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HomeMy WebLinkAboutWI0700012_Monitoring (Report)_20180619Routine Monitoring Report Review (RMRR) Checklist PermitNi :: 1-5/9 ?-000 /2_- Permittee:-. -1 CS'- -Pi✓ ' / Facility Name: .k L¢ rr�F Reviewer: - . Ai Date Reviewed: all, 1. BIMS: Permit Issued date: . /Z /ry Expiration date: j3/al If Expired, check with Permittee f they want to renew. For Non -Discharge (ND) permit, if they don't want to renew, they will have to request rescission. 2. BIMS: Log report in Events Tab:, Select-> `Compliance Schedule Met' and enter name and date of report, and date we received. Also, note chat a RIVIRR,was completed and inserted into repo t report./ Comp leted: /9119 3. BIMS: For 51 reports- has Injection Event Report (IER) been received and info entered into BIMS de (Yes or No). If No, check file to see if we have received and then enter into B If never received, then request from Consultant and CC Permittee via email. After receipt of IERs from these parties, enter into BIMS. For Non -Discharge (ND) reports- Is billing is up to date? x (Yes or No). If past due, notify Permittee/Consultant via email, and include contact info for Teresa Revis to send payment (contact info below). NC Department of Environmental Quality Division of Water Resources Budget Office Attn: Teresa Revis 1617 Mail Service Center Raleigh, NC 27699-1617 Te resa. Revi s @ n cd e n r.gov (919) 807-6316 4. BIMS: Check Wells Tab and see if GW-1s/GW-30s (if applicable) have been entered: iJ (Yes, No, or N/A). If No and well status is still `proposed', then check file to see if we have received GW-1 s and then enter into BIMS. If not received, then request from consultant and CC Permittee. After receipt from these parties, enter as -built well construction into BIMS (change status of well from proposed to active); and well abandonment data, if applicable. Continued On Other Side Page 1 of 2 Rev. 6-22-2018 5. For 51/In-situ groundwater remediation reportsz Do a quick review of report to see if -there are any obvious impacts from injection activities by readmg-Summary and- Conclusions/Recommendation_Section,_and monitoring data -tables RCompare pre-- - injection levels of sulfate, iron, phosphate, etc. to post injection levels and note this below. If there are no impacts evident, indicate `No" mpacts from=injection evident'. NOTE: The groundwater quality at the site mustbe anosiitored-until concentrations meet pre -injection levels or 2L standards before the pernnt caneventually be Completed in BIMS, and a Completion Letter Sent to Permittee. For Non -Discharge reports- -Also .check inflnentarid=effluenfconce itrations, most - permits require a minimum 95% reduction in concentrations. NOTES/COMMENTS: /�2 F j 6. When this Monitoring Report Review is complete, securely insert inside cover of monitoring report and f le. Completed: fo l / 9 (8 (date) Page 2 of 2 Rev. 6-22-2018 klutrien- Feeding the Future - May 25, 2018 Inactive Hazardous Sites Branch Attn: Sue Murphy CERTIFIED MAIL Subject: Underground Injection Control Program Quarterly Groundwater Monitoring Report February 2018 — April 2018 Injection Well Permit #WI0700012 PCS Phosphate Company, Inc.' Tank Farm Remedial Action System Beaufort Co. CUEIVED/NCUFQIUV\ JUN 0 7 201 'Vater Quality' �Pr�Itln Please find the subject groundwater monitoring report attached. This includes the sampling and reporting requirements of the above referenced permit as well as the reporting requirements of the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7, b) MWTF1-CR, c) Form GW-59 for each of the fourteen withdrawal wells, d) piezometer level monitoring field sheet and e) the summary operational and maintenance report. Please do not hesitate to contact me at (252) 322-8283 if you have any questions regarding this information. Sincerely, AUVU4I D. Daniel Winstead III Senior Environmental Engineer Nutrien Attachments 1530 NC Hwy 306 South, Aurora, NC USA 27806 1 nutrien.oarr, pc: Will Hart — Aquifer Protection DWQ, WaRO (w/ attachments) 12-07-02 (w/ attachments) Alex Hunt (w/ attachments) R. B. Lee (w/ attachments) Electronically submitted: Inactive Hazardous Sites Branch Attn: Sue Murphy 1 Effective January 1, 2018, PCS Phosphate Company, Inc. is an indirect subsidiary of Nutrien Ltd. PCS Phosphate Company, Inc. remains the legal operating entity and permittee. 