WI0700012_Monitoring (Report)_20001127

GROUN`DWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter:
4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: NIA ft. below measuring point.
Measuring Point is NIA ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 7.5 , Specific Conductance 674
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
CONTINUOUS
uMhos
Temp. 24.2 oC, Odor NONE Appearance:
CLEAR
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
Mail Original
to:
PERMIT #:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636
Phone: [phone]
WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallo
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
X Other
l
rcD
Note: Values should reflect dissolved and
colloidal concentrations
10/11/00
V
C�
O
10/11/00 to 11/10/00 N �. J
PCS PHOSPHATE and EigIRONgENT 1
330 10
l..
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A mg/I
N/A /100m1
<1.0 /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 472
pH (when
TOC
Chloride
analyzed) 7.2
6.4
10.5
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I
units
mg/I
mg/I
N/A mg/I
N/A mg/I
N/A mg/I
29.1 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified X Yes No
N/A mg/I Ni - Nickel
N/A _ mg/I Pb - Lead
0.171 mg/I Zn - Zinc
N/A mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
<0.001 mg/I
<0.005 mg/I
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
ry
m
1='N/A3 ug/I
ug/I
N/A ug/I
0.56
N/A
N/A
N/A
N/A
N/A mg/I VOC •method#
0.073 mg/1
method#
method#
mg/I
mg/l
mg/1
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pegmittee (of Authorized Agen Name and Title - Please type or print
41.44 % 7/db
Signat of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name:
Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter:
2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 11.90 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.3 , Specific Conductance 574 uMhos
Temp. 22.6 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636
Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES �y
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Rotary Distributor
Other
Remediation: Infiltration Gallery
c.3
Land Application of Sludge cm
C7 i-`-1
CZ) a O
CIal
cprn
Note: Values should reflect dissolved and N a_ rri
0
colloidal concentrations &m
Date sample collected: 10/11/00 -pirn o
Date sample analyzed: 10/11/00 to 11/10/00 21='
Laboratory Name: PCS PHOSPHATE and thVII IAENT 1
Certification No(s) 330 10 �
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
mg/I
/100m1
/100m1
X Yes
Nitrite (NO2 as N)
No and field acidified X Yes
N/A
Nitrate (NO3 as N)
Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 400 mg/I Al - Aluminum
pH (when analyzed) 6.7 units Ba - Barium
TOC 4.7 mg/I Ca - Calcium N/A
N/A
0.275
N/A
N/A
N/A
Chloride
Arsenic
Grease and Oils
9.2 mg/I Cd- Cadmium
N/A mg/1 Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
37.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
<0.001
<0.005
N/A
N/A
N/A
N/A
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
0.046
mg/1
mg/I
mg/I
mgll
mg/I
mg/I
mg/I
mg/I
mg/1
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
No
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.55
N/A
N/A
N/A
N/A
VOC : method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pejwttt_etee (of Authorized nt) ame and Title - Please type or pr nt
i%7
24
a
Signat Permittee (or Authorized Agent) (D
te)
��a

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Orson
Well Identification Number (from Permit):
WeII Depth: 22.50 ft. Well Diamter:
SWW-1
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level:
Measuring Point is
GALLONS
4 inch
7.68 ft. below measuring point.
1.52 ft above land surface.
of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2715 uMhos
Temp. 21.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
O r5
3h
d•<•
10/13/00 •
10/13/00 to 11/13/00
PCS PHOSPHATE f\j rrr
Note:
Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1836
pH (when analyzed)
TOC
Chloride
Nitrite (NO2 as N)
Yes n/a No and field acidified
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as
Orthophosphate
mg/I Al - Aluminum
6.0 units Ba - Barium
11.2 mg/I Ca - Calcium
77.3 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
902.2 mg/I Hg - Mercury
Specific Conductance N/A uMhos K- Potassium
Total Ammonia
TKN as N
N/A mg/I Mg - Magnesium
N/A mg/1 Mn - Manganese
N/A mg/I
N/A mg/I
Ni - Nickel
Pb - Lead
Yes n/a No
N/A ug/I
N/A ug/I
P 118.500 mg/I Zn - Zinc N/A ug/I
N/A Ammonia Nitrogen vci-ng/I
N/A Other (Specify Compounds and Concentration Units) (.)
N/A mg/I Fluoride 0.59 , .4hg/1
N/A mg/I MIBK N/A mg/I
N/A mg/I Ag - Silver N/A • mg/I
N/A mg/I Se Selenium N/A to/I
N/A mg/I Sodium N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
mg/1
mg/1
N/A mg/I VOC
N/A mg/I
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Signatu
me and Title - Please type or pri
//
Permittee (or Authorized Agent)
(Date

