WI0700012_1998 Monitoring (Report)_19981125

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
m,.
Mail Original
to:
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter: 4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 6.40 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2618
uMhos
Temp. 21.4 oC, Odor NONE Appearance:
CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Studgg,
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/15/98
Date sample analyzed: 10/15/98 to 10/28/98
Laboratory Name: PCS PHOSPHATE
Certification No(s)
330
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
mg» Nitrite (NO2 as N)
/100m1
/100m1
1676 mg/1
6.4 units
11.8 mg/I
49.5 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
764.9 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Nitrate (NO3 as N)
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
179.000 mg/I Zn - Zinc
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
ug/I
ug/I
ug/I
ug/I
ug/I
u g/1
ug/I
ug/I
ug/l
Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration-Wnits)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
ug/I VOC
ug/I
0.46
N/A
N/A
N/A
N/A
mg/1
mg/I
ug/I
u g/I
ug/I
ug/I
(1) No (2)
: method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate, and completeand that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
GW-59 Rev 4/98
Permittee uthorize
Signatu of Permittee (or Authorized Agent)
Name and Title - Please type or print
//- L S -9
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval:
Depth to Water Level:
Measuring Point is
18.80 ft. to 21.63 ft.
6.86 ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 2208 uMhos
Temp. 20.6 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge X
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE: 09/30/01
UIC
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/15/98
..t
10/15/98 to 10/28/9e.
PCS PHOSPHATE
330
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid samples)
N/A
N/A
N/A
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
mg/1 Nitrite (NO2 as N)
/100m1
/100m1
1500 mg/I
6.7 units
11.1 mg/I
37.5 mg/I
N/A mg/I
Grease and Oils
N/A mg/1
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
No
N/A
Nitrate (NO3 as N)
Phosphorus: Total as
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
and field acidified X
N/A
P 59.000
N/A
N/A
N/A
N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
647.1 mg/I Hg - Mercury
N/A
N/A
N/A
N/A
N/A
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
N/A
mg/I
mg/l
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
ug/l
ug/I
ug/I
ug/I
ug/I
ug/I VOC
ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes No )
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride 0.20
MIBK N/A
Ag - Silver N/A
Se- Selenium N/A
Sodium N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
N/A ug/I
r j N/A ug/I
N/A ug/I
mg/1
(1) No
method#
method#
method#
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
GW-59 Rev 4/98
Crrv. 1.0".
Permittee (9€y4uthorjed b.gynt) )lame and Title - Please type or print
(Date)
Signature of Permittee (or Authorized Agent)
�.cc. c.0 (-IA

+
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
(ham p'n
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval:
Depth to Water Level:
Measuring Point is
20.17 ft. to 23.00 ft.
8.34 ft. below measuring point.
3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2346 uMhos
Temp. 23.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORE
Lagoon Remediation: Infiltratiori.91lery
Spray Field X Remediation :
Rotary Distributor Land Application of Slud
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/15/98
10/15/98 to 10/28/98
PCS PHOSPHATE
330
09/30/01
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1484
pH (when analyzed) 6.2
TOC 10.1
Chloride 39.6
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate 653.3
Specific Conductance N/A
Total Ammonia N/A
TKN as N N/A
mg/I
/100m1
/100m1
mg/1
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
X Yes
Nitrite (NO2 as N)
No and field acidified X Yes No )
N/A mg/1 Ni - Nickel
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/1 Pb - Lead
106.500 mgll Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
co.( 3 N/A ug/I
..1•� N/A ug/I
�. mg/l
N/A ug/I Other (Specify Compounds and ConcentrationlUnits)
N/A ug/I Fluoride
N/A ug/I
N/A ug/I
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No (2)
N/A ug/I VOC : method#
method#
method#
N/A ug/I
0.22
N/A
N/A
N/A
N/A
mg/I
ug/I
ugll
ug/I
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
GW-59 Rev 4/98
I v l'4 ArV2 171eC o C/' - O I. ' ilr• E' Nd l' n G...,,
Permittee (of A rized ) e and Title - Please type or print
„eow
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
from
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter: 4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 7.13 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Field Analysis: pH 6.2 , Specific Conductance 2493 uMhos
Temp. 34.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of SIu
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/15/98
10/15/98 to 10/28/98
PCS PHOSPHATE
09/30/01
330
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1388
6.2
8.8
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
42.6
N/A
N/A
N/A
603.6
N/A
N/A
N/A
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
-73
•
N/A ug/I
N/A mg/I Pb - Lead N/A;, ug/I
110.500 mg/I Zn - ZincN/A ug/I
N/A mg/1 Ammonia Nitrogen Co mg/1
N/A ug/I Other (Specify Compounds and Concentration (irks)
N/A ug/I Fluoride -,-a 0.10 mg/I
N/A ug/I MIBK -c' N/A ug/I
N/A ug/I Ag - Silver N/A ug/I
N/A ug/I Se- Selenium ---1 N/A ug/I
N/A ug/l Sodium"""' N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No (2)
N/A ug/I VOC : method#
N/A ug/I method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
GW-59 Rev 4/98
60 . Pic Go . E.1 v_ 6 M4s•1.ee,
Permittee (of
e gent Name and Title - Please type or print
//--As-sc
Signature of Permittee (or Authorized Agent) (Date)

