WI0700012_Monitoring (Report)_20070528

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter: 4 inch
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH N/A , Specific Conductance
Temp. N/A oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
N/A uMhos
Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2
Coliform: MF Fecal / /100m1 Nitrate (NO3
Coliform: MF Total / /1 • Phosphorus:
(Note: Use MPN method for highly tur. Orthophosph
Dissolved Solids: Total I Al - Aluminum
pH (when analyzed) a Ba - Barium
TOC /I Ca - Calcium
Chloride /1 Cd- Cadmiu
Arsenic N Chromium: Tota
Cu - Copper
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
N/A mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
s n/a
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
MI Mill
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed:
Laboratory Name:
Certification No(s)
No an • . iel
ug/I
N/A ug/I
N/A ug/I
g - Silver
4/26/2007 to 5/11/2007
PCS PHOSPHATE
Se- Selenium
Sodium
N/A ug/I Organics: (GC, GC/MS
N/A ug/I (Specify test method #
N/A ug/I Report attached? Yes
N/A ug/I VOC
( 6"
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A
N/A ug/I
ug/I
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
mit (of Authorized ent) /Lame and Title - Please type or print
PiQ � 1?/115 S/ °?
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge
UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
18 1 1 Rotary Distributor
Well Identification Number (from Permit):
Well Depth: 52.15 ft. Well Diamter:
CWW-2
4 inch
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level: 5.46 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Remediation: Infiltration Gallery
Land Application of Sludge
For Groundwater Treatment Other
Sys ems Check One:
Influent (98) Note: Values should reflect dissolved and
Effluent (99) 1 colloidal concentrations
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2981 uMhos
Temp. 19.4 oC, Odor NONE Appearance: CLEAR
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name:
PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note : Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I
/100m1
/100m1
2474 mg/I
6.4 units
10.7 mg/I
70.2 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
1052.4 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
No and field
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 135.000 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/l
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium N/A ug/I
Chromium: Total N/A ug/I
Cu - Copper N/A ug/I
Fe - Iron N/A ug/I
Hg - Mercury N/A ug/I
K- Potassium N/A ug/l
Mg - Magnesium N/A ug/I
Mn - Manganese N/A ug/I
acidified Yes n/a No )
Ni - Nickel N/A ug/I
Pb - Lead N/A ug/I
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Con Units)
fa
Fluoride RF�0*.TN
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No
VOC : method#
method#
method#
0.19 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
X (2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager. Environmental Affairs
P rmiitee (of Authorize Agent) Name and Title - Please type or print
Ai) w.<A,--d r M� S/z4 A7-
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-3
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level: 4.36 ft. below measuring point.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Measuring Point is 3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2432 uMhos
Temp. 23.0 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/I
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2070 mg/I
pH (when analyzed) 6.3 units
TOC 6.5 mg/I
Chloride 59.0 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/1
Phenol N/A mg/1
861.0 mg/I
Specific Conductance N/A uMhos
Total Ammonia NIA mg/I
TKN as N N/A mg/1
Sulfate
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No
N/A
N/A
and field acidified
mg/I
mg/I
7.060 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Ni - Nickel
Pb - Lead
Yes n/a No )
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds and Concentratio its)
Fluoride `` ,Vtjj 0.15
MIBK 1i 1ERQOALITY N/A
N/A
N/A
N/A
Ag - Silver
ug/I
ug/I
ug/I
mg/I
mg/1
ug/I
N/A ug/I
Se- Selenium MAY 3 0 Z00/ N/A ug/I
Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #.
N/A ug/I Report attached? Yes
N/A ug/I VOC
N/A ug/I
N/A ug/I
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
�rmee (of Authorized Agent) Name and Title - Please type or print J
i awt-i0 kj,t Q 1 vc, r /1/15 s a `�
Signature of Permittee (or Authorized Agent) (Date)
/

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level: 4.27 ft. below measuring point.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Measuring Point is 2.75 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2805 uMhos
Temp. 24.6 oC, Odor NONE Appearance: LT RUST
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC X
01/15/08
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4I26/2n^'
Date sample analyzed.
