WI0700012_Monitoring (Report)_20060509

•
PCS �
Phosphate
AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
May 9, 2006
Evan O. Kane
1636 Mail Service Center
Raleigh, North Carolina, 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
February 2006 — April 2006
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Evan:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) piezometer level
monitoring field sheet, and d) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
4.CctAIAROC it144:Z—•L•04
D. Daniel Winstead I11
Environmental Engineer
PCS Phosphate
Attachments
ul c>

pc: Will Hart— Aquifer Protection DWQ, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
W. A. Schimming (w/ attachments)
Total Two Copies Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
E-Mail: M. D. Johnson
Nubia Guzman
R. B. Lee
H:\Reports\2006\Quarterly\TFRAS Report Second Quarter 2006.doc
2

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter:
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level:
Measuring Point is
4 inch
N/A ft. below measuring point.
N/A ft above land surface.
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: N/A
Field Analysis: pH 6.9 , Specific Conductance 589 uMhos
Temp. 17.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/5/06
4/5/06 to 4/27/06
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples
for metals were collected unfiltered X Yes
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total 1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 444
pH (when analyzed) 7.1
TOC 5.5
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
19.0
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/l
units
mg/l
mg/l
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified X
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
0.022 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
<0.001 ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.008 ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.56
N/A
N/A
N/A
N/A
N/A ug/I VOC
0.017 ug/I
: method#
: method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/l
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
mite. (o Authorized Agent Name and Title - Please type or pr t
1(:( )/ 1/ rs 5
Signature of Permittee (or Aut orized Agent) D )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 10.25 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling: 2100
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
Field Analysis: pH 7.2 , Specific Conductance 655 uMhos
Temp. 20.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/06
Date sample analyzed: 4/5/06 to 4/27/06
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples
COD
Coliform: MF Fecal
Coliform: MF Total
for metals were collected
N/A
N/A
<1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 464
pH (when analyzed) 6.9
TOC
Chloride
Arsenic
mg/I
/100m1
/100m1
mg/I
units
5.3 mg/I
18.2 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
<10.0 mg/1
N/A uMhos
N/A mg/I
N/A mg/I
unfiltered X Yes
No and field acidified X Yes No )
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 0.635 mg/1
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
<0.001 ug/I
0.016 ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
0.058 ug/l
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.44
N/A
N/A
N/A
N/A
VOC method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Srr}ith - Manager, Environmental Affairs
Pmrn it�e) (of Authorized Agent) Na a and Title - Please type or pri t
,ff /4-4 A4 . r 5 5D
Signature of Permittee (or Autho zed Agent) (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter:
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level:
Measuring Point is
4 inch
5.11 ft. below measuring point.
2.25 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2284 uMhos
Temp. 19.1 oC, Odor NONE Appearance: LT RUST
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15108
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06
4/4/06 to 4/27/06
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2024
pH (when analyzed) 6.3
TOC 9.2
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
73.0
N/A
N/A
N/A
733.4
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
16.250 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
Yes n/a No )
N/A ug/I
NIA ug/I
N/A ug/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
0.24
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
method#
N/A ug/I VOC
N/A ug/I
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ugi
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
ermittee (of Authorized Agent) Name and Title - Please type or print
e
Signature of Permittee (or Au horized Agent)
S /0 O(c
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 52.15 ft. Well Diamter:
CWW-2
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level:
Measuring Point is
4 inch
5.04 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2471 uMhos
Temp. 19.9 oC, Odor NONE
Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to 4/27/06
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Dissolved Solids: Total 2136 mg/I
pH (when analyzed) 6.3 units
TOC 11.5 mg/I
Chloride
Arsenic N/A mg/I
Grease and Oils N/A mg/I
76.3 mg/I
Phenol
Sulfate 822.0 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
11.750 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.20
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC method#
method#
method#
N/A ug/I
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
kisis 6-4,
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-3
Screened Interval: 36.42 ft. to 50.67 ft.
4 inch
Depth to Water Level: 5.39 ft. below measuring point.
