WI0700012_Monitoring (Report)_20171122

tk PotashCorp'
Helping Nature Provide
November 17, 2017
Inactive Hazardous Sites Branch
Attn: Sue Murphy
UIC Program Staff
1636 Mail Service Center
Raleigh, NC 27699-1636
RECEIVED/NCDEQ/D WR
NOV 2 2 2017
Water Quality
Regional Operations Section
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
August 2017 — October 2017
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
PotashCorp - Aurora
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed is the summary operational and maintenance
report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this information.
Sincerely,
/6 cut/4 /J..7r.
D. Daniel Winstead III
Senior Environmental Engineer
PCS Phosphate
Attachments
1530 NC Hwy 306 South, Aurora, NC USA 27806 T [phone]
PotashCorp. I www.potashcorp.com

pc: Will Hart — Aquifer Protection DWQ, WaRO (w/ attachments)
12-07-02 (w/ attachments)
Alex Hunt (w/ attachments)
R. B. Lee (w/ attachments)
Electronically submitted: Inactive Hazardous Sites Branch
Attn: Sue Murphy
R:\Reports\2017\Quarterly\TFRAS Report Third Quarter 2017.docx
2

is
PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
OUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
August 2017 — October 2017
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Infection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
during the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
August
229,538
0
229,538
5.1
15.0
September
186,123
0
186,123
4.3
15.0
October
192,439
0
192,439
4.3
15.0
TOTALS
608,100
0
608,100
H:\Reports\2017\Quarterly\TFRAS Report Third Quarter 2017.docx
3

l 1It
Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
August
1,481,740
1,146,201
2,627,941
58.9
September
1,530,833
1,147,774
2,678,607
64.1
October
1,050,611
1,644,376
2,694,987
60.4
TOTALS
4,063,184
3,938,351
8,001,535
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the system were experienced. Details of these activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 9/6 pulled and cleaned pump.
SWW-2:
SWW-3:
S W W-4: On 10/31 pulled for cleaning.
SWW-5:
SWW-6:
SWW-7: On 10/18 replaced counter.
H:\Reports\2017\Quarterly\TFRAS Report Third Quarter 2017.docx
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2:
CWW-3:
CWW-4:
CWW-5:
CWW-6:
CWW-7:
R:\Reports\2017\Quarterly\TFRAS Report Third Quarter 2017.docx
5

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Mail Original
and 1 copy to:
DEPARTMENT OF ENVRRONMENNNT &AfiA1tiRAL RESYIIIRGES
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH, NC 27626-1617 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
PERMIT #:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
WI0700012
EXPIRATION DATE:
UIC X
01131 /18
18
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter: 4 inch
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level: NIA ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Water Source Heat Pump
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 5560 uMhos
Temp. 20.4 oC, Odor NONE Appearance: CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/12/2017
10/12/2017 to 10/17/2017
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here:
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 3400
pH (when analyzed) 6.2
TOC 2.4
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
810.0
N/A
N/A
N/A
1240.0
N/A
N/A
N/A
mg/L
/100mL
/100mL
mg/L
units
mg/L
mg/L
ug/L
mg/L
mg/L
mg/L
uMhos
mg/L
mg/L
Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
n/a
No
N/A
N/A
14.100
N/A
N/A
N/A
N/A
N/A
N/A
Cu - Copper N/A
Fe - Iron N/A
Hg - Mercury N/A
K- Potassium N/A
Mg - Magnesium N/A
Mn - Manganese
N/A
and field
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
mg/L
ug/L
acidified Yes nla No )
Ni - Nickel N/A ug/L
Pb - Lead N/A ug/L
Zn - Zinc N/A ug/L
Ammonia Nitrogen mg/L
Other (Specify Compounds and Concentration Units)
Fluoride <0.3 mg/L
MIBK N/A ug/L
Ag - Silver N/A ug/L
Se- Selenium N/A ug/L
Sodium N/A ug/L
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE.
GW-59 Rev 4/98
Mark D. Johnson. General Manager
Permittee (Qf {+uthonzed Agent) Name and Title - Please type or print
SSA ti l [76a1
Signature o Permittee (or Authorized Agent) (Dat )

GROUNDWATER
COMPLIANCE
QUALITY MONITORING:
REPORT FORM
DEPARTMENT:
Mail Original DIVISION
and 1 copy to: 1647
RALEIGH,
OF
MAIL
SERVICE
NC
OF ENVRONMENT a, NATURAL RESOURCES
WATER RESOURCES -INFORMATION PROCESSING
CENTER
27626-1617 Phone: [phone]o6.
UNIT
FACILITY INFORMATION
PERMIT #: WI0700012 EXPIRATION DATE: 01/31/18
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Non -Discharge UIC X
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Spray Field X Remediation :
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
Well Identification Number (from Permit): CWW-2
For Groi ndwater Treatment
Well Depth: 52.15 ft. Well Diamter: 4 inch
Systems Check One:
Screened Interval: 30.57 ft. to 49.82 ft.
Influent (98)
Note: Values should reflect dissolved and
If WELL WAS
colloidal concentrations
Date sample collected: 10/12/2017
DRY at time
of sampling,
Depth to Water Level: N/A ft. below measuring point.
Effluent (99)
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling: N/A
Date sample analyzed: 10/12/2017 to 10/12/2017
check
Laboratory Name: PCS PHOSPHATE
here:
Field Analysis: pH N/A , Specific Conductance NIA uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
Certification No(s) 330 10
,f
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
(Note. Use MPN method for highly turb
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/L
/100mL
/100m
units
mg/L
mg/L
ug/L
mg/L
mg/L
mg/L
uMhos
mg/L
mg/L
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total a
Yes
nla
No
N/A
N/A
N/A
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
and field acidified Yes
mg/L Ni - Nickel
mg/L Pb - Lead
%a4/I— %a Zt ariilc
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
mg/L
ug/L
Fluoride
MIBK
Ag - Silver
Se- Selenium
nla
No)
NIA
N/A
N/A
u an c ncentration Units)
Sodium
Organics: (GC. GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
VOC
(1) No
method#
method#
method#
N/A
N/A
N/A
N/A
N/A
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
X (2)
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations
NOTE.
GW-59 Rev 4/98
Mark D. Johnson. General Manager
Permittee !ofluthorized Agent) Name and Title - Please type or print
Signature Permittee (or Authorized Agent)
t\i15�2�
Date)

