WI0700012_1999 Monitoring (Report)_19990225

PCS
Phosphate AURORA DIVISION
P.O. BOX 48, AURORA, NC 27806
February 25, 1999
Underground Injection Control Program
Division of Water Quality, Groundwater Section
North Carolina DENR
P. O. Box 29578
Raleigh, North Carolina 27626-0578
Attention: Mark Milligan
Subject: First Quarterly Groundwater Monitoring Report for 1999
Injection Well Permit #WI0700012
PCS Phosphate Co., Inc.
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find enclosed, the 1st Quarterly Tank Farm Remedial Action System groundwater monitoring report
for 1999, per the requirements of the above referenced permit. Additional Compliance Monitoring Report
Forms for well CIW-7 and the WLCT are included in this report along with the monthly piezometer level
monitoring field sheets and a summary performance report of the individual wells.
Ioiith
Injected (gal)
Withdrawn (gal)
November
December
January
565,310
549,020
441,800
734,659
766,055
844,566
Totals
1,556,130
2,345,280
Please contact me at [phone] if you have any questions regarding this information.
Sincerely,
Karen C. West
Environmental Scientist
Attachments
pc: Willie Hardison - DWQ, WaRO (w/attch)

bpc: W. A. Schinnuing (w/o attch)
B. A. Peacock / 00-22-000 (w/o attch)
T. L. Baker/T. W. Davis (w/attch)
M. L. Asby / J. A. Hardy (w/attch)
15-03-003-02 (w/ attch)
12-01-008-03-002 (w/ attch)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter:
Screened Interval: 33.27 ft. to 52.68 ft.
4 inch
Depth to Water Level: 7.91 ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
_ Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2255 uMhos
Temp. 16.5 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE:
09/30/01
Non -Discharge x UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Uv
Lagoon Remediation: Infiltration Gaiter?
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
O
C./1
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
Date sample analyzed: 1/19/99 to 2/1/99 I
Laboratory Name: PCS PHOSPHATE
1/40
W
Certification No(s) 330 N/A
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1 Nitrate (NO3 as N)
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
1960 mg/I
6.6 nits
9.8 mg/I
65.9 mg/I
N/A mg/I
Grease and Oils N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
711.3 mg/1
N/A uMhos
N/A mg/I
N/A mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
1.930 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
r,JN/Af ug/I
r\)N/A? ug/I
N/A- ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
0.25
N/A
N/A
N/A
N/A
N/A ug/I VOC : method#
method#
method#
N/A ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (o thorize and Title - Please type or print
Z—L$
Signature of Perm' ee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
dram n,
Well Identification Number (from Permit): CWW-2
Well Depth: 52.15 ft. Well Diamter: 4 inch
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level: 7.54 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Sys erns Check one:
Influent (98)
Effluent (99)
Field Analysis: pH 6.1 , Specific Conductance 2443 uMhos
Temp. 18.7 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge X
NPDES
UIC
,TYPE OF PERMITTED OPERATION BEING MONITORED c.
Lagoon Remediation: Infiltration Gallery O1
Spray Field X Remediation : ---
Rotary Distributor Land Application of Sludge Cn
C)
Other G
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
1/19/99 to 2/1/99
Certification No(s)
330 N/A
0
xs•
tv
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
mg/I Nitrite (NO2 as N)
/100m1
/100m1
2044 mg/I
6.5 nits
10.5 mg/I
105.8 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/l
Specific Conductance
Total Ammonia
TKN as N
Nitrate (NO3 as N)
Yes
n/a
No and field acidified
N/A mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
5.750 mg/I
Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A mg/I Ammonia Nitrogen
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
701.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
(A _ iig/I
A citg/I
N/A Tg/l
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.19
N/A
N/A
N/A
N/A
N/A ug/I VOC : method#
method#
method#
N/A ug/I
mg/I
mg/I
ug/l
ug/I
ug/l
ug/l
(2)
I certify thatto the best of my knowledge and belief, the information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permitteuth .ze gent Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-3
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.25 ft. below measuring point.
3.08 ft above land surface.
