WI0700012_Monitoring (Report) Nov 2001 - Jan 2002_20020225

PCS
Phosphatece AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
February 25, 2002
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
November 2001— January 2002
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF 1 CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
The initial coliform sample taken from CIW-7 tested 47 / 100 ml. This well is supplied water from WLCT
which tested < 1.0 / 100 ml. CIW-7 was resampled and tested 17 / 100 ml. The Water Level Control Tank
(WLCT) and CIW-7 was chlorinated and the well's outer protective casing was modified to allow direct
access to the well casing for cleaning. CIW-7 was resampled and tested 25 / 100 ml. CIW-7 has been
resampled using a different sampling method to eliminate the possibility of sample contamination. Should
this sample contain coliform the entire injection system will be sanitized.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
ibzA,IALe 0.e„t,:teLcp-rr-
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
I

i
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/ attachment)
T. L. Baker/12-01-008-03-002 (w/ attachment)
R. A. Allen / T. Lewis (w/ attachment)
E-Mail:
S. A. Beckel
J. A. Hardy / R. B. Lee
W. A. Schimming
C:\MyData\Reports\2002\Quarterly\Fourth Quarter TFRAS Report 2001.DOC
2

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CIW-7
Well Depth:
48.00 ft. Well Diamter:
Screened Interval: 31.00 ft. to 45.25 ft.
4 inch
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling: N/A
Field Analysis: pH 7.2 , Specific Conductance 584 uMhos
Temp. 17.8 oC, Odor NONE Appearance: CLEAR
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
09/30/01
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/28/02 '*'1
Date sample analyzed: 1/28/02 to 2/19/02 r t -
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10 —.)
PARAMETERS: (Samples for metals were
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total 47*
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
440
7.3
5.9
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
14.5
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
collected unfiltered X Yes
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified X Yes No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/I
units
mg/I
mg/1
mg/1
mg/1
mg/I
mg/I
uMhos
mg/I
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
<0.001 mg/I
0.028 mg/I Zn - Zinc
N/A`r` , . ug/I
ug/I
N/A mg/I Ammonia Nitrogen
cc -N/A ug/I
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/1 MIBK
Ag - Silver
<0.005 mg/I Se- Selenium
N/A mg/1 Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/I VOC
0.52
N/A
N/A
N/A
N/A
<0.010 mg/I
method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
"RESAMPLED @ 17/100 MLS
*RESAMPLED @ 25/100 MLS
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per tte_e_(of Authorized Agest).Nar a and Title - Please type or print
22.4
ermittee (or Authorized Agent)
tiC/Zrt—
Date
♦