GROUNDWATER QUALITY MONITORING
COMPLIANCE REPORT FORM
Mail Original ;
and 1 copyto
i.
F�PAkRiMENT OF ENVi#2btNT $NATURAL RESOURCES
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
I
!&>t7:MAIL SERVICE CENTER
F it-EtGH, NC 27626-1617: Phone_, (919) 807.6p06
FACILITY INFORMATION
PERMIT #: WI0700012 EXPIRATION DATE: 01/31/18
Non -Discharge UIC X
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
NPDES
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Aurora, NC 27806 County: Beaufort
Spray Field X Remediation :
Contact Person: Danny Winstead Telephone: [phone]
Rotary Distributor Land Application of Sludge
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Other Water Source Heat Pump
Well Identification Number (from Permit): CWW-3
For Groundwater Treatment
Well Depth: 53.00 ft. Well Diamter: 4 inch
Systems Check One:
Screened Interval: 36.42 ft. to 50.67 ft.
Influent (98)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/12/2017
If WELL WAS
DRY at time
of sampling,
Depth to Water Level: N/A ft. below measuring point.
Effluent (99)
Measuring Point is 3.08 ft above land surface.
Date sample analyzed: 10/12/2017 to 10/19/2017
check
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Laboratory Name: PCS PHOSPHATE
here:
Field Analysis: pH 6.4 , Specific Conductance 7500 uMhos
Certification No(s) 330 10
Temp. 22.8 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 4590
pH (when analyzed) 6.2
1.7
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/L
/100mL
/100mL
mg/L
units
mg/L
1740.0 mg/L
N/A ug/L
N/A mg/L
N/A mg/L
1030.0 mg/L
N/A uMhos
N/A mg/L
N/A mgfL
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
n/a
No
N/A
Phosphorus Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium _
and field acidified
mg/L
N/A mg/L
30.750 mg/L
N/A mg/L
N/A mg/L
N/A ug/L
N/A mg/L
Cd- Cadmium N/A ug/L
Chromium: Total N/A ug/L
Cu - Copper N/A mg/L
Fe - Iron N/A ug/L
Hg - Mercury N/A ug/L
K- Potassium N/A mg/L
Mg - Magnesium N/A mg/L
Mn - Manganese N/A ug/L
Yes
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
n/a
No)
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS
(Specify test method #
Report attached? Yes
VOC
<0.3
N/A
N/A
N/A
N/A
•
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTF
GW-59 Rev 4/98
Signature oPermittee (or Authorized Agent)
Mark D. Johnson, General Manager
Permittee (f fwthorized Agent) Name and Title - Please type o print
i1115L'2.G1i
(Da

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DEPARTMENT OF ENVIRONMENT & NATI/RAi RESOURCES
Mail Original DIVISION OF WATER RESOURCES•INFORMATION PROCESSING UNIT
and 1 copy to: 1617 MAIL SERVICE CENTER
6
RQLEIGti NC 27626 1617 Phone: [phone]
FACILITY INFORMATION
PERMIT #: WI0700012 EXPIRATION DATE: 01/31/18
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Non -Discharge UIC X
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Spray Field X Remediation :
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
Well Identification Number (from Permit): CWW-4
For Groundwater Treatment
Well Depth: 53.00 ft. Well Diamter: 4 inch
Sys ems Check One:
Screened Interval: 41.67 ft. to 50.92 ft.
Influent (98)
Note: Values should reflect dissolved and
If WELL WAS
colloidal concentrations
Date sample collected: 10/12/2017
DRY at time
of sampling,
Depth to Water Level: N/A ft. below measuring point.
Effluent (99)
Measuring Point is 2.75 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Date sample analyzed: 10/12/2017 to 10/19/2017
check
Laboratory Name: PCS PHOSPHATE
here:
Field Analysis: pH 6.4 , Specific Conductance 5260 uMhos
Temp. 26.4 oC, Odor NONE Appearance: CLEAR
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 3170
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/L
/100mL
/100mL
mg/L
6.3 units
2.2 mg/L
860.0 mg/L
N/A ug/L
N/A mg/L
N/A mg/L
1090.0 mg/L
N/A uMhos
N/A mg/L
N/A mg/L
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
n/a
No
N/A
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
and field acidified
mg/L
N/A mg/L
17.580 mg/L
N/A mg/L
N/A mg/L
N/A ug/L
N/A mg/L
Cd- Cadmium N/A ug/L
Chromium: Total N/A ug/L
Cu - Copper N/A mg/L
N/A ug/L
N/A ug/L
K- Potassium N/A mg/L
Mg - Magnesium N/A mg/L
Mn - Manganese N/A ug/L
Fe - Iron
Hg - Mercury
Ni - Nickel
Yes
n/a
No)
N/A ug/L
Pb - Lead N/A ug/L
Zn - Zinc N/A ug/L
Ammonia Nitrogen mg/L
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
<0.3
N/A
N/A
N/A
N/A
Organics. (GC, GC/MS
(Specify test method #
Report attached? Yes
VOC
mg/L
ug/L
ug/L
ug/L
ug/L
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D. Johnson, General Manager
Permittee (of thorized Agent) Name and Title - Please type or print
Lure of
er
mittee rmittee (or Authorized Agent)
(Dab )

