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HomeMy WebLinkAboutWI0700012_Monitoring (Report)_20081121GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): SWW-1 Well Depth: 22.50 ft. Well Diamter: 4 inch Screened Interval: 18.30 ft. to 21.12 ft. Depth to Water Level: Measuring Point is 4.45 ft. below measuring point. 1.52 ft above land surface. For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.3 , Specific Conductance 1541 uMhos Temp. 22.1 oC, Odor NONE Appearance: CLEAR Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 01/31/13 Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/22/2008 PCS PHOSPHATE and ENVIRONMENT 1 Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Coliform: MF Total N/A /100m1 Phosphorus: Total as P 186.500 mg/I (Note Use MPN method for highly turbid samples) Orthophosphate N/A mg/l Dissolved Solids: Total 1248 mg/I Al - Aluminum N/A ug/I pH (when analyzed) 5.8 units Ba - Barium N/A ug/I TOC 4.4 mg/I Ca - Calcium N/A ug/l 89.8 mg/I Cd- Cadmium N/A ug/I N/A mg/I Chromium: Total N/A ug/I N/A mg/I Cu - Copper N/A ug/I N/A mg/I Fe - Iron N/A ug/I 267.3 mg/I Hg - Mercury N/A ug/I N/A uMhos K- Potassium N/A ug/I N/A mg/I Mg - Magnesium N/A ug/I N/A mg/I Mn - Manganese N/A ug/I Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N No and field acidified Yes n/a No ) Ni - Nickel N/A Pb - Lead N/A Zn - Zinc N/A ug/I ug/I ug/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Fluoride 0.60 mg/I MIBK N/A ug/I Ag - Silver N/A ug/I N/A ug/I N/A ug/l Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC method# Se- Selenium Sodium method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 GEC o c: lnforrnati, RECEIVED / DENR / DWQ AQUIFER PR(ITFr.TIt1N SFCTION DEC 12 2008 Ross M. Smith - Manager, Environmental Affairs `�}+`(�tee of Authorized Agent) Name and Title - Please type or print .L. ,C.2i ems /i/2iA$ Signature of Permittee (or Authorized Agent) (Date) 003 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jack H. Taylor, Jr. County: Beaufort Well Locations/Site Name: Tank Farm Telephone: (252)322-8155 No. of Wells to be Sampled 18 Ororn Mail Original to: Well Identification Number (from Permit): SWW-2 Well Depth: 23.00 ft. Well Diamter: 4 inch Screened Interval: 18.80 ft. to 21.63 ft. Depth to Water Level: Measuring Point is 7.69 ft. below measuring point. 3.42 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 5.3 , Specific Conductance 3322 uMhos Temp. 21.4 oC, Odor NONE Appearance: CLEAR DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH. NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 EXPIRATION DATE: 01/31/13 Non -Discharge UIC X NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/22/2008 PCS PHOSPHATE and ENVIRONMENT 1 Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD N/A mg/I Nitrite (NO2 as N) Coliform: MF Fecal N/A /100m1 Coliform: MF Total N/A /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 5008 pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate 5.0 7.8 49.8 N/A N/A N/A Specific Conductance Total Ammonia TKN as N 646.6 N/A N/A N/A mg/1 units mg/I mg/I mg/l mg/I mg/I Fe - Iron mg/I Hg - Mercury uMhos mg/l mg/I Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper K- Potassium Mg - Magnesium Mn - Manganese No and field N/A mg/I Ni - Nickel N/A mg/I Pb - Lead 1265.000 mg/I Zn - Zinc acidified Yes n/a No ) N/A mg/I Ammonia Nitrogen N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I Other (Specify Compounds and Concentration Units) Fluoride MIBK N/A ug/l Ag - Silver N/A ug/I N/A ug/I Se- Selenium Sodium mg/I 0.91 mg/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X (2) N/A ug/I VOC : method# method# method# N/A ug/I I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 Ross M. Smith - Manager, Environmental Affairs e (of Aut orized Agent) Name and Title - Please type or print /t) r-r)S ///2/Signature of ermittee (or Authorized Agent) ((/(Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): SWW-3 Well Depth: 24.50 ft. Well Diamter: 4 inch Screened Interval: 20.17 ft. to 23.00 ft. Depth to Water Level: Measuring Point is 3.17 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH N/A , Specific Conductance Temp. N/A oC, Odor NONE 4.20 ft. below measuring point. For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) X N/A N/A uMhos Appearance: CLEAR PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic N/A N/A N/A N/A N/A Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A N/A N/A N/A N/A mgll /100m1 /I s K tum Nitrite (NO2 as N) Nitr. 03 as N) _ P s: Total a- hate m im Total mg/I mg/I Mg - Magnesium Mn - Manganese Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 01/31/13 Rotary Distributor Land Application of Sludge Other Yes nla No an N/A N/A N/A N/A Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 ug/I ug/I ug/I ug/I ug/I m and ntration Units) Iver eleniurr um Organics: (GC, GC/MS. HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC method# method# method# N/A N/A N/A N/A N/A N/A N/A N/A ug/I ug/I ug/I mg/I mg/I ug/I ug/I ug/I ug/I X (2) certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 El Ross M. Smith - Manager, Environmental Affairs P rmdt e (of Au orized A ent) Name and Title - Please type or print � ./2, Signature of Permittee (or Authorized Agent) (D$te) 8 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor. Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): SWW-4 4 inch For Groundwater Treatment Well Depth: 25.00 ft. Well Diamter: systems check one: Screened Interval: 20.50 ft. to 23.30 ft. Influent (98) Depth to Water Level: 6.47 ft. below measuring point. X Effluent (99) Measuring Point is 3.42 ft above land surface. GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 5.5 , Specific Conductance 3981 uMhos Temp. 31.1 oC, Odor NONE Appearance: CLEAR Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 01/31/13 Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 10/15/2008 Date sample analyzed: 10/15/2008 to 10/22/2008 Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1 Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered Yes nla No and field acidified COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Coliform: MF Total N/A /100m1 Phosphorus: Total as P 865.000 mg/I (Note Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Dissolved Solids: Total 4116 mg/l Al - Aluminum N/A ug/I pH (when analyzed) 5.3 units Ba - Barium N/A ug/I TOC 8.5 mg/I Ca - Calcium N/A ug/I Chloride 42.9 mg/I Cd- Cadmium N/A ug/I Arsenic N/A mg/I Chromium: Total N/A ug/I Se- Selenium Grease and Oils N/A mg/I Cu - Copper N/A ug/I Sodium Phenol N/A mg/I Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC) Sulfate 810.0 mg/I Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.) Specific Conductance Total Ammonia TKN as N N/A uMhos K- Potassium N/A ug/I Report attached? Yes (1) No N/A mg/I Mg - Magnesium N/A ug/I VOC method# N/A mg/I Mn - Manganese N/A ug/I method# method# Yes nla No ) N/A ug/I Pb - Lead N/A ug/I Zn - Zinc N/A ug/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Fluoride 0.09 mg/I MIBK N/A ug/I Ag - Silver N/A ug/I N/A ug/I N/A ug/1 X (2) I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 Ross M. Smith - Manager, Environmental Affairs P rmi e (of A%'thorized gent) Name and Title - Please type or print W Cvr MS "/Z/D Signature of Permittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): SWW-5 Well Depth: 28.21 ft. Well Diamter: 4 inch Screened Interval: 24.83 ft. to 27.21 ft. Depth to Water Level: 0.33 ft. below measuring point. For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) Measuring Point is 2.96 ft above land surface. GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.3 , Specific Conductance 2510 uMhos Temp. 28.5 oC, Odor NONE Appearance: CLEAR Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 01/31/13 Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/22/2008 PCS PHOSPHATE and ENVIRONMENT 1 Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD N/A mg/I Nitrite (NO2 as N) Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) Coliform: MF Total N/A /100m1 Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total 1744 mg/1 Al - Aluminum pH (when analyzed) 6.0 units Ba - Barium TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N 7.2 mg/I Ca - Calcium 44.9 mg/I N/A mg/I N/A mg/I Cd- Cadmium Chromium: Total Cu - Copper N/A mg/I Fe - Iron 709.5 mg/I Hg - Mercury N/A uMhos K- Potassium N/A mg/I Mg - Magnesium N/A mg/1 Mn - Manganese 371.000 mg/I N/A mg/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/1 No and field acidified N/A mg/I Ni - Nickel N/A mg/I Pb - Lead Zn - Zinc Yes n/a No ) N/A N/A N/A Ammonia Nitrogen Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium Sodium 0.29 N/A N/A N/A N/A N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No N/A ug/I N/A ug/l VOC method# method# method# ug/I ug/I ug/I mg/I mg/I ug/I ug/I ug/I ug/l (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 GEC 0 I 2Gj Information processing Unit D WQ/BOG Ross M. Smith - Manager, Environmental Affairs rmit]op (of Aujhorized Agent) Name and Tittle - Please type or print Signature of Permittee (or Authorefit Agent) Z r+f L/YI> / C/2( 09 (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): SWW-6 Well Depth: 26.00 ft. Well Diamter: Screened Interval: 22.25 ft. to 24.62 ft. Depth to Water Level: Measuring Point is 2.58 