WI0700012_Monitoring (Report)_20170929

PCS_PHOS. M ON
Parameter
Well ID
Jan-96
Apr-96
Jul-96
(units)
regulatory std
Field pH
Supply
7.1
WLCT
7
CIW7
7.7
pH 6.5-8.5
MWTF-1C
7
Temperature
Supply
18.5
(Centigrade)
WLCT
78
CIW7
32.7
<35.5
MWTF-1C
23
Total coliform
Supply
NA
_
(cts per 100m1)
WLCT
<1
CIW7
<1
< 1/100m1
MWTF-1C
<1
TDS
Supply
464
(mg/I)
WLCT
96
CIW7
155
<475
MWTF-1C
364
TOC
Supply
5.9
(mg/I) _
WLCT
4.5
CIW7
1.9
<10
MWTF-1C
3.5
Chloride
Supply
66.6
(mg/I)
WLCT
1.8
CIW7
11.8
<55.0
MWTF-1C
41.3
Fluoride
Supply
0.57
(mg/I)
WLCT
0.03
CIW7
0.12
< 1.0
MWTF-1C
0.52
Sulfate
Supply
<10
(mg/I)
WLCT
<10
CIW7
<10
<50.0
MWTF-1C
<10
Total Phosphorus
Supply
0.049
(mg/I)
WLCT
0.121
CIW7
0.019
<0. 15
MWTF-1C
0.14
Page 1

4' .
PCS_PHOS.MON
Parameter
Well ID
(units)
regulatory std
Cadmium
Supply
NA
(mg/I)
WLCT
0.00051
CIW7
<.001
<0.005
MWTF-1C
<.001
Chromium
Supply
NA
(mg/I)
WLCT
0.02766
CIW7
<.001
<0.05
MWTF-1C
<.001
Manganese
Supply
NA
(mg/I)
WLCT
<0.01
CIW7
<0.01
<0.05
MWTF-1C
<0.01
Page 2

Attachment 1
PCS Phosphate - Aurora Division
Pilot Plant Study - Injection Well Water Supply
Parameter
08/01/95
08/15/95
09/07/95
09/21/95
10/11/95
11/01/95
11/30/95
Avgs
Limits
Total Phosphorus mg/I
0.027
0.024
0.024
0.010
0.014
0.025
0.025
0.021
0.150
Fluoride mg/I
0.73
0.69
0.69
0.68
0.70
0.68
0.71
0.70
1.00
Chloride mg/I
10.8
10.7
9.0
10.6
13.0
10.0
11.5
10.8
55.0
Sulfate mg/I
<10
<10
<10
<10
<10
<10
<10
<10
50
i
TOC mg/I
4.0
6.0
6.0
4.8
4.2
6.0
5.2
5.2
'`
(p 4.3
TDS mg/I
528
412
330
380
496
357
354
408
S0°475
Cadmium mg/I
<0.005
<0.005
<0.005
<0.001
N/A
<0.001
N/A
<0.005
0.005
Chromium mg/I
<0.05
<0.05
<0.005
<0.001
N/A
<0.001
N/A
<0.001
0.05
Manganese mg/I
<0.05
<0.05
<0.05
<0.05
N/A
<0.01
N/A
<0.01
0.05
Total Coliform /100 ml
'<1
<1
<1
<1
<1
<1
N/A
<1
<1
pH
7.9 @19 oC
7.4 @26 oC
7.5 @22 oC
7.4
@24 oC
7.1 @21 oC
7.2 @19 oC
7.4
N/A
1
6.0 - 7.0
t. 5.
L..
"i•U
k•O1 •

_
We
/INe-11 I.D. Tuhw tt. 51:IPPLY
11e.ld Ainatr. JAI
rDaie ; <xei
Colliartir 1410Taial
marr"-- NA%
111110•010""^..............,
11111111111111.11=1111F
1 ; •
'Ivosptiorug Tao/ P
CiJ
tor 19J* cr.-
Otiovr FLUORIDE

VIV fI V,I,J14,14.11
F
F
•
A
1 9 9 z
z !
nsk
U I
.91
4.
z
3
n)
.) ,-,..). 0 0

at.unt.ni t.1.4111ti
14000
f On>
Jr JO LZ—dTra
wrwalun-isi
lout mortRuosto
alauIP123 -
1.73u. yJ
yaw ot
i elm 96t:
Ow SIT 11 JIL MOW/ I ;*
It'1011 ,411013 Palloss!CI
Mo./ nu1ar14):
'00
430
,100
- - ••• -•-••