For Groundwater Treatment
Sys errs Check One:
_ Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2477 uMhos
Temp. 25.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
09/30/01
UIC
W
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
1/19/99 to 2/1/99
Certification No(s) 330 N/A
tV
•
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1724
6.7
8.4
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
102.0
N/A
N/A
N/A
559.0
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
nits Ba - Barium
mg/I Ca - Calcium
mg/l Cd- Cadmium
mg/I Chromium: Total
mg/1 Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/1 Mg - Magnesium
mg/I Mn - Manganese
N/A ug/l VOC
N/A ug/I
4.975 mg/I Zn - Zinc
N/A mg/1 Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/l
N/A— ug/l
N/A ug/l
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
method#
0.22
N/A
N/A
N/A
N/A
mg/I
method#
method#
mg/I
ug/I
ug/l
ug/I
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations,
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee Auth 'zed jentLhlame and Title - Please type or print
404/1
Signature of Permittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level:
Measuring Point is
GALLONS
6.94 ft. below measuring point.
2.75 ft above land surface.
For Groundwater Treatment
Systems Check One:
FlInfluent (98)
Effluent (99)
of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2532 uMhos
Temp. 27.7 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
09/3o/01
UIC
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
to
440
Iva
Date sample analyzed: 1/19/99 to 2/1/99N)
Laboratory Name:
PCS PHOSPHATE
c.;..r
Certification No(s) 330 N/A
cf 1- t
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1752
6.7
8.4 mg/I Ca - Calcium
mg/1
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Orthophosphate
mg/I Al - Aluminum
nits Ba - Barium
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
5.340 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
103.6 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
566.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/1 Mn - Manganese
N/A ug/I
N/A ug/I
f
tv -r
ra Ni" / ug/I
N/A ug/I
N/A ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
0.15 mg/I
N/A ug/l
N/A ug/I Ag - Silver
N/A ug/I
N/A ug/I
Se- Selenium
Sodium
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC
N/A ug/I
method#
meth od#
method#
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of horized Ag a nd Title - Please type or print
Ari
Signsiurof Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-5
Well Depth: 53.17 ft. Well Diamter: 4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level: 7.86 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2046 uMhos
Temp. 30.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge X
NPDES
EXPIRATION DATE:
UIC
09/30/01
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field _ X Remediation :
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and to cn
colloidal concentrations
to
Date sample collected: 1/19/99 g3.. n
Date sample analyzed: 1/19/99 to 2/1/99 -,-
Laboratory Name: PCS PHOSPHATE i v ;
Certification No(s) 330 N/A
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1272
pH (when analyzed) 6.6
TOC 7.3
Chloride 82.3
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
342.9
N/A
N/A
N/A
mg/I
nits
mg/I
mg/1
mg/I
mg/I
mg/I
mg/l
uMhos
mg/1
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
8.900 mg/1
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
c:�
N/ '9ug/I
NIPNIt ug/I
N//Se ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
Se- Selenium
Sodium
0.17
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
method#
method#
mg/I
mg/1
ug/I
ug/I
ug/I
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of A zed nt d Title - Please type or print
y! — 7
Signat re o Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-6
Screened Interval: 36.62 ft. to 50.88 ft.
4 inch
Depth to Water Level: 6.86 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 1845 uMhos
Temp. 31 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC
09/03/01
TYPE OF PERMITTED OPERATION BEING MONITORED
0
0
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor
Other
Land Application of Sludge
C.)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
1/19/99
1/19/99 to 2/1 /99
PCS PHOSPHATE -
Certification No(s) 330 N/A
PARAMETERS: (Samples for metals
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
were collected
mg/I
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1124
6.7
8.2
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
94.5
N/A
N/A
N/A
254.3
N/A
N/A
N/A
mg/I
nits
mg/I
mg/I
mg/I
mg/I
mgll
mg/I
uMhos
mgll
mg/I
unfiltered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified Yes n/a No) h) =-
N/A mg/1 Ni - Nickel \'') NIA ug/I
N/A mg/I Pb - Lead N/A ug/I
8.050 mg/I Zn - Zinc N/A ug/I
N/A mg/1 Ammonia Nitrogen mg/I
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/1 Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
0.20
N/A
N/A
N/A
N/A
mgll
ug/I
ug/I
ug/I
ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC
N/A ug/I
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true.