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH N/A , Specific Conductance Temp. N/A oC, Odor NONE 4 inch 6.14 ft. below measuring point. PARAMETERS: (Samples for metals were collected COD N/A mg/I Coliform: MF Fecal N/A /100m1 Coliform: MF Total N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A N/A N/A N/A N/A N/A N/A N/A NIA N/A For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) N/A N/A uMhos Appearance: CLEAR unfiltered Nitrite (NO2 as N) Nitr - 03 as N) s: Total a Yes n/a Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 01/31/13 Rotary Distributor Land Application of Sludge Other No an ry NIA sium mg/I Mg - Magnesium N/F mg/I Mn - Manganese Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 Iver eleniu tum N/A N/A N/A N/A N/A tgll Organics: (GC, GC/MS, HPLC) ug/I (Specify test method #. Attach lab report.) ug/I Report attached? Yes (1) No X ug/I VOC : method# ug/I : method# method# ug/I ug/I ug/I mg/I mg/I ugll ug/I ug/I ug/l (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 Ross M. Smith - Manager, Environmental Affairs Per itteg (o Authoriz d Agen Name and Title - Please type or pint �jU, h/ -C>r 112i►1S HA( Signature of Permittee (or Authorized Agent) (Date) DEC 01 2CC3 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): SWW-7 Well Depth: 29.50 ft. Well Diamter: 4 inch Screened Interval: 25.17 ft. to 27.50 ft. Depth to Water Level: Measuring Point is 6.90 ft. below measuring point. 3.00 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH NIA , Specific Conductance Temp. N/A oC, Odor NONE For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) N/A NIA uMhos Appearance: CLEAR PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note. Use MPN method for highly turbid samples) Dissolved Solids: Total N/A pH (when analyzed) N/A TOC N/A Chloride N/A Arsenic N/A Grease and Oils N/A Phenol N/A Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A mg/I Nitrite (NO2 as N) /100m1 Nitr- - 03 as N) N/A mg/I N/A mg/I ssium Mg - Magnesium Mn - Manganese Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery EXPIRATION DATE: UIC X 01 /31 /13 Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Yes n/a No an Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 ug/t N/A ug/I N/A ug/I N/A ug/l N/A ug/I ug/I N/A ug/I ug/I mg/I mg/I ug/I ug/I ug/I ug/I Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC : method# method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurateand complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 3/2000 Ross M. Smith - Manager, Environmental Affairs Perm ee (of Authorize Agent) Name and Title - Please type or p int p.A h% - .'r Qm5 11/Zr Signature of Permittee (or Authorized Agent) (Date) tnf GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 1, perms) Well Identification Number (from Permit): MWTF1-A Well Depth: 6.40 ft. Well Diamter: 2 inch Screened Interval: 3.40 ft. to 5.40 ft. Depth to Water Level: Measuring Point is 5,10 ft. below measuring point. 3.86 ft above land surface. MILILITERS of water pumped/bailed before sampling: Field Analysis: pH 6.5 , Specific Conductance Temp. 24.9 oC, Odor NONE For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) 2600 2146 uMhos Appearance: CLEAR - Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation EXPIRATION DATE: UIC X 01/31/13 Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/16/2008 10/16/2008 to 10/22/2008 PCS PHOSPHATE Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD Coliform: MF Fecal Coliform: MF Total N/A mg/l N/A /100m1 N/A /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate 1280 mg/I Al - Aluminum 6.4 units Ba - Barium 10.7 mg/I Ca - Calcium 18.6 mg/I Cd- Cadmium N/A mg/I Chromium: Total N/A mg/I Cu - Copper N/A mg/I Fe - Iron 383.3 mg/I Hg - Mercury N/A uMhos K- Potassium N/A mg/I Mg - Magnesium N/A mg/I Mn - Manganese 0.520 mg/I N/A mg/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I No and field acidified N/A mg/I Ni - Nickel N/A mg/I Pb - Lead Zn - Zinc Ammonia Nitrogen Other (Specify Compounds and Concentration Units) Fluoride MIBK Yes n/a No ) Ag - Silver N/A ug/I Se- Selenium N/A ug/I Sodium N/A N/A N/A 1.24 N/A N/A N/A N/A N/A ug/l Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No N/A ug/I VOC : method# method# method# N/A ug/I ug/I ug/I ug/I mg/I mg/I ug/I ug/I ug/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 DEC 0 1 2033 Information. Processing Unit DWQ/BOG Ross M. Smith - Manager, Environmental Affairs P,Qrmittee (of Authorized Agent) Name and Title - Please type or print (Date Signature of Permittee (or Authorized Agent) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jack H. Taylor, Jr. County: Beaufort Telephone: (252)322-8155 No. of Wells to be Sampled Well Locations/Site Name: Tank Farm 18 Mail Original to: Well Identification Number (from Permit): MWTF1-B Well Depth: 13.50 ft. Well Diamter: 2 inch Screened Interval: 10.60 ft. to 12.60 ft. Depth to Water Level: 5.68 ft. below measuring point. Measuring Point is 3.86 ft above land surface. MILILITERS of water pumped/bailed before sampling: Field Analysis: pH 5.7 , Specific Conductance 433 uMhos For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) 2600 Temp. 24.8 oC, Odor NONE Appearance: CLEAR DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mal Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT#: WI0700012 EXPIRATION DATE: 01/31/13 Non -Discharge UIC X NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/16/2008 10/16/2008 to 10/22/2008 PCS PHOSPHATE and ENVIRONMENT 1 Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered COD N/A mg/I Nitrite (NO2 as N) Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) Yes n/a Coliform: MF Total N/A /100m1 Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total 260 mg/I Al - Aluminum pH (when analyzed) 5.7 units Ba - Barium TOC 2.1 mg/I Ca - Calcium Chloride 52.7 mg/I Cd- Cadmium Arsenic N/A mg/I Chromium: Total Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/I Cu - Copper N/A mg/I Fe - Iron 29.8 mg/I Hg - Mercury N/A uMhos K- Potassium N/A mg/I Mg - Magnesium N/A mg/I Mn - Manganese No and field acidified Yes n/a No ) N/A mg/I Ni - Nickel N/A ug/I N/A mg/I Pb - Lead N/A ug/I 3.700 mg/I Zn - Zinc N/A ug/I N/A mg/I Ammonia Nitrogen mg/I N/A ug/I Other (Specify Compounds and Concentration Units) N/A ug/I Fluoride 1.78 mg/I N/A ug/I MIBK N/A ug/I N/A ug/I Ag - Silver N/A ug/I N/A ug/I Se- Selenium N/A ug/I N/A ug/I Sodium N/A ug/I N/A ug/I Organics: (GC. GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X (2) N/A ug/I VOC method# N/A ug/I : method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is trueaccurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 RECEIVED DEC 0 1 2003 Information Processing Unit DWO/BOG Ross M. Smith - Manager, Environmental Affairs rmd (of A orized Agent) Na e and Title - Please type or print .t�..G�'e-o��( 'tamer iZMS Signature of Permittee (or Authorized Agent) (bate) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CIW-7 For Groundwater Treatment Well Depth: 48.00 ft. Well Diamter: Systems Check one: Screened Interval: 31.00 ft. to 45.25 ft. Influent (98) Depth to Water Level: N/A ft. below measuring point. Effluent (99) Measuring Point is N/A ft above land surface. GALLONS of water pumped/bailed before sampling: 0 Field Analysis: pH 7.1 , Specific Conductance 673 uMhos Temp. 22.3 oC, Odor NONE Appearance: CLEAR 4 inch Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge X EXPIRATION DATE: UIC X 01/31/13 NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation : Rotary Distributor Land Application of Sludge X Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 10/16/2008 Date sample analyzed: 10/16/2008 to 10/22/2008 Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1 Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered COD N/A mg/I Coliform: MF Fecal N/A /100m1 Coliform: MF Total <1.0 /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 392 mg/I pH (when analyzed) 6.8 units TOC 4.7 mg/I Chloride 19.8 mg/l Arsenic N/A mg/1 Grease and Oils N/A mg/I Phenol N/A mg/I Sulfate Specific Conductance Total Ammonia TKN as N <10.0 mg/I N/A uMhos N/A mg/I N/A mg/I Yes n/a No and field acidified Nitrite (NO2 as N) N/A mg/I Nitrate (NO3 as N) N/A mg/I Phosphorus: Total as P 0.004 mg/I Orthophosphate N/A mg/1 Al - Aluminum N/A ug/I Ba - Barium N/A ug/I Ca - Calcium N/A ug/I Cd- Cadmium <0.001 mg/I Chromium: Total <0.005 mg/I Cu - Copper N/A ug/I N/A ug/I N/A ug/I K- Potassium N/A ug/I Mg - Magnesium N/A ug/I Mn - Manganese <0.010 mg/I Fe - Iron Hg - Mercury Yes n/a No ) Ni - Nickel N/A ug/I Pb - Lead N/A ug/I Zn - Zinc N/A ug/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Fluoride 0.57 mg/I MIBK N/A ug/I N/A ug/I N/A ug/I N/A ug/I Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC : method# Ag - Silver Se- Selenium Sodium method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE GW-59 Rev 3/2000 DECa 1 207' Information Processing Unit DWQ/BOG Ross M. Smith - Manager, Environmental Affairs Rerm• ee (of uthorized Agent) Name and Title - Please type or print % . , > J. )I'Ylr$ I vWZ r / o rya Date Signature of Permittee (or Authorized Agent) g ) ( ) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): Well Depth: N/A ft. Well Diamter: Screened Interval: Depth to Water Level: Measuring Point is WLCT N/A ft. to N/A ft. N/A N/A ft. below measuring