Laboratory Name:
Certification No(s)
PARAMETERS: (Samples
COD
Coliform: MF Fecal
Coliform: MF Total
for metals were collected
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2313
pH (when analyzed) 6.7
TOC 7.8
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
69.8
N/A
N/A
N/A
982.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
unfiltered Yes nla
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
c.ho7
NVIRONMENT 1
N/A mg/I Ni - Nick N/A
N/A mg/l Pb - Lea( N/A
31.115 mg/1 Zn - Zinc N/A
N/A mg/I Ammonia
N/A ug/I Other (Specit _.... concentration Units)
N/A ug/l Fluoride yU��
N/A ug/l MIBK Ag - Silv(gY; 4,1. OF vOTER QUAL1TY
N/A ug/I
N/A ug/I
N/A ug/I
Se- Selenium 3 0 2007
Sodium ti9AY
N/A ug/I Organics: (GC, GC/MS,
N/A ug/I (Specify test method #.
N/A ug/I Report attached? Yes
N/A ug/I VOC
N/A ug/I
0.18
N/A
N/A
N/A
N/A
HPLC)
Attach lab report.)
(1) No X
: method#
• method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
P ittt/e,((gg}} (of Authorized /Agent) Name and Title - Please type or print /
N. Nr�.X i/.v1A 4 �o r WY)S .6/2z1 0
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-5
Well Depth: 53.17 ft. Well Diamter: 4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level:
Measuring Point is
6.13 ft. below measuring point.
2.58 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 2765 uMhos
Temp. 26.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS:
(Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2144 mg/I
pH (when analyzed) 6.6 units
TOC 10.4 mg/I
Chloride 57.7 mg/I
Arsenic N/A mg/I
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A mg/1
988.0 mg/1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
29.350 mg/I
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK REGFF \!Ei) N/A ug/I
,- WATER OUAL� 1 ¥ N/A ug/I
N/A ug/I
mg/I
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium k 1 av ? fk ?O N/A ug/I
N/A ug/I Organics: (GC, GC/MS', LC)
N/A ug/I (Specify test method #. Attach lab report.)
0.08 mg/I
N/A ug/I Report attached? Yes (1) No
N/A ug/I VOC method#
method#
method#
X (2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
f\ern}it;ee (of Authorized Agent) Name and Title - Please type or print
�llpup p ,�„� �,� F�r i2MS 5/24 l6 j7-
Signature of Permitte (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-6
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: 10.49 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 3335 uMhos
Temp. 30.1 oC, Odor NONE Appearance: CLEAR
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01 /15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS:
COD
(Samples for metals were collected unfiltered Yes
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/I
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2418 mg/I
pH (when analyzed) 6.6 units
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
13.5 mg/I
75.4 mg/I
n/a
No and field acidified
Yes n/a No )
Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A ug/I
Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A ug/I
Phosphorus: Total as P 42.130 mg/I Zn - Zinc N/A ug/I
Orthophosphate N/A mg/I Ammonia Nitrogen mg/1
Al - Aluminum N/A ug/I Other (Specify Compounds and Qper.eptration Units)
Ba - Barium N/A ug/I Fluoride O" ` -v; ,��1 0.07 mg/l
Ca Calcium N/A ug/I MIBK Q�' N/A ug/I
Cd- Cadmium N/A ug/I Ag - Silver N/A ug/I
N/A mg/I Chromium: Total N/A ug/I Se- Selenium. 3 't% L007 N/A ug/l
file
N/A mg/I Cu - Copper N/A ug/I Sodium N/A ug/I
N/A mg/I Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC)
1127.7 mg/I Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.)