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of orize� and Title -Please type or print
Sig ture of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-7
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 36.58 ft. to 50.83 ft.
4 inch
Depth to Water Level: 7.02 ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 1276 uMhos
Temp. 24.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge X
NPDES
EXPIRATION DATE:
UIC
09/03/01
CD
TYPE OF PERMITTED OPERATION BEING MONITORED "
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
%la
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
1 /19/99
1 /19/99 to 2/1 /99
PCS PHOSPHATE
330 N/A
s
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 856
pH (when analyzed) 7.0
TOC 7.0
Chloride 70.5
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
169.8
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
nits
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/l
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
nla
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
1.700 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A ug/l
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Se- Selenium
Sodium
N —i
NIA ug/I
N/A ug/I
N/A ug/I
0.19
N/A
N/A
N/A
N/A
mg/I
mg/I
ug/I
ug/l
ug/I
ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
method#
method#
N/A ug/I
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of oriz// isar tyre and Title Please type or print
// 7 Ls -ff
(Date)
Signature of Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.94 ft. below measuring point.
1.52 ft above land surface.
For Groundwater Treatment
Systerrs Check One:
lInfluent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2622 uMhos
Temp. 19.5 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A /100m1 Nitrate (NO3 as N)
N/A /100m1 Phosphorus: Total as P
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 09/30/01
Non -Discharge X UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation:
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
%.O
CD
Infiltration Gallery
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
Date sample analyzed: 1/19/99 to 2/1/99
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 N/A
No and field acidified Yes n/a No )
N/A mg/I
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1880
pH (when analyzed) 6.4
TOC 10.7
Chloride 39.2
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate 880.9
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
mg/I
nits
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
uMhos
mg/I
mg/I
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
N/A mg/1
148.000 mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
IN)
m
1- V/A t? ug/I
Nisl/A c—, ug/I
N/A" ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/l Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.57
N/A
N/A
N/A
N/A
N/A ug/I VOC
N/A ug/I
method#
method#
method#
mg/I
mg/1
ug/I
ug/I
ug/I
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true.
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurateand complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee or ed A...soze and Title - Please type or print
Signature of Permi ee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 7.27 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
For Groundwater Treatment
Systems Check One:
FlInfluent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2171 uMhos
Temp. 19.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
UIC
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
c-7.)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
1/19/99 to 2/1/99
Certification No(s)
330 N/A
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1452
pH (when analyzed) 6.6
TOC 8.9
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
34.2
N/A
N/A
N/A
666.5
N/A
N/A
N/A
No and field acidified
mg/I Nitrite (NO2 as N) N/A mg/I
/100m1 Nitrate (NO3 as N) N/A mg/I
/100m1 Phosphorus: Total as P 74.500 mg/I
Orthophosphate N/A mg/I
mg/1 Al - Aluminum N/A ug/I
nits Ba - Barium N/A ug/l
mg/I Ca - Calcium N/A ug/I
mg/I Cd- Cadmium N/A ug/l
mg/I Chromium: Total N/A ug/I
mg/I Cu - Copper N/A ug/I
mg/I Fe - Iron N/A ug/l
mg/I Hg - Mercury N/A ug/I
uMhos K- Potassium N/A ug/I
mg/I Mg - Magnesium N/A ug/I
mg/I Mn - Manganese N/A ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.21 mg/I
MIRK N/A ug/I
Ag - Silver N/A ug/I
N/A ug/I
N/A ug/1
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
Yes n/a No )
Se- Selenium
Sodium
VOC
method#
: method#
: method#
ry N/A ug/I
N/A ug/I
I certify thatto the best of my knowledge and belief, the information submitted in this report is true.
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information. including the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee #46107ed 11.017and Title - Please type or print
.•-• ss"p,
ignature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 24.50 ft. Well Diamter:
SWW-3
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.62 ft. below measuring point.