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter:
Screened Interval: 38.70 ft. to 40.70 ft.
ft. below measuring point.
2 inch
Depth to Water Level: 11.75
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling: 2600
Field Analysis: pH 7.4 , Specific Conductance 622 uMhos
Temp. 21.5 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge N •
r*J
to
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/28/02 no
P1
[:77
(: z3
Date sample analyzed: 1/28/02 to 2/19/02
Laboratory Name: PCS PHOSPHATE and:#NVIRONMENT 1
Certification No(s) 330 10 ,
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
mg/I
/100m1
/100m1
X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
406 mg/I Al - Aluminum
7.5 units Ba - Barium
5.5 mg/I Ca - Calcium
Chloride
13.5 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
No and field acidified
X Yes No
N/A mg/l Ni - Nickel
N/A mg/1 Pb - Lead
Zn - Zinc
0.143 mg/I
w
N/A
N/A
N/A mgll Ammonia Nitrogen
N/A mg/I
N/A mgll
N/A mg/I
<0.001 mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
16.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
0.046 mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
<0.005 mg/I Se- Selenium
ug/I
ug/I
ug/I
mg/I
0.50 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mgll Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/1 (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A ug/I
N/A mg/I VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Perm ee of Authorized Agent Na and Title - Please type or print
gnature -.' • -rmiftee (or u horized Agent) (D te)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636
Phone: [phone]:7
N
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
SWW-1
22.50 ft. Well Diamter: 4 inch
Screened Interval:
Depth to Water Level:
Measuring Point is
GALLONS
Field Analysis: pH
Temp. 20.2
18.30 ft. to 21.12 ft.
6.73 ft. below measuring point.
1.52 ft above land surface.
of water pumped/bailed before sampling:
6.1 , Specific Conductance
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2123 uMhos
oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/3D101
Lagoon
Spray Field
Rotary Distributor
Other
CJI
Remediation: Infiltration Galler}=,
X Remediation :
Land Application of Sludge
t
i •3
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/24/02 _�
Date sample analyzed: 1/24/02 to 2/19/02
Laboratory Name: PCS PHOSPHATE andrNVtRONMENT 1
Certification No(s) 330 10 (-0
0s
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1360
pH (when analyzed) 6.9
TOC 8.5
Chloride 81.5
Arsenic N/A
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
523.5
N/A
N/A
N/A
mg/1 Nitrite (NO2 as N)
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/1
mg/1
mg/I
mg/I
uMhos
mg/I
mg/1
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
Nitrate (NO3 as N) N/A mg/I Pb - Lead
Phosphorus: Total as P 128.000 mg/I Zn - Zinc
N/A
N/A
N/A
Orthophosphate N/A mg/I Ammonia Nitrogen
Al - Aluminum N/A mgll
Ba - Barium N/A mg/1
Ca - Calcium N/A mg/1
N/A mg/1
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/1
N/A
N/A
K- Potassium
Mg - Magnesium
Mn - Manganese
mg/1
mg/1
N/A mg/I
mg/1
N/A
N/A mg/I
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.59
N/A
N/A
N/A
N/A
VOC method#
method#
method#
ug/I
ug/I
ug/I
mg/1
mg/I
mg/I
mg/l
mg/1
ug/I
(2)
I certify that, to the best of my knowledge and belief the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Signatur Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 23.00
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 7.18 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
SWW-2
ft. Well Diamter: 4 inch
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 1947 uMhos
Temp. 20.2 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Galle
Spray Field X Remediation : �7
09120/01
Rotary Distributor
Other
N
O
Land Application of Sludge, _�
C77
r\)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/24/02
r,)
J
Date sample analyzed: 1/24/02 to 2/19/02-°
Laboratory Name: PCS PHOSPHATE anFNVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1344
6.7
7.8
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
50.1
N/A
N/A
N/A
510.1
N/A
N/A
N/A
No and field acidified Yes n/a No
mg/I Nitrite (NO2 as N) N/A
/100m1 Nitrate (NO3 as N) N/A
/100m1
mg/I
units
m g/1
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
42.250
N/A
N/A
Ba - Barium N/A
Ca - Calcium N/A
Cd- Cadmium N/A
Chromium: Total N/A mg/I
Cu - Copper N/A mg/1
N/A mg/1
N/A mg/I
K- Potassium N/A mgll
Mg - Magnesium N/A mg/I
Mn - Manganese N/A mg/I
mg/I
mgll
Fe - Iron
Hg - Mercury
Ni - Nickel
Pb - Lead
mg/1 Zn - Zinc
mg/I Ammonia Nitrogen
mg/1
mg/1
mg/1
m g/l
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.24
N/A
N/A
Se- Selenium N/A
Sodium N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
ug/I
ug/I
ug/l
mg/I
mg/l
mg/I
mg/I
mg/I
ugll
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per tee of Authorized Agent Na e and Title - Please type or print
7/1
gnatur . Permittee (or Authorized Agent) (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Mem permit
Well Identification Number (from Permit): SWW-3
Well Depth:
24.50 ft. Well Diamter:
4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 6.91 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1659 uMhos
Temp. 25.6 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
091301K31
Non -Discharge UIC X
NPDES t!1
TYPE OF PERMITTED OPERATION BEING MONITORED %.p
Lagoon Remediation: Infiltration Gallery0
Spray Field X Remediation : Q
Rotary Distributor Land Application of Sludge tip
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/24/02
Date sample analyzed: 1/24/02 to 2/19/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1188 mg/l
pH (when analyzed) 6.4 units
TOC 6.4 mg/I
Chloride 42.0 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A mg/I
N/A mg/I
501.4 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Yes n/a No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A mg/I Ni - Nickel =-^o N/A ug/I
Nitrate (NO3 as N) N/A mg/I Pb - Lead WA ug/I
Phosphorus: Total as P 83.000 mg/I Zn - Zinc N/A ug/I
Orthophosphate N/A mg/I Ammonia Nitrogen mg/I
Al - Aluminum N/A mg/I Other (Specify Compounds and Concentration Units)
Ba - Barium N/A mg/I Fluoride 0.12 mg/1
Ca - Calcium N/A mg/I MIBK N/A mg/1
Cd- Cadmium N/A mg/I Ag - Silver N/A mg/I
Chromium: Total N/A mg/I Se- Selenium N/A mg/I
Cu - Copper N/A mg/I Sodium N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/1 Report attached? Yes (1) No X (2)
N/A mg/1 VOC : method#
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager. Environmental Affairs
Permittee (of Authorized Ag t N e and Title - Please type or pri t
/- t46
(Da )
Signat f Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 25.00 ft. Well Diamter:
SWW-4
4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 6.16 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.6 , Specific Conductance
Temp. 24.5 oC, Odor NONE
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1569 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of S8dge
Iv)
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/25/02
Date sample analyzed:
Laboratory Name:
Certification No(s)
J
1/25/02 to 2/19/02 - - oo
PCS PHOSPHATE andAVIROAIMENT 1
330 10
A
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1012 mg/I Al - Aluminum
pH (when analyzed) 6.8 units Ba - Barium
TOC 5.6 mg/I Ca - Calcium
Chloride 139.1 mg/I Cd- Cadmium
14.750 mg/I Zn - Zinc
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/l
N/A mg/I
N/A mg/1
N/A mg/I
Arsenic N/A mg/I Chromium: Total
Grease and Oils N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
279.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mgll Report attached? Yes (1) No X
0.37
N/A
N/A
N/A
N/A
N/A mg/I VOC
N/A mg/I
method#
method#
method#
ug/I
ug/I
ug/I
mg/1
mg/l
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) Npme and Title - Please type or print
j�hlC-Nd'
ignatur ermittee (or Authorized Agent)
t,

