WI0700012_Monitoring (Report)_20050209

PCS
Phosphate
AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
February 9, 2005
EVAN O. KANE
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
August 2004 — October 2004
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Evan:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTFIB, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
The flow data and downtime information presented is from August, September and October. The
withdrawal data was collected in October. The injection well data was collected in November and
December. The report to be issued in February 2005 will represent data from November, December and
January.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
.XD x osi-Q rk, ,
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments

pc: Annalee Harris — Aquifer Protection DWQ, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
W. A. Schimming (w/ attachments)
E-Mail:
M. D. Johnson
Doug Koeppen
R. B. Lee
\\aurdata2\users\AUR1DDW\Reports\2004\Quarterly\TFRAS Report Third Quarter 2004.doc
2

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 48.00 ft. Well Diamter:
CIW-7
4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
N/A
Field Analysis: pH 7.0 , Specific Conductance 782 uMhos
Temp. 14.8 oC, Odor NONE Appearance: CLEAR
PARAMETERS:
COD
Coliform: MF Fecal
Coliform: MF Total
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
12/28/04
12/28/04 to 1/20/05
PCS PHOSPHATE and ENVIRONMENT 1
330 10
(Samples for metals were collected unfiltered X Yes
N/A
N/A
390
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 543
pH (when analyzed) 7.0
TOC 5.5
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
16.6
N/A
N/A
N/A
81.7
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/1
Nitrite (NO2 as N)
No and field acidified X Yes No )
N/A mg/I
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
4.146 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
<0.001 mg/I
<0.005 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds
Fluoride
MIBK
Ag - Silver
Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/I VOC
0.031 mg/I
: method#
: method#
method#
N/A mg/I
N/A mg/I
N/A mg/I
mg/I
and Concentration Units)
0.58 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Iiii
1/-59 Rev 03/2000
Ross M. Smith - Manager Environmental Affairs
Perm ft (of Author fed Ageme and Title - Pleas ; type or .r
Signature of Permittee (or Au horized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: _ 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 11.60* ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 3100
Field Analysis: pH 6.9 , Specific Conductance 1743 uMhos
Temp. 16.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
12/15/04
12/15/04 to 1/20/05
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples
COD
Coliform: MF Fecal
Coliform: MF Total
for metals were collected
N/A
N/A
<1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 965
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
mg/I
/100m1
/100m1
mg/I
7.2 units
6.0 mg/I
320.0 mg/I
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
50.9 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
unfiltered X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
4.990 mg/I Zn - Zinc
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
<0.001 mg/I
0.027 mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
0.097 mg/1
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
0.37
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
VOC
: method#
: method#
method#
mg/I
ug/I
ug/I
ug/I
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Mana
er, Environmental Affairs
7eo:7nzedynt)
Nam and Title - lease pe or print
i4/tnature of Prermittee (• Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter: 4 inch
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level: 6.45* ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
_ Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2276 uMhos
Temp. 20.3 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes nia
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1800 mg/1 Al - Aluminum
pH (when analyzed) 6.6 units Ba - Barium
TOC 10.9 mg/I Ca - Calcium
Chloride 85.3 mg/I Cd- Cadmium
Arsenic N/A mg/I Chromium: Total
Grease and Oils
Phenol
Sulfate
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
733.3 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
2.025 mg/I
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mgA Ammonia Nitrogen
N/A mgA
N/A mg/I
N/A mg/I
N/A mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mgA Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
0.24
N/A
N/A
N/A
N/A
N/A mg/I VOC : method#
: method#
method#
N/A mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
pP - it�ee(of///tbutthori(zyyaef�ient) Name and Title Pleas type or print
Signature of Permittee or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-2
Well Depth: 52.15 ft. Well Diamter:
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level:
Measuring Point is
4 inch
9,89* ft. below measuring point.