3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
TlInfluent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 2113 uMhos
Temp. 24.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
09/30/01
UIC
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
LO
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
1/19/99 to 2/1/99
Certification No(s) 330 N/A
fV
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/I
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1280 mg/I
pH (when analyzed) 6.3 nits
TOC
8.3 mg/I
Chloride
Arsenic
34.1 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
542.2 mg/I
N/A uMhos
N/A mg/1
N/A mg/I
Hg - Mercury
n/a
No and field acidified
N/A mg/I Ni - Nickel
116.500 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
Yes n/a No )
N/A ug/I
N/A ug/I
N/A ug/I
ry
' N/A • ug/I
N/A - ug/l
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
0.16
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
method#
method#
N/A ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permitteeeame and Title - Please type or print
l—Ls-9f
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter:
Screened Interval: 20.50 ft. to 23.30 ft.
4 inch
Depth to Water Level: 6.95 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
LI Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2528 uMhos
Temp. 31.7 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1484
pH (when analyzed) 6.4
TOC 8.8
Chloride 50.7
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
650.6
N/A
N/A
N/A
mg/l
/100m1
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I
nits
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Al - Aluminum
Ba - Barium
Ca - Calcium
Yes n/a
Mail Original
to
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 N/A
No and field acidified Yes n/a No )
U0
1/19/99 to 2/1/99
m_7?
Nitrite (NO2 as N) N/A mg/I Ni - Nickel Ny N/A ,,ug/I
Nitrate (NO3 as N) N/A mg/1 Pb - Lead N// ug/I
90.500 mg/I Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen mg/I
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride 0.13 mg/I
N/A ug/I MIBK N/A ug/I
Cd- Cadmium N/A ug/I Ag - Silver N/A ug/I
Chromium: Total N/A ug/1 Se- Selenium N/A ug/I
Cu - Copper N/A ug/I Sodium N/A ug/I
Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC)
Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.)
K- Potassium N/A ug/I Report attached? Yes (1) No X (2)
Mg - Magnesium N/A ug/I VOC method#
Mn - Manganese N/A ug/I : method#
method#
certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee thor' d 1.0.0.79nd Title - Please type or print
z -�s-yF
ignature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter: 4 inch
Screened Interval: 24.83 ft. to 24.83 ft.
Depth to Water Level:
Measuring Point is
GALLONS
7.40 ft. below measuring point.
2.96 ft above land surface.
For Groundwater Treatment
Systems Check One:
_Influent (98)
Effluent (99)
of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2519 uMhos
Temp. 29.3 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/1
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1624 mg/1
pH (when analyzed) 6.6 nits
TOC 7.3 mg/I
Chloride 61.5 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol
Sulfate 679.0 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
n/a
Lagoon
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
09/30/01
UIC
Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Cn
f'l
Note: Values should reflect dissolved and
colloidal concentrations
1/19/99
1/19/99 to 2/1/99
PCS PHOSPHATE
330 N/A
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
26.000 mg/I
NIA mg/1 Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
IU
(NJ —i
NN/AE3 ug/I
N/A- ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.24
N/A
N/A
N/A
N/A
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
N/A ug/I
: method#
: method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false informationincluding the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Si•nature of Permitfee (or Authorized Agent) (Date)fr
Permute horiz d A.//A and Title - Please type or print

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name:
Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 26.00 ft. Well Diamter:
SWW-6
4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.03 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1996 uMhos
Temp. 29.7 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N) N/A mg/l
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 72.000 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I
Dissolved Solids: Total 1236 mg/I Al - Aluminum N/A ug/I
pH (when analyzed) 6.5 nits Ba - Barium N/A ug/I
TOC 12.2 mg/I Ca - Calcium N/A ug/I
112.9 mg/I Cd- Cadmium N/A ug/I
N/A mg/I Chromium: Total N/A ug/I
N/A mg/I Cu - Copper N/A ug/I
N/A mg/I Fe - Iron N/A ug/I
275.4 mg/I Hg - Mercury N/A ug/I
N/A uMhos K- Potassium N/A ug/1
N/A mg/I Mg - Magnesium N/A ug/I
N/A mg/I Mn - Manganese N/A ug/l
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 09/30/01
Non -Discharge UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
1/19/99 to 2/1/99
tO
Certification No(s) 330 N/A
No and field acidified Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
cn
r�.
ry Ni "°ug/t
N.) N/A ug/I
N/A:: ug/l
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.10
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC
method#
method#
method#
mg/I
mg/I
ug/I
ug/l
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee uthori ed nt ame and Title - Please type or print
f"f
gnature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jimmy Hardy
County: Beaufort
Telephone:
[phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter: 4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
7.14 ft. below measuring point.