N/A uMhos K Potassium N/A ug/I Report attached? Yes (1) No X (2)
N/A mg/I Mg - Magnesium N/A ug/I VOC : method#
Mn - Manganese N/A ug/I
N/A mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Pitte�t�iX Agen��aae and Title - Please type or print
jQ (k�//�j �t l0-�X r p� s 6/2' t/0 -
Signature of Permittee (or Authorize Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): CWW-7
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level: 4.87 ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 1080 uMhos
Temp. 23.7 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified Yes n/a No )
COD N/A mg/1 Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A ug/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A ug/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 6.698 mg/1 Zn - Zinc N/A ug/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total 770 mg/1 Al - Aluminum N/A ug/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) 6.7 units Ba - Barium N/A ug/I Fluoride Pc. ' ` `" 0.16 mg/I
TOC 5.3 mg/1 Ca - Calcium N/A ug/I MIBK N/A ug/l
Chloride 45.9 mg/I Cd- Cadmium N/A ug/I Ag - Silver N/A ug/I
Arsenic N/A mg/1 Chromium: Total N/A ug/I Se- Selenium Y;. U 2007 N/A ug/l
Grease and Oils N/A mg/1 Cu - Copper N/A ug/I Sodium N/A ug/I
Phenol N/A mg/1 Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC)
1138.2 mg/1 Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A ug/I Report attached? Yes (1) No X (2)
N/A mg/I Mg - Magnesium N/A ug/I VOC : method#
Sulfate
Specific Conductance
Total Ammonia
TKN as N N/A mg/I Mn - Manganese
N/A ug/I : method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Permitt e (of Authorized A ent) Name and Title - Please type or print
!:�•�JRNLtQ�( j s .5/24 /o
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter: 4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level:
Measuring Point is
N/A ft. below measuring point.
1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly tur
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Nitrite (NO2
/100m1 Nitrate (NO3
Phosphorus:
Orthophosph
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmiu
Chromium: Tota
Cu - Copper
N/A mg/I Fe - Iron
N/A mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date samples--
Laboraton ,73')�`j�
Certificatic
N/A ug/I
N/A ug/I
5/11/2007
N/A ug/I
N/A ug/I
N/A ug/I
mg/I
ion Units)
N/A
mg/I
yt l"N/A ug/I
N/A ug/I
Se- Selenium 227 N/A ug/I
Sodium N/A ug/I
Organics: (GC, GC/MS, HPLC)
N/A ug/l (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
N/A ug/l
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Permi ee (of Authorized AgentZName and Title - Please type or print
-e�✓ �QMs 5-72q
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level:
Measuring Point is
7.15 ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2444 uMhos
Temp. 20.0 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate 570.8 mg/I Hg - Mercury
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
2294 mg/I Al - Aluminum
6.1 units Ba - Barium
9.3 mg/1 Ca - Calcium
55.6 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A mg/I Ni - Nickel
Yes n/a No )
ug/I
N/A mg/1 Pb - Lead ug/I
345.000 mg/I Zn - Zinc ug/I
N/A mg/I Ammonia Nitrogen mg/I
N/A
N/A
N/A
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride �-ty. 0.26 mg/I
N/A ug/I MIBK dug/I
N/A ug/I Ag - Silver n" ug/I
N/A ug/I Se- Selenium N/A ug/I
N/A ug/I Sodium \'°`'' ' k, 2007 N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC method#
N/A ug/I method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
P rmi ee (of Authorized Agent) Name and Title - Please type or print
5124 7o7-
MA �/14,,n.;t if'��it4r r 2013
Signature of Permit ee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.25 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2003 uMhos
Temp. 20.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1810
pH (when analyzed) 6.0
TOC 10.3
Chloride 37.1
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
553.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Yes n/a No and field acidified Yes n/a No )
N/A mg/I ug/I
N/A mg/I ug/I
P 217.016 mg/I ug/I
N/A mg/I Ammonia Nitrogen mg/I
N/A ug/I Other (Specify Compounds and Concentration Un'ts)
N/A ug/I Fluoride 0.06 mg/I
N/A ug/I MIBK N/A ug/I
Cd- Cadmium N/A ug/I Ag - Silver N/A ug/I
Chromium: Total N/A ug/I Se- Selenium N/A ug/l
Cu - Copper N/A ug/I Sodium N/A ug/I
Fe - Iron N/A ug/I Organics: (GC. GC/MS, HPLC)
Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.)