4.
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter: 4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 7.13 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2480
uMhos
Temp. 29.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/15/98
Date sample analyzed: 10/15/98 to 10/28/98
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
09/30/01
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
mg/I Nitrite (NO2 as N)
/100m1
/100m1
1512 mg/I
6.4 units
11.2 mg/I
62.9 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/1
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
651.2 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Nitrate (NO3 as N)
No and field acidified X Yes No )
N/A mg/I
N/A mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
46.000 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
Ni - Nickel/A ug/I
Pb - Lead C 1VllA ug/I
Zn - ZincCAJ PJ/ ug/l
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units) ,CJ
Fluoride 0.211- mg/I
MIBK N/tpug/I
Ag - Silver N/A_,lug/I
Se- Selenium N/Aug/I
Sodium N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
N/A ug/I VOC
N/A ug/I
(1) No
method#
method#
method#
(2)
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
GW-59 Rev 4/98
10
Permittee (of ' oriz
. 'a mt
ame and Title - Please type or print
Signature of Permittee (or Authorized Agent)
(Date)

4
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
SWW-6
Well Depth: 26.00 ft. Well Diamter: 4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level:
Measuring Point is 2.58 ft above land surface.
7.48 ft. below measuring point.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2111 uMhos
Temp. 32.5 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation
Rotary Distributor Land Application of Sludgl.
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/15/98
Date sample analyzed: 10/15/98 to 10/28/98-
Laboratory Name: PCS PHOSPHATE -
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1244
6.4
11.4
103.4
N/A
N/A
N/A
307.1
N/A
N/A
N/A
mgll Nitrite (NO2 as N)
/100m1
/100m1
mg/1
units
mg/l
mg/I
mg/I
mg/I
mg/l
mg/l
uMhos
mg/I
mg/I
Nitrate (NO3 as N)
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
40.500 mg/l
N/A mg/l
N/A ug/I
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A ug/I
• N/A ug/l
N/A ug/I
Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
mg/I
0.08 ulg/1
N/A WI
N/A d /I
N/A ug/I Se- Selenium N/A
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC) --!
N/A ug/I (Specify test method #. Attach lab report.) uI
N/A ug/I Report attached? Yes (1) No (2)
N/A ug/I VOC : method#
method#
method#
N/A
I certify that. to the best of my knowledge and beliefthe information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
GW-59 Rev 4/98
Signature of Prmittee (or Authorized Agent)
gr• E•zv. �.+f.�ma.L
Permittee (of th zed Pent) Name and Title - Please type or print
`7- 4s -yF
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
(frog pamm.,
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter: 4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
7.13 ft. below measuring point.
3.00 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 1466 uMhos
Temp. 27.6 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/15/98
10/15/98 to 10/28/98
PCS PHOSPHATE
330
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1048 mg/I Al - Aluminum
pH (when analyzed) 5.9 units Ba - Barium
TOC 14.0 mg/1 Ca - Calcium
Chloride 84.6 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A
mg/I Pb - Lead
81.000 mg/1 Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/i
N/A ug/I
N/A ug/I
N/A ug/I
N/A mg/I Chromium: Total