3
• • • -
> ; )
Cf.)tt'Or,. f
r
WcV 1.1). P.4Sarrkber:
kiAflapII
ya k f
Colikuut MJToaI
(}i5Aolved Solids: Tout
TOC
Chloriik
Sultast
me/
Cr. — Cadmium
CI minium Total
la.-01.11 •
FR tf)RflIF.
_ tp;24).^N • •%4 rfk: •
t t,
• .• t ''
24.0 of.: Odor

r'
p� PtCpS%
Phosphate !.i .AURORA 91V191Oh
__ __
PO SC\ 68 AJRCP4• NC ;;.i_. p_-
.November 29, i 9a95
11-rd injectii3ii 1. L':ltl c 1 - / ngram
_:':x '_9535
:ciQIl, North Carolina 762'5-0 35
'IV iry}ii;t�i
it!oahS3rirc, Data
i 2T- l$eliEeUal Atitwn .System
L',: be ;._ ,rsl tl)M ii;VJplonn:'.iltal Tali: arm Ranubdisil Action systom c(uutarly
mu'liwri:ie data for your information. These data are from samples collected
' ring L)ctooer :-;Q5 rile sampling and analysis of water from the injection well system as '
equiicd Per,.,. 06-0071-W0-0005 is also includeci.
r - -';-� L'slis i" you have any questions regarding this information.'
r
.--rtag_ %.Iivirc:111'•i1;Ze1 Affh:i'S
Will Hi.rdisstri -
[2 ("_Jc'05 (vtio, at:):1

ris ;it D. member
Pre_ld Asolysie pal
Law .s.univie coati:
sear 41 trY11:11
6_9
Colifenee .64F Feca/ rvA ,t1Olk
Conform: INF Total NA Pbcosehorur Total as P
.5.16_27
1111,r3 •
Cod
Chr
Sulfate <ao IRA
= '14
SIGNATURE OF-PttiMITT E.!
Ma -
. .
- . AUTHOPPED AG
orno • met
any 20.5 nC Odor
Other FLUOIUDE

Ali 7,11
41.114.1uPsa
(162 90114>
Ittir an-
10011>
4 ' SEIM
Lv CL.7-17.ik)Of--111r: ' 1) 33.11110117.1:3c: JO DlifliVNEAS
- 7r,
mautellereig ur
14.941 ten !pony
ulmcw. Pw3 —10
Awn 01>
4,2u. 44-105.2
LA" t. "irT I
Vitro
uur. aura -eurioq zraitiossucr
341 WW1 ai1-"Eu5iNiti I 1•00/1 1> qojjp :1110PIDD
771:4,1P.N >Omer; 'xrPf.T •
sruiretry mat

I/ i D. 11 r ahc. •
_ psi
zarf asople tmexes
A, A
111
slob
01M/95
Oissoihicd Sarxhr Total
OC
Mori&
;ask
ridartmi
246 sort
11 wiN4
318 owl
<W hily1
Phosphor Total AS P
A — Carliniinn
<U,J4.14
CAA.-R.W
Mawr <035
pl/di;;:t
SIGNATURE OF PERMITT EE (OR AUTHORIZED ENT)
ctrip
Other FLUOR rnp
0.26 wislt
r
;.-
3
r
c
c
1

M W TF[ - c. y
ield
-Toc
i
asghor+e -ddai M.i'
} Ica Cadmium
[ Chromium Total
irk' { / + • ,
SIGNATURE OF PERMITTEE (OR AUTHORIZED AGE
as Tenn 74,n ..!
<ORO other FLUORIDE user ler
7/-#ATE

• IL J VJ 1 V • JJ 1 LIYY, /1I I f11\V VLF I, '
VIJ 1.1J UJUULR'L
1J.Lefr:Tilia.ie Yi4 i n 1 n ti \i 131 V V
Mt(' Il' 1. • 'Ivl t..
•.•(11"UC! ." �nalhpe nnen1
` .ri i `��!.� r•:Yili.l AC::On t'lvsteni
•(a) T3r1: Farm ir.'"i].i:c{� HL`.11llt 'iysterc
iafortnal.ina1. st dad are frniin savny3ie.s :'Ol Bored
'and al121.VSis w :Cq r?'^IT. ?!-i^ i je.iio: '•.l'CII ..rstem as
li"..-O005 :s a;y:1 incluc:B!11.