K- Potassium N/A ug/I Report attached? Yes (1) No X (2)
Mg - Magnesium N/A ug/I VOC : method#
Mn - Manganese N/A ug/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Ni - Nickel N/A
Pb - Lead N/A
Zn - Zinc N/A
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
�P rmittee (of Authorized Agent) Name and Title - Please type or print
• sk i) G,/ 8A15 5-724 /4 7
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 25.00 ft. Well Diamter:
SWW-4
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
Measuring Point is
4 inch
5.81 ft. below measuring point.
3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 5.7 , Specific Conductance
Temp. 30.9 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2362 uMhos
Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
2052
5.9
6.8
34.4
N/A
N/A
N/A
593.9
N/A
N/A
N/A
Yes n/a
No and field acidified
Nitrite (NO2 as N) N/A
/100m1 Nitrate (NO3 as N)
N/A
/100m1 Phosphorus: Total as P 282.500
Orthophosphate N/A mg/I
mg/I Al - Aluminum N/A ug/I
units Ba - Barium N/A ug/I
mg/I Ca - Calcium N/A ug/I
mg/I Cd- Cadmium N/A ug/I
mg/I Chromium: Total N/A ug/I
mg/I Cu - Copper N/A ug/I
mg/I Fe - Iron N/A ug/I
mg/1 Hg - Mercury N/A ug/I
uMhos K- Potassium N/A ug/I
mg/I Mg - Magnesium N/A ug/I
mg/I Mn - Manganese N/A ug/I
mg/I Ni - Nickel
mg/1 Pb - Lead
mg/I Zn - Zinc
Yes n/a No )
Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium 007
Organics: (GC, GC/MS, HPLC')
(Specify test method #. Attach lab report.)
Report attached? Yes
(1) No
VOC : method#
method#
method#
mg/1
0.11 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
X (2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Pefmitttf e (of Authorized �Age/00 Name and Title - Please type or print /
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level:
Measuring Point is
4 inch
5.26 ft. below measuring point.
2.96 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2408 uMhos
Temp. 27.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1570
6.6
8.9
44.0
N/A
N/A
N/A
712.1
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/l Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
Yes n/a No )
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/I
78.713 mg/I Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen mg/I
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride 0.34 mg/I
N/A ug/I MIBK ug/I
N/A ug/I Ag - Silver N/A ug/I
N/A ug/I Se- Selenium MAY a U ?D07 N/A ug/I
N/A ug/I Sodium N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
N/A ug/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
rmii t Pee (of Authorized Aggcnt) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level:
Measuring Point is
4 inch
4.15 ft. below measuring point.