x

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter:
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.22 ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2274 uMhos
Temp. 20.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636
Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery 03
Spray Field X Remediation :
Rotary Distributor Land Application of Sludgetzt
(,'2
0 Q
c)
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/13/00
10/13/00 to 11/10/00
PCS PHOSPHATE
Certification No(s) 330
n
`3
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
mg/l
/100m1
/100m1
1412 mg/I
6.4 units
10.1 mg/I
58.7 mg/I
N/A mg/I
N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Yes n/a
No and field acidified
N/A mg/l
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/1
92.500 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I Fe - Iron
568.7 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
N/A mg/I
Yes n/a No
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
mg/1
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
0.27 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
N/A ug/I
N/A mg/I Report attached? Yes (1) No X (2)
method#
N/A mg/I VOC
N/A mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ittee (of Authorized Agent) ame Title - Please type or pri t
ZZ
eU
Signatu ermittee (or Authorized Agent) (Da

DIVISION OF WATER QUALITY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]a1
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 24.50 ft. Well Diamter:
SWW-3
4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.83 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 1923 uMhos
Temp. 22.7 oC, Odor NONE
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Aj
� 1
Note: Values should reflect dissolved and 'C Q''/
Cs C-3
colloidal concentrations to b
Date sample collected:
Date sample analyzed: —C r 1
Laboratory Name: rfi
Certification No(s) 330
10/13/00
10/13/00 to 11/10/00
PCS PHOSPHATE
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
Use MPN method for highly turbid samples)
1244
6.4
8.9
33.2
N/A
N/A
N/A
519.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
uMhos
mg/I
mg/I
n/a
No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 46.500 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A mg/1
Ba - Barium N/A mg/I
Ca - Calcium N/A mg/I
Cd- Cadmium N/A mg/I
Chromium: Total N/A mg/I
Cu - Copper N/A mg/I
Fe - Iron
Hg - Mercury
N/A
N/A
K- Potassium
Mg - Magnesium
Mn - Manganese
mg/I
mg/I
N/A mg/I
N/A mg/I
N/A mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium _
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.15
N/A
N/A
N/A
N/A
VOC : method#
method#
method#
mg/l
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe tee (of Authorized Ag Na e and Title - Please type or print
/L //2
(Dat
Signal f Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter:
4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 7.05 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.0 , Specific Conductance 2540 uMhos
Temp. 33.8 oC, Odor NONE
For Groundwater Treat.men
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentratio
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
ns
111
10/13/00 -5 Aq
10/13/00 to 11/10/00 Z rn
PCS PHOSPHATE 1V �b
330 h �-,
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
Yes n/a
No and field acidified
N/A
(Note Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1556 mg/I Al - Aluminum
pH (when analyzed) 6.2 units Ba - Barium N/A
TOC 8.4 mg/I Ca - Calcium N/A
Chloride 44.0 mg/I Cd- Cadmium _ N/A
Arsenic N/A mg/I Chromium: Total _ N/A
Grease and Oils N/A mg/I Cu - Copper N/A
Phenol N/A
Sulfate 656.2
N/A
98.500
N/A
N/A
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I Fe - Iron
mg/I Hg - Mercury
N/A
N/A
uMhos K- Potassium
mg/I Mg - Magnesium
mg/1 Mn - Manganese
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
mg/l
mg/I
Ni - Nickel
Pb - Lead
Yes n/a No
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.11
N/A
N/A
N/A
N/A
VOC
method#
method#
method#
ug/I
ug/I
ug/I
mg/l
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P
Signat
f Authorized Agee$. Na/ne and Title - Please type or prin
e /t Z/G
(Date)
L
-Permittee (or Authorized Agent)