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MANAGEMENT I
I
P.O. BOX 29535
Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071- WO -0005
Non -Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
_Spray Field _Subsurface Low -Pressure
_Land Appl of Sludge
Well Location : Tank Farm
— .a r
--. - --_ .
Well I.D. Number. INJ. SUPPLY Well Depth: 179.0 Well Depth:
Well Diameter 6" Sample (Screened) Interval NIA
Ft. to N/A Ft.
Depth to Water Level N/A Ft. below meas. pt.(before sampling) or
N/A Ft. (MSL)
Measuring Point is 1.00 Ft. above land surface or
N/A Ft. (MSL)
Gallons of water before sampling CONTINUOUS
pumped/bailed
Field Analysis: 7.0 Specific Conductance
800 uMhosTemp 19.0 oC Odor
NONE
pit
Date Sample Collected 04/27/95 Date Lab Sample Analyzed 04/27-05/26 1994 Appearance: CLEAR
Laboratory Name : PCS PIIOSPHATE ENV. AFFAIRS LAB Certification No. 330 AND 102 (TOC ONLY)
FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
SAMPLES
NO2 as N
N/A mg/l
Ni - Nickel
N/A mg/1
COD N/A mg/l
Coliform: MF Fecal N/A /100m1
�
NO3 as N
N/A mg/I
Pb - Lead
N/A mg/1
Coliform: MF Total N/A 1100m1
Phosphorus: Total as P
0.016 mg/I
Zn - Zinc
N/A mg/I
Dissolved Solids: Total 532 mg/1
Al - Aluminum
N/A mg/I
Pesticides/Herbicides (Specify)
.p}}(wherrartglyzed) 7. udMC
Ba - Barium
N/A mg/1
ug/I
'FOC 6 m /l
Ca - Calcium
N/A mg/I
ug/I
Chloride 94.8 met
`Cd - Cadmium
N/A mg/I
ug/I
Arsenic N/A mg/1
Chromium: Total
N/A mg/I
Other FLUORIDE
0.58 mg/I
Grease and Oils N/A mg/l
Cu - Copper
N/A mg/l
Other MIBK
N/A ug/I
mg/I Hardness: Total N/A m
Fe - Iron
N/A mg/I
Other Ag - Silver
N/A mg/I
Phenol N/A mg/1
Hg - Mercury
N/A mg/I
Other Se - Selenium
N/A mg/I
K - Potassium
N/A mgll
ug/I
Sulfate <10 mg/1
Mg - Magnesium
N/A mg/l
ug/1
Specific Conductance N/A uMohs
Total Ammonia(NH4 + NH3) N/A mg/I
Mn - Manganese
N/A mg/I
TKN as N N/A mg/I
Na - Sodium
N/A mg/l
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTEE (AUTHORIZED AGENT)
er
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
DATE
F fn
Uri
n

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MANAG VMENT.
P.O. BOX 29535
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION
Address P.O. BOX 48 AURORA, NC 27806
Well Location : Tank Farm
Well I.D. Number: WLCT
County: BEAUFORT
Well Depth:
n/a
PERMIT NO.: 06-0071— WO-0005
Non -Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
_Spray Field Subsurface Low -Pressure
Land Appl of Sludge
Rotary Distributor _x_Other
Well Diameter n/a
Depth to Water Level n/a
Measuring Point is n/a
Gallons of water pumped/bailed before sampling
Sample (Screened) Interval
Ft. belowmeas. pt.(before sampling) or
Ft. above land surface or
CONTINUOUS
Field Analysis: pH 7.0 Specific Conductance
Date Sample Collected 04/27/95
n/a
Na
Ft. to n/a Ft.
n/a Ft. (MSL)
Date Lab Sample Analyzed 0427-05/26
Laboratory Name : PCS PII05PI ,ATE ENV. AFFAIRS LAB Certification No.
Ft. (MSL)
800 uMhos Temp
1994
26.0 oC Odor NONE
Appearance: CLEAR
330(Tg Env. Lab). 102 (TOC and Metals). 78 ( Coliform Only)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total <1 /100m1
Dissolved Solids: Total
TH"(whsrr aria i dJ
TOC
Chloride
544 mg/I
7:4-s-
5.6 mg/I
81.7 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/1
Hardness: Total N/A mg/1
Phenol N/A mg/I
Sulfate <10 mg/I
Specific Conductance N/A uMohs
Total Ammonia(NH4 + NH3) N/A mg/1
TKN as N N/A mg/I
NO2 as N
NO3 as N
Phosphorus: Total as P
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd - Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K - Potassium
Mg - Magnesium
Mn - Manganese
Na - Sodium
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
/10,d(1,t4'"
SIGNATURE OF PERMITTEE (OR
THORIZED AGENT)
N/A mg/I
N/A mg/I
0.024 mg/1
N/A mg/I
N/A mg/I
N/A mg/I
<0.001 mg/I
<0.02 mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/1
<0.01 mg/1
N/A mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
NO
Pesticides/Herbicides (Specify)
Other FLUORIDE
Other MIBK
Other Ag - Silver
Other Se - Selenium
N/A mg/1
N/A mg/1
N/A mg/I
ug/I
ug/I
ug/I
0.50 mg/I
N/A ug/I
N/A mg/1
N/A mg/I
ug/I
ug/I
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
DATE