N/A mg/1 Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1 Fe - Iron
263.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/l
Other (Specify Compounds and Concentration
Fluoride
MIBK
(,) N/A ug/I
c—' N/A ug/I
N/A ug/I
mg/I
Units)
—!0.1 ng/1
N/ACg/I
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
Ag - Silver N/ACg/I
Se- Selenium N/Attg/I
N/Aug/I
N/A ug/I VOC
N/A ug/I
(1) No
method#
method#
method#
(2)
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
Permittee (of zed Ag
i'r P .C4, C
and Title - Please type or print
G/ Lr�9L
GW-59 Rev 4/98
Signature of Permittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
(*"
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter: 2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.01 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
MILLILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 7.3 , Specific Conductance 572 uMhos
Temp. 24.0 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/16/98
10/16/98 to 10/28/98
PCS PHOSPHATE
330 t='
09/30/01
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 312
pH (when analyzed) 7.2
TOC 4.9
Chloride
Arsenic
Grease and Oils
N/A mg/1 Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
N/A /100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
10.4 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mgll Fe - Iron
<10.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
No and field acidified X
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
0.365 mg/I
N/A mg/I
N/A ug/1
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
Yes No )
Zn - Zinc
Ammonia Nitrogen
N/A
NIA
'N)A
ca
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
N/A ug/I VOC
N/A ug/I
(1) No
: method#
method#
method#
2.29
N/A
N/A
N/A
N/A
ug/I
ug/1
crg/I
mi
ug
ug
ug
ug/lco
(2)
certify that, to the best of my knowledge and belief. the information submitted in this report is trueaccurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
Permittee (of Aut%d A ent am nd Title - Please type or print
GW-59 Rev 4/98
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter: 2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 5.00 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILLILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 5.9 , Specific Conductance 606 uMhos
Temp. 25.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Slud
Other
EXPIRATION DATE:
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/16/98
10/16/98 to 10/28/98' '
PCS PHOSPHATE 3
330
09/30/01
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 392
pH (when analyzed) 7.2
TOC 4.5
Chloride 68.2
Arsenic N/A mg/I
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Grease and Oils
Phenol
Sulfate
No and field acidified X
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/1
units
mg/I
mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
49.2 mg/1
N/A uMhos
N/A mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
8.950 mg/I Zn - Zinc
Yes No )
N/A mg/I Ammonia Nitrogen
ra/A 'ug/I
N/A ug/I
Nl'A ug/I
N/A ug/I Other (Specify Compounds and Concentration Units)
mg/l
N/A ug/I Fluoride 0.272ng/I
N/A ug/I MIBK N/A; eytg/I
N/A ug/I Ag - Silver N/A ,,.lrrg/I
N/A ug/I Se- Selenium N/A Mil
N/A ug/I Sodium N/A ugA
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/l (Specify test method #. Attach lab report.)
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I Report attached? Yes (1) No (2)
N/A ug/I VOC : method#
N/A ug/1
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
GW-59 Rev 4/98
rcJ J`° cX I ta--c c k
Permittee (of A 4 orized Agen ame and Title - Please type or print
7/ ZsYF
(Date)
Signature of Permittee (or Authorized Agent)
• •� • V. �nf.A°G"