GROUNDWATER 0UALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
PERMIT #:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
DEPARTMENT OF ENVfRONMEt r:i3 iJililttti4i RESOURCES
.......... . ...................... .........
DWISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH NC 27626-1617 • Phone:' (919) 8O 4306
WI0700012
EXPIRATION DATE:
UIC X
01 /31 /18
18
Well Identification Number (from Permit):
Well Depth: 53.17 ft. Well Diamter:
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level: NIA ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
CWW-5
4 inch
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Water Source Heat Pump
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 3197 uMhos
Temp. 28,6 oC, Odor NONE Appearance: CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/12/2017
Date sample analyzed: 10/12/2017 to 10/17/2017
Laboratory Name:
Certification No(s)
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here:
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids. Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/L
/100mL
/100mL
2180 mg/L
6.2 units
5.1 mg/L
76.0 mg/L
N/A ug/L
N/A mg/L
N/A mg/L
1040.0 mg/L
N/A uMhos
N/A mg/L
N/A mg/L
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
nla
No and field acidified Yes
N/A mg/L
N/A mg/L
10.200 mg/L
N/A mg/L
N/A mg/L
N/A ug/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A mg/L
N/A ug/L
nla
No)
Ni- Nickel N/A ug/L
Pb - Lead N/A ug/L
Zn - Zinc N/A ug/L
Ammonia Nitrogen mg/L
Other (Specify Compounds and Concentration Units)
Fluoride <0.3 mg/L
MIBK N/A ug/L
Ag - Silver N/A ug/L
Se- Selenium N/A ug/L
Sodium N/A ug/L
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D. Johnson, General Manager
Permitteg (of 4u orized Agent) Name and Title - Please type or print
O H-S 11. 11
Signature of F`ermittee (or Authorized Agent) (Dat )

GROUNDWATER
COMPLIANCE
QUALITY MONITORING:
REPORT FORM
DEPARIVIENT:OF
Mail Original DIVISION
and 1 copy to: 16i7MAIL
RALEIGH,
ENVIRONMENT &
OF WATER RESOURCES -INFORMATION
SERVICE CENTER
NC 27626-1617' ': Phone::
NATURAL RESOURCES
PROCESSING
[phone]
UNIT
FACILITY INFORMATION
PERMIT #: W10700012 EXPIRATION DATE: 01/31/18
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Non -Discharge UIC X
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Spray Field X Remediation :
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
Well Identification Number (from Permit): CWW-6
For Groundwater Treatment
Well Depth: 53.00 ft. Well Diamter: 4 inch
Systems Check One:
Screened Interval: 36.62 ft. to 50.88 ft.
Influent (98)
Note: Values should reflect dissolved and
If WELL WAS
colloidal concentrations
Date sample collected: 10/12/2017
DRY at time
of sampling,
Depth to Water Level: N/A ft. below measuring point.
Effluent (99)
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Date sample analyzed: 10/12/2017 to 10/17/2017
check
Laboratory Name: PCS PHOSPHATE
here:
Field Analysis: pH 6.4 , Specific Conductance 2573 uMhos
Temp. 28.3 oC, Odor NONE Appearance: CLEAR
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 1560
pH (when analyzed) 6.2
TOC 5.8
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
67.0
N/A
N/A
N/A
755.0
N/A
N/A
N/A
mg/L
/100mL
/100mL
mg/L
units
mg/L
mg/L
ug/L
mg/L
mg/L
mg/L
uMhos
mg/L
mg/L
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
n/a
No
N/A
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
and field acidified
mg/L
N/A mg/L
20.400 mg/L
N/A mg/L
N/A mg/L
N/A ug/L
N/A mg/L
Cd- Cadmium N/A ug/L
Chromium: Total N/A ug/L
Cu - Copper N/A mg/L
N/A ug/L
N/A ug/L
K- Potassium N/A mg/L
Mg - Magnesium N/A mg/L
Mn - Manganese N/A ug/L
Fe - Iron
Hg - Mercury
Ni - Nickel
Yes
n/a
No)
N/A ug/L
Pb - Lead N/A ug/L
Zn - Zinc N/A ug/L
Ammonia Nitrogen mg/L
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS,
(Specify test method #.
Report attached? Yes
VOC
<0.3
N/A
N/A
N/A
N/A
mg/L
ug/L
ug/L
ug/L
ug/L
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D. Johnson General Manager
Permittee ( f uthorized Agent) Name and Title - Please type or print
4 "�2 11
Signature o Permittee (or Authorized Agent) ate)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DEPARTMENT 4F ENViROMN0NT & NATURAL RESOURCES
Mail Original DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
and 1 copy to: 1617 MAIL SERVICE CENTER
RALEIGH, NC 27626<1$IT Phone: [phone]
FACILITY INFORMATION
PERMIT #: WI0700012 EXPIRATION DATE: 01131/18
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Non -Discharge UIC X
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Spray Field X Remediation :
Well Locations/Site Name: Tank Farm No. of Wells to
be Sampled
18
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
Well Identification Number (from Permit): CWW-7
For
Systems
Groundwater
Treatment
Check One.
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Note: Values should reflect dissolved and
If WELL
DRY at time
of sampling,
check
here:
WAS
Depth to Water Level: N/A ft. below measuring point.
colloidal concentrations
Date sample collected: 10112/2017
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling: N/A
Date sample analyzed: 10/12/2017 to 10/12/2017
Field Analysis: pH N/A , Specific Conductance NIA uMhos
CLEAR
Laboratory Name: PCS PHOSPHATE
✓
Temp. N/A oC, Odor NONE Appearance:
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
NIA mg/L Nitrite (NO2 as N)
N/A /100mL Nitrate (NO3 as N)
/r1 /100mL Phosphorus: Total
(Note. Use MPN method for highly turbid , •n •
Dissolved Solids: Total r:, _I IL !� 1 i
pH (when analyzed) N/A units Ba - Barium
TOC N/A mg/L Ca - Calcium
Chloride N/A mg/L Cd- Cadmium
Arsenic N/A ug/L Chromium: Total
Grease and Oils N/A mg/L Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/L Fe - Iron
N/A mg/L Hg - Mercury
N/A uMhos K- Potassium
N/A mg/L Mg - Magnesium
N/A mg/L Mn - Manganese
Yes
n/a
No
N/A mg/L
N/A mg/L
'-• n Ilify
Nimg d nd ntration Units)
N/A ug/L Fluoride , 1 N/A mg/L
N/A mg/L MIBK N/A ug/L
NIA ug/L Ag - Silver N/A ug/L
n/a
No)
and field acidified Yes
Ni - Nickel
Pb - Lead
N/A ug/L
N/A ug/L
N/A ug/L
mg/L
N/A ug/L Se- Selenium N/A ug/L
N/A mg/L Sodium N/A ug/L
N/A ug/L Organics: (GC, GC/MS, HPLC)
N/A ug/L (Specify test method #. Attach lab report.)
N/A mg/L Report attached? Yes (1) No X (2)
N/A mg/L VOC method#
N/A ug/L
method#
method#
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE.
GW-59 Rev 4/98
Mark D Johnson. General Manager
Permitte
Authorized Agent) Name and Title - Please type or print
Date)
Signature of Permittee (or Authorized Agent)