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MANNE1113NT;
•
Y.O. BOX 29535
Facility Name: PCS PHOSPHATE CO. — AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071- WO-0005
Non -Discharge Tank Farm Remedial System
_ Lagoon _Septic Tank/Drain Field
_Spray Field _Subsurface Low -Pressure
_Land Appl of Sludge
Well Location : Tank Farm
visuiouror
_x_vu
�motary
Well I.D. Number: CIW-7 Well Depth: 48.00 Well Depth:
Well Diameter 4" Sample (Screened) interval
31.00 Ft. to 45.25 Ft.
Depth to Water Level n/a Ft. below meas. pt.(before sampling) or
n/a Ft. (MSL)
Measuring Point is 3.33 Ft. above land surface or
13.13 Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pll 7.0 Specific Conductance
725 uMhos Temp 20.0 oC Odor
NONE
Date Sample Collected 04/27/95 Date Lab Sample Analyzed 04/27-05/26 1994 Appearance: CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330(Tg Env Lab). 102 (TOC and METALS) and 78 (Coliform Only)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD N/A mg/I
NO2 as N
N/A mg/1
Ni - Nickel
N/A
mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/1
Pb - Lead
N/A
mg/1
Coliform: MF Total <1 /100m1
Phosphorus: Total as P
0.019 mg/1
Zn - Zinc
N/A
mg/I
Dissolved Solids: Total 608 mg/1
Al - Aluminum
N/A mg/I
Pesticides/Herbicides(Specify)
7.4-nits
Ba - Barium
N/A mg/1
ug/I
per )
TOC 5 mg/1
Ca - Calcium
N/A mg/I
ug/I
Chloride 83.6 mg/I
Cd - Cadmium
<0.001 mg/1
ug/l
Arsenic N/A mg/I
Chromium: Total
<0.02 mg/I
Other FLUORIDE
0.51
mg/1
Grease and Oils N/A mg/I
Cu - Copper
N/A mg/I
Other MIBK
N/A
ug/l
Hardness: Total N/A mg/I
Fe - Iron
N/A mg/1
Other Ag - Silver
N/A
mg/1
Phenol N/A mg/1
Hg - Mercury
N/A mg/1
Other Se - Selenium
N/A
mg/1
Sulfate <10 mg/1
K - Potassium
N/A mg/i
ug/I
Specific Conductance N/A uMohs
Mg - Magnesium
N/A mg/I
u�
Total Ammonia(NH4 + NH3) N/A mg/I
Mn - Manganese
<0.01 mg/I
TKN as N N/A mg/1
Na - Sodium
N/A mg I
CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
/j%44(44
SIGNATURE OF PERMITTEE (Of3 UTHORIZED AGENT)
er
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
j ,5
DATE
C7
t� cTt
c/1
rn
..r C7.

' COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MA AGFMEN.J'
P.O. BOX 29535
RALEIGII. NC 27626-0535
[phone]
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071 -WI-0238
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
Spray Field _Subsurface Low —Pressure
_Land Appl of Sludge
Well Location : Tank Farm
Rotary Distributor _x_OU
Well I.D. Number. MWTFI—C
Well Depth: 41.20 Ft.
Well Diameter 2"
Sample (Screened) Interval
38.70 Ft.
to 40.70 Ft.
Depth to Water Level
5.10 Ft. below meas. pt.(before sampling) or
5.39 Ft. (MSL)
Measuring Point is
0.00 Ft. above land surface or
10.49 Ft. (MSL)
Milliliters of water purged before sampling
2200
Field Analysis: pH 7.1
Specific Conductance
710 uMhos Temp 21.5 oC Odor
NONE
Date Sample Collected 04/27/95
Date Lab Sample Analyzed
04/27-05/02
1994 Appearance: LT YLLW CLDY
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330(Tg Env Lab). 102 (TOC and METALS) and 102 (Metals and Coliform)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD
N/A
mg/I
NO2 as N
N/A
mg/1
Ni — Nickel N/A
mg/1
Coliform: MF Fecal
N/A
/100m1
NO3 as N
N/A
mg/1
Pb — Lead N/A
mg/I
Coliform: MF Total
<1
/100m1
Phosphorus: Total as P
0.234
mg/1
Zn — Zinc N/A
mg/1
Dissolved Solids: Total
576
mg/I
AI — Aluminum
N/A
mg/I
Pesticides/Herbicides (Specify)
piftwtrei ana a
Ba — Barium
N/A
mg/I
ug/1
TOC
5.6
mg/I
Ca — Calcium
N/A
mg/I
ug/1
Chloride
80.8
mg/1
Cd — Cadmium
<0.001
mg/I
ug/I
Arsenic
N/A
mg/I
Chromium: Total
<0.02
mg/I
Other FLUORIDE 0.46
mg/1
Grease and Oils
N/A
mg/I
Cu — Copper
N/A
mg/I
Other MIBK N/A
ug/1
Hardness: Total
N/A
mg/I
Fe — Iron
N/A
mg/1
Other Ag - Silver N/A
mg/I
Phenol
N/A
mg/I
fig — Mercury
N/A
mg/1
Other Se — Selenium N/A
mg/I
Sulfate
<10
mg/1
K — Potassium
N/A
mg/1
ug/I
Specific Conductance
N/A
uMohs
Mg — Magnesium
N/A
mg/I
ug/I
Total Ammonia(NH4 + NH3)
N/A
mg/1
Mn — Manganese
<0.01
mg/I
TKN as N
N/A
mg/I
Na — Sodium
N/A
mg/I
Note: Micro —Purge System used for Sampling
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
"1/%44-i4
SIGNATURE OF PERMITTEE (OR AUTRIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Jr5U'/ j-
DATE
er
11:C nd z- Nnr s6

PCS�•
Phosphate AURORA DIVISION
P. O. BOX 48, AURORA, NC 27806
May 30, 1995
Underground Injection Control Program
Groundwater Section
NC - DEHNR, Division of Environmental Management
P. O. Box 29535
Raleigh, North Carolina 27626-0535
Subject: Quarterly Monitoring Data
for Tank Farm Remedial Action System
Dear Sirs:
W
Please find enclosed the Supplemental Tank Farm Remedial Action System quarterly
groundwater monitoring data for your information. These data are from samples collected
during April, 1995. The sampling and analysis of water from the injection well system as
required by Permit No. 06-0071-W0-0005 is also included.
Please contact me or Tim Walls if you have any questions_ regarding this information.
Sincerely,
��L%Ki�?i41
W. A. Schimming
WAS:TFW/tfw
Attachments
pc: Willie Hardison - DEM, WRO (w/attch)
12-01-005-06 (w/o attch)
00-12-000 (w/o attch)
12-01-008-03-002 (w/ attch)
C:\WORD\TFQTRFT.TFW
U: \WALLS \ TFQTRPT.TF W