2 Date: Time: Tech: PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring /OM System Gauge Pressures i SWW-1 WA SWW-7 N/A •CWW-1 N/A CWW-7 N/A File: 12-07-02 pc: TLB Rumor. L velRel PMMMSL , bUBL Ditch 12.91 7/4/ Barge Slip Water Level Control Tank %=MSL 10.59 Sand Layer Peizometers Level Indicators Well ID TOC Elevation MSL' TOC Stc Wtr' Level' , Level - Relative To MSL Ft. Well ID TOC Elevation MSL' TOC , Stc Wtr Level' Level Relative To MSL Ft Spz-1 10.47 ooy%61 Cpz-1 10.51 // 25,1 Spz-2 11.21 V'o� Cpz-2 _' 10.25 Spz-3 11.87 C!or9v7ce Cpz-3 11.12 1 77p47evYd Spz-4 11.45 ,/- f/6,A CPW 9:65 -,/ es�r2°d Spz-5 11.45 7 8 MWTF-1A ' 14.35 3 79 Spz-6 ' 11.23 /3/'' B7 MWTF-1B • 14.36 2/019 Spz-7 11.59 7.95 MWTF-1C • 14.44 /1 Q8 Spz-8 11.57 ' '.01% MWTF-2A 14.05 ;tS Spz-9 11.01 MWTF-2B 14.02 .. g'80 Spz-10 12.16 . v ,`1/ MWTF-2C 14.08 i4.5-:-9o? SPW 9.95- ' �-- et, i-weI MW rF-3A 12.21 v-432 MWTF-3B 12.18 770 MWTF-3C 12.19 /3,8? Sand Layer And Croatan Formation Withdrawal Wells' Well ID TOC Elevation MSL' Max Stc ' Wtr Level Ft. Pump Activation Depth Rel MSL Max Level Relative To MSL Ft. Control Point MSL' . Is Wen , •' Pumping?' (Y)es/(N)o Comments • SWW-1 10.70 N/A 6' . WA - +1'to+2' CWW-1 10.60 N/A 9' N/A -2'to-p SWW-2 9.99 N/A 6' N/A +1 'to+2'_. CWW-2 10.23 N/A 9' N/A . -2'to 1 SWW-3 9.97. WA 6' N/A +1' to+2' _ CWW-3 9.95 WA - 9' N/A -2'to-1' SWW-4 10.73 N/A -, 6' . WA +1 ' to+2' CWW-0 10.73 WA 9' N/A -2'to-1' SWW-5 10.80 N/A 6' WA `.. +1'to+2' CWW-5 10.74 N/A 9' N/A -2'to-1' SWW-6 10.66 N/A 6' N/A +1 ' to+2' CWW-6 9.92 N/A 9' N/A -2'to-1' SWW-7 10.70 N/A 6' WA +1' to+2' CWW-7 9.95 N/A 9' N/A -2'to-1' evlse • Riser length added to TOC elevation 124/97 D:1DatelFouns1Well FomfTank Farm Remed W&lsads P 71 OFFICE 8NG CWWd MWLFf CLUSTER / DRAINAGE DITCH 003 WRNDRAWµ WELL . FLOW TOTALIZERS AND CONTROL VALVES 005 PIPER ' ONTAINMENT PAD WATER LEVEL CONTROL TAN MWTF4 CLUSTER SPL4O SPLD 004 SCALE,—. T.00 LEGEND SYMBOL DESCRIPTION PWIOMETER • MNNNOR WELL ® CONFINED RAND IAVER WITHDRAWAL WELL ® CROATAN FORMATION WNNDRAWµ WELL, J'1 CROATAN FORMATION INJECTION WELL • INJECTION WELL HEADER PIPE CLEAN -OUT • INJECTION WELL SVUIEM WATER LEVEL CONTROL TANK LOCATION PLAN:FOR TANK;Fm/ M GROUNDWA COMPLIANCE REPORT FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled Mail Original and 1 copy to. PERMIT #: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED bpikt2rongPii'QF4froRONMENT$ idATURgAt o41RE i1fI81 1• N QFVYiq pF! R ;;QIJR ErS-tltlfc!RIVi rpN PRocEssiN a AL G) i NG ;tr625 t?(f17:: Phoif2:: (949) 84 *$30fi: i';' !i WI0700012 EXPIRATION DATE: UIC X 01/31/18 18 Well Identification Number (from Permit): CWW-1 Well Depth: 55.00 ft. Well Diamter: 4 inch Screened Interval: 33.27 ft. to 52.68 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 2.25 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery Remediation : Land Application of Sludge Water Source Heat Pump CONTINUOUS Field Analysis: pH 6.3 , Specific Conductance 4838 uMhos Temp. 22.1 oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 4/25/2018 4/25/2018 to 5/21/2018 PCS PHOSPHATE 330 10 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered Yes No and field acidified COD N/A mg/L Nitrite (NO2 as N) N/A mg/L Coliform: MF Fecal N/A /100mL Nitrate (NO3 as N) N/A mg/L Coliform: MF Total N/A /100mL Phosphorus: Total as P 14.400 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/L Dissolved Solids: Total 3360 mg/L Al - Aluminum N/A mg/L pH (when analyzed) 6.3 units Ba - Barium N/A ug/L TOC 2.7 mg/L Ca - Calcium N/A mg/L Chloride 805.0 mg/L Cd- Cadmium N/A ug/L Arsenic N/A ug/L Chromium: Total N/A ug/L Grease and Oils N/A mg/L Cu - Copper N/A mg/L Phenol N/A mglL Fe - Iron N/A ug/L Sulfate 957.0 mg/L Hg - Mercury N/A ug/L Specific Conductance N/A uMhos K- Potassium N/A mg/L Total Ammonia N/A mg/L Mg - Magnesium N/A mg/L TKN as N N/A mg/L Mn - Manganese N/A ug/L n/a Yes Ni - Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen n/a No ) N/A ug/L N/A ug/L N/A ug/L mg/L Other (Specify Compounds and Concentration Units) Fluoride <0.3 mg/L MIBK N/A ug/L N/A ug/L Se- Selenium N/A ug/L Sodium N/A ug/L Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC method# method# method# Ag - Silver I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 4/98 Mark D. Johnson, General Manager Permmte ( thorized Agent) Name and Title - Please type or int Signature o Permittee (or Authorized Agent) I (Date) GROUNDWATER QUALITY MONITORING:; COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Mail Original and 1 copy to: PERMIT #: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED DiEPARjMfENT QF ENV Rbf M1lT & Nlk'i 1 RESOURiCF,$: DMVI81O1'i! OF WATER RESOURCES-INFORMATIQ►S( p1 QCESS G 1617 MAIL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: (919) 807-6306 WI0700012 EXPIRATION DATE: 01/31/18 UIC X Well Identification Number (from Permit): CWW-2 Well Depth: 52.15 ft. Well Diamter: 4 inch Screened Interval: 30.57 ft. to 49.82 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 3.00 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery X Remediation : Land Application of Sludge Water Source Heat Pump N/A Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 5/23/2018 5/23/2018 to 5/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered COD N/A Coliform: MF Fecal N/A Coliform: MF Total /A (Note. Use MPN method for highly t Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N mg/L /100mL /100 Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: To I as P Yes n/a No and field acidified N/A mg/L N/A mg/L N/ N/A N/A Le N/A N/A mg/L Ca - Calcium N/A mg/L Cd- Cadmium N/A ug/L Chromium: Total N/A mg/L Cu - Copper N/A mg/L Fe - Iron N/A mg/L Hg - Mercury N/A uMhos K- Potassium N/A mg/L Mg - Magnesium N/A mg/L Mn - Manganese N/A mg/L N/A ug/L N/A ug/L N/A mg/L N/A ug/L N/A ug/L N/A mg/L N/A mg/L N/A ug/L Yes n/a No) Ni - Nickel N/A Pb - Lead N/A IZn N/A Am 