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1635 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
28.21 ft. Well Diamter:
SWW-5
4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 7.05 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatrnent
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2733 uMhos
Temp. 29.5 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
UIC X
09/30/01
Lagoon Remediation: Infiltration GalleryN .
Spray Field X Remediation : O
Rotary Distributor Land Application of Sludge
r-.1
Other
--1
crl
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/24/02
Date sample analyzed: 1/24/02 to 2/19/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1680 mg/l Al - Aluminum
pH (when analyzed) 6.5 units Ba - Barium
TOC 9.6 mg/l Ca - Calcium
Chloride
Arsenic
61.0 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
83.000 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
Yes n/a No
N/A mg/I Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/l Cu - Copper
N/A mg/1 Fe - Iron
769.3 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I
N/A mg/I
N/A mg/I Mg - Magnesium
N/A mg/1 Mn - Manganese
N/A mgll
Se- Selenium
Sodium
N/A
N/A
N/A
0.34
N/A
N/A
N/A
N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/I VOC method#
method#
method#
ug/I
ug/l
ug/I
mg/ I
mg/I
mg/1
mg/1
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per -e (of Authorized Agent) Natle -Please type or print
ignatur ermittee (or Authorized Agent) (Da )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled '18
�xo„ v.mrc)
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.03 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.0 , Specific Conductance
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2536 uMhos
Temp. 29.4 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X
09/30/01
Rotary Distributor
Other
Remediation: Infiltration Galleryp
Remediation : IV •
Land Application of Sludge, =.
P
Note: Values should reflect dissolved and ; ,a
colloidal concentrations S
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
1/24/02
1/24/02 to 2/19/02
PCS PHOSPHATE anSI;ENV.IRONMENT 1
330 10 '
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
Use MPN method for highly turbid samples)
1752
6.7
12.2
94.7
N/A
N/A
N/A
720.3
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/1 Mg - Magnesium
mg/I Mn - Manganese
20.250 mg/I
Yes n/a No
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
0.04
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/I
N/A mg/I VOC : method#
method#
method#
N/A mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per jjtee (Qf Authorized AgeJu-
l5ermitteee and Title - Please type or print
(or Authorized Agent) (Efate)
ignature