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MANAGEMENT
P.O. BOX 29535
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071-WO-0005
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
_Spray Field _Subsurface Low —Pressure
_Land Appl of Sludge
Well Location :
Tank Farm
I Rotary Distributor _x_Ot
Il
Well I.D. Number:
IN!. SUPPLY Well Depth: 179.0 Well Depth:
Well Diameter
6" Sample (Screened) Interval N/A
Ft. to N/A Ft.
Depth to Water Level
N/A Ft. below meas. pt.(before sampling) or
N/A
Ft. (MSL)
Measuring Point is
1.00 Ft. above land surface or
N/A
Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.9 Specific Conductance
790 uMhos Temp 18.5 oC Odor
NONE
Date Sample Collected
01/18/95 Date Lab Sample Analyzed 01/18-01/30
1994 Appearance: CLEAR
Laboratory Name
TEXASGULF INC. Certification No. 330 AND 102 (TOC ONLY)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD
N/A mg/I
NO2 as N
N/A
mg/1
Ni — Nickel
N/A
mg/I
Coliform: MF Fecal
N/A /100m1
NO3 as N
N/A
mg/1
Pb — Lead
N/A
mg/1
Coliform: MF Total
N/A /100m1
Phosphorus: Total as P
0.015
mg/1
Zn — Zinc
N/A
mg/I
Dissolved Solids: Total
656 mg/I
Al — Aluminum
N/A
mg/1
Pesticides/Herbicides (Specify)
. (011‘rratmly..t.d)
7.4--.stai s—
Ba — Barium
N/A
mg/I
ug/1
TOC
2 mg/1
Ca — Calcium
N/A
mgll
ug/I
Chloride
94.1 mg/I
Cd — Cadmium
N/A
mg/I
ug/I
Arsenic
N/A mg/I
Chromium: Total
N/A
mg/1
Other FLUORIDE
0.62
mg/1
Grease and Oils
N/A mg/I
Cu — Copper
N/A
mg/I
Other MIBK
N/A
ug/I
Hardness: Total
N/A mg/1
Fe — Iron
N/A
mg/I
Other Ag — Silver
N/A
mg/1
Phenol
N/A mg/I
Fig — Mercury
N/A
mg/I
Other Se — Selenium
N/A
mg/I
Sulfate
<10 mg/I
K — Potassium
N/A
mg/I
ug/I
Specific Conductance
N/A uMohs
Mg — Magnesium
N/A
mg/I
ugfl
Total Ammonia(NH4 + NII3)
N/A mg/I
Mn — Manganese
N/A
mg/I
TKN as N
N/A mg/I
Na — Sodium
N/A
mg/l
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
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COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MANAGEMENT:
P.O. BOX 29535
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071 —WO-0005
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
_Spray Field _Subsurface Low —Pressure
_Land Appl of Sludge
Well Location :
Tank Farm
t_HQINYuistnoutor
_x_vu
WeII I.D. Number:
WLCT
Well Depth: n/a
Well Diameter
n/a
Sample(Screened) Interval
n/a
Ft. to n/a Ft.
Depth to Water Level
n/a
Ft. below meas. pt.(before sampling) or
n/a
Ft. (MSL)
Measuring Point is
Na
Ft. above land surface or
n/a
Ft. (MSL)
Galbns of water pumped/bailed before sampling
CONTINUOUS
Field Analysis: pH 6.8
Specific Conductance
790 uMhoa Temp 30.0 oC Odor
NONE
Date Sample Collected
01/18/95
Date Lab Sample Analyzed
01/18-01/30
1994 Appearance: CLEAR
Laboratory Name
TEXASGULF INC. Certification No.
330 (Tg Env. Lab). 102 (TOC and Metals), 78 ( Coliform Only)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD N/A mg/I
NO2 as N N/A
mall
Ni — Nickel
N/A
mg/I
Coliform: MF Fecal
N/A
/100m1
NO3 as N
N/A
mg/I
Pb — Lead
N/A
mg/I
Coliform: MF Total
<1
/100ml
Phosphorus: Total as P
0.014
mg/I
Zn — Zinc
N/A
mg/I
Dissolved Solids: Total
490
mg/l
Al — Aluminum
N/A
mg/1
Pesticides/Herbicides (Specify)
twitetrsne )
7
nfia--
Ba — Barium
N/A
mg/I
ug/1
,pl
TOC
2
mg/I
Ca — Calcium
NIA
mg/I
ug/I
Chloride
72.2
mg/I
Cd — Cadmium
<0.001
mg/l
ug/1
Arsenic
N/A
mg/I
Chromium: Total
<0.001
mg/1
Other FLUORIDE
0.48
mg/1
Grease and Oils
N/A
mg/I
Cu — Copper
N/A
mg/I
Other MIBK
N/A
ug/I
Ilardness: Total
N/A
mg/I
Fe — Iron
N/A
mg/I
Other Ag — Silver
N/A
mg/I
Phenol
N/A
mg/I
Hg — Mercury
N/A
mg/1
Other Se — Selenium
N/A
mg/I
Sulfate
<10
mg/I
K — Potassium
N/A
mall
ug/I
Specific Conductance
N/A
uMohs
Mg — Magnesium
N/A
mg/I
ug/I
Total Ammonia(NH4 + NH3)
N/A
mg/l
Mn — Manganese
0.06
mg/I
TKN as N
N/A
mg/1
Na — Sodium
N/A
mg/l
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
er
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COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MANAGEMENT
P.O. Box 29535
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071—WO-0005
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
_ Spray Field _Subsurface Low —Pressure
_Land Appl of Sludge
Well Location :
Tank Farm
HOtaly UISIIIDUTor
_x_VII
Well I.D. Number:
CIW-7 Well Depth: 48.00 Well Depth:
Well Diameter
4" Sample (Screened) Interval
31.00 Ft. to 45.25 Ft.
Depth to Water Level
n/a Ft. belowmeas. pt.(before sampling) or
n/a Ft. (MSL)
Measuring Point is
3.33 Ft. above land surface or
13.13 Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 7.0 Specific Conductance
700 uMhos Temp 18.0 oC Odor
NONE
Dale Sample Collected
01/18/95 Date Lab Sample Analyzed 01/18-01/30 1994 Appearance: CLEAR
Laboratory Name
TEXASGULF INC. Certification No. 330(Tg Env Lab), 102 (TOC and METALS) and 78 (Coliform Only)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD N/A mg/I
NO2 as N
N/A mg/1
Ni — Nickel
N/A
mg/1
Coliform: MF Fecal
N/A /100m1
NO3 as N
N/A mg/I
Pb — Lead
N/A
mg/I
Coliform: MF Total
<1 /100m1
Phosphorus: Total as P
0.014 mg/1
Zn — Zinc
N/A
mg/1
Dissolved Solids: Total
614 mg/I
Al — Aluminum
N/A mall
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.4 units
Ba — Barium
N/A mall
ugjl
TOC
1.7 mg/1
Ca — Calcium
N/A mg/I
ug/1
Chloride
88.9 mg/1
Cd — Cadmium
<0.001 mg/1
ug/1
Arsenic
N/A mg/1
Chromium: Total
<0.001 mg/1
Other FLUORIDE
0.59
mg/1
Grease and Oils
N/A mg/1
Cu — Copper
N/A mg/I
Other MIBK
N/A
ug/1
Hardness: Total
N/A mg/I
Fe — Iron
N/A mg/1
Other Ag — Silver
N/A
mall
Phenol
N/A mg/1
Hg — Mercury
N/A mg/I
Other Se — Selenium
N/A
mall
Sulfate
<10 mg/I
K — Potassium
N/A mg/I
ug/f
Specific Conductance
N/A uMohs
Mg — Magnesium
N/A mg/1
ug/I
Total Ammonia(N1I4 + NH3)
N/A mg/I
Mn — Manganese
0.05 mg/1
TKN as N
N/A mg/I
Na — Sodium
N/A mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
n�^' I A In,— r'r nr 3IAITT/f7( 81 ITLIC 1I7Cr1 t o.pqn
er
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
-/; 9JI
IlATF
tiZ :£ bid 9 I AVW S6