1n Othe • •m• •sand Concentration knits) N/A N/A N/A N/A N/A ride MIBK Ag - Silver Se- Selenium Sodium ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L Organics: (GC. GC/MS. HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC : method# method# method# certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE. GW-59 Rev 4/98 Mark D. Johnson, General Manager Perme (f thorized Agent) Name and Title - Please type or print Signature o Permittee (or Authorized Agent)i eI (D Jte) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Om. pent.o PERMIT #: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery DEPAR'TMEN' QF ENV1RO1�YiEEfiT &NATU ALIRE DIVISION OF WATER RESOUROES�IIilFC1R 1 11¢ 1617AIL SERVICE CENTER ... MAIL RALEIGH, NC 27626-1617 WI0700012 SOURCES; : ;'• PRQCESS1N0:UNIT Phone: (919) 807.6306 EXPIRATION DATE: UIC X 01 /31 /18 Well Identification Number (from Permit): CWW-3 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 36.42 ft. to 50.67 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 3.08 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Water Source Heat Pump N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. _ N/A oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 5/23/2018 5/23/2018 to 5/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbis) Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A N/A N/A N/A N/A N/A N/A ug/L mg/L mg/L mg/L uMhos mg/L mg/L mg/L /100mL /100mL Nitrite (NO2 as N) Nitrate (NO3 as N) Yes Phosphorus: Total as P Orthophosphate g/ tini u mg/LSaum mglL Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K- Potassium Mg - Magnesium Mn - Manganese n/a No and field acidified N/A mg/L N/A mg/L N/A mg/L N/A L N/A N/A N/A N/A N/A N/A N/A N/A mg uglL ug/L mg/L uglL ug/L mg/L mg/L ug/L NI - Nickel Pb - Lead Zn - Zinc mo - - trogen er (t Flu MI Ag - Silver Se- Selenium Yes n/a No ) N/A N/A N/A Sodium Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC method# method# method# N/A N/A N/A N/A N/A ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 4/98 Mark D. Johnson, General Manager Permittee (o A tp horized Agent) Name and Title - Please type or print Signs ure of ermittee (or Authorized Agent) ttDat GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Mail Original and 1 copy to: PERMIT #: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED DEPART IEtl7:QF. 00004 NMENT &NATURAL RESOURCt DIVISION OFitt/ATER RESOURCES-INFQRMATI0N PROCESS`kIG 1617 MAIL SERVICE CENTER RALEIGH. NC 27626-1617 W10700012 Phone: (919) 807-6306 EXPIRATION DATE: UIC X Loot 01 /31 /18 Well Identification Number (from Permit): Well Depth: CWW-4 53.00 ft. Well Diamter: 4 inch Screened Interval: 41.67 ft. to 50.92 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 2.75 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery X Remediation : Land Application of Sludge Water Source Heat Pump CONTINUOUS Field Analysis: pH 6.3 , Specific Conductance 4559 uMhos Temp. 26.2 oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 4/25/2018 4/25/2018 to 5/21/2018 PCS PHOSPHATE 330 10 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 2840 pH (when analyzed) 6.4 TOC 2.4 mg/L /100mL /100mL Yes Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate mg/L Al - Aluminum units Ba - Barium mg/L Ca - Calcium Chloride 675.0 mg/L Cd- Cadmium Arsenic N/A ug/L Chromium: Total Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/L Cu - Copper N/A mg/L Fe - Iron 755.0 mg/L Hg - Mercury N/A uMhos K- Potassium N/A mg/L Mg - Magnesium N/A mg/L Mn - Manganese n/a No and field acidified N/A mg/L N/A mg/L 16.200 mg/L N/A mg/L N/A mg/L N/A ug/L N/A mg/L N/A uglL Ni - Nickel Pb - Lead Yes Zn - Zinc Ammonia Nitrogen n/a No) N/A NIA N/A Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver N/A uglL Se- Selenium N/A mg/L N/A ug/L N/A uglL N/A mg/L N/A mg/L NIA ug/L Sodium Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC • method# method# method# <0.3 N/A N/A N/A N/A ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L X (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 4/98 Mark D. Johnson, General Manager Permittee (ofAu horized Agent) Name and Title - Please type or prin <-16 3C Z.C. Signature of ermittee (or Authorized Agent) ( te) GROUNOV iATER QUALITY; MQNITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 OTOM Well Identification Number (from Permit): CWW-5 Well Depth: 53.17 ft. Well Diamter: 4 inch Screened Interval: 41.75 ft. to 51.08 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 2.58 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Mail Original and 1 copy to: PERMIT #: Non -Discharge NPDES DEPARTMENT OF ENVIRONMENT &NATUtRA RESOURCES DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: {919) 807-6306 W10700012 EXPIRATION DATE: UIC X 01 /31 /18 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Water Source Heat Pump N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 4/23/2018 4/23/2018 to 4/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered Yes COD N/A mg/L Coliform: MF Fecal N/A /100mL Coliform: MF Total N/A /100mL (Note' Use MPN method for highly turbid samples) Dissolved Solids: Total