/ \�\%tti-•
:241
«

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 7.51 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.1 , Specific Conductance 2662 uMhos
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Temp. 30.1 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Galled
c_
X Remediation :
c./3
Land Application of Sludge
ts�
L7
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/13/00
10/13/00 to 11/10/00
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1628
pH (when analyzed)
TOC
Chloride
6.4
12.4
56.9
Arsenic
Grease and Oils
Phenol
Sulfate
mg/I
units
mg/I
mg/I
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
Yes n/a No and field acidified Yes n/a No
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
N/A mg/1 Ni - Nickel
N/A mg/I Pb - Lead
52.000 mg/l Zn - Zinc
mg/1
mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
Orthophosphate N/A Ammonia Nitrogen
Al - Aluminum N/A Other (Specify Compounds and Concentration Units)
Ba - Barium Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS. HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/1 VOC : method#
N/A mg/I
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
778.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
:,N/An vg/I
WN/A:::1 ug/I
Witt ug/I
0.28
N/A
N/A
N/A
N/A
method#
method#
mg/1
mg/I
mg/I
mg/I
mg/I
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Perrmittee (of Authorized . entj/Name and Title - Please type or print
r 4'
igS natuPermittee (or Authorized Agent)
1/z7/ t
(Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
Screened Interval: 22.25 ft. to 24.62 ft.
4 inch
Depth to Water Level: 7.38 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2112 uMhos
Temp. 30 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
09/30/01
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations O )
Date sample collected: 10/13/00 c�
Date sample analyzed: 10/13/00 to 11/10/01V CD
CO Laboratory Name: PCS PHOSPHATE >�
Certification No(s) 330 -0 _ac--i\
rrIk-
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1464 mg/1
pH (when analyzed) 5.9 units
TOC 12.5 mg/I
Chloride 106.2 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I
Sulfate 401.7 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mgll
N/A mg/I
Yes n/a No and field acidified Yes n/a No 'v ru'.,
Nitrite (NO2 as N) N/A mg/l Ni - Nickel .c' VA ug/I
Nitrate (NO3 as N) N/A mg/I Pb - Lead (" A ug/I
Phosphorus: Total as P 53.500 mg/I Zn - Zinc /A ug/I
Orthophosphate N/A mg/I Ammonia Nitrogen mg/I
Al - Aluminum N/A mg/I Other (Specify Compounds and Concentration Units)
Ba - Barium N/A mg/I Fluoride 0.08 mg/I
Ca - Calcium N/A mg/I MIBK N/A mg/I
Cd- Cadmium N/A mg/I Ag - Silver N/A mg/I
Chromium: Total N/A mg/I Se- Selenium N/A mg/I
Cu - Copper N/A mg/I Sodium N/A ug/I
Fe - Iron N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC method#
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mgll : method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Ageae and Title - Please type or prin
// �7
Signatur-,J Permittee (or Authorized Agent)
(Da

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter:
Screened Interval: 25.17 ft. to 27.50 ft.
4 inch
Depth to Water Level: 7.11 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.8 , Specific Conductance 1220 uMhos
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
G7
Other C�
W
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/13/00
Date sample analyzed: 10/13/00 to 11/10/00
Laboratory Name: PCS PHOSPHATE
a
.t=
Gj
Temp- 26.5 oC, Odor NONE Appearance: LT YELLOW Certification No(s) 330
rr
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 880 mg/I Al - Aluminum
pH (when analyzed) 6.0 units Ba - Barium
TOC 12.2 mg/I Ca - Calcium
Chloride 75.4 mg/I Cd- Cadmium
/A Z ;i3/1
76.500 mg/I Zn - Zinc I/ANC/I
N/A mg/I Ammonia Nitrogen y mg/I
N/A mg/I Other (Specify Compounds and Concentration Units) O
N/A mg/I Fluoride 0.1mg/I
N/A mg/I Pb - Lead
N/A mg/I MIBK N/A mg/I
N/A mg/I Ag - Silver N/A mg/1
Arsenic N/A mg/I Chromium: Total
Grease and Oils N/A mg/I Cu - Copper
Phenol N/A mg/I Fe - Iron
N/A mg/I Se- Selenium N/A mg/I
N/A mg/I Sodium N/A ug/l
N/A mg/I Organics: (GC, GC/MS, HPLC)
Sulfate 214.0 mg/I Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos K- Potassium
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC
N/A mg/I
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P- tee (of Authorized A•_ t) N .me and Title - Please type or print
Signat ,(_'• Permittee (or Authorized Agent)
(Date)

0.