point. N/A ft above land surface. For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 7.1 , Specific Conductance 613 uMhos Temp. 18.8 oC, Odor NONE Appearance: CLEAR Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge X EXPIRATION DATE: UIC X 01/31/13 NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery Remediation : Land Application of Sludge Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 10/16/2008 10/16/2008 to 10/22/2008 PCS PHOSPHATE and ENVIRONMENT 1 330 10 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD Coliform MF Fecal Coliform: MF Total N/A N/A <1.0 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N No and field acidified mg/I Nitrite (NO2 as N) N/A mg/I /100m1 Nitrate (NO3 as N) N/A mg/l /100m1 Phosphorus: Total as P 0.007 mg/I Orthophosphate N/A mg/I 408 mg/l Al - Aluminum N/A ug/I 6.8 units Ba - Barium N/A ug/I 4.7 mg/I Ca - Calcium N/A ug/I 16.5 mg/I Cd- Cadmium <0.001 mg/I Ni - Nickel Pb - Lead Zn - Zinc Yes n/a No ) N/A ug/I N/A ug/I N/A ug/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver N/A mg/I Chromium: Total <0.005 mg/I Se- Selenium N/A mg/I Cu - Copper N/A ug/I Sodium N/A mg/I Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC) <10.0 mg/I Hg - Mercury _ N/A ug/I (Specify test method #. Attach lab report.) N/A uMhos K- Potassium N/A ug/I Report attached? Yes (1) No N/A mg/l Mg - Magnesium N/A ug/I VOC N/A mg/I Mn - Manganese <0.010 mg/I method# method# method# 0.55 mg/I N/A ug/I N/A ug/l N/A ug/I N/A ug/I X (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 Ross M. Smith - Manager, Environmental Affairs ,(P�rmi��jjee (of A horized Agent) Name and Title - Please type or print ,C/�ICJ, � �al )?MS Signature of ermdtee (or Authorized Agent) r (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jack H. Taylor, Jr. Well Locations/Site Name: Tank Farm County: Beaufort Telephone: (252)322-8155 No. of Wells to be Sampled 18 ,(torn Well Identification Number (from Permit): CWW-1 Well Depth: 55.00 ft. Well Diamter: 4 inch Screened Interval: 33.27 ft. to 52.68 ft. Depth to Water Level: 4.18 ft. below measuring point. Measuring Point is 2.25 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH N/A , Specific Conductance N/A uMhos For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) N/A Temp. N/A oC, Odor NONE Appearance: CLEAR PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note Use MPN method for highly turbid sam Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N N mg/I mg/I /100m1 m1 N/A mg/I Nitrite (NO2 as N) Nitrate (NO3 a osphorus: ophosph Aluminu Barium - Calcium Cadmium omium: T - Copper Iron Mercury Potassium Mg - Magnesium Mn - Manganese Yes n/a No Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge EXPIRATION DATE: UIC X 01/31/13 NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X Remediation : Remediation: Infiltration Gallery Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 and ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I ug/I N/A ug/I ug/I mg/I Fluo N/A mg/1 MIB _ N/A ug/I Ag - N/A ug/I Se- NIA ug/I Sodium N/A ug/I Organics: (GC. GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC method# method# method# (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 Ross M. Smith - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print /0460.. a. ..4.r A/+ZS /e/2i/OSP Signature of Permittee (or Aut orized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-2 Well Depth: 52.15 ft. Well Diamter: 4 inch Screened Interval: 30.57 ft. to 49.82 ft. Depth to Water Level: 4.99 ft. below measuring point. Measuring Point is 3.00 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR PARAMETERS: (Samples for metals were collected unfiltered COD N/A mg/I Coliform: MF Fecal N/A /100m1 Coliform: MF Total N/A J3GOm1 (Note: Use MPN method for highly turbid sa Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/1 mg/1 Nitrite (NO2 as N Nitrate (NO3 hosphorus: hophosp - Aluminu - Barium - Calcium Cadmium romium: - Copper - Iron g - Mercury K- Potassium Mg - Magnesium Mn - Manganese Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery EXPIRATION DATE: UIC X 01/31/13 Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 ug/I ug/I ug/I mg/1 N/A mg/I N/A ug/I Ag N/A ug/I Se- N/A ug/I So rum N/A ug/I ug/l Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No VOC : method# method# method# N/A ug/I N/A ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 Ross M. Smith - Manager, Environmental Affairs /� P rmitt e (of Authorized Agent) Name and Title - Please type or print .ld • iJ Zr. /2 2-.S fr/2 , /4,.:. Signature of Permittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jack H. Taylor, Jr. Well Locations/Site