WI0700012_Monitoring (Report)_20040528

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
CI
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter: 4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
For Groundwater Treatment
Systems Check One:
X Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: N/A
Field Analysis: pH 7.1 , Specific Conductance 558 uMhos
Temp. 17.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/14/04
Date sample analyzed: 4/14/04 to 5/19/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
7.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
373
7.2
5.4
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
19.4
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
unfiltered X Yes
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
0.057 mg/I
N/A mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/I
N/A mg/I
<0.001 mg/I
<0.005 mg/I
N/A mg/I
N/A mg/I
N/A mg/1
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified X
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes No )
N/A mg/I
N/A mg/I
N/A mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units) r2.
Fluoride
MIBK IW
Ag - Silver N/A ug/I
Se- Selenium N/A- ugh
Sodium N/A'? ug/I
Organics: (GC, GC/MS, HPLC)
mg/I
ug/I
(Specify test method #. Attach lab report.)
ON N/A mg/I Report attached? Yes (1) No X (0) 0
N/A mg/I VOC
0.012 mg/I
: method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - M--
P-
ger Environmental Affairs
ame and Title - Please type or print
aturf ermittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): MWTF1-CR
Well Depth:
42.00 ft. Well Diamter:
Screened Interval: 38.70 ft. to 40.70 ft.
2 inch
Depth to Water Level: 11.28 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
5200
Field Analysis: pH 7.0 , Specific Conductance 950 uMhos
Temp. 19.6 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT#: W10700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/14/04
Date sample analyzed: 4/14/04 to 5/19/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total >600.0
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
629
7.2
5.4 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
106.0
N/A
N/A
N/A
22.8
N/A
N/A
N/A
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
<0.010 mg/I
No and field acidified X Yes No )
N/A mg/I
N/A mg/l
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
0.764 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
<0.001 mg/I
<0.005 mg/I
N/A mg/I
N/A mg/I
N/A mg/l (Specify test method #. Attach lab report.) :? c
N/A mg/I Report attached? Yes (1) No XL (2yc
N/A mg/I VOC : method#
method#
method#
N/fit ug/I
Ni - Nickel N/A mg/I
Pb - Lead N/A mg/I
Zn - Zinc N/A mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Unit
Fluoride '0.59 mg/I
MIBK ./A ug/I
Ag - Silver ICl/A ugll
Se- Selenium NtA ug/t
Sodium
Organics: (GC, GC/MS, HPLC)
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Ross M._Smith - Manager, Environmental Affairs
Permitte (o uthg►izedt) e and Title - Please type or print
GW-59 Rev 03/2000
Sig ture ofPerMittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 55.00 ft. Well Diamter:
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level:
Measuring Point is
CWW-1
4 inch
6.59 ft. below measuring point.
2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
X
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2190 uMhos
Temp. 19.2 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
4/15/04 to 5/13/04
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1940
pH (when analyzed) 5.7
TOC 7.5
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
78.8
N/A
N/A
N/A
696.7
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/I
units
mg/I
mg/1
mg/I
mg/I
mg/I
mg/1
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
0.500 mg/l
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/1
Yes n/a No )
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
C'D.23
'"- N/A
c 7S/A
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
N/A
NIA
mg/l
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/1"_.
(Specify test method #. Attach lab report.) - =o
N/A mg/I Report attached? Yes (1) No X1 ? (2
method# -' o
cd) 7G
method#
method#
N/A mg/I
N/A mg/1
VOC
I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M_- ith - Mana
(of
r, Environmental Affairs
Permittee.u thor d A) NCnnand Title - Please type or print
ure of Pe Sign fmittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-2
Well Depth: 52.15 ft. Well Diamter:
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level:
Measuring Point is
4 inch
8.96 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.4 , Specific Conductance 5970 uMhos
Temp. 19.1 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: (9'f9)733-3221
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
C-4 7
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed: 4/15/04 to 5/13/04
Laboratory Name: PCS PHOSPHATE and
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I
/100m1
/100m1
4660 mg/I
5.8 units
8.7 mg/I
Chloride
Arsenic
1790.0 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mgll
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
1001.8 mg/I
N/A uMhos
N/A mg/I
N/A mg/1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
n/a No and field acidified
N/A mg/I
N/A mg/I
17.720 mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
3
ENVIRONMENT 1
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
N/A ug/1
VOC : method#
: method#
• method#
(2)
mg/I
mg/I
mg/1
mg/t
0.3ert mg/I
N/A ' ugtst.. =
N/A:? ug/F',
N/A ttg/iY
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M_-S► h - Managgar, Environmental Affairs
Permitte (o utho d
Sign re of P rmi tee (or Authorized Agent)
and Title - Please type or print
es- z
(Date)
adi

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level:
CWW-3
4 inch
6.28 ft. below measuring point.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Measuring Point is 3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2426 uMhos
Temp. 22.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed: 4/15/04 to 5/13/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/l Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note' Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
2100 mg/I Al - Aluminum
6.5 units Ba - Barium
7.4 mg/I Ca - Calcium
172.0 mg/I
N/A mg/I
N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
949.8 mgll Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A
N/A
9.050
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
mg/I
mg/I
mg/I
mg/I
r'11.17 mg/1
N/A ug/I
NfA ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC) -o
(Specify test method #. Attach lab report.) ' t,-:
Report attached? Yes (1) No X a (2)
VOC : method# OA a
method#
method#
I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
er, Environmental Affairs
Signgrure of Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level:
5.12 ft. below measuring point.
