WI0700012_Monitoring (Report) Aug - Oct 2011_20111219

W. PotashCorp'
Helping Nature Provide
November 21, 2011
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
CERTIFIED MAIL
RECEIVED / DENR / DWQ
Aquifer Protection Section
DEC 19 2011.
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
August 2011— October 2011
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Qi:
I'S
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) piezometer level
monitoring field sheet, and d) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this information.
Sincerely,
At,‘fl,tie
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
RECEIVED
Information Processing Unit
DWQ/BOG
1530 NC Hwy 306 South, Aurora, NC USA 27806 T [phone]
PCS Phosphate I www.potashcorp.com

pc: Will Hart — Aquifer Protection DWQ, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
Mike Brom (w/ attachments)
David Harmon (w/ attachments)
R. B. Lee (w/ attachments)
Total Two Copies
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
RECEIVED
DEC 1 - 201J
Information Processing Unit
DWQ/BOG
H:\Reports\2011\Quarterly\TFRAS Report Third Quarter 2011.docx
2

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CIW-7
Well Depth:
48.00 ft. Well Diamter:
4 inc
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check one:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.9 , Specific Conductance 731 uMhos
Temp. 22.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/25/2011
10/25/2011 to 10/31/2011
PCS PHOSPHATE
330 10
PARAMETERS:
COD
Coliform: MF Fecal N/A
(Samples for metals were collected unfiltered X Yes
N/A mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 476 mg/I Al - Aluminum
pH (when analyzed) 7.0 units Ba - Barium
TOC 8.1 mg/I Ca - Calcium
Chloride 19.4 mg/I Cd- Cadmium
Arsenic N/A ` mg/1 Chromium: Total
N/A mg/I Cu - Copper
N/A mg/1 Fe - Iron
10.4 mg/1 Hg - Mercury
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
<0.020 mg/I Zn - Zinc
N/A
N/A
N/A
N/A mg/1 Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/1 Fluoride
N/A mg/I MIBK
<0.001 mg/1 Ag - Silver
0.55
N/A
N/A
<0.005 mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A mg/I Report attached? Yes (1) No
N/A mg/I Mg - Magnesium N/A mg/I VOC : method#
N/A mg/I Mn - Manganese
<0.010
mg/I
method#
method#
N/A
N/A
mg/I
mg/1
mg/I
mg/I
mg/1
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
j.f. ?lift
Information Processing Unit
OWQ/BOG
eckel General Mana•er