2.58 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 3277 uMhos
Temp. 27.5 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge
UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS:
COD
(Samples for metals were collected unfiltered Yes n/a
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Dissolved Solids: Total 2546 mg/l
pH (when analyzed) 6.4 units
TOC 15.3 mg/I
Chloride 79.8 mg/l
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
1136.3 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
59.395 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
No and field acidified
Yes n/a No )
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/l Pb - Lead N/A ug/I
Zn - Zinc N/A ug/l
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.07 mg/I
MIBK 9 i N/A ug/l
N/A ug/I Ag - Silver il}t"4^! N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
P,��IIrm ee (of Authorized A�9ent) Name and Title - Please type or print
ftJ,�t Wet 5-(2"
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Faciity Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 29.50 ft. Well Diamter:
SWW-7
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.62 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 5.8 , Specific Conductance
Temp. 23.7 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
658 uMhos
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/26/2007
Date sample analyzed: 4/26/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A mg/I
N/A /100m1
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
440 mg/I Al - Aluminum
6.0 units Ba - Barium
5.8 mg/I Ca - Calcium
36.5 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
121.2 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/1 Mn - Manganese
n/a No
N/A
N/A
23.61
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
and field acidified Yes n/a No )
mg/I Ni - Nickel N/A
mg/I Pb - Lead N/A
7 mg/I Zn - Zinc N/A
mg/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/l
ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.13 mg/I
MIBK 4ii4/ 2Ljo % N/A ug/I
Ag - Silver N/A ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
Se- Selenium
Sodium
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager. Environmental Affairs
Permitte (of Authorized Agent) Name and Title - Please type or print
-(1/. 10115 312 1-1 h 7-
Signature of Permittee (o Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 6.40 ft. Well Diamter:
MWTF1-A
2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 5.33 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 6.9 , Specific Conductance 835 uMhos
Temp. 20.6 oC, Odor NONE
Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/25/2007
Date sample analyzed: 4/25/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 542
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
7.0
5.2
9.6
N/A
N/A
N/A
75.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Yes n/a No and field
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 0.361 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium N/A ug/I
Chromium: Total N/A ug/I
Cu - Copper N/A ug/I
N/A ug/I
N/A ug/I
K- Potassium N/A ug/I
Mg - Magnesium N/A ug/I
Mn - Manganese N/A ug/I
Fe - Iron
Hg - Mercury
acidified Yes n/a Nn
(� U)LA'I
i- IY`
)0
N/A
N/A
N/A
rr
2002
1.39
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 3/2000
Ross M. Smith - Manager. Environmental Affairs
PPrmittt�tee���e (of Authorized Ag,ent) Name and Title - Please type or print
Signature of Perm' tee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter:
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level:
Measuring Point is
2 inch
5.38 ft. below measuring point.
3.86 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 5.5 , Specific Conductance 361 uMhos
Temp. 22.1 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/25/2007
Date sample analyzed: 4/25/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/1
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
250
6.0
5.0
45.9
N/A
N/A
N/A
29.8
N/A
N/A
N/A
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
4.563 mg/I
No and field acidified
N/A mg/1 Ni - I -
N/A mgll Pb -
Zn - ;
N/A mg/I Amm
N/A ug/I Other
NIA ug/I FI
N/A ug/I M
N/A ug/I Ac
N/A ug/I Se
N/A ug/I Sodium
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
r
ifP f G10J
- vIur7i
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/I
0.17 mg/I
N/A ug/I
N/A ug/l
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC) AA07
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
P mit e (of Author ed Age ) Name and Title - Please type or print
r 5./2 Cr /d 7z
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO.. INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 11.79 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.0 , Specific Conductance 652 uMhos
Temp. 21.7 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01 /15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/25/2007
Date sample analyzed: 4/25/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes No and field acidified X Yes No )
COD N/A mgll Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A ug/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A ug/I
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.620 mg/I Zn - Zinc N/A ug/l
(Note Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total 432 mg/I Al - Aluminum N/A ug/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) 7.1 units Ba - Barium N/A ug/I Fluoride 0.47 mg/I
TOC 4.7 mg/I Ca - Calcium N/A ug/I MIBK N/A ug/I
Chloride 17.0 mg/I Cd- Cadmium <0.001 ug/I Ag - Silver N/A ug/I
Arsenic N/A mg/I Chromium: Total 0.005 ug/I Se- Selenium N/A ug/I
Grease and Oils N/A mg/1 Cu - Copper N/A ug/I Sodium N/A ug/I
Phenol N/A mgll Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC)
21.2 mg/I Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A ug/I Report attached? Yes (1) No X (2)
N/A mg/l Mg - Magnesium N/A ug/I VOC • method#
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mgll Mn - Manganese 0.055 ug/I : method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
P mittfe (of Authorized Agen) Nang. and Title - Please type or print
$,U,. r P,vrs 572Y
Signature of Permitt (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
r born R.,
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter:
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level:
Measuring Point is
4 inch
N/A ft. below measuring point.