Measuring Point is 2.75 ft above land surface.
For Groundwater Treatment
Sys ems Check one:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2547 uMhos
Temp. 25.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/15/04
4/15/04 to 5/13/04
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2160
pH (when analyzed) 6.6
TOC 7.5
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
108.0
N/A
N/A
N/A
728.7
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1
/100m1
mg/I
units
Nitrate (NO3 as N)
No and field acidified Yes n/a No )
N/A mg/I
N/A mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/l Hg - Mercury
8.500 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A mg/l
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
0.12 mg/I
ug/I
N(/A ug/1
N/A ug/1
NA N ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
tom`
N/A mg/I (Specify test method #. Attach lab report.) r A
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/1 VOC : method# r•J
method# Z
method#
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M, mith - Mvlager, Environmental Affairs
Perrt itttee (9(Au Age ame and Title - Please type r print
Siyrt ture,6f Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr,
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
m1.
Well Identification Number (from Permit):
Well Depth: 53.17 ft. Well Diamter:
CWW-5
4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level: 7.60 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2422
uMhos
Temp. 27.9 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed: 4/15/04 to 5/13/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 1580
pH (when analyzed) 6.5
TOC 6.8
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
174.5
N/A
N/A
N/A
592.2
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field
N/A
N/A
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
11.300
N/A
N/A
N/A
N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A
N/A
N/A
N/A
N/A
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
acidified Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds
Fluoride
MIBK
Ag - Silver
N/A mg/I
, mg/I
, i1/A mg/I
mg/l
and Concentration Units)
0. Q mg/I
N/A ugil --
N/A ug11-,y
Se- Selenium N/A; J ug/t T
Sodium N/A rug/I
Organics: (GC, GC/MS, HPLC) c.)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
h - Mana
r, En
ironmental Affairs
and Title - Please type or print
Sig 3' re of PArmittee (or Authorized Agent)
ate)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-6
4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: 7.36 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
Temp. 28.9 oC. Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2189 uMhos
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
4/15/04 to 5/13/04
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 1460
pH (when analyzed) 5.5
TOC 8.9
Chloride 92.2
Arsenic N/A
Grease and Oils N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
626.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/1
units
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Yes n/a
No and field acidified
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 21.250 mg/1
Orthophosphate N/A mg/I
Al - Aluminum N/A mg/I
Ba - Barium N/A mg/I
Ca - Calcium N/A mg/I
Cd- Cadmium N/A mg/1
Chromium: Total N/A mg/I
Cu - Copper N/A mg/I
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/l
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.17
N/A
N/A
t#/A
mg/I
mg/l
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)'.
Report attached? Yes (1) No _X, (2):-
VOC : method#
method# ;-3 ;�
method# vt
1
W
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and completeand that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross.M. h - Mana.-r, Environmental Affairs
fnitte (o ut
ure of �m
Per ho Ced A .'t) a • - and Title - Please type orprint
Cgs/or/
Sign ittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-7
4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level: 7.42 ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.7 , Specific Conductance
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1156 uMhos
Temp. 22.6 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
4/15/04 to 5/13/04
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform:
Coliform:
(Note.