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval:
Depth to Water Level:
Measuring Point is
38.70 ft. to 40.70 ft.
21.46 ft. below measuring point.
3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.9 , Specific Conductance
Temp. 22.3 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
771 uMhos
Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 01/31/13
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/25/2011
10/25/2011 to 10/31/2011
PCS PHOSPHATE
330 10
PARAMETERS: (Samples
COD
Coliform: MF Fecal
Coliform: MF Total
for metals were collected unfiltered X Yes
N/A
N/A
<1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 490
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.9
13.7
18.0
N/A
N/A
N/A
51.8
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
No and field acidified X Yes No )
N/A mg/I Ni - Nickel N/A mg/I
N/A mg/I Pb - Lead N/A mg/I
0.465 mg/I Zn - Zinc N/A mg/I
N/A mg/l Ammonia Nitrogen mg/I
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride 0.53 mg/I
N/A mg/I MIBK N/A ug/I
<0.001 mg/I Ag - Silver N/A ug/I
<0.005 mg/I Se- Selenium N/A ug/I
N/A mg/I Sodium N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
0.049 mg/I
• method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
DEC 1 - 2011
information ProcessingOUnit
DWQ
ckel, General
`'Sig re of • ermittee . SthoKzed Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
per ma)
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter: 4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: NIA ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 2209 uMhos
Temp. 21.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01 /31113
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/20/2011
Date sample analyzed: 10/20/2011 to 10/25/2011
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1628 mg/I Al - Aluminum
pH (when analyzed) 6.0 units Ba - Barium
TOC 6.4 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
32.5 mg/l Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/l Cu - Copper
N/A mg/I Fe - Iron
623.8 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I
108.000 mg/1
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/l
N/A ug/I
Pb - Lead N/A ug/1
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.40 mg/I
MIBK N/A ug/I
Ag - Silver N/A ug/I
N/A ug/I
NIA ug/I
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
kibThation
DWQ/63Zsing Unit
eckel, General Manager
thorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH N/A , Specific Conductance
Temp. N/A oC, Odor N/A
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
N/A
N/A uMhos
Appearance: N/A
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/20/2011
10/20/2011 to 10/20/2011
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid sa -s) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC N/A mg/I
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mgll Cd- Cadmium
N/A mg/1 Chromium: Total
N/A mg/1 Cu - Copper
N/A mg/I Fe - Iron
N/A mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I
N/A mg/I
/I
N/ ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/l
N/A ug/I
N/A ug/I
N/A ug/I
Pb - Lead
Yes n/2 No )
N/A ug/I
N/A ug/I
Zn - Zinc N/A ug/I
m - itrogen mg/1
they .- f n. and Concentration Units)
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
N/A ug/I
N/A ug/l
N/A ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
EC i 2D11
Information Processing Unit
DWQ/BOG
kel, Gen
I!lanager
igna ure of Permittee (or A'orized Agent)
(Datk)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.5 , Specific Conductance 2260 uMhos
Temp. 21.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/20/2011
10/20/2011 to 10/25/2011
PCS PHOSPHATE
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes nia
COD N/A mg/l Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 2272
pH (when analyzed) 5.5
TOC 9.1
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
33.1
N/A
N/A
N/A
479.0
N/A
N/A
N/A
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/l Fe - Iron
mgll Hg - Mercury
uMhos K- Potassium
mg/1 Mg - Magnesium
mg/l Mn - Manganese
395.000 mg/I
N/A mg/1
N/A ug/I
N/A ug/I
N/A ug/I
No and field acidified Yes n/k No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I
N/A ug/I
Se- Selenium
Sodium
0.46
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS,
N/A ug/I (Specify test method #.
N/A ug/I Report attached? Yes
N/A ug/I VOC
N/A ug/I
ug/I
ug/I
ug/I
mg/1
mg/1
ug/I
ug/I
ug/I
ug/I
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
DEC a 2011
InformatiDon WQea Unit
uthonzed Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter: 4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH N/A , Specific Conductance N/A uMhos
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
X
N/A
Temp. N/A oC, Odor N/A Appearance: N/A
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/20/2011
10/20/2011 to 10/20/2011
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A mg/I
N/A /100m1
N/A /100m1
(Note: Use MPN method for highly turbid s.
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg
uni
mg/I
mg/I
mg/I
mg/l
mg/l
mg/I
uMhos
mg/I
mg/I
Yes n/a No and field acidified
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I N; - Nickel
N/A mg/I Pb - Lead
N/A mg/I Zn - Zinc
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
ug
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
K
Ag - Silver
Se- Selenium
Sodium
Yes n/2 No )
N/A
N/A
N/A
Organics: (GC, GC/MS. HPLC)
(Specify test method #.
Report attached? Yes
VOC
N/A
N/A
N/A
N/A
N/A
Attach lab report.)
(1) No X
method#
method#
method#
ug/1
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
)EC 1- zo»
Mnbnneltion Processing Unit
DWQ/BOG
Steven
P mitte
Sig
ckel. Ge
ne
a r
A t) ame i le
�` //
mi ee (or Authorized Agent)
p .r pnn
fib
Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter: 4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.0 , Specific Conductance 3206 uMhos
Temp. 29.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/20/2011
Date sample analyzed: 10/20/2011 to 10/25/2011
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
Yes n/a No and field acidified Yes n/a No )
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A ug/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A ug/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 94.000 mg/1 Zn - Zinc N/A ug/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total 3400 mg/I Al - Aluminum N/A ug/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) 5.2 units Ba - Barium N/A ug/I Fluoride <0.3 mg/I
TOC 9.8 mg/I Ca - Calcium N/A ug/l MIBK N/A ug/I
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
42.0 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
805.7 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC method#
N/A ug/I
Ag - Silver
Se- Selenium
Sodium
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
DEL 1 2011
Information Processing Unit
DWQ/BOG
onzed Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 26.00 ft. Well Diamter:
SWW-6
4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1940 uMhos
Temp. 25.3 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/20/2011
10/20/2011 to 10/25/2011
PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1268 mg/I
pH (when analyzed) 6.1 units
TOC 8.9 mg/I
Chloride 41.2 mg/1
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A mg/I
N/A mg/I
515.2 mgll
N/A uMhos
N/A mg/I
N/A mg/I
unfiltered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified Yes nl2 No )
N/A mg/I
N/A mg/I
90.000 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A mg/1 Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
N/A ug/I Sodium
N/A ug/l Organics: (GC, GC/MS,
N/A ug/I (Specify test method #.
N/A ug/I Report attached? Yes
VOC
N/A ug/I
N/A ug/I
mg/1
<0.3 mg/1
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
SEC -- 201'
Mlbrma DWQ/BOG
Png Unit
Steven AM kel, Gene
P mitte fthonz flgt) Name
Sig re bf eimittee (or Authonz-d Agent)
print
ate)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter: 4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling: N/A
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. NIA oC, Odor N/A Appearance: N/A
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01 /31 /13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/20/2011
Date sample analyzed: 10/20/2011 to 10/20/2011
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
N/A mg/I
N/A /100m1
N/A /100m1
COD
Coliform: MF Fecal
Coliform: MF Total
(Note Use MPN method for highly tur. _ a es)
Dissolved Solids: Total
pH (when analyzed)
TOC /A mg
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A mg/I
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Yes n/a No and field acidified Yes nlz No )
N/A
N/A
N/A
mg/I Ni - Nickel
mg/I Pb - Lead
mg/I
Orthophosphate A mg/1
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
N/A mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/l
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Zn - Zinc
N/A ug/I
N/A ug/l
N/A ug/l
nia Nitrogen mg/I
nds and Concentration Units)
N/A mg/1
N/A ug/I
N/A ug/I
N/A ug/I
Sodium N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
Ag - Silver
Se- Selenium
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
DEC 1-2011
Information Processing Unit
DWQ/BOG
Steve
eckel, Ge al Ma -qer
g )
uth'
zed
err z Na , leas
at f rmittee ~ or
d Agent)
pe//or nn
(D te)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter: 4 inch
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor N/A Appearance: N/A
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC X
01/31/13
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/20/2011
10/20/2011 to 10/20/2011
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals
COD
Coliform: MF Fecal
Coliform: MF Total
were collected unfiltered
(Note. Use MPN method for highly tur
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
/100m1
/100m1
Yes nia
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
mg/1 Cd- Cadmium
mg/l Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
No and field acidified
N/A mg/1 Ni - Nickel
N/A mg/I Pb - Lead
N/A mg/I Zn - Zinc
N/A ug/I
N/A ug/l
N/A ug/l
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Yes n/a No )
nia Nitrogen
Ag - Silver
Se- Selenium
nds and Concentration Units)
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
: method#
method#
N/A ug/l
N/A ug/I
N/A ug/I
mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/l
N/A ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
V II
NOTE:
GW-59 Rev 3/2000
R
DEC 1- 2011
Information Processing Unit
DWQ/BOG
Steven ckel. Gen I N1 qer
P itt e Na e
ease'pe or nt
112g
Y
Si
ture e mittee (o rized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
„
Well Identification Number (from Permit): CWW-2
Well Depth:
52.15 ft. Well Diamter:
4 inch
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.6 , Specific Conductance 2174 uMhos
Temp. 21.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/20/2011
10/20/2011 to 10/25/2011
PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 410.000 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 2052 mg/I Al - Aluminum N/A ug/I
pH (when analyzed) 5.6 units Ba - Barium N/A ug/I
TOC 10.3 mg/I Ca - Calcium N/A ug/I
Chloride 34.3 mg/I Cd- Cadmium N/A _ ug/I
Arsenic N/A mg/I Chromium: Total N/A ug/I
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
338.3 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium N/A ug/I
N/A mg/I Mn - Manganese N/A ug/I
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
No and field acidified Yes n/E No )
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A _ ug/I
Ni - Nickel N/A ug/I
N/A ug/I
N/A ug/I
mg/1
Other (Specify Compounds and Concentration Units)
Fluoride 0.49 mg/1
MIBK N/A ug/I
Ag - Silver N/A ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
Se- Selenium
Sodium
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
DEC1-2011
littinnation Processing Unl
DWQIBOG
Steve
Signatu
el, Gen
o ermittee (or Au
er
on ed Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-3
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level: N/A ft. below measuring point.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
Measuring Point is 3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling: N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor N/A Appearance: NIA
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC X
01/31/13
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/20/2011
10/2012011 to 10/20/2011
PCS PHOSPHATE
330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
. _ Orth•.h.sphat
N/A mg/I Ca - Calciu
N/A mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
N/A mgll Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
N/A mg/I Zn - Zinc
IA
of
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/l
MIBK
Ag - Silver
Se- Selenium
Yes n1a No )
ri
o en
d
Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC method#
method#
method#
N/A ug/l
N/A ug/I
N/A ug/I
mg/I
ds and Concentration Units)
N/A mg/1
N/A ug/I
N/A ug/l
N/A ug/I
N/A ug/I
N/A ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
DEC 1 - 2011
Information Processing Unit
DWQ/BOG

