.9 227.6 97.2 -42.1 NM 29.7 107.1 310.7 Turbidity NTU 0.00 0.00 0.00 0.00 7.24 1.90 1.40 5.08 7.90 NM 0.10 9.24 0.00 *Ferrous Iron m /L 1.5 4.0 1.0 0.2 2.4 4.0 1.0 0.9 1.2 NM 0.2 2.0 0.00 *Carbon Dioxide m /L 38 32 32 30 100 26 16 35 28 NM 40 30 10 Wet Chemistry Alkalinity m /L NA NA 67.1 34.6 NA 22.4 NA NA NA NA NA NA < 5.0 Ethene u /L NA 14.4 < 10.0 < 10.0 NA < 10.0 NA NA < 10.0 NA NA NA < 10.0 Ethane u /L NA < 10.0 < 10.0 < 10.0 NA < 10.0 NA NA 27.2 NA NA NA < 10.0 Methane u /L NA 4210 285 < 10.0 NA 2320 NA NA 2410 NA NA NA 52.2 TOC m /L 329 18.7 23.5 8.6 95.3 5.3 1.7 3.9 3.7 3.1 29.1 3.9 3.0 Chemical Name Sample ID Sample Date MW-104C 11/4/2009 MW-10B 11/3/2009 Duplicate MW-10B 11/3/2009 MW-10D 11/3/2009 MW-16B 11/3/2009 MW-16D 11/3/2009 MW-18B 11/4/2009 MW-18D 11/4/2009 MW-19B 11/3/2009 MW-19D 11/3/2009 MW-20B 11/3/2009 MW-20D 11/3/2009 Units Field Parameters Temperature °C 20.77 NM 20.99 20.87 21.27 21.54 20.02 19.03 20.87 19.86 20.94 19.09 H SU 4.74 NM 4.74 5.66 4.08 6.63 4.52 4.54 5.10 4.72 4.60 4.30 Specific Conductivity PS/cm 83 NM 105 137 55 76 111 68 64 62 51 65 Dissolved Oxygen m /L 0.50 NM 0.49 0.48 0.52 0.25 5.64 1.33 0.30 2.28 1.29 5.62 ORP my 269.1 NM 68.5 30.2 240.1 36.9 253.9 271.0 203.6 176.9 191.8 246.0 Turbidity NTU 0.00 NM 4.3 0.00 0.00 12.30 9.24 6.90 0.00 3.40 0.00 0.81 *Ferrous Iron m /L 0.00 NM NM NM 0.00 0.00 0.00 0.00 2.8 0.2 NM NM *Carbon Dioxide m /L 18 NM NM NM 12 10 10 12 30 10 NM NM Wet Chemistry Alkalinity m /L NA NA NA NA 6.1 32.5 NA NA NA NA NA NA Ethene u /L NA NA NA NA NA NA NA NA NA NA NA NA Ethane u /L NA NA NA NA NA NA NA NA NA NA NA NA Methane u /L NA NA NA NA NA NA NA NA NA NA NA NA TOC m /L 3.1 3.6 3.0 6.2 2.9 1.2 1.6 2.3 2.5 2.1 2.7 < 1.0 Notes: uS/cm: microseimens per centimeter mg/L: milligrams per liter ug/L: micrograms per liter SU: Standard Units °C: Degrees Celsius ORP: oxidation-reduction potential NTU: Nephelometric Turbidity Units mv: millivolts NA: Not analyzed NM: Not Measured TOC: total organic carbon *Ferrous iron and carbon dioxide measurements were collected and analyzed using a HACH field Colorimeter. Bold: Constituent concentration reported above the method detection limit. Table 2-3 Volatile Organic Compound Analytical Results in Groundwater: November 2009 Former Abbott Facility Laurinburg, Scotland County, North Carolina Chemical Name 1,1,1-TCA 1,1-DCA 1,1-DCE 1,2-DCA Chloroform cis-1,2- DCE MEK MTBE Methylene Chloride Toluene trans-1,2- DCE TCE Freon 113 Vinyl Chloride Sample ID Date Units pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L 2L Standard (pg/L) 200 6 7 0.4 70 70 4,000 20 5 600 100 3 200,000 0.03 Method MW-100A 11/5/2009 8260B 720 < 500 < 500 < 500 < 500 38,000 < 2500 < 500 920 2,300 < 500 3,200 5,200 < 500 MW-100B 11/5/2009 8260B 870 < 500 680 < 500 < 500 47,000 4400 < 500 890 2,400 < 500 < 500 25,000 < 500 MW-101A 11/5/2009 8260B 5,400 < 500 510 < 500 < 500 12,000 < 2500 < 500 < 500 2,700 < 500 55,000 29,000 < 500 MW-101 B 11/5/2009 8260B 1,700 < 500 < 500 < 500 < 500 28,000 < 2500 < 500 < 500 1,200 < 500 1,100 14,000 < 500 MW-102A 11/4/2009 8260B 84 < 50 550 < 50 < 50 24,000 < 250 < 50 < 50 150 < 50 790 8,900 < 50 MW-102B 11/4/2009 8260B 17 < 5 71 < 5 < 5 1,100 < 25 < 5 < 5 13 < 5 590 3,900 < 5 MW-102C 11/4/2009 8260B < 5 < 5 5.8 < 5 < 5 11 < 25 < 5 < 5 < 5 < 5 < 5 1,500 < 5 MW-103A 11/4/2009 8260B < 20 < 20 < 20 < 20 < 20 220 < 100 < 20 < 20 < 20 < 20 29 21,000 < 20 MW-103B 11/4/2009 8260B < 5 < 5 31 < 5 < 5 290 < 25 < 5 < 5 6.6 < 5 27 8,800 12 MW-103C DUP 11/4/2009 8260B < 200 < 200 < 200 < 200 < 200 340 < 1000 < 200 < 200 < 200 < 200 < 200 7,600 < 200 MW-103C 11/4/2009 8260B < 10 < 10 22 < 10 < 10 280 < 50 < 10 < 10 < 10 < 10 23 7,300 12 MW-104A 11/4/2009 8260B < 10 3.1 2.8 3.8 2.1 590 < 50 < 10 < 10 < 10 3.3 2.4 1 940 12 MW-104B 11/4/2009 8260B < 5 < 5 12 < 5 < 5 99 < 25 9.2 < 5 < 5 < 5 18 2,100 < 5 MW-104C 11/4/2009 8260B < 5 < 5 20 < 5 < 5 150 < 25 8 < 5 < 5 < 5 15 2,700 < 5 MW-10B DUP 11/3/2009 8260B < 5 < 5 8 < 5 < 5 90 < 25 2.1 < 5 < 5 < 5 3.3 610 1.3 MW-10B 11/3/2009 8260B < 1 < 1 9 < 1 < 1 87 < 5 2 < 1 < 1 < 1 3.5 640 1.2 MW-10D 11/3/2009 8260B < 1 < 1 10 < 1 1.3 130 < 5 2.4 < 1 < 1 < 1 4.7 820 2 MW-16B 11/3/2009 8260B < 1 < 1 < 1 < 1 < 1 3.4 < 5 1.2 < 1 < 1 < 1 < 1 1 36 < 1 MW-16D 11/3/2009 8260B < 1 < 1 < 1 < 1 < 1 3.8 < 5 < 1 < 1 < 1 < 1 < 1 5.8 < 1 MW-18B 11/4/2009 8260B <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <5 <1 MW-18D 11/4/2009 8260B < 1 < 1 1.3 < 1 < 1 18 < 5 < 1 < 1 < 1 < 1 1.4 220 < 1 MW-19B 11/3/20091 8260B <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <5 <1 MW-19D 11/3/20091 8260B < 1 < 1 3.3 1 < 1 1 54 1 < 5 < 1 < 1 < 1 < 1 7.7 670 < 1 MW-20B 111/3/20091 8260B I <1 <1 <1 1 <1 1 <1 <1 1 <5 <1 1 <1 <1 <1 <1 <5 <1 MW-20D 111/3/20091 8260B I <1 <1 <1 1 <1 1 <1 <1 1 <5 <1 1 <1 <1 <1 <1 <5 <1 Notes: 1,1,1-TCA: 1,1,1-Trichloroethane MEK: Methyl Ether Ketone 1,1-DCA: 1,1-Dichloroethane MTBE: Methyl tert butyl ether 1,1-DCE: 1,1-Dichloroethylene TCE: Trichloroethylene 1,2-DCA: 1,2-Dichloroethane trans-1,2-DCE: trans- 1,2-dichloroethene cis-1,2-DCE: cis- 1,2-dichloroethene Freon 113: Trichlorotrifluoroethane Only those VOCs detected in one or more wells during the November 2009 sampling event are listed in this table. 21-Standard: North Carolina Administrative Code (15A NCAC) Subchapter 2L Groundwater Standards (January 2010) µg/L: micrograms per liter Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Table 3-1 Dehalogenating Bacteria Analytical Results: December 2009 Former Abbott Facility Laurinburg, Scotland County, North Carolina Sample ID Date Analysis DHC cells/mL TCE cells/mL BVC cells/mL VCR cells/mL DHB cells/mL Units Method MW-100B 12/1/2009 Census <0.5 <0.5 <0.5 <0.5 <1.0 MW-101A 12/1/2009 Census 0.50 <0.3 <0.3 0.1J 1280 MW-102C 1 12/1/20091 Census I 0.2J 1 <0.5 1 <0.5 1 0.4J I <1.0 GW09N-10 (17-22) 12/15/2009 Census <0.3 NA NA NA 4.00 GW09N-12 (41-46) 1 12/14/2009 Census <1.0 I NA I NA I NA 1 2.70 Notes: Shaded cells indicate detectable concentrations of microbes cells/mL- cells per milliliter DHC= Dehalococcoides spp. TCE= tceA Reductase BVC= bvcA Reductase VCR= Vinyl Chloride Reductase DHB= Dehalobacterspp. Table 3-2 Historical Free Phase Product Observations Former Abbott Facility Laurinburg, Scotland County, North Carolina Monitoring Well Observed Thickness of Free Phase Product (in inches) 6/13//06 9/19/2006 12/19/2006 4/2/2007 10/30/2007 4/2/2008 10/29/2008 11/3/2009 MW-100A 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 MW-100B 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 MW-101A 2.75 0.00 1.25 0.25 0.25 2.00 1.25 0.00* MW-101 B 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 MW-102A 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 MW-102B 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 *MW-101A contained an oily emulsion with droplets on 11/3/09; no distinct or measurable free phase layer was present. 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(919) 872-6600 FAX: (919) 872-7996 WEB: HTTP://WWW.AECOM.COM A=COM I DESIGNED BY: REVISIONS NO.: DESCRIPTION: DATE: BY: DRAWN BY: KLR CHECKED BY: APPROVED BY: D � ' I ' r�o o F� p n (n ,iv00 9-0 -) ODW�GW�r�m SO m mm(D �D�m�znm�<pccn W<j p,�z�z'pmm �"' z�r �7 �� m ���OAm=�D� �._ p vG)G) ^�0mG� mG) xZ �D ^�� ^�W v xO x' T T DX frl o =�gmr-m�p�5cm �� / —'_•� ._,_��_ moz �mOp0 mO (min ZD xM�(mi co')zop D �O m z z COo Oz(��Om=m<mmpO / �z� �m�pz �z OG Op Iv0O EOM, D oz M, m m Cnm � m D z v r- -v v O �D���W� / �, Ozer -z�m� O� �m �z o�� Np22p m >� m z z oW II c�z=v <nD0 W Dm -n zD zD �p zm ,�,z� oz- D m m D< �m mcn<O c m �� �� Gov G�(n NG�D r O� mm �� DT�m� / my XyDm Tlm O - Z zm �X NO m�>Dompcn / / m�r�J �x r-c m m� mO m r�J z �� _ mmm m�VzO� = r z r r r z n r 0 O r r r m p N omo--<ZooOz;0 0 D Drc�i-ImOZzMgDM °�/ x �CA G) i ! rm � pm co m M c to p m NC I = V C ; m N ; M W a p , N 1 W z v , 0 !2C V < CA -4 v 10 W ®' / C� G V W / \ 0 m o y // W y� V C co V7 s Cam' � < Cu M c < w NOD v 00 O D N /W v / W N > O® V O N p 'a O 0 D N D\4 I I 0 I ' W IV 0 I' ' C DEEP GROUNDWATER POTENTIOMETRIC SURFACE MAP NOVEMBER 2009 Former Abbott Facility Laurinburg, North Carolina SCALE: DATE: PROJECT NUMBER: 1"=120' 2/23/10 60135880.400 0 AECOM North Carolina, Inc. 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RALEIGH, NORTH CAROLINA 27616 PHONE: (919) 872-6600 FAX: (919) 872-7996 WEB: HTTP://WWW.AECOM.COM M A_COM '� N CJ 4 7 7 10 3.0. 1*1 0 o� �jCnK o O 00 01 D I I ❑ �� ° a l DESIGNED BY: REVISIONS NO.: DESCRIPTION: DATE: BY: DRAWN BY: KLR CHECKED BY: APPROVED BY: <0 FC/) m D G D r- �, m m Oz7 z E D -n D 70 m rO CO 00 y{ II M om X N mm � r 00 v N O 0 N 0 Oc / my 1 w � 0 I > 00 I W 0_ 0 (0 Q m � c m Ln c I z V ; c s � m m AKA - K < V� v I v m w C z CD O ii ! m �so� om-ao m li i ' m TImmI A cNi, o I i! p mO xcnz W W ;�Z I D WI I i D F� O -m7 T cnT=Tmm mD 022 022 mDOOm OpOmOzXX--j�O�zmOqzom �O m� GG p -G oz OO C,Om . O� D rmm CD X ZDm>m(ArvOzmm��-mX -0O �O �o zN�z z �rz m0� �> r� m�Vm �O cn� rO rZ� �mm� m mmz me 0orz m z o�°zm zz m 03 m(0m m > cn = = cQ m cn m x / �CA G) r,M 1 rm / "'*'�-om TCE IN GROUNDWATER: DEEP AQUIFER ZONE NOVEMBER 2009 Former Abbott Facility Laurinburg, North Carolina SCALE: DATE: PROJECT NUMBER: 1"=120' 2/23/10 60135880.400 CD � D CD a W co \ \ \ \ 0 q, N m ;0 2 = ° / -p 0 coD m� / l' o, ll GG o cop �� W� �\ N 00< D / 2 cAA� K K � `W W cM W W W C O 0 D w n N p W n 70 30 -4� �00 ♦ _ W 0 0 _ N O V W CD � W / D W I I / � � I � J � C ® 0 A a J( I I 1 I AECOM North Carolina, Inc. RALEIGH, NORTH CAROLINA 27616 PHONE: (919) 872-6600 FAX: (919) 872-7996 WEB: HTTP://WWW.AECOM.COM A_COM DESIGNED BY: REVISIONS NO.: DESCRIPTION: DATE: BY: DRAWN BY: KLR CHECKED BY: APPROVED BY: AECOM Environment Appendix A Semi -Annual Groundwater Sampling Records 60135880 February 2010 ENSR I AEC Well ID: MW-10B Low Flow Ground Water Sample Collection Record [�U-�" Client: Abbott Date: of Time: Start /Sc55 am/pm Project No: 00005-024-400 Finish WO am/pm Site Location: Laurinburg, NC WeatherConds: ";b °VSdnnyCollector(s): Babine / Joe Ladd 1, WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length c. Length of Water Column Q-0)a (a-b) Casing Diameter/Material J 4x— b. Water Table Depth d. Calculated System Volume (see back) �- 2. WELL PURGE DATA a. Purge Method: eri it / Monsoon b. Acceptance Criteria defined (see workplan) -Temperature 3% -D.O. 10% - pH + 1.0 unit ORP ± 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model Serial Nupm YSI 556 �001 'L Volume Time Removed Temp. PH Spec. Cond. DO ORP Turbidity FIOw R to Drawwdown Color/Odor ®_®'G��d��r�V/�ll�f��l$g/J��il��� / r LYlllii�l� ��r,�r,�✓ •r"S?I71�f�'LY��l�l�� i Ir C� llllllllllllll,—_llllllll,lllll_®_—_—_®_—_®_�_ ®®�llllllllll,--Illllllll-Illlllllllllll, f d. Acceptance criteria passrran yes rvo rvi„ Has required volume been removed ❑ ❑ 49 Has required turbidity been reached (W ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION Sample ID Container Type MW-lOB kvA Comments 00D • - Method: No. of�ontalners Analysis Req. Time I.S7 U Signature Date Well ID: MW-10D Low Flow Ground Water Sample Collection Record Client: Abbott Date: //- 3 -o Time: Start J!5 0,0am/ Project No: 00005-024-400 Finish /gf o am/ Site Location: Laurinburg, NC Weather Cords: 2 ° Collector(s): D. Babineau / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length i10. COc.c. Length of Water Column J� (a-b) b. Water Table Depth //, %y d. Calculated System Volume (see back) 1l. 90 2. WELL PURGE a. Purge Meth( b. Acceptance Crit Tia-defined (see workplah) -Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cord. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model YSI 556 Casing Diameter/Material all / A,/ Serial Number Volume Time Removed Temp. pH Spec. Cord. DO ORP Turbidity Flow Ratel Drawdown I Color/Odor ion kA fl if—x I-M 1mn/I 1 %mVl /NTI II (fr itmin)(Teel) I��l�ll►�7111111111��� : r i r.�!'0�®lllt'i'i�� ®—IIIIIIIII,1111111111111--IIIIIIIIIIIIIII,lllllllllllllll,®—� d. Acceptance criteria pass/fail Has required volume been removed Has required turbidity been reached Have parameters stabilized If no or N/A - Explain below. Yes ® ® No ❑ ❑ ❑ N/A (continued on back) ❑ ❑ ❑ 3. SAMPLE COLLECTION: Method: ristalti Sample ID Container Type No. of Containers MW-10D V0A / Monsoon Preservation Analysis Req. Time yo-C, 6:1n.06 16t/O MA a 1221&4 � gg,, I Comments Signature fir.(' Date Well ID: MW-16B Low Flow Ground Water Sample Collection Record Client: Abbott Date: [JI(316� Time: Start )YLI am/pm Project No 00005-024-400 Finish /4l6 am/pm Site Location: Laurinburg, NC WeatherConds: 7o0, W5yA!l,a Collector(s): D ] binea / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length f < 3 c. Length of Water Column (a-b) Casing Diameter/Material b. Water Table Depth q,�4 d. Calculated System Volume (see back) R, C q �^ 2. WELL PURGE DATA a. Purge Method:. eristalf / Monsoon b. Acceptance Criteria defined (see workplan) -Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3, c. Field Testing Equipment used: Make Model Serial Number YSI'. 556 Lamotte 2020d Volume Time Removed Temp. pH Spec: Cond. DO ORP Turbidity Flow Ratel Drawdown I Color/Odor (24hr) (Liters) . M) (us/cm) (ma/L) (mv) (NTU) (ml/min)(Teel) d. Acceptance criteria pass/fail Yes No N/A (continued on back) Has required volume been removed ❑ ❑ Has required turbidity been reached 10 ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: erista ' / Monsoon Sample ID Container Type No. of Containers Preservation An lysis2Req. Time Mw_1fiR i/n,d. TS' /�!'i/ �()6 IUAS Comments Signature WeIIID: MW-16D Low Flow Ground Water Sample Collection Record Dlient: Abbott Date: Time: Start /qo o am/pm Project No: 00005-024-400 Finish NT am/ Ul Site Location: Laurinburg, NC VVeather Cords: /)a ° (" /Pa, Collector(s): D. Babineau / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length id' S c. Length of Water Column s (a-b) b. Water Table Dept 1t Calculated System Volume (see back) 2. WELL PURGE DATA a. Purge Method: .cristaltic /Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -DO. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' Casing Diameter/Material c. Field Testing Equipment used: Make Model Serial Number YSl 556 Lamotte 2020 Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Ratel Drawdown I Color/Odor (24hr) (Liters) (T) 66/cm) 6mc/L) (mV) (NTu) (ml/min) ee d. Acceptance criteriapass/fail Yes No N/A (continued on back) Has required volume been removed 0 ❑ ❑ Has required turbidity been reached ® ❑ Have parameters stabilized ® ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: erisSa tic / Monsoon Sample ID Container Type No. of Containers Preservation Analysis Req. Time Comments Signature ( Date /Z s Q ENSRIAECOM Well ID: MW-18B Low Flow Ground Water Sample Collection Record Client: Abbott Date: ff q-03 Time: Start f pm Project No: 00005-024-400 Finishpo,T-U pm Site Location: Laurinbur , NC Weather Cords: (/Q� Collector(s): D. Babineau /Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length c. Length of Water Column i. "] (a-b) Casing Diameter/Material l PUS b. Water Table Depth /U. 4Z' d. Calculated System Volume (see back) 6 WO 2. WELL PURGE DATA a. Purge Method: Peristaltic / Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing. Equipment used: Make Model Serial Number YSI 556 Lamotte 2020 Volume Time Removed Temp. pH Spec. Cond, DO ORP Turbidity Flow Ratel Drawdown Color/Odor Kati o.� Cl uS/eml mnrLi lmVl NTUI (ml/mlm ee �'. ®I�ll�lllllllrt��ll�c��lll��lllrr��lll�/� ry������//��►���/�'1Z����IIIIIIIiiill/� -Illlllll■®-�®---� d. Acceptance criteria pass/tau Yes NO N/A Has required volume been removed ® ❑' ❑ Has required turbidity been reached ❑ Have parameters stabilized Q4 ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Sample ID Container Type Comments Method: Peristaltic / Monsoon No. of Containers (conUnuec on back) Analysis Req. Time (tr,A i 17, u_At ioc uirr 1 „ Signature (( //i��CG/ Date /� ENSRIAECOM Well ID: MW-18D Low Flow Ground Water Sample Collection Record Client: Abbott Date: Id Time: Time: Start QOY5 am/pm Project No: 00005-024-400 Finish 6$3,0 am/pm Site Location: Laurinburg, NC Weather Conds: ~5*VO Sarin Collector(s): D. Bab ne / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well LengthS&X) c. Length of Water Column l/J. 5 (a-b) Casing Diameter flaterial b. Water Table Depth d. Calculated System Volume (see back) a 9 O 2. WELL PURGE DATA "ic a. Purge Method' Perista / Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model Serial Number YSI 556 Lamotte 2020 Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Rate Drawdown Coioi•/Odor t1A6r\6r� /I 1{ur.% !°C\ A A/eml !mn/L1 rmvt TNTui (MI/min) ee r;��lnMc■c�rr.�c� d. Acceptance criteria pass/tail Yes No N/A Has required volume been removed ❑ ❑ 0 Has required turbidity been reached ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Sample ID Container Type Comments Signature Method: No. of Containers Preservation (continueo on back) Req. Time L Date fllh�d v Well ID: MW-196 Low Flow Ground Water Sample Collection Record Client: Abbott Date: //- 3 (1 Time: Start dam/ Project No: 00005-024-400 Finish am/pm Site Location: Laurinbur , NC _ Weather Conds: ° C PCL✓ Collector(s): D. Babineau /Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length c. Length of Water Column )t%, (a-b) Casing Diameter/Material 2" l Pvc. b. Water Table Depth d. Calculated System Volume (see back) 2. WELL PURGE DATA a. Purge Method: Peristaltic% / Monsoon I b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < Off c. Field Testing Equipment used: Make Model Serial Number YSI 556 Volume Time Removed Temp. pH (24hr) (Liters) CM Spec. Cond. DO ORP (US/cm) (matt) M IlMillill ��N14}L11����r�E.l�'® � • IIIIIIII�/® d. Acceptance criteria pass/fail Yes No N/A (continued on back) Has required volume been removed ® ❑ ❑ Has required turbidity been reached ®. ❑ ❑ Have parameters stabilized ® ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Sample ID Container Type Method: (Perista0/ Monsoon No. of Containers Comments Signature Req. Time Date J/ (? a 9 ENSR yAECOM Well ID: MW-19D Low Flow Ground Water Sample Collection Record � Client: Abbott Date: Time: Start mcc am/pm Project No: 00005-024-400 Finish C-t $ am/pm Site Location: Laurinburg, NC WeatherConds:—*?0a`tSr/nd4, Collector(s): Babinea / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length 2q c. Length of Water Column j9h Lb (a-b) Casing Diameter/Material ' ��. 3 a o b. Water Table Depth d. Calculated System Volume (see back) b 2. WELL PURGE DATA a. Purge Method: eristalt / Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model Serial Number S YSI 556 flw Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Rate Drawdown Color/Odor (24hr) MMus)le PM (Us/cm) (ma(mV) (NTu) (mI/min)tfeeil d. Acceptance criteria pass/fail Yes No N/A Has required volume been removed ❑ ❑ fo Has required turbidity been reached ❑ ❑ Have parameters stabilized ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: Sample ID Container Type No. of Containers Comments 8Kd, f, 1 Signature _ � - Date �[��/Q9 (continued on back) Time S Well ID: MW-20B Low Flow Ground Water Sample Collection Record Client: Abbott Date: /)-3 G 9 Time: Start foam/aiir Project No: 00005-024-400 Finish am/pm Site Location: Laurinburg, NC Weather Cords: 5:5 ° C lecrr Collector(s): D. Babineau / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length of%r CO c. Length of Water Columnar leS (a-b) Casing Diameter/Material 2 / Pye, b. Water Table Depth9%3Y "d. Calculated System Volume (see back) 2. WELL PURGE DATA--- --•a a. Purge Method: ristalti / Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% -pH + 1.0 unit ORP + 10mV - Sp. Cord. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model Serial Number YS1 556 Lamotte 2020 Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Rate Drawdown Color/Odor OAI.r1 (Iuo.�t i°c) h1Slcml (mnn l (mVI - (NTU) (ml/min)(Teel) IEitZf'llll�O��.tII3�l��l�a�ll�IIL�J•�`�! d. Acceptance criteria pass/tan d. Acceptance criteria pass/tan Yes NO NIA (continued on nacK) Has required volume been removed Z] ❑ ❑ Has required turbidity been reached El ❑ -1❑ Have parameters stabilized m ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: .�ristalt Monsoon Sample ID Container Type No. of Containers Preservation Analysis Req. Time MW-2013 IMA 3 8e l__ Awa Comments Signature Date /�- T6 j Well ID: MW-20D ri! Low Flow Ground Water Sample Collection Record Client: Abbott Date: tt13101 Time: Start 160 am/pm Project No: 00005-024-400 Finish 1 i iS am/pm Site Location: Laurinburg, NC Weather Cords: ` WS()m Collector(s): . Babine / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) J a. Total Well Length 7�-9 c. Length of Water ColumnCC, )D (a-b) Casing Diameter/Material b. Water Table Depth 11,67 d. Calculated System Volume (see back) La, 8`1 a / � V4, 2. WELL PURGE DATA a. Purge Method: eristalt / Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model Serial Number YSI 556 a O.Wi Volume Time Removed Temp. pH (24hr) (Liters) Oc) Spec. Cond. DO ORP Turbidity Flow Ratel Drawdown j Color/Odor (us/cm) (ma/L) (mv) (NTU) (ml/min) ee ,MILt • llllllllllll®�IIIII�IIIIIIII�O�llll�-�®- d. Acceptance criteria pass/fail Yes No N/A Has required volume been removed ❑ ❑ e Has required turbidity been reached ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: ( Perista�ity; / Monsoon (continued on back) Sample ID Container Type No. of Containers Preservation Analysis Req. Time MW-20D Vov t' 3 11-e, l bu6 8d 6'U % o7a D Comments Signature Date MC1, i Well ID: MW-1 00A Low Flow Ground Water Sample Collection Record Client: Abbott Date: i( $ Time: Start 0j 3d am/pm Project No: 00005-024-400 Finishlut> am/pm Site Location: Laurinburg, NC WeatherConds: rj;oq- Collector(s): abin Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length U c. Length of Water Column �,,Z_ (a-b) CasinaiDieter/Material p � lam , b. Water Table Depth p � � d. Calculated System Volume (see sack) l . 2. WELL PURGE DATA a. Purge Method: (fie isiait' / Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model Serial Number YSI 556 ao; `S Lamotte 2020 ;)0 b- Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Ratel Drawdown I Color/Odor (24hr) (Liters) (°C) - (us/cm) (mo/L) (mv) (NTU) Iml/min)(feel) FAMN ON ���1:��� w tea. �%�s��®>•WHYPEMP d. Acceptance criteria pass/fail Yes No. N/A (continued on back) Has required volume been removed ❑ ❑ a Has required turbidity been reached ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Sample ID Container Type No. of Containers Preservation Analysis R( Comments Signature L"'��� Date `/, ENSRIAECOM Well ID: MV1-100B Req. (continued on back) Low Flow Ground Water Sample Collection Record Client: Abbott Date: (/ 5 Time: Start a/ X5 am/pm Project No: 00005-024-400 Finish ISj (3 am/pm Site Location: Laurinburg, NC Weather Conds: Collector(s): Babe3d / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length L/>CCc. Length of Water Column U, 0) (a-b) b. Water Table Depth % C L d. Calculated System Volume (see back) 2. WELL PURGE DATA a. Purge Method: rist c / Monsoon b. Acceptance Criteria defined (see workplan) -Temperature 3% -DO. 10% -pH + 1.0 unit ORP + 10mV - Sp. Cord. 3%0. Drawdown < 0.3' c. Field Testing Equipment used: Make YSI �1 � 6a- Casing Diameter/Material a w / 4 V" Model Serial Number 556 aLoty Volume Time Removed Temp. PH Spec. Cond. DO ORP TurbidU Flow Rafel own I Color/Odor l9dhrl 11 ifcral /°C1 Gi8leml /mnn\ lmV) (NTIII (milmul)(Teal) tl'iL�11MMM� �� k4. .