Measuring Point is 3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINOUS
Field Analysis: pH 6.1 , Specific Conductance 2425 uMhos
Temp. 21.9 oC, Odor NONE
Appearance: CLEAR
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
4/4/06 to 4/27/06
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2120
pH (when analyzed)
TOC
Chloride
Arsenic
mg/l Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
6.3 units Ba - Barium
9.9 mg/1 Ca - Calcium
70.5 mg/l Cd- Cadmium
No and field acidified
N/A mg/I Ni - Nickel
16.550 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
Yes n/a No )
N/A ug/I Fluoride
N/A ug/l MIBK
N/A ug/I Ag - Silver
N/A mg/1 Chromium: Total
Grease and Oils
Phenol
Sulfate
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
791.2 mg/I Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos K- Potassium
N/A ug/I
N/A ug/I
N/A mg/I Mg - Magnesium
N/A mg/l Mn - Manganese
Se- Selenium
Sodium
N/A
N/A
N/A
0.16
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC. GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC
N/A ug/I
method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Auth sized Agent) Name and Title - Please type or print
166 k�v 2/Yjs 6— /0 /40G
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level:
Measuring Point is
4 inch
4.27 ft. below measuring point.
2.75 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2735 uMhos
Temp. 23.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06
4/4/06 to 4/27/06
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2348
pH (when analyzed) 6.3
TOC 8.4
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
90.3
N/A
N/A
N/A
896.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/l
mg/I
mg/I
mg/1
mg/1
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
11.000 mg/I
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/l
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Se- Selenium
Sodium
0.12
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/1
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC
N/A ug/I
: method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am awa
false information, including the possibility of fines and imprisonment for knowing violations.
and complete, and that the laboratory analytical data was produced
re that there are significant penalties for submitting
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
/.08 0. 1��-. r /i S SJ 0/O�
Signature o ermi tee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-5
Well Depth: 53.17 ft. Well Diamter: 4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level: 6.59 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2385 uMhos
Temp. 28.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor
Other
Remediation: Infiltration Gallery
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06
4/4/06 to 4/27/06
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1724
6.4
6.9
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
77.6
N/A
N/A
N/A
625.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
unfiltered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified _
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
10.500 mg/I Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
0.15
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A _ ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC
N/A ug/I
: method#
: method#
method#
ug/I
ug/l
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. 1 am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
RMS s/,o/
Signature of Permittee (or u horized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-6
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level:
Measuring Point is
7.28 ft. below measuring point.
2.92 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2272 uMhos
Temp. 30.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06
4/4/06 to 4/27/06
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
turbid samples)
1520
6.4
10.0
95.0
Arsenic
Grease and Oils
Phenol
Sulfate
mg/I
/100m1
/100m1
Yes n/a No and field acidified
Yes n/a No )
Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A
Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A
Phosphorus: Total as P 15.750 mg/I Zn - Zinc N/A
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
492.9 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A ug/I Se- Selenium
N/A ug/I Sodium
0.17
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/1 Report attached? Yes (1) No X
N/A ug/I VOC : method#
N/A ug/I
: method#
method#
ug/I
ug/I
ug/I
ug/I
mg/1
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of AuVrized Agent) Name and Title - Please type or print
2i is 6116 06
Signature of Permittee (or Authorized Agent) ! (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-7
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level:
Measuring Point is
4.38 ft. below measuring point.
1.25 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 1182 uMhos
Temp. 23.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to 4/27/06
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
852 mg/I Al - Aluminum
6.5 units Ba - Barium
5.7 mg/I Ca - Calcium
Chloride
Arsenic
54.7 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/1 Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
188.8 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/l Mn - Manganese
No and field acidified
N/A
N/A
5.300
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/1
mg/I Ammonia Nitrogen
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/l
ug/I
ug/l
ug/I VOC
ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes nla No )
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.18
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
method#
: method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of uthoriizzeedAgent) Name and tTiittle - Please type or print
print
4.4. ,......14.1cot 1 't5 s!'0 AG
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO.. INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
Screened Interval: 18.30 ft. to 21.12 ft.
