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HomeMy WebLinkAboutWI0700012_4th Quater Monitoring (Report)_19960523Phosphate AURORA DIVISION P.O. BOX 48, AURORA, NC 27806 May 23,1996 Underground Injection Control Program Groundwater Section NC - DEHNR, Division of Environmental Management P. O. Box 29578 Raleigh, North Carolina 27626-0578 Attn: Mark Milligan Subject: Fourth Quarter Monitoring Data for Tank Farm Remedial Action System Dear Mark: Please find enclosed the Tank Farm Remedial Action System 4th quarter groundwater monitoring data for your information. The samples were collected during April 1996. The sampling and analysis of water from the injection well system as required by Permit No. W10700012 is also included. Additional Compliance Monitoring Report Forms for well CIW-7-and the WLCT are included in this report. Please contact me at (919) 322-8193 if you have any questions regarding this information. Sincerely, L. M. Montgmery Environmental Engineer Attachments pc: Willie Hardison - DEM, WaRO (w/attch) 12-01-005-06 (w/o attch) 00-19-000 (w/o attch) S. R. Phillips / 12-01-008-03-002 (w/ attch) Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: WI0700012 Non —Discharge Tank Farm Remedial System _Lagoon —_Septic Tank/Drain Field _Spray Field Subsurface Law —Pressure Well Location : Tank Farm Rotary Distributor x 01 Well I.D. Number: CWW— 1 Well Depth: 55.0 Ft. Well Diameter 4' Sample (Screened)Interval 33.27 Ft. to 52.68 Ft. Depth to Water Level 11.50 Ft. below meas. pt.(before sampling)or —0.90 Ft. (MSL) Measuring Point is 2.25 Ft. above land surface or 10.60 Ft. (MSL) Gallons of water purged before sampling CONTINUOUS Field Analysis: pH 6.4 Specific Conductance 2216 uMhosTemp 185 oC Odor NONE Date Sample Collected 04/17/96 Date Lab Sample Analyzed 4/17-4/29 1996 Appearance: CLEAR Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mgA NO2asN N/A mg/1 Ni — Nickel N/A mg/1 Coliform: MF Fecal N/A /100m1 NO3 as N N/A mgA Pb — Lead N/A mg, Coliform: MF Total N/A /100m1 Phosphorus: Total as P 0.538 mg/1 Zn — Zinc N/A mg/ Dissolved Solids: Total 2104 mg/I Al — Aluminum N/A mg/I Pesticides/Herbicides (Specify) r pH (when analyzed) 65 units Ba — Barium N/A mg/I ug/1 TOC 9.9 mgil Ca — Calcium N/A mg/I J ug/1 Chloride 92.7 mg/1 Cd — Cadmium N/A mgA ug/1 Arsenic N/A mg/I Chromium: Total N/A mgA Other FLUORIDE 0.26 mgi Grease and Oils N/A mgA Cu — Copper N/A mg l Other MIBK N/A ug/1 Hardness: Total N/A mg1 Fe — Iron N/A mg/I OtherAg — Silver N/A mg/I Phenol N/A mg/1 llg — Mercury N/A mg, Other Se — Selenium N/A mg.4... Sulfate 694.9 mg/1 K — Potassium N/A mgA ug/1 Specific Conductance N/A uMohs Mg — Magnesium N/A mgA ug/1 Total Ammon►a(NH4 + NH3) N/A mgA Mn — Manganese N/A mg/I TKN as N N/A mg/1 Na — Sodium N/A mgA I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERMITTLF)(OR AUTHORIZED AGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) 7/9i Date er ) 7 COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISIONI OF ENVIRONMENTAL. MANAGEMENT I',0 BOX 29. 35 RALEI GH, NC 27626-0535< (919) 733-3221 s Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMITNO.: WI0700012 Non —Discharge Tank Farm Remedial System _Lagoon _Septic Tank/Drain Field _Spray hield Subsurface Low —Pressure Well Location : Tank Farm Rotary Distributor _x_01 Well I.D. Number: CWW-2 Well Depth: 52.15 Ft. Well Diameter 4" Sample (Screened) Interval 30.57 Ft. to 49.82 Ft. Depth to Water Level N/A Ft. below meas. pt.(before sampling) or N/A Ft. (MSL) Measuring Point is 3.00 Ft. above land surface or 10.23 Ft. (MSL) Gallons of water pumped/bailed before sampling NOT PUMPING Field Analysis: pH N/A Specific Conductance N/A uMhos Temp N/A oC Odor Date Sample Collected 04/17/96 Date Lab Sample Analyzed 0 1996 Appearance: N/A Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 AND FIELD ACIDIFIED YES NO SAMPLES FOR METALS WERE COLLECTED UNFILTERED COD N/A mg/1 NO2 as N N/A mg/I Ni — Ns kel N/A mg/I Colifam: MF Fecal N/A /100m1 NO3 as N N/A mg/I Pb — Lead N/A mg/1 Colifam: MFTotal N/A /100m1 Phosphorus: Total as P N/A mg/1 Zn — Zinc N/A mg/I Dissolved Solids: Total N/A mg/1 Al — Aluminum N/A mg/I Pesticides/Herbicides (Specify) pH (when analyzed) N/A units Ba — Barium N/A mg/I ug/I TOC N/A mg/1 Ca — Catium N/A mg/I ug/1 Chloride N/A mg/1 Cd — Cadmium N/A mg/1 ug/I Arsenic N/A mg/1 Chromium: Total N/A mg/1 Other FLUORIDE N/A mg/1 Grease and Oih N/A mg/I Cu — Copper N/A mg/1 Other MIBK N/A ug/I Hardness: Total N/A mg/I Fe — Iron N/A mg/1 Other Ag — Silva N/A mg/I Phenol N/A mg/I fig — Mercury N/A mg/I Other Se — Selenium N/A mg/1 Sulfate N/A mg/I K — Potassium N/A mg/I ug/l Specific Conductance N/A uMhhs Mg — Magnesium N/A mg/1 ug/I Total Ammonia(NH4 + NH3) N/A mg/1 Mn — Manganese N/A mg/I TKN as N N/A mg/1 Na — Sodium N/A mg/1 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF P RMITTEISR AUTHORIZEDAGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) s-AgAt DATE r N/A Cn CD co '_r lQ I1'i -i COMPLIANCE MONITORING DIVISION OF•ENVIRONMENTAL MANAGEMENT GROUNDWATER QUALITY MONITORING: P.O.BOX 29535 COMPLIANCE REPORT FORM RALEIGH. NC 27626-0535 (919)'733-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PER MIT NO.: WI0700012 Non —Discharge Tank Farm Remedial System _Lagoon _Septic Tark/Drain Field Spray Held Subsurface Low—Nressure Land Appl of Sludge Well Location : Tank Farm Rotary Distributor _x_Ot Well I.D. Number: CWW-3 Well Depth: 53.00 Ft. Well Diameter 4" Sample (Screened) Interval 36.42 Ft. to 50.67 Ft. Depth to Water Level N/A Ft. below meas. pt.