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter:
2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.42 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.2 , Specific Conductance 486 uMhos
Temp. 22.7 oC, Odor
NONE Appearance: CLEAR
Mail Original
to
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED Q
Lagoon Remediation: Infiltration Gall
Spray Field X Remediation :
UIC X
Rotary Distributor Land Application of Sludge
Other
•
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/13/00
Date sample analyzed: 10/13/00 to 11/10/00
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified Yes n/a No N "c
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel 4g/A r f
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead .01/A 41g/I
Coliform: MF Total N/A I100m1 Phosphorus: Total as P 0.538 mg/I Zn - Zinc N/A 2 ug/I
Orthophosphate N/A mg/I Ammonia Nitrogen mg/1
mg/1 Al - Aluminum N/A mg/l Other (Specify Compounds and Concentration Units)
units Ba - Barium N/A mg/I Fluoride 2.30 mg/I
mg/I Ca - Calcium N/A mg/I MIBK N/A mg/I
mg/1 Cd- Cadmium N/A mg/1 Ag - Silver N/A mg/I
mg/I Chromium: Total N/A mg/I Se- Selenium N/A mg/I
mg/I Cu - Copper N/A mg/I Sodium N/A ug/I
mg/I Fe - Iron N/A mg/I Organics: (GC. GC/MS, HPLC)
mg/I Hg - Mercury N/A mg/I (Specify test method #. Attach lab report.)
uMhos K- Potassium N/A mg/I Report attached? Yes (1) No X (2)
mg/I Mg - Magnesium N/A mg/I VOC : method#
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 312
pH (when analyzed) 7.0
TOC 4.6
Chloride 4.0
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate <10.0
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I Mn - Manganese N/A mg/I method#
method#
I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe ttee of Authorized Age Nee and Title - Please type or print
1//2- 7(e
PPermittee (or Authorized Agent) (Date
'rrn
Signatu

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter:
2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 5.18 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 5.8 , Specific Conductance 400 uMhos
Temp. 23.7 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
UIC X
Lagoon
Spray Field
Rotary Distributor
X Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/13/00
Date sample analyzed: 10/13/00 to 11/10/00
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1
292 mg/I
5.9 units
Yes n/a
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
3.6 mg/I Ca - Calcium
Chloride
42.7 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/1
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
34.4 mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
7.800 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
A
/A /I
mg/l
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC. GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
0.29
N/A
N/A
N/A
N/A
N/A mg/I VOC method#
method#
method#
N/A mg/I
mg/I
mg/1
mg/I
mg/1
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P ittee of Authorized Ag ,a Nrme and Title - Please type or pri t
zed A
Signatuy�of Permittee (or Authori gent ) (Dat )

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.7.

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: N/A ft. Well Diamter:
WLCT
N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.5 , Specific Conductance 574 uMhos
Temp. 16.4 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/11/00
Date sample analyzed: 10/11/00 to 11/10/00
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A mg/I Nitrite (NO2 as N) N/A
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.038
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A
Dissolved Solids: Total 500 mg/I Al - Aluminum N/A
pH (when analyzed) 7.3 units Ba - Barium N/A
TOC 6.8 mg/I Ca - Calcium N/A
Chloride 10.4 mg/I Cd- Cadmium <0.001
Arsenic N/A mg/l Chromium: Total <0.005
Grease and Oils N/A mg/I Cu - Copper N/A
N/A mg/I Fe - Iron
17.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A mg/I Mn - Manganese
<0.001
No and field acidified X
mg/I Ni - Nickel
mg/I
mgll
Pb - Lead
Zn - Zinc
Yes No
mg/I Ammonia Nitrogen
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
N/A �� C.
N/A %/I :
N/Aitttg/ly
mcq
054
N/A c3ng/I
N/A '"mg/1
N/A mg/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe rittee (of Authorized Ageaij Name and Title - Please type or print
f/
1t7 416
Signatu
ermittee (or Authorized Agent)
(Dat