4 inch
Depth to Water Level: 7.07 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
X
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1440 uMhos
Temp. 18.6 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to 4/27/06
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
mg/I
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
1124 mg/I Al - Aluminum
6.0 units Ba - Barium
5.9 mg/I Ca - Calcium
Chloride
Arsenic
75.2 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I
125.500 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
Yes n/a No )
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
245.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
N/A
0.69
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No
N/A ug/I VOC
N/A ug/I
method#
method#
method#
ug/I
ug/I
ug/I
u g/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permit e (of Authorized Agent) Name and Title - Please type or print
/6to
_ hi ` 4, R AS 5/40 o /0
Signature of Permittee (or Authorized Agent) Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 7.94 ft. below measuring point.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1859 uMhos
Temp. 19.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01115/08
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to 4/27/06
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified Yes nla No )
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A ug/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A ug/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 80.000 mg/I Zn - Zinc N/A ug/I
(Note Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen ug/I
Dissolved Solids: Total 1316 mg/I Al - Aluminum N/A ug/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) 6.3 units Ba - Barium N/A ug/1 Fluoride 0.18 mg/I
TOC 7.8 mg/I Ca - Calcium N/A ug/I MIBK N/A ug/I
Chloride 55.1 mg/I Cd- Cadmium N/A ug/I Ag - Silver N/A ug/I
Arsenic N/A mg/I Chromium: Total N/A ug/I Se- Selenium N/A ug/I
Grease and Oils N/A mg/I Cu - Copper N/A ug/I Sodium N/A ug/I
N/A mg/I Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC)
414.8 mg/I Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A ug/l Report attached? Yes (1) No X (2)
N/A mg/I Mg - Magnesium N/A ug/I VOC method#
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Mn - Manganese N/A ug/I method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Perm tee (of uthquzed Agent) Name and Title - Please type or print
Qt ‘ tefflS S�o/ 0
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO.. INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter:
Screened Interval: 20.17 ft. to 23.00 ft.
4 inch
Depth to Water Level: 8.36 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 1787 uMhos
Temp. 19,8 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to 4/27/06
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1376
6.3
7.0 mg/I Ca - Calcium
mg/I
/100m1
/100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
37.2 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
485.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Yes n/a
No and field acidified
N/A
N/A
P 69.000
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/1
mg/I
mg/I
ug/l
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.10
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC
method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
u g/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permitteemin'(of Authorized Agent) Name and - Please type or print
NU IV at K/ �! 5 5/
Signature of Permittee (or Authorized Agent)
'O (o
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
Telephone: [phone]
No. of Wells to be Sampled
18
doom, en
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter:
4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 6.45 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 5.7 , Specific Conductance 2203 uMhos
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Temp. 27.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06
4/4/06 to 4/27/06
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1 Nitrate (NO3 as N)
No and field
acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
1680 mg/I Al - Aluminum
5.9 units Ba - Barium
7.9 mg/I Ca - Calcium
Chloride
Arsenic
34.2 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
220.000 mg/I Zn - Zinc
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A mg/1 Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
590.7 mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.21
NIA
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC
N/A ug/I
method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 28.21 ft. Well Diamter:
SWW-5
Screened Interval: 24.83 ft. to 27.21 ft.
4 inch
Depth to Water Level: 7.87 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2524 uMhos
Temp. 27 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to 4/27/06
Laboratory Name:
Certification No(s) 330 10
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1568 mg/I
pH (when analyzed) 6.2 units
TOC 11.3 mg/I
Chloride
Arsenic
40.0 mg/l
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
739.9 mg/I Hg - Mercury
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/l
51.000 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
Yes n/a No )
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/l Se- Selenium
N/A ug/l Sodium
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.41
N/A
N/A
N/A
N/A
NIA ug/I Organics: (GC. GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach
N/A ug/l Report attached? Yes (1) No
N/A ug/I
N/A ug/I
VOC : method#
method#
method#
lab report.)
X
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
". rmittee (of AyJthorized Agent) Name and Title - Please type or print
ICJAD.YV . -for km S 5/o OG
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.16 ft. below measuring point.
2.58 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 3374 uMhos
Temp. 27.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06
4/4/06 to 4/27/06
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Use MPN method for highly turbid samples)
2440
6.2
14.5
76.5
N/A
N/A
N/A
1194.0
N/A
N/A
N/A
mg/I
units
mg/l
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
unfiltered
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
No and field
acidified Yes n/a No )
N/A mg/I Ni - Nickel
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
29.000 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/l
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
0.08
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authoriz Agent) Name and Title - Please type or print
4/6 PM3
Signatu e of Permi ee (or Au horized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter:
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 5.7 , Specific Conductance
4 inch
7.52 ft. below measuring point.