Name: Tank Farm County: Beaufort Telephone: (252)322-8155 No. of Wells to be Sampled 18 Mail Original to: Well Identification Number (from Permit): CWW-3 Well Depth: 53.00 ft. Well Diamter: Screened Interval: 36.42 ft. to 50.67 ft. Depth to Water Level: 4.64 ft. below measuring point. Measuring Point is 3.08 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR 4 inch For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) N/A PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note Use MPN method for highly turbid sam Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/I /100m1 ml mg/I Nitrite (NO2 as N) Nitrate (NO3 a osphorus: ophosph Aluminu Barium _ - Calcium Cadmium omium: T - Copper Iron - Mercury Potassium Mg - Magnesium Mn - Manganese Yes n/a No DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 EXPIRATION DATE: 01/31/13 Non -Discharge UIC X NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X Remediation : Remediation: Infiltration Gallery Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 and ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I MIB Ag - Se - Sodium Organics: (GC, GC/MS. HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC : method# method# method# ug/I ug/I ug/I mg/I mg/I ug/I ug/I ug/I ug/I (2) 1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 DEC 012 Ross M. Smith - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print ,.ns /q/2/ Signature of Permittee (or Authorized Agent) (Date Information Processing Unit OWr»Rnr-' GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): Well Depth: 53.00 ft. Well Diamter: CWW-4 Screened Interval: 41.67 ft. to 50.92 ft. Depth to Water Level: Measuring Point is 4 inch 3.46 ft. below measuring point. 2.75 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) N/A Field Analysis: pH N/A , Specific Conductance NIA uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total (Note: Use MPN method for highly turbid sa Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A N/A N/A N/A mg/I /100m1 Oml mg/I mg/I Nitrite (NO2 as N Nitrate (NO3 hosphorus: hophosp Aluminu - Barium - Calcium Cadmium romium: - Copper - Iron g - Mercury K- Potassium Mg - Magnesium Mn - Manganese ,Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone. (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery EXPIRATION DATE: UIC X 01 /31 /13 Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Yes n/a No an Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 IUm ug/l Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X (2) VOC : method# method# method# N/A N/A N/A N/A N/A ug/I ug/I ug/I mg/1 mg/1 ug/I ug/I ug/l ug/I N/A ug/l N/A ug/I I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 R7CEIVED DEC 0 1 2003 Information Processing Unit ntAjn,Dr,r Ross M. Smith - Manager, Environmental Affairs Per�tee (of Authorized Agent) Name and Title - Please type or print Signature of Permittee (or Authorized 4t) A ,n5 f DMZ/ GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jack H. Taylor, Jr. Well Locations/Site Name: Tank Farm County: Beaufort Telephone: (252)322-8155 No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-5 Well Depth: 53.17 ft. Well Diamter: Screened Interval: 41.75 ft. to 51.08 ft. Depth to Water Level: Measuring Point is 4 inch 5.26 ft. below measuring point. 2.58 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR PARAMETERS: (Samples for metals were collected unfiltered COD N/A mg/I Nitrite (NO2 as N Coliform: MF Fecal N/A /100m1 Nitrate (NO3 Coliform: MF Total N/A (Note Use MPN method for highly turbid sa Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/I mg/I hosphorus: hophosp Aluminu - Barium - Calcium - Cadmium romium: - Copper Iron - Mercury K- Potassium Mg - Magnesium Mn - Manganese Yes n/a Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION. GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone. (919)733-3221 PERMIT #: WI0700012 Non -Discharge EXPIRATION DATE: UIC X 01/31/13 NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X Remediation : Remediation: Infiltration Gallery Rotary Distributor Land Application of Sludge Other an Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 Sorum and Concentration Units) ugllOrganics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X (2) N/A ug/I VOC : method# N/A ug/I ug/l ug/I ug/I mg/I mg/I ug/I ug/I ug/I ug/I method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 -DIVE® Ross M. Smith - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print �inS !r Signature of Permittee (or Authorized Agent) (D te) L' E L 0 1 2003 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Mail Original to: Well Identification Number (from Permit): Well Depth: 53.00 ft. Well Diamter: CWW-6 Screened Interval: 36.62 ft. to 50.88 ft. Depth to Water Level: Measuring Point is 4 inch 5.76 ft. below measuring point. 