� �II1ZrtJ� A7L1�J d. Acceptance criteria pass/fail Yes No N/A Has required volume been removed ❑ ❑' 2 Has required turbidity been reached ❑ [j Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: nstal is / Monsoon Sample ID Container Type No. of Containers Preservation MW-100B L rA 14� I , Comments Signature ����1 Date li%s'%ON ENSR I AECOM Well ID: MW-101A Low Flow Ground Water Sample Collection Record Client: Abbott Date: i)�s�rfl Time: Start 6500 am/pm Project No: 00005-024-400 Finish U am/pm Site Location: Laurinburg, NC Weather Conds: 1'" 6'aswA!gy Collector(s): �abmeauJoeLadd 1. WATER LEVEL DATA: (measured from Top of Casing) a..Total Well Length �O c. Length of Water Column a l,63 (a-b) Casing Diameter/Material gI"t / NVc, b. Water Table Depth d. Calculated System Volume (see back) a aZ ol 2. WELL PURGE DAT a. Purge Method: b. Acceptance Criteria defined (see workplan) -temperature 3% -D.O. p + 1.0 unit -Sp.Cond. 3% ORP, Drawdown \o c. Field Equipment used: Make \Testing YS1 Lamotte Volume 10% + 10mV < 0.3' Model Serial Number gaO Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Ratel Drawdown I Color/Odor (94hr) (Piters) ('cl his/cml (ma/Ll (my) (NTU) (ml/min)(feel) d. Acceptance criteria pags/fail Yes No N/A (continued on back) Has required volume been removed ❑ ❑ 0 Has required turbidity been reached N ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: rPerrtgtaltjc / Monsoon Sample )D Container Type No. of Containers Preservation Analysis Req. Time MW-101A VaA 3 /mil lint q_114.ri �I,3a Comments s bloom o,p�r Qt�a+l ( 11 Signature ��� ��� Date ✓) h&n b ENSR I AECOM Well ID: MW-101B Low Flow Ground Water Sample Collection Record Client: Abbott Date. 1115` Time: Start Oe G' am/pm Project No: 00005-024-400 Finish D am/pm Site Location: Laurinburg, NC Weather Conds: --('0" *50A Collector(s): .95au / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length N5 c. Length of Water Column 35(a-b) Casing Diameter/Material b. Water Table Depthl170 2. WELL PURGE DATA a. Purge Method, d. Calculated System Volume tree back) �. IY�V b. Acceptance Criteria defined (see workplan)' - Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model Serial Number Volume Time Removed Temp. pH Spec. Cond, DO ORP Turbidity Flow Ratel down I Color/Odor (24hr) - (Liters) Cc) (as/cm) (mc/L) (mv) (NTU) (ml/min) TeeL l•Y'Z�2 � 1.1I�,�®fti���Yi� " • I♦-�i�(�c�'��.�/.fT/�J� Its®II��G�1IM1111111 • . Y ®liltiilfirii i e �� � • II,�� �• IIIIIIIIIIIII■ - IIIIIII■ IIIIIIIII■ ®- IIIIIII" IIIIIIIIIIIIIII■ II, IIIIIIII■ IIIIIIIIIIIII■-IIIIIII■--� IIIIIIIIIIIII■ IIIIIIIIIIIII■ II�� IIIIIII■ IIIIIIIII■®®®IIIIIIIIIIIIII♦�-- d. Acceptance criteria pass/fail Yes No N/A (continued on back) Has required volume been removed ❑ ❑ M Has required turbidity been reached ® ❑ ❑ Have parameters stabilized PR,, ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: Peristaltic / Monsoon Sample ID Container Type No. of Containers Preservation Analysis Req. Time Comments 60 `5� 224 ODar oeJo y L ®r4 vt,c/G Signature 15 f rDate 1//slin Well ID: MW-102A Low Flow Ground Water Sample Collection Record lient: Abbott Date: U- 0 Time: Start jj 3d arra, pm roject No: 00005--024-400 Finish 1,209' a m to Location: Laurinburg, NC leather Conds: b 9- - G eg,-- Collector(s): D. Babineau / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length '30.6 ' c. Length of Water Column Q. y (a-b) b. Water Table Depth 1,2, � 3 " d. Calculated System Volume (see back) 2. WELL PURGE DATA a. Purge Method: Peristaltic / Monsoon Casing Diameter/Material 2" l PVL b. Acceptance Criteria defined (see workplan) Temperature 3% -D.O. 10% pH + 1.0 unit ORP + 10mV Sp. Cord, 3% Drawdown < Off c. Field Testing Equipment used: Make Model Serial Number YSI 556 Lamotte 2020 Volume Time Removed Temp. pH Spec. Cord. DO ORP Turbiditv Flow Rate Drawdown I Color/Odor tWhr\ /l ilnrot PPA I A-Rlent\ [;; /l\ m twTtn imi/min)(Teel) 00c) 9. 4�95 1170 9 '9,0 905 0 19,912 g 4s" /al 913 t• , ff 0.5b 45,2- .o� / . ys ' lays L`i. as' 169- 43 3, s� . z J.2. �l , d. Acceptance criteria pass/fail Yes No N/A (continued on back) . Has required volume been removed ❑ ❑ Has required turbidity been reached ® ❑ Have parameters stabilized [� ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: Peristaltic / Monsoon Sample ID Container Type No. of Containers Preservation Analysis Req. Time MW-102A %f9/i 9(4i1 5.2( 0' .% �t /-I9 -50 u Tuc Comments 7 Signature L /I( Algn(r' Date // C/-C)(I Well ID: MW-1 22B Low Flow Ground Water Sample Collection Record Client: Abbott Date: Time: Start /YU Q/pm Project No: 00005-024-400 Finish am/pm Site Location: Laurinbur , NC Weather Conds $ 4 C to Collector(s): ca i au)/ Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length L ,5� 6'' c. Length of Water Column T,3. S5 (a-b) Casing Diameter/Material b. Water Table Depth I L13, d. Calculated System Volume (see back) +7 2. WELL PURGE DA' a. Purge Method: ) / Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -DO. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cord. 3% Drawdown < 0.3, c. Field Testing Equipment used: Make YSI Model Serial Number .Volume Time Removed Temp. PH Spec. Cord. DO ORP Turbidity Flow Rate Drawdown Color/Odor Iona.) n �m.e� i^m hAlnnnN - (mn/I 1 (mv) (NTU) /ml/min)(Teel) �sllll�a��llllllllllll�lllllllllllll��®® d. Acceptance criteria pass/tail Yes NO N/A (conbnuea on oacK) Has required volume been removed ❑ ❑ �4 Has required turbidity been reached ❑ ❑ Have parameters stabilized ❑, ❑ ' If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: e—nsta I / Monsoon Sample ID Container Type No. of Containers Preservation Analysis Req. Time Ubde- Dedaa'A' vwa lri. Signature �` Date Well ID: MWA02C Low Flow Ground Water Sample Collection Record Client: Abbott Date: U°/ Time: Start 1.2 qd arnQg Project No: 00005-024-400 Finish am/pm Site Location: Laurinburg, NC Weather Conds: fo /4 ° Cleo,,— Collector(s): D. Babineau / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length IDS.— c. Length of Water Column 5(D.'Q (a-b) b. Water Table Depth d. Calculated System Volume (see back) 9 -)0 2. WELL PURGE DATA a. Purge Method: Peristaltic / Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cord. 3% Drawdown, < 0.3' c. Field Testing Equipment used: Make YSI' Model Casing Diameter/Material .2 " l A/C Serial Number Volume Time Removed Temp, pH Spec. Cond. DO ORP Turbidity Flow Ratel Drawdown 1. Color/Odor VlM-rtn (ml/mnlnA./14-1 I-M (I Alnml /mnln UT ee II���II���I�IIIILE.l���llllllll�� f�J1�1•I��.iI[�lir7�®Ill►I+Tc�'11111�$r'1■0��11111111//lam 111111G�'�_I�/�JIII��_�_I�IIIII��_�_IIIIIIIIIIII/� ®—ll_llllllllllll,--11111111111111111111111111111111111111111,—_— d. Acceptance criteria pass/fail Yes No N/A (continued on back) Has required volume been removed ® ❑ ❑ Has required turbidity been reached ® ❑ ❑ Have parameters stabilized 9 ❑, ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: Peristaltic / Monsoon Sample ID Container Type No. of Containers Preservation Analysis Req. Time Comments d',Cjk-,- J&YmlL re 2 �- /,0 mS%L Signature Date // �/'e,1 ARM Well ID: MW-103A Low Flow Ground Water Sample Collection Record Client: Abbott Date: II-q-og Time: Start W10 am m Project No: 00005-024-400 Finish am/pm Site Location: Laurinburg, NC Weather Conds: Collector(s): D. Babineau / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length 30 ' c. Length of Water Column g2n. I1(a-b) Casing Diameter/Material r� b. Water Table Depth d. Calculated System Volume (see back) 3, 2. WELL PURGE DATA a. Purge Method: Peristaltic / Monsoon b. Acceptance Criteria defined (see workplan) -Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model Serial Number YSI 556 Lamotte 2020 Volume Time Removed Temp. pH Spec. Cond. DO ORP TurbiditV Flow Ratel Drawdown Color/Odor 04hr1 11 itArcl !°Cl Gib/rml /mn/I.1 (mV) (NT0i (ml/min)[TeB11 llli���l��� r � llllll►7�_®�lllll�� IIIQJ�®l�ll���ll®lllll►���r =�1111111111�/� ®lllllll■ ®_ _ ®llllllllllllll■-® -lllllll■ lllllllllllll,-- llllllllllllll■ llllllllllllll■ _ � - llllllllllllll■-lllllll■lllllllllllll,-®llllllllllllll■llllllllllllllllll' ®® d. Acceptance criteria pass/fail Yes No N/A (continued on back) Has required volume been removed ❑ ❑ Has required turbidity been reached 0 ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: Peristaltic / Monsoon Sample ID Container Type No. of Containers Preservation Analysis Req. Time MW-103A ILIA 3 A�.L NaZ � line?:' Comments Signature N Date //.- q- Dd m WellID: MW-103B Low Flow Ground Water Sample Collection Record Client: Abbott Date: /j- U9 Time: Start 1�www�am/pm ,,,...//////��a��� Project No: 00005-024-400 Finish�am/pm Site Location: Laurinburg, NC Weather Conds: "700y L)AiVa Collector(s): abm Joe Ladd 1. WATER LEVEL DATA: (measured from Top of casing) a. Total Well Length 6 ,6 c. Length of Water Column V.Sl. (a-b) b. Water Table Depth 1? d. Calculated System Volume (see back) , S(, 2. WELL PURGE DATA a. Purge Method: F b. Acceptance Criteria defined (see workplan) -Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' Casing Diameter/Material N / 1 U( i c. Field Testing Equipment used: Make Model Serial Number YSI 556 d o8 Lamotte 2020 Volume Time Removed Temp. pH Spec. Cond. QO .' ORP Turbidity FlowRatel Drawdown I Color/Odor innw.n u.....� /-rl a,S/rm\ /inn/I 1 1m\h (NT11) (mVminl(Teel) li��r�G�3Tl :�FLrf1• � � I��.�.IIIIIIII,� �®C�AyY���C�d�yii���lY�f:�fll�.11lllllll,® '�"i' �i yam• t[;.'�2��.e1 �� iYl1'aC:�il���-��►Y ��✓�ia1J li>_■I>•11•IIIIIIIIIII,--It•It•IIII,_—� ii>_��Is-®It•It•ii•��� d. Acceptance Criteria passiTall Yes NO IV/H 9 Has required volume been removed ❑ ❑ Has required turbidity been reached 0 ❑ Have parameters stabilized ❑ ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: Sample ID Container Type No. of Containers fl MW-103B V Comments Preservation Icominueo on nacre/ Signature _ __ ei; Dater / 6`i. Time WeIIID: MW-1 33C Low Flow Ground Water Sample Collection Record Client: Abbott Date: //-q-02 Time: Start 101)O am/ m Project No: 00005-024-400 Finish Site Location: Laurinburg, NC Weather Conds: 1404CIe I�wlld/Ne Collector(s): D. Babineau / Joe Ladd 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length (5�S• c. Length of Water Column S/. (a-b) Casing Diameter/Material 2 � i RUC b. Water Table Depth 13. I d. Calculated System Volume (see back) ;? q& 2. WELL PURGE DATA a. Purge Method: (P b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing Equipment used: Make Model Serial Number YSI 556 Lamotte 2020 Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidi Plow Ratel Drawdown I Color/Odor (94hr) (I itarnl M.) hiS/cml (mo/L) (mV) (NTU) (ml/min) ee 111Y/(���ll���llll�®®�lllllllllllll/® ®-_--®lllllllllllllll, I"--� d. Acceptance criteria pass/fail Has required volume been removed Has required turbidity been reached Have parameters stabilized If no or N/A - Explain below. Yes ® ® �N No ❑ ❑ ❑ N/A ❑ ❑ ❑ (continued on back) 3. SAMPLE COLLECTION: Method: 6 istaltidMonsoon Sample ID Container Type No. of Containers Preservation MW-103C A -3 ); r Analysis Req, Time W6 Q r7lS Comments �.(7 t- Signature Date EN ff I Al COM I Well ID: MW-ID4A Low Flow Ground Water Sample Collection Record Client: Abbott Date: /1-1/-09 Time: Start /q-50 am/ Project No: 00005-024-400 Finish S 3o art p Site Location: Laurinburg Weather Cords: —L " Collector(s): D. 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length c. Length of Water Column .ij Sri (a-b) b. Water Table Depth'Ova3 d. Calculated System Volume (see back) 6, �2 � I 2. WELL PURGE DATA a. Purge Method: Peristaltic / Monsoon b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' Casing Diameter/Material a" / 19v c. Field Testing Equipment used: Make Model Serial Number YSI 556 Lamotte 2020 Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Rate Drawdown Color/Odor ;(24hr) (Liters) ('C) !uS/cml !mo/I.1 lmvl MTIn !ml/mint PP 1���r��s®��IIIII!•� llllllllle�lll�llllll�_�IIIIIIIII�II�—®��� a. Acceptance criteria pass/tail Has required volume been removed Has required turbidity been reached Have parameters stabilized If no or N/A - Explain below. Yes No ❑ ❑ ❑ N/A ❑ ❑ ❑ (continued on back) 3. SAMPLE COLLECTION: Method: Peristaltic / Monsoon Sample ID Container Type No. of Containers Preservation MW-104A _ 004 3 ]k I Analysis Req. Time hoo URIy) 2 / Z -5 Comments 145 Signature Date fl (/- O Well ID:xw _104(3 Low Flow Ground Water Sample Collection Record "lient: Abbott Date: 4 d°I Time: Start S73S am/pm 'roject No: 00005-024-400 Finish t 0-am/pm Site Location: Laurinburg, NC Neather Conds: e-go Collector(s): Babine u / Joe Ladd 1., WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length 4qS c. Length of Water Column 334(a-b) Casing Diameter/Material b. Water Table Depth d. Calculated System Volume tree back) as -6 S 2. WELL PURGE DATA a. Purge Method: Pe ' is / Monsoon b. Acceptance CriteNa defined (see workplah) - Temperature , 3% -DO. 10% - pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < Off c. Field Testing Equipment used: Make Model Serial Number YSI 556 �)da2w Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Rate Drawdown Color/Odor (24hr) (Liters) (*M (Us/cm) (ma/L) (mv) (NTU) (ml/min) ee Iff9M�Mffl�� lllllllllllllll,-lllllllll,lllllllllll,-®®®--- d. Acceptance criteria pass/tail Yes No N/ (continued on back) Has required volume been removed ❑ ❑ Has required turbidity been reached 0 ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: � s alt / Monsoon Sample ID Container Type No. of Containers Preservation AnalysisAeq. Time Comments �fir.®ww l! Signaturek T7 Date ��All � l Well ID: /� 1 Low Flow Ground Water Sample Collection Record Client: Abbott Date: ///JOI Time: Start lgS5 am/pm Project No: 00005-024-400 Finish 1,14 am/pm Site Location: Laurinburg, NC WeatherConds: M 71"IFSt/wW Collector(s): abineau Joe Ladd 1. WAI EK LEVEL DA I A: (Measured trom: I Opof casing) a. Total Well Length -741 c. Length of Water Colum J S (a-b) Casing Diameter/Material a 11, / b. Water Table Depth 3I ras d. Calculated System Volume (see back) 51tJ.5 2. WELL PURGE DAT a. Purge Method: Pe istalt' / Monsoon b. Acceptance Criteria defined (see workplan) -Temperature 3% -DO. 10% -pH + 1.0 unit ORP + 10mV - Sp. Cond. 3% Drawdown < 0.3' c. Field Testing Equipment used: i Make Model Serial Number YSI 556 910W1 Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Ratel Drawdown I Color/Odor (24hr) (Liters) (°C) (us1cm) (mo/L) (mV) 7FTE (ml/min) i tee 1111111 M. RAW. I MI d. Acceptance criteria pass7fail Yes No N/A Has required volume been removed ❑ ❑ 69 Has required turbidity been reached ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Sample ID Container Type No. of Containers Comments Signature / Monsoon (continued on back) Req. Time Date /)Zg1J`1 AECOM Environment Appendix B Laboratory Analytical Reports (November 2009 Groundwater Samples) 60135880 February 2010 aceAnalytical —pacelabs.com November 23, 2009 Mr. Grant Watkins AECOM Environment 7041 Old Wake Forest Road Raleigh, NC 27616 RE: Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Dear Mr. Watkins: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 06, 2009. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Brandon Helton brandon.helton@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 34 acmnalytical www.pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Minnesota Certification IDs Alaska Certification #: UST-078 Arizona Certification #: AZ-0014 1700 Elm Street SE, Suite 200 Minneapolis, MN Wisconsin Certification #: 999407970 Washington Certification #: C754 Tennessee Certification #: 02818 Pennsylvania Certification #: 68-00563 Oregon Certification #: MN200001 North Dakota Certification #: R-036 North Carolina Certification #: 530 New York Certification #: 11647 Asheville Certification IDs North Carolina Wastewater Certification #: 40 2225 Riverside Dr. Asheville, NC 28804 North Carolina Bioassay Certification #: 9 New Jersey Certification #: NC011 Massachusetts Certification #: M-NC030 Louisiana/LELAP Certification #: 03095 Florida/NELAP Certification #: E87648 Connecticut Certification #: PH-0106 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS New Jersey Certification #: MN-002 Montana Certification #: MT CERT0092 55414 Minnesota Certification #: 027-053-137 Maine Certification #: 2007029 Louisiana Certification #: 03086 California Certification #: 01155CA Florida/NELAP Certification #: E87605 Illinois Certification #: 200011 Iowa Certification #: 368 Kansas Certification #: E-10167 Louisiana Certification #: LA080009 West Virginia Certification #: 356 Virginia Certification #: 00072 Tennessee Certification #: 2980 South Carolina Certification #: 99030001 South Carolina Bioassay Certification #: 99030002 Pennsylvania Certification #: 68-03578 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. A-o1 9 c �®x Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 34 aceAnalytical —pacelabsxom Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Lab ID Sample ID Matrix Date Collected Date Received 9257024001 MW-101B Water 11/05/0909:25 11/06/09 16:45 9257024002 MW-102B Water 11/04/0912:20 11/06/09 16:45 9257024003 MW-101A Water 11/05/09 09:30 11/06/09 16:45 9257024004 MW-103B Water 11/04/0916:40 11/06/09 16:45 9257024005 MW-104B Water 11/04/0916:05 11/06/09 16:45 9257024006 MW-16B Water 11/03/0914:25 11/06/09 16:45 9257024007 MW-16D Water 11/03/0914:40 11/06/09 16:45 9257024008 MW-100B Water 11/05/0911:00 11/06/09 16:45 9257024009 MW-102A Water 11/04/0912:20 11/06/09 16:45 9257024010 MW-102C Water 11/04/0913:10 11/06/09 16:45 9257024011 MW-103A Water 11/04/0916:25 11/06/09 16:45 9257024012 MW-103C Water 11/04/0912:15 11/06/09 16:45 9257024013 MW-104A Water 11/04/0915:20 11/06/09 16:45 9257024014 MW-104C Water 11/04/0915:15 11/06/09 16:45 9257024015 DUP-1 Water 11/03/0915:35 11/06/09 16:45 9257024016 DUP-2 Water 11/04/0917:20 11/06/09 16:45 9257024017 MW-10B Water 11/03/0915:30 11/06/09 16:45 9257024018 MW-10D Water 11/03/0915:40 11/06/09 16:45 9257024019 MW-18B Water 11/04/09 09:25 11/06/09 16:45 9257024020 MW-18D Water 11/04/09 09:20 11/06/09 16:45 9257024021 MW-19B Water 11/03/0916:40 11/06/09 16:45 9257024022 MW-19D Water 11/03/0916:30 11/06/09 16:45 9257024023 MW-20B Water 11/03/0912:20 11/06/09 16:45 9257024024 MW-20D Water 11/03/0912:20 11/06/09 16:45 9257024025 MW-100A Water 11/05/0910:55 11/06/09 16:45 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 34 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100 www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: FORMER ABBOTT LABS 9257024 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 9257024001 MW-101B RSK 175 CJR 3 PASI-M SM 2320B TEE 1 PASI-A SM 5310B SAJ 1 PASI-A 9257024002 MW-102B RSK 175 CJR 3 PASI-M SM 2320B TEE 1 PASI-A SM 5310B SAJ 1 PASI-A 9257024003 MW-101A RSK 175 CJR 3 PASI-M SM 2320B TEE 1 PASI-A SM 5310B SAJ 1 PASI-A 9257024004 MW-103B RSK 175 CJR 3 PASI-M SM 5310B SAJ 1 PASI-A 9257024005 MW-104B RSK 175 CJR 3 PASI-M SM 2320B TEE 1 PASI-A SM 5310B SAJ 1 PASI-A 9257024006 MW-16B SM 2320B TEE 1 PASI-A SM 5310B SAJ 1 PASI-A 9257024007 MW-16D SM 2320B TEE 1 PASI-A SM 5310B SAJ 1 PASI-A 9257024008 MW-100B RSK 175 CJR 3 PASI-M SM 5310B SAJ 1 PASI-A 9257024009 MW-102A SM 5310B SAJ 1 PASI-A 9257024010 MW-102C SM 5310B SAJ 1 PASI-A 9257024011 MW-103A SM 5310B SAJ 1 PASI-A 9257024012 MW-103C SM 5310B SAJ 1 PASI-A 9257024013 MW-104A SM 5310B SAJ 1 PASI-A 9257024014 MW-104C SM 5310B SAJ 1 PASI-A 9257024015 DUP-1 SM 5310B SAJ 1 PASI-A 9257024016 DUP-2 SM 5310B SAJ 1 PASI-A 9257024017 MW-10B SM 5310B SAJ 1 PASI-A 9257024018 MW-10D SM 5310B SAJ 1 PASI-A 9257024019 MW-18B SM 5310B SAJ 1 PASI-A 9257024020 MW-18D SM 5310B SAJ 1 PASI-A 9257024021 MW-19B SM 5310B SAJ 1 PASI-A 9257024022 MW-19D SM 5310B SAJ 1 PASI-A 9257024023 MW-20B SM 5310B SAJ 1 PASI-A 9257024024 MW-20D SM 5310B SAJ 1 PASI-A 9257024025 MW-100A SM 5310B SAJ 1 PASI-A REPORT OF LABORATORY ANALYSIS Page 4 of 34 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-101B Parameters Lab ID: 9257024001 Collected: 11/05/09 09:25 Results Units Report Limit DF Received: 11/06/09 16:45 Matrix: Water Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane ND ug/L 10.0 1 11/12/0915:50 74-84-0 Ethene ND ug/L 10.0 1 11/12/0915:50 74-85-1 Methane ND ug/L 10.0 1 11/12/0915:50 74-82-8 pH 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 34.6 mg/L 5.0 1 11/13/09 20:44 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 8.6 mg/L 1.0 1 11/12/09 10:34 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 34 aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-102B Parameters Lab ID: 9257024002 Collected: 11/04/09 12:20 Results Units Report Limit DF Received: 11/06/09 16:45 Matrix: Water Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane ND ug/L 10.0 1 11/12/0916:16 74-84-0 Ethene ND ug/L 10.0 1 11/12/0916:16 74-85-1 Methane 2320 ug/L 10.0 1 11/12/0916:16 74-82-8 E,pH 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 22.4 mg/L 5.0 1 11/13/09 20:43 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 5.3 mg/L 1.0 1 11/11/09 00:18 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 34 aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-101A Parameters Lab ID: 9257024003 Collected: 11/05/09 09:30 Results Units Report Limit DF Received: 11/06/09 16:45 Matrix: Water Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane ND ug/L 10.0 1 11/12/0916:41 74-84-0 Ethene ND ug/L 10.0 1 11/12/0916:41 74-85-1 Methane 285 ug/L 10.0 1 11/12/0916:41 74-82-8 pH 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 67.1 mg/L 5.0 1 11/13/09 20:44 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 23.5 mg/L 1.0 1 11/12/09 10:51 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 34 aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-103B Parameters Lab ID: 9257024004 Collected: 11/04/09 16:40 Results Units Report Limit DF Received: 11/06/09 16:45 Matrix: Water Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane ND ug/L 10.0 1 11/12/0917:07 74-84-0 Ethene 27.2 ug/L 10.0 1 11/12/0917:07 74-85-1 Methane 2410 ug/L 10.0 1 11/12/0917:07 74-82-8 E,pH 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.7 mg/L 1.0 1 11/11/09 00:39 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 34 aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-104B Parameters Lab ID: 9257024005 Collected: 11/04/09 16:05 Results Units Report Limit DF Received: 11/06/09 16:45 Matrix: Water Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane ND ug/L 10.0 1 11/12/0917:32 74-84-0 Ethene ND ug/L 10.0 1 11/12/0917:32 74-85-1 Methane 52.2 ug/L 10.0 1 11/12/0917:32 74-82-8 pH 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 ND mg/L 5.0 1 11/13/09 20:43 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.0 mg/L 1.0 1 11/11/09 00:49 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 34 aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16B Lab ID: 9257024006 Collected: 11/03/09 14:25 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 6.1 mg/L 5.0 1 11/13/09 20:42 5310E TOC Analytical Method: SM 5310B Total Organic Carbon 2.9 mg/L 1.0 1 11/11/09 00:58 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 34 aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16D Lab ID: 9257024007 Collected: 11/03/09 14:40 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 32.5 mg/L 5.0 1 11/13/09 20:42 5310E TOC Analytical Method: SM 5310B Total Organic Carbon 1.2 mg/L 1.0 1 11/11/09 01:08 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 34 aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-100B Lab ID: 9257024008 Collected: 11/05/09 11:00 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane ND ug/L 10.0 1 11/12/0917:58 74-84-0 Ethene 14.4 ug/L 10.0 1 11/12/0917:58 74-85-1 Methane 4210 ug/L 10.0 1 11/12/0917:58 74-82-8 E,pH 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 18.7 mg/L 1.0 1 11/12/09 11:00 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-102A Lab ID: 9257024009 Collected: 11/04/09 12:20 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 95.3 mg/L 4.0 4 11/19/09 14:52 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 13 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-102C Lab ID: 9257024010 Collected: 11/04/09 13:10 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.7 mg/L 1.0 1 11/19/09 15:13 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 34 aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-103A Lab ID: 9257024011 Collected: 11/04/09 16:25 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Total Organic Carbon Date: 11/23/2009 01:11 PM Analytical Method: SM 5310B 3.9 mg/L 1.