N/A ft above land surface.
For Groundwater Treatment
Systems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: N/A
Field Analysis: pH 7.0 , Specific Conductance 584 uMhos
Temp. 18.8 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/25/2007
Date sample analyzed: 4/25/2007 to 5/11/2007
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
(Note• Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
427
7.3
4.7
18.4
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/I
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified X
Yes No )
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/l Pb - Lead N/A ug/I
0.023 mg/I Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen mg/I
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride 0.56 mg/I
N/A ug/I MIBK N/A ug/l
<0.001 ug/I Ag - Silver N/A ug/I
<0.005 ug/l Se- Selenium N/A ug/I
N/A ug/I Sodium N/A ug/I
N/A ug/l Organics: (GC, GC/MS. HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
<0.010 ug/I : method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
``Pmitte, (of Authorized Agenn4 Name and Title - Please type or print /
� �Q.�c IN.c..-,-a�/(r 2M5 S-/2 4 /v 77
Signature of Permittee (or Authorized Agent) (Date)

Date:
Time:
Tech:
PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
/71/46427
System Gauge
Pressures
SWW-1
,=N eV,.
SWW-7
2270Sp-
CWW-1
" _2-717op
CWW-7
j%!'vp.
File: 12-07-02
pc: TLa
Ref nn ce
Pan SOL .
Level Rel
to fl
Ditch
12.91
839'
Barge Slip
10.69
/. /(o
Water Level
Control Tank
%= MSL
j2 4
Sand Layer Pelzometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Ste Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft
Spz-1
10.47
+i/. /5
/O, sa
Cpz-1
10.51
// //a
- 0. 9/
Spz-2
1121
B 5 0
a. "7/
Cpz-2
1025
/• (o
/O
- AC
Spz-3
11.87
0,73
//, 19
Cpz-3
11.12
//. //
e if)/
spz-4
11.45
6.6 /
A/ BY
cPW
9.65
// O/
-/ &'
Spz-5
11.45
9.03-
/ 90
MWTF-1A•
14.35
.5; 33 .
9, OA
Spz-6
1123
/075`
' /, 01
MWTF-1B•
14.36 -
`JJ 3S
4 e . 98
Spz-7
11.59
- 973
/ 8
MWTF-1C•
14.44
// 79
46,5
Spz-8
1157
% gyp//O
7. `//
MWTF-2A
14.05
5:90
- •8./5
Spz-9
11.01
p - 5/0
c?./p/
MWTF-2B
14.02
// /7
..785
/5:5a,
-/-'/8i
Spz-10
12.16
6.Qr
6. 9/ -
MWTFdc
14.08 -
SPW
9.95:
785
7 /0
MWTF3A
1221
- f.Sr
B.OB&
MWTF38
12.18
/0.33
/ psi
MWTF-3C
12.19
/.3.96
- /- 77
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Ste
Wtr'
Level Ft.
Pump
Activation Depth
Rol MSL
Max Level
Relative To
MSL Ft
Control
Point
MSL'
Is Well
Pumping?
Mes/(N)_o
Comments
SWW-1
10.70
/5 05
6'
-
+1'to+2'
No�ain,ot%y91/
NO
�
/V%d
/ozv sk--,&e/
cww-1
10.90
z/ 96
9
-
-2'to -1'
SWW-2
9.99
7/5-
B
/- /5
+140+2'
Y5
CWW-2
1023
,5 4/ '
9'
- 3.5i/
-2'to-1'
S7
SWW-3
9.97
7,R,5" "
S'
/• S
+1'to+2'_
015 .