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
MF Fecal
MF Total
N/A
N/A
N/A
Use MPN method for highly turbid samples)
809
6.7
5.5
59.4
N/A
N/A
N/A
287.5
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I Ca - Calcium
mg/I
mg/I
mg/I
mg/l Fe - Iron
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Cd- Cadmium
Chromium: Total
Cu - Copper
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
4.375 mg/I
Yes n/a No )
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
mg/I
uMhos
mg/I
mg/I
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
Fluoride
MIBK
Ag - Silver
N/A
N/A
N/A
0.17
N/A
Se- Selenium ' N/A
Sodium `'a/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report:r
N/A mg/I Report attached? Yes
N/A mg/l VOC
N/A mg/I
(1) No
method#
method#
method#
mg/I
mg/l
mg/l
mg/l
mg/I
ug/I
ug/I
ug/I
ug/I
(S'
C.)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and completeand that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M-. ith - Manager, Environmental Affairs
Permittee)(of uthoed ent) ime and Title - Please type or pn
Si a of ermittee (or Authorized Agent) (Date)
1.4

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 11.32 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 6.1 , Specific Conductance 1576 uMhos
Temp. 17.9 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
I
PERMIT #: WI0700012
EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
4/15/04 to 5/13/04
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Notes Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1200
6.4
7.0
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
42.3
N/A
N/A
N/A
767.4
N/A
N/A
N/A
No and field acidified
mg/I Nitrite (NO2 as N) N/A
/100m1 Nitrate (NO3 as N) N/A
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/l Cu - Copper
mg/I Fe - Iron
127.000
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I Hg - Mercury
uMhos
mg/1
mg/I
N/A
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
mg/1
mg/l
mg/l
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
mg/I
mg/I
mg/I
mg/I
0.67 mg/I
N/A ug/1
N/A ug/I
N/A
.a N/A
ug/l
ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report
Report attached? Yes (1) No
VOC method#
method#
method#
X- ()
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M.
mith - Manager, Environmental Affairs
Permittee (o Authed ent) e and Title - Please type or print
4/2
/7
3iture of ermittee (or Authorized Agent)
ate)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 5.30 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 1914 uMhos
Temp. 18.6 oC, Odor NONE Appearance:
CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed: 4/15/04 to 5/13/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
N/A
N/A
Coliform: MF Fecal
Coliform: MF Total
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
mg/I
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
1610 mg/I Al - Aluminum
6.5 units Ba - Barium
8.0 mg/I Ca - Calcium
36.7 mg/1
N/A mg/I
N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
No and field acidified
N/A
N/A
77.000
N/A
N/A
N/A
N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
585.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A
N/A
N/A
N/A
N/A
N/A
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
mg/1
mg/1
mg/I Zn - Zinc
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l VOC
N/A mg/I
Ni - Nickel
Pb - Lead
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.29
N/A
N/A
Se- Selenium
Sodium
mg/I
mg/1
mg/l
mg/I
mg/1
ug/I
ug/I
ug/I
--N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab repor
Report attached? Yes (1) No Yc
method#
method#
method#
(2)
rJ
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M ith - Mana.er, Environmental Affairs
Permlftee (of thhoo ed , - t
�� cs %i,7 'sy/
e and Title - Please type or print
Sign nitre of Vermittee (or Authorized Agent)
( ate)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth:
24.50 ft. Well Diamter:
SWW-3
4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.81 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
X
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 1602 uMhos
Temp. 19.5 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone' [phone]
PERMIT#: WI0700012 EXPIRATION DATE:
01/15108
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
4/15/04 to 5/13/04
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1170
6.3
8.1
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
30.4
N/A
N/A
N/A
445.0
N/A
N/A
N/A
mg/l Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I
units
mg/I
mg/I
mg/I
mg/1
mg/I Fe - Iron
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
mg/I Hg - Mercury
uMhos
mg/I
mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
115.750 mg/I
No and field acidified
Yes n/a No )
N/A mg/I Ni - Nickel N/A mg/I
N/A mg/l Pb - Lead N/A mg/I
Zn - Zinc N/A mg/1
N/A mg/l Ammonia Nitrogen mg/I
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/l Fluoride 0.09 mg/I
N/A mg/I MIBK N/A ug/I
N/A mg/I Ag - Silver N/A ug/I
N/A mg/I Se- Selenium N/A ug/I
N/A mg/1 Sodium C3 N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC) t�
N/A mg/l (Specify test method #. Attach lab rep.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/1 VOC : method#
N/A mg/1
: method# Q
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M.,,.