GROUNDWATER
COMPLIANCE
REPORT
•
*QUALITY MONITORING
FORM
DEPARTMENT OF ENVIRONMENT &NATU RAL RESOURCES.
Mail Original DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
and 1 copy to: 1617 MAIL SERVICE CENTER
RALEFGH, NC 27626-161T Phone: [phone]
FACILITY INFORMATION
PERMIT #: WI0700012 EXPIRATION DATE: 01/31/18
Non -Discharge UIC X
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
NPDES
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Spray Field X Remediation :
Well Locations/Site Name: Tank Fami No. of Wells to be Sampled 18
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
Well Identification Number (from Permit): SWW-1
For Groundwater Treatment
Well Depth: 22.50 ft. Well Diamter: 4 inch
Systems Check One:
Screened Interval: 18.30 ft. to 21.12 ft.
Influent (98)
Note: Values should reflect dissolved and
If WELL WAS
colloidal concentrations
Date sample collected: 10/12/2017
DRY at time
of sampling,
Depth to Water Level: N/A ft. below measuring point.
Effluent (99)
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling: N/A
Date sample analyzed: 10/12/2017 to 10/12/2017
check
Laboratory Name: PCS PHOSPHATE
here:
Field Analysis: pH N/A , Specific Conductance NIA uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
Certification No(s) 330 10
V
PARAMETERS: (Samples for metals
COD
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids. Total
N/A
were collected unfiltered
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/L
/100mL Nitrate (NO3 as N)
/100mL
mg/L
ug/L
mg/L
mg/L
mg/L
uMhos
mg/L
mg/L
Nitrite (NO2 as N)
Yes
Phosphorus Total as P
Orthophosphate
-
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
n/a
No
N/A mg/L
and field acidified
N/A mg/L
N/A mg/L
N/A mg/L
N/A mg/
�Ig/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
Mg - Magnesium N/A mg/L
Mn - Manganese N/A ug/L
Yes
nla
No )
N/A ug/L
Pb - Lead N/A ug/L
Zn - Zinc N/A ug/L
Ammonia Nitrogen mg/L
r hCoi
Ni - Nickel
Ag - Silver
Se- Selenium
N/A
N/A
N/A
N/A
Sodium N/A
Organics: (GC. GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
method#
mg/L
ug/L
ug/L
ug/L
ug/L
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D. Johnson General Manager
Permitt e (f thonzed Agent) Name and Title - Please type or print
i
A 1
Signature o Permittee (or Authorized Agent) Dat