N/A •• •/L H( hen analyzed) Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate Al - Aluminu p wni TOC Chloride A g RI Arsenic N/A ug/L Chromium: Total Grease and Oils N/A mg/L Cu - Copper Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/L Fe - Iron N/A mg/L Hg - Mercury N/A uMhos K- Potassium N/A mg/L Mg - Magnesium N/A mg/L Mn - Manganese n/a No N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A and field acidified mg/L mg/L mg/L mg/L g/L r ug/L mg/L ug/L ug/L mg/L mglL ug/L Yes n/a No ) Ni - Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen N/A ug/L N/A ug/L N/A ug/L mg/L Specify Compounds and Concentration Units) g -- ilve Se- Selenium Sodium Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC method# method# method# N/A mg/L N/A ug/L N/A ug/L N/A ug/L N/A ug/L X (2) 1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE. GW-59 Rev 4/98 Mark D. Johnson, General Manager Permittee (of 4u orized Agent) Name and Title - Please type or print -5 136 (zcie Signature of rmittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-6 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 36.62 ft. to 50.88 ft. Depth to Water Level: NIA ft. below measuring point. For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Mail Original and 1 copy to: PERMIT #: Non -Discharge NPDES DEPARTMENT i71= ENVJROi!I NT &N ATURAt RESOURCE III i DIVISION OF WATER RESQURCE JNFORMATIQN PRQiCE840G 1617 MAIL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: (919) 807.6306 WI0700012 EXPIRATION DATE: UIC X 01/31/18 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Water Source Heat Pump Measuring Point is 2.92 ft above land surface. GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.3 , Specific Conductance 2300 uMhos Temp. 28.2 oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 4/25/2018 4/25/2018 to 5/21/2018 PCS PHOSPHATE Certification No(s) 330 10 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note. Use MPN method for highly turbid samples) Dissolved Solids: Total 1560 pH (when analyzed) 6.3 TOC 6.3 Chloride 57.0 Arsenic N/A Grease and Oils N/A Phenol N/A Sulfate 28.9 Specific Conductance Total Ammonia TKN as N N/A N/A N/A mg/L Nitrite (NO2 as N) /100mL Nitrate (NO3 as N) Yes /100mL Phosphorus. Total as P Orthophosphate mg/L Al - Aluminum units Ba - Barium mg/L Ca - Calcium mg/L Cd- Cadmium ug/L Chromium: Total mg/L Cu - Copper mg/L Fe - Iron mg/L Hg - Mercury uMhos K- Potassium mg/L Mg - Magnesium mg/L Mn - Manganese n/a No and field acidified Yes N/A mg/L N/A mg/L 34.200 mg/L N/A mg/L N/A mg/L N/A ug/L N/A mg/L N/A ug/L N/A ug/L N/A mg/L N/A ug/L N/A ug/L N/A mg/L N/A mg/L N/A ug/L Ni - Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen n/a No) N/A N/A N/A Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium <0 3 N/A N/A N/A Sodium N/A Organics: (GC. GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC • method# method# method# ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 4/98 Mark D. Johnson, General Manager Permittee (f thorized Agent) Name and Title - Please type orprint Signature o Permittee (or Authorized Agent) • (D4Ze GROUNDWATER QUALITYMONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled Mail Original and 1 copy to: PERMIT #: Non -Discharge NPDES DEPARTMENT OF ENV RONMENi &NAT1J A(RESOI)RCES DIVISION OF WATER RESOIJRCES•INFORMATION:PROCESSING UNIT 1617 MAIL_ SERVICE CENTER RALEIGH, NC 27626-11617 Phone: (919) 807.6306 W10700012 EXPIRATION DATE: UIC X 01 /31 /18 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : 18 Well Identification Number (from Permit): CWW-7 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 36.58 ft. to 50.83 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 1.25 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Rotary Distributor Land Application of Sludge Other Water Source Heat Pump N/A Field Analysis: pH N/A ,Specific Conductance NIA uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 4/23/2018 4/23/2018 to 4/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total (Note: Use MPN method for highly to Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N mg/L /100mL /100 Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: To units tsa N/A mg/L Ca - Calcium N/A mg/L Cd- Cadmium N/A ug/L Chromium: Total N/A mg/L Cu - Copper N/A mg/L Fe - Iron N/A mg/L Hg - Mercury N/A uMhos K- Potassium N/A mg/L Mg - Magnesium N/A mg/L Mn - Manganese Yes n/a No N/A N/A N/ N/A /A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A and field acidified Yes mg/L Ni - Nickel mg/L Pb - Lead el■Am Lthe ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L uoride MIBK Ag - Silver Se- Selenium n/a No ) s and Concentration Units) Sodium Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC method# method# method# N/A N/A N/A N/A N/A N/A N/A N/A ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 4/98 Mark D. Johnson, General Manager Permittee (o A horized Agent) Name and Title - Please type or prin 513C /Cie Signature of Permittee (or Authorized Agent) ( ate) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled PERMIT #: Non -Discharge NPDES pART00.0t::QiF:Ei4ii'I#000-4.