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
* WELL OUT OF COMMISSION
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-C*
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Milliliters of water pumped/bailed before sampling: N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge,
Other
09/30/01
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed: to
Laboratory Name:
Certification No(s) 330
PCS PHOSPHATE
C)
'17,1""
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and
Phenol
Sulfate
N/A
N/A
N/A
Use MPN method for highly turbid samples)
N/A
N/A
N/A
N/A
N/A
Oils N/A
N/A
N/A
N/A
N/A
N/A
Specific Conductance
Total Ammonia
TKN as N
mg/I Nitrite (NO2 as N)
/100m1
/100m1
mgll
units
mg/I
No
N/A
and field acidified X Yes No )
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I Ni - Nickel N/A ug/I
mg/I Pb - Lead N/A ug/I
mg/I Zn - Zinc ..NJ/A ug/I
mg/I Ammonia Nitrogen - mrtg/I
ug/I Other (Specify Compounds and Concentration Urnts)
ug/I Fluoride N/A rfyl'
ug/l MIRK N/A ugh
ug/I Ag Silver N/A ug/1D
ug/I Se- Selenium N/A ug/r.
ug/l Sodium N/A ugh)
ug/I Organics: (GC, GC/MS, HPLC) —a
ug/I (Specify test method #. Attach lab report.) "'Y
ug/I Report attached? Yes (1) No (2)
ug/I VOC : method#
ug/I method#
method#
I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurateand complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
* NOTE: WELL DAMAGED, NO SAMPLE
+� t . iqe-41.c. Pi v. , ;-► cnt
Permittee (o thorize) Name and Title - Please type or print
GW-59 Rev 4/98
Signature of Permittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter: 4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.2 , Specific Conductance 536 uMhos
Temp. 24.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
sample collected: 10/13/98 c
Date
e,-)
Date sample analyzed: 10/13/98 to 11/12/98-"
Laboratory Name: PCS PHOSPHATE/ENVIRONMENT 1
Certification No(s) 330 10 r
09/30/01
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total <1.0 /100m1
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Use MPN method for highly turbid samples)
336
7.4
4.5
Chloride
mg/I
units
mg/I
8.1 mg/1
Arsenic
Grease and Oils
N/A mg/I
N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/l
<10.0 mg/I
N/A uMhos
N/A mg/I
N/A mg/l
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
0.025
N/A
N/A
N/A
N/A
1.7
<5.0
N/A
N/A
N/A
N/A
N/A
<10.0
mg/l Zn - Zinc
mg/I Ammonia Nitrogen
ug/I
ug/I
ug/I
ug/I
ug/l
ug/I
ug/I
ug/l
ug/I
ug/I
ug/I
t /A ig/I.
1 /A
`l /A(I.
i439/1
Other (Specify Compounds and Concentration Units)
Fluoride 0.65 rrila
MIBK N/A ug
Ag - Silver N/A ug a�
Se- Selenium N/A ug/I
Sodium N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
GW-59 Rev 4/98
�eC4 GOLi
Permittee (of Authorized ) m_
Signature of
rmittee (or Authorized Agent)
cc/. GICI Li. IVMtge.
le - Please type or print �j
//Ls —sue
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): WLCT
Well Depth: N/A ft. Well Diamter: N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level:
Measuring Point is
N/A ft. below measuring point.
N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.4 , Specific Conductance 474 uMhos
Temp. 19.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge X UIC
NPDES Non Discharge
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/13/98
10/13/98 to 11/12/98
PCS PHOSPHATE/ENVIRONMENT 1
330 10
t.n
7
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A mgll Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Orthophosphate
332 mg/I Al - Aluminum
7.6 units Ba - Barium
4.4 mg/I Ca - Calcium
7.9 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
0.022 mg/I Zn - Zinc
-1/A
..N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
<1.0 ug/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
<10.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
<5.0 ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
0.63
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/I
mg}4f,
ug/I�
ug/I
ug/l
ug/I
1/4-C7
N/A ug/I Report attached? Yes (1) No (2)
: method#
method#
method#
N/A ug/I VOC
<10.0 ug/I
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE: WELL DAMAGED, NO SAMPLE
tr.c.c �ecc coc��
Permittee (of t) d Title - Please type or print
GW-59 Rev 4/98
Sign oTPermittee (or Authorized Agent)
ZSitf
(Date)

PCS
Phosphate
memo
Date November 9, 1998
To L. M. Montgomery Location Env. Affairs
From T. L. Baker Location Ops. Env.
Subject TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT
FOR AUGUST, 1998 — OCTOBER, 1998
The attached subject report, with required operational and
maintenance data, is provided for submittal to NC DENR-
Division of Water Quality, Ground Water Section, Underground
Injection Control Program. This report should be submitted
along with the laboratory sampling and water level monitoring
data.
If you have any questions concerning this information, please
contact me.
T. L. Baker, Superintendent
Operations Environmental
Attachment
pc: W. K. Thornton
S. A. Beckle/W. H Paulson/G. Coghill
Randy Allen
Tommy Lewis
T. W. Davis/OE-00-01-00-08
C:\Mydata\OEDept\TFRAP\OPDATA1098.doc