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 41.67 ft. to 50.92 ft.
4 inch
Depth to Water Level: N/A ft. below measuring point,
Measuring Point is 2.75 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor N/A Appearance: N/A
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01131 /13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10120/2011
10/20/2011 to 10/20/2011
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1
/100m1
N A mg
N/A mg/I
N/A mg/I
N/A mg/l
N/A mg/I
N/A mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Nitrate (NO3 as N)
Yes n/a
Phosphorus: Total as P
Orthophosphate
a Calciu
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
N/A mg/I Zn - Zinc
N/
g/I Am
Oth
/A ug
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ugll
Yes nk No )
N/A
N/A
N/A
Nitrogen
s and Concentration Units)
Ag - Silver
Se- Selenium
Sodium
N/A
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
!)EC - 2011
information Processing unit
DwoisoG
orized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-5
Well Depth: 53.17 ft. Well Diamter: 4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level: NIA ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor N/A
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
N/A
Appearance: N/A
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01 /31 /13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/20/2011
10/20/2011 to 10/20/2011
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples
COD
Coliform: MF Fecal
Coliform: MF Total
for metals were collected
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samp
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I
/100m1
/100m1
/1
s
N/A mg/I Ca - Calcium
unfiltered
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
N/A mg/1 Cd- Cadmium
N/A mg/1 Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
N/A mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/1 Mn - Manganese
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
N/A mg/1 Zn - Zinc
N
N/
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
mo
Yes n/2 No )
d Concentration Units)
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
N/A ug/I
N/A ug/I
N/A ug/I
mg/1
N/A mg/l
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
I]EC - 2011
won Processing Unit
DWQIBOG