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699.1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter: 4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level: 7.10 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 5.9 , Specific Conductance
Fo GroundwaterTreatnent
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
961 uMhos
Temp. 24.8 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field X Remediation : N •
Rotary Distributor
Other
Remediation: Infiltration Gallerya.
Land Application of Sludge. G)
o U1
rV
LO
EJ
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
ry
1/24/02
1/24/02 to 2/19/04
PCS PHOSPHATE anri NVtRQNMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal
Coliform: MF Total
Yes n/a
No and field acidified
N/A
N/A /100m1 Nitrate (NO3 as N) N/A
N/A /100m1 Phosphorus: Total as P
38.750
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A
Dissolved Solids: Total 660 mg/I Al - Aluminum N/A mg/1
pH (when analyzed) 6.3 units Ba - Barium N/A mg/I
TOC N/A mg/1
7.0 mg/I Ca - Calcium
Chloride
Arsenic
71.8 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
N/A mg/1 Chromium: Total
N/A mg/1 Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
166.4 mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/l Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/1
NIA mg/1
N/A mg/l
mg/I
mg/l
N/A
N/A
mg/l
m g/1
mg/1
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No
mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
mg/I
0.08 mg/I
N/A mg/1
Ag - Silver
Se- Selenium
Sodium
N/A mg/I
N/A mg/I
N/A ug/I
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No
VOC : method#
method#
method#
X (2)
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Age, N. e and Title - Please type or rint
A
Signatur-. 'erinittee (or Authorized gent) ( ate)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
6.40 ft. Well Diamter:
MWTF1-A
Screened Interval: 3.40 ft. to 5.40 ft.
2 inch
Depth to Water Level: 4.17 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.5 , Specific Conductance
Temp. 16.1 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
542 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation : c, O •
Rotary Distributor Land Application of Stfdge •
09/30/01
Other
-,1 n 4A
, '.
r�
fr.]
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/28/02
Date sample analyzed: 1/28/02 to 2/19/04-,.)
Laboratory Name: PCS PHOSPHATE an_SNVIRONMENT 1
Certification No(s) 330 10 rso
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 352 mg/I
pH (when analyzed) 7.5 units
TOC 5.0 mg/I
Chloride 11.4 mg/I
Arsenic N/A mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
20.2 mg/I
N/A uMhos
N/A mg/1
N/A mg/I
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
0.416 mg/I Zn - Zinc
Yes n/a No
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
N/A mg/1 Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
2.05
N/A
N/A
N/A
N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/l Report attached? Yes (1) No
N/A mg/1 VOC
N/A mg/I
method#
method#
method#
ug/I
ug/I
ug/I
mg/1
mg/l
mg/I
mg/l
mg/1
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Perp�ttee of Authorized Agepti N e and Title - Please type or print2117 Xi
Signatur ermittee (or Authorized Agent) (Da e
)
4

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 13.50
Screened Interval:
Depth to Water Level:
Measuring Point is
10.60
4.84
3.86
MWTF1-B
ft. Well Diamter: 2 inch
ft. to 12.60 ft.
ft. below measuring point.
ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.1 , Specific Conductance
Temp. 19.9 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
354 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gaileg
Spray Field X Remediation : O
Rotary Distributor
09/30/01
Other
Land Application of Sludge (.11
r �
CD
r,
1V
Note: Values should reflect dissolved and to
colloidal concentrations
Date sample collected: 1/28/02
Date sample analyzed: 1/28/02 to 2/19/02
Laboratory Name: PCS PHOSPHATE ancitNV1RONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/1
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Yes n/a No and field acidified
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
240 mg/1 Al - Aluminum
6.2 units Ba - Barium
4.1 mg/I Ca - Calcium
36.0 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
30.7 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
3.725
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
Ni - Nickel
Pb - Lead
Yes n/a No
Zn - Zinc
Ammonia Nitrogen
w
INk.A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.37
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Perm •e of Authorized A en arr and Title - Please type or print
a
,'74/ 7 4
gnature •i=ermittee (or Authorized Agent) (Date)
4