2.92 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: }Influent (98) X Effluent (99) N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR PARAMETERS: (Samples for metals were collected unfiltered COD N/A Coliform: MF Fecal N/A Coliform: MF Total N/A (Note. Use MPN method for highly turbid sa Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/I /100m1 Oml mg/I mg/I Nitrite (NO2 as N Nitrate (NO3 hosphorus: hophosp Aluminu - Barium - Calcium - Cadmium romium: - Copper Iron g - Mercury - Potassium Mg - Magnesium Mn - Manganese Yes n/a DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION. GROUNDWATER SECTION 1636 Mail Service Center RALEIGH. NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 EXPIRATION DATE: 01/31/13 Non -Discharge UIC X NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X Remediation : Remediation: Infiltration Gallery Rotary Distributor Land Application of Sludge Other an Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 and Concentration Units) ug/I N/A ug/I ug/I mg/1 Flue N/A mg/1 MI: _ NIA ug/I Ag N/A ug/l Se- N/A ug/I So rum N/A ug/I ugtl Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X (2) N/A ug/I VOC : method# N/A ug/I : method# method# certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 Ross M. Smith - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or rint Qv»S Signature of Permittee (or Au orized Agent) ,D GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jack H. Taylor, Jr. Telephone: (252)322-8155 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-7 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 36.58 ft. to 50.83 ft. Depth to Water Level: Measuring Point is 4.08 ft. below measuring point. 1.25 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) N/A Field Analysis: pH N/A , Specific Conductance N/A uMhos Temp. N/A oC, Odor NONE Appearance: CLEAR PARAMETERS: (Samples for metals were collected unfiltered COD N/A mg/1 Coliform: MF Fecal N/A /100m1 Coliform: MF Total N/A •0ml (Note. Use MPN method for highly turbid sa Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/I mg/I Nitrite (NO2 as N Nitrate (NO3 hosphorus: hophosp Aluminu - Barium - Calcium Cadmium romium: - Copper - Iron g - Mercury K- Potassium Mg - Magnesium Mn - Manganese Yes n/a Mail Original to: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone' (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 01/31/13 Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 10/15/2008 10/15/2008 to 10/15/2008 PCS PHOSPHATE Certification No(s) 330 Sotum ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) ug/I ug/I ug/I mg/I mg/1 ug/I ug/I ug/I ug/l N/A ug/I Report attached? Yes (1) No X (2) N/A ug/I VOC method# N/A ug/I • method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate, and completeand that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 3/2000 Jul Information Processing Unit DWQ/BOG Ross M. Smith - Manager, Environmental Affairs P mi tee (• Authorized Agent) Name and Title - Please type or print Q%Y7 // Z 02 (Date) Signature of Permittee (or Authorized Agent) t Date: Time: Tech: • PCS Phosphate Co., Inc. - sTank..Farm Remediation System Quarterly Monitoring /o//o/o® System Gauge Pressures SWW-1 yio, SWW-7 /90/% CWW-1 PIA/70A CWW-7 _ [< a"- File: 12-07-02 RCTUB Reference Point IISL Level Ref to ESL Ditch 12.91 7,' Barge Slip Water Level Control Tank %=MSL 10.59 /. iv/ Sand Layer Pelzometers Level Indicators Well ID TOC Elevation MSL' TOC Ste Wtr Level' Level Relative To MSL Ft. Well ID TOC Elevation MSL' TOC Stc Wtr Level' Level Relative To MSL Ft. Spz-; 10.47 j, 9-g (O 3 Cps-1 10.51 /,1 yO -/ B9 Spz-2 1121 B.-/D/l "Se Cpz-2 10.25. //. 9i? '/(0'7 spz-3 11.87 O, sv // 33 7 cpza 11.12 2 4,SA - /Of 0 Spz-4 11.45 4.0 .2 ,J' /a CPW 9.65 /a.64% -at Oq Spz-5 11.45 9 V/ / 97 MWTF-1A• 14.35 ij /0 97'o1S ©•�O8 spz-6 11.23 /0.//ef{ a8/ W MTF-1B• 14.36 6: o Spz-7 11.59 9 9.5 / / 61 MWTF-,C• 14.44 / yogi 05c5 Spz-8 11.57 B. 33 t5ail MWTF-2A 14.05 4 . 424 /p3 Spz-9 11.01 B'® �• 8/ MWTF-2B 14.02 /Q, �� S. / I/ Spz-10 12.16 714 7/ MWTF-2C 14.08 /tp.p O -07/,2 W SP 9.95 - 775 0744 MWTF-3A 12.21 308/� 8•.23 MWTF-3B - 12.18 / 4' - 4 ^ 7 90 MWTF-3C 12.19 / 9 - - OM 5 Sand Layer And Croatan Formation Withdrawal Wells Well ID TOC Elevation MSL' Max Stc Wtr Level Ft. Pump Activation Depth Rel MSL Max Level Relative To MSL Ft. Control Point, MSL' Is Well Pumping? (1�esl(t�0 Comments SWW-1 10.70 y -7/5-- 6 -/�/.SS +1'to+2' '/C i W CW-1 10.60 /I 9' - '7. 