3.00 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.0 , Specific Conductance 1135 uMhos
Temp. 21.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Dissolved Solids: Total 1360 mg/l
pH (when analyzed) 7.0 units
TOC 5.8 mg/1
Chloride
149.0 mg/1
Arsenic
Grease and Oils
Phenol N/A mg/I Fe - Iron
N/A mg/I
N/A mg/I
Sulfate
Specific Conductance
Total Ammonia
TKN as N
636.0 mg/I Hg - Mercury
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
6.250 mg/I Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.48
N/A
N/A
N/A
N/A
N/A mg/1 Organics: (GC. GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/1 VOC
N/A mg/I
method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is trueaccurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Per (of Aut orized -eat) Name and Title 2 lease typ
r41 /N 1
Signature of Permittee (orAuthorized Agent)
or print
�/,
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-3
4 inch
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level: 6.49* ft. below measuring point.
Measuring Point is 3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 2549 uMhos
Temp. 23.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2070
pH (when analyzed) 6.4
TOC 8.5
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
107.0
N/A
N/A
N/A
753.8
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
N/A
N/A
4.050
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.19
N/A
N/A
N/A
N/A
VOC : method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environment
Perrpjitee (of AuuthorizedAName and Title -
Sin
gnature of Parmittee (oAuthorized
Agent)
I Affairs
ease type >"r print
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level:
Measuring Point is
4 inch
4.52* ft. below measuring point.
2.75 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2308 uMhos
Temp. 24.8 oC, Odor NONE Appearance: LT RUST
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1880
pH (when analyzed) 6.5
TOC 9.0
Chloride
mg/I
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
90.9 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
697.5 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A
N/A
19.500
mg/I Ni - Nickel
mg/I Pb - Lead
mg/I Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.17
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Perm ittr( Aut}iorjzed Agen
Signature of Permittee (or Au
e and Title - Please pe or nett
orized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
CWW-5
Well Depth: 53.17 ft. Well Diamter: 4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level:
Measuring Point is
5.03* ft. below measuring point.
2.58 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2380 uMhos
Temp. 28.2 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
N/A mg/I
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
N/A /100m1
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1670 mg/l
pH (when analyzed) 6.5 units
TOC
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
N/A
N/A
Phosphorus: Total as
Orthophosphate
Al - Aluminum
Ba - Barium
P 10.050
N/A
N/A
N/A
7.6 mg/I Ca - Calcium N/A
Chloride 89.6 mg/I
Arsenic N/A mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/1
Specific Conductance
Total Ammonia
TKN as N
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
651.4 mg/1 Hg - Mercury
mg/I Ni - Nickel
Yes n/a No )
mg/I Pb - Lead
mg/I Zn - Zinc
mg/I Ammonia Nitrogen
N/A
N/A
N/A
mg/l Other (Specify Compounds and Concentration Units)
mg/I Fluoride
mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A uMhos K- Potassium
N/A mgll Mg - Magnesium
N/A mg/I Mn - Manganese
0.15
N/A
N/A
N/A
N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/1 VOC
N/A mg/I
•
•
method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/l
ug/I
ug/I
ug/1
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Pe tt {of A�orized P,yen �a and Title - Ple e type cK �int / %�
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
53.00 ft. Well Diamter:
CWW-6
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level:
4 inch
6.69* ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
Temp. 30 oC, Odor NONE
For Groundwater Treatment
Systems Check one:
Influent (98)
X Effluent (99)
CONTINUOUS
2840 uMhos
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal
Coliform: MF Total
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2050 mg/I
pH (when analyzed) 6.4 units
12.4
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
79.0
N/A
N/A
N/A
887.0
N/A
N/A
N/A
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/l Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
35.500 mg/I
N/A mg/l
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
Yes n/a No )
N/A mg/I
N/A mg/I
Zn - Zinc N/A mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.25 mg/I
MIBK
Ag - Silver
Se- Selenium
Sodium
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
N/A mg/1 Report attached? Yes (1) No X (2)
N/A mg/I VOC
N/A mg/I
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Per eg (of Authorized Agent )(lame and Title - P e ty�rint
"—
let
N4
Signature of Permittee (or ed Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-7
Well Depth: 53.00 ft. Well Diamter:
4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level: 5.49* ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.7 , Specific Conductance 1196 uMhos
Temp. 23.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 759
pH (when analyzed) 6.7
TOC 6.0
Chloride
mg/I
/100m1
/100m1
mg/I
units
mg/I Ca - Calcium
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
65.3 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/l Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
147.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A
N/A
6.150
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/1
mg/1
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
0.25
N/A
N/A
N/A
Sodium N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/1
ug/I
ug/I
ug/I
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
Ross M. Smith - Mana
er, Environmental Affairs
Perrgittee (of Autyforized) Name and Title rase type prinor t
( ,C ? / `' 1
Signature of
Y'C
/
ermittee (oi 'Authorized Agent) (Date)
GW-59 Rev 03/2000

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
(born pan.