(be fore sampling) cx N/A Ft. (MSL) Measuring Point's 3.08 Ft. above land surface or 9.95 Ft. (MSL) Gallons of water pumped/bailed before sampling NOT PUMPING Field Analysis: pil N/A Specific: Conductance N/A uMhos Temp N/A oC: Odor Date Sample Collected 04/17/96 Date Lab Sample Analyzed N/A 1996 Appearance: N/A Laboratory Name : PCS PHIOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/1 NO2 as N N/A mg/I Ni — Nickel N/A mg/I Colderm: MF Fecal N/A /100m1 NO3 as N N/A mgl Pb — Lead N/A mg/I Colderm: MF Total N/A /100m1 Phosphorus: Total as P N/A mgl Zn — Zinc N/A mg/1 Dissolved Solids: Total N/A mg/I Al — Aluminum N/A mg/1 Pesticides/Herbicides (Specify) plI (when analyzed) N/A units Ila — Barium N/A mg1 ug/1 TOC NIA mg/1 Ca — C:al ium N/A mg1 ug/l Chloride N/A mg/1 Cd — Cadmium N/A mg/1 ug/I Arsenic N/A mg/1 Chromium: Total N/A ing/I Other FLUORIDE N/A mg/I Grease and Oik N/A mg/1 Cu — Copper N/A mg/1 Other MI N/A ugl Ilardness: Total N/A mg/1 Fe — Iron N/A mg/1 Other Ag — Silver N/A mg/I Phenol N/A mg/l Hg — Mercury NIA mg/1 Other Se — Selenium N/A mg/1 Sulfate N/A mg/1 K — Potassium N/A mg/1 ug/1 Specific Conductance N/A uMohs Mg — Magnesium N/A mgrl ugil Total Ammonia(NII4 + NH3) N/A mg/I Mn — Manganese N/A mg/1 TKN as N N/A mgI Na — Sodium N/A mg,/1 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) er N/A t.p C71 C!7 SIGNATURE OFE (OR AUTHORIZED AGENT) DA E COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 RALEIGII, NC27626-0535 (919) 733-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: WI0700012 Non —Discharge Tank Farm Remedial System _Lagoon _Septic Tark/Drain Field _Spray Field Subsurface Low —Pressure _Land Appl of Sludge Well Location : Tank Farm _Rotary Distributor _x_O1 We11I.D. Number: CWW-4 Well Depth: 53.00 Ft. Well Diameter 4" Sample (Screened) Interval 41.67 Ft. to 50.92 Ft. Depth to Water Level 11.64 Ft. below meas. pt.(before sampling) or —0.91 Ft. (MS .) Measuring Point's 2.75 Ft. above land surface or 10.73 Ft. (MSL) Gallons of water pumped/bailed before sampling CON1INUOUS Field Analysis: pH 6.1 Specific Conductance 2843 uMhos Temp 27.8 oC Odor NONE Date Sample Collected 04/17/96 Date Lab Sample Analyzed 4/17-429 1996 Appearatre: CLEAR Laboratory Name : PCS PHOSPHIA'IE ENV. AFFAIRS LAB Certifration No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/1 NO2 as N NIA mg/1 Ni — Nickel N/A mg(I Coiiform: MF Fecal N/A /100m1 NO3 as N N/A mg(I Pb — Lead N/A mg/1 Coliferm: MF Total N/A /100m1 Phosphorus: Total as P 5.500 ntgl Zn — Ziir N/A mg/1 Dissolved Solids: Total 2284 mg/1 Al — Aluminum N/A mg/1 Pesticides/Herbicides (Specify) pH (when analyzed) 6.3 units Ba — Barium N/A mgil ug/I TOC 9.4 mg/1 Ca — Cat;ium N/A mgil ug/I Chloride 118.5 mg/I Cd — Cadmium N/A mg/1 ug/I Arsenic N/A mg/1 Chromium: Total N/A mg,1 Other iLUORIDE 0.16 mg/I Grease and Oik N/A mg/I Cu — Copper N/A mg/1 Other MIBK N/A ug/l hardness: Total N/A mg/1 Fe — Iron N/A mg/1 Other Ag — Silver N/A mg,1 Phenol N/A mg/1 IIg — Mercury N/A mg/I Other Se — Selenium NIA mgrl Sulfate 714.7 mg/I K — Potassium N/A mg/I ug/I Specific Conductance NIA uMohs Mg — Magnesium N/A mg/1 ug/I Total Ammonia(NH4 + N113) N/A mg,/ Mn — Manganese N/A mg/I TKN as N N/A mgil Na — Sodium N/A mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERMITTEE ( AUTHORIZED AGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) ‘9, S9( DATE er r-r t� U 1 _. COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM otvistON OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 RALEIGH, NC 27626-0535 (919) 733-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: WI0700012 Non —Discharge Tank Farm Remedial System _Lagoon _Septic Tark/Drain Field Sprayhield Subsurface Low—Hressure _Land Appl of Sludge Well Location : Tank Farm Rotary Distributor _x_Otl Well I.D. Number: CWW-5 Well Depth: 53.17 Ft. Well Diameter 4" Sample (Screened) Interval 41.75 Ft. to 51.08 Ft. Depth to Water Level 12.00 Ft. below meas. pt.(before sampling) or —1.26 Ft. (MSL) Measuring Point's 2.58 Ft. above land surface or 10.74 Ft. (MSL) Gallons of water pumped/bailed before sampling CONIINUOUS Field Analysis: p1l 6.3 Specific Conductance 2917 uMhos Temp 31.4 oC Odor NONE Date Sample Collected 04/17/96 Date Lab Sample Analyzed 4/17-429 1996 Appearance: LTYLLW Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/I NO2 as N N/A mg/I Ni — Nickel N/A mg/1 Colifcrm: MF Fecal N/A /100m1 NO3 as N N/A mg/I Pb — Lead N/A mg/1 Colifcrm: MF Total N/A /100m1 Phosphorus: Total as P 9.900 mg/I Zn — Zinc N/A mg/I Dissolved Solids: Total 2156 mg/I Al — Aluminum N/A mg/1 Pesticides/Herbicides (Specify) 01 (when analyzed) 6.5 units Ba — Barium N/A mg/I ug/1 TOC 10.0 mg/1 Ca — Cabium N/A mg/I ug/1 Chloride 127.8 mg/1 Cd — Cadmium N/A mg/I ug/I Arsenic N/A mgrl Chromium: Total N/A mg/1 Other FLUORIDE 0.15 mgrl Crease and Ois N/A mg/I Cu — Copper N/A mg/1 Other MIBK N/A ug/I Hardness: Total N/A