Perprttte- (of
Si
a
e of
rm
- Mana.er, Environmental Affairs
Narniand Title - Please type or_print
CAS,
ee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
I
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
18 1 1 Rotary Distributor Land Application of Sludge
Well Identification Number (from Permit):
Well Depth: 25.00 ft. Well Diamter:
SWW-4
4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 8.50 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.6 , Specific Conductance 1869 uMhos
Temp. 21.6 oC. Odor NONE Appearance: CLEAR
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed: 4/15/04 to 5/13/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1510
pH (when analyzed) 6.2
TOC 7.1
Chloride
Arsenic
Grease and Oils
mg/I
/100ml
/100m1
mg/I
units
mg/I
39.0 mg/I
N/A mg/1
N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified Yes n/a No )
N/A
N/A
130.000
N/A
N/A
N/A
N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
452.7 mg/I Hg - Mercury
N/A
N/A
N/A
N/A
N/A
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
N/A
mg/1
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
0,10
(/A
"'VA
NJA
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #.
Report attached? Yes
VOC
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I;
N/A ug/t
r� 1
Attach lab report.)
(1) No X (2) c'�
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Perrnitfe- (of utho bed Aunt) Nayfe and Title - Please type or print
Ds:
/y/
Sig : ure of ermittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr,
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 28.21 ft. Well Diamter:
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level:
Measuring Point is
SWW-5
4 inch
6.25 ft. below measuring point.
2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2661 uMhos
Temp. 27.2 oC, Odor NONE Appearance: LT YELLOW CLDY
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed: 4/15/04 to 5/13/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1660
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.4
10.6
46.2
N/A
N/A
N/A
757.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I Se- Selenium << =. N/A
k
N/A
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report
N/A mg/I Report attached? Yes (1) No C
Sodium
87.000 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I
N/A mg/I
N/A mg/I
Fluoride
MIBK
Ag - Silver
0.31
NIA
Er N/A
N/A mg/I
N/A mg/I VOC : method# rJ
N/A mg/I
method# �,t1
method# w
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Ross
Pe • i tee of
ti
th - Manager, Environmental Affairs
hord AoerR1 Na
and Title - Please type or print655
GW-59 Rev 03/2000
Sign ure of P,
rmittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
Telephone: [phone]
No. of Wells to be Sampled 18
Orom
Well Identification Number (from Permit):
Well Depth: 26.00 ft. Well Diamter:
SWW-6
4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 8.92 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 3341 uMhos
Temp. 28.7 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 2480 mg/1 AI - Aluminum
pH (when analyzed) 6.3 units Ba - Barium
TOC 15.4 mg/I Ca - Calcium
Chloride 83.6 mg/I Cd- Cadmium
Arsenic N/A mg/I Chromium: Total
Grease and Oils
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
1319.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed: 4/15/04 to 5/13/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
Yes n/a No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
76.250 mg/I
N/A mg/l
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds
Fluoride
MIBK
Ag - Silver
N/A
N/A
N/A
mg/I
mg/l
mg/I
mg/I
and Concentration Units)
mg/1
4"N/A
iglA ug/I
Se- Selenium N(A ug/I
Sodium N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.) to
t,•
N/A mg/I Report attached? Yes
N/A mg/I VOC
N/A mg/1
(1) No
method#
: method#
method#
X r::.? (2)
c!A
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and completeand that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Signature ofjPermittee (or Authorized Agent)
Ross M. ith - Manager, Environmental Affairs
Pe ittee(o>f uthoed�/ geJt) t�t(me and Title - Please type or_print
$f 0/d%
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter:
4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level: 6.46 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.8 , Specific Conductance 936 uMhos
Temp. 22.6 oC. Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
4/15/04 to 5/13/04
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 715
pH (when analyzed) 6.0
TOC 8.8
Chloride
Arsenic
Grease and Oils
mg/l
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
67.2 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
210.1 mg/1 Hg - Mercury
N/A uMhos K- Potassium
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
80.000 mg/I
Zn - Zinc
N/A mg/l Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
N/A mg/I MIBK
11
N/A mg/I Ag - Silver
N/A mg/I
Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/1
N/A mg/l
N/A mg/1
mg/I
mg/1
mg/l
mg/I
mg/I
ug/I
ug/I_
tg(I
ug4 7
Report attached? Yes (1) No X )
VOC : method# ' Z
method#
method#
cA�A
N/f�4
N/A
(Specify test method #. Attach lab report.)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M,_ 'th - Manager, Environmental Affairs
Peunitte (of hori d A Na and Title - Please type or print
Si ne re of P rmittee (or Authorized
Agent) g g )
pS"c
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter: 2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.20 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.4 , Specific Conductance 536 uMhos
Temp. 20 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/15/04
Date sample analyzed: 4/15/04 to 5/13/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
373 mg/I
7.3 units
3.0 mg/I
9.1 mg/I
N/A mg/I
N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Yes n/a
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
58.5 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A
N/A
0.350
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/1
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
mg/l
mg/I
Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 2.2Q mg/I
MIBK N/A ug/I
Ag - Silver Al/A ug/I
Se- Selenium It/A ug/I
Sodium M/A ug/(.