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
AUGUST, 1998 - OCTOBER, 1998
The Tank Farm Remediation System consists of a series of seven
injection water wells located on the south side of the Tank
Farm Area and a series of fourteen (14) water withdrawal wells
located on the north side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water -
Anthracite Sand Filter / Ultraviolet Light (ASF/UV)
disinfection system throughout the period. Short periods of
planned downtime were experienced for preventative maintenance
and inlet DPW Water strainer cleaning.
Daily operational data are collected by the Shipping Department
and reported to the Operations Environmental Department. The
total monthly and quarterly volumes of water injected as well
as the month end water level in the Water Level Control Tank
are:
INJECTED WATER TOTALS.
1998
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Aug
538,020
0
538,020
12.1
15.0
Sep
- 524,760-
- - 0
524,760 -
- 12.1-
-- 14.9-
Oct
554,030
0
554,030
12.4
14.9
TOTALS
1,616,810
0
1,616,810
Withdrawal Well System
The Withdrawal Well System operated the entire period. The
withdrawal water well pumps are monitored daily by the area
Maintenance Department and preventative maintenance work is
performed is needed. The total monthly and quarterly
withdrawal water volumes for the period are:
WITHDRAWAL WATER -TOTALS
1998
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Aug
532,319
323,534
855,853
19.2
Sep
518,237
282,124
800,361
18.5
Oct
458,040
284,780
742,820
16.6
TOTALS
1,508,596
890,438
2,421,668
2

Some additional short periods of planned downtime for
preventative maintenance, pipe header cleaning, and
troubleshooting on individual pumps in the fourteen well system
were experienced. Details of these activities are:
Air Compressor for the Withdrawal Well Pumps
An air compressor with air dryer supplies the pneumatic power
for the fourteen withdrawal well pumps. On 9/21 a problem was
detected with a valve on the south tower of the air dryer. The
air compressor was shutdown for three hours to clean the cooler
and to change the separator and air filter. On 9/22 the faulty
valve on the south tower of the air dryer was replaced. On
9/24 the air compressor was shutdown for two hours to replace
belts and change the oil and oil filter.
Withdrawal Well Pump Discharge Piping
On 10/28 the underground discharge piping headers from the SWW-
1, 2, and 3 and CWW-1, 2, and 3 pumps were cleaned with
hydrochloric acid (HC1);.
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1; On 8/10 the pump stopped due to scale buildup. On 8/11
the pump was cleaned with HC1 and placed back in operation.
SWW-2; The pump operated the period with no problems.
SWW-3; On 8/10 the pump stopped due to scale buildup. On 8/11
the pump was cleaned with HC1 and placed back in operation. On
10/19 it was determined that the pump required rebuilding with
new parts and the well was cleaned with HC1. On 10/20 the pump
was returned to operation with a new type cycle counter. On
10/22 the pump stopped and was shaken to start.
SWW-4; On 10/29 the pump stopped and was shaken to start.
SWW-5; On 8/20 the pump was determined to be scaled up and was
cleaned with HC1.
SWW-6; The pump operated the period with no problems.
SWW-7; On 8/3 the pump stopped and was shaken to start.
3

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1; On
On 8/6
operation
9/10 the
pump was
9/24, 25,
On 9/29
operation
8/4 and 8/5 the pump stopped and was shaken to start.
the pump was cleaned with HC1 and placed back in
▪ On 9/9 the pump cycle counter malfunctioned. On
cycle counter was replaced with the new type and the
cleaned with HC1 for preventative maintenance. On
28, and 29 the pump stopped and was shaken to start.
the pump was cleaned with HC1 and placed back in
. On 10/22 the pump stopped and was shaken to start.
CWW-2; The pump operated the period with no problems.
CWW-3; On 8/25 the pump stopped and was shaken to start. On
10/29 the pump cycle counter malfunctioned. A leak in the air
supply line to the counter was found and repaired on 10/30.
CWW-4; The pump operated the period with no problems.
CWW-5; On 9/22 the pump stopped and was shaken to start. On
10/1 the pump cycle counter malfunctioned and was replaced with
the new type counter.
CWW-6; The pump operated the period with no problems.
CWW-7; On 9/1 the pump stopped and was shaken to start.
4

• Pcs
Phosphate AURORA DIVISION
P.O. BOX 48, AURORA, NC 27806
November 20,1998
Underground Injection Control Program
Division of Water Quality, Groundwater Section
North Carolina DENR
P. O. Box 29578
Raleigh, North Carolina 27626-0578
Attention of Mark Milligan
Subject: Fourth Quarterly Groundwater Monitoring Report for 1998
Injection Well Permit #WI0700012
PCS Phosphate Co., Inc.
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find enclosed, the 4th Quarterly Tank Farm Remedial Action System groundwater
monitoring report for 1998, per the requirements of the above referenced permit. Additional
Compliance Monitoring Report Forms for well CIW-7 and the WLCT are included in this report
along with the monthly piezometer level monitoring field sheets and a summary performance
report of the individual wells.
Month In'ected :al Withdrawn (. al)
August
September
October
538,020
524,760
554,030
855,853
800,361
742,820
Totals
1,616,810
2,399,034
Please contact me at [phone] if you have any questions regarding this information.
Sincerely,
Leon M. Montgomery
Environmental Engineer
Attachments
pc:
Willie Hardison - DWQ, WaRO (w/attch)