mg/I Fe — Iron N/A mg/1 Other Ag — Silver N/A mg/1 Phenol N/A mg/1 lig — Mercury N/A mgl Other Se — Selenium N/A mg/1 Sulfate 833.3 mg/1 K — Potassium N/A mg/1 ug/1 Specific Conductance N/A uMohs Mg — Magnesium N/A mg/l ugh Total Ammonia(N114 + NE13) N/A mg/1 Mn — Manganese N/A mg/I 'I KN as N N/A mg/1 Na — Sodium N/A mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERMITTEE(OR AUTHORIZED AGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) ,.cAcrg, D TE er COMPLIANCE MONITORING DIVISION OF ENVIRONMENTAL MANAGEMENT.. GROUNDWATER QUALITY MONITORING: P.o.BOX 29535 COMPLIANCE REPORT FORM RAL.EIGII.NC27626-0535 (919) 733-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: WI0700012 Non —Discharge I ank Farm Hemedial System _Lagoon _Septic Tank/Drain Field Spray Held Subsurface Low —Pressure _Land Appl of Sludge Well Location : Tank Farm Rotary Distributor x_Ot Well I.D. Number: CWW-6 Well Depth: 53.00 Ft. Well Diameter 4" Sample (Screened) Interval 36.62 Ft. to 50.88 Ft. Depth to Water Level N/A Ft. below meas. pt.(before sampling) or N/A Ft. (MSL) Measuring Point's 2.92 Ft. above land surface or 9.92 Ft. (MSL) Gallons of water pumped/bailed before sampling NOT PUMPING Field Analysis: pIl N/A Specific Conductance N/A uMhos Temp N/A oC Odor Date Sample Collected 04/17/96 Date Lab Sample Analyzed N/A 1996 Appearance: N/A Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND IIELDACIDIIIED YES NO COD N/A mg/1 NO2 as N N/A mg!l Ni — Nckel N/A mg/I Colitant: MF Focal N/A /100m1 NO3 as N N/A mg/I Pb — Lead N/A mg/I Colifcrm: MI? Total N/A /100m1 Phosphorus: Total as P N/A mg/I Zn — Zinc N/A mg/1 Dissolved Solids: Total N/A mg/I Al — Aluminum N/A mg/I Pesticides/Herbicides (Specify) pH (when analyzed) N/A units Ba — Barium N/A mg/1 ug/1 'I'OC NIA mg/I Ca — Cabium N/A mg/1 ug/I Chloride N/A mg/1 Cd — Cadmium N/A mg/I ug/l Arsenic N/A mg/I Chromium: Total N/A mgil Other FLUORIDE N/A mg/I Grease and Oils N/A mg/I Cu — Copper N/A mg/I Other MIBK N/A ug/I Hardness: Total N/A mg/I Fe — Iron N/A mg/1 Other Ag — Silver N/A mg/1 Phenol N/A mgl lig — Mercury N/A mg!l Other Se — Selenium N/A mg/I Sulfate N/A mg/I K — Potassium N/A mg/I ug/I Specific Conductance N/A uMohs Mg — Magnesium N/A mgfl ug/1 Total Ammonia(N114 + NH3) N/A mg/1 Mn — Manganese N/A mg9 'I'KN as N N/A mg/I Na — Sodium N/A mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERMITTEEOR AUTHORIZED AGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) DATE N/A COMPLIANCEMONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 RALEIGH. NC 27626-0535 (9.19) 733-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMITNO.: WI0700012 Non -Discharge Iark Farm Hemedial System _Lagoon _Septic Twi</Drain Field Spray Field Subsurface Low -Pressure _Land Appl of Sludge Well Location : Tank Farm Rotary Distributor _x_Ot Well I.D. Number: CWW-7 Well Depth: 53.00 Ft. Well Diamd er 4" Sample (Screened) Interval 36.58 Ft. to 50.83 Ft. Depth to Water Level 8.48 Ft. below meas. pt.(before sampling) a 1.47 Ft. (MSL) Measuring Point is 1.25 Ft. above land surface or 9.95 Ft. (MST.) Gallons of water pumped/bailed before sampling CONTINUOUS Field Analysis: pH 6.8 Specific Conductance 1033 uMhos Temp 21.2 oC Odor NONE Date Sample Collected 04/17/96 Date Lab Sample Analyzed 4/17-4/29 1996 Appearance: CLEAR Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/I NO2 as N N/A mg/I Ni - Nickel N/A mg/1 Colifcrm: MF Fecal N/A /100m1 NO3 as N N/A mg/1 Pb - Lead N/A mg/1 Colitorm: MI' Total N/A /100ml Phosphorus: Total as P 1.580 mg/1 Zn - "Line N/A mg/1 Dissolved Solids: Total 860 mg/l Al - Aluminum N/A mg/1 Pesticides/Herbicides (Specify) p1I (when analyzed) 6.9 units Ba - Barium N/A mgl ugl 1 OC 7.65 mg/1 Ca - Cabium N/A mg1 ug/1 Chloride 67.9 mg,/1 Cd - Cadmium N/A mg/I ug/1 Arsenic N/A mg/I Chromium: Total N/A mg/1 Other FLUORIDE 0.29 mg/I Grease and Oi N/A mg/1 Cu - Copper N/A mg/1 Othex MIBK N/A ug/I Hardness: Total N/A mg/I Fe - Iron N/A mg/I Other Ag - Silver N/A mg/1 Phenol N/A mg/1 lig - Mercury N/A mg/1 Other Se - Selenium N/A mg,/1 Sulfate 158.7 mgil K - Potassium N/A mg/1 ug/1 Specific Conductance N/A uMohs Mg - Magnesium N/A mg/I ug/1 Total Ammonia(NH4 + N113) N/A mg/1 Mn - Manganese N/A mg/1 TKN as N N/A mg/1 Na - Sodium N/A mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PEMITTEE-(OR AUTHORIZED AGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) 51ar1ciG ATE er COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 R ALEI GH. NC 27626-0535 (919) 733-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT PER MIT NO.: WI0700012 Non -Discharge Tank Farm Remedial System Lagoon _Septic Tank/Drain Field Spray -ield Subsurface Low -Pressure Land Appl of Sludge Address P.O. BOX 48 AURORA, NC 27806 Well Location : Tank Farm Rotary Distributor _x_Ot Well I.D. Number: SWW-1 Well Depth: 22.5 Ft. Well Diameter 4" Sample (Screened) Interval 18.29 Ft. to 21.12 Ft. Depth to Water Level 7.64 Ft. below meas. pt.