Temp. 22.9 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
753 uMhos
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06
4/4/06 to 4/27/06
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Dissolved Solids: Total 572 mg/I
pH (when analyzed) 5.8 units
TOC 7.0 mg/I
Chloride
Arsenic
45.4 mg/I
Grease and Oils
Phenol
Sulfate 100.4 mg/I
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
Yes n/a
No and field acidified Yes n/a No )
Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A
Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A
Phosphorus: Total as P 44.750 mg/I Zn - Zinc N/A
Orthophosphate N/A mg/I Ammonia Nitrogen
Al - Aluminum N/A ug/I Other (Specify Compounds and Concentration Units)
Ba - Barium N/A ug/1 Fluoride 0.13
Ca - Calcium N/A ug/I MIBK N/A
Cd- Cadmium N/A ug/I Ag - Silver N/A
Chromium: Total N/A ug/I Se- Selenium N/A
Cu - Copper N/A ug/I Sodium N/A
N/A ug/l Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
Fe - Iron
Hg - Mercury
N/A uMhos K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
N/A ug/I : method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and completeand that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of A thorized Agent) Name and Title - Please type or print
,.l�, ,t�� kris c/o/ G
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 6.40 ft. Well Diamter:
MWTF1-A
2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.72 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.5 , Specific Conductance
Temp. 18 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2000
660 uMhos
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01 /15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/06
Date sample analyzed: 4/5/06 to 4/27/06
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
480
6.8
4.7
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
10.1
N/A
N/A
N/A
28.2
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
0.248 mg/l
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
Yes n/a No )
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/l Sodium
N/A ug/i Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A
N/A
N/A
1.62
N/A
N/A
N/A
N/A
N/A ug/l VOC
N/A ug/I
method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
-Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
MWTF1-B
Well Depth: 13.50 ft. Well Diamter: 2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 4.88 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 5.6 , Specific Conductance 363 uMhos
Temp. 19.5 oC, Odor NONE Appearance:
LT YELLOW
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/06
Date sample analyzed: 4/5/06 to 4/27/06
Laboratory Name:
Certification No(s) 330 10
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n!a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Dissolved Solids: Total 264 mg/I
pH (when analyzed) 5.7 units
TOC 3.2 mg/I
Chloride
Arsenic N/A mg/1
54.1 mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium _
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
18.3 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A
N/A
3.850
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I Ni - Nickel
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Yes nla No )
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.21
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
W . 2/Y1 S SA�
Signature of Permittee (or Authorized Agent) (Date)

1
PCS Phosphate Co., Inc
Date: y-hOo Y%lP
Time:
Tech:
-WaL.
System Gauge Pressures
SWW-1
•` tem ,
�/
o p/Tt,4
SWW-7
9
//
CW W-1
1
//
CW W-7
A
//
Tank Farm Remediation Sy' •m Quarterly Monitoring
File: 12-07-02
pc TL9
Reference
Pat AISL
La S Rel
to Mt
Ditch
12.91
Reza
Barge Slip
10.69
bag
Water Level
Control Tank
%c MSL
Sand Layer Pelzometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft
Spz-1
10.47
//
7 V
I o,OZ
Cpz-1
10.51
/0.05-
0. 4%�
Spz-2
1121
,Se
a.83
Cpz-2
1025.
/0- 90
-D. 6.5-
Spz3
11.87
&' 0
9 o 7
Cpz-3
11.12
9/7/
/ i//
Spz-4
11.45
CO, 9'
*C 3
CPW
9.65
/�O/./0
- 0 S
Spz-5
11.45
9Sa---
a./3
MWTF-1A•
14.35
H•/%R
9la3
Spz-6
11.23
9.1572
/ 7/
MWTF-18•
14.36
y.BB
9, 5/8'
Spz-7
11.59
8
9,7'
/,//%s
MWTF-1C•
14.44
/o.oir
4 %9
Spz-8
11.57
(a, 98
/-,J`-9
MWTF-2A
14.05
4, Aso
7, 55-
Spz-9
11.01
8 `SSA
o�•OG
MWTF-28
14.02
//9,2
a/0
Spz-10
12.16
O%. 98
./hS
MWTF-2C
14.08
/�i/..96
-O %O
sPW
9.95
775/
�C : •cif
c/
MWTF-3A
1221
OPo?
�. . 9
MWTF-3B
12.18
/©,/6
6% 03
MWTF3C
12.19
/0 �,3
- /,&Y
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Ste
Wtr
Level Ft.
Pump
Activation Depth
Rel MSL
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping?