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 11/19/0915:32 7440-44-0 Page 15 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-103C Lab ID: 9257024012 Collected: 11/04/09 12:15 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 29.1 mg/L 1.0 1 11/19/09 15:48 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-104A Lab ID: 9257024013 Collected: 11/04/09 15:20 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.9 mg/L 1.0 1 11/19/09 16:33 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 17 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-104C Lab ID: 9257024014 Collected: 11/04/09 15:15 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.1 mg/L 1.0 1 11/19/09 16:42 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 18 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: DUP-1 Lab ID: 9257024015 Collected: 11/03/09 15:35 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.6 mg/L 1.0 1 11/19/09 16:52 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 19 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: DUP-2 Lab ID: 9257024016 Collected: 11/04/09 17:20 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.1 mg/L 1.0 1 11/19/09 17:01 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 20 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-10B Lab ID: 9257024017 Collected: 11/03/09 15:30 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.0 mg/L 1.0 1 11/19/09 17:13 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 21 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-10D Lab ID: 9257024018 Collected: 11/03/09 15:40 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 6.2 mg/L 1.0 1 11/19/09 17:22 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 22 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-18B Lab ID: 9257024019 Collected: 11/04/09 09:25 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1 11/19/09 17:32 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 23 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-18D Lab ID: 9257024020 Collected: 11/04/09 09:20 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.3 mg/L 1.0 1 11/19/09 17:41 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 24 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-19B Lab ID: 9257024021 Collected: 11/03/09 16:40 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.5 mg/L 1.0 1 11/19/09 17:51 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 25 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-19D Lab ID: 9257024022 Collected: 11/03/09 16:30 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.1 mg/L 1.0 1 11/19/09 18:00 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 26 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-20B Lab ID: 9257024023 Collected: 11/03/09 12:20 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.7 mg/L 1.0 1 11/19/09 18:39 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 27 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-20D Lab ID: 9257024024 Collected: 11/03/09 12:20 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon ND mg/L 1.0 1 11/19/09 18:50 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 28 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Sample: MW-100A Lab ID: 9257024025 Collected: 11/05/09 10:55 Received: 11/06/09 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 329 mg/L 15.0 15 11/20/09 09:54 7440-44-0 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 29 of 34 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100 www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ABBOTT LABS Pace Project No.: 9257024 QC Batch: WET/10465 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320E Alkalinity Associated Lab Samples: 9257024001, 9257024002, 9257024003, 9257024005, 9257024006, 9257024007 METHOD BLANK: 365709 Matrix: Water Associated Lab Samples: 9257024001, 9257024002, 9257024003, 9257024005, 9257024006, 9257024007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 mg/L ND 5.0 11/13/09 20:41 LABORATORY CONTROL SAMPLE: 365710 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 49.3 99 90-110 SAMPLE DUPLICATE: 365711 9257024006 Dup Max Parameter Units Result Result RPD RPD Qualifiers Alkalinity, Total as CaCO3 mg/L 6.1 6.1 0 20 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 30 of 34 aceAnalytical —pacelabs.com Project: FORMER ABBOTT LABS Pace Project No.: 9257024 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: AIR/9370 Analysis Method: RSK 175 QC Batch Method: RSK 175 Analysis Description: RSK 175 AIR HEADSPACE Associated Lab Samples: 9257024001, 9257024002, 9257024003, 9257024004, 9257024005, 9257024008 METHOD BLANK: 712405 Matrix: Water Associated Lab Samples: 9257024001, 9257024002, 9257024003, 9257024004, 9257024005, 9257024008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethane ug/L ND 10.0 11/12/0914:08 Ethene ug/L ND 10.0 11/12/0914:08 Methane ug/L ND 10.0 11/12/0914:08 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE & LCSD: 712406 712407 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Ethane ug/L 114 141 135 124 119 70-130 4 30 Ethene ug/L 106 134 126 126 118 70-130 7 30 Methane ug/L 60.7 75.9 72.6 125 120 70-130 4 30 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 31 of 34 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100 www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ABBOTT LABS Pace Project No.: 9257024 QC Batch: WETA/6228 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 9257024001, 9257024002, 9257024003, 9257024004, 9257024005, 9257024006, 9257024007, 9257024008 METHOD BLANK: 364017 Matrix: Water Associated Lab Samples: 9257024001, 9257024002, 9257024003, 9257024004, 9257024005, 9257024006, 9257024007, 9257024008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 11/10/09 20:16 LABORATORY CONTROL SAMPLE: 364018 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 23.2 93 90-110 MATRIX SPIKE SAMPLE: 364019 9256946003 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L ND 25 26.0 102 75-125 MATRIX SPIKE SAMPLE: 364021 9256946013 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 4.3 25 28.2 96 75-125 SAMPLE DUPLICATE: 364020 9256946004 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 4.7 4.7 0 20 SAMPLE DUPLICATE: 364022 9256946014 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 4.3 4.3 0 20 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 32 of 34 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100 www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ABBOTT LABS Pace Project No.: 9257024 QC Batch: WETA/6285 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 9257024009,9257024010,9257024011,9257024012,9257024013,9257024014,9257024015,9257024016, 9257024017,9257024018,9257024019,9257024020,9257024021,9257024022,9257024023,9257024024, 9257024025 METHOD BLANK: 368721 Matrix: Water Associated Lab Samples: 9257024009,9257024010,9257024011,9257024012,9257024013,9257024014,9257024015,9257024016, 9257024017,9257024018,9257024019,9257024020,9257024021,9257024022,9257024023,9257024024, 9257024025 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 11/19/09 14:19 LABORATORY CONTROL SAMPLE: 368722 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 23.1 92 90-110 MATRIX SPIKE SAMPLE: 368723 9257024009 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 95.3 25 114 75 75-125 MATRIX SPIKE SAMPLE: 368724 9257024010 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 1.7 25 27.3 102 75-125 SAMPLE DUPLICATE: 368725 9257024011 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 3.9 4.0 1 20 SAMPLE DUPLICATE: 368726 9257024012 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 29.1 29.3 1 20 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 33 of 34 aceAnalytical _pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 QUALIFIERS Project: FORMER ABBOTT LABS Pace Project No.: 9257024 DEFINITIONS (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference k MEMO Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. U - Indicates the compound was analyzed for, but not detected. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-M Pace Analytical Services - Minneapolis ANALYTE QUALIFIERS E Analyte concentration exceeded the calibration range. The reported result is estimated. pH Post -analysis pH measurement indicates insufficient VOA sample preservation. (704)875-9092 Date: 11/23/2009 01:11 PM REPORT OF LABORATORY ANALYSIS Page 34 of 34 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. feys to n ��vc M E M B E R e LABORATORIES, INC. rleac 13 November 2009 Brandon Helton Pace Analytical -NC 9800 Kincey Ave. Ste. 100 Huntersville, NC 28078 RE: Subcontract 9257024 Enclosed are the results of analyses for samples received by the laboratory on 11/10/09 12:15. If you have any questions concerning this report, please feel free to contact me at 1-800-858-5227. ANALYTICAL REPORT FOR SAMPLES Client Sample ID Laboratory ID Matrix Date Sampled Date Received MW-101B 19KO439-01 Water 11/05/09 09:25 11/10/09 12:15 MW-102B 19KO439-02 Water 11/04/0912:20 11/10/09 12:15 MW-101A 19KO439-03 Water 11/05/09 09:30 11/10/09 12:15 MW-103B 19KO439-04 Water 11/04/0916:40 11/10/09 12:15 Client Supplied Containers The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must be reproduced in its entirety. Page 1 of 10 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 IL'feystone O 9O \q�c. ., t' v.; '9ti� M E M B E R �o LABORATORIES, INC. pie Pace Analytical -NC Project: Subcontract Reported 9800 Kincey Ave. Ste. 100 Project Number: 9257024 11/13/09 10:41 Huntersville NC, 28078 Project Manager: Brandon Helton J Z CD Ac 0) N G W E _: ':. N C O p N CDN N m d y 'a d N N t� K' p; r 6 1 y 7 3x, C E � { C o c G v \ l�1 _ 0 r 2 tJ +G m —90 m ¢ Oa Cl- _ 0 In of Q C N N O N O M a N R y / 0 0 0 0 ,6 O rv, tf O N O U N 10 O U O ,p d C> i W Ud m In U N O O L > U 0] ccQ m pNj C2 d C U � U Q Z. O y v c= ma m c c u�i n` Q w 16 O m o c o loco = E E A Q' (D a- m= d W The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must he reproduced in its entirety. Page 2 of 10 Phone 641-792-8451 600 East 17th Street South Newton, IA 50208 Fax 641-792-7989 feys ACCC9O to n LABORATORIES, INC. U �el--c Pace Analytical -NC Project: Subcontract Reported 9800 Kincey Ave. Ste. 100 Project Number: 9257024 11/13/09 10:41 Huntersville NC, 28078 Project Manager: Brandon Helton MW-101B 19K0439-01 (Water) Date Sampled:11/5/2009 9:25:OOAM Reporting Analyte Result Limrt Units Dilution Batch Prepared Analyzed Method Notes Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Acetic Acid (C2) 45.1 1.0 mg/1 1 1K91307 11/12/09 11/12/09 BPLC/UV Butyric Acid (C4) 25.7 1.0 " Lactic Acid (0) ND 1.0 " Propionic Acid (C3) 53.6 1.0 " Pyruvic Acid (0) ND 0.1 " The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must be reproduced in its entirety. Page 3 of 10 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 feys ACCC9O to n LABORATORIES, INC. U �el--c Pace Analytical -NC Project: Subcontract Reported 9800 Kincey Ave. Ste. 100 Project Number: 9257024 11/13/09 10:41 Huntersville NC, 28078 Project Manager: Brandon Helton MW-102B 19K0439-02 (Water) Date Sampled:11/4/2009 12:20:OOPM Reporting Analyte Result Limrt Units Dilution Batch Prepared Analyzed Method Notes Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Acetic Acid (C2) ND 1.0 mg/1 1 1K91307 11/12/09 11/13/09 BPLC/UV Butyric Acid (C4) ND 1.0 " Lactic Acid (0) ND 1.0 " Propionic Acid (0) ND 1.0 " Pyruvic Acid (0) ND 0.1 " The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must be reproduced in its entirety. Page 4 of 10 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 feys ACCC9O to n LABORATORIES, INC. U �el--c Pace Analytical -NC Project: Subcontract Reported 9800 Kincey Ave. Ste. 100 Project Number: 9257024 11/13/09 10:41 Huntersville NC, 28078 Project Manager: Brandon Helton MW-101A 19K0439-03 (Water) Date Sampled:11/5/2009 9:30:OOAM Reporting Analyte Result Limrt Units Dilution Batch Prepared Analyzed Method Notes Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Acetic Acid (C2) 40.1 1.0 mg/1 1 1K91307 11/12/09 11/13/09 BPLC/UV Butyric Acid (C4) 5.5 1.0 " Lactic Acid (0) ND 1.0 " Propionic Acid (C3) 32.7 1.0 " Pyruvic Acid (0) ND 0.1 " The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must be reproduced in its entirety. Page 5 of 10 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 feys ACCC9O to n LABORATORIES, INC. U �el--c Pace Analytical -NC Project: Subcontract Reported 9800 Kincey Ave. Ste. 100 Project Number: 9257024 11/13/09 10:41 Huntersville NC, 28078 Project Manager: Brandon Helton MW-103B 19KO439-04 (Water) Date Sampled:11/4/2009 4:40:OOPM Reporting Analyte Result Limrt Units Dilution Batch Prepared Analyzed Method Notes Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Acetic Acid (C2) ND 1.0 mg/1 1 1K91307 11/12/09 11/13/09 BPLC/UV Butyric Acid (C4) ND 1.0 " Lactic Acid (0) ND 1.0 " Propionic Acid (0) ND 1.0 " Pyruvic Acid (0) ND 0.1 " The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must be reproduced in its entirety. Page 6 of 10 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 feys ACCC9O to n LABORATORIES, INC. U �el--c Pace Analytical -NC Project: Subcontract Reported 9800 Kincey Ave. Ste. 100 Project Number: 9257024 11/13/09 10:41 Huntersville NC, 28078 Project Manager: Brandon Helton Determination of Metabolic Acids - Quality Control Keystone Laboratories, Inc. - Newton Reporting Spike Source %REC RPD malyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch 19K1301 - 1K91307 Calibration Check (19K1301-CCVI) Prepared & Analyzed: 11/12/09 Pyruvic Acid (C3) 24.12 m9/1 22.5000 107 80-120 Lactic Acid (0) 115.2 97.5000 118 80-120 Acetic Acid (C2) 97.22 107.200 90.7 80-120 Propionic Acid(C3) 96.74 107.400 90.1 80-120 Butyric Acid (C4) 94.64 103.200 91.7 80-120 Calibration Check (19K1301-CCV2) Prepared: 11/12/09 Analyzed: 11/13/09 Pyruvic Acid (0) 19.48 m9/1 22.5000 86.6 80-120 Lactic Acid(C3) 101.3 97.5000 104 80-120 Acetic Acid (C2) 116.1 107.200 108 80-120 Propionic Acid(C3) 105.6 107.400 98.4 80-120 Butyric Acid (C4) 102.2 103.200 99.0 80-120 Batch 1K91307 - General Preq HPLC/IC Blank (1K91307-BLK1) Prepared & Analyzed: 11/12/09 Pyruvic Acid (C3) ND 0.1 mg/l Lactic Acid (0) ND 1.0 " Acetic Acid (C2) ND 1.0 Propionic Acid (0) ND 1.0 " Butyric Acid (C4) ND 1.0 " LCS (1K91307-BS1) Prepared & Analyzed: 11/12/09 Pyruvic Acid (0) 14.06 0.1 mg/1 12.4000 113 79-128 Lactic Acid (0) 97.49 1.0 95.5400 102 82-127 Acetic Acid (C2) 103.2 1.0 104.400 98.8 90-115 Propionic Acid (0) 93.82 1.0 107.400 87.4 82-115 Butyric Acid (C4) 96.48 1.0 104.900 92.0 90-111 The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must be reproduced in its entirety. Page 7 of 10 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 feys ACCC9O to n LABORATORIES, INC. U �el--c Pace Analytical -NC Project: Subcontract Reported 9800 Kincey Ave. Ste. 100 Project Number: 9257024 11/13/09 10:41 Huntersville NC, 28078 Project Manager: Brandon Helton Determination of Metabolic Acids - Quality Control Keystone Laboratories, Inc. - Newton Reporting Spike Source %REC RPD malyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch 1K91307 - General Prep HPLC/IC Matrix Spike (1K91307-MS1) Source: 19KO316-01 Prepared: 11/12/09 Analyzed: 11/13/09 Pyruvic Acid (C3) 14.26 0.1 m9/1 12.4000 ND 115 68-132 Lactic Acid (0) 105.7 1.0 95.5400 ND 111 77-128 Acetic Acid (C2) 111.0 1.0 104.400 ND 106 81-127 Propionic Acid (0) 105.3 1.0 107.400 ND 98.0 83-115 Butyric Acid (C4) 105.6 1.0 104.900 ND 101 85-115 Matrix Spike Dup (1K91307-MSD1) Source: 19KO316-01 Prepared: 11/12/09 Analyzed: 11/13/09 Pyruvic Acid (0) 14.35 0.1 m9/1 12.4000 ND 116 68-132 0.615 16 Lactic Acid (0) 100.6 1.0 95.5400 ND 105 77-128 4.85 16 Acetic Acid (C2) 110.0 1.0 104.400 ND 105 81-127 0.894 15 Propionic Acid(C3) 113.8 1.0 107.400 ND 106 83-115 7.75 10 Butyric Acid (C4) 105.4 1.0 104.900 ND 100 85-115 0.236 12 Certified Analyses Included in This Report Method/Matrix Analvte Certifientinnc Code Certifying Authority IA-NT Iowa Department of Natural Resources KS-NT Kansas Department of Health and Environment NELAC New Jersey Department of Environmental Protection Certificate Number Expires 095 02/01/2010 E-10287 07/31/2010 IA001 06/30/2010 The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must be reproduced in its entirety. Page 8 of 10 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 feys ACCC9O to n LABORATORIES, INC. U �el--c Pace Analytical -NC Project: Subcontract Reported 9800 Kincey Ave. Ste. 100 Project Number: 9257024 11/13/09 10:41 Huntersville NC, 28078 Project Manager: Brandon Helton Notes and Definitions DET Analyte DETECTED ND Analyte NOT DETECTED at or above the reporting limit NR Not Reported dry Sample results reported on a dry weight basis RPD Relative Percent Difference The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must be reproduced in its entirety. Page 9 of 10 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 feys ACCC9O to n LABORATORIES, INC. U �el--c Pace Analytical -NC Project: Subcontract Reported 9800 Kincey Ave. Ste. 100 Project Number: 9257024 11/13/09 10:41 Huntersville NC, 28078 Project Manager: Brandon Helton Sue Thompson Project Manager I The results in this report apply to the samples analyzed in accordance with the Chain -of -Custody record. This analytical report must be reproduced in its entirety. Page 10 of 10 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Global Environment, Health and Safety Laboratory c} NELAC Accredited Illinois Accreditation No.: 100310 New Jersey Accreditation No.: IL005 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Page 1 of 104 Report Date: 24-Nov-09 Lab Project Number: 301917 Sample Group Number: E302694 Enclosed is the analytical report for the following samples submitted to Abbott Global Environment, Health and Safety Laboratory of Abbott Park for analysis. Project Description: Laurinburg, NC Field Sample No. Sample 1 317136 TB-0023 317137 MW-20B 317138 MW-20D 317139 Dup-1 317140 MW-10D 317141 MW-16B 317142 MW-16D 317143 MW-10B 317144 MW-19D 317145 MW-19B 317146 EB-1 317147 MW-18D 317148 MW-18B 317149 MW-102A 317151 MW-102B 317153 MW-102C 317155 MW-104A MS 317156 MW-104A MSD 317157 MW-104C Abbott 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 Date/Time Taken 27-Oct-09 1:26 PM 3-Nov-09 12:20 PM 3-Nov-09 12:20 PM 3-Nov-09 1:35 PM 3-Nov-09 1:40 PM 3-Nov-09 2:25 PM 3-Nov-09 2:40 PM 3-Nov-09 3:30 PM 3-Nov-09 4:30 PM 3-Nov-09 4:40 PM 3-Nov-09 5:00 PM 4-Nov-09 9:20 AM 4-Nov-09 9:25 AM 4-Nov-09 12:20 PM 4-Nov-09 12:20 PM 4-Nov-09 1:10 PM 4-Nov-09 3:15 PM 4-Nov-09 3:15 PM CS►rM1>*199 iiBiZ!�kyi Date/Time Received 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM ra ► maI> r1 `111116y_u• Environmental Lab Report �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. 