(beforesampling) er 3.06 Ft. (MSL) Measuring Points 1.42 Ft. above land surface or 10.70 Ft. (MSL) Gallons of water pumped/bailed before sampling CONIINUOUS Field Analysis: pH 6.3 Specific Conductance 2052 uMhos Temp 17.2 oC Odor NONE Date Sample Collected 04/17/96 Date Lab Sample Analyzed 4/17-4/29 1996 Appeararre: CLEAR Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/1 NO2 as N N/A mg/1 Ni - Nickel N/A mg/1 Coliform: MF Fecal N/A /100m1 NO3 as N N/A mg/1 Pb - Lead N/A mg/l Coliform: MF Total N/A /100m1 Phosphorus: Total as P 158.000 mg/I Zn - Zit N/A mg/I Dissolved Solids: Total 1772 mg/1 Al - Aluminum N/A mg/I Pesticides/Herbicides (Specify) plI (when analyzed) 6.4 units Ba - Barium N/A mg/1 ug/1 TOC 11.2 mgl Ca - Ca1 ium N/A mg/I ug/1 Chloride 88.5 mg/1 Cd - Cadmium N/A mg/1 ug/I Arsenic N/A mg/1 Chromium: Total N/A mg/1 Other FLUORIDE 0.51 mg/I Grease and Oik N/A mg/I Cu - Copper N/A mg/I Othc' MIBK N/A ug/1 Hardness: 'Total N/A mg/1 Fe - Iron N/A mg/I Other Ag - Silver N/A mg/1 Phenol N/A mg/1 Ilg - Mercury NIA nig/I Other Se - Selenium N/A mg/1 Sulfate 531.7 mg/1 K - Potassium N/A mg1 ug/I Specify Conductance N/A uMoos Mg - Magnesium N/A mg/I ugil Total Ammonia(N114 + NH3) N/A mg/1 Mn - Manganese N/A mg/I TKN as N N/A mg/I Na - Sodium N/A m49 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) er t.0 OZ SIGNATUR OF PERMITTE(OR AUTHORIZED AGENT) DAT COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE. REPORT FORM DIVISION, OF ENVIRONMENTAL MANAGEMENI ,. P.O. BOX 29535 R ALEI GH, NC 27626-0535 (919) 733-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O, BOX 48 AURORA, NC 27806 PER MIT NO.: WI0700012 Non —Discharge I ark I -arm Hemedial System _Lagoon _Septic Tar*/Drain Field Spray Field Subsurface Law —Pressure _Land Appl of Sludge Well Location : Tank Farm Rotary Distributor _x_Ot Well I.D. Number: SWW-2 Well Depth: 23 Ft. Well Diameter 4" Sample (Screened) Interval 18.80 Ft. to 21.63 Ft. Depth to Water Level N/A Ft. below meas. pt.(beforesampling) or N/A Ft. (MSL) Measuring Point is 3.42 Ft. above land surface or 9.99 Ft. (MSL) Gallons of water pumped/bailed before sampling NOT PUMPING Field Analysis: pH N/A Specific Conductance N/A uMhos Temp N/A oC Odor Date Sample Collected 04/17,96 Date Lab Sample Analyzed N/A 1996 Appearance: N/A Laboratory Name : PCS PIIOSPIiA1E ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECIED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/1 NO2 as N N/A mgll Ni — Nickel N/A mg/1 Colifcrm: MF Fecal N/A /100m1 NO3 as N N/A mg/I Pb — Lead N/A mg/1 Coliform: MFTotal N/A /100m1 Phosphorus: Total as P N/A mg'1 Zn — Zinc N/A mg/1 Dissolved Solids: Total N/A mg/I Al — Aluminum N/A mg/1 Pesticides/lierbicides (Specify) pl1 (when analyzed) N/A units Ba — Barium N/A mg/I ug/l TOC N/A mg/I Ca — Calcium N/A mg/l ug/l Chloride N/A mg/I Cd — Cadmium N/A mg/1 ug/1 Arsenic N/A mg/1 Chromium: Total N/A mgl Other FLUORIDE NIA mg,/1 Grease and Oik N/A mg/1 Cu — Copper N/A mg/1 Other MIBK N/A ug/I Hardness: Total N/A mg/I Fe — Iron N/A mg/1 Other Ag — Silver N/A mg/I Phenol N/A mg'l Fig — Mercury N/A mg/I Other Se — Selenium N/A mg/1 Sulfate N/A mg/I K — Potassium N/A mg/I ug/1 Specific Conductance N/A uMohs Mg — Magnesium N/A mg/1 ug/1 Total Ammonia(N114 + N113) N/A mg/I Mn — Manganese N/A mg/1 Note: Values should reflect total concentrations TKN as N N/A mg/I Na — Sodium N/A mg/1 Note: I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE 0 PERMITTED (OR AUTHORIZED AGENT) Values should reflect dissolved and colloidal concentrations. (see #3 on back) _ciarAt, DATE er N/A t.ra cr C.11 C:) CD r\,) • COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 RALEIGH. NC 27626-0535 (919) 733-3221 PERMITNO.: WI0700012 Non —Discharge I arlc Farm Hemedial System _Lagoon _Septic Tank/Drain Field Spray F laid Subsurtace Law —Pressure _Land Appl of Sludge Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 Well Location : Tank Farm Rotary Distributor _x_Ot Well I.D. Number: SWW-3 Well Depth: 24.5 Ft. Well Diameter 4" Sample (Screened) Interval 20.17 Ft. to 23.0 R. Depth to Water Level 6.18 Ft. below meas. pt.(beforesampling) or 3.79 Ft. (MSL) Measuring Point is 3.17 Ft. above land surface or 9.97 Ft. (MSL) Gallons of water pumped/bailed before sampling CONTINUOUS Field Analysis: pH 6.2 Specific Conductance 1353 uMhos Temp 19.9 oC Odor NONE Date Sample Collected 04/17/96 Date Lab Sample Analyzed 4/17--429 1996 Appearartre: CI FAR Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/I NO2 as N N/A mgil Ni — Nickel N/A mg/I Coliform: MF Fecal N/A /100m1 NO3 as N N/A mg/1 Pb — Lead N/A mg/I Co]iform: MF Total N/A /100m1 Phosphorus: Total as P 51.000 nig/1 Zn — Zinc N/A mg/1 Dissolved Solids: Total 1208 mg/1 Al — Aluminum N/A mg/1 Pesticides/Herbicides (Specify) pH (when analyzed) 6.4 units Ba — Barium N/A mg/1 ug/1 "IOC 9.1 mg1 Ca — Caesium N/A mgfl ug/l Chloride 45.1 mg/I Cd — Cadmium N/A mg/I ug/I Arsenic NIA mgl Chromium: Total N/A mg/I Other FLUORIDE 0.09 mg/1 Grease and Oi6 N/A mg/I Cu — Copper N/A mg/I Other MIRK N/A ug/1 EEardness: Total N/A mg/I Fe — Iron N/A mg/1 Other Ag — Silver N/A mgil Phenol N/A mg/1 Hg — Mercury N/A mgil Other Se — Selenium N/A mgfl Sulfate 390.5 mg/1 K — Potassium N/A mg/1 ug/1 Specific Conductance N/A uMoos Mg — Magnesium N/A mg/1 ug1 Total Ammonia(NII4 + NH3) N/A mg/1 Mn — Manganese N/A mg/1 TKN as N N/A mg/1 Na — Sodium N/A mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PER TEE (OR AUTHORIZED AGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) DA E er cD CD INJ COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 R ALEI GH. NC 27626-0535 (919) 733-322i. Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMITNO.: WI0700012 Nov —Discharge Tack FeralR emedial System Lagoon Sep& Tank!Dra In Field _Spray Field _Subsurface Low—Prexure Land Appl of Sludge Well Location : Tank Farm _Rotary Distributor _x_Other Well I.D. Number: SWW-4 Well Depth: 25 Ft. Well Diameter 4' Sample (Screened) Interval 20.50 Ft. to 23.3 R. Depth to Water Level 8.80 Ft. below meas. pt.(before sampling) a- 1.93 Ft. (MSL) Measuring Point is 3.42 Ft. above land surface or 10.73 Ft. (MSL) Gallons of water pumped/bailed before sampling CONTINUOUS Field Analysis: pil 5.9 Specific Conductance 1971 uMhos Temp 32.1 oC Odor NONE Date Sample Collected 04/17/96 Dare Lab Sample Analyzed 4/17-4/29 1996 Appcararce: LTYLLWCLDY Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COI 1 FCIED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A me NO2 is N N/A mg/I Ni — Nickel N/A mg/1 Colifcrm: MF Fecal N/A /100m1 NO3 as N N/A mg/I Pb — Lead N/A mg/1 Coli[am: MFTotal N/A /100ml Phosphorus: 'rotal as P 128.000 mg/1 Zn — Zinc N/A mg/1 Dissolved Solids: Total 1524 mg/I Al — Aluminum N/A mg/I Pesticides/Herbicides (Specify) p11 (when analyzed) 6.1 units Ba — Barium NIA rng/1 ug/I TOC 8.4 mgfl Ca — Calcium N/A nig/1 ug/I Chloride 59.7 mgA Cd — Cadmium N/A mg/1 ug/I Arsenic N/A mg/1 Chromium: Total N/A mg/I Other FLUORIDE 0.08 mg/1 Grease and Oils N/A mg/I Cu — Copper N/A mg/1 Other MIBK N/A ugll Ilardness: Total N/A mg/I Fe — Iron N/A mg/1 Other Ag — Silver N/A mg/I Phenol N/A mg/I Hg —. Mercury N/A mg/1 Other Se — Selenium N/A mg/I. Sulfate 507.6 mgl K — Potassium N/A mg/1 ugil Specific Conductance N/A uMhhs Mg — Magnesium N/A mg/1 ugjl Total Ammonia(N114 + NH3) N/A mg/I Mn — Manganese N/A mg/1 Note: Values should reflect total concentratiors TKN as N N/A mg/I Na — Sodium N/A mg1 Note: I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERM! TEE (OR AUTHORIZED AGENT) Values should reflect dissolved and colloidal concentrations. (see #3 on back) rL DA E COMPLIANCE MONITORING GROUNDWATER QUALITY MO COMPLIANCE REPORT FORM NITORING: DIVISION OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 RALEIGII: NC 27626-0535 (919) 733-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMITNO.: W10700012 Non —Discharge Tank Farm Remedial System Lagoon _Septic Tark/Drain Field Spray Held Subsurface Low —Pressure _Land Appl of Sludge Well Location : 'Tank Farm Rotary Distributor _x_Otl Well I.U.Number: SWW-5 Well Depth: 28.21 Well Diameter 4" Sample (Screened) Interval 24.83 Ft. to 27.2 R. Depth to Water Level N/A Ft. below meas. pt.(before sampling) or N/A Ft. (MSL) Measuring Point's 2.96 Ft. above land surface or 10.80 Ft. (MSL) Gallons of water pumped/bailed before sampling NOT PUMPING Field Analysis: pII N/A Specific Conductance N/A uMhos Temp N/A oC Odor Date Sample Collated 04/17/96 Date Lab Sample Analyzed N/A 1996 Appearance: N/A Laboratory Name : PCS PIHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg1 NO2 as N NIA nig/1 Ni — Nickel N/A mg/1 Coliform: MF Fecal N/A /100m1 NO3 as N N/A mg/1 Pb — Lead N/A mg/I Coiiform: ME' Total N/A /100m1 Phosphorus: Total as P N/A mg/1 Zn — Zinc N/A mg/1 Dissolved Solids: Total N/A mg/1 Al — Aluminum N/A mg/1 Pesticides/I1erbiides (Specify) (when analyzed) N/A units Ba — Barium N/A mg!l ug/1 pH TOC N/A mg/1 Ca — Calcium N/A mg/I ug/1 Chloride N/A mg/I Cd — Cadmium N/A mg/1 ug/I Arsenic NIA mg/I Chromium: Total NIA mg1 Other FLUORIDE N/A mg/l Grease and Oils N/A mgJl Cu — Copper N/A mg/1 Other MIBK N/A ugh Hardness: Total N/A mg/1 Fe — Iron N/A mgi1 Other Ag — Silver N/A mg/1 Phenol N/A mg(l lig — Mercury N/A mg/1 Other Se — Selenium N/A mg/1 Sulfate N/A mg/1 K. — Potassium N/A mg/I ug/1 Specific Conductance N/A uMohs Mg — Magnesium NIA mg/I ug/1 TotalAmmonia(N114 + N113) N/A mg/I Mn — Manganese NIA mg/l TKN as N N/A mg/I Na — Sodium N/A mg/1 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERMITTEE ( AUTHORIZED AGENT) er Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) •-c-2.94 c DATE N/A COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OFENVIRONMENTAL MANAGEMENT P.O. BOX 29535 RALEIGH, NC 27626-0535 (919) 733 —3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMITNO.: WI07W012 Non —Discharge Tank Farm Remedlal System _Lagoon _Septic Tank'Drato Field _Spray Pleld _Subsurface Low —Prelate _Land Appl of Sludge Well Location : Tank Farm _Rotary Distributor x_Otber Well I.D. Number: SWW-6 Well Depth: 26 Ft. Well Diameter 4" Sample (Screened) Interval 22.25 Ft. to 24.62 Ft. Depth to Water Level 8.48 Ft. below meas. pt.