**Tt3J 4 R SOURC•ES: DIVISIONOFWA.TE6d RESOURCE$=INFORMATION PROCESSING UNIT 1617 (AAfL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: (919) 807-6306 WI0700012 EXPIRATION DATE: UIC X 01 /31 /18 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery 18 Well Identification Number (from Permit): SWW-1 Well Depth: 22.50 ft. Well Diamter: 4 inch Screened Interval: 18.30 ft. to 21.12 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 1.52 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH N/A , Specific Conductance N/A uMhos For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Water Source Heat Pump N/A Temp. N/A oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 4/23/2018 Date sample analyzed: 4/23/2018 to 4/23/2018 Laboratory Name: Certification No(s) PCS PHOSPHATE 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A N/A N/A N/A N/A N/A N/A mg/L /100mL /100mL /L Nitrite (NO2 as N) Nitrate (NO3 as N) Yes nla No N/A Phosphorus: Total as P Orthophosphate mg/L Cd- Cadmium ug/L Chromium: Total mg/L Cu - Copper mg/L Fe - Iron mg/L Hg - Mercury uMhos K- Potassium and field acidified Yes n/a No ) mg/L Ni - Nickel N/A mg/L Pb - Lead N/A mg/L Zn - Zinc N/A N/A N/,imi N/A N/A N/A N/A N/A N/A N/A mg/L Mg - Magnesium N/A mg/L Mn - Manganese N/A ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L N/A N/A N/A mg/L eI1:i nia Nitrogen et•concentration Units) on y NIA Ag - Silver N/A Se- Selenium N/A Sodium N/A Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC method# method# method# ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 4/98 Mark D. Johnson, General Manager Permittee (o Ci,n Signature of Permittee (or Authorized Agent) horized Agent) Name and Title - Please type or print. ( te) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 m.) Mail Original and 1 copy to PERMIT #: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED DEPARTMENT QF:E 1V R00.1if0NT&NATURA1.RESOI:URCES DIVISION 0V07'ER RESOURCES INFQR MATIQtst PROCESSING UNIT 1617 MAIL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: (919) 807.6306 W10700012 EXPIRATION DATE: UIC X 01 /31118 Well Identification Number (from Permit): SWW-2 Well Depth: 23.00 ft. Well Diamter: 4 inch Screened Interval: 18.80 ft. to 21.63 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 3.42 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH N/A , Specific Conductance N/A uMhos For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery X Remediation : Land Application of Sludge Water Source Heat Pump NIA Temp. N/A oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 4/23/2018 4/23/2018 to 4/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total (Note Use MPN method for highly turbid sa -s) Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A mg/L /100mL /100mL mg/L mg/L ug/L mg/L mg/L mg/L uMhos mg/L mg/L Nitrite (NO2 as N) Nitrate (NO3 as N) Yes Phosphorus Total as P 0 hhophophate u Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K- Potassium Mg - Magnesium Mn - Manganese n/a No and field acidified N/A mglL N/A mg/L N/A mg/L N/A •i/ Ni - Nickel Pb - Lead Zn - Zinc nia y ' en peci on Yes n/a No) N/A N/A N/A N/A mg/L MIBK N/A ug/L N/A ug/L N/A mg/L N/A ug/L N/A ug/L N/A mg/L N/A mg/L N/A ug/L Ag - Silver Se- Selenium oncentration Units) Sodium Organics: (GC. GC/MS. HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC method# method# method# N/A N/A N/A N/A N/A X ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE. GW-59 Rev 4/98 Mark D. Johnson, General Manager Permit e ( A horized Agent) Name and Title - Please type or print Signature o Permittee (or Authorized Agent) ` Nate) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled PERMIT #: Non -Discharge DEPARTMENT OF:ENVIRONMENTi&NATIJRAl RESOURCES DIVISION Of WATER RESOURCES -INFORMATION PROCESSING UNIT 1617MAIL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: (919) 607-6306 W10700012 EXPIRATION DATE: 01/31/18 UIC X NPDES TYPE OF PERMITTED OPERATION BEING MONITORED 18 Well Identification Number (from Permit): SWW-3 Well Depth: 24.50 ft. Well Diamter: 4 inch Screened Interval: 20.17 ft. to 23.00 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 3.17 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery X Remediation : Land Application of Sludge Water Source Heat Pump N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 4/23/2018 4/23/2018 to 4/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered Yes COD N/A mg/L Nitrite (NO2 as N) Coliform: MF Fecal N/A /100mL Nitrate (NO3 as N) Coliform: MF Total N/A /100mL Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total ■ NIA /L Al - Aluminu pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A N/A N/A N/A N/A N/A N/A mg/L ug/L mg/L mg/L mg/L uMhos mg/L mg/L Cd- CLUmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K- Potassium Mg - Magnesium Mn - Manganese n/a , No N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A and field acidified Yes mg/L mg/L mg/L mg/L g/L ell ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L Ni - Nickel ,n/a No) Pb - Lead Zn - Zinc Ammonia Nitrogen pecify Compounds and Concentration Units) Ag - Sily Se- Selenium