317158 317159 317160 317161 317162 317163 317164 317165 317167 317169 317171 Global Environment, Health and Safety Laboratory MW-104A MW-104B MW-103A MW-103B EB-2 MW-103C Dup-2 MW-101 B MW-101A MW-100A MW-100B Sample Descrip c} NELAC Accredited Illinois Accreditation No.: 100310 New Jersey Accreditation No.: IL005 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Date/Time Taken 4-Nov-09 3:20 PM 4-Nov-09 4:05 PM 4-Nov-09 4:25 PM 4-Nov-09 4:40 PM 4-Nov-09 5:10 PM 4-Nov-09 5:15 PM 4-Nov-09 5:25 PM 5-Nov-09 9:25 AM 5-Nov-09 9:30 AM 5-Nov-09 11:00 AM Report Date: 24-Nov-09 Lab Project Number: 301917 Sample Group Number: E302694 Case Narrative Sample Receipt - Samples were received on ice at a temperature of 1.2 degrees celsius. EPA method 8260B - There were no QA exceptions to note. Date/Time Received 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM 7-Nov-09 10:05 AM Page 2 of 104 Sample Analysis in support of the project referenced above has been completed and results are presented on the following pages. These results apply only to the samples analyzed. Reproduction of this report only in whole is permitted. Procedures used follow Abbott Standard Operating Procedures which reference the methods listed in your report. Approved by: BRIAN WANNER MANAGERII Date: 24-Nov-09 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317136 TB-0023 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,1,1,2-TETRACHLOROETHANE 1,1,1-TRICH LOROETHAN E 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICH LOROETHAN E 1,1-DICHLOROETHANE 1,1-DICHLOROETHYLENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 3 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317136 TB-0023 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 4 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317136 TB-0023 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 5 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317136 TB-0023 Method: EPA 8260B 317143 MW-10B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 8-Nov-09 BW < 0.005 MG/L 0.005 8-Nov-09 BW < 0.005 MG/L 0.005 8-Nov-09 BW < 0.001 MG/L 0.001 8-Nov-09 BW 104 % 86-115 8-Nov-09 BW 100 % 86-118 8-Nov-09 BW 98 % 88-110 8-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE 0.009 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.001 MG/L 0.001 12-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.005 MG/L 0.005 12-Nov-09 BW 1,2-DIBROMOETHANE <0.001 MG/L 0.001 12-Nov-09 BW Page 6 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317143 MW-10B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 7 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317143 MW-10B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 0.087 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 0.002 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 8 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317143 MW-10B Method: EPA 8260B 317140 MW-10D Global Environment, Health and Safety Laboratory c} NELAC Accredited Illinois Accreditation No.: 100310 New Jersey Accreditation No.: IL005 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter PERCH LOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units < 0.001 MG/L < 0.001 MG/L < 0.001 MG/L < 0.001 MG/L < 0.001 MG/L < 0.001 MG/L < 0.001 MG/L 0.0035 MG/L < 0.001 MG/L 0.64 MG/L < 0.005 MG/L 0.0012 MG/L 95 % 98 % 96 % Reporting Limit 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.005 0.005 0.001 86-115 86-118 88-110 Report Date: 24-Nov-09 Lab Project Number: 301917 Sample Group Number: E302694 Date Analyzed 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 iVZ 41remiIll Analyst Initials Additional Info BW BW BW BW BW BW BW BW BW BW BW BW 1,1,1,2-TETRACHLOROETHANE 1,1,1-TRICHLOROETHANE <0.001 <0.001 MG/L MG/L 0.001 0.001 12-Nov-09 12-Nov-09 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 1,1-DICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW BW BW BW BW BW BW BW Page 9 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317140 MW-10D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,1-DICHLOROETHYLENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 0.01 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 10 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317140 MW-10D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 0.0013 MG/L 0.001 < 0.001 MG/L 0.001 0.13 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 11 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317140 MW-10D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLU0ROM ETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 0.0024 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 0.0047 MG/L 0.001 < 0.001 MG/L 0.001 0.82 MG/L 0.005 < 0.005 MG/L 0.005 0.002 MG/L 0.001 97 % 86-115 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 12 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 Global Environment, Health and Safety Laboratory c} CURTIS MICHOLS Company Name: ABBOTT NELAC Accredited Report Date: 24-Nov-09 Sampling Division: GES Illinois Accreditation No.: 100310 Lab Project Number: 301917 Sampling Site: OTHER New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 Sampling Dept.: DEA Registration No.: RA0218784 Field Sample No. Sample Description Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 317140 MW-10D DIBROMOFLUOROMETHANE (SURR) 97 % 86-118 12-Nov-09 BW TOLUENE-D8 (SURR) 99 1 % 88-110 12-Nov-09 BW Method: EPA 8260B _ 317141 MW-16B 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.001 MG/L 0.001 12-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.005 MG/L 0.005 12-Nov-09 BW 1,2-DIBROMOETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROPROPANE <0.001 MG/L 0.001 12-Nov-09 BW 1,3,5-TRIMETHYLBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,3-DICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW Page 13 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317141 MW-16B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 0.0034 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 14 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317141 MW-16B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 0.0012 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 15 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317141 MW-16B Method: EPA 8260B 317142 MW-16D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW 0.036 MG/L 0.005 12-Nov-09 BW < 0.005 MG/L 0.005 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW 96 % 86-115 12-Nov-09 BW 98 % 86-118 12-Nov-09 BW 99 % 88-110 12-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW Page 16 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317142 MW-16D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 17 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317142 MW-16D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 0.0038 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 18 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317142 MW-16D Method: EPA 8260B 317148 MW-18B Abbott 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW 0.0058 MG/L 0.005 12-Nov-09 BW < 0.005 MG/L 0.005 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW 94 % 86-115 12-Nov-09 BW 96 % 86-118 12-Nov-09 BW 98 % 88-110 12-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L _ 0.001 9-Nov-09 BW Page 19 of 104 Environmental Lab Report �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317148 MW-18B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICH LOROETHAN E 1,1-DICHLOROETHANE 1,1-DICHLOROETHYLENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPAN E 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 20 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317148 MW-18B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 21 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317148 MW-18B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROM ETHANE TRICHLOROTRI FLUOROETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 22 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 Global Environment, Health and Safety Laboratory c} CURTIS MICHOLS Company Name: ABBOTT NELAC Accredited Report Date: 24-Nov-09 Sampling Division: GES Illinois Accreditation No.: 100310 Lab Project Number: 301917 Sampling Site: OTHER New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 Sampling Dept.: DEA Registration No.: RA0218784 Field Sample No. Sample Description Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 317148 MW-18B VINYL ACETATE < 0.005 MG/L 0.005 9-Nov-09 BW VINYL CHLORIDE < 0.001 MG/L 0.001 9-Nov-09 BW 4-BROMOFLUOROBENZENE (SURR) 105 % 86-115 9-Nov-09 BW DIBROMOFLUOROMETHANE (SURR) 103 % 86-118 9-Nov-09 BW TOLUENE-D8 (SURR) 97 % 88-110 9-Nov-09 BW Method: EPA 8260B 317147 MW-18D 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE 0.0013 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,4-TRIMETHYLBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.005 MG/L 0.005 12-Nov-09 BW 1,2-DIBROMOETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW Page 23 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317147 MW-18D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 24 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317147 MW-18D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLENE PERCHLOROETHYLENE SEC-BUTYLBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 0.018 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 25 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317147 MW-18D Method: EPA 8260B 317145 MW-19B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 0.0014 MG/L 0.001 < 0.001 MG/L 0.001 0.22 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 96 % 86-115 96 % 86-118 97 % 88-110 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 10-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L 0.001 10-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 10-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 10-Nov-09 BW 1,1-DICHLOROETHANE <0.001 MG/L 0.001 10-Nov-09 BW 1,1-DICHLOROETHYLENE <0.001 MG/L 0.001 10-Nov-09 BW 1,1-DICHLOROPROPENE <0.001 MG/L 0.001 10-Nov-09 BW Page 26 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317145 MW-19B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPAN E 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 27 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317145 MW-19B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 28 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317145 MW-19B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 108 % 86-115 104 % 86-118 99 % 88-110 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 10-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 29 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description Method: EPA 8260B 317144 MW-19D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE 0.0033 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2,4-TRIMETHYLBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.005 MG/L 0.005 12-Nov-09 BW 1,2-DIBROMOETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROETHANE <0.001 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROPROPANE <0.001 MG/L 0.001 12-Nov-09 BW 1,3,5-TRIMETHYLBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,3-DICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW 1,3-DICHLOROPROPANE <0.001 MG/L 0.001 12-Nov-09 BW 1,4-DICHLOROBENZENE <0.001 MG/L 0.001 12-Nov-09 BW Page 30 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317144 MW-19D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN O N E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 0.001 MG/L 0.001 < 0.001 MG/L 0.001 0.054 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 31 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317144 MW-19D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 32 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317144 MW-19D Method: EPA 8260B 317137 MW-20B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 0.0077 MG/L 0.001 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW 0.67 MG/L 0.005 12-Nov-09 BW < 0.005 MG/L 0.005 12-Nov-09 BW < 0.001 MG/L 0.001 12-Nov-09 BW 96 % 86-115 12-Nov-09 BW 99 % 86-118 12-Nov-09 BW 98 % 88-110 12-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROETHYLENE <0.001 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROPROPENE <0.001 MG/L 0.001 9-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.001 MG/L 0.001 9-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.001 MG/L 0.001 9-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.001 MG/L 0.001 9-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.001 MG/L 0.001 9-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.005 MG/L 0.005 9-Nov-09 BW Page 33 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317137 MW-20B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 34 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317137 MW-20B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 35 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317137 MW-20B Method: EPA 8260B 317138 MW-20D Abbott 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW < 0.005 MG/L 0.005 9-Nov-09 BW < 0.005 MG/L 0.005 9-Nov-09 BW < 0.001 MG/L 0.001 9-Nov-09 BW 103 % 86-115 9-Nov-09 BW 102 % 86-118 9-Nov-09 BW 99 % 88-110 9-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 9-Nov-09 BW Page 36 of 104 Environmental Lab Report �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317138 MW-20D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,1-DICHLOROETHANE 1,1-DICHLOROETHYLENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPAN E 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 37 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317138 MW-20D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 38 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317138 MW-20D Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 39 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 Global Environment, Health and Safety Laboratory c} CURTIS MICHOLS Company Name: ABBOTT NELAC Accredited Report Date: 24-Nov-09 Sampling Division: GES Illinois Accreditation No.: 100310 Lab Project Number: 301917 Sampling Site: OTHER New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 Sampling Dept.: DEA Registration No.: RA0218784 Field Sample No. Sample Description Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 317138 MW-20D 4-BROMOFLUOROBENZENE (SURR) 107 % 86-115 9-Nov-09 BW DIBROMOFLUOROMETHANE (SURR) 103 1 — % _ 86-118 9-Nov-09 BW TOLUENE-D8 (SURR) 99 % 88-110 9-Nov-09 BW Method: EPA 8260B 317169 MW-100A 1,1,1,2-TETRACHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1,1-TRICHLOROETHANE 0.72 MG/L 0,001 8-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1,2-TRICHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHYLENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROPROPENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,3-TRICHLOROBENZENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,3-TRICHLOROPROPANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,4-TRICHLOROBENZENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <2.5 MG/L 0.005 8-Nov-09 BW 1,2-DIBROMOETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2-DICHLOROBENZENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2-DICHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2-DICHLOROPROPANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,3,5-TRIMETHYLBENZENE < 0.5 MG/L 0.001 8-Nov-09 BW Page 40 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317169 MW-100A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 1 MG/L 0.002 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 41 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317169 MW-100A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCH LOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 38 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 1 MG/L 0.002 < 2.5 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 0.92 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 42 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317169 MW-100A Method: EPA 8260B 317171 MW-100B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROM ETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 2.3 MG/L 0.001 8-Nov-09 BW < 0.5 MG/L 0.001 8-Nov-09 BW < 0.5 MG/L 0.001 8-Nov-09 BW 3.2 MG/L 0.001 8-Nov-09 BW < 0.5 MG/L 0.001 8-Nov-09 BW 5.2 MG/L 0.005 8-Nov-09 BW < 2.5 MG/L 0.005 8-Nov-09 BW < 0.5 MG/L 0.001 8-Nov-09 BW 109 % 86-115 8-Nov- 09 BW 103 % 86-118 8-Nov- 09 BW 101 % 88-110 8-Nov- BW 1,1,1,2-TETRACHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1,1-TRICHLOROETHANE 0.87 MG/L 0.001 8-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1,2-TRICHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHYLENE 0.68 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROPROPENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,3-TRICHLOROBENZENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,3-TRICHLOROPROPANE < 0.5 MG/L 0.001 8-Nov-09 BW Page 43 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317171 MW-100B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-HEXANONE 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 1 MG/L 0.002 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 44 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317171 MW-100B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 2.5 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 47 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 1 MG/L 0.002 4.4 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 0.89 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 45 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317171 MW-100B Method: EPA 8260B 317167 MW-101A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCH LOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) 1,1,1,2-TETRACHLOROETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 2.4 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 25 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 106 % 86-115 104 % 86-118 99 % 88-110 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW < 0.5 MG/L 0.001 9-Nov-09 BW Page 46 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317167 MW-101A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,1,1-TRICH LOROETHAN E 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICH LOROETHAN E 1,1-DICHLOROETHANE 1,1-DICHLOROETHYLENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE Result Flag Units Reporting Limit 5.4 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 0.51 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 Date Analyzed 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 47 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317167 MW-101A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 1 MG/L 0.002 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 12 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 48 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317167 MW-101A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter ETHYL BENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLENE PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 1 MG/L 0.002 < 2.5 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 2.7 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 55 MG/L 0.001 < 0.5 MG/L 0.001 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 49 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317167 MW-101A Method: EPA 8260B 317165 MW-101B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 29 MG/L 0.005 9-Nov-09 BW < 2.5 MG/L 0.005 9-Nov-09 BW < 0.5 MG/L 0.001 9-Nov-09 BW 104 % 86-115 9-Nov-09 BW 102 1 % 86-118 9-Nov-09 BW 1 97 % - 88-110 9-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW _ 1,1,1-TRICHLOROETHANE 1.7 MG/L 0.001 8-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1,2-TRICHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHYLENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROPROPENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,3-TRICHLOROBENZENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,3-TRICHLOROPROPANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,4-TRICHLOROBENZENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <2.5 MG/L 0.005 8-Nov-09 BW 1,2-DIBROMOETHANE < 0.5 MG/L 0.001 8-Nov-09 BW 1,2-DICHLOROBENZENE < 0.5__j MG/L _ 0.001 8-Nov-09 BW Page 50 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317165 MW-101B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-HEXANONE 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 1 MG/L 0.002 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 51 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317165 MW-101B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 28 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 1 MG/L 0.002 < 2.5 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 52 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317165 MW-101B Method: EPA 8260B 317149 MW-102A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 1.2 MG/L 0.001 < 0.5 MG/L 0.001 < 0.5 MG/L 0.001 1.1 MG/L 0.001 < 0.5 MG/L 0.001 14 MG/L 0.005 < 2.5 MG/L 0.005 < 0.5� MG/L 0.001 105 % 86-115 104 % 86-118 99 % 88-110 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW 1,1,1,2-TETRACHLOROETHANE <0.05 MG/L 0.001 9-Nov-09 BW 1,1,1-TRICHLOROETHANE 0.084 MG/L 0.001 9-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.05 MG/L 0.001 9-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.05 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROETHANE <0.05 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROETHYLENE 0.55 MG/L 0.001 9-Nov-09 BW Page 53 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317149 MW-102A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1<0.05 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-HEXANONE 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE 4 ACETONE BENZENE Result Flag Units Reporting Limit <0.05 MG/L 0.001 <0.05 MG/L 0.001 MG/L 0.001 <0.05 MG/L 0.001 < 0.05 MG/L 0.001 <0.25 MG/L 0.005 <0.05 MG/L 0.001 <0.05 MG/L 0.001 <0.05 MG/L 0.001 <0.05 MG/L 0.001 <0.05 MG/L 0.001 <0.05 MG/L 0.001 <0.05 MG/L 0.001 <0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.25 MG/L 0.005 < 0.05 MG/L 0.001 < 0.1 MG/L 0.002 < 0.25 MG/L 0.005 < 0.05 MG/L 0.001 Date Analyzed 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 54 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317149 MW-102A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYL BENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE Result Flag Units Reporting Limit < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.25 MG/L 0.005 < 0.25 MG/L 0.005 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 24 MG/L 0.001 <0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.25 MG/L 0.005 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.05 MG/L 0.001 < 0.1 MG/L 0.002 L< 0.25 MG/L 0.005 Date Analyzed 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 55 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317149 MW-102A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLENE PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROM ETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) Result < 0.25 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.15 <0.05 <0.05 0.79 < 0.05 8.9 < 0.25 < 0.05 105 104 Flag Units MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L % % Reporting Limit 0.005 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.005 0.005 0.001 86-115 _ 86-118 Date Analyzed 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 56 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317149 MW-102A Method: EPA 8260B 317151 MW-102B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info TOLUENE-D8 (SURR) 100 % 88-110 9-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE 0.017 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE 0.071 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.005 MG/L 0.001 12-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.025 MG/L 0.005 12-Nov-09 BW 1,2-DIBROMOETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROPROPANE <0.005 MG/L 0.001 12-Nov-09 BW 1,3,5-TRIMETHYLBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,3-DICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,3-DICHLOROPROPANE <0.005 MG/L 0.001 12-Nov-09 BW Page 57 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317151 MW-102B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 1.1 MG/L 0.001 < 0.005 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 58 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317151 MW-102B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCH LOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 0.013 MG/L 0.001 < 0.005 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 59 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317151 MW-102B Method: EPA 8260B 317153 MW-102C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 12-Nov-09 BW 0.59 MG/L 0.001 12-Nov-09 BW < 0.005 MG/L 0.001 12-Nov-09 BW 3.9 MG/L 0.005 12-Nov-09 BW < 0.025 MG/L 0.005 12-Nov-09 BW < 0.005 MG/L 0.001 12-Nov-09 BW 97 % 86-115 12-Nov-09 BW 99 % 86-118 12-Nov-09 BW 99 % 88-110 12-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE 0.0058 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.005 MG/L 0.001 12-Nov-09 BW Page 60 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317153 MW-102C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 61 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317153 