(beforesampling) a 2.18 Ft. (MSL) Measuring Point is 2.58 Ft. above land surface or 10.66 Ft. (MSL) Gallons of water pumped/bailed before sampling CONTINUOUS Field Analysis: pH 6.1 Specific Conductance 1480 uMhos Temp 24.5 oC Odor NONE Date Sample Collected 04/17/96 Date Lab Sample Analyzed 4/17-4,29 1996 Appearance: LT YLLW CLDY Laboratory Name : PCS PHOSPIIATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A ntg/l NO2 as N NIA mg/I Ni — Nickel N/A mg/I Colifcrm: MF Fecal N/A /100m1 NO3 as N N/A mg/1 Pb — Lead N/A mg/1 Coliform: MF Total N/A /100m1 Phosphorus: Total as P 14.000 mgil Zn — Zinc N/A mg/1 Dissolved Solids: Total 1088 mg/1 Al — Aluminum NIA mg/I Pesticides/Herbicides (Specify) pH (when analyzed) 6.2 units Ba — Barium NIA mgil ug&l TOC 18.7 mgll Ca — Calcium - N/A mg l ugjl Chloride 140.3 mg/I Cd — Cadmium N/A mg/1 ug/1 Arsenic NIA mg/1 Chromium: Total N/A mg./1 Other FLUORIDE 0.12 mg/1 Grease and Oils N/A mg/1 Cu — Copper N/A mg/I Other MIBK N/A ug/1 Hardness: Total N/A mg/1 Fe — Iron N/A mg/1 Other Ag — Silver NIA mgil Phenol N/A mg/1 lig — Mercury N/A mgrl Other Se — Selenium N/A mgil Sulfate 309.6 nig/1 K — Potassium N/A nig/1 ug/1 Specific Conductance N/A uMohs Mg — Magnesium N/A nig/1 ug/1 Total Ammonia(NH4 + NH3) N/A mg/I Mn — Manganese N/A mg/1 Note: Values should reflect total concentrations TKN as N N/A mg/1 Na — Sodium N/A tng/l Note: I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE 0 PEII ITTEE(R AUTHORIZED AGENT) alues should retlect dissolved an colloidal concentrations. (see #3 on back) .17 DATE LO • 01 COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING:' COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 RALEIGH, NC 27626-0535 (919) 733-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PER MIT NO.: WI0700012 Non—Disharge Tank Far mRmedia l System Lagoon Sepik Tank/Drain Field Spray Field Subsurface Low—Prezure _Land Appl of Sludge Well Location : Tank Farm _Rotary Distributor _x_Osher Well I.D. Number: SWW-7 Well Depth: 29.5 Ft. Well Diameter 4" Sample (Screened) Interval 25.17 Ft. to 27.50 Ft. Depth to Water Level 10.28 Ft. below meas. pt.(before sampling) cr 0.42 Ft. (MSL) Measuring Point's 3.00 Ft. above land surface or 10.70 Ft. (MSL) Gallons of water pumped/bailed before sampling CONTINUOUS Field Analysis: pli 6.2 Specific Conductance 1550 uMhos Temp 25.4 oC Odor NONE Date Sample Collected 04/17/96 Date Lab Sample Analyzed 4/17-429 1996 Appearance: LT ORNGCLDY Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECIEI) UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/1 NO2 as N N/A nig/1 Ni — Nickel NIA mg/1 Coliferm: MFFeca1 N/A /100m1 NO3 as N N/A mgI Pb — Lead N/A mgl Coliform: MFTotal N/A /100m1 Phosphorus: Total as P 27.500 mg/1 Zn — Zinc N/A mg/1 Dissolved Solids: Total 1176 mg/l Al — Aluminum N/A mg/1 Pesticidesflierbicides (Specify) p11 (when analyzed) 6.0 units Ba — Barium N/A mgl ug/1 'FOC 15.5 mg/I Ca — Caliuin NIA nig/1 ug/1 Chloride 131.1 nigh Cd — Cadmium NIA mg/l ugh Arsenic N/A ing/l Chromium: Total N/A nig/1 Other FLUORIDE 0.14 nig/1 Grease and Oils N/A mg/1 Cu — Copper N/A mg/1 Other MIRK N/A ug/1 Hardness: Total N/A mgl Fe — Iron N/A mg/1 Other Ag — Silver N/A mgjl Phenol N/A mg/1 Ilg — Mercury N/A mg/1 Other Se — Selenium N/A mg/1 Sulfate 299.3 mg,/1 K — Potassium N/A mg/1 ug/1 Specific Conductance N/A uMohs Mg — Magnesium N/A ingil ug1 Total Ammonia(NH4 + NH3) N/A mg/I Mn — Manganese N/A nig/1 Note: Values should reflect totalconcentrations TKN as N N/A mg/1 Na — Sodium N/A mg/1 Note: I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERMITTEE(!DR AUTHORIZED AGENT) alues should retlect afssolveo an colloidal concentrations. (see #3 on back) DATE I-) COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTAL MANAGEMENT P.O. E0X 29535 RALEIGH, NG27626-0535 (919) 793-3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: WI0700012 Non —Discharge Tank Farm Remedial System _Lagoon _Septic Tark/Drain Field Spray Hold Subsurface Low —Pressure _Land Appl of Sludge Well Location : Tank Farm _Rotary Distributor _x_Otl Well 1.D. Number: MWI-FI—A Well Depth: 6.4 Ft. Well Diameter 2" Sample (Screened) Interval 3.40 Ft. to 5.40 Ft Depth to Water Level 1.04 Ft. below meas. pt.(before sampling) or 9.45 Ft. (MSL) Measuring Point's 0.00 Ft. above land surface or 10.49 Ft. (MSL) Milliliters of water purged before sampling 2200 Field Analysis: pH 6.6 Specific Conductance 406 uMhos Temp 21.0 oC Odor NONE Date Sample Collerted 04/16i96 Date Lab Sample Analyzed 4/16-4/29 1996 Appearance: CLEAR Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED X YES NO COD N/A mg/l NO2 as N N/A mg/I Ni — Nickel N/A mg/1 Coliform: MI' Fecal N/A /100ml NO3 as N N/A mg/I Pb — Lead N/A mg/I Colifcrm: MFTotal N/A /100m1 Phosphorus: Total as P 0.275 mg!1 Zn — Zinc. N/A mg/I Dissolved Solids: "Total 280 mg/I Al — Aluminum N/A mg/I Pesticides/Herbicides (Specify) pH (when analyzed) 7.1 units Ba — Barium N/A mg/l ugh TOC 2.5 mg/I Ca — Calcium N/A mg/I ug/1 Chloride 2.6 mg/I Cd — Cadmium N/A nig/1 ug/1 Arsenic N/A mg1 Chromium: Total N/A mg/1 Other FLUORIDE 2.76 mgl Grease and Oils N/A mg/I Cu — Copper N/A ntg/1 Other MIRK N/A ug/1 Hardness: Total N/A mg/1 Fe — Iron N/A mg/ Other Ag — Silver N/A mg/1 Phenol N/A mg/I Hg — Mercury N/A mgll Other Se — Selenium N/A mg/I Sulfate <10 mg/1 K — Potassium N/A mg/1 ug/I Specific Conductance N/A uMohs Mg — Magnesium N/A mg/I ugil Total Ammonia(NI14 + N113) N/A mg/1 Mn — Manganese N/A mg/l TKN as N N/A mg/I Na — Sodium N/A mg/I Note: Micro —Purge System used for Sampling I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE 1' SIGNATURE OF PERMITTEE (OR'AIJTHORIZED AGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) C/r- DAT er t.fJ Cif T lid •;J UJJ 01 U7 CD cp 1 • •> COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTALMANAGEMENT P.O. BOX 29535 RALEIGIL NC 27626-0535 (919) 933 —3221 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMITNO.: WI0700012 Non —Discharge Tank Farm Remedial System _Lagoon Septic Tank/Drain Field Spray Fie Id Subsurface Low —Pressure _Land Appl of Sludge Well Location : Tank Farm Rotary Distributor _x_Ot1 Well I.D. Number: MWTF1—B Well Depth: 13.10 Ft. Well Diameter 2" Sample (Screened) Interval 10.60 Ft to 12.60 Ft Depth to Water Level 1.20 Ft. below meas. pt.