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-6
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 1944 uMhos
Temp. 26.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC X
01/31/13
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/20/2011
Date sample analyzed: 10/20/2011 to 10/25/2011
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
Yes n/a No and field acidified Yes n/z No )
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 42.750 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I
Dissolved Solids: Total 1268 mg/I Al - Aluminum N/A ug/I
pH (when analyzed) 6.5 units Ba - Barium N/A ug/I
TOC 6.2 mg/I Ca - Calcium N/A ug/I
Chloride 44.5 mg/I Cd- Cadmium N/A ug/I
Arsenic N/A mg/I Chromium: Total N/A ug/I
Grease and Oils N/A mg/l Cu - Copper N/A ugll
Phenol N/A mg/I Fe - Iron N/A ug/I
424.7 mg/I Hg - Mercury N/A ug/I
N/A uMhos K- Potassium N/A ug/I
N/A mg/1 Mg - Magnesium N/A ug/I VOC
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride <0.3 mg/I
MIBK N/A ug/I
Ag - Silver N/A ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
Se- Selenium
Sodium
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations. �TEt,t/ � —�� 6,
NOTE:
GW-59 Rev 4/98
RECEIVED
JET 2011
Intonation Processing Unit
DWQ/BOG
ign: . - ermittee (o Au orized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-7
Screened Interval: 36.58 ft. to 50.83 ft.
4 inch
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH N/A , Specific Conductance
Temp. N/A oC, Odor N/A
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
N/A
N/A uMhos
Appearance: N/A
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
01/31/13
UIC X
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/20/2011
10/20/2011 to 10/20/2011
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected
COD N/A
N/A
N/A
Coliform: MF Fecal
Coliform: MF Total
(Note. Use MPN method for highly turbid s
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/l
/100m1
/100m1
mg
uni
mg/I
N/A mg/I
N/A mg/l
N/A mg/I
N/A mg/I
N/A mg/I
N/A uMhos
N/A mg/1
N/A mg/I
unfiltered
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
Phosphorus: Total as P
Orthophosphate
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
N/A mg/I Zn - Zinc
Yes n/e No )
N/A
N/A
N/A
g/I Am :_ _ Nitrogen
Othe
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
ug/I
ug/I
ug/I
mg/1
mg/I
K ug/I
ug/I
ug/I
ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
Ag - Silver
Se- Selenium
Sodium
N/A
N/A
N/A
N/A
N/A
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
`P'1`11
� .
Information
PrO Ossing Unit
D\N
Steven A is;/kel, General
P•`mi
.•-
en a e and "/ se` •e or r' t
/
Signature of Pe mi - ee (or Authorized gent) (Da )