GROUNDWATER
COMPLIANCE
QUALITY
REPORT
MONITORING:
FORM
DEPARTMENT OF ENVIRONMENT". NATURAIRESOURCES
Mail Original DIVISION OF WATER RESOURCES-INFORMAf)QN
and 1 copy to: 1617 MAIL SERVICE CENTER
RALEIGH. NC 27626-1617 Phone: (919) 807
PROCESSING UNIT
63Qb...: . .
FACILITY INFORMATION
PERMIT #: WI0700012 EXPIRATION DATE: 01/31/18
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Non -Discharge UIC X
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Spray Field X Remediation :
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
Well Identification Number (from Permit): SWW-2
For Groundwater Treatment
Well Depth: 23.00 ft. Well Diamter: 4 inch
Systems Check One:
Screened Interval: 18.80 ft. to 21.63 ft.
Influent (98)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/12/2017
If WELL WAS
DRY at time
of sampling,
Depth to Water Level: N/A ft. below measuring point.
Effluent (99)
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling: N/A
Date sample analyzed: 10/12/2017 to 10/12/2017
check
Laboratory Name: PCS PHOSPHATE
here:
/
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
Certification No(s) 330 10
1/
PARAMETERS: (Samples for
COD
Coliform: MF Fecal
Coliform: MF Total
metals were collected unfiltered
NIA
N/A
N/A
(Note: Use MPN method for hi
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
sa t .les)
N/A
N/A
N/A
NIA
N/A
N/A
N/A
N/A
NIA
mg/L
/100mL
/100mL
a
mg/L
mg/L
ug/L
mg/L
mg/L
mg/L
uMhos
mg/L
mg/L
Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
rthophosDha`
Ca - Caum
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
n/a
No and field acidified Yes
N/A mg/L Ni - Nickel
N/A mg/L Pb - Lead
N/A mg/L Zn - Zinc
N/
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/L
ug/L
ug/L
mg/L
ugfL
ug/L
mg/L
mg/L
ug/L
n/a
No )
N/A
N/A
N/A
m itro:en
the
MIBK
Ag - Silver
Se- Selenium
and Concentration Units)
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No
VOC method#
method#
method#
NIA
N/A
N/A
N/A
N/A
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
X (2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D. Johnson, General Manager
Permittee ( A to horized Agent) Name and Title - Please type or print
Signature o Permittee (or Authorized Agent) (D te)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Mail Original
and 1 copy to:
PERMIT #:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
DEPARTMENT OF. EN ✓ ONMEFIT NATUR(Ck;RESOURCES
DIVISION OF WATER RESOURCES.INFORMA`11ON PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH, NC 27626-161T Phone: [phone]
WI0700012
EXPIRATION DATE:
UIC X
01/31/18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: N/A ft. below measuring point.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling: N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/12/2017
Date sample analyzed: 10/12/2017 to 10/12/2017
Laboratory Name:
Certification No(s)
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here: V
PARAMETERS: (Samples for metals were collected unfiltered ri Yes
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for
Dissolved Solids: Tota
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/L
/100mL
mL
n/a
No
Nitrite (NO2 as N) N/A
Nitrate (NO3 as N) N/A
Phosphorus: -:dotal as P
ril1(3
I
r
-
N/A mg/L Ca - Calcium
N/A mg/L Cd- Cadmium
N/A ug/L Chromium: Total
N/A mg/L Cu - Copper
N/A mg/L Fe - Iron
N/A mg/L Hg - Mercury
N/A uMhos K- Potassium
N/A mg/L Mg - Magnesium
N/A mg/L Mn - Manganese
N1YIg
and field acidified Yes
mg/L Ni - Nickel
mg/L
L Ii'
N/A "ug/L F u ride
N/A mg/L MIBK
N/A ug/L Ag - Silver
N/A ug/L
N/A mg/L
N/A ug/L
Se- Selenium
n/a
No )
N/A ug/L
N/A ug/L
N/A ug/L
( mg/L
Sodium
Organics: (GC, GC/MS, HPLC)
N/A ug/L
N/A ug/L
N/A ug/L
N/A ug/L
N/A ug/L (Specify test method #. Attach lab report.)
N/A mg/L Report attached? Yes (1) No X (2)
N/A mg/L VOC method#
N/A ug/L method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D Johnson. General Manager
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Itermittee (or Authorized Agent)
jr2!S 17C,,V)
ate)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
and 1 copy to:
PERMIT #:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
DEPAR7MENT:QF ENVtROt MEWT &NATURA i RESOURCES
DIVISION OF WATER RESOURCES -INFORMATION PROCESSENG UNIT
1617'MAIL SERVICE 'CENTER
RALEIGH, NC 27626-1617 Phone: [phone]
W10700012
EXPIRATION DATE:
UIC X
01/31/18
Well Identification Number (from Permit): _ SWW-4
Well Depth: 25.00 ft. Well Diamter: 4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
Measuring Point is
N/A ft. below measuring point.
3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Water Source Heat Pump
N/A
Field Analysis: pH N/A , Specific Conductance NIA uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/12/2017
10/12/2017 to 10112/2017
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here:
•
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/L
Coliform: MF Fecal N/A /100mL
Coliform: MF Total N/A /100mL
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus. Total
(Note Use MPN method for highly to • es rt• • • • • • - -
Dissolved Solids: Total , . , mg t i � r N
pH (when analyzed) A un -
TOC N/A mglL Ca - Calcium
Chloride N/A mg/L Cd- Cadmium
Arsenic N/A ug/L Chromium: Total
Grease and Oils N/A mg/L Cu - Copper
N/A mg/L Fe - Iron
N/A mg/L Hg - Mercury
N/A uMhos K- Potassium
N/A mg/L Mg - Magnesium
N/A mg/L Mn - Manganese N/A
Yes
nia
No
N/A
N/A
N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A mg/L
ug/L
and field acidified Yes
mg/L Ni - Nickel
mg/L Pb - Lead
mg/L Zinc
et
MIBK
Ag - Silver
Se- Selenium
nla
No )
N/A
N/A
N/A
centration Units)
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No
VOC • method#
method#
method#
ug/L
ug/L
ug/L
mg/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A ug/L
N/A ug/L
X (2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D. Johnson, General Manager
Permittee ( f uthorized Agent) Name and Title - Please type or print
�d rjJ-Cri
Signature o Permittee (or Authorized Agent) (Dat )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
(from rerr.
PERMIT #:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
DO:AlktNIENT OF ENVfIRONMENT &3JATURAL RESOURCES
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH, NC 27626-1617 Phone: [phone]
.. .. ...... .. ......... . ....... .
WI0700012
EXPIRATION DATE:
UIC X
01/31/18
Well Identification Number (from Permit):
Well Depth: 28.21 ft. Well Diamter:
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH N/A , Specific Conductance
Temp. N/A oC, Odor NONE
SWW-5
4 inch
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
NIA
N/A uMhos
Appearance: CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/12/2017
Date sample analyzed: 10/12/2017 to 10/12/2017
Laboratory Name:
Certification No(s)
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here:
PARAMETERS: (Samples for metals were collected
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/L
/100mL
/100mL
mg/L
ug/L
mg/L
mg/L
mg/L
uMhos
mg/L
mg/L
unfiltered
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
Yes
n/a
No and field acidified
N/A mg/L
N/A mg/L
N/A mg/L
N/A
N/A
Yes
n/a
No )
Ni - Nickel ug/L
Pb - Lead ug/L
Zn - Zinc ug/L
m•/L Am Nitro en mg/L
e `jYC tration Units)
ug a '� mg/L
N/A m u /L
N/A ug/L ug/L
N/A ug/L ug/L
ug/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A mg/L
N/A ug/L
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS,
(Specify test method #.
Report attached? Yes
VOC
HPLC)
Attach lab report.)
(1) No
method#
method#
method#
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
X (2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D. Johnson. General Manager
Permitt e (o A ttt horized Agent) Name and Title - Please type or print
v� �_ ( 5 .fit L
Signature of Permittee (or Authorized Agent) Date)