Date:
Time:
Tech:
PCS Phosphate Co. Inc. - Tank Farm Remediation System Quarterly Monitoring
/01/08
IQ/%/
System Gauge Pressures
SW W-1
SWW-7
cW W-1
CW W-7
0-// Air
D - 9 Sr
File: 15-03-003.02
pc: TLB
Level (msl)
Ditch Level
-1/ B
Barge Slip
2Lc?
Water Level
99/
Control Tank
%= MSL
/5:07'
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level. ''
Level
Relative To
MSL Ft.
Spz-1
10.47
-p. ro
4. 07
Cpz-1
10.51
9 1
A 7
Spz-2
11.21
y/- 46
of 7
Cpz-2
10.25
/19. en
0. A/
Spz-3
11.87
/p‘,9V
cc/
Cpz-3
11.12
9 99
/22
-0.n.'9,
9, 93
Spz-4
11.45
47-7$
o 9
CPW
9.65
/, D/Y
Spz-5
11.45
9. -re
/ 97
MWTF-1A"
14.35
//.�.?
Spz-6
11.23
9 /a/
15 9
MWIT-1B*
14.36
5`/)
9. /1'
Spz-7
11.59
/Q.. 4
/ 53
MWTF-1C`
14.44
//4D
IJ/i
Spz-8
11.57
7Y"
i
MWTF-2A
14.05
- -al
-2. -7
Spz-9
11.01
p„ 5'6
P% «5
MWrF-2B
14.02
/4 4/
� 6E
Spz-10
12.16
4. /I
6. / f
MWTF-2C
14.08
/4 a
-DD.. 4<1
SPW
9.95
791
ct D%
MWTF-3A
12.21
.92
p.d17
50z 1,4-
eome%r
don
Covered U% 4t- 1
Acn'/ in, 2 i /
MWrF-3B
12.18
/Q•il
I O O
MWTF-3C
12.19
/ q/O
-/A/
-�../
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level
Relative To
MSL Fit .
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o4
Comments
SWW-1
10.70
/61
+1' to+2'
CWW-1
10.60
..771/'
/.01,5.-
'Ic77s
-2'to -1'
y�i
ei
SWW-2
9.99
7,1a
l
.+, 'to+2'
/�'f5
CWW-2
10.23
/,5.�f
'o/�
/e. «'3ia
-2'to-1'
/y y
SW
9.97
/. 0 J
/ D
+1' to +2'
yam,
VV-3
CWW-3
9.95
'7/j9
V. pJ 1)
-2 'to-,'
yeS
10.73
7as-
/9S-
+1'to+2'
y
SWW4
CWW4
10.73
6"i1
yA5
07•o2/G
-2' to-1'
y/)/
10.80
'7i577
/ 57
+1' to+2'
9'3
SVVW-5
CWW-5
10.74
`yo%Q
-/ fO
-2'to-1'
,ef
W SW-6
10.66
Is/ e
/. 3s.1ca
+1' to +2'
/6'0.
CWW-6
9.92
..5 3
7 7
-2' to-1'
71
10.70
7//
1. ////
+1 'to+2'
Xpy
SWW-7
W CW-7
9.95
2Ok
-/9
-2'to-1'
yeti
Revised 8/12/97
* Riser length added to TOC elevation 1/24/97
PCS095.XLS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
August 2000 — October 2000
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
2000
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
August
337,250
0
337,250
7.6
13.8
September
293,820
0
293,820
6.8
13.8
October
335,630
0
335,630
7.5
13.8
TOTALS
966,700
0
966,700
3

Withdrawal Well System
The Withdrawal Well System was down for a total of 3.0 hours during the period. The system was down
on 10-25-00 for 3.0 hours to repair the air compressor. The withdrawal water well pumps are monitored
daily by the area Maintenance Department and preventative maintenance work is performed as needed.
The total monthly and quarterly withdrawal water volumes for the period are:
2000
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
August
487,519
165,475
652,994
14.6
September
517,822
192,635
710,457
16.4
October
316,261
166,948
483,209
10.8
TOTALS
1,321,602
525,058
1,846,660
Some addrtionaI short penods of planned downtime for preventative maintenance,—pipe-headercleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 8/14 replaced totalizer. On 8/17 the pump was shaken to start. On 9/1 the pump was
replaced.
SWW-2: On 8/17 & 8/22 the pump was shaken to start. On 10/11 the pump was replaced.
SWW-3: On 9/19 the airline was found plugged this was repaired. On 10/2 the pump was shaken to start.
SWW-4: On 10/11 the pump was shaken to start. On 10/13 the counter was replaced. On 10/31 the pump
was replaced.
SWW-5: On 10/20 the pump was shaken to start.
SWW-6: On 10/18 the pump was replaced.
S W W-7: Pump operated without incident.
4
•

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 10/25 the pump was replaced.
CWW-2: On 8/31 & 9/26 the pump was shaken to start. On 10/5 the pump was acid washed.
CWW-3: On 8/14 the pump was replaced.
CWW-4: Pump operated without incident.
CWW-5: Pump operated without incident.
CWW-6: Pump operated without incident.
CWW-7: On 10/12 the air -regulating valve was replaced.

November 27 2000
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
PCS
PhosphateW AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
ti
CD�:-
r.) oC
ADM
'0 rr
�C -;*
rV rn
Subject: Underground Injection Control Program .c
CD
Third Quarter Groundwater Monitoring Report `''
August 2000 - October 2000
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF 1 A and MWTF 1 B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
&tivIA3LQ. \).(1'11:0` jjr-
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison / Keith Starner - DWQ- GWS, WaRO (w/attch)
•

bpc: T. L. Baker / 12-01-008-03-002 (w/ attch)
J. A. Hardy / R. B. Lee / T. W. Davis (w/ attch)
R. A. Allen / T. Lewis (w/attch)
D. D. Winstead / 00-24-000 (w/o attch)
W. A. Schimming (w/o attch)
s
2