3.00 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.6 , Specific Conductance 1485 uMhos
Temp. 26.9 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/l Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC
09/30/01
ILO
TYPE OF PERMITTED OPERATION BEING MONITORED •
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery.
X Remediation :
Land Application of Sludge —
cs
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/19/99
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
1/19/99 to 2/1/99
Certification No(s) 330 N/A
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
1064 mg/I Al - Aluminum
6.0 nits Ba - Barium
13.7 mg/I Ca - Calcium
Chloride
Arsenic
90.5 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
90.500 mg/I
N/A mg/1 Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
r'v -.
r\)N/AF-, ug/I
N/A-- ug/I
N/A ug/I
mg/I
0.12 mg/I
N/A ug/l
N/A ug/l Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
277.5 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC. GC/MS, HPLC)
N/A ug/I (Specify test method #.
N/A ug/I Report attached? Yes
N/A ug/I VOC
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that. to the best of my knowledge and belief. the information submitted in this report is true, accurate.
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am awa
false information, including the possibility of fines and imprisionment for knowing violations.
and complete, and that the laboratory analytical data was produced
re that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of orize Agent) Na e and Title - Please type or print
nature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter:
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level:
2 inch
3.68 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
For Groundwater Treatment
Systems Check One:
Fi Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 7.2 , Specific Conductance 539 uMhos
Temp. 14.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
to
O
rn
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/20/99
Date sample analyzed: 1/20/99 to 2/1/99
in
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 N/A
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
No and field acidified
N/A mg/1 Ni - Nickel
N/A mg/I Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
316 mg/1 Al - Aluminum
7.4 nits Ba - Barium
4.7 mg/I Ca - Calcium
8.6 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
0.610 mg/I Zn - Zinc
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
13.3 mg/1 Hg - Mercury
Yes n/a No )
ry N/F;r. _ug/I
r'.N/A ug/I
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
1.93
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC
N/A ug/I
method#
meth od#
method#
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee of Autt19rized /)g�nt)Qfame and Title - Please type or print
.M.l� 2,b5-^9,rT
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter:
Screened Interval: 10.60 ft. to 12.60 ft.
2 inch
Depth to Water Level: 4.58 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
For Groundwater Treatment
Systems Check One:
TlInfluent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 5.8 , Specific Conductance 473 uMhos
Temp. 18 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI070001 2
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge t]
IV
EXPIRATION DATE:
09/30/01
UIC
0
0
Remediation: Infiltration Galleryo71
Other
Note: Values should reflect dissolved andtO
�p
colloidal concentrations
Date sample collected: 1/20/99 A
Date sample analyzed: 1/20/99 to 2/1/99
Laboratory Name: PCS PHOSPHATE fV
Certification No(s) 330 N/A
4
PARAMETERS: (Samples for metals were collected
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 296
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.1
3.6
58.6
N/A
N/A
N/A
39.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
nits
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
unfiltered
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Yes n/a No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
7.600 mg/I Zn - Zinc
N/A mg/I
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/l
N/A ug/I
N/A ug/I
Ammonia Nitrogen
—' rr::+s
rV N/P4 ug/I
ry N/43 ug/I
N/f :47ug/l
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.31
N/A
N/A
N/A
N/A
N/A ug/I VOC : method#
method#
: method#
N/A ug/I
mg/I
mg/l
ug/l
ug/I
ug/I
ug/I
(2)
I certify that. to the best of my knowledge and belief. the information submitted in this report is trueaccurate. and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock -
Perm
Aut
a• - , Environmental Affairs
ame and Title - Please type or print
2-oaf—ff
Signature of
ermittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
* WELL OUT OF COMMISSION