GROUNDWATER QUALITY: MONITORING
COMPLIANCE REPORT FORM
•
DEPARTMENT OF ENVIRONMENT & NATURAL
Mail Original ..DIVISION OF WATER RESOURCES -INFORMATION
and 1 copy to. 1617 MAIL SERVICE CENTER
RALEIGH, NC 27626.1617. >. Phone: (919)
807-6306
RESOURCES
PROCESSING
UNIT
FACILITY INFORMATION
PERMIT #: WI0700012 EXPIRATION DATE: 01/31/18
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Non -Discharge UIC X
NPDES
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Spray Field X Remediation :
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
Well Identification Number (from Permit): SWW-6
For Groundwater Treatment
Well Depth: 26.00 ft. Well Diamter: 4 inch
Systems Check One:
Screened Interval: 22.25 ft. to 24.62 ft.
Influent (98)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/12/2017
If WELL WAS
DRY at time
of sampling,
Depth to Water Level: N/A ft. below measuring point.
Effluent (99)
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Date sample analyzed: 10/12/2017 to 10/17/2017
check
Laboratory Name: PCS PHOSPHATE
here:
Field Analysis: pH 6.0 , Specific Conductance 2440 uMhos
Temp. 30.4 oC, Odor NONE Appearance: CLEAR
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/L
Coliform: MF Fecal N/A /100mL
Coliform: MF Total N/A /100mL
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1930 mg/L
pH (when analyzed) 5.8 units
7.0 mg/L
Chloride 47.0 mg/L
Arsenic N/A ug/L
Grease and Oils N/A mg/L
Phenol N/A mg/L
Sulfate 1250.0 mg/L
TOC
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/L
N/A mg/L
Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
n/a
No
N/A
and field acidified Yes
mg/L
N/A mg/L
228.000 mg/L
Ni - Nickel
Pb - Lead
Zn - Zinc
n/a
No)
N/A
N/A
N/A
N/A mg/L Ammonia Nitrogen
N/A mg/L Other (Specify Compounds and Concentration Units)
N/A ug/L Fluoride <0.3 mg/L
_ N/A mg/L MIBK N/A ug/L
Cd- Cadmium N/A ug/L Ag - Silver N/A ug/L
Chromium: Total N/A ug/L Se- Selenium N/A ug/L
Cu - Copper N/A mg/L Sodium N/A ug/L
Fe - Iron N/A ug/L
Hg - Mercury N/A ug/L
K- Potassium N/A mg/L
Mg - Magnesium N/A mg/L
Mn - Manganese N/A ug/L
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No
VOC : method#
method#
method#
ug/L
ug/L
ug/L
mg/L
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D. Johnson, General Manager
Permittee (of uthorized Agent) Name and Title - Please type or print
I.+11tl�.(7
Signature (f Permittee (or Authorized Agent) ( e)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
Mail Original
and 1 copy to:
PERMIT #:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
DEPARTMENT OF ENV ONMEN T $0m,UHA1: RESOURCES
DIVISION OF WATER RESO1,JRCE,S lNFQRMAT10N PROCESSING UNIT
3611 MAIL SERVICE CENTER :.'
RALEIGH, NC 27626-1617 Phone: (919)
WI0700012
8074306
EXPIRATION DATE:
UIC X
01/31/18
18
Well Identification Number (from Permit):
Well Depth: 29.50 ft. Well Diamter:
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
SWW-7
4 inch
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
N/A
Field Analysis: pH N/A , Specific Conductance N/A
uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/12/2017
10/12/2017 to 10/12/2017
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here:
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note. Use MPN method for highly turbid
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
N/A
N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/L Nitrite (NO2 as N)
/100mL Nitrate (NO3 as N)
Yes
�W /100mL s Phosphorus: Total as
/L I t rr �
Nix, _ units a - Barium
N/A mg/L Ca - Calcium
N/A mg/L Cd- Cadmium
N/A ug/L Chromium: Total
N/A mg/L Cu - Copper
N/A mg/L Fe - Iron
N/A mg/L Hg - Mercury
N/A uMhos K- Potassium
N/A mg/L Mg - Magnesium
N/A mg/L Mn - Manganese
n/a
No and field acidified
N/A mg/L
N/A mg/L
Ni - Nickel
Pb - Lead
Zn
N/A Nit "� �.►
/A mg tr, .e ' c
N/A ug/L uonde
N/A mg/L MIBK
N/A ug/L Ag - Silver
N/A ug/L
Yes
n/a
No )
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A mg/L
N/A ug/L
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach
Report attached? Yes
VOC
lab report.)
(1) No
method#
method#
method#
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
X
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 4/98
Mark D. Johnson, General Manager
Permittee (of Authorized Agent) Name and Title - Please type or print
A It1ij�2L'l1
Signature of Per ittee (or Authorized Agent) (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
Mail Original
and 1 copy to:
PERMIT #:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
........................................................
......................................... .............
.............................................
DEPARTMENTiOFiE NVIAONMENTi&�NATURAI. RESOURCES
.......................... ......................
......................................... ........ .
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEFGH NC 27626-1617 Phone: [phone]
WI0700012
EXPIRATION DATE:
UIC X
01131 /18
18
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter:
Screened Interval: 3.40 ft. to 5.40 ft.
2 inch
Depth to Water Level: 4.28 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
2100
Field Analysis: pH 6.6 , Specific Conductance 958 uMhos
Temp. 31.1 oC, Odor NONE Appearance: CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/24/2017
Date sample analyzed: 10/24/2017 to 10/31/2017
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
If WELL WAS
DRY at time
of sampling,
check
here:
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/L
/100mL
/100mL
Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
362 mg/L Al - Aluminum
6.3 units Ba - Barium
4.6 mg/L Ca - Calcium
23.0 mg/L Cd- Cadmium
N/A ug/L Chromium: Total
N/A mg/L Cu - Copper
N/A mg/L Fe - Iron
<5.0 mg/L Hg - Mercury
N/A uMhos K- Potassium
N/A mg/L Mg - Magnesium
N/A mg/L Mn - Manganese
nla
No and field acidified
N/A mg/L
N/A mg/L
4.220 mg/L
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes
nla
No )
N/A
N/A
N/A
N/A mg/L Ammonia Nitrogen
N/A mg/L
N/A ug/L
N/A mg/L
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/L Ag - Silver
N/A ug/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A mg/L
N/A ug/L
Se- Selenium
Sodium
0.72
N/A
N/A
N/A
N/A
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
method#
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 4/98
Mark D. Johnson, General Manager
Permittee (of Authorized Agent) Name and Title - Please type or print
9,) tt(511C(1
Signature of Perrr ttee (or Authorized Agent) (D e)