MW-102C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 0.011 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 62 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317153 MW-102C Method: EPA 8260B 317160 MW-103A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 1.5 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 95 % 86-115 98 % 86-118 98 % 88-110 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW 1,1,1,2-TETRACHLOROETHANE <0.02 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.02 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.02 MG/L 0.001 12-Nov-09 BW Page 63 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317160 MW-103A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,1,2-TRICH LOROETHAN E 1,1-DICHLOROETHANE 1,1-DICHLOROETHYLENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPAN E 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.1 MG/L 0.005 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.1 MG/L 0.005 < 0.02 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 64 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317160 MW-103A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYL BENZENE HEXACHLOROBUTADIENE Result Flag Units Reporting Limit < 0.04 MG/L 0.002 < 0.1 MG/L 0.005 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.1 MG/L 0.005 < 0.1 MG/L 0.005 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 0.22 MG/L 0.001 <0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.1 MG/L 0.005 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 Date Analyzed 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 65 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317160 MW-103A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLENE PERCH LOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE Result Flag Units Reporting Limit < 0.02 MG/L 0.001 < 0.04 MG/L 0.002 < 0.1 MG/L 0.005 < 0.1 MG/L 0.005 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 < 0.02 MG/L 0.001 <0.02 MG/L 0.001 <0.02 MG/L 0.001 0.029 MG/L 0.001 < 0.02 MG/L 0.001 21 MG/L 0.005 < 0.1 MG/L 0.005 Date Analyzed 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 66 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 Global Environment, Health and Safety Laboratory c} CURTIS MICHOLS Company Name: ABBOTT NELAC Accredited Report Date: 24-Nov-09 Sampling Division: GES Illinois Accreditation No.: 100310 Lab Project Number: 301917 Sampling Site: OTHER New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 Sampling Dept.: DEA Registration No.: RA0218784 Field Sample No. Sample Description Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 317160 MW-103A VINYL CHLORIDE < 0.02 MG/L 0.001 12-Nov-09 BW 4-BROMOFLUOROBENZENE (SURR) 96 % 86-115 12-Nov-09 BW DIBROMOFLUOROMETHANE (SURR) 95 % 86-118 12-Nov-09 BW TOLUENE-D8 (SURR) 98 % 88-110 12-Nov-09 BW Method: EPA 8260B 317161 MW-103B 1,1,1,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE 0.031 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.005 MG/L 0.001 12-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.025 MG/L 0.005 12-Nov-09 BW 1,2-DIBROMOETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROPROPANE <0.005 MG/L 0.001 12-Nov-09 BW Page 67 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317161 MW-103B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN O N E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 68 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317161 MW-103B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCH LOROETHYLENE SEC-BUTYLBENZENE STYRENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 0.29 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 69 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317161 MW-103B Method: EPA 8260B 317163 MW-103C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) 1 Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 0.0066 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 0.027 MG/L 0.001 < 0.005 MG/L 0.001 8.8 MG/L 0.005 < 0.025 MG/L 0.005 0.012 MG/L 0.001 97 % 86-115 98 % 86-118 100 % 88-110 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW 1,1,1,2-TETRACHLOROETHANE <0.01 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.01 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.01 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.01 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.01 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE 0.022 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.01 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.01 MG/L 0.001 12-Nov-09 BW Page 70 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317163 MW-103C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-HEXANONE 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE Result Flag Units Reporting Limit <0.01 MG/L 0.001 <0.01 MG/L 0.001 < 0.01 MG/L 0.001 <0.05 MG/L 0.005 <0.01 MG/L 0.001 <0.01 MG/L 0.001 <0.01 MG/L 0.001 <0.01 MG/L 0.001 <0.01 MG/L 0.001 <0.01 MG/L 0.001 <0.01 MG/L 0.001 <0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.05 MG/L 0.005 < 0.01 MG/L 0.001 < 0.02 MG/L 0.002 < 0.05 MG/L 0.005 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 Date Analyzed 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 71 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317163 MW-103C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.01 MG/L 0.001 < 0.05 MG/L 0.005 < 0.05 MG/L 0.005 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 0.28 MG/L 0.001 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.05 MG/L 0.005 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.01 MG/L 0.001 < 0.02 MG/L 0.002 < 0.05 MG/L 0.005 < 0.05 MG/L 0.005 < 0.01 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 72 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317163 MW-103C Method: EPA 8260B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info METHYLENE CHLORIDE < 0.01 MG/L 0.001 12-Nov-09 BW N-BUTYLBENZENE < 0.01 MG/L 0.001 12-Nov-09 BW N-PROPYLBENZENE < 0.01 MG/L 0.001 12-Nov-09 BW NAPHTHALENE < 0.01 MG/L 0.001 12-Nov-09 BW O-XYLENE < 0.01 MG/L 0.001 12-Nov-09 BW PERCHLOROETHYLENE < 0.01 MG/L 0.001 12-Nov-09 BW SEC-BUTYLBENZENE < 0.01 MG/L 0.001 12-Nov-09 BW STYRENE < 0.01 MG/L 0.001 12-Nov-09 BW TERT-BUTYLBENZENE < 0.01 MG/L 0.001 12-Nov-09 BW TOLUENE < 0.01 MG/L 0.001 12-Nov-09 BW TRANS-1,2-DICHLOROETH ENE <0.01 MG/L 0.001 12-Nov-09 BW TRANS-1,3-DICHLOROPROPENE <0.01 MG/L 0.001 12-Nov-09 BW TRICHLOROETHYLENE 0.023 MG/L 0.001 12-Nov-09 BW TRICHLOROFLUOROMETHANE < 0.01 MG/L 0.001 12-Nov-09 BW TRICHLOROTRIFLUOROETHANE 7.3 MG/L 0.005 12-Nov-09 BW VINYL ACETATE < 0.05 MG/L 0.005 12-Nov-09 BW VINYL CHLORIDE 0.012 MG/L 0.001 12-Nov-09 BW 4-BROMOFLUOROBENZENE (SURR) 97 % 86-115 12-Nov-09 BW DIBROMOFLUOROMETHANE (SURR) 99 % 86-118 12-Nov-09 BW TOLUENE-D8 (SURR) 99 % 88-110 12-Nov-09 BW Page 73 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317158 MW-104A Global Environment, Health and Safety Laboratory c} NELAC Accredited Illinois Accreditation No.: 100310 New Jersey Accreditation No.: IL005 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter Result 1,1,1,2-TETRACHLOROETHANE <0.01 1,1,1-TRICHLOROETHANE <0.01 1,1,2,2-TETRACHLOROETHANE <0.01 1,1,2-TRICHLOROETHANE <0.01 1,1-DICHLOROETHANE 0.0031 1,1-DICHLOROETHYLENE 0.0028 1,1-DICHLOROPROPENE <0.01 1,2,3-TRICHLOROBENZENE <0.01 1,2,3-TRICHLOROPROPANE <0.01 1,2,4-TRICHLOROBENZENE <0.01 1,2,4-TRIMETHYL BENZENE < 0.01 1,2-DIBROMO-3-CHLOROPROPANE <0.05 1,2-DIBROMOETHANE <0.01 1,2-DICHLOROBENZENE <0.01 1,2-DICHLOROETHANE 0.0038 1,2-DICHLOROPROPANE <0.01 1,3,5-TRIMETHYLBENZENE <0.01 1,3-DICHLOROBENZENE <0.01 1,3-DICHLOROPROPANE <0.01 1,4-DICHLOROBENZENE <0.01 2,2-DICHLOROPROPANE < 0.01 Flag Units MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L Reporting Limit 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.005 0.001 0.001 1111/111 Report Date: 24-Nov-09 Lab Project Number: 301917 Sample Group Number: E302694 Date Analyzed 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 iVQI41 M1111 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 Analyst Initials Additional Info BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 74 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317158 MW-104A Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter Result 2-CHLOROTOLUENE < 0.01 2-HEXANONE < 0.05 4-CHLOROTOLUENE < 0.01 4-ISOPROPYLTOLUENE < 0.02 ACETONE < 0.05 BENZENE < 0.01 BROMOBENZENE < 0.01 BROMODICHLOROMETHANE < 0.01 BROMOFORM < 0.01 BROMOMETHANE < 0.05 CARBON DISULFIDE < 0.05 CARBON TETRACHLORIDE < 0.01 CHLOROBENZENE < 0.01 CHLOROBROMOMETHANE < 0.01 CHLOROETHANE < 0.01 CHLOROFORM 0.0021 CHLOROMETHANE < 0.01 CIS-1,2-DICHLOROETHENE 0.59 CIS-1,3-DICHLOROPROPENE <0.01 DIBROMOCHLOROMETHANE < 0.01 DIBROMOMETHANE < 0.01 Flag Units MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L Reporting Limit 0.001 0.005 0.001 0.002 0.005 0.001 0.001 0.001 0.001 0.005 0.005 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 Date Analyzed 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 75 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317158 MW-104A Global Environment, Health and Safety Laboratory c} NELAC Accredited Illinois Accreditation No.: 100310 New Jersey Accreditation No.: IL005 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter Result DICHLORODIFLUOROMETHANE < 0.05 ETHYL BENZENE < 0.01 HEXACHLOROBUTADIENE < 0.01 ISOPROPYLBENZENE < 0.01 M AND P XYLENE < 0.02 METHYL ETHYL KETONE < 0.05 METHYL ISOBUTYL KETONE < 0.05 METHYL TERT-BUTYL ETHER < 0.01 METHYLENE CHLORIDE < 0.01 N-BUTYLBENZENE < 0.01 N-PROPYLBENZENE < 0.01 NAPHTHALENE < 0.01 O-XYLENE < 0.01 PERCHLOROETHYLENE < 0.01 SEC-BUTYLBENZENE < 0.01 STYRENE < 0.01 TERT-BUTYLBENZENE < 0.01 TOLUENE < 0.01 TRANS-1,2-DICHLOROETHENE 0.0033 TRANS-1,3-DICHLOROPROPENE <0.01 TRICHLOROETHYLENE 0.0024 Flag Units MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L Reporting Limit 0.005 0.001 0.001 0.001 0.002 0.005 0.005 0.001 0.001 0.001 0.001 0.001 0.001 0.001 1111/111 Report Date: 24-Nov-09 Lab Project Number: 301917 Sample Group Number: E302694 Date Analyzed 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 iVZ 41 M1111 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 MG/L 0.001 12-Nov-09 Analyst Initials Additional Info BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 76 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317158 MW-104A Method: EPA 8260B 317159 MW-104B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info TRICHLOROFLUOROMETHANE < 0.01 MG/L 0.001 12-Nov-09 BW TRICHLOROTRIFLUOROETHANE 0.94 MG/L 0.005 12-Nov-09 BW VINYL ACETATE < 0.05 MG/L 0.005 12-Nov-09 BW VINYL CHLORIDE 0.012 MG/L 0.001 12-Nov-09 BW 4-BROMOFLUOROBENZENE (SURR) 97 % 86-115 12-Nov-09 BW DIBROMOFLUOROMETHANE (SURR) 99 % 86-118 12-Nov-09 BW TOLUENE-D8 (SURR) 99 % 88-110 12-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE <0.005 MG/L 0.001 9-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.005 MG/L 0.001 9-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.005 MG/L 0.001 9-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.005 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROETHANE <0.005 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROETHYLENE 0.012 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROPROPENE <0.005 MG/L 0.001 9-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.005 MG/L 0.001 9-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.005 MG/L 0.001 9-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.005 MG/L 0.001 9-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.005 MG/L 0.001 9-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.025 MG/L 0.005 9-Nov-09 BW 1,2-DIBROMOETHANE <0.005 MG/L 0.001 9-Nov-09 BW Page 77 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317159 MW-104B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 78 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317159 MW-104B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 0.099 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 0.0092 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 79 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317159 MW-104B Method: EPA 8260B 317157 MW-104C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter PERCH LOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 0.018 MG/L 0.001 < 0.005 MG/L 0.001 2.1 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 107 % 86-115 105 % 86-118 98 % 88-110 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW 1,1,1,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW Page 80 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317157 MW-104C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,1-DICHLOROETHYLENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 0.02 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 81 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317157 MW-104C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 0.15 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 82 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317157 MW-104C Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLU0ROM ETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 0.008 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 0.015 MG/L 0.001 < 0.005 MG/L 0.001 2.7 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 98 % 86-115 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 83 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 Global Environment, Health and Safety Laboratory c} CURTIS MICHOLS Company Name: ABBOTT NELAC Accredited Report Date: 24-Nov-09 Sampling Division: GES Illinois Accreditation No.: 100310 Lab Project Number: 301917 Sampling Site: OTHER New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 Sampling Dept.: DEA Registration No.: RA0218784 Field Sample No. Sample Description Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 317157 MW-104C DIBROMOFLUOROMETHANE (SURR) 99 % 86-118 12-Nov-09 BW TOLUENE-D8 (SURR) 94 1 % 88-110 12-Nov-09 BW Method: EPA 8260B _ 317139 Dup-1 1,1,1,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROETHYLENE 0.008 MG/L 0.001 12-Nov-09 BW 1,1-DICHLOROPROPENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2,4-TRIMETHYL BENZENE < 0.005 MG/L 0.001 12-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.025 MG/L 0.005 12-Nov-09 BW 1,2-DIBROMOETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROETHANE <0.005 MG/L 0.001 12-Nov-09 BW 1,2-DICHLOROPROPANE <0.005 MG/L 0.001 12-Nov-09 BW 1,3,5-TRIMETHYLBENZENE <0.005 MG/L 0.001 12-Nov-09 BW 1,3-DICHLOROBENZENE <0.005 MG/L 0.001 12-Nov-09 BW Page 84 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317139 Dup-1 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 0.09 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 85 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317139 Dup-1 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 0.0021 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 12-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 86 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317139 Dup-1 Method: EPA 8260B 317164 Dup-2 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 12-Nov-09 BW < 0.005 MG/L 0.001 12-Nov-09 BW 0.0033 MG/L 0.001 12-Nov-09 BW < 0.005 MG/L 0.001 12-Nov-09 BW 0.61 MG/L 0.005 12-Nov-09 BW < 0.025 MG/L 0.005 12-Nov-09 BW 0.0013 MG/L 0.001 12-Nov-09 BW 96 % 86-115 12-Nov-09 BW 100 % 86-118 12-Nov-09 BW 99 El % 88-110 12-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE < 0.2 MG/L 0.001 9-Nov-09 BW 1,1,1-TRICHLOROETHANE < 0.2 MG/L 0.001 9-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE < 0.2 MG/L 0.001 9-Nov-09 BW 1,1,2-TRICHLOROETHANE < 0.2 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROETHANE < 0.2 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROETHYLENE < 0.2 MG/L 0.001 9-Nov-09 BW 1,1-DICHLOROPROPENE < 0.2 MG/L 0.001 9-Nov-09 BW 1,2,3-TRICHLOROBENZENE < 0.2 MG/L 0.001 9-Nov-09 BW 1,2,3-TRICHLOROPROPANE < 0.2 MG/L 0.001 9-Nov-09 BW 1,2,4-TRICHLOROBEl' < 0.2 MG/L 0.001 9-Nov-09 BW Page 87 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317164 Dup-2 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE ' 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.2 MG/L 0.001 < 1 MG/L 0.005 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 1 MG/L 0.005 < 0.2 MG/L 0.001 < 0.4 MG/L 0.002 < 1 MG/L 0.005 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 1 MG/L 0.005 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 88 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317164 Dup-2 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 1 MG/L 0.005 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 0.34 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 1 MG/L 0.005 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.4 MG/L 0.002 < 1 MG/L 0.005 < 1 MG/L 0.005 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 89 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317164 Dup-2 Method: EPA 8260B 317155 MW-104A MS Abbott 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 < 0.2� MG/L 0.001 < 0.2 MG/L 0.001 < 0.2 MG/L 0.001 7.6 MG/L 0.005 < 1 MG/L 0.005 < 0.2 MG/L 0.001 108 % 86-115 104 % 86-118 101 I % 88-110 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 9-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW 1,1,1,2-TETRACHLOROETHANE 104 % 0.001 20-Nov-09 BW 1,1,1-TRICHLOROETHANE 115 % 0.001 20-Nov-09 BW Page 90 of 104 Environmental Lab Report �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317155 MW-104A MS Global Environment, Health and Safety Laboratory A c c 0 66.E O NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICH LOROETHAN E 1,1-DICHLOROETHANE 1,1-DICHLOROETHYLENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE ' 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E Result Flag 99 102 1 105 122 102 97 98 97 98 103 104 96 110 98 98 95 91 97 101 94 113 Units Reporting Limit % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.005 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.005 Date Analyzed 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 91 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317155 MW-104A MS Global Environment, Health and Safety Laboratory A c c 0 66.E O NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE Result Flag 97 97 103 96 93 109 105 107 107 111 96 104 104 108 109 100 100 108 103 109 95 Units Reporting Limit % 0.001 % 0.002 % 0.005 % 0.001 % 0.001 % 0.001 % 0.001 % 0.005 % 0.005 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.005 % 0.001 Date Analyzed 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 92 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317155 MW-104A MS Global Environment, Health and Safety Laboratory A c c 0 66.E O NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROM ETHANE TRICHLOROTRI FLUOROETHANE Result Flag 93 101 ` 96 111 118 103 101 95 93 103 98 96 98 101 96 100 104 110 100 121 111 Units Reporting Limit % 0.001 % 0.001 % 0.002 % 0.005 % 0.005 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.005 Date Analyzed 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 93 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317155 MW-104A MS Method: EPA 8260B 317156 MW-104A MSD Global Environment, Health and Safety Laboratory A c c 0 66.E O NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) 1,1,1,2-TETRACH LOROETHAN E 1,1,1-TRICH LOROETHAN E 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICH LOROETHAN E 1,1-DICHLOROETHANE 1,1-DICHLOROETHYLENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 130 % _ 0.005 20-Nov-09 BW It 99 i % 0.001 20-Nov-09 BW 111 % 86-115 20-Nov-09 BW 105 % 86-118 20-Nov-09 BW 1 99 % _ 88-110 20-Nov-09 BW 102 % 0.001 20-Nov-09 BW 113 % 0.001 20-Nov-09 BW 100 % 0.001 20-Nov-09 BW 104 % 0.001 20-Nov-09 BW 105 % 0.001 20-Nov-09 BW 119 % 0.001 20-Nov-09 BW 103 % 0.001 20-Nov-09 BW 97 % 0.001 20-Nov-09 BW 98 % 0.001 20-Nov-09 BW 99 % 0.001 20-Nov-09 BW 99 % 0.001 20-Nov-09 BW 105 % 0.005 20-Nov-09 BW 106 % 0.001 20-Nov-09 BW 95 % 0.001 20-Nov-09 BW 107 % 0.001 -3 20-Nov-09 BW Page 94 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317156 MW-104A MSD Global Environment, Health and Safety Laboratory A c c 0 66.E O NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE Result Flag 100 99 96 93 99 101 95 110 99 97 97 99 96 112 105 110 107 113 97 107 105 Units Reporting Limit % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.005 % 0.001 % 0.002 % 0.005 % 0.001 % 0.001 % 0.001 % 0.001 % 0.005 % 0.005 % 0.001 % 0.001 % 0.001 % 0.001 Date Analyzed 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 95 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317156 MW-104A MSD Global Environment, Health and Safety Laboratory A c c 0 66.E O NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYLETHYLKETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLENE PERCHLOROETHYLENE SEC-BUTYLBENZENE Result Flag 108 107 1 102 102 112 106 104 96 92 103 96 110 121 102 100 95 95 104 98 95 98 Units Reporting Limit % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.005 % 0.001 % 0.001 % 0.001 % 0.002 % 0.005 % 0.005 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 % 0.001 Date Analyzed 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 20-Nov-09 Analyst Initials BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Additional Info Page 96 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317156 MW-104A MSD Method: EPA 8260B 317146 EB-1 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 100 % 0.001 20-Nov-09 BW 97 I % 0.001 20-Nov-09 BW 102 % 0.001 20-Nov-09 BW 105 % 0.001 20-Nov-09 BW 111 % 0.001 20-Nov-09 BW 104 % 0.001 20-Nov-09 BW 123 % 0.001 20-Nov-09 BW 112 % 0.005 20-Nov-09 BW 130 % 0.005 20-Nov-09 BW 106 % 0.001 20-Nov-09 BW 110 % 86-115 20-Nov-09 BW 104 % 86-118 20-Nov-09 BW 100 % 88-110 20-Nov-09 BW 1,1,1,2-TETRACHLOROETHANE <0.005 MG/L 0.001 8-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.005 MG/L 0.001 8-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.005 MG/L 0.001 8-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.005 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHANE <0.005 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHYLENE <0.005 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROPROPENE <0.005 MG/L 0.001 8-Nov-09 BW Page 97 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317146 EB-1 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPAN E 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYL BENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN ON E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 98 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317146 EB-1 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.01 MG/L 0.002 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 99 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317146 EB-1 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRI FLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.005 MG/L 0.001 < 0.025 MG/L 0.005 < 0.025 MG/L 0.005 < 0.005 MG/L 0.001 104 % 86-115 100 % 86-118 100 % 88-110 