(beforesampling) or 9.30 Ft. (MSL) Measuring Point is 0.00 Ft. above land surface or 10.50 Ft. (MSL.) Milliliters of water purged before sampling 2200 Field Analysis: pl1 5.6 Specific Conductance 840 uMhos Temp 23.0 oC Odor NONE Date Sample Collected 04/16/96 Date Lab Sample Analyzed 4/16-4(29 1996 Appearance: LT CLDY WHT Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLEC:1ED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/1 NO2 as N N!A mg/1 Ni — Nickel N/A mg/I Coliform: MF Fecal N/A /100m1 NO3 as N N/A mg/1 Pb — Lead N!A mg./1 Colifcrm: MFTotal N/A /I00m1 Phosphorus: Total as P 55.000 mg/I Zn — Zinc N/A mg,/1 Dissolved Solids: Total 656 mg/1 Al — Aluminum N/A mg/I Pesticides/flerbicides (Specify) p11 (when analyzed) 5.8 units Ba — Barium N/A mg/1 ug/1 TOC 6.7 mg/I Ca — CaFium N/A mg7 ug,7 Chloride 110.9 mg/1 Cd — Cadmium N/A mg/I ug/1 Arsenic N/A mg/1 Chromium: Total N/A mg/I Other FLUORIDE 0.34 mg/1 Grease and Oik N/A mg/1 Cu — Copper N/A mg/I Other MIBK N/A ug/1 Ilardness: Total N/A mg/1 Fe — Iron N/A mg/1 Other Ag — Silver N/A mg/l Phenol N/A mg9 Ilg — Mercury N/A ntg l Other Se — Selenium NIA mg/I Sulfate 104.9 mg/1 K — Potassium N/A mgrl ug/1 Specific Conductance N/A uMohs Mg — Magnesium N/A mg/I ug/1 Total Ammonia(N114 + N113) N/A mg/l Mn — Manganese N/A mg/1 TKN as N NIA mg/1 Na — Sodium N/A mg/I Note: Micro —Purge System used for Sampling I CERTIFY THAT THIS REPO 1S IS TRUE AND ACCURATE SIGNATURE OF PERMITTEE(ORTHORIZEDAGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) er ko U\ rV '0 --4 COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 RALEIGH. NC 27626-0535 (919) 733-3221, Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: WI0700012 Non —Discharge I antic farm Hemedial System _Lagoon _Septic Tarit/Drain Field Spray Held Subsurface Low —Pressure _Land Appl of Sludge Well Location : Tank Farm Rotary Distributor _x_Ott Well L.D. Number: MWTF1—C Well Depth: 41.20 Ft. Well Diameter 2" Sample (Screened) Interval 38.70 Ft. to 40.70 Ft. Depth to Water Level 5.34 Ft. below meas. pt.(beforesampling) or 5.15 Ft. (MSL) Measuring Point is 0.00 Ft. above land surface or 10.49 Ft. (MSL) Milliliters of water purged before sampling 2500 Field Analysis: pH 7.0 Specify; Conductance 528 uMhos Temp 23.0 oC Odor NONE Dal eSample Collected 04/16,96 Dale Lab Sample Analyzed 4/16-4,29 1996 Appearance: LTRSTORNG Laboratory Name : PCS PIiOSPIINIE ENV. AFFAIRS LAB Certification No. 330 (Tg Env Lab). and 102 (Metals and Colifcrm) SAMPLES FOR METALS WERE COLLECIED UNFILTERED AND FIELD ACIDIFIED X YES NO COD N/A mg/1 NO2 as N N/A mgil Ni — Nckel N/A mg!1 Colifam: MF Fecal N/A /100m1 NO3 as N N/A mg/I Pb — Lead N/A mg/1 Colifam: MI' Total <1 /100m1 Phosphorus: Total as P 0.140 mg/I Zn — Zirr N/A mg/1 Dissolved Solids: Total 364 mg/I Al — Aluminum N/A mg/I Pesticides/Ilerbicides (Specify) plI (when analyzed) 6.8 units Ba — Barium NIA mg1 uWI TOC 3.5 mg/1 Ca — Cakium N/A mg/1 ug/l Chiaide 41.3 mg/1 Cd — Cadmium <1.0 ppb ug/1 Arsenic N/A mg/1 Chromium: Total <1.0 ppb Other FLUORIDE 0.52 mg/l Grease and Oils N/A mg/1 Cu — Copper N/A mg/I Other MIBK N/A ug/1 hardness: Total N/A mg/1 Fe — Iron N/A mg/I Other Ag — Silver N/A mg/1 Phenol N/A mg/I Iig — Mercury N/A mg/I Other Se — Selenium N/A mg/1 Sulfate <10 mg/I K — Potassium N/A mg/I ug/I Specific Conductance N/A uMoiu Mg — Magnesium N/A mg/I ug/l Total Ammonia(Nh4 + NH3) N/A mg/I Mn — Manganese <0.01 ppm TKN as N N/A mg/1 Na — Sodium N/A mg/I Note: Micro —Purge System used for Sampling I CERTIFY THAT THIS RORT IS TRUE AND ACCURATE SIGNATURE OF PRMITTEE ( AUTHORIZED AGENT) er Note: Values should reflect dissolved and `I colloidal concentrations. (see #3 on back) COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING COMPLIANCE REPORT FORM DIVYS[ONOF ENVIRONMENTAL MANAGEMENT P.O. Box 29.535 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: WI0700012 Non —Discharge I ark Farm Hemedial System _Lagoon _Septic Tark/Draln Field _Spray Field _Subsurface Low —Pressure _Land Appl of Sludge Well Location : Tank Farm Rotary Distributor _x_Ott Well I.D. Number: WLCT Well Depth: n/a Well Diameter n/a Sample (Screened) Interval n/a Ft. to n/a R. Depth to Water Level n/a Ft. below meas. pt.