GROUNDWATER QUALITY MONITORING
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
(from pertml
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter: 2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 4.72 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Mail Original
and 1 copy to
PERMIT #:
Non -Discharge
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES•INFORIVIAT10N PROCESSING UNIT
17116.4.,SERVICE CENTER
LE#GH, NG 276264617 Phone: [phone]
WI0700012
EXPIRATION DATE:
UIC X
01/31/18
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Rotary Distributor
Remediation: Infiltration Gallery
Land Application of Sludge
Other Water Source Heat Pump
2600
Field Analysis: pH 5.4 . Specific Conductance 769 uMhos
Temp. 29.4 oC, Odor NONE Appearance: CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/24/2017
10/24/2017 to 10/31/2017
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here:
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A mg/L
Nitrite (NO2 as N)
N/A /100mL Nitrate (NO3 as N)
Yes
N/A /100mL Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 476
pH (when analyzed)
Orthophosphate
mg/L Al - Aluminum
5.2 units Ba - Barium
TOC 4.4 mg/L Ca - Calcium
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
54.0 mg/L Cd- Cadmium
N/A ug/L Chromium: Total
N/A mg/L Cu - Copper
N/A mg/L Fe - Iron
169.0 mg/L Hg - Mercury
N/A uMhos K- Potassium
N/A mg/L Mg - Magnesium
N/A mg/L Mn - Manganese
,n/a
No and field acidified Yes n/a No )
N/A mg/L
N/A mg/L
8.470 mg/L
N/A mg/L
N/A mg/L
N/A ug/L
N/A mg/L
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/L Ag - Silver
N/A ug/L Se- Selenium
N/A mg/L Sodium
N/A ug/L
N/A ug/L
N/A mg/L
N/A mg/L
N/A ug/L
<0.3
N/A
N/A
N/A
N/A
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
NOTE.
GW-59 Rev 4/98
Mark D. Johnson, General Manager
Permittee (ofA thorized Agent) Name and Title - Please type or print
-- it` 11am. lWit-,
Signature of ermittee (or Authorized Agent) Dater

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
and 1 copy to:
PERMIT #:
DERARFME ititi ENVIRONMENT & NATURALRESdURCES:
QIVI510N OF WATER RESOURCES -INFORMATION PROCESSING UNIT
1617 MAILSERVICE CENTER
RALEIGH NC 2 t26.1617 Phone: (919) SU7-6396
. ..............
.................. .......... .. .. ........ ......... .
W10700012
Non -Discharge X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01 /31 /18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 12.28 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Rotary Distributor Land Application of Sludge
Other Water Source Heat Pump
2100
Field Analysis: pH 6.8 , Specific Conductance 911 uMhos
Temp. 27.5 oC, Odor NONE Appearance:
CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/24/2017
Date sample analyzed: 10/24/2017 to 10/31/2017
Laboratory Name:
Certification No(s)
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here:
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 525
pH (when analyzed) 6.5
TOC 4.0
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/L
/100mL Nitrate (NO3 as N)
/100mL Phosphorus: Total as P
LI
Yes
Nitrite (NO2 as N)
Orthophosphate
mg/L Al - Aluminum
units Ba - Barium
mg/L Ca - Calcium
31.0 mg/L Cd- Cadmium
N/A ug/L Chromium: Total
N/A mg/L Cu - Copper
N/A mg/L Fe - Iron
31.0 mg!L Hg - Mercury
N/A uMhos K- Potassium
N/A mg/L Mg - Magnesium
N/A mg/L Mn - Manganese
nla
No and field acidified
N/A mg/L
N/A mg/L
4.530 mg/L
N/A mg/L
N/A mg/L
N/A ug/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A ug/L
N/A ug/L
N/A mg/L
N/A mg/L
0.044 mg/L
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes
nla
No)
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.46
N/A
N/A
N/A
N/A
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
method#
I certify thatto the best of my knowledge and belief. the information submitted in this report is true. accurate. and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and imprisonment for knowing violations
NOTE:
GW-59 Rev 4/98
r
Mark D. Johnson, General Manager
t�Il�Lul1
Signature ittee (or Authorized Agent) (Da )
re of P
Permittee (of ut orized Agent) Name and Title - Please type or print
J.1
rm

GROUNDWATER QUALITY MQNITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter: 4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
Mail Original
and 1 copy to:
PERMIT #:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
DEPARTMENT OF ENVIRCO1A0fiiiii0ORAL RESOURCES
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH, NC 27626-1617 Phone:-(9'l9) 807-6306
W10700012
EXPIRATION DATE:
UIC X
01/31/13
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Water Source Heat Pump
CONTINUOUS
Field Analysis: pH 7.0 , Specific Conductance 829 uMhos
Temp. 27.8 oC, Odor NONE Appearance: CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/24/2017
Date sample analyzed: 10/24/2017 to 10/31/2017
Laboratory Name:
Certification No(s)
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here:
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
504
6.6
4.4
28.0
N/A
N/A
N/A
49.1
N/A
N/A
N/A
mg/L
/100mL
/100mL
mg/L
units
mg/L
mg/L
ug/L
mg/L
mg/L
mg/L
uMhos
mg/L
mg/L
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
n/a
No
N/A
N/A
0.894
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
0.012
and field acidified
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
mg/L
mg/L
Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS,
(Specify test method #.
Report attached? Yes
VOC
0.59
N/A
N/A
N/A
N/A
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and completeand that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations
NOTE
GW-59 Rev 4/98
Mark D. Johnson, General Manager
Permittee (of Aut on ed Agent) Name and Title - Please type or print
/ 17-611
Signature of Per ittee (or Authorized Agent) (Dal