bpc: W. A. Schimming (w/o attch)
S. R. Phillips / 00-19-000 (w/o attch)
T. L. Baker/T. W. Davis (w/attch)
M. L. Asby / J. A. Hardy (w/attch)
15-03-003-02 (w/ attch)
12-01-008-03-002 (w/ attch)

t_ r
PCS Phosphate Co., Inc.y - Tank Farm Remediation System Monitoring
A%/i/
Date:
Time:
Tech:
System Gauge Pressures
SWW-1
0 - 459 7s;
SWW-7
0- `iy`'
CWW-1
- / "7 ,
CWW-7
%
- . .42-:; ,
File: 15-03-003-02
pc: TLB
L
Level (mist)
Ditch Level
,5 0/
Barge Slip
9 O '
Water Level
_�
Control Tank
I✓ v
°Jo=MSL
i'Y n94
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level '
Level
Relative To
MSL Ft.
Spz-1
10.47
,,L//evel
/- .1,/
,,,23
Cpz-1
10.511
7/'
f-3el
/ 07
Spz-2
11.21
7 90
5 3 j
Cpz-2
10.25
9 , / N
Spz-3
11.87
..0
57-.63
Coz-3
11.12
7 7,
,". 3�&
Spz-4
11.45
�• (4.2
y.�J3
CPW
9.65
cg. 6 /
0• /7
Spz-5
11.45
g- 82
.. t, 3
MWTF-1A •
14.351
.5- J7
// /p5 -
Spz-6
11.23
8- /f
,fig--.5
MWrF-113 *
14.36
/7" /
9 9.g
Spz-7
11.59
/. O
/, '
/ 3 7
W
MTF-1C •
14.44
V,.912,96c-60
/j/
Spz-8
11.57
.:49
, &'/
MWTF-2A
14.05
A,-2fj
!l 79'
Spz-9
11.01
7/9A
S 17,
W
MTF-2B
14.02
/0.
.3 '7.)" �
Spz-10
12.16
^ Y/, 7C1
73g
MWTF-2C
14.08
l-f :q
�•'72
SPW
9.95
7
.:__., 6, 9
MWTF-3A
12.21
^
g
8• �(p
MWTF-3B
12.18
L
j, .Jij
a . 647
MWTF-3C
12.19
Al, 1:5
0-31
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Wet
Pumping
(Y)es/(N)o
Comments
SWW-1
10.70
4, S i.
O. . /
+1. to +2'
It j
CWW-1
10.60
7 7
-/ 73
-2'to-1'
}i
SWW-2
9.99
J y/
/ �/
+1. to +2'
}�
CWW-2
10.23
, 4
-:?7. - 7
-2 ' to -1'
�
SWW-3
9.97
77/
/, y/
+1'to+2'
i
CVWV-3
9.95
g /i!l
�
- D. L7i1it-
-2 ' to -1'
J? )
SVVW
10.73
8-4
7 g/
'6'
+1 ' to +2'
kJ
CWW-4
10.73
7 j
'/ y//
-2 ' to -1'
J%
SW-5
W
10.80
1 , .
� I Q
+1 . to +2'
{,
C1MV-5
10.74
729
-/, '7/
-2'to-1'
/
SVWV-6
10.66
6. /.2
. y,2.--
+1 ' to +2'
f'/9
CWW-0
9.92
-.
(..9
- -,;/2,,j /
-2'to-1'
/ lj'
W SW-7
10.70
73�
/.3.1.-
+1'to+2'
Te'.
CWW-7
9.95
7 5 (a
1, yy
-2 ' to -1'
��
Revised 8/12/97
• Riser length added to TOC elevation 1/24/97
PCS095.XLS

swW-1
cwW-1
co-1
cIw-1
CUT—OFF WALL
1 SWW-5
CPZ-2-
ASPHALT ROAD cww-s
S.P.A
PLANT
CIW-2
0
0
L,
J
SWW-4 CWW-4
CWW-3
SWW-3
`-WITHDRAWAL WELL
FLOW TOTALIZERS
AND CONTROL VALVES
005
O CPZ-3
Y--SPZ-9
PIPERACK SPILL CONTAINMENT PAD
00
r"1
r
.J
S.P.A
PLANT
L
1
WATER LEVEL
CONTROL TANK
MWTF-3
CLUSTER
SPZ-6
019) (0 21
/_SPZ-8
SWW-7 CWW-7
002
004
®'SPZ-1D
CRY-4
MWTF-1
CLUSTER
00