CWW3
9.95
-�•e86
Er
- '5' 6 V
-2'to-1'
SWW-4
10.73
a- 8/
9'
-Q./ 9
-+1'to +2'
/Y--5
cc9
CWW-4
ion
4/.027
9'
- �% 7.,5
-2'to-1'
W SW-5
10.80
.j;a10
B
- O.79
+1'to+2'
yyy�ei
CWW-5
10.74
.. /3
e'
"a7/7
-2'to-1'
,%eS'
SWW3
10.66
y /5�
S
-/.6
+1 'to+2'
/y/ /5
5
CWW-6
9.92
/t V 9
9'
. / /17
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6'
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/O
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CWW-7
9.95
/
7.0�
9'
-AZ/5
-2'to-1'
//y
qC1
Revised 729/02
• Riser length added to TOC elevation 124/97
DADati%Forms\Wea Fonn\Tenk Farm Renee WeIIs.lds

sPz
•
SPZ-1
CPZ-1
OFFICE
CUT-OFF WALL
CPZ-2 .
SWW4 1
CWW-2
MWTF-2
CLUSTER
I DRAINAGE DITCH
S.P.A
PLANT
CHI-2
SWW:s
ASPHALT ROAD CWw-s
SWW-4 CWWJ
SPZ-5 SPZ-7
0
CPW SPW CTW+
SEAT+
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W1OTAAI WELL
MWCOTI1OL A
AND CONTROL VALVES
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PIPERACK SPILL CONTAINMENT PAD
E
f'
O E
O S.P.A
O PLANT
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czi
0
WATER LEVEL
CONTROL TANK
MWTF-1
CLUSTE
MWIFA
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7
SPZ-10 _.
002
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• I ,•p. •. l.........I n wl l.mn. W AI *I II
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LOCATION PLAN FOR TANK FARM:
AREA REMEDIAL ACTION SYSII M
WELLS AND PIEZOMETI II':
FIGURE 1

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
February 2007 — April 2007
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
during the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank.are:
7271
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Feb
961,563
0
961,563
23.8
15.0
March
972,895
0
972,895
22.5
15.0
April
997,532
0
997,532
23.1
15.0
TOTALS
2,931,990
0
2,931,990
H:\Reports\2007\Quarterly\TFRAS Report First Quarter 2007.doc
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Feb
237,876
26,744
264,620
6.6
March
304,828
28,992
333,820
7.7
April
259,987
37,154
297,142
6.9
TOTALS
802,691
92,891
895,582
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
-activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
All Pumps were flushed on 2/2, 2/7, 2/14, 2/23, 3/1, 3/9, 4/3, 4/10 and 4/27.
SWW-1: On 4/26 acid washed and changed pump.
SWW-2: On 4/17 acid washed and changed pump.
SWW-3:
SWW-4: On 4/18 changed pump. On 4/21 changed pump and counter.
SWW-5:
SWW-6: On 4/16 shook pump. On 4/22 cleared discharge hose.
SWW-7:
H:\Reports\2007\Quarterly\TFRAS Report First Quarter 2007.doc
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2:
CWW-3: On 3/6 changed pump.
CWW-4: On 4/12 reset pump.
CWW-5: On 4/26 changed pump.
CWW-6:
CWW-7:
H:\Reports\2007\Quarterly\TFRAS Report First Quarter 2007.doc
5

h
PCS
Phosphatece AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
May 22, 2007
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
February 2007 — April 2007
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Evan:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) piezometer level
monitoring field sheet, and d) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
Lc,,,,,sat..).;:x_-„e_gz_
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments

pc: Will Hart — Aquifer Protection DWQ, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
W. A. Schimming (w/ attachments)
Anthony Shrewsbury (w/ attachments)
R. B. Lee (w/ attachments)
Total Two Copies
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
H:\Reports\2007\Quarterly\TFRAS Report First Quarter 2007.doc
2