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: 1530 NC Hwy 306 South
Aurora, NC 27806 County: Beaufort
Contact Person: Danny Winstead Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
Mail Original
and 1 copy to:
PERMIT #:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
....... ....... ............... ............... ..
DMENT EPARTOF ENVIROW MMENT & NATURA :RESOURCES
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH;.N .27G264617 Phone: [phone]
............ .. .
WI0700012
EXPIRATION DATE:
UIC X
01 /31 /18
18
Well Identification Number (from Permit): WLCT
Well Depth: N/A ft. Well Diamter: N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level:
Measuring Point is
GALLONS
N/A ft. below measuring point.
N/A ft above land surface.
of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Water Source Heat Pump
CONTINUOUS
Field Analysis: pH 7.0 , Specific Conductance 849
uMhos
Temp. 27.5 oC, Odor NONE Appearance:
CLEAR
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/24/2017
Date sample analyzed: 10/24/2017 to 10131/2017
Laboratory Name:
Certification No(s)
PCS PHOSPHATE
330 10
If WELL WAS
DRY at time
of sampling,
check
here:
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/L Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100mL Nitrate (NO3 as N)
Coliform: MF Total N/A /100mL Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 491 mg/L Al - Aluminum
pH (when analyzed) 6.6 units Ba - Barium
TOC 4.2 mg./L Ca - Calcium
Chloride 33.0 mg/L Cd- Cadmium
Arsenic N/A ug/L Chromium: Total
Grease and Oils N/A mg/L Cu - Copper
Phenol N/A mg/L Fe - Iron
Sulfate 37.3 mg/L Hg - Mercury
Specific Conductance N/A uMhos K- Potassium
Total Ammonia
TKN as N _
N/A mg/L Mg - Magnesium
N/A mg/L Mn - Manganese
Yes
n/a
N/A ug/L
N/A ug/L
N/A mg/L
N/A mg/L
<0.010 mg1L
No
N/A mg/L
N/A mg/L
0.023 mg/L
and field acidified
Yes
n/a
No)
Ni - Nickel N/A ug/L
Pb - Lead N/A ug/L
Zn - Zinc N/A ug/L
N/A mg/L Ammonia Nitrogen mg/L
N/A mg/L Other (Specify Compounds and Concentration Units)
N/A ug/L Fluoride 0.59 mg/L
N/A mg/L MIBK N/A ug/L
N/A ug/L Ag - Silver NIA ug/L
N/A ug/L Se- Selenium N/A ug/L
N/A mg/L Sodium N/A ug/L
Organics: (GC. GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of
analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 4/98
f
Mark D. Johnson, General Manager
Permittee ( Authorized Agent) Name and Title Please type orprint
(Date)
Signature of ermittee (or Authorized Agent)

PCS Phosph . to Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
Date: /Pi ' 1
Time:
File: 12-07-02
Tech:
System Gauge Pressures
SWW-1
N/A
. SWW-7
WA
• CWW-1
WA
CWW-7
N/A
pc: TLB
Reference Level Rol
Point ISl.
,o VSL
Ditch
Barge Slip
Water Level
Control Tank
= MSL
12.91
10.59
(90
73.6
Well ID
Spz-1
Spz-2
Spz-3
Spz-4
Spz-5
Spz-6
Spz-7
Spz-8
Spz-9
Spz-10
SPW
TOC
Elevation
MSL'
10.47
11.21
11.87
11.45
11.45
11.23
11.59
11.57
11.01
Sand Layer Pelzometers Level Indicators
TOC
Stc Wtr
Level '
easy
1p 95"
8.32
9. 02
/0,.5 to
0,75"
12.16 1 k6-?7/
9.95
Level
Relative To
MSL Ft.
3/434,
ADO
e3-/3
Foe Lis
Well ID
Cpz-1
Cpz-2
Cpz-3
CPW
MVTTF-1A •
MWTF-1B •
MWTF-1C
MWTF-2A
MWTF-28
MWTF-2C
MWTF-3A
MWTF-3B
MWTF-3C
TOC
Elevation
MSL'
10.51
10.25
11.12
9.65
14.35
14.36
14.44
14.05
14.02
14.08
12.21
12.18
12.19
TOC
Ste Wtr
Level'
/A /8
44a0
7.2
6,Og.
9,27
/9/3
a82
B-B9
/9.'73
Level
Relative To
MSL Ft
/A 9
/O, 02
a./6
805
8/
e.a12
-7,s9
Sand Layer And Croatan Formation Withdrawal Wells •
Well ID
TOC
Elevation
MSL'
Max Stc
' Wtr
Level Ft
Pump
Activation Depth
Rel MSL
Max Level Control
Relative To Point
MSL Ft. MSL'
Is Well
' Pumping?
esl(N)o
Comments .
SWW-1
10.70
N/A
6'
N/A
+1 'to+2'
.
CW W-1
10.60
N/A -
9'
N/A
-2' to -1'
/
SWW-2
9.99
N/A
6'
WA
+1'to+2'. -
/v4
CWW-2
10.23
N/A
9'
N/A
-2'to-1'
W SW-3
9.97
N/A
6'
N/A
+1 'to+2'
///j///���'///yppp,
/J
I,
CWW-3
9.95
N/A •
_ 9'
N/A
-2'to-1'
YLJ`
SWW-4
10.73
N/A
6' .
N/A
+1'to+2'
CWW.4
10.73
N/A
9'
N/A
-2'to-1'
SWW-5
10.80
N/A
6'
N/A
+1'to+2'
CWw.s
10.74
N/A
9'
N/A
-2'to-1'
I
SWW.810.66
N/A6'WA+1
'to+2'CWW.69.92
WA
9'N/A-2'to-1'
SWW-7
10.70
N/A
6'
N/A
+1' to+2'
CWW-7
9.95
N/A
9'
N/A
-2 • to -1'
7'
evised 729/02
• Riser length added to TOC elevation 124/97
D:\DatalFomis\Well Fonn\Tenk Farm Rimed Welisxls

SPL1
CPI/
PLANT C
L__1 LT
MWIFT
CLUSTER
SPZE
SPZA
ROLE - T WT
LEGEND
SYMBOL DESCRIPTION
MUMMER
• MONRON WELL
• COMM CARD LATER WITHDRAWAL WELL
• CROATAN FORMATION WITHDRAWAL WELL
G9 CROATAN FORMATION OLIECLION WELL
• INJECTION WELL HEADER PIPE CLEAMOLR
• INJECTION WELL MENEM WATER LEVEL
CONTROL WOE
LOCATION PLAN FOR TANK:F% RM