PCS Phosphate co., Inc. - Tank Farm Remediation System Quarterly Monitoring
Date: /O//f /'
Time:
Tech:
System Gauge
Pressures
SWW-1
0,.
SWW-7
Jjvc3 2i
CWW-1
p ..jje%%%�/,'
'f,/%
�/2
CWW-7 _
File: 12-07-02
Sand Layer Pelzometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Wet ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
.3 7/
. 7
Cpz-1
10.51
/7 29
'f vs
Spz-2
11.21
A -/v4
C '7
Cpz-2
10.25
i3 Z
- ,c. 7
Spz-3
11.87
e9•
//. 75
Cpz-3
11.12
/ 5. 9V
- /7 . 14
Spz-4
11.45
6. /8
Boa%
CPW
9.65
ii'lk5:-
7
Spz-5
11.45
9 i/?
�,
6. . O]� 3
MWTF-1A `
14.35
%l.
'l0
9,
Spz-6
11.23
,o4S
o.
� !7,9
MWTF-18'
14.36
r - /90
�j'
Spz-7
11.59
if"60
- (�%l
MWTF-1C *
14.44
,4a, v�j
'�.:J-
-6, 0
Spz-8
11.57
/e 13
z 4/4
MWTF-2A
14.05
;p, fJ l
7 3
Spz-9
11.01
j • //
r ,
MWTF-2B
14.02
/7 f 5
p9..5?
Spz-10
12.16
9 c� 7
/90
c:.�f. G'9 9
MWTF-2C
14.08
//J ; 79
` / 9/
SPW
9.95
9';ot9 _
c.,4,,r
MWTF3A
12.21
V• 7
,CJ
MWTF-38
12.18
/e%, n&
C., l/C
MWTF-3C
12.19
/'7 .3
` 67 / /
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Pump
Activation Depth
Rel MS_ L
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping?
V es/ N o
Comments
10.70
//
+1 to +2
.
-2 ' to -1'
+1 to+2
____
-2.to-1'
o
��
��0 oGn9
:0
0.70
CWW-7
9.95
9'
-2'to-1'
Revised 7/29/02
' Riser length added to TOC elevation 1/24/97
D:1Data\Forms\Well Forth\Tank Farm Remed Wells.xis

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
August 2011— October 2011
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Infection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
during the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
August
544,542
0
544,542
12.2
15.0
September
576,347
0
576,347
13.3
15.0
October
576,814
0
576,814
12.9
15.0
TOTALS
1,697,703
0
1,697,703
Q CENE®
i ��
pV.b - ZoVi
Processing Unit
Inert pW QIBOG
H:\Reports\2011\Quarterly\TFRAS Report Third Quarter 2011.docx
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
August
1,006,976
212,825
1,219,801
29.2
September
503,886
321,646
825,532
19.1
October
222,794
79,985
302,780
6.8
TOTALS
1,733,657
614,456
2,348,113
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWAN') Pumps
On 8% 15 replaced the main water meter.
SWW-1:
SWW-2: On 10/24 replaced counter.
SWW-3:
SWW-4: On 9/28 replaced pump.
SWW-5:
SWW-6:
SWW-7:
H:\Reports\2011\Quarterly\TFRAS Report Third Quarter 2011.docx
RECovED
DEC 1 2011
Information Processing Unit
DWQIBOG
4

Croatan Formation \Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2:
CWW-3:
CWW-4:
CWW-5:
CWW-6: On 10/27 replaced counter.
CWW-7: On 10/28 replaced pump.
RECEIVED
DEC 1 ® 2011
Information Processing Unit
DWQ/BOG
H:\Reports\2011\Quarterly\TFRAS Report Third Quarter 2011.docx
5