,,PCS Phosphate Co., Inc. - Tank Farm Remediation System Monitoring File: 15-03-003-02
Date: 9////9
pc: TLB
Time: ,-//r L ih /'-
Tech: /urGy/ee- -"
System Gauge Pressures
SWW-1
- �5---/Jvi
SWW-7
_7)-�/,5;0.'1
n._ //4j,'
CWW-1
CWW-7
/2- /%,aS,,
Level (msl
Ditch Level
�rl'e .
Barge Slip
9 3f'
Water Level
y,-,
Control Tank
% u MSL
iy3_5'
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level '
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level '
Level
Relative To
MSL Ft.
Spz-1
10.47
Y 0-5-6.
Z
Cpz-1
10.51
/0
. ? y/
Spz-2
11.21
7 �..�
3. 0
Cpz-2
10.25
�%y
/. /.=
/.,Z
Spz-3
11.87
f'�
G. /
Cpz-3
11.12
766
✓� '/6
Spz-4
11.45
G ..3y
Jam. //
CPW
9.65
J
/ //
Spz-5
11.45
g B.
a? ',5
MWTF-1A •
14.35
.3. 5.5/
/4 &
Spz-6
11.23 '
P, 77
•.4/&,
MWTF-1 B •
14.36
4 9f
9 9/3
Spz-7
11.59
/9.an
/J--9
MWTF-1C•
14.44
49/ijr96/Z2//
ij� 4/4
7 %1/
Spz-8
11.57
.5
99
MWTF-2A
14.05
Spz-9
11.01
7. 9-5/
. '7MWTF-2B
14.02
/_5,-.�. 77
. , ,
Spz-10
12.16
•2/ 7�0
'�/
/. y 'Y 6
MWTF-2C
14.08
/.. . ,3.?
C , %r!L'
SPW
9.95
7,:Fc''
,% 5-7
MWTF-3A
12.21
3/?6
c ), 3_
MWTF-3B
12.18
9 Se'
.9
MWTF-3C
12.19
// 9.2
,0, 7
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o
Comments //
(,% t%:i!//C!/ye- "/;.r`)
a 6/9,.// /4//-/ .
SWW-1
10.70
6. 5
a loS'
+1 ' to +2'
VP_':,
CWW-1
10.60
% 3
3 /
2 ' to -1'
f P�
C7..3 9n//'./e c/'
SWW-2
9.99
6, 7C'
Q %o
+1 ' to +2'
f'FS
0 �9 y4 ///'/�G
CWW-2
10.23
6. 99
< /
-2 ' to -1'
l P�
e �Y79X////`!/e�
Q-�e17q/,� C///e
l% 7•54, /91f/C
SVWV-3
9.97
O, ,. 7
,:, 3%
+1'to+2'
ycr',
VW CV-3
9.95
L. /�
�. / 7
-2 ' t0 -1'
i
SWW-4
10.73
757
/ 57
+1 'to +2'
TL'i
g. /lD Q/.:/l%j/r'�.
(% 1 6/C,//�
CW Wra
10.73
Dn
�.�. 00
-2 ' to -1'
%fi
SW W-5
10.80
6. G� 5+
r �
+1. to +2'
f �S
7,
• .5: • C�l l�f=
CWW-5
10.74
"% 1i•?
.- / ,3-7
-2 ' to -1'
/FJ
,/94�
>� .5-6 Q�C //C
,
SWW-6
10.66
7 1
/ - //2
+1 'to +2'
yt-
�, 999 t/6-
CW W-6
9.92
7 „..?n
-/ 8
-2 ' to -1'
'
/1)
0-y� 9//G�d
%_
C
CJ.-Sr0GY//`��e
0.37 4v/ /0`C/e.
SWW-7
10.70
7/W !i'
//&
+1'to+2'
TCJ
CWW-7
9.95
7 n 9
~/ 9/
-2 ' to -1'
Tf'_
Revised 8/12/97
• Riser length added to TOC elevation 1/24/97
PCS095.XLS