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 100 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description Method: EPA 8260B 317162 EB-2 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info 1,1,1,2-TETRACHLOROETHANE <0.001 MG/L 0.001 8-Nov-09 BW 1,1,1-TRICHLOROETHANE <0.001 MG/L 0.001 8-Nov-09 BW 1,1,2,2-TETRACHLOROETHANE <0.001 MG/L 0.001 8-Nov-09 BW 1,1,2-TRICHLOROETHANE <0.001 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHANE <0.001 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROETHYLENE <0.001 MG/L 0.001 8-Nov-09 BW 1,1-DICHLOROPROPENE <0.001 MG/L 0.001 8-Nov-09 BW 1,2,3-TRICHLOROBENZENE <0.001 MG/L 0.001 8-Nov-09 BW 1,2,3-TRICHLOROPROPANE <0.001 MG/L 0.001 8-Nov-09 BW 1,2,4-TRICHLOROBENZENE <0.001 MG/L 0.001 8-Nov-09 BW 1,2,4-TRIMETHYLBENZENE <0.001 MG/L 0.001 8-Nov-09 BW 1,2-DIBROMO-3-CHLOROPROPANE <0.005 MG/L 0.005 8-Nov-09 BW 1,2-DIBROMOETHANE <0.001 MG/L 0.001 8-Nov-09 BW 1,2-DICHLOROBENZENE <0.001 MG/L 0.001 8-Nov-09 BW 1,2-DICHLOROETHANE <0.001 MG/L 0.001 8-Nov-09 BW 1,2-DICHLOROPROPANE <0.001 MG/L 0.001 8-Nov-09 BW 1,3,5-TRIMETHYLBENZENE <0.001 MG/L 0.001 8-Nov-09 BW 1,3-DICHLOROBENZENE <0.001 MG/L 0.001 8-Nov-09 BW 1,3-DICHLOROPROPANE <0.001 MG/L 0.001 8-Nov-09 BW 1,4-DICHLOROBENZENE <0.001 MG/L 0.001 8-Nov-09 BW Page 101 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317162 EB-2 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter 2,2-DICHLOROPROPANE 2-CHLOROTOLUENE 2-H EXAN O N E 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE ACETONE BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 102 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317162 EB-2 Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE M AND P XYLENE METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYL TERT-BUTYL ETHER METHYLENE CHLORIDE N-BUTYLBENZENE N-PROPYLBENZENE NAPHTHALENE O-XYLEN E PERCHLOROETHYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.002 MG/L 0.002 < 0.005 MG/L 0.005 < 0.005 MG/L 0.005 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 < 0.001 MG/L 0.001 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 8-Nov-09 BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW BW Page 103 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 �7 CURTIS MICHOLS Company Name: ABBOTT Sampling Division: GES Sampling Site: OTHER Sampling Dept.: Field Sample No. Sample Description 317162 EB-2 Method: EPA 8260B Global Environment, Health and Safety Laboratory c} NELAC Accredited Report Date: 24-Nov-09 Illinois Accreditation No.: 100310 Lab Project Number: 301917 New Jersey Accreditation No.: IL005 Sample Group Number: E302694 North Carolina Accreditation No.: 639 DEA Registration No.: RA0218784 Parameter TRICHLOROETHYLENE TRICHLOROFLUOROMETHANE TRICHLOROTRIFLUOROETHANE VINYL ACETATE VINYL CHLORIDE 4-BROMOFLUOROBENZENE (SURR) DIBROMOFLUOROMETHANE (SURR) TOLUENE-D8 (SURR) Result Flag Units Reporting Limit Date Analyzed Analyst Initials Additional Info < 0.001 MG/L 0.001 8-Nov-09 BW < 0.001 MG/L 0.001 8-Nov-09 BW < 0.005 MG/L 0.005 8-Nov-09 BW < 0.005 MG/L 0.005 8-Nov-09 BW < 0.001 MG/L 0.001 8-Nov-09 BW 103 % 86-115 8-Nov-09 BW 100 % 86-118 8-Nov-09 BW 98 % 88-110 8-Nov-09 BW Page 104 of 104 Abbott Environmental Lab Report 200 Abbott Park Rd. D-051H, AP52 Abbott Park, IL 60064 Phone: (847) 935-6337 KIElfbialinsi is 2340 Stock Creek Blvd. Rockford TN 37853-3044 Phone: (865) 573-8188 Fax: (865) 573-8133 Email: info@microbe.com Client: Matt Allen Phone: 919.872.6600 AECOM Environment (ENSR) 7041 Old Wake Forest Road Suite 103 Raleigh, NC 27616 Fax: 919.872.7996 Identifier: 011GL Date Rec: 12/04/2009 Report Date: 12/09/2009 Client Project #: 60135880.200 Purchase Order #: 2822 Analysis Requested: CENSUS Reviewed By: L. P�' ;? 4'�" Client Project Name: ABBOTT LABS - Laurinburg, NC NOTICE: This report is intended only for the addressee shown above and may contain confidential or privileged information. If the recipient of this material is not the intended recipient or if you have received this in error, please notify Microbial Insights, Inc. immediately. The data and other information in this report represent only the sample(s) analyzed and are rendered upon condition that it is not to be reproduced without approval from Microbial Insights, Inc. Thank you for your cooperation. Page 1 of 3 MICROBIAL INSIGHTS, INC. 2340 Stock Creek Blvd. Rockford, TN 37853-3044 CENSUS Tel. (865) 573-8188 Fax. (865) 573-8133 Client: AECOM Environment (ENSR) MI Project Number: 011GL Project: ABBOTT LABS - Laurinburg, NC Date Received: 12/04/2009 Sample Information Client Sample ID: MW-100B MW-101A MW-102C Sample Date: 12/01/2009 12/01/2009 12/01/2009 Units: cells/ml- cells/ml- cells/ml- Analyst: ab ab ab Dechlorinating Bacteria Dehalococcoides spp. DHC <5.00E-01 5.00E-01 2.00E-01 (J) Dehalobacter spp. DHB <1.00E+00 1.28E+03 <1.00E+00 Functional Genes tceA Reductase TCE <5.00E-01 <3.00E-01 <5.00E-01 bvcA Reductase BVC <5.00E-01 <3.00E-01 <5.00E-01 Vinyl Chloride Reductase VCR <5.00E-01 1.00E-01 (J) 4.00E-01 (J) Legend: NA = Not Analyzed NS = Not Sampled J = Estimated gene copies below PQL but above LQL I = Inhibited < = Result not detected Page 2 of 3 fElfbialinsi ts Identifier: 011 GL Client Project #: 60135880.200 Purchase Order #: 2822 Comments: Date Rec: 12/04/2009 2340 Stock Creek Blvd. Rockford TN 37853-3044 Phone: (865) 573-8188 Fax: (865) 573-8133 Email: info@microbe.com Report Date: 12/09/2009 Client Project Name: ABBOTT LABS - Laurinburg, NC Page 3of3 KIElfbialinsi is 2340 Stock Creek Blvd. Rockford TN 37853-3044 Phone: (865) 573-8188 Fax: (865) 573-8133 Email: info@microbe.com Client: Matt Allen Phone: 919.872.6600 AECOM Environment (ENSR) 7041 Old Wake Forest Road Suite 103 Raleigh, NC 27616 Fax: 919.872.7996 Identifier: 048GL Date Rec: 12/17/2009 Report Date: 12/22/2009 Client Project #: 00005-024-200 Client Project Name: Abbott Labs Purchase Order #: 2822 Analysis Requested: Cancelled, CENSUS Reviewed By: L. P�' ;? 4'�" NOTICE: This report is intended only for the addressee shown above and may contain confidential or privileged information. If the recipient of this material is not the intended recipient or if you have received this in error, please notify Microbial Insights, Inc. immediately. The data and other information in this report represent only the sample(s) analyzed and are rendered upon condition that it is not to be reproduced without approval from Microbial Insights, Inc. Thank you for your cooperation. Page 1 of 3 MICROBIAL INSIGHTS, INC. 2340 Stock Creek Blvd. Rockford, TN 37853-3044 CENSUS Tel. (865) 573-8188 Fax. (865) 573-8133 Client: AECOM Environment (ENSR) MI Project Number: 048GL Project: Abbott Labs Date Received: 12/17/2009 Sample Information Client Sample ID: GW09N-10 GW09N-12 (17-22&rsquo;) (41-46&rsquo;) Sample Date: 12/15/2009 12/14/2009 Units: cells/mL cells/mL Analyst: ab ab Dechlorinating Bacteria Dehalococcoides spp. DHC <3.00E-01 <1.00E+00 Dehalobacter spp. DHB 4.00E+00 2.70E+00 Legend: NA = Not Analyzed NS = Not Sampled J = Estimated gene copies below PQL but above LQL I = Inhibited < = Result not detected Page 2 of 3 0 2340 Stock Creek Blvd. Rockford TIN 37853-3044 Phone: (86565) 573-8173-8188 jMlrbiafinsi Is Fax: l: inf 5 info@microbe.com Email: info@microbe.com Identifier: 048GL Date Rec: 12/17/2009 Report Date: 12/22/2009 Client Project #: 00005-024-200 Client Project Name: Abbott Labs Purchase Order #: 2822 Comments: Page 3of3 AECOM Environment Appendix C Historical VOC Analytical Results at Solvent Plume Wells (Table C.1) 60135880 February 2010 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in p g/L) 2L Standards MW-100A Jan-10 Oct-02 Feb-03 Apr-03 Jun-03 Sep-03 Dec-03 May-04 Sep-04 Dec-04 Jun-05 Dec-05 Mar-06 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 1000 U 500 U 1000 U 500 U 500 U 500 U 50 U 500 U 100 U 350 500 U 2500 U 2500 U 2500 U 2500 U 2500 U Chloromethane 3 1000 U 500 U 1000 U 500 U 500 U 500 U 50 UJ 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U Vinyl chloride 0.03 1000 U 500 U 1000 U 500 U 500 U 500 U 50 U 500 U 120 150 380 J 500 U 500 U 500 U 500 U 500 U Chloroethane 3000 1000 U 500 U 1000 U 500 U 500 U 500 U 50 U 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U Trichlorofluoromethane 2,000 1000 U 500 U 1600 U 500 U 500 U 500 U 50 U 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1-Dichloroethene 7 1,400 1,000 1 1,200 500 U 1 940 1,100 1 350 1,000 1 810 960 1 500 U 960 1 810 1,200 1 910 1,100 Trichlorotrifluoroethane 200,000 27,000 32,000 37,000 30,000 18,000 33,000 6,200 59,000 28,000 37,000 23,000 J 30,000 25,000 18,000 17000 26,000 Carbon disulfide 700 5000 U 2500 U 5000 U 2500 U 2500 U 2500 U 250 U 2500 U 500 U 500 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Acetone 6000 10,000 2500 U 5000 U 2500 U 2500 U 16,000 740 2500 U 500 U 500 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Methylene chloride 5 200,000 42,000 42,000 31,000 26,000 20,000 14,000 13,000 6,800 6,300 J 4,700 2,500 3,100 34,000 3,100 2,600 trans- 1,2-Dichloroethene 100 1000 U 500 U 1000 U 500 U 500 U 500 U 50 U 500 U 100 U 100 U 1,800 500 U 500 U 500 U 500 U 500 U Meth I-tert-but I -ether MTBE 20 1000 U 500 U 1000 U 500 U 500 U 500 U 50 U 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1-Dichloroethane 6 1000 U 500 U 1000 U 500 U 500 U 500 U 53 500 U 89 J 100 U 500 U 500 U 500 U 500 U 500 U 500 U cis- 1,2-Dichloroethene 70 15,000 14,000 14,000 18,000 J 19,000 29,000 31,000 55,000 66,000 63,000 77,000 71,000 58,000 55,000 70,000 59,000 2-Butanone (MEK) 4,000 31,000 19,000 5000 U 2500 U 18,000 2500 U 8,200 5,800 5000 U 3,800 6,000 2,900 5,700 2500 U 2500 U 2500 U Chloroform 70 1000 U 500 U 1000 U 500 U 500 U 260 J 130 500 U 170 140 500 U 500 U 500 U 500 U 500 U 500 U 1,1,1-Trichloroethane 200 6,500 5,000 5,900 5800 J 5,300 6,000 1,600 3,700 2,900 3,600 4,300 J 3,500 2,800 1,800 2,200 2,100 Benzene 1 1000 U 500 U 1000 U 500 U 500 U 500 U 50 U 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U 1,2-Dichloroethane 0.4 1000 U 350 J 1000 U 250 J 290 J 380 J 180 500 U 210 200 500 U 500 U 500 U 500 U 500 U 500 U Trichloroethene 3 150,000 120,000 120,000 100,000 82,000 70,000 32,000 37,000 18,000 15,000 14,000 7,400 11,000 32,000 7,300 6,600 4-Methyl-2-pentanone (MIBK) NE 5000 U 2500 U 5000 U 2500 U 2500 U 2500 U 110 J 2500 U 500 U 500 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Toluene 600 5,300 4,700 5,400 4,600 3,900 4,600 2,700 4,100 3,200 3,400 5,400 4,400 3,700 3,800 3,900 3,900 Tetrachloroethene 0.7 1000 U 500 U 1000 U 500 U 500 U 500 U 54 500 U 68 J 73 J 500 U 500 U 500 U 500 U 500 U 500 U m&p-Xylenes 500 2000 U 1000 U 2000 U 1000 U 1000 U 1000 U 51 J 1000 U 200 U 200 U 1000 U 1000 U 1000 U 1000 U 1000 U 1000 U o-X lene 500 1000 U 500 U 1000 U 500 U 500 U 500 U 50 U 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U Styrene 70 1000 U 500 U 1000 U 500 U 500 U 500 U 50 U 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U n-But (benzene 70 1000 U 500 U 1000 U 500 U 500 U 500 UJ 50 U 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U Naphthalene 6 1000 U 500 U 1000 U 500 UJ 500 U 500 U 190 550 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U 1,2,3-Trichlorobenzene NE 1000 U 500 U 1000 U 500 U 500 U 250 J 50 U 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U Vinyl acetate NE NA 2500 U 5000 UJ 2500 UJ 2500 U 2500 UJ 250 U 2500 U 500 U 500 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Eth (benzene 600 1000 U 500 U 1000 U 500 U 500 U 500 U 50 U 500 U 100 U 100 U 500 U 500 U 500 U 500 U 500 U 500 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 1 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in p g/L) 2L Standards MW-100B Jan-10 Oct-02 Feb-03 Apr-03 Jun-03 Sep-03 Dec-03 May-04 Sep-04 Dec-04 Jun-05 Dec-05 Mar-06 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 1000 U 500 U 1000 U 1000 U 500 U 500 U 200 500 U 500 U 640 500 U 2500 U 2500 U 2500 U 2500 U 2500 U Chloromethane 3 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 UJ 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Vinyl chloride 0.03 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Chloroethane 3000 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Trichlorofluoromethane 2,000 1000 U 500 U 1600 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1-Dichloroethene 7 2,000 1,300 1 1000 U 1,200 1 1,500 1,700 1 1,800 1,100 1 1,400 2,200 1 1,500 1,100 1 960 840 1 1,000 1,400 Trichlorotrifluoroethane 200,000 35,000 36,000 9,200 34,000 27,000 46,000 80,000 71,000 28,000 32,000 39,000 33,000 28,000 26,000 27000 26,000 Carbon disulfide 700 5000 U 2500 U 5000 U 5000 U 2500 U 2500 U 500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Acetone 6000 13,000 2500 U 5000 U 2,400 J 2500 U 24,000 J 500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Methylene chloride 5 230,000 54,000 31,000 37,000 46,000 48,000 60,000 20,000 68,000 75,000 J 27,000 12,000 10,000 1,700 1,700 28,000 trans- 1,2-Dichloroethene 100 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 1,200 500 U 500 U 500 U 500 U 500 U Meth I-tert-but I -ether MTBE 20 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1-Dichloroethane 6 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U cis- 1,2-Dichloroethene 70 12,000 10,000 15,000 14,000 19,000 30,000 45,000 59,000 59,000 41,000 69,000 73,000 61,000 65,000 67,000 61,000 2-Butanone (MEK) 4,000 27,000 12,000 5000 U 9,200 9,600 2500 U 4,800 2500 U 2500 U 1,900 2500 U 2500 U 2500 U 5,500 4,900 2,800 Chloroform 70 1000 U 290 J 1000 U 1000 U 270 J 350 J 280 500 U 310 J 340 500 U 500 U 500 U 500 U 500 U 500 U 1,1,1-Trichloroethane 200 8,000 6,100 3,100 6100 6,900 6,300 4,100 4,300 2,300 2,800 3,300 J 2,900 2,900 2,400 2,100 1,800 Benzene 1 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,2-Dichloroethane 0.4 1000 U 400 J 1000 U 1000 U 420 J 400 J 250 500 U 500 U 340 500 U 500 U 500 U 500 U 500 U 500 U Trichloroethene 3 190,000 160,000 65,000 120,000 120,000 100,0001 98,000 50,000 64,000 43,000 29,000 13,000 21,000 1,900 3,100 27,000 4-Methyl-2-pentanone (MIBK) NE 5000 U 2500 U 5000 U 5000 U 2500 U 2500 U 500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Toluene 600 6,900 5,700 3,400 4,900 5,900 5,800 5,400 4,900 4,200 4,400 5,300 4,300 4,200 3,600 3,800 4,600 Tetrachloroethene 0.7 1000 U 210 J 1000 U 1000 U 500 U 500 U 200 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U m&p-Xylenes 500 2000 U 1000 U 2000 U 2000 U 1000 U 1000 U 100 J 1000 U 1000 U 400 U 1000 U 1000 U 1000 U 1000 U 1000 U 1000 U o-X lene 500 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Styrene 70 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U n-But (benzene 70 1000 U 500 U 1000 U 1000 U 500 U 500 UJ 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Naphthalene 6 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 550 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,2,3-Trichlorobenzene NE 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Vinyl acetate NE NA 2500 U 5000 UJ 5000 U 2500 U 2500 UJ 500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Eth (benzene 600 1000 U 500 U 1000 U 1000 U 500 U 500 U 100 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 2 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in p g/L) 2L Standards MW-101A Jan-10 Oct-02 2 Feb-03 2 Apr-03 Jun-03 Sep-03 Dec-03 May-04 Sep-04 Dec-04 Jun-05 Dec-05 Mar-06 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 2500 U 2500 U 2500 U 2500 U 2500 U Chloromethane 3 100 U 5000 U 1000 U 500 U 500 U 500 U 500 UJ 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Vinyl chloride 0.03 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Chloroethane 3000 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Trichlorofluoromethane 2,000 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1-Dichloroethene 7 1,200 5000 U 1000 U 650 1 770 500 U 1 870 570 1 370 J 630 1 500 500 U 1 520 500 U 1 550 500 U Trichlorotrifluoroethane 200,000 56,000 62,000 93,000 42,000 40,000 14,000 110,000 92,000 24,000 34,000 37,000 33,000 31,000 15,000 32000 16,000 Carbon disulfide 700 500 U 25000 U 5000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Acetone 6000 500 U 31,000 5000 U 2500 U 2500 U 6,300 1,700 J 2500 U 2500 U 2,000 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Methylene chloride 5 20,000 5000 U 3,800 4,300 6,400 5,000 7,700 2,000 1,800 2,900 J 1,500 770 800 500 U 500 U 500 U trans- 1,2-Dichloroethene 100 48 J 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Meth I-tert-but I -ether MTBE 20 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1-Dichloroethane 6 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U cis- 1,2-Dichloroethene 70 800 5000 U 1000 U 340 J 500 J 550 2,600 1,200 800 1,000 4,400 3,400 1,900 1,100 5,900 1,000 2-Butanone (MEK) 4,000 2,700 25000 U 5000 U 2500 U 2500 U 2500 UJ 2500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Chloroform 70 590 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1,1-Trichloroethane 200 37,000 20,000 22,000 13,000 11 000 7 300 12,000 9,100 5,500 9,000 8,200 6,000 5,400 3,600 4,500 1,900 Benzene 1 120 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,2-Dichloroethane 0.4 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Trichloroethene 3 390,000 270,000 250,000 110,000 99 000 73 000 190,000 100,000 76,000 62,000 91,000 64,000 66,000 36,000 54,000 23,000 4-Methyl-2-pentanone (MIBK) NE 500 U 25000 U 5000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Toluene 600 13,000 9,400 14,000 6,500 4 400 3 100 5,900 4,100 2,700 3,100 4,100 3,100 2,800 1,600 2,600 1000 Tetrachloroethene 0.7 470 5000 U 670 J 500 U 500 U 500 U 500 U 500 U 500 U 160 J 500 U 500 U 500 U 500 U 500 U 500 U m&p-Xylenes 500 270 10000 U 2000 U 1000 U 1000 U 1000 U 1000 U 1000 U 1000 U 400 U 1000 U 1000 U 1000 U 1000 U 1000 U 1000 U o-X lene 500 93 J 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Styrene 70 72 J 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U n-But (benzene 70 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Naphthalene 6 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 540 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,2,3-Trichlorobenzene NE 100 U 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Vinyl acetate NE NA 25000 U 5000 U 2500 U 2500 U 2500 UJ 2500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Eth (benzene 600 89 J 5000 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 3 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in p g/L) 2L Standards MW-1018 Jan-10 Oct-02 Feb-03 Apr-032 Jun-032 Sep-032 Dec-032 May-042 Sep-042 Dec-042 Jun-052 Dec-052 Mar-06 Jun-062 Sep-062 Apr-072 Oct-072 Dichlorodifluoromethane 1,000 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 2500 U 2500 U 2500 U 2500 U 2500 U Chloromethane 3 500 U 500 U 1000 U 500 U 500 U 500 U 500 UJ 500 U 500 UJ 200 U 500 U 500 U 500 U 500 U 500 U 500 U Vinyl chloride 0.03 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 UJ 200 U 500 U 500 U 500 U 500 U 500 U 500 U Chloroethane 3000 500 U 260 J 1000 U 500 U 500 U 500 U 500 U 500 U 500 UJ 200 U 500 U 500 U 500 U 500 U 500 U 500 U Trichlorofluoromethane 2,000 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1-Dichloroethene 7 1800 1300 1 1200 1300 1 1400 1400 1 1200 620 1 850 1,100 1 1,300 1,100 1 1,100 1,100 1 1,200 1,200 Trichlorotrifluoroethane 200,000 39,000 34000 33,000 26,000 21,000 43,000 83,000 73,000 47,000 42,000 35,000 31,200 29,000 29,000 29000 28,000 Carbon disulfide 700 2500 U 2500 U 5000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Acetone 6000 2500 U 2500 U 5000 U 2500 U 2500 U 19,000 J 2500 U 2500 U 2500 UJ 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Methylene chloride 5 13,000 10,000 11,000 8,300 10,000 8,000 8,100 2,300 3,600 6,200 J 4,500 3,000 2,600 2,600 2,400 2,400 trans- 1,2-Dichloroethene 100 500 U 500 UJ 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Meth I-tert-but I -ether MTBE 20 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1-Dichloroethane 6 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 UJ 200 U 500 U 500 U 500 U 500 U 500 U 500 U cis- 1,2-Dichloroethene 70 1,000 700 870 J 900 1,200 1,400 1,300 2,100 2,300 10,000 27,000 28,000 24,000 31,000 22,000 20,000 2-Butanone (MEK) 4,000 2500 U 2500 U 5000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 UJ 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Chloroform 70 450 J 380 J 1000 U 330 J 350 J 320 J 500 U 500 U 500 UJ 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,1,1-Trichloroethane 200 18,000 8,700 9,100 9,800 8 800 7 500 8,100 7,400 8,200 J 8,100 6,200 4,900 4,900 4,300 3,500 3,000 Benzene 1 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,2-Dichloroethane 0.4 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 UJ 200 U 500 U 500 U 500 U 500 U 500 U 500 U Trichloroethene 3 380,000 120,000 140,000 130,000 130 000 94 000 150,000 93,000 99,000 79,000 69,000 58,700 64,000 44,000 53,000 46,000 4-Methyl-2-pentanone (MIBK) NE 2500 U 2500 U 5000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Toluene 600 9,000 4,400 5,000 4,400 4 600 3,700 4,100 3,500 3,600 3,100 3,900 3,400 3,400 3,100 2,800 2,700 Tetrachloroethene 0.7 330 J 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 150 J 200 U 500 U 500 U 500 U 500 U 500 U 500 U m&p-Xylenes 500 1000 U 1000 U 2000 U 1000 U 1000 U 1000 U 1000 U 1000 U 1000 U 400 U 1000 U 1000 U 1000 U 1000 U 1000 U 1000 U o-X lene 500 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 UJ 200 U 500 U 500 U 500 U 500 U 500 U 500 U Styrene 70 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U n-But (benzene 70 500 U 500 U 1000 U 500 U 500 U 500 UJ 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Naphthalene 6 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 590 500 UJ 200 U 500 U 500 U 500 U 500 U 500 U 500 U 1,2,3-Trichlorobenzene NE 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Vinyl acetate NE NA 2500 UJ 5000 UJ 2500 U 2500 U 2500 UJ 2500 U 2500 U 2500 UJ 1000 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U Eth (benzene 600 500 U 500 U 1000 U 500 U 500 U 500 U 500 U 500 U 500 U 200 U 500 U 500 U 500 U 500 U 500 U 500 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 4 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in k g1L) 2L Standards MW-102A Jan-10 Oct-02 Feb-03 Apr-03 Jun-03 Sep-03 Dec-03 May-04 Sep-04 Dec-04 Jun-05 Dec-05 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 100 U 50 U 25 U 14 50 U 25 U 20 U 10 U 10 U 5 U 1.6 5 U 25 U 25 U 5 U Chloromethane 3 100 U 50 U 25 U 10 U 50 U 25 U 20 UJ 10 U 10 U 5 U 1 U 1 U 5 U 5 U 1 U Vinyl chloride 0.03 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 U 10 0 5 U 1 U 1 U 5 U 5 U 1 U Chloroethane 3000 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 U 10 U 5 U 1 U 1 U 5 U 5 U 1 U Trichlorofluoromethane 2,000 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 U 10 0 5 U 1 U 1 U 5 U 5 U 1 U 1,1-Dichloroethene 7 100 U 48 J 25 U 20 25 J 25 U 20 U 10 U 10 0 5 U 2.2 4.4 5 U 13 1 U Trichlorotrifluoroethane 200,000 3,700 4600 970 4,100 2,500 3,300 6,500 4,100 2,600 1,500 580 1500 1,000 1,800 1,400 Carbon