(p
Report attached? Yes (1) No X J (2)c.,'
VOC : method# ••
method# u)
method#
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Perrnittee (of
Sign re of rmittee (or Authorized Agent)
nt) Ne and Title - Please type or print
l2S%

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr.
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth:
13.50 ft. Well Diamter:
MWTF1-B
Screened Interval: 10.60 ft. to 12.60 ft.
2 inch
Depth to Water Level: 4.70 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 5.7 , Specific Conductance 336 uMhos
Temp. 20.6 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/15/04
4/15/04 to 5/13/04
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
N/A mg/I
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 226
pH (when analyzed) 5.9
TOC 2.7
Chloride
Arsenic
mg/I
units
mg/I
41.2 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
24.2 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
No and field
N/A
N/A
7.750
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1 VOC
mg/1
acidified Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds and Concentration Un
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.) N
Report attached? Yes (1) No X LP (2) 2
method#
method#
method#
N/A mg/I
N/A mg/I
N/A mg/I
mg/1
0.29 "rng/I
c../A ug/I
• N/A ug4 NIA lgt[
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross smith - Manager, Environmental Affairs
Pecmittee (of uth zecjf ent) 9t6me and Title - Please type or print
gg ture o>rPermittee (or Authorized Agent) ( ate)
N/6

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): WLCT
Well Depth: N/A ft. Well Diamter: N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
Field Analysis: pH 7.1 , Specific Conductance 580 uMhos
Temp. 18.4 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/14/04
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
4/14/04 to 5/19/04
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
X Yes
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total 3.0 /100m1 Phosphorus: Total as P
(Note
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
r Grease and
Use MPN method for highly turbid samples)
368
7.2
5.4
14.3
N/A
Oils N/A
N/A
<10.0
N/A
N/A
N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I
units
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
uMhos
mg/l
mg/I
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified X
N/A mg/I
N/A mg/I
0.082 mg/l
N/A mg/I
N/A mg/l
N/A mg/I
N/A mg/I
<0.001 mg/I
<0.005 mg/I
Yes No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
mg/I
mg/I
mg/I
mg/I
Fluoride OM mg/1
MIBK C=' Ni?,.... ug/l
Ag - Silver N/A ug/I
Se- Selenium `.N/A ug/I
N/A mg/I Sodium 1 N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/l (Specify test method #. Attach lab report
N/A mg/l Report attached? Yes (1) No - (2)
method#
01
method#
N/A mg/I VOC
0.012 mg/I
method#
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permiffee f A ori Ag�rft) Name and Title - Please type or print
natur of Permittee (or Authorized Agent)
�SIFo�
( ate)

Date:
Time:
Tech:
PCS Phosphate Co., In Tank Farm Remediation S' em Quarterly Monitoring
S/-/e-09
J9%%%
System Gauge Pressures
SwW-1
O-/3
SWW-7
O-S
cww-1
O -/ 7
CWW-7
0 -3074
File: 12-07-02
pc: TLB
Reference
Paint MSL
Level Rel
to MSL
Ditch
12.91
74i5
Barge Slip
10.59
Water Level
Control Tank
%= MSL
/OD/
,5✓3
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft. I
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level' '
Level
Relative To
MSL Ft.
Spz-1
10.47
«0,2.
4, Vs-
Cpz-1
10.51
/0, 3 3
a /B
Spz-2
11.21
8.0/
J /4'
Cpz-2
10.25
//./4/
- 0.89
Spz-3
11.87
6,06-
.5 8a
Cpz-3
11.12
0
/(6
a y4
Spz-4
11.45
lJO
.5./S
CPW
9.65
//%, 3/0
- 0.71
Spz-5
11.45
8-
p7.59
MWTF-1A *
14.35
yp'Jb
/0,/5
Spz-6
11.23
'/9/
5/
9 '
/ 77
MWTF-1B •
14.36
y, 70
9 14.