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-C*
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
Milliliters of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge X UIC
09/30/01
NPDES Non Dischargekia
TYPE OF PERMITTED OPERATION BEING MONITORED o
Lagoon Remediation: Infiltration Galirary
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
to
PCS PHOSPHATE
330
rc7
N
r)
elm
am
cw c-r
rn
3
ri
'+i
PARAMETERS: (Samples for metals were collected unfiltered X Yes No
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
Use MPN method for highly turbid samples)
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/l
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
N/A
and field acidified X
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Ni- Nickel
Pb - Lead
Zn - Zinc
Yes No )
Ammonia Nitrogen
N/A ug/I
Other (Specify Compounds and Concentration Units)
mg/I
Fluoride N/A mg/I
MIBK N/A ug/I
Ag - Silver N/A ug/I
Se- Selenium N/A ug/I
Sodium N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
aiNstGtney
Permitted ut oriz) Name and Title - P(ase type or prin
* NOTE: WELL DAMAGED, NO SAMPLE
GW-59 Rev 4/98
zS—lei
Signature of Perfhittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): CIW-7
Well Depth:
n/a ft. Well Diamter: 4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level:
N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
F]Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.3 , Specific Conductance 446 uMhos
Temp. 15.3 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE: 09/30/01
UIC
0
TYPE OF PERMITTED OPERATION BEING MONITORED '`n
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
k_n
1.0
t C3.c.
Date sample collected: 1/20/99 :v '=rs1
Date sample analyzed: 1/20/99 to 2/1/99 Z.
Laboratory Name: PCS PHOSPHATEIENVIROIiMENT
Certification No(s)
Note: Values should reflect dissolved and
colloidal concentrations
330 10 N/A _ r^�
PARAMETERS: (Samples for metals were collected
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total <1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 318
pH (when analyzed) 7.7
TOC 4.4
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
8.5
N/A
N/A
N/A
28.8
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
nits
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
uMhos
mg/I
mg/I
unfiltered X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified X
N/A
N/A
0.246
N/A
N/A
N/A
N/A
<1.0
<5.0
N/A
N/A
N/A
N/A
N/A
46.0
mg/I
mg/I
mg/l
mg/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Ni - Nickel
Pb - Lead
Yes No )
Zn - Zinc
Ammonia Nitrogen
rN)
N/A— ug/I
N/A ug/I
N/A ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.63
N/A
N/A
N/A
N/A
VOC method#
method#
method#
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify thatto the best of my knowledge and belief: the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permi izede and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: N/A ft. Well Diamter:
WLCT
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level:
Measuring Point is
N/A
N/A ft. below measuring point.
N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
ri Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.6 , Specific Conductance 451 uMhos
Temp. 15.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES (11_
TYPE OF PERMITTED OPERATION BEING MONITORED
CD
Lagoon Remediation: Infiltration Ga 1e
Spray Field X Remediation :
30/01
EXPIRATION DATE:
UIC
Rotary Distributor Land Application of Sludge
Other
tO
l!]
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
c c-i
rr1
1/20/99 N r
1/20/99 to 2/1/99
PCS PHOSPHATE/ENVIRO_AMEN1ti
Certification No(s) 330 10
N/A•,�-`�
PARAMETERS: (Samples for metals were collected unfiltered
X Yes
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100mI Nitrate (NO3 as N)
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 316 mg/I Al - Aluminum
pH (when analyzed) 7.5 nits Ba - Barium
TOC 4.2 mg/I Ca - Calcium
Chloride 5.9 mg/I Cd- Cadmium
0.026 mg/I
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
Arsenic N/A mg/I Chromium: Total
Grease and Oils N/A mg/I Cu - Copper
Phenol N/A mg/I Fe - Iron
Sulfate <10.0 mg/I Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
N/A ug/I
N/A ug/I
<1.0 ug/I
<5.0 ug/I
N/A ug/I
N/A uMhos K- Potassium
N/A ug/I
N/A ug/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
Ni
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.63
N/A
N/A
N/A
N/A
N/A ug/I VOC
<10.0 ug/I
method#
: method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify thatto the best of my knowledge and beliefthe information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permitteeize t ame and Title - Please type or print
?
ignature of Pe ittee (or Authorized Agent) (Date)