(`�esl(N,o
Comments
SWW-i
10.70
7, o7
c
/ 07
+1'to+2'
7/
fl�j
cwW-1
10.60
1'j ///
9' 9'
-Sg9
-2'to-1'
t"GS
SWW-2
9.99
- 797
6'
/ 9/
+1'to+2'
l
cWW-2
10.23
Cr, oy
9
-3, 9�
-2'to-1•
�/
SWW3
9.97
c, •9
5
0?�j36
+1'to+2'
l
CWw3
9.95
5:39
9
-1/4.9 /
-2'to-1'
s
SWW4
ion
6.
9
0 «3
+1 'to+2'
CWW-4
10.73
7.97
9'
- 4./73
-2'to-1'
G
SwW-5
10.80
7 Y7
6
/ 87
+1 ' to+2'
CWW-5
10.74
6•,%
9
-0c.,//
-2'to-1'
SWW3
10.66
/�
5
/th/p
+1'to+2'S
CWW-6
9.92
�/77
//616
9'
-/ 7R
-2'to-1'
tlf
SWW-7
10.70
6
6'
+1 • to +2'
�Pii
/.sa
CWW-7
9.95
��,a
'7/ 3p
9'
3'S 7
-2'to-1'
/*•
Revised 729/02
• Riser length added to TOC elevation 124197
DADatalFonns well Fonn\Tank Farm Remed Wellsads

SPZ
sPZ-1 ,a
CPZe1 a
OFFICE
CUT—OFF WALL
CP2-2
SPZ-2 0
SVM4
CWw-2
UWTF-2
CLUSTER
1 DRAINAGE DITCH
ASPHALT ROAD ccvars
5n4CWW4
SPZ-6 SPZ-7
VITMORAWAL WELL
FLOWTOTAAmR$
AND CONTROL VALVES OOS
CP2-3 if
SPZ-9 ,(
PIPERACK SPILL CONTAINMENT PAD
WATER LEVEL
CONTROL TANK
cnv ijo 01
MWTF4
CLUSTER
CP7l-6 _ CIW-T
'0
SPZ-10
002
004
_.J
nl„t
I I NI NO
::YMIIUI All YI Mr I II N
AM lid AN rI•
• •.wrr..n w11r
• ...rn.« o .4N• r..l n pnuunnwu *1"
• n...14r r.N1Yu.Nr wrn Ynl.wu Mein
. n...r.u..+r4u AIN IN Ni LA AL "Llt
L•
•1N. r.nl ILA I IN 41n ogre' .I� 11
LILAC, Id SkIII 1IVIA
LOCATION PLAN FOR TANK FARM,
AREA REMEDIAL ACTION SYS II M
WELLS AND PIEZOMETFII';
FIGURE 1

r
PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
February 2006 — April 2006
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
during the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Feb
950,629
0
950,629
23.6
15.0
March
888,890
0
888,890
19.9
15.0
April
466,368
0
466,368
10.8
15.0
TOTALS
2,305,887
0
2,305,887
H:\Reports\2006\Quarterly\TFRAS Report Second Quarter 2006.doc
3

1
Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Feb
297,820
92, 635
390,455
9.7
March
321,275
121,780
443,055
9.9
April
289,941
87,782
377,723
8.7
TOTALS
909,037
302,197
1,221,234
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
On 2/9, 2/14, 2/23, 2/28, 3/7, 3/15, 3/21, 3/31, 4/6, 4/12, 4/20 and 4/25 flushed out pumps and lines on each
of the Confined Sand Formation Withdrawal Well (SSW) and the Croatan Formation Withdrawal Well
(CWW) Pumps. On 2/7 changed oil and filters in the system air compressor.
SWW-1: On 4/18 reset counter.
SWW-2: On 3/23 changed pump. On 3/28 reset pump. On 3/29 changed pump.
SWW-3:
SWW-4: On 2/22 shook pump. On 2/24 changed pump. On 4/25 reset pump. On 4/28 changed pump.
SWW-5: On 4/11 reset pump. On 4/25 reset pump.
SWW-6: On 2/1 changed counter.
SWW-7:
H:\Reports\2006\Quarterly\TFRAS Report Second Quarter 2006.doc
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 3/1 reset pump head. On 3/16 changed pump.
CWW-2: On 2/22 reset pump head. On 3/9 changed pump.
CWW-3:
CWW-4: On 3/23 changed pump. On 4/17 changed counter.
CWW-5: On 2/6 changed pump.
CWW-6: On 4/17 reset pump.
CWW-7:
H:\Reports\2006\Quarterly\TFRAS Report Second Quarter 2006.doc
5