Mail Original
to:
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter: 4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level:
Measuring Point is
8.96* ft. below measuring point.
1.52 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1764 uMhos
Temp. 21.6 oC, Odor NONE Appearance:
CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1110
6.3
7.3
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
68.3
N/A
N/A
N/A
395.3
N/A
N/A
N/A
mg/I
/100m1
/100m1
mgll
units
mg/I
mg/1
mg/1
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
116.000 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/1
mg/1
mg/I
mg/I
mg/1
mg/I
mg/I VOC
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.75
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
: method#
method#
method#
mg/1
mg/l
mg/l
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurateand completeand that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
7orized7ZrnetIe
tteee(of Ppe, orrpp t '1ez%/pture of Permittee (or Adthorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter:
Screened Interval:
Depth to Water Level:
Measuring Point is
4 inch
18.80 ft. to 21.63 ft.
7.91* ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2176 uMhos
Temp. 20.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1570
6.5
8.3
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
37.9
N/A
N/A
N/A
625.8
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
N/A mg/I
N/A mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
66.250 mg/I
N/A mg/l
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
0.26
N/A
N/A
N/A
N/A mg/l Sodium N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/I VOC : method#
N/A mg/l
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and completeand that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
`LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Mana
PermJfte (of Authh ized A
1.44f / I�IM. / f `a'?
Permittee (or Authorized Agent)
Signature o
er,. Environmental
airs
'Name and Title - Plea type of print
{ 24. D7U
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.71* ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 6.3 , Specific Conductance 1787 uMhos
Temp. 21.9 oC. Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone. [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1400
6.4
7.3
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
73.8
N/A
N/A
N/A
554.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
N/A
N/A
Phosphorus: Total as
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
P 64.000
N/A
N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mgll Zn - Zinc
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I VOC
mg/I
Ni - Nickel
Pb - Lead
and ENVIRONMENT 1
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
method#
0.19
N/A
N/A
N/A
N/A
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1 /28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permif5be of Author zed Ag�yt{) ime and Title - Please pe or. mt/
Si nature of Permittee(or A horized Agent) Date
9 9 ) (Date)
1• t

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-4
Well Depth:
25.00 ft. Well Diamter:
Screened Interval: 20.50 ft. to 23.30 ft.
4 inch
Depth to Water Level: 7.51* ft. below measuring point.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2064 uMhos
Temp. 23.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 169.000 mg/I
(Note. Use MPN method for highly turbid samples) Orthophosphate N/A mg/I
Dissolved Solids: Total 1660 mg/I Al - Aluminum N/A mg/I
pH (when analyzed) 6.1 units Ba - Barium N/A mg/I
TOC 7.6 mg/I Ca - Calcium N/A mg/I
Chloride 38.0 mg/I Cd- Cadmium N/A mg/I
N/A mg/I Chromium: Total N/A mg/I
N/A mg/1 Cu - Copper N/A mg/I
N/A mg/I Fe - Iron N/A mg/l
641.1 mg/1 Hg - Mercury N/A mg/I
N/A uMhos K- Potassium N/A mg/l
N/A mg/I Mg - Magnesium N/A mg/I
N/A mg/I Mn - Manganese N/A mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
No and field
acidified Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.14
N/A
N/A
N/A
N/A
VOC : method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/l
ug/I
ug/l
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permitt (of uth rized •gegt) e d Title - Please typ or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.32* ft. below measuring point.