disulfide 700 500 U 250 U 120 U 50 U 250 U 120 U 100 U 12 J 50 U 25 U 5 U 5 U 25 U 25 U 5 U Acetone 6000 500 U 250 U 120 U 50 U 250 U 1,500 100 U 50 U 50 U 25 UJ 5 U 5.3 25 U 25 U 5 U Methylene chloride 5 130 50 U 25 U 10 U 60 25 U 100 10 U 10 U 5 U 1.6 1 U 5 U 5 U 1 U trans- 1,2-Dichloroethene 100 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 U 10 U 5 U 1 U 1 U 5 U 5 U 1 U Meth I-tert-but I -ether MTBE 20 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 U 10 U 5 U 1 U 1 U 5 U 5 U 1 U 1,1-Dichloroethane 6 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 U 10 U 5 U 1 U 1 U 5 U 5 U 1 U cis- 1,2-Dichloroethene 70 51 J 86 25 U 5.2 J 56 25 U 20 U 10 U 10 U 6.5 29 17 8.6 61 8 2-Butanone (MEK) 4,000 500 U 250 U 120 U 50 U 250 U 120 UJ 100 U 50 UJ 50 U 25 U 8.2 10 25 U 25 U 5 U Chloroform 70 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 0 10 0 5 U 1 U 1 U 5 U 5 U 1 U 1,1,1-Trichloroethane 200 180 180 83 45 77 25 U 20 U 10 U 10 U 5 U 2.8 1 U 5 U 23 1 U Benzene 1 1000 50U 25U 10U 50U 25U 20U 10U 10U 5U 1 U 1 U 5U 5U 1 U 1,2-Dichloroethane 0.4 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 U 10 U 5 U 1 U 1 U 5 U 5 U 1 U Trichloroethene 3 6,200 3,500 1,200 760 1,700 25 J 33 25 22 11 44 14 14 920 11 4-Methyl-2-pentanone (MIBK) NE 500 U 250 U 120 U 50 U 250 U 120 U 100 U 50 UJ 50 U 25 U 5 U 5 U 25 U 25 U 5 U Toluene 600 220 130 67 28 73 25 U 20 U 10 U 10 U 5 U 4.4 1.9 5 U 62 1 U Tetrachloroethene 0.7 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 U 10 U 5 U 1 U 1 U 5 U 5 U 1 U m&p-Xylenes 500 200 U 100 U 50 U 20 U 100 U 50 U 40 U 20 U 20 U 5.2 J 2 U 2 U 10 U 10 U 2 U o-X lene 500 100 U 50 U 25 U 10 0 50 U 25 U 20 U 10 U 10 U 5 U 1 U 1 U 5 U 5 U 1 U Styrene 70 1000 50U 25U 100 50U 25U 20U 101-1 10U 5U 1U 1U 5U 5U 1U n-But (benzene 70 100 U 50 U 25 U 10 0 50 U 25 U 20 U 10 UJ 10 U 6.2 1 U 1 U 5 U 5 U 1 U Naphthalene 6 100 U 50 U 25 U 10 UJ 50 U 25 U 20 U 10 0 10 U 7.6 1 U 1 U 5 U 5 U 1 U 1,2,3-Trichlorobenzene NE 100 U 50 U 25 U 10 0 50 U 25 U 20 U 10 0 10 U 5 U 1 U 1 U 5 U S U 1 U Vinyl acetate NE NA 250 U 120 U 50 UJ 250 U 120 UJ 100 U 50 UJ 50 U 25 U 5 U 5 U 25 U 25 U 5 U Eth (benzene 600 100 U 50 U 25 U 10 U 50 U 25 U 20 U 10 U 10 U 5 U 1 U 1 U S U S U 1 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 5 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in k g1L) 2L Standards MW-102B Jan-10 Oct-02 Feb-03 Apr-03 Jun-03 Sep-03 Dec-03 May-04 Sep-04 Dec-04 Jun-05 Dec-05 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 250 U 250 U 250 U 250 U Chloromethane 3 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U Vinyl chloride 0.03 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U Chloroethane 3000 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U Trichlorofluoromethane 2,000 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U 1,1-Dichloroethene 7 70 J 270 100 200 210 190 160 50 U 170 1101 170 98 110 130 120 Trichlorotrifluoroethane 200,000 1,600 24000 6,900 15,000 12,000 14,000 17,000 20,000 11,000 7,900 9,500 5,800 6,700 7,000 6,700 Carbon disulfide 700 500 U 500 U 500 U 500 U 500 U 500 U 500 U 250 U 250 U 100 U 250 U 250 U 250 U 250 U 250 U Acetone 6000 500 U 500 U 500 U 500 U 500 U 5000 U 320 J 250 U 250 U 100 UJ 250 U 250 U 250 U 250 U 250 U Methylene chloride 5 100 U 58 J 100 U 100 57 J 100 U 100 U 50 U 72 23 50 U 50 U 50 U 50 U 50 U trans- 1,2-Dichloroethene 100 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U Meth I-tert-but I -ether MTBE 20 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U 1,1-Dichloroethane 6 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U cis- 1,2-Dichloroethene 70 75 J 48 J 100 U 100 U 75 J 57 J 100 U 53 60 33 94 730 2,000 3,200 2,400 2-Butanone (MEK) 4,000 500 U 500 U 500 U 500 U 500 U 500 U 500 U 250 UJ 250 U 100 U 250 U 250 U 250 U 250 U 250 U Chloroform 70 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U 1,1,1-Trichloroethane 200 59 J 1,700 670 900 740 480 290 290 310 140 200 110 110 97 71 Benzene 1 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U 1,2-Dichloroethane 0.4 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U Trichloroethene 3 7,400 31,000 11,000 17,000 14,000 9,100 11,000 10,000 10,000 5,500 8,800 5,500 3,300 2,800 2,300 4-Methyl-2-pentanone (MIBK) NE 500 U 500 U 500 U 500 U 500 U 500 U 500 U 250 UJ 250 U 100 U 250 U 250 U 250 U 250 U 250 U Toluene 600 100 U 820 380 450 390 220 200 190 160 110 150 J 100 87 110 83 Tetrachloroethene 0.7 100 U 46 J 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U m&p-Xylenes 500 200 U 200 U 200 U 200 U 200 U 200 U 200 U 100 U 100 U 40 U 100 U 100 U 100 U 100 U 100 U o-X lene 500 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U Styrene 70 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U n-But (benzene 70 100 U 100 U 100 U 100 U 100 U 100 UJ 100 U 50 UJ 50 U 20 U 50 U 50 U 50 U 50 U 50 U Naphthalene 6 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U 1,2,3-Trichlorobenzene NE 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U Vinyl acetate NE NA 500 U 500 UJ 500 U 500 U 500 UJ 500 U 250 UJ 250 U 100 U 250 U 250 U 250 U 250 U 250 U Eth (benzene 600 100 U 100 U 100 U 100 U 100 U 100 U 100 U 50 U 50 U 20 U 50 U 50 U 50 U 50 U 50 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 6 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in k g1L) 2L Standards MW-102C Jan-10 Oct-02 Feb-03 Apr-03 Jun-03 Sep-03 Dec-03 May-04 Sep-04 Dec-04 Jun-05 Dec-05 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 50 U 50 U 10 U 5 U 10 U 10 U 24 20 U 20 U 20 U 5.8 25 U 250 U 50 U 500 U Chloromethane 3 50 U 50 U 10 U 5 U 10 U 10 U 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U Vinyl chloride 0.03 50 U 50 U 10 U 5 U 10 U 10 U 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U Chloroethane 3000 50 U 50 U 10 U 5 U 10 U 10 U 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U Trichlorofluoromethane 2,000 50 U 50 U 10 U 5 U 10 U 10 U 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U 1,1-Dichloroethene 7 94 51 26 12 42 10 U 67 82 82 20 U 46 110 130 61 380 Trichlorotrifluoroethane 200,000 2,500 1800 1,600 530 990 1,200 2,300 3,200 1,800 1,800 1,000 3,300 2,400 1,500 5,800 Carbon disulfide 700 250 U 250 U 50 U 25 U 50 U 50 U 50 U 100 U 100 U 100 U 25 U 25 U 250 U 50 U 500 U Acetone 6000 250 U 250 U 50 U 140 50 U 570 190 100 U 100 U 100 UJ 25 U 27 250 U 50 U 500 U Methylene chloride 5 50 U 50 U 10 U 5 U 8.1 J 10 0 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U trans- 1,2-Dichloroethene 100 50 U 50 U 10 U 5 U 10 U 10 0 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U Meth I-tert-but I -ether MTBE 20 50 U 50 U 10 U 5 U 10 U 10 0 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U 1,1-Dichloroethane 6 50 U 50 U 10 U 5 U 10 U 10 U 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U cis- 1,2-Dichloroethene 70 91 410 380 130 100 230 240 210 220 240 300 460 640 870 5,400 2-Butanone (MEK) 4,000 250 U 250 U 50 U 26 50 U 50 UJ 24 J 100 UJ 100 U 100 U 25 U 32 250 U 50 U 500 U Chloroform 70 25 J 50 U 5.2 J 3.1 J 7.7 J 11 10 U 20 U 20 U 20 U 5 U 7.2 50 U 10 U 100 U 1,1,1-Trichloroethane 200 74 50 U 91 17 49 55 34 50 39 26 5 U 32 50 U 12 100 U Benzene 1 50U 50U 10U 5U 10U 10U 10U 20U 20U 20U 5U 5U 50U 10U 1000 1,2-Dichloroethane 0.4 31 J 50 U 10 U 3.2 J 7.9 J 11 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U Trichloroethene 3 8,000 4,200 2,100 920 2,600 2,300 2,700 3,500 3,700 3,900 2,100 6,800 5,800 2,500 12,000 4-Methyl-2-pentanone (MIBK) NE 250 U 250 U 50 U 25 U 50 U 50 U 50 U 100 UJ 100 U 100 U 25 U 25 U 250 U 50 U 500 U Toluene 600 43 J 110 66 6.7 16 17 25 17 J 13 J 20 U 8.3 J 21 50 U 11 100 U Tetrachloroethene 0.7 50 U 50 U 5.9 J 5 U 10 U 10 0 10 U 20 U 20 U 20 U 5 U 5.9 50 U 10 U 100 U m&p-Xylenes 500 100 U 100 U 20 U 10 0 20 U 20 U 20 U 40 U 40 U 40 U 10 U 10 U 100 U 20 U 200 U o-Xlene 500 50U 50U 10U 5U 10U 100 10U 20U 20U 20U 5U 5U 50U 10U 1000 Styrene 70 50U 50U 10U 5U 10U 100 10U 20U 20U 20U 5U 5U 50U 10U 1000 n-But (benzene 70 50 U 50 U 10 U 5 U 10 U 10 0 10 U 20 UJ 20 U 20 U 5 U 5 U 50 U 10 U 100 U Naphthalene 6 50U 50U 10U 5UJ 10U 100 10U 20U 20U 20U 5U 5U 50U 10U 1000 1,2,3-Trichlorobenzene NE 50 U 50 U 10 U 5 U 10 U 10 0 10 U 20 U 20 U 20 U 5 U 5 U 50 U 10 U 100 U Vinyl acetate NE NA 250 U 50 U 25 UJ 50 U 50 UJ 50 U 100 UJ 100 U 100 U 25 U 25 U 250 U 50 U 500 U Eth (benzene 600 50 U 1 50 U 1 10 U 5 U 10 U 10 U 10 U 20 U 20 U 20 U 5 0 1 5 U 50 U I 10 ii I100 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 7 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in k g1L) 2L Standards MW-103A Jan-10 Oct-02 Feb-03 Apr-03 Jun-03 Sep-03 Dec-03 May-04 Sep-04 Dec-04 Jun-05 Dec-05 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 19 500 U 250 U 60 100 U 100 U 130 20 U 100 U 10 U 5 U 25 U 25 U 25 U 25 U Chloromethane 3 1.6 500 U 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U Vinyl chloride 0.03 1 U 500 U 250 U 50 U 67 J 60 J 61 35 100 U 18 8.7 8.3 20 18 41 Chloroethane 3000 1 U 280 J 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U Trichlorofluoromethane 2,000 1.3 500 U 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U 1,1-Dichloroethene 7 1 U 500 U 250 U 47 J 82 J 100 U 61 20 U 100 U 15 J 6.4 9.9 47 25 27 Trichlorotrifluoroethane 200,000 5,700 25000 16,000 12,000 25,000 12000 21,000 9,800 17,000 2,800 1,900 4,800 13,000 9,600 6,600 Carbon disulfide 700 5 U 2500 U 1200 U 250 U 500 U 500 U 250 U 100 U 500 U 50 U 25 U 25 U 25 U 25 U 25 U Acetone 6000 5 U 2500 U 1200 U 250 U 500 U 5,400 810 100 U 460 J 50 UJ 25 U 25 U 25 U 25 U 25 U Methylene chloride 5 0.92 J 500 U 250 U 50 U 67 J 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U trans- 1,2-Dichloroethene 100 1 U 500 UJ 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5.7 5 U 5 U 5 U 5 U Meth I-tert-but I -ether MTBE 20 7.8 500 U 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U 1,1-Dichloroethane 6 0.44 J 500 U 250 U 50 U 100 U 100 U 50 U 14 J 100 U 10 U 5 U 5 U 5 U 5 U 5 U cis- 1,2-Dichloroethene 70 88 290 J 540 720 1,000 1,100 1,800 3,900 1,700 720 380 360 320 230 670 2-Butanone (MEK) 4,000 5 U 2500 U 1200 U 250 U 500 U 500 UJ 250 U 100 UJ 500 U 50 U 25 U 25 U 25 U 25 U 25 U Chloroform 70 2.8 500 U 250 U 50 U 100 U 100 U 50 U 101 100 U 10 U 5 U 5 U 5 U 5 U 5 U 1,1,1-Trichloroethane 200 1 U 500 U 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U Benzene 1 0.59 J 500 U 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U 1,2-Dichloroethane 0.4 0.91 J 500 U 250 U 50 U 100 U 100 U 50 U 30 100 U 10 U 5 U 5 U 5 U 5 U 11 Trichloroethene 3 36 500 U 250 U 72 230 88 J 52 27 100 35 23 9.2 27 20 56 4-Methyl-2-pentanone (MIBK) NE 5 U 2500 U 1200 U 250 U 500 U 500 U 250 U 100 UJ 500 U 50 U 25 U 25 U 25 U 25 U 25 U Toluene 600 0.61 J 500 U 250 U 50 U 100 U 100 U 50 U 12 J 100 U 10 U 5 U 8.4 5 U 5 U 15 Tetrachloroethene 0.7 0.63 J 500 U 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U m&p-Xylenes 500 2 U 1000 U 500 U 100 U 200 U 200 U 100 U 40 U 200 U 20 U 10 U 10 U 10 U 10 U 10 U o-X lene 500 1 U 500 U 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U Styrene 70 1U 5000 250U 50U 1000 1000 50U 20U 1000 10U 5U 5U 5U 5U 5U n-But (benzene 70 1 U 500 U 250 U 50 U 100 U 100 U 50 U 20 UJ 100 U 1 10 U 5 U 5 U 5 U 5 U 5 U Naphthalene 6 1 U 500 U 250 U 50 UJ 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U 1,2,3-Trichlorobenzene NE 1 U 500 U 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U Vinyl acetate NE NA 2500 UJ 1200 U 250 UJ 500 U 500 UJ 250 U 100 UJ 500 U 50 U 25 U 25 U 25 U 25 U 25 U Eth (benzene 600 1 U 500 U 250 U 50 U 100 U 100 U 50 U 20 U 100 U 10 U 5 U 5 U 5 U 5 U 5 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 8 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in k g1L) 2L Standards MW-103B Jan-10 Oct-02 Feb-03 Apr-03 Jun-03 Sep-03 Dec-03 May-04 Sep-04 Dec-04 Jun-05 Dec-05 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 14 50 U 50 U 49 J 100 U 100 U 100 U 200 U 100 U 20 U 38 25 U 25 U 25 U 25 U Chloromethane 3 1.8 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U Vinyl chloride 0.03 1 U 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 23 27 12 18 21 27 Chloroethane 3000 1 U 26 J 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U Trichlorofluoromethane 2,000 0.83 J 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 1 U 5 U 5 U 5 U 1,1-Dichloroethene 7 1 U 50 U 50 U 59 100 100 U 110 200 U 100 U 20 U 41 37 50 90 40 Trichlorotrifluoroethane 200,000 8,100 15000 1,800 15,000 17,000 21,000 50,000 34,000 26,000 18,000 12,000 16,000 9,900 16,000 16,000 Carbon disulfide 700 5 U 250 U 250 U 250 U 500 U 500 U 500 U 1000 U 500 U 100 U 25 U 25 U 25 U 25 U 25 U Acetone 6000 5 U 250 U 250 U 250 U 500 U 9,700 1,900 1000 U 500 U 100 UJ 25 U 25 U 25 U 25 U 25 U Methylene chloride 5 1.1 50 U 50 U 50 U 100 U 100 U 110 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U trans- 1,2-Dichloroethene 100 1 U 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 6.7 5 U 5 U 5 U 5 U Meth I-tert-but I -ether MTBE 20 7.8 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U 1,1-Dichloroethane 6 0.47 J 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U cis- 1,2-Dichloroethene 70 99 160 190 580 750 600 970 2,100 990 690 690 440 420 410 550 2-Butanone (MEK) 4,000 5 U 250 U 250 U 250 U 500 U 500 UJ 500 U 1000 UJ 500 U 100 U 25 U 25 U 25 U 25 U 25 U Chloroform 70 3.3 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U 1,1,1-Trichloroethane 200 1 U 50 U 110 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U Benzene 1 1 U 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U 1,2-Dichloroethane 0.4 1.1 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 8 Trichloroethene 3 34 83 1,300 71 150 110 100 200 U 79 J 65 53 77 41 39 49 4-Methyl-2-pentanone (MIBK) NE 5 U 250 U 250 U 250 U 500 U 500 U 500 U 1000 UJ 500 U 100 U 25 U 25 U 25 U 25 U 25 U Toluene 600 1.2 50 U 82 50 U 100 U 100 U 130 200 U 100 U 20 U 5 U 5.2 5 U 5 U 9 Tetrachloroethene 0.7 0.57 J 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U m&p-Xylenes 500 2 U 100 U 100 U 100 U 200 U 200 U 200 U 400 U 200 U 40 U 10 U 10 U 10 U 10 U 10 U o-X lene 500 1 U 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U Styrene 70 1 U 50 U 50 U 50 U 100 0 100 0 100 0 200 0 100 0 20 U 5 U 5 U 5 U 5 U 5 U n-But (benzene 70 1 U 50 U 50 U 50 U 100 U 100 U 100 U 200 UJ 100 U 20 U 5 U 5 U 5 U 5 U 5 U Naphthalene 6 1 U 50 U 50 U 50 UJ 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U 1,2,3-Trichlorobenzene NE 1 U 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U 5 U 5 U 5 U 5 U Vinyl acetate NE NA 250 U 250 U 250 UJ 500 U 500 UJ 500 U 1000 UJ 500 U 100 U 25 U 25 U 25 U 25 U 25 U Eth (benzene 600 1 U 50 U 50 U 50 U 100 U 100 U 100 U 200 U 100 U 20 U 5 U S U 1,11 5 U S U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 9 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in k g1L) 2L Standards MW-103C Jan-10 Oct-02 Feb-03 Apr-03 Jun-03 Sep-03 Dec-03 May-04 Sep-04 Dec-04 Jun-05 Dec-05 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 8.4 13 100 U 23 50 U 50 U 110 100 U 25 U 10 U 37 25 U 25 U 25 U 25 U Chloromethane 3 1 U 10 U 100 U 10 U 50 U 50 U 50 U 100 U 25 U 10 U 10 0 5 U 5 U 5 U 5 U Vinyl chloride 0.03 1 U 10 U 100 U 10 U 50 U 50 U 50 U 100 U 23 J 16 16 6.1 20 17 20 Chloroethane 3000 1 U 10 U 100 U 10 U 50 U 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5 U 5 U Trichlorofluoromethane 2,000 14 9.3 J 100 U 8 J 50 U 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5 U 5 U 1,1-Dichloroethene 7 1 U 19 100 U 18 50 U 50 U 50 U 100 U 25 U 10 U 25 13 30 37 39 Trichlorotrifluoroethane 200,000 2,900 3500 4,300 3,400 6,400 6,500 17,000 15,000 11,000 5,900 7,600 7,100 6,200 7,400 9,800 Carbon disulfide 700 5 U 50 U 500 U 50 U 250 U 250 U 250 U 500 U 120 U 50 U 50 U 25 U 25 U 25 U 25 U Acetone 6000 5 U 50 U 500 U 50 U 250 U 2,700 660 500 U 120 U 50 UJ 50 U 25 U 25 U 25 U 25 U Methylene chloride 5 1.2 10 U 100 U 10 0 28 J 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5 U 5 U trans- 1,2-Dichloroethene 100 0.55 J 10 U 100 U 10 U 50 U 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5 U 5 U Meth I-tert-but I -ether MTBE 20 1 U 10 U 100 U 10 U 50 U 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5 U 5 U 1,1-Dichloroethane 6 1.2 10 U 100 U 10 U 50 U 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5 U 5 U cis- 1,2-Dichloroethene 70 300 290 500 510 520 500 650 960 1,000 690 760 360 720 700 810 2-Butanone (MEK) 4,000 5 U 50 U 500 U 50 U 250 U 250 UJ 250 U 500 UJ 120 U 50 U 50 U 25 U 25 U 25 U 25 U Chloroform 70 4.6 5.1 J 100 U 6.4 J 50 U 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5.2 5 1,1,1-Trichloroethane 200 1 U 10 U 100 U 4.3 J 49 J 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5 U 5 U Benzene 1 1U 101.1 1000 100 50U 50U 50U 1000 25U 10U 10U 5U 5U 5U 5U 1,2-Dichloroethane 0.4 3.5 10 U 100 U 6.6 J 50 U 50 U 50 U 100 U 25 U 10 U 10 U 5 U 7 6.9 8 Trichloroethene 3 43 270 500 150 550 60 76 60 J 71 47 57 28 50 56 56 4-Methyl-2-pentanone (MIBK) NE 5 U 50 U 500 U 50 U 250 U 250 U 250 U 500 UJ 120 U 50 U 50 U 25 U 25 U 25 U 25 U Toluene 600 0.59J 13 1000 100 50U 50U 50U 1000 25U 10U 10U 5U 5U 5U 5U Tetrachloroethene 0.7 0.55 J 10 U 100 U 10 U 50 U 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5 U 5 U m&p-Xylenes 500 2 U 20 U 200 U 20 U 100 U 100 U 100 U 200 U 50 U 20 U 20 U 10 U 10 U 10 U 10 U o-Xlene 500 1U 10U 1000 100 50U 50U 50U 1000 25U 10U 10U 5U 5U 5U 5U Styrene 70 1U 10U 1000 100 50U 50U 50U 1000 25U 10U 10U 5U 5U 5U 5U n-But (benzene 70 1 U 10 U 100 U 10 0 50 U 50 U 50 U 100 UJ 25 U 10 U 10 U 5 U 5 U 5 U 5 U Naphthalene 6 1U 10U 1000 10 UJ 50U 50U 50U 1000 25U 10U 10U 5U 5U 5U 5U 1,2,3-Trichlorobenzene NE 1 U 10 U 100 U 10 0 50 U 50 U 50 U 100 U 25 U 10 U 10 U 5 U 5 U 5 U 5 U Vinyl acetate NE NA 50 U 500 U 50 UJ 250 U 250 UJ 250 U 500 UJ 120 U 50 U 50 U 25 U 25 U 25 U 25 U Eth (benzene 600 1 U 10 U 100 U 10 U 50 U 50 U 50 U 100 U 25 U 10 U 10 U S U 1,11 5 U S U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 10 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in p g/L) 2L Standards MW-104A MW-104B Jan-10 Sep-04 Dec-04 Jun-05 Dec-05 Jun-06 Sep-06 Apr-07 Oct-07 Sep-042 Dec-042 Jun-052 Dec-052 Jun-062 Sep-062 Apr-072 Oct-07 Dichlorodifluoromethane 1,000 20 U IOU 2 U 99 25 U 50 U 25 U 25 U 20 U 10 U 2 U 16 50 U 50 U 25 U 25 U Chloromethane 3 20U 10U 2U 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U Vinyl chloride 0.03 20U 10U 2.9 10U 5U 10U 5U 7 20U 10U 2U 10U 10U 10U 5U 5U Chloroethane 3000 20U 10U 2U 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U Trichlorofluoromethane 2,000 20 U IOU 2 U IOU 5 U IOU 5 U 5 U 20 U IOU 2 U IOU 10 U IOU 5 U 5 U 1,1-Dichloroethene 7 20 U IOU 2 U 15 5 U IOU 5 U 7 20 U IOU 2 U IOU 1 23 30 1 37 30 Trichlorotrifluoroethane 200,000 3,300 2,500 2,200 3,400 980 1,900 1,700 1,400 3,900 1,900 1,300 1,900 1,600 2,000 3,500 2,800 Carbon disulfide 700 100 U 50 U IOU 50 U 25 U 50 U 25 U 25 U 100 U 50 U 10 U 50 U 50 U 50 U 25 U 25 U Acetone 6000 100 U 50 U 10 UJ 50 U 25 U 50 U 25 U 25 U 100 U 50 U 10 UJ 50 U 50 U 50 U 25 U 25 U Methylene chloride 5 20U 10U 2U 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U trans- 1,2-Dichloroethene 100 20 U IOU 2.3 IOU 5 U IOU 5 U 5 U 20 U IOU 2 U IOU 10 U IOU 5 U 5 U Meth I-tert-but I -ether MTBE 20 20 U IOU 2 U IOU 5 U IOU 5 U 5 U 47 49 2 U 14 12 IOU 5 U 10 1,1-Dichloroethane 6 20U 10U 2J 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U cis- 1,2-Dichloroethene 70 470 490 450 890 310 740 700 600 76 75 56 110 110 150 300 170 2-Butanone (MEK) 4,000 100 UJ 50 U IOU 50 U 25 U 50 U 25 U 25 U 100 UJ 50 U 10 U 50 U 50 U 50 U 25 U 25 U Chloroform 70 20U 10U 1.7J 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U 1,1,1-Trichloroethane 200 20 U IOU 2 U IOU 5 U IOU 5 U 5 U 20 U IOU 2 U IOU 10 U IOU 5 U 5 U Benzene 1 20U 10U 2U 10U 5U 10U 5U 5U 20U 6.1J 4 10U 10U 10U 5U 5U 1,2-Dichloroethane 0.4 20 U 10 U 3.1 10 U 5 U 10 U 5 U 5 U 20 U 10 U 2 U 10 U 10 U 10 U 5 U 5 U Trichloroethene 3 20 U 10 U 2.5 10 U 5 U 10 U 5 U 5 U 17 J 17 14 26 22 30 28 27 4-Methyl-2-pentanone (MIBK) NE 100 UJ 50 U 10 U 50 U 25 U 50 U 25 U 25 U 100 UJ 50 U 10 U 50 U 50 U 50 U 25 U 25 U Toluene 600 20U 10U 2U 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U Tetrachloroethene 0.7 20U 10U 2U 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U m&p-Xylenes 500 40 U 20 U 4 U 20 U 10 U 20 U 10 U 10 U 40 U 20 U 4 U 20 U 20 U 20 U 10 U 10 U o-Xlene 500 20U 10U 2U 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U Styrene 70 20U 10U 2U 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U n-But (benzene 70 20 UJ 10U 2U 10U 5U 10U 5U 5U 20 UJ 10U 2U 10U 10U 10U 5U 5U Naphthalene 6 20U 10U 2U 10U 5U 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 1 5U 1,2,3-Trichlorobenzene NE 20 U 10 U 2 U 10 U 5 U 10 U 5 U 5 U 20 U 10 U 2 U 10 U 10 U 10 U 5 U 5 U Vinyl acetate NE 100 UJ 50 U 10 U 50 U 25 U 50 U 25 U 25 U 100 UJ 50 U 10 U 50 U 50 U 50 U 25 U 25 U Eth (benzene 600 20U 10U 2U 10U SU 10U 5U 5U 20U 10U 2U 10U 10U 10U 5U 5U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 11 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in u g1L) 2L Standards MW-104C Jan-10 Sep-04 Dec-04 Jun-05 Dec-05 Jun-06 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 5 U 1 U 1 U 2 5 U 50 U 25 U 25 U Chloromethane 3 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Vinyl chloride 0.03 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Chloroethane 3000 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Trichlorofluoromethane 2,000 4.2 J 1.4 1 U 1 U 1 U 10 U 5 U 5 U 1,1-Dichloroethene 7 5 U 1 U 1 U 1 U 1 9 17 1 6.8 26 Trichlorotrifluoroethane 200,000 1,300 360 480 220 660 1,200 390 2,200 Carbon disulfide 700 25 U 5 U 5 U 5 U 5 U 50 U 25 U 25 U Acetone 6000 25 U 5 U 5 UJ 5 U 5 U 50 U 25 U 25 U Methylene chloride 5 5 U 1 U 1 1 U 1 U 10 U 5 U 5 U trans-1,2-Dichloroethene 100 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Meth I-tert-but I -ether MTBE 20 5 U 1.2 1 U 1.3 4.4 10 U 5 U 7 1,1-Dichloroethane 6 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U cis- 1,2-Dichloroethene 70 45 16 37 31 60 80 49 170 2-Butanone (MEK) 4,000 25 UJ 5 U 5 U 5 U 5.6 50 U 25 U 25 U Chloroform 70 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U 1,1,1-Trichloroethane 200 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Benzene 1 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U 1,2-Dichloroethane 0.4 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Trichloroethene 3 4.8 J 12 4.3 5.1 7.7 10 U 6.2 18 4-Methyl-2-pentanone (MIBK) NE 25 UJ 5 U 5 U 5 U 5 U 50 U 25 U 25 U Toluene 600 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Tetrachloroethene 0.7 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U m&p-Xylenes 500 10 U 2 U 2 U 2 U 2 U 20 U 10 U 10 U o-X lene 500 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Styrene 70 5U 1U 1U 1U 1U 10U 5U 5U n-But (benzene 70 5 UJ 1 U 1 U 1 U 1 U 10 U 5 U 5 U Naphthalene 6 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U 1,2,3-Trichlorobenzene NE 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Vinyl acetate NE 25 UJ 5 U 5 U 5 U 5 U 50 U 25 U 25 U Eth (benzene 600 5 U 1 