Sodium Organics: (GC, GC/MS. (Specify test method #. Report attached? Yes VOC N/A N/A N/A N/A N/A N/A N/A N/A HPLC) Attach lab report.) (1) No X (2) method# ug/L ug/L ug/L mg/L method# method# mg/L ug/L ug/L ug/L ug/L I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE. GW-59 Rev 4/98 Mark D. Johnson General Manager PermLtee of uthorized Agent) Name and Title - Please type or print /72(9 tcig Signature f Permittee (or Authorized Agent) (D e) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail Original and 1 copy to: DEPAR1 MENT OF ENVIRONMENT & NATURAL RESOURCES DiviSioN OF WATER RESOURCES•INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: (919) 807-6306 FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled PERMIT #: Non -Discharge W10700012 EXPIRATION DATE: UIC X 01 /31 /18 NPDES TYPE OF PERMITTED OPERATION BEING MONITORED 18 Well Identification Number (from Permit): SWW-4 Well Depth: 25.00 ft. Well Diamter: 4 inch Screened Interval: 20.50 ft. to 23.30 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 3.42 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH N/A , Specific Conductance N/A uMhos For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery X Remediation : Land Application of Sludge Water Source Heat Pump N/A Temp. N/A oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 4/23/2018 4/23/2018 to 4/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling. check here: PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total N/A pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A N/A N/A N/A N/A N/A mg/L /100mL Nitrate (NO3 as N) /100mL Nitrite (NO2 as N) Yes Phosphorus: Total as P Orthophosphate Al - Aluminum mg/L C•- a■ lum ug/L Chromium: Total mg/L Cu - Copper mg/L Fe - Iron mg/L Hg - Mercury uMhos K- Potassium mg/L Mg - Magnesium mg/L Mn - Manganese n/a No N/A N/A N/A N/A and field acidified Yes mg/L mg/L mg/L mg/L Ni - Nickel n/a No ) N/A Pb - Lead Zn - Zinc Ammonia Nitrogen N/A N/A ' r O+eafy Compounds and Concentration Units) II le'L N ug/L N/A ug/L N/A mg/L N/A ug/L N/A ug/L N/A mg/L N/A mg/L N/A ug/L g - Silver N/A Se- Selenium Sodium Organics (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC method# method# method# ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 4/98 Mark D. Johnson General Manager Permittee f A thorized Agent) Name and Title - Please type or print •,,1)t% Signature Permittee (or Authorized Agent) 61jr,IZDi� (¢ate) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled Mail Original and 1 copy to: PERMIT #: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery :DEPARTMENT OF I:tvvtt t NM6Nt a NAT(iRM RESOURCES i DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER RALEIGH, NC 27626-1817 Phone: (919} 807-6306 WI0700012 EXPIRATION DATE: UIC X 01 /31 /18 18 Well Identification Number (from Permit): Well Depth: 28.21 ft. Well Diamter: SWW-5 Screened Interval: 24.83 ft. to 27.21 ft. Depth to Water Level: Measuring Point is 4 inch NIA ft. below measuring point. 2.96 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Water Source Heat Pump N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 4/23/2018 4/23/2018 to 4/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note Use MPN method for highly turbid samples) Dissolved Solids: Total /A pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A N/A N/A N/A N/A N/A mg/L /100mL /100mL Nitrite (NO2 as N) Nitrate (NO3 as N) Yes Phosphorus Total as P Orthophosphate Al - Aluminum a ug/L Chromium: Total mg/L Cu - Copper mg/L Fe - Iron mg/L Hg - Mercury uMhos K- Potassium mg/L Mg - Magnesium mg/L Mn - Manganese n/a No and field acidified N/A mg/L N/A mg/L N/A mg/L N/A mg/L N/ ' g N/A .V/A N/A •. L N/A ug/L N/A mg/L N/A ug/L N/A ug/L N/A mg/L N/A mg/L N/A ug/L Yes n/a No ) Ni - Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen tiller A N/A N/A N/A fy Compounds and Concentration Units) Se- Selenium Sodium Organics: (GC. GC/MS. HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC : method# method# method# N/A N/A N/A N/A N/A ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L X (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the Laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE. GW-59 Rev 4/98 Mark D. Johnson, General Manager Permittee (Qf Authorized Agent) Name and Title - Please type or grin Signature o%Permittee (or Authorized Agent) .514 ( te) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT;FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled Mail Original and 1 copy to: PERMIT #: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED 'DEPARTMENT OF ENViRON11iJENT:&NAT13R14L.RESOLIRCES' DIVISION OF WATER RESOURCES•INFORMATlQN:P.R. QCESS. iNCa UNIT 1617 MAIL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: (9t9) 807-6306 WI0700012 EXPIRATION DATE: UIC X 01/31/18 18 Well Identification Number (from Permit): SWW-6 Well Depth: 26.00 ft. Well Diamter: 4 inch Screened Interval: 22.25 ft. to 24.62 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 2.58 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery X Remediation : Land Application of Sludge Water Source Heat Pump N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC. Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 4/23/2018 4/23/2018 to 4/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered Yes COD N/A mg/L Nitrite (NO2 as N) Coliform: MF Fecal N/A /100mL Nitrate (NO3 as N) Coliform: MF Total N/A /100mL Phosphorus: Total as (Note Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total • N/A wig/L Al - Alumin pH (when analyzed) TOC am Chloride N/A mg/L Cd- i :dmium Arsenic N/A ug/L Chromium: Total Grease and Oils N/A mg/L Cu - Copper Phenol N/A mg/L Fe - Iron Sulfate N/A mg/L Hg - Mercury Specific Conductance N/A uMhos K- Potassium n/a No N/A N/A N/A N/A Total Ammonia N/A mg/L Mg - Magnesium TKN as N N/A mg/L Mn - Manganese N/A N/A N/A N/A N/A N/A N/A N/A and field acidified mg/L mg/L mg/L mg/L m•/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L AA Yes Ni - Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen n/a No) N/A ug/L N/A ug/L N/A ug/L mg/L Specify Compounds and Concentration Units) Ag - Silv Se- Selenium Sodium Organics: (GC, GC/MS. (Specify test method #. Report attached? Yes VOC N/A mg/L N/A ug/L N/A ug/L N/A ug/L N/A ug/L HPLC) Attach lab report.) (1) No X (2) • method# method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 4/98 Mark D. Johnson, General Manager Permittee Signature o A thorized Agent) Name and Title - Please type or rint Permittee (or Authorized Agent) (Dat ) GROUNDWATER QUALITY MONITORING:. COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): SWW-7 Well Depth: 29.50 ft. Well Diamter: 4 inch Screened Interval: 25.17 ft. to 27.50 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is 3.00 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Mail Original and 1 copy to: PERMIT #: Non -Discharge NPDES DEPiCk! .. ENT QFENVlRONMENT1& NATURAL RESOURCES 11 DiVI$IQNt WATER RESOURCES INFORMATION PRC3CESSJNG UNIT 1617 MAILSERVICE CENTER RALEIGH, NC 27626-1617 Phone: (919) 807.6306 W10700012 EXPIRATION DATE: UIC X 01/31/18 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Water Source Heat Pump N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 4/23/2018 4/23/2018 to 4/23/2018 PCS PHOSPHATE Certification No(s) 330 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A mg/L Nitrite (NO2 as N) N/A /100mL Nitrate (NO3 as N) N/A /100mL (Note Use MPN method for h Dissolved Solids: Total pH (when analyzed) id samples) A m ti A Yes Phosphorus. Total as P Orthophos. .te 7 TOC w/A m �`t Chloride N/A mg/L Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A ug/L N/A mg/L N/A mg/L N/A mg/L N/A uMhos N/A mg/L N/A mg/L Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K- Potassium Mg - Magnesium Mn - Manganese n/a No N/A N/A N/A and field acidified Yes mg/L Ni - Nickel mg/L mg/L mg/L N/A ug/L N/A ug/L N/A mg/L N/A ug/L NIA ug/L N/A mg/L N/A mg/L N/A ug/L A Pb - Lead Zn - Zinc n/a No) N/A N/A N/A onia Nitrogen Id MI Ag - Silver pounds and Concentration Units) Se- Selenium Sodium Organics: (GC, GC/MS. (Specify test method #. Report attached? Yes VOC N/A N/A N/A N/A N/A HPLC) Attach lab report.) (1) No method# method# method# ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L X (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE. GW-59 Rev 4/98 Mark D. Johnson, General Manager Permittee '�r Signature thorized Agent) Name and Title - Please type o print f Permittee (or Authorized Agent) (D te) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail Original and 1 copy to: DEPARTMENT OF ENVIROSNANENT &%IATt1RlAi RESOURCES DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: (919) 807-6306 FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Mean p.m, PERMIT #: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery WI0700012 EXPIRATION DATE: UIC X 01/31/13 Well Identification Number (from Permit): CIW-7 Well Depth: 48.00 ft. Well Diamter: 4 inch Screened Interval: 31.00 ft. to 45.25 ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is N/A ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Sys ems Check One: Influent (98) Effluent (99) Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Water Source Heat Pump CONTINUOUS Field Analysis: pH 6.8 , Specific Conductance 723 uMhos Temp. 21.1 oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 4/25/2018 4/25/2018 to 5/21/2018 PCS PHOSPHATE 330 10 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered n/a Yes COD N/A mg/L Nitrite (NO2 as N) Coliform: MF Fecal Coliform: MF Total (Note Use MPN method for highly turbid samples) Dissolved Solids: Total 516 pH (when analyzed) 6.8 TOC 4.8 Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A /100mL Nitrate (NO3 as N) N/A /100mL Phosphorus Total as P Orthophosphate mg/L Al - Aluminum units Ba - Barium mg/L Ca - Calcium 25.0 mg/L Cd- Cadmium N/A ug/L Chromium: Total N/A mg/L Cu - Copper N/A mg/L Fe - Iron 40.2 mg/L Hg - Mercury N/A uMhos K- Potassium N/A mg/L Mg - Magnesium N/A mg/L Mn - Manganese No and field acidified N/A mg/L N/A mg/L 0.920 mg/L N/A mg/L N/A mg/L N/A ug/L N/A mg/L N/A ug/L N/A ug/L N/A mg/L N/A ug/L N/A ug/L N/A mg/L N/A mg/L 0.013 mg/L Yes n/a No ) Ni - Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen N/A