2.96 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2401 uMhos
Temp. 28 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1550
6.3
9.6
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
48.0
N/A
N/A
N/A
666.7
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/l
mg/I
mg/I
mg/I
mg/1
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as
Orthophosphate
Al - Aluminum
Ba - Barium
No and field acidified
N/A
N/A
P 97.750
N/A
N/A
N/A
Ca - Calcium N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A
N/A
N/A
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
N/A
N/A mg/1
mg/I Ni - Nickel
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I VOC
Yes n/a No )
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
N/A
N/A
N/A
0.33
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
method#
method#
meth od#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Perrryitt e (of A thgrize 4 t) Name and Titl Please t e or print
,fir e-,ram. r C . (#e . /e)% i--
Signature of Permittee or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT#: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
18 Rotary Distributor Land Application of Sludge
Well Identification Number (from Permit):
Well Depth: 26.00 ft. Well Diamter:
SWW-6
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level:
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
4 inch
7.46* ft. below measuring point.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 3354
Temp. 30.8 oC, Odor NONE
uMhos
Appearance: CLEAR
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 2340
pH (when analyzed) 6.3
TOC 15.0
Chloride 75.2
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate 1148.2
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I
/100m1
/100m1
No and field acidified
Nitrite (NO2 as N) N/A
Nitrate (NO3 as N) N/A
Phosphorus: Total as P 65.000
Orthophosphate N/A
mg/1 Al - Aluminum N/A
units Ba - Barium N/A
mg/I Ca - Calcium N/A
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/1
mg/I
mg/I
mg/1
mg/I
mg/l
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
mg/l
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.05
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Per llipee (of Authorized Aged me and Title - Pleas type er ri
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
SWW-7
Well Depth: 29.50 ft. Well Diamter:
Screened Interval: 25.17 ft. to 27.50 ft.
4 inch
Depth to Water Level: 7.80* ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 742 uMhos
Temp. 25.3 oC, Odor NONE Appearance: LT CLDY BROWN
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01 /15108
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 11/2/04
Date sample analyzed: 11/2/04 to 11/20/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
Yes nla No and field acidified
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
531
6.0
9.1 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
51.5
N/A
N/A
N/A
102.4
N/A
N/A
N/A
Orthophosphate
mg/l Al - Aluminum
units Ba - Barium
mg/1 Cd- Cadmium
mg/I Chromium: Total
mgll Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A mg/I
N/A mg/I
62.250 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/l
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
0.11
N/A
N/A
N/A
N/A
N/A mg/I VOC
N/A mg/I
method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ugi
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Perrpdtee of A thorized•Age,) me and Title - Please pe or pr nt -
(Date)
Signature of Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
6.40 ft. Well Diamter:
MWTF1-A
Screened Interval: 3.40 ft. to 5.40 ft.
2 inch
Depth to Water Level: 4.21* ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2500
Field Analysis: pH 7.0 , Specific Conductance 465 uMhos
Temp. 15.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 12/15/04
Date sample analyzed: 12/15/04 to 12/28/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
Yes n/a No and field
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 291
pH (when analyzed) 7.1
TOC 3.8
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
13.4
N/A
N/A
N/A
25.5
N/A
N/A
N/A
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
N/A
N/A
0.244
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A
N/A
N/A
acidified Yes n/a No )
mg/I Ni - Nickel
mg/I Pb - Lead
mg/I Zn - Zinc
mg/I Ammonia Nitrogen
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I VOC
mg/I
N/A mg/1
N/A mg/I
N/A mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
mg/I
2.28 mg/l
N/A ug/I
N/A ug/I
N/A ug/I
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
N/A ug.
Report attached? Yes (1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Permit”, Author
/44
Signature of Permittee (or Auth rized Agent)
Ross M. Smith - Manager, Environmental Affairs
d Agent) and Title - Please typ
or print
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-B
Well Depth:
13.50 ft. Well Diamter: 2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 4.83* ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 5.8 , Specific Conductance 325 uMhos
Temp. 17.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 12/15/04
Date sample analyzed: 12/15/04 to 12/28/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 232 mg/I Al - Aluminum
pH (when analyzed) 6.3 units Ba - Barium
TOC 3.5 mg/I Ca - Calcium
Chloride 44.1 mg/I Cd- Cadmium
Arsenic N/A mg/1 Chromium: Total
Grease and Oils N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
27.7 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
n/a
No and field
N/A
N/A
4.150
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
acidified
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Yes n/a No )
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.30
N/A
N/A
N/A
N/A
mg/I Organics: (GC, GC/MS, HPLC)
mg/I (Specify test method #.
mg/I Report attached? Yes
mg/I VOC
mg/I
Attach lab report.)