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): WLCT
Well Depth: NIA ft. Well Diamter: N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level: NIA ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 7.4 , Specific Conductance
Temp. 18.8 oC, Odor NONE
Fo Groundwater Treatrnent
Sys ems Check One:
X Influent (98)
Effluent (99)
CONTINUOUS
599 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Galleb
Spray Field X Remediation :
09/30/01
Other
ttt
Rotary Distributor Land Application ofrS1 dge
I
r▪ r▪ t
uD
Note: Values should reflect dissolved and rV
colloidal concentrations r
Date sample collected: 1/28/02
Date sample analyzed: 1/28/02 to 2/19/
Laboratory Name: PCS PHOSPHATE ar?ENVIRONMENT 1
Certification No(s) 330 10 co :.
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
416
7.3
7.0
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
14.2
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified X
N/A mg/l
N/A mg/I
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/I
units
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
uMhos
mg/l
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
0.025 mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
<0.001 mg/I
<0.005 mg/I
Ni - Nickel
Pb - Lead
Yes No
Zn - Zinc
Ammonia Nitrogen
N/A ug/I
N/A ug/l
N/A ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
0.52 mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS. HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A ug/I
N/A mg/I VOC
<0.010 mgll
method#
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
PNee (of AuthorizedAge a and Title - Please type or prin
A
ignaturey/YPermittee (or Authorized Agent)
Terry L. Baker - Manager, Environmental Affairs
�/'•f.� L c `' z
(Dat

PAGE
01 / 01-;
Date:
Time:
Tech:
02/22/2002 17:20 252 '; - 'PCS PHOSPHATE
PCS Phosphate Co., Inc.; : Tank Farm Remediation System Quarterly Monitoring
/_fit/ -dam
System Gauge Pressures
smW-1
0- ozzi25.,
�..
6ww-7
/1- 9
fax
cm-7
.0 -5as.' -
FilB: 1303-003-02
pet n8
soteeso
Pant ma
Laval Rul
to rteL
Ditch
12.91
7.27
Barge Slip
10.59
-0,z/
Water Level
Control Tank
5'. = MSL
94
%s!63
Sand Layer Peizometers Level lndleators '
Well ICI
TOC
Elevation
MSL'
- TOC
Ste Wtr
.
Level ,
¥ Relative 7o
MSL Ft..
Wall ID
TOC
Elevation '
MSL'
TOC
Ste Wtr
Level
Relative TO
MSL Ft.
Spz-1
10.47
,Level'
7 .4
4_0 /
Cpz-1 '
10.51
//L�evel'
f. V.
O, 79
Spz-2
11.21
/D.//o
/ 125
coz-z
10.25
RgO
/ 75".
Spz-3
11.87
/ir ail -
543
Cpz-3
- 11.12
/t 4,7
0-• VW r
Spr4
11A5
6, 9.6
isr
CPW
9.65
/430
0.65
Spz-5
11,45
9, 5'0
/.'9.S
MWTF-1A4
14.35
ifl
/D-/O
Spz-6
11.23
/D.4
D, 9i
MWTF-1S•
14.36
44M
9:5:.
Spz-7
11.59
/0. 0
/89
MWTF-1C•.
14.44
//.7S
.07,69
spt a
t] 57
_ . 7, 9,C
9 66
MWTF-2A
1495
t 4/0
6.5
Spz-9
11.01
8..99
X,6.2--
MWTF-2S
14.02
• //,.38
.?.4y
Spz-10
12.16
J, USr
S 6/
MWTF-2C
14.06
/4<64/
-a 66
SPW
9.95
776
,2./9
MWTF-3A
12.21
g 99
29;e27
/-.95V
MWTF-313
12.18
/1259/
MwrFaC
12.19
/,.3., 30
- / //
• Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Ste
Wtr
Level Ft.
Max Level
Relative To
MSL FL
Control
Point
MSL'
Is Well
Pumping
enas/M)o
Comments
SWWW-1
10,70
l , 73
D. 7.,1
+1'to +2'
4N5 .
iyE'ao on /4.YsA
CWW-1
70.80
�0'�0
- .'7. 8iD0
-2't0.1'
/P 5
of / i /
SWW-2
9.99
7./8
1
+1„to+2'
�,f�S
f1ll
CWw-2
10.23
'742
`/6
I- /-17
.-2'to-1'
0_.0
SWW3
9.97
�, 9/�/
e ai /
+1'to+2'
CWW-3
9.95
5:9S
' 3n. /.5
-2'to -1.
��y//(f
7P1
,.
6WW-4
10.73
6./6
A/6,/
+1'to+2'
f��el
Cww-4
10,73
6. 7e.
- °W I
-2'bp -1'
YES
SWWS
10.90
r Of
+1'to+2'
Ye;
CWW-5
10.74
��7y05
/•Dlog
^- /, 7,99
-2•to4
7/J'�,lr
SWW6
10.66
70_9
_/.Off
rt. to+2'
!t
CWWS
9.92
6,57
mC.4/
-2'to-l'
Vell
SWW-7
10.70
7/0
//4
+1 'to +2'r��/ef
CWW-7 _
9.95
6.56
-n2. 4'
-2'to-1'
%GJ
I'k
Revised 12/03/01
• Riser length added to TOC elevation 1(24/97
PCS095.XLS'i