8a -2'to-1' N� SWW-2 9.99 rr// /,./G9 e a?.3 +1'to+2' YCs CWW-2 1023 ' 44 99 9' - zi. -2'to-1' Ai0 SWW-3 9.97 //'0/%0,/ 8 00/ -1.6 +1. to+2' NO CWW3 9.95 7/'!OY 9' -7..3/O -2'W-1' A�J%'D SWW4 10.73 //g� . 2///7 9' o• H9 +1.to+2' kb CWW4 ion S- 1 6'1 9' -s. s -2'to-1' � AM SWW-5 10.80 0.59 6 - 4.7 +1'to+2' y,,e,ys CWW-5 10.74 I5'Q,/p/ 9' 3.7y -2'to-1' NO SWW-6 10.66 6./7/ e +1.to+2' NO CWW-6 9.92 .J/s74 9' .-Off./4/'/ 3.�ay I7 -2'to-1' /��290 SWW-7 10.70 A 90p s' 0 90 +1.to+2' �O CWW-7 9.95 /. O�J 9' -2/9v2- -2'to-1' A 0 Revised 7/29/02 • Riser length added to TOC elevation 1/24/97 DADataWotmslWell FonnlTankl=arm Remed Wells.fds svi SPZ-1 CPZ-1 OFFICE CUT—OFF WALL S,Mys CPZ-2 ASPHALT ROAD yap SWWJ'_ CWW-4 SPZ-2 SWW4 CWW-2 IIWTV-2 CLUSTER 1 DRAINAGE DITCH WITHDRAWAL WELL FLOWTOTALIERS AND CONTROL VALVES CPZ-3 X SPZ-D PIPERACK SPILL CONTAINMENT PAD S.P.A • PLANT WATER LEVEL CONTROL TANK MWIF1 CLUSTER CIW41001 SPW c Wi. ,SWWJ C0.2 ° 1\ 044 TWA \ r MWTFA CLUSTER - CIW6 _ CIW-T O SPZ-10 SPZ-S T 002 004 T _T J I I lil NO l:YMHUI Id I u111•WIN rands UM ▪ 1.4.001004 Win • . ..N..N,,.A.N..•,I 41411101•WAI WI II • . n..uAN...w . W.VN.AWY WI II • n.....M ..+.Y...... 04 AI 11•04 WI11 ...I.....I M...M Y.In .vl . I I.M..111 0 0•41• 10. .n.. .....11 *All n IIVII LOCATION PLAN FOR TANK. FARM; AREA REMEDIAL ACTION SYS I I M, WELLS AND PIEZOMETFIc+ FIGURE 1 PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR THE INJECTION AND WITHDRAWAL WATER WELLS August 2008 — October 2008 The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north side of the Tank Farm Area. Iniection Water Well System The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system during the period. Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs Department. The total monthly and quarterly volumes of water injected as well as the month end water level in the Water Level Control Tank are: DPW WATER GALLONS TOTAL GALLONS AVERAGE GPM TANK LEVEL FEET, MSL August 684,214 0 684,214 15.8 15.0 September 414,146 0 414,146 9.6 15.0 October 1,011,799 0 1,011,799 23.4 15.0 TOTALS 2,110,159 0 2,110,159 H:\Reports\2008\Quarterly\TFRAS Report Third Quarter 2008.doc 3 Withdrawal Well System The withdrawal water well pumps are monitored daily by the area Maintenance Department and preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water volumes for the period are: SAND FORMATION GALLONS CROATAN FORMATION GALLONS TOTAL GALLONS AVERAGE GPM August 164,576 0 164,576 4.1 September 189,408 0 189,408 4.4 October 187,882 0 187,882 4.2 TOTALS 541,865 0 541,865 Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning, and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these activities are: Confined Sand Formation Withdrawal Well (SWW) Pumps- - — - - On 8/8 changed filters on air compressor. Rebedded / rebuilt the filters beginning 9/11 and finishing on 9/25. On 9/24 changed oil and filters on air compressor. SWW-1: On 10/29 reset counter. SWW-2: On 8/14 changed pump. On 8/20 changed pump. On 10/7 changed pump. SWW-3: SWW-4: On 9/18 reset head. On 9/23 replaced pump. On 10/22 acid washed well and replaced pump. SWW-5: On 8/5 replaced pump. On 10/7 replaced pump and counter. On 10/24 reset head. SWW-6: SWW-7: H:\Reports\2008\Quarterly\TFRAS Report Third Quarter 2008.doc 4 Croatan Formation Withdrawal Well (CWW) Pumps CWW-1: CWW-2: CWW-3: CWW-4: CWW-5: CWW-6: CWW-7: H:\Reports\2008\Quarterly\TFRAS Report Third Quarter 2008.doc 5 PCS Phosphate AURORA PCS PHOSPHATE COMPANY, INC. P.O. BOX 48, AURORA, NC U.S.A. 27806 November 21, 2008 Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina, 27699 Attn: Information Management CERTIFIED MAIL Subject: Underground Injection Control Program Quarterly Groundwater Monitoring Report August 2008 — October 2008 Injection Well Permit #WI0700012 Tank Farm Remedial Action System Beaufort Co. Dear Qi: Please find the subject groundwater monitoring report attached. This includes the sampling and reporting requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) piezometer level monitoring field sheet, and d) the summary operational and maintenance report. Please do not hesitate to contact me at (252) 322-8283 if you have any questions regarding this information. Sincerely, /01121.t,:2.0 D. Daniel Winstead II1 Environmental Engineer PCS Phosphate Attachments 10 pc: Allen Clark — Aquifer Protection DWQ, WaRO (w/ attachments) R. M. Smith/12-07-02 (w/ attachments) T. S. Ingra - Ardaman & Assoc. (w/attachments) R. A. Allen (w/ attachments) Mike Brom (w/ attachments) Anthony Shrewsbury (w/ attachments) R. B. Lee (w/ attachments) Total Two Copies Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina, 27699 Attn: Information Management H:\Reports\2008\Quarterly\TFRAS Report Third Quarter 2008.doc 2