(1) No X
method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*LEVEL WAS TAKEN ON 1/28/05.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (o utho ized gent) e/V�d Title-leeasse typ /r print'
(/ tc„, 4 , M :/ 4 7``2 / S -
Signature of Permittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): WLCT
Well Depth: N/A ft. Well Diamter: N/A
Screened Interval:
Depth to Water Level:
Measuring Point is
N/A ft. to N/A ft.
N/A ft. below measuring point.
N/A ft above land surface.
For Groundwater Treatment
Sys ems Check one:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.1 , Specific Conductance 572 uMhos
Temp. 17.4 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT#: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 12/28/04
Date sample analyzed: 12/28/04 to 1/20/05
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total 5
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
400
7.2
5.3
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
17.6
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
uMhos
mg/I
mg/I
X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified X
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
0.008 mg/I
N/A mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
<0.001 mg/1
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes No )
N/A
N/A
NIA
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
<0.005 mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
0.51
N/A
N/A
N/A
N/A
N/A mg/I VOC
<0.010 mg/I
method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name end Title - Please typ or print
fP A
Signature of Permittee (or Authorized Agent)
(Date)
z�v� S—

PCS Phosphate Co., Ini Tank Farm Remed'aation Im Quarterly Monitoring
Date:
Time:
Tech:
A//7
az-
System Gau
a Pressures
SWW-1
`"
SWW-7
p-C%3 i31
CWW-1
--
CWW-7
1- /9 .®62.-
File: 12-07-02
pc: 11J3
RM.nnw
Poet MSL
Level R.I
W MBL
Ditch
12.91
7/'H
Barge Slip
10.59
/.'f 1
Water Level
Control Tank
'h=MSL
ay/
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
S. 91
4. 4.14
Cpz-1
10.51
/e! •i!4/
tot ei 7
Spz-2
11.21
A 5t'
S. 9/
Cpz-2
10.25
//. lb
- e%• 9/
Spz-3
11.87
l • 7t9
...577 r%
Cpz-3
11.12
/.0. 8-9
e.37.2
Spz-4
11.45
/O. /..2G9
.J S %
CPW
9.65
40. ✓&
- 0-8
Spz-5
11.45
9/4'
07..5-'
MWTF-1A•
14.35
%:.C/
/P. /'/
Spz-6
11.23
7.57
/64
MWTF-1B•
14.36
//. d.9.9
9:
Spz-7
11.59
9. 9e
./i Gee(
MWTF-1C•
14.44
/./• '0
d SeV
Spz-8
11.57
9. '%G
AA"/
MWTF-2A
14.05
O. 4/7
7.j b
Spz-9
11.01
7 93
5. -4
MWTF-28
14.02
/0. 74%
SAY'{'^,
Spz-10
12.16
6P. 'l'
Jam. 90
MWTF-2C
14.08
/y; 99
w&•'Lc
SPW
9.95
/%/ 15
r'i/Of.3
MWTF-3A
12.21
S. da
R. `/g
MWTF-3B
12.18
. 94
'So,
MWTF-3C
12.19
/ '. `voq
- /ay
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft
Pump
Activation Depth
Rel MSL
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping?
(y)es/(NZo
Comments
SWW-1
10.70
a' 7
6'
4.4. 96-
+1'to+2'
ir'
CWW-1
10.60
&'''.. //✓''.
9'
v/' '.J6--
-2'to-1'
Ir
SWW-2
9.99
7 `%//
6'
> 9/
+1'to+2'
Y
CW W-2
10.23
7. 8
9'
e. 7
-2' to -l'
7
)
SWW-3
9.97
'7 '%/
6'
1• 7/
+1'to+2'
I
CWW-3
9.95
6. 9 9
9'
..i /
-2'to-1'
Y
SWW-4
10.73
7...57
6'
�y
/,. 57
+1 'to+2'
ci
W CW-4
10.73
41.5-a
9'
#`/€
-2'to-1'
SWW-5
10.80
• .7 3&
6'
/J
+1' to+2'
:✓
CWW-5
10.74
6-.OS
9'
`j 97
-2'to-1'
i
SWW-6
10.66
%K/(o
6'
/:94
+1' to+2'
��'
CWW-6
9.92
/ ' /
9'
-ere.