Spz-7
11.59
/O„ 2s!
735
MWTF-1C •
14.44
// p'/8
i - / 4
Spz-8
11.57
7.. OR
y, /9
MWTF-2A
14.05
1p, 67
7 yA
Spz-9
11.01
!' 7/
.3 0
MWTF-28
14.02
/0. ,q-6
. 2/6
Spz-10
12.16
4.04
/0./0
MWTF-2C
14.08
/5:0/
JV', 9
940
-O.9.3
R,&d,
0?..5B
SPW
9.95
7/a
a.e
MWTF-3A
12.21
MWTF-3B
12.18
MWTF-3C
12.19
/S1/4
-/a7
Sand Layer And Croatan Formation Withdrawal Wells
Well 10
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Pump
Activation Depth
Rel MSL
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping?
(Y)es/(N)o
Comments
W SW-1
10.70
/1./2
6'
Ll. 3a
+1 'to+2'
fr f
.GF4ie- 4o/
W CW-1
10.60
1, 59
9'
- 07. ///
-2'to-1'
W SW-2
9.99
pj•L//
6'
a, '9/
+1. to +2'
Ly/es
/,vf
W
CW-2
10.23
4, 9b
9'
-0. 0y
-2'to-1'
SWW-3
9.97
OS/
6'
/ B/
+1 ' to+2'
gf
CWW-3
9.95
441
9'
-02-7c2
-2'to-1'
ref
W SW-4
10.73
BSV
6'
01S0
+1 ' to+2'
%tfY
CWW-4
10.73
O/K
9'
- J. B8
-2 ' to-1'
9e/
SWW-5
10.80
6.25-
6'
o•as
+1'to+2'
yef
CWW-5
10.74
9'
/ 90
-2' to -1'
SWW-6
10.66
/7oe,
6/ 999,
6'
O� 9a
+1'to+2'
CWW-6
9.92
/i.4'
9'
'/(64//
-2' to -1'
At
SWW-7
10.70
/'
Gj, 41(jj
6'
a $c
+1' to +2'
/�/.'J
ref
CWW-7
9.95
2;94
9'
/ 56
-2 ' to-1'
511,5
/-/Gigged .49 evdr
Revised 7/29/02
• Riser length added to TOC elevation 1/24/97
DAData\Forms\Well Farm\Tank Farm Rented Welis.xls

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
February 2004 — April 2004
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Infection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Feb
476,620
0
476,620
11.8
15.0
March
405,390
0
405,390
9.1
15.0
April
352,990
0
352,990
8.2
15.0
TOTALS
1,235,000
0
1,235,000
C:\MyData\Reports\2004\Quarterly\TFRAS Report First Quarter 2004.doc
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Feb
348,965
116,391
465,356
12.9
March
384,420
161,970
546,390
13.1
April
364,329
132,926
497,255
11.2
TOTALS
1,097,714
411,287
1,509,002
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
System air compressor was down February 3 until February 4 and again from February 23 until March 8 .
During these periods the system operated on Plant Air.
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1:
SWW-2:
SWW-3: On 4/22 shook pump to start.
S W W-4: On 3/10 changed pump. On 4/20 cleaned hose.
S W W-5: On 2/26 changed pump. On 4/28 changed pump.
SWW-6: On 2/12 shook pump. On 4/21 shook pump.
SWW-7: On 2/9 washed well. On 3/22 repaired pump. On 4/6 changed pump.
c:\MyData\Reports\2004\Quarterly\TFRAS Report First Quarter 2004.doc
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2: On 4/14 acid washed well.
CWW-3: On 3/8 changed pump.
CWW-4: On 3/17 changed pump.
CWW-5: On 4/14 acid washed well. On 4/22 changed pump.
CWW-6:
CWW-7: On 4/29 changed pump.
C:\MyData\Reports\2004\Quarterly\TFRAS Report First Quarter 2004.doc
5

PCS
Phosphate
AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
May 21, 2004
EVAN O. KANE
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
February 2004 — April 2004
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Evan:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
,6. �a.,rt:e--i�;rn� �. �,l //r
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
W. A. Schimming