(before sampling) or n/a Ft. (MSL) Measuring Point is n/a Ft. above land surface or n/a Ft. (MSL) Gallons of water pumped/bailed before sampling CONTINUOUS Field Analysis: pH 7.0 Specific Conductance 119 uMhos Temp 78.0 oC Odor NONE Date Sample Collected 04/16/96 Date Lab Sample Analyzed 4/16-4/29 1996 Appearance: CLEAR Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 (Tg Env. Lab) and 78( Coliform Only) SAMPLES FOR METALS WERE AND FIELD ACIDIFIED X YES NO COLLECTED UNFILTERED COD N/A mg/I NO2 as N N/A mg/I Ni — Nickel N/A mgfl Coliform: MF Fecal N/A /100m1 NO3 as N N/A mg/I Pb — Lead N/A mg/I Conform: MFTotal <1 /100m1 Phosphorus: Total as P 0.121 mg/1 Zn — Zinc N/A mg/I Dissolved Solids: Total 96 mg/I Al — Aluminum N/A mg/1 Pesticides/Herbicides (Specify) pH (when analyzed) 7.5 units Ba — Barium N/A mg/1 ug/1 TOC 4.5 mg/1 Ca — Calcium N/A mg/1 ug/1 Chloride 1.8 mg/I Cd — Cadmium 0.51 ppb ug/I Arsenic N/A mg/I Chromium: Total , 27.66 ppb Other FLUORIDE 0.03 mg/1 Grease and Oifi N/A mg/1 Cu — Copper N/A mg/I Other MIBK N/A ug/I Hardness: Total N/A mg/1 Fe — Iron N/A mg/1 Other Ag — Silver N/A mgfl Phenol N/A mg/1 llg — Mercury N/A mg/1 Other Se — Selenium N/A mg/I Sulfate <10 mg/1 K — Potassium N/A mg/1 ug/I Specific Conductance N/A uMohs Mg — Magnesium N/A mg/I ug/I Total Ammonia(NH4 + NH3) N/A mg/1 Mn — Manganese <0.01 ppm TKN as N N/A mg/1 Na — Sodium N/A mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) SIGNATURE OF PE'MITTER AUTHORIZED AGENT) -43()9.6. DATE r I. 1 COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION OF ENVIRONMENTAL MANAGEMENT: P.O. BOX 29535 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMITNO.: WI0700012 Non —Discharge Iark Farm Hemedial System _Lagoon _Septic Twit/Drain Field _Spray Held Subsurtace Low —Pressure Land Appl of Sludge Well Location : Tank Farm I Rotary Distributor x Otl Well I.D. Number: CIW-7 Well Depth: 48.00 Well Depth: JI Well Diameter 4" Sample (Screened)Interval 31.00 Ft. to 45.25 Ft. Depth to Water Level n/a Ft. below meas. pt.(before sampling) a n/a Ft. (MSL) Measuring Point's 3.33 Ft. above land surface or 13.13 Ft. (MSL) Gallons of water pumped/bailed before sampling CONTINUOUS Field Analysis: pH 7.7 Specific Conductance 163 uMhos Temp 32.7 oC Odor NONE Date Sample Collected 04/16/96 Date Lab Sample Analyzed 4/16-429 1996 Appearance: CLEAR Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 (Tg Env Lab) and 78 (Coliform Only) SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED X YES NO COD N/A mg/I NO2 as N N/A mg/I Ni — NY kel N/A mg/I Coliform: MF Fecal N/A /100m1 NO3 as N N/A mg/1 Pb — Lead N/A mg/1 Coliform: MFTotal <1 /100m1 Phosphorus: Total as P 0.019 mg/I Zn — Zinc N/A mg/I Dissolved Solids: Total 155 mg/1 Al — Aluminum N/A mg/I Pesticides/Herbicides (Specify) pH (when analyzed) 7.1 units Ba — Barium N/A mg/I ug/1 TOC 1.9 mg/I Ca — Calcium N/A mg/I ug/1 Chloride 11.8 mg/1 Cd — Cadmium <1.0 ppb ug/I Arsenic N/A mg/I Chromium: Total <1.0 ppb Other FLUORIDE 0.12 mg/1 Grease and Oils N/A mg/I Cu — Copper N/A mg/I Other MIRK N/A ug/I Hardness: Total N/A mg/1 Fe — Iron N/A mg/1 Other Ag — Silver N/A mg/I Phenol N/A mg/1 Hg — Mercury N/A mg/1 Other Se — Selenium N/A mg/1 Sulfate <10 mg/1 K — Potassium N/A mg/1 ug/1 Specific Conductance N/A uMohs Mg — Magnesium N/A mg/1 ug/1 Total Ammonia(NH4 + NI13) N/A mg/1 Mn — Manganese <0.01 ppm TKN as N N/A mg/1 Na — Sodium N/A mg/1 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERMIT'EE (OR AUTHORIZED AGENT) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) DATE t0 u k17 crk tJ1 • COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM DIVISION.OF ENVIRONMENTAL MANAGEMENT P.O. BOX 29535 Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT Address P.O. BOX 48 AURORA, NC 27806 PERMITNO.: WI0700012 Non-Uischarge I arlc Farm Remedial System _Lagoon _Septic Tark/Drain Field Spray Held Subsurface Low-t'ressure _Land Appl of Sludge Well Location : Tank Farm Rotary Distributor _x_Otl Well I.D. Numbcr: INJ. SUPPLY Well Depth: 179.0 Well Depth: Well Diatnier 6" Sample (Screened) Interval N/A Ft. to N/A Ft. Depth to Water Level N/A Ft. below meas. pt.(before sampling) or NIA Ft. (MSL) Measuring Points 1.00 Ft. above land surface or NIA Ft. (MSL) Gallons of water pumped/baikd before sampling CONIINUOUS Field Analysis: pH 7.1 Specific Conductance 828 uMhos "Temp 18.5 oC Odor NONE Date Sample Collected 04/16196 Date Lab Sample Analyzed 4/16 -4/29 1996 Appeararce: (TEAR Laboratory Name : l'CS PIIOSPIIATE ENV. AFFAIRS LAB Certification No. 330 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD N/A mg/I NO2 as N N/A mg/I Ni - Nickel N/A nrgl Coliferm: MF Fecal N/A /100ml NO3 as N N/A mg/f Pb - Lead N/A mg/I Colifcrm: MFTotal N/A /100m1 Phosphorus: Total as P 0.049 mg/1 Zn - Zinc NIA mg/1 Dissolved Solids: Total 464 mg/1 Al - Aluminum N/A mg/1 Pesticides/llerbicides (Specify) pH (when analyzed) 7.8 units Ba - Barium N/A mg1 ugil TOC 5.9 MO Ca - Cahium N/A mg11 ugil Chloride 66.6 mg/1 Cd - Cadmium N/A mg/1 ug/l Arsenic N/A mg/I Chromium: Total N/A mgil Other FLUORIDE 0.57 mg/I Grease and Oik N/A mg/1 Cu - Copper N/A mg/1 Other MIBK N/A ug/I llardness: Total N/A mg/1 Fe - Iron N/A mg/1 Other Ag - Silver N/A mg1 Phenol N/A mg/1 Iig - Mercury N/A mg/1 Other Se - Selenium N/A mg/I Sulfate <10 mg/I K - Potassium N/A mg/1 ugil Specific Conductance N/A uMohs Mg - Magnesium N/A mgl ugil Total Ammonia(NH4 + N113) N/A mg/I Mn - Manganese N/A mg/I TKN as N N/A mg/1 Na - Sodium N/A mg/1 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE SIGNATURE OF PERMITTEf= (OR AUTHORIZED AGENT) Note: Values should reflect dissolved and colloidal concentrations. 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