N/A N/A Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium 0.56 N/A N/A N/A Sodium N/A Organics: (GC. GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC method# method# method# ug/L ug/L ug/L mg/L mg/L ug/L ug/L ug/L ug/L I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 4/98 Mark D. Johnson, General Manager Permi e (5f A thorized Agent) Name and Title - Please type or prin Signature Permittee (or Authorized Agent) ( te) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled Mail Original and 1 copy to: PERMIT #: Non -Discharge NPDES DEPARTMENT OF ENVIRON11M NT:&t'IATURAl RESOURCES DIOSION:Of WATER RESOt;IRCES•I►i1FORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER RALEIGH, NC 27626-1617 Phone: (919) 807406 WI0700012 EXPIRATION DATE: UIC X 01/31/18 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : 18 Well Identification Number (from Permit): MWTF1-CR Well Depth: 42.00 ft. Well Diamter: 2 inch Screened Interval: 38.70 ft. to 40.70 ft. Depth to Water Level: 11.08 ft. below measuring point. Measuring Point is 3.95 ft above land surface. MILILITERS of water pumped/bailed before sampling: Field Analysis: pH 6.8 , Specific Conductance 745 uMhos For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Rotary Distributor Land Application of Sludge Other Water Source Heat Pump 2200 Temp. 24.2 oC, Odor NONE Appearance: CLEAR Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 4/25/2018 4/25/2018 to 5/21/2018 PCS PHOSPHATE 330 10 If WELL WAS DRY at time of sampling, check here: PARAMETERS: (Samples for metals were collected unfiltered In/a COD N/A mg/L Nitrite (NO2 as N) Coliform: MF Fecal N/A /100mL Nitrate (NO3 as N) Yes Coliform: MF Total N/A /100mL Phosphorus: Total as P (Note Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total 512 mg/L Al - Aluminum pH (when analyzed) 6.7 units Ba - Barium TOC 4.3 mg/L Ca - Calcium Chloride 29.0 mg/L Cd- Cadmium Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A ug/L Chromium: Total N/A mg/L Cu - Copper N/A mg/L Fe - Iron 35.9 mg/L Hg - Mercury N/A uMhos K- Potassium N/A mg/L Mg - Magnesium N/A mg/L Mn - Manganese No N/A N/A 1.060 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 0.039 and field acidified Yes n/a No ) mg/L Ni - Nickel N/A ug/L mg/L Pb - Lead N/A ug/L mg/L Zn - Zinc N/A ug/L mg/L Ammonia Nitrogen mg/L mg/L Other (Specify Compounds and Concentration Units) ug/L Fluoride 0.45 mg/L mg/L MIBK N/A ug/L ug/L Ag - Silver N/A ug/L ug/L Se- Selenium N/A ug/L mg/L Sodium N/A ug/L uglL Organics: (GC, GC/MS, HPLC) ug/L (Specify test method #. Attach lab report.) mg/L Report attached? Yes (1) No X (2) mg/L VOC method# mg/L method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 4,98 Mark D. Johnson, General Manager Permit(o Signature of Authorized Agent) Name and Title - Please type pr prin ermittee (or Authorized Agent) t ( ate) PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR THE INJECTION AND WITHDRAWAL WATER WELLS February 2018 — April 2018 The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north side of the Tank Farm Area. Iniection Water Well System The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system during the period. The unusually cold weather experienced in January 2018 resulted in damage to the injection water supply from the DPW system. Extensive repairs were required resulting in the injection water supply remaining down from January 15, 2018 until March 5, 2018. Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs Department. The total monthly and quarterly volumes of water injected as well as the month end water level in the Water Level Control Tank are: DPW WATER GALLONS TOTAL GALLONS AVERAGE GPM TANK LEVEL FEET, MSL February 0 0 0 0 15.0 March 173,280 0 173,280 8.6 15.0 April 246,352 0 246,352 12.2 15.0 TOTALS 419,632 0 419,632 1 Effective January 1, 2018, PCS Phosphate Company, Inc. is an indirect subsidiary of Nutrien Ltd. PCS Phosphate Company, Inc. remains the legal operating entity and permittee. 3 Withdrawal Well System The withdrawal water well pumps are monitored daily by the area Maintenance Department and preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water volumes for the period are: SAND FORMATION GALLONS CROATAN FORMATION GALLONS TOTAL GALLONS AVERAGE GPM February 1,429,927 1,204,873 2,634,800 65.3 March 1,616,492 1,510,984 3,127,476 74.9 April 1,639,676 1,780,172 3,419,848 79.2 TOTALS 4,686,095 4,496,029 9,182,124 Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning, and troubleshooting on individual pumps in the system were experienced. Details of these activities are: Confined Sand Formation Withdrawal Well (SWW) Pumps SWW-1: SWW-2: SWW-3: SWW-4: SWW-5: SWW-6: SWW-7: 1 Effective January 1, 2018, PCS Phosphate Company, Inc. is an indirect subsidiary of Nutrien Ltd. PCS Phosphate Company, Inc. remains the legal operating entity and permittee. 4 Croatan Formation Withdrawal Well (CWW) Pumps CWW-1: CWW-2: CWW-3: CWW-4: CWW-5: CWW-6: CWW-7: 1 Effective January 1, 2018, PCS Phosphate Company, Inc. is an indirect subsidiary of Nutrien Ltd. PCS Phosphate Company, Inc. remains the legal operating entity and permittee. 5