-2'to-1'
SWW-7
10.70
'7 re)
6'
/ J O
+1' to+2'
CWW-7
9.95
LJ `//%
9'
'S. /
-2' to-1'
Revised 7/29/02
• Riser length added to TOC elevation 1/24/97
D:1DatetForms\Well Form\Tank Farm Remed Wellsads

PCS PHOSPHATE.- TANK FARM REMEDIAL ACTION PLAN
OUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
August 2004 — October 2004
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system until
October 13, 2004 when the injection well system was shutdown to replace the filters and Ultraviolet Light
disinfection system. The new equipment installation was completed and brought online on October 24,
2004. The system operated with frequent trips, resulting in the replacement of the controller for the UV
System. Troubleshooting and optimization of the system continues with assistance from Culligan Water
Conditioning. Preliminary sampling was conducted at the Water Level Control Tank and CIW — 7. Both
samples were sampled for total coliform. The sample results were 260 and 41 (mf), 100 Mls respectively.
The following steps were taken to troubleshoot, facilitate sterilization and prevent contamination of the
injection water.
1. Install sample tap valve on the discharge line from the UV columns.
2. Down stream of sample tap install a means to inject NaOCI into the discharge line using a metering
pump.
3. Seal the Water level control tank outside the building by having all of the bolts put in place. Currently
there are only 4 bolts securing the flange.
4. Replace the screen on the 1" air vent on top of the water level control tank.
A total of 15 gallons of 12% NaOC1 was metered into the system down stream of the UV system. Samples
were taken down stream of the UV prior to NaOC1 injection to insure the performance of the UV system.
Additional sampling was conducted at the Water Level Control Tank and CIW — 7 on December 28, 2004.
Both samples were sampled for total coliform. The sample results were 5 and 390 (mf), 100 Mls
respectively. The source of high coliform in CIW — 7 was suspected to be the result of a failure of the well
header system. The system was inspected and no comprise in the header was located. It is theorized that
the source of the coliform is groundwater entering the well when the injection well system trips or is
shutdown. Additional testing was performed on January 26, 2005 which supports this theory. The sample
results for the Water Level Control Tank and CIW — 7 were 2 and 12 (mf), 100 Mls respectively. This data
reflects improved performance of the injection well system. Additional testing to determine the source of
the coliform is in process.
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3

Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Aug
415,720
0
415,720
9.3
15.0
Sept
386,520
0
366,520
8.9
15.0
Oct
189,060
0
189,060
4.2
15.0
TOTALS
991,300
0
991,300
The DPW flow for November was 462,375 gallons for an average flow of 10.7 GPM.
Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Aug
296,935
129,194
426,129
9.5
Sept
321,003
142,702
463,705
10.7
Oct
470,947
116,029
586,976
14.1
TOTALS
1,088,885
387,924
1,476,809
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The flows for November are Sand Formation 359,390 gallons, Croatan Formation 107,463 gallons. The
total flow is 466,853 gallons or 10.8 GPM.
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 8/4 changed pump. On 8/23 shook pump. On 9/29 changed pump. On 10/5 repaired pump.
On 10/6 changed pump.
SWW-2: On 8/10 repaired counter. On 8/20 repaired counter. On 8/24 shook pump. On 9/14 changed
pump. On 9/23 replaced exhaust seat.
SWW-3: On 8/17 changed pump. On 8/24 shook pump. On 8/31 shook pump. On 10/8 changed airline.
On 10/11 changed pump.
SWW-4: On 8/9 repaired counter. On 8/17 changed counter. On 8/17 changed totalizer. On 9/27 changed
pump. On 10/25 flushed pump
SWW-5: On 8/18 changed totalizer. On 8/27 changed pump.
SWW-6:
SWW-7: On 8/2 shook pump. On 8/23 changed pump.
Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2:
CWW-3: On 8/4 changed counter. On 8/31 shook pump.
CWW-4: On 9/7 repaired counter.
CWW-5: On 9/14 acid washed pump. On 9/15 changed pump. On 10/6 changed counter.
CWW-6:
CWW-7:
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