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
November 2001— January 2002
The Tank Farm Itemediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Nov
417,770
0
417,770
9.7
12.9
Dec
445,710
0
445,710
10.0
12.8
Jan
431,920
0
431,920
9.7
13.5
TOTALS
1,295,400
0
1,295,400
C:\MyData\Reports\2002\Quarterly\Fourth Quarter TFRAS Report 2001.DOC
3

Withdrawal Well System
The system was down for 4 hours in January for preventive maintenance on the air compressor. The
withdrawal water well pumps are monitored daily by the area Maintenance Department and preventative
maintenance work is performed as needed. The total monthly and quarterly withdrawal water volumes for
the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Nov
338,477
201,005
539,482
12.1
Dec
377,178
233,771
610,949
13.7
Jan
377,525
182,101
559,625
12.5
TOTALS
1,093,180
616,877
1,710,056
Some additional short periods of_planned downtime for preventative maintenance,_pipe header cleaning,_
and troubleshooting on individual pumps in the fourteen well system were experienced. The discharge
header was cleaned between 12/17 and 12/19. Details of these activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 11/5 repaired pump. On 11/13 repaired air line. On 12/4 pulled and cleaned pump.
SWW-2: On 12/17 cleaned discharge of pump. On 1/22 changed pump.
SWW-3: On 1/9 cleaned pump. On 1/18 pulled and cleaned pump.
SWW-4: On 1/22 pulled and cleaned pump.
SWW-5: On 11/1 changed meter. On 11/13 cleaned pump. On 12/4 changed counter.
SWW-6: On 12/19 pulled pump and cleaned discharge.
SWW-7: On 12/18 pulled pump and changed check valve.
C:\MyData\Reports\2002\Quarterly\Fourth Quarter TFRAS Report 2001.DOC
4
NI

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 12/7 pulled and cleaned pump.
CWW-2: On 11/15 pulled pump. On 11/28 pulled and cleaned pump. On 1/3 changed pump. On 1/16
changed pump. On 1/18 pulled pump and replaced float.
CWW-3: On 11/20 repaired failed counter.
CWW-4: On 1/11 repaired air line.
CWW-5: On 11/14 acid cleaned well and changed pump On 12/4 changed counter.
CW W-6: On 12/19 pulled pump and replaced magnet.
CWW-7: On 1/4 changed air line. On 1/30 pulled pump and changed float.
C:\MyData\Reports\2002\Quarterly\Fourth Quarter TFRAS Report 2001.DOC
5