swW-1
CWw-1
co-1
cIw-1
CUT-OFF WALL
CPZ-2-• r ASPHALT ROAD
SWW-2
CWW-2
MWTF-2
CLUSTER
! DRAINAGE DITCH
S.P.A
PLANT
0
0
SWW-4
CWW-3
— SW W-3
SWW-5
CW W-s
WITHDRAWAL WELL
FLOW TOTALIZERS
AND CONTROL VALVES
PIPERACK SPILL CONTAINMENT PAD
0
007 EE-0-1-1)1 009
�1
S.P.A
PLANT
WATER LEVEL
CONTROL TANK
°lc=
MWTF-1
CLUSTER
00
CO-3
MWTF-3
CLUSTER
S�PZ-8
LSPZ-8
SWW-7 CWW-7
I`1w-7
0—
ive
•
SPZ-1100
I • 4
N
002
l
Feer ,n.'1+r.

0.w V
Date:
Time:
Tech:
WY . ..VipL.at VV.. ...V. -
AV/9/9B
Ain
��LeeZIL
. a...• . vas so ••v...ins.0..v....rva.....tents moan ...0
System Gauge Pressures
SW W-1
0- 3O`tt/
SWW-7
O-/#,ts/
O-a.?,a
cwW-i
CWW-7
I,- /p?100 i
pe: TLB
Level (mal)
Ditch Level
53a
Bergo Slip
. . 98
Water Level
95�
Control Tank
%. = MSL
/B3
y
'
Sand Layer Pelzometers Level Indicators
WeI ID
TOC
Elevation
MSL'
TOC
Ste Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSl'
TOC
Ste WV
Level'
Level
Relative To
MSL FL
Spz-1
10.47
4489
563
Cpz-1
10.51
%n4Jr
7. -..21n
Spz-2
11.21
9.0..5
/!n
A.
Cpz-2
10.25
7. a.
//.7
Spz-3
11.87
A 68
.J/ 9
Cpz-3
11.12
7 S!
. 0Z5"
Spz-4
11.45
a .90
-V-5-
.
CPW
9.65
g.840
0.79
Spz-5
11.45
6.0/
✓:441/
MWTF-1A •
14.35
1/ 0/
/z7 3l
Spz-6
11.23
B. 98
2..75-
MWTF-1B•
14.36
5:00
9,3G
Spz-7
11.59
/O. O"/
/ 5
MWTF-1C•
14.44
-
12enweeo
Spz$
11.57
th, lei
.J /0
MWTF-2A
14.05
l.70
755
Spz-9
11.01
Bap
..-8/
MWTF-26
. 14.02
//n(•4
2. 96
Spz-10
12.16
3,1
4..82.-
MWTF-2C
14.08
Xi..q
. /0
spw
_ 9.ss
758
i7
MWTF-3A
12.21
2/46
7 9..5"
MWTF-313
-Iva
/D.0.,2
2,./0
MWTF-3C
12.19
/�./0p
-a 03
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Ste
WV
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
('nes/(N)o
Comments
swW-1
10.70
6.NO
O.4/O
+1'to+2'
;
CWW-1
10.60
%
- /. Q10
-2'to-1'
e�,_:.)
SWW-2
9.99
a. 810
Q.86
+1' to +2'
YPS
CWW-2
10.23
70-7d
-/ 96
-2'to-1'
i/es
SIWV-3
9.97
B.3y
�.3i/
+1'to+2'
1.
C71W-3
9.95
79'/
-/0a
-2'to-1'
e
SWW-4
10.73
7/ /34'%
/./3
+1'to+2'
Y,/J
CWW-4
10.73
6 .
-0%SS
-2'to-1'
V "es
SWW-5
10.80
7.. /.3
/ /5
+1 . to+2'
Fief
CW W-5
10.74
6.97p
tt o..93
-2'to -1'
Y,Je6
SWV✓-5
10.66
%9%O
/ 4'
H' to +2'
Ply
y�
C1NW-8
9.92
OR
-/. 9..2
-2'to -1'
SWW-7
10.70
�77
/ 13
/ 1.5
+1'to+2'
i✓
CWW-7
9.95
7/'
- /'OW
-2'to-1'
vJ
Revised 8/12/97
• Riser length added to TOC &ovation 124/97
PCS095.XLS