U 1 U 1 U 1 U 10 U 5 U 5 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 12 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in p g/L) 2L Standard MW-108 MW-10D Jan-10 Sep-02 Sep-03 Sep-04 Sep-05 Sep-06 Apr-07 Oct-07 Sep-02 Sep-032 Sep-04 Sep-05 Sep-062 Apr-072 Oct-072 Dichlorodifluoromethane 1,000 0.14 U 1 U 5 U 1 U 5 U 5 U 5 U 0.14 U 1 U 5 U 1 U 5 U 5 U 5 U Chloromethane 3 0.16 U 1 U 5 U 1 UJ 1 U 1 U 1 U 0.16 U 1 U 5 U 1 UJ 1 U 1 U 1 U Vinyl chloride 0.03 0.18 U 1 U 5 U 1 U 1.8 3.1 1 0.18 U 1 U 5 U 1 U 3.8 4.6 2 Chloroethane 3000 0.21 U 1 U 5 U 1 U 1 U 1 U 1 U 0.21 U 1 U 5 U 1 U 1 U 1 U 1 U Trichlorofluoromethane 2,000 0.22 U 1 U 5 U 1 U 1 U 1 U 1 U 0.22 U 0.6 J 5 U 1 U 1 U 1 U 1 U 1,1-Dichloroethene 7 0.19 U 1 U 5 U 1 U 17 27 11 0.19 U 1 U 5 U 1 U 23 24 15 Trichlorotrifluoroethane 200,000 72 670 890 470 1,300 1,600 820 100 750 1200 1200 1,900 1,400 1,200 Carbon disulfide 700 0.4U 5U 25U 5U 5U 5U 5U 0.4U 5U 25U 5U 5U 5U 5U Acetone 6000 1.5U 5U 25U 5U 5U 24 5U 1.5U 5U 25U 5U 5U 5U 5U Methylene chloride 5 0.19 U 1 U 5 U 1 U 1 U 1 U 1 U 0.19 U 1 U 5 U 1 U 1 U 1 U 1 U trans- 1,2-Dichloroethene 100 0.21 U 1 U 5 U 1 U 1 U 1 U 1 U 0.21 U 1 U 5 U 1 U 1 U 1 U 1 U Meth I-tert-but I -ether MTBE 20 0.21 U 1 U 5 U 2.6 J 5.2 3.6 8 0.21 U 1 U 4.6 J 2.5 J 3.4 3 9 1,1-Dichloroethane 6 0.2 U 1 U 5 U 1 U 1 U 1 U 1 U 0.2 U 1 U 5 U 1 U 1 U 1 U 1 U cis- 1,2-Dichloroethene 70 6.6 29 22 20 120 160 81 12 38 26 49 190 170 120 2-Butanone (MEK) 4,000 1.7 U 5 U 25 U 5 UJ 5 U 6.2 5 U 1.7 U 5 U 25 U 5 UJ 5 U 5 U 5 U Chloroform 70 0.23 U 0.99 J 5 U 1 U 1.2 1.4 1 U 0.23 U 1.2 5 U 1 U 1.8 1.4 1 1,1,1-Trichloroethane 200 0.22 U 1 U 5 U 1 U 1 U 1 U 1 U 0.22 U 1 U 5 U 1 U 1 U 1 U 1 U Benzene 1 0.2U 1U 5U 1U 1U 1U 1U 0.2U 1U 5U 1U 1U 1U 1U 1,2-Dichloroethane 0.4 0.25 U 1 U 5 U 1 U 1 U 1.1 1 U 0.25 U 1 U 5 U 1 U 1.4 1.2 1 U Trichloroethene 3 1.4 2.2 5 U 1.9 5.4 5.4 5 1.7 2.8 8.3 2.6 6.1 5.4 8 4-Methyl-2-pentanone (MIBK) NE 0.92 U 5 U 25 U 5 U 5 U 5 U 5 U 0.92 U 5 U 25 U 5 U 5 U 5 U 5 U Toluene 600 0.21U 1U 5U 1U 1U 1U 1U 0.21U 1U 5U 1U 1U 1U 1U Tetrachloroethene 0.7 0.2 U 1 U 5 U 1 U 1 U 1 U 1 U 0.2 U 1 U 5 U 1 U 1 U 1 U 1 U m&p-Xylenes 500 0.39U 2U 10U 2U 2U 2U 2U 0.39U 2U 10U 2U 2U 2U 2U o-Xlene 500 0.21U 1U 5U 1U 1U 1U 1U 0.21U 1U 5U 1U 1U 1U 1U Styrene 70 0.23U 1U 5U 1U 1U 1U 1U 0.23U 1U 5U 1U 1U 1U 1U n-But (benzene 70 0.22 U 1 U 5 U 1 U 1 U 1 U 1 1 U 0.22 U 1 U 5 U 1 U 1 U 1 U 1 U Naphthalene 6 0.34U 1U 5U 1U 1U 1U 1U 0.34U 1U 5U 1U 1U 1U 1U 1,2,3-Trichlorobenzene NE 0.24 U 1 U 5 U 1 U 1 U 1 U 1 U 0.24 U 1 U 5 U 1 U 1 U 1 U 1 U Vinyl acetate NE NA 5 U 25 U 5 U 5 U 5 U 5 U NA 5 U 25 U 5 U 5 U 5 U 5 U Ethlbenzene 600 0.2U 1U 5U 1U 1U 1U 1U 0.2U 1 1U 5U 1U 1U 1U 1U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 13 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in k g1L) 2L Standard MW-16B Jan-10 Sep-02 Apr-03 Sep-03 Mar-04 Sep-04 Mar-05 Sep-05 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 0.14 U 0.14 U 1 U 1 U 1 U 1 U 1 U 5 U 5 U 5 U Chloromethane 3 0.16 U 0.16 U 1 U 1 U 1 U 1 U 1 UJ 1 U 1 U 1 U Vinyl chloride 0.03 0.18 U 0.18 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Chloroethane 3000 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Trichlorofluoromethane 2,000 0.22 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1-Dichloroethene 7 0.19 U 0.19 U 1 U 1 U 1 U 1 U 1 U 1 1.3 2.2 1 U Trichlorotrifluoroethane 200,000 21 22 47 40 31 16 20 71 91 19 Carbon disulfide 700 0.4 U 0.4 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U Acetone 6000 6.7 1.5 U 5 U 8.5 5 U 5 U 5 U 5 U 5 U 5 U Methylene chloride 5 0.19 U 0.19 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U trans-1,2-Dichloroethene 100 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Meth I-tert-but I -ether MTBE 20 0.21 U 0.21 U 1 U 1.8 1.5 1.1 1.3 J 4.6 9.7 1 1,1-Dichloroethane 6 0.2 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U cis- 1,2-Dichloroethene 70 1.9 1.1 2.4 2 1.2 1.2 1.5 4.2 7.2 2 2-Butanone (MEK) 4,000 1.7 U 1.7 U 5 U 5 U 5 U 5 U 5 UJ 5 U 5 U 5 U Chloroform 70 0.23 U 0.23 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1,1-Trichloroethane 200 0.22 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Benzene 1 0.2U 0.2U 1U 1U 1U 1U 1U 1U 1U 1U 1,2-Dichloroethane 0.4 0.25 U 0.25 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Trichloroethene 3 0.34 J 0.32 J 0.57 J 0.57 J 0.53 J 1 U 1 U 1.9 3.5 1 U 4-Methyl-2-pentanone (MIBK) NE 0.92 U 0.92 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U Toluene 600 0.21U 0.21U 1U 1U 1U 1U 1U 1U 1U 1U Tetrachloroethene 0.7 0.2 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U m&p-Xylenes 500 0.39 U 0.39 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U o-Xlene 500 0.21U 0.21U 1U 1U 1U 1U 1U 1U 1U 1U Styrene 70 0.23U 0.23U 1U 1U 1U 1U 1U 1U 1U 1U n-But (benzene 70 0.22 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Naphthalene 6 0.34 U 0.34 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1,2,3-Trichlorobenzene NE 0.24 U 0.24 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl acetate NE NA 0.47 UJ 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U Eth (benzene 600 0.2 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 14 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (inµ g1L) 2L Standard MW-16D Jan-10 Sep-02 Apr-032 Sep-03 Mar-042 Sep-042 Mar-052 Sep-052 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 6.9 2.5 1 U 1 U 1 U 1 U 1 U 5 U 5 U 5 U Chloromethane 3 0.16 U 0.16 U 1 U 1 U 1 U 1 U 1 UJ 1 U 1 U 1 U Vinyl chloride 0.03 0.18 U 0.18 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Chloroethane 3000 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Trichlorofluoromethane 2,000 2.6 0.73 J 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1-Dichloroethene 7 0.19 U 1.1 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Trichlorotrifluoroethane 200,000 890 180 78 49 29 13 12 28 18 12 Carbon disulfide 700 0.4 U 0.4 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U Acetone 6000 1.5 U 1.5 U 5 U 11 5 U 5 U 5 U 5 U 7 8 Methylene chloride 5 1.2 0.19 U 1 U 0.69 J 1 U 1 U 1 U 1 U 1 U 1 U trans- 1,2-Dichloroethene 100 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Meth I-tert-but I -ether MTBE 20 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 UJ 1 U 1 U 1 U 1,1-Dichloroethane 6 0.45 J 0.34 J 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U cis-1,2-Dichloroethene 70 90 63 64 38 41 36 27 70 39 38 2-Butanone (MEK) 4,000 1.7 U 1.7 U 5 U 5 U 5 U 5 U 5 UJ 5 U 5 U 5 U Chloroform 70 1.3 0.55 J 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1,1-Trichloroethane 200 0.22 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Benzene 1 0.2U 0.2U 1U 1U 1U 1U 1U 1U 1U 1U 1,2-Dichloroethane 0.4 1.2 0.81 J 0.9 J 1 U 1 U 1 U 1 U 1 U 1 U 1 U Trichloroethene 3 7.1 3.3 1.6 1.2 1.3 1.2 1 U 1.1 1 U 1 4-Methyl-2-pentanone (MIBK) NE 0.92 U 0.92 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U Toluene 600 0.21U 0.21U 1U 1U 1U 1U 1U 1U 1U 1U Tetrachloroethene 0.7 0.2 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U m&p-Xylenes 500 0.39 U 0.39 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U o-Xlene 500 0.21U 0.21U 1U 1U 1U 1U 1U 1U 1U 1U Styrene 70 0.23U 0.23U 1U 1U 1U 1U 1U 1U 1U 1U n-But (benzene 70 0.22 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Naphthalene 6 0.34 U 0.34 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1,2,3-Trichlorobenzene NE 0.24 U 0.24 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl acetate NE NA 0.47 UJ 5 U 5 U 5 U 5 U 5 U 5 U 5 U S U Eth(benzene 600 0.2U 0.2U 1U 1U 1U 1U 1U 1U 1U 1U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 15 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in u g1L) 2L Standard MW-18B Jan-10 Sep-02 Apr-03 Sep-03 Mar-04 Sep-04 Mar-05 Sep-05 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 0.14 U 0.14 U 1 U 1 U 1 U 1 U 1 U 5 U 5 U 5 U Chloromethane 3 0.16 U 0.16 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl chloride 0.03 0.18 U 0.18 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Chloroethane 3000 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Trichlorofluoromethane 2,000 0.22 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1-Dichloroethene 7 0.19 U 0.19 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Trichlorotrifluoroethane 200,000 0.22 U 0.22 U 1 U 1 U 1 U 1 U 1 U 5 U 5 U 5 U Carbon disulfide 700 0.4 U 0.4 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U Acetone 6000 1.5U 1.5U 5U 5U 5U 5U 5U 5U 5U 5U Methylene chloride 5 0.19 U 0.19 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U trans-1,2-Dichloroethene 100 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Meth I-tert-but I -ether MTBE 20 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1-Dichloroethane 6 0.2 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U cis- 1,2-Dichloroethene 70 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 2-Butanone (MEK) 4,000 1.7 U 1.7 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U Chloroform 70 0.23 U 0.23 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1,1-Trichloroethane 200 0.22 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Benzene 1 0.2U 0.2U 1U 1U 1U 1U 1U 1U 1U 1U 1,2-Dichloroethane 0.4 0.25 U 0.25 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Trichloroethene 3 0.21 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 4-Methyl-2-pentanone (MIBK) NE 0.92 U 0.92 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U Toluene 600 0.21U 0.21U 1U 1U 1U 1U 1U 1U 1U 1U Tetrachloroethene 0.7 0.2 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U m&p-Xylenes 500 0.39 U 0.39 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U o-Xlene 500 0.21U 0.21U 1U 1U 1U 1U 1U 1U 1U 1U Styrene 70 0.23U 0.23U 1U 1U 1U 1U 1U 1U 1U 1U n-But (benzene 70 0.22 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Naphthalene 6 0.34U 0.34U 1U 1U 1U 1U 1U 1U 1U 1U 1,2,3-Trichlorobenzene NE 0.24 U 0.24 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl acetate NE NA 0.47 UJ 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U Ethlbenzene 600 0.2U 0.2U 1U 1U 1U 1U 1U 1U 1U 1U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 16 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (in u g1L) 2L Standard MW-18D Jan-10 Sep-02 Apr-03 Sep-03 Mar-04 Sep-04 Mar-05 Sep-05 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 0.14 U 2.5 1 U 5 U 1 U 1 U 1 U 5 U 5 U 5 U Chloromethane 3 0.16 U 0.16 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl chloride 0.03 0.18 U 0.18 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U Chloroethane 3000 0.21 U 0.21 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U Trichlorofluoromethane 2,000 0.22 U 0.22 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1-Dichloroethene 7 0.19 U 0.19 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 2 Trichlorotrifluoroethane 200,000 250 330 310 330 270 120 78 120 170 260 Carbon disulfide 700 0.4 U 0.4 U 5 U 25 U 5 U 5 U 5 U 5 U 5 U 5 U Acetone 6000 1.5 U 1.5 U 5 U 64 5 U 5 U 5 U 5 U 5 U 5 U Methylene chloride 5 0.19 U 0.19 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U trans-1,2-Dichloroethene 100 0.21 U 0.21 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U Meth I-tert-but I -ether MTBE 20 0.21 U 0.21 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1-Dichloroethane 6 0.2 U 0.2 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U cis- 1,2-Dichloroethene 70 21 26 30 24 18 16 13 14 16 21 2-Butanone (MEK) 4,000 1.7 U 1.7 U 5 U 25 U 5 U 5 U 5 U 5 U 5 U 5 U Chloroform 70 0.23 U 0.23 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1,1-Trichloroethane 200 0.22 U 0.22 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U Benzene 1 0.2U 0.2U 1U 5U 1U 1U 1U 1U 1U 1U 1,2-Dichloroethane 0.4 0.25 U 0.25 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U Trichloroethene 3 2.7 3 3.1 2.6 J 2.3 2.2 1.7 1.7 1 U 2 4-Methyl-2-pentanone (MIBK) NE 0.92 U 0.92 U 5 U 25 U 5 U 5 U 5 U 5 U 5 U 5 U Toluene 600 0.21U 0.21U 1U 5U 1U 1U 1U 1U 1U 1U Tetrachloroethene 0.7 0.2 U 0.2 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U m&p-Xylenes 500 0.39 U 0.39 U 2 U 10 U 2 U 2 U 2 U 2 U 2 U 2 U o-Xlene 500 0.21U 0.21U 1U 5U 1U 1U 1U 1U 1U 1U Styrene 70 0.23U 0.23U 1U 5U 1U 1U 1U 1U 1U 1U n-But (benzene 70 1 0.22 U 0.22 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U Naphthalene 6 0.34 U 0.34 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U 1,2,3-Trichlorobenzene NE 0.24 U 0.24 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl acetate NE NA 0.47 UJ 5 U 25 U 5 U 5 U 5 U 5 U 5 U 5 U Eth (benzene 600 0.2 U 0.2 U 1 U 5 U 1 U 1 U 1 U 1 U 1 U 1 U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 17 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (inµ g1L) 2L Standard MW-19B MW-19D Jan-10 Sep-022 Sep-03 Sep-04 Sep-05 Sep-06 Apr-07 Oct-07 Sep-02 Sep-03 Sep-04 Sep-05 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 0.14 U 1 U 1 U 1 U 5 U 5 U 5 U 0.14 U 1 U 1 U 1.8 5 U 5 U 5 U Chloromethane 3 0.16 U 1 U 1 U 1 U 1 U 1 U 1 U 0.16 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl chloride 0.03 0.18U 1U 1U 1U 1U 1U 1U 1 1U 1U 1U 1U 1U 1U Chloroethane 3000 0.21U 1U 1U 1U 1U 1U 1U 0.21U 1U 1U 1U 1U 1U 1U Trichlorofluoromethane 2,000 1.5 1 U 1 U 1 U 1 U 1 U 1 U 1.5 1.7 2.4 2.9 3.5 3.7 3 1,1-Dichloroethene 7 0.89 J 1 U 1 U 1 U 1 1 U 1 U 1 U 1.1 1 U 1 U 1 U 2.1 3 3 Trichlorotrifluoroethane 200,000 160 1 U 1 U 1 U 5 U 5 U 5 U 200 190 560 370 430 620 760 Carbon disulfide 700 0.4U 5U 5U 5U 5U 5U 5U 0.4U 5U 5U 5U 5U 5U 5U Acetone 6000 1.5U 5U 5U 5U 5U 5U 7 1.5U 5U 5U 5U 5U 5U 5U Methylene chloride 5 0.19 U 1 U 1 U 1 U 1 U 1 U 1 U 0.19 U 1 U 1 U 1 U 1 U 1 U 1 U trans-1,2-Dichloroethene 100 0.33 J 1 U 1 U 1 U 1 U 1 U 1 U 0.34 J 1 U 1 U 1 U 1 U 1 U 1 U Meth I-tert-but-ether MTBE 20 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1-Dichloroethane 6 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U cis- 1,2-Dichloroethene 70 11 1 U 1 U 1 U 1 U 1 U 1 U 18 13 21 23 31 37 55 2-Butanone (MEK) 4,000 1.7 U 5 U 5 U 5 U 5 U 5 U 34 2 J 5 U 5 U 5 U 5 U 5 U 5 U Chloroform 70 0.3 J 1 U 1 U 1 U 1 U 1 U 1 U 0.33 J 1 U 1 U 1 U 1 U 1 U 1 1,1,1-Trichloroethane 200 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U Benzene 1 0.2U 1U 1U 1U 1U 1U 1U 0.2U 1U 1U 1U 1U 1U 1U 1,2-Dichloroethane 0.4 0.25 U 1 U 1 U 1 U 1 U 1 U 1 U 0.25 U 1 U 1 U 1 U 1 U 1 U 1 U Trichloroethene 3 3.1 1 U 1 U 1 U 1 U 1 U 1 U 3.2 3.6 5.3 6.3 8.1 9.4 11 4-Methyl-2-pentanone (MIBK) NE 0.92 U 5 U 5 U 5 U 5 U 5 U 5 U 0.92 U 5 U 5 U 5 U 5 U 5 U 5 U Toluene 600 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 0.44 J 1 U 1 U 1 U 1 U 1 U 1 U Tetrachloroethene 0.7 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U m&p-Xylenes 500 0.39U 2U 2U 2U 2U 2U 2U 0.39U 2U 2U 2U 2U 2U 2U o-Xlene 500 0.21U 1U 1U 1U 1U 1U 1U 0.21U 1U 1U 1U 1U 1U 1U Styrene 70 0.23U 1U 1U 1U 1U 1U 1U 0.23U 1U 1U 1U 1U 1U 1U n-Butlbenzene 70 0.22U 1U 1U 1U 1U 1U 1U 0.22U 1U 1U 1U 1U 1U 1U Naphthalene 6 0.34U 1U 1U 1U 1U 1U 1U 0.34U 1U 1U 1U 1U 1U 1U 1,2,3-Trichlorobenzene NE 0.24 U 1 U 1 U 1 U 1 U 1 U 1 U 0.24 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl acetate NE NA 5U 5U 5U 5U 5U 5U NA 5U 5U 5U 5U 5U 5U Ethlbenzene 600 0.2U 1U 1U 1U 1U 1U 1U 0.2U 1U 1U 1U 1U 1U 1U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 18 of 19 Table CA Historical VOC Analytical Results at Solvent Plume Wells Former Abbott Facility Laurinburg, Scotland County, North Carolina Parameter (inµ g/L) 2L Standard MW-20B MW-20D Jan-10 Sep-02 Sep-03 Sep-05 Sep-06 Apr-07 Oct-07 Sep-02 Sep-03 Sep-04 Sep-05 Sep-06 Apr-07 Oct-07 Dichlorodifluoromethane 1,000 0.14 U 1 U 1 U 5 U 5 U 5 U 0.14 U 1 U 1 U 1 U 5 U 5 U 5 U Chloromethane 3 0.16 U 1 U 1 U 1 U 1 U 1 U 0.16 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl chloride 0.03 0.18U 1U Ilu 1U 1U 1U 1U 0.18U 1U 1U 1U 1U 1U 1U Chloroethane 3000 0.21U 1U 1U 1U 1U 1U 0.21U 1U 1U 1U 1U 1U 1U Trichlorofluoromethane 2,000 0.22 U 1 U 1 U 1 U 1 U 1 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1-Dichloroethene 7 0.19 U 1 U 1 U 1 U 1 U 1 U 0.19 U 1 U 1 U 1 U 1 U 1 U 1 U Trichlorotrifluoroethane 200,000 0.22 U 1 U 1 U 1 U 5 U 5 U 5 U 0.87 J 1 U 1 U 1 U 5 U 5 U 5 U Carbon disulfide 700 0.4U 5U 5U 5U 5U 5U 5U 0.4U 5U 5U 5U 5U 5U 5U Acetone 6000 1.5U 5U 5U 5U 5U 5U 5U 1.5U 5U 5U 5U 5U 5U 5U Methylene chloride 5 0.19 U 1 U 1 U 1 U 1 U 1 U 1 U 0.19 U 1 U 1 U 1 U 1 U 1 U 1 U trans-1,2-Dichloroethene 100 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U Meth I-tert-but I -ether MTBE 20 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 1,1-Dichloroethane 6 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U cis- 1,2-Dichloroethene 70 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 0.21 U 1 U 1 U 1 U 1 U 1 U 1 U 2-Butanone(MEK) 4,000 1.7U 5U 5U 5U 5U 5U 5U 1.7U 5U 5U 5U 5U 5U 5U Chloroform 70 0.23U 1U 1U 1U 1U 1U 1U 0.23U 1U 1U 1U 1U 1U 1U 1,1,1-Trichloroethane 200 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U Benzene 1 0.2U 1U 1U 1U 1U 1U 1U 0.2U 1U 1U 1U 1U 1U 1U 1,2-Dichloroethane 0.4 0.25 U 1 U 1 U 1 U 1 U 1 U 1 U 0.25 U 1 U 1 U 1 U 1 U 1 U 1 U Trichloroethene 3 0.21U 1U 1U 1U 1U 1U 1U 0.21U 1U 1U 1U 1U 1U 1U 4-Methyl-2-pentanone (MIBK) NE 0.92 U 5 U 5 U 5 U 5 U 5 U 5 U 0.92 U 5 U 5 U 5 U 5 U 5 U 5 U Toluene 600 0.21U 1U 1U 1U 1U 1U 1U 0.21U 1U 1U 1U 1U 1U 1U Tetrachloroethene 0.7 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U 0.2 U 1 U 1 U 1 U 1 U 1 U 1 U m&p-Xylenes 500 0.39U 2U 2U 2U 2U 2U 2U 0.39U 2U 2U 2U 2U 2U 2U o-Xlene 500 0.21U 1U 1U 1U 1U 1U 1U 0.21U 1U 1U 1U 1U 1U 1U Styrene 70 0.23U 1U 1U 1U 1U 1U 1U 0.23U 1U 1U 1U 1U 1U 1U n-But (benzene 70 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U 0.22 U 1 U 1 U 1 U 1 U 1 U 1 U Naphthalene 6 0.34U 1U 1U 1U 1U 1U 1U 0.34U 1U 1U 1U 1U 1U 1U 1,2,3-Trichlorobenzene NE 0.24 U 1 U 1 U 1 U 1 U 1 U 1 U 0.24 U 1 U 1 U 1 U 1 U 1 U 1 U Vinyl acetate NE NA 5U 5U 5U 5U 5U 5U NA 5U 5U 5U 5U 5U 5U Ethlbenzene 600 0.2U 1U 1U 1U 1U 1U 1U 0.2U 1U 1U 1U 1U 1 1U 1U Notes: 2L Standard = North Carolina Administrative Code 2L Groundwater Standards (January 2010) Remediation goals have not been developed for the constituents that are listed as "NE". ug/L = micrograms per liter NE = Not Established NA = Not Analyzed U = consituent not detected at a concentration above the reported value J = Estimated concentration UJ = Constituent not detected at a concentration above the estimated reported value Bold: Constituent concentration reported above the method detection limit. Bold and Shaded: Constituent concentratrion reported above the NCAC 2L Groundwater Standard Page 19 of 19 AECOM Environment Appendix D TCE and cis-1,2-DCE Trend Plots for Selected Wells 60135880 February 2010 200,000 180,000 160,000 J 140,000 120,000 c 0 100,000 i a+ L 80,000 0 60,000 40,000 20,000 0 M W-100A HRC Injection HRC Injection tTCE - f7- cis-1,2-DCE too' 'a -C3 . ,o, - o. � �fl 0- 0 Ci& 00� O°� O°�o O°�b O°�i Oy° Date 200,000 180,000 160,000 J 140,000 ao 120,000 c 0 100,000 c 80,000 c 0 60,000 40,000 20,000 0 HRC Inject 450,000 400,000 350,000 300,000 ec c 250,000 m 200,000 d U C 150,000 100,000 50,000 rem MW-101A HRC Injection HRC Injection November2002 June2004 fTCE - f7- cis-1,2-DCE -rq .�--�•�7--� OOti OOti OOD OOh 00� 00� 000 O,�O Date 35,000 30,000 25,000 m c 20,000 0 15,000 c 0 10,000 5,000 0 2ETD10OW HRClnjection HRC Injection fTCE nrte-208� • {} •cis-1,2-DCE O°1 O°ti O°a O°h OR6 0�10\� �\ti�ti y\ya�ti \�$�ti yo\yo�ti ry\�ti�ti �\b�ti yy\y$�ti h 35,000 30,000 25,000 on 3 20,000 0 v 15,000 c 0 10,000 5,000 0 Date MW-102B HRC Injection HRC Injection November2002 June 2004 fTCE qD- - cis-1,2-DCE 4 Ir OAS" b�tiO\'L O\1�ti 35,000 30,000 25,000 m e 20,000 0 a 15,000 10,000 5,000 0 Date MW-102C HRC Injection HRC Injection fTCE November 2002 June 2004 - 4} cis-1,2-DCE •R Doti O°°` 0) 1 h�ti�\� o�tio\� 'y ti�tiry\� Date �\6�ti yy\y$�ti 4500 4000 3500 m 3000 0 2500 2000 c to 1500 1000 500 0 MW-103A HRC Injection HRC Injection f TCE November 2002 Q - {} •cis-1,2-DCE � r r i 0 o q rvI a, rx\tip'\ti o\y�ti y\ya�ti y\���ti y°\y°�ti ry\�ti�ti �\b�ti yy\y��ti 4500 4000 3500 m 3000 0 2500 .2 2000 v 1500 1000 Soo 0 Date MW-103B HRC Injection HRC Injection tTCE November 2002 June 2004 - f7- •cis-1,2-DCE 0 moo•' ' -o - �. El- -EJ ❑ oy oti ob` o o` ob o� o e � yo `5\y\ryo a\yo\moo h\ti�\ryo yo\yo\�o yy\yo0, Date 4500 4000 3500 3000 m 3 0 2500 R 2000 41 C to 1500 1000 500 0 MW-103C HRC Injection HRC Injection —0—TICE November 2002 June 2004 - {} .cis-1,2-DCE .a' ''O El •a . •o n 0 0 0 °�y\� o\tio\� Date 1000 900 800 700 600 c 0 500 e w 400 c 0 300 200 100 0 M W-104A HRC Injection HRC Injection f TICE - {} cis-1,2-DCE • G7 ❑' �j OOy 00� 1000 900 800 700 n� 600 c 0 500 c d 400 e 0 300 200 100 0 1000 900 800 700 MID r' 600 c 0 500 e w 400 c 0 300 200 100 0 OOb 00� 000 00� 00� O,O y y Date MW-104B HRC Injection HRC Injection f TCE • {} cis-1,2-DCE O B 0• -BL.J. . Li- OOy 006 y Date MW-104C 00� 00� O,O H RC Injection HRC injection fTCE nn,.— 2004 C- cis-1,2-13CE - 0- - • a ' . p p.. pEl - ooy �ti �b Doti o00 �w ooa oyo °j yy\y�\� Date 250 200 J 150 c r CU 100 Uo 50 0 MW-10B HRC Injection HRC Injection November 2002 June 2004 t TCE - C- cis-1,2-DCE • • P • VL1 ' b . .�' 0 �. Ooy oo'L 00� Oo� Ooo Oo� Ooo O,O Date MW-10D 250 HRC Injection HRC Injection f TCE November 2002 June 2004 - f7- cis-1,2-DCE 200 ❑-1 J ❑ 150 • L� c \ \ o d W 100 \ ` 0 • . C 0 U Q 50 0 0 oOti OOti (3 oo� o00 Ooo 00o OyO \� a�tio\� o��\�tio�tio\� Date 140 120 100 I MW-16B HRC Injection HRC Injection November 2002 June 2004 f TCE E]- cis-1,2-DCE EJ Ch OOy 00L 00� 00� 000 00� 000 O,O 4,11 Date MW-16D 140 120 100 ou 3 = 80 ++ = 60 a c O 40 20 0 HRC Injection HRC Injection f TCE ❑ November 2002 June 2004 1 f]- cis-1,2-DCE 1 1 Lg1 .o o p a�tio\�oo� e (30, oo� o00 ti Date oo� oo� otio AECOM Environment Appendix E Historical Cumulative Trend Plots for TCE, cis-1,2-DCE, Freon 113, and Methylene Chloride 60135880 February 2010 TCE Concentration 450000 400000 350000 300000 J 250000 c 0 m L M C 200000 c 0 u 150000 100000 50000 0 Apr-01 Sep-02 Jan-04 May-05 Oct-06 Feb-08 Jul-09 Date Nov-10 +MW-100A tMW-100B --*--MW-101A --X—MW-101B --I- M W-102A tMW-102B tMW-102C M W-103A MW-103B MW-103C 35 30 25 10 5 0 Apr-01 TCE Concentration Sep-02 Jan-04 May-05 Oct-06 Feb-08 Jul-09 Date Nov-10 M W-104A tMW-104B M W-104C MW-10B MW-10D MW-16B MW-16D MW-18B MW-18D BMW-19B MW-19D --*--MW-20B —*—,MW-20D cis 1,2-DCE 90,000 HRC Injection HRC-X Injection November 2002 June 2004 80,000 70,000 60,000 J 3 50,000 +MW 100A C t M W-100B 0 M W-101A L r y 40,000 MW-101B u C 0 --*— M W-102A MW-102B 30,000 M W-102C 20,000 10,000 0 Apr-01 Sep-02 Jan-04 May-05 Oct-06 Feb-08 Jul-09 Nov-10 Date 140,000 120,000 100,000 J 3 80,000 c 0 M L a c 60,000 0 v 40,000 20,000 0 HRC Injection HRC-X Injection November 2002 June 2004 1 Freon 113 Apr-01 Sep-02 Jan-04 May-05 Oct-06 Feb-08 Jul-09 Nov-10 Date +MW-100A tMW-100B M W-101A ---M— MW-101B --)K--- M W-102A MW-102B MW-102C 250,000 200,000 150,000 100,000 50,000 0 Apr-01 Sep-02 Jan-04 Methylene Chloride May-05 Oct-06 Feb-08 Jul-09 Date Nov-10 +MW-100A tMW-100B M W-101A ---M— MW-101B --)K--- M W-102A MW-102B MW-102C