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COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MANAGEMENT
p O BOX 29535
RALEIGH. NC 27626-0535
[phone]
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-007 1 —W1-0238
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
_Spray Field _Subsurface Low —Pressure
_Lend Appl of Sludge
Well Location : Tank Farm
Rotary Distributor _x_Ot
Well I.D. Number: MWTF1—C
Well Depth: 41.20 Ft.
Well Diameter 2"
Sample(Screened) interval
38.70 Ft.
to 40.70 Ft.
Depth to Water Level
6.24 Ft. below meas. pt.(before sampling) or
425 Ft. (MSL)
Measuring Point is
0.00 Ft. above land surface or
10.49 Ft. (MSL)
Milliliters of water purged before sampling
3600
Field Analysis: pH 6.7 Specific Conductance
690 uMhos Temp 18.5 oC Odor
NONE
Date Sample Collected 01/18/95 Date Lab Sample Analyzed 01/18-01/30
1994 Appearance: LT CLDY YLLW
Laboratory Name TEXASGULF INC. Certification No. 330 (Tg Env Lab). 102 (TOC and METALS) and 102 (Metals and Coliform)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD N/A mg/I
NO2 as N
NIA
mg/l
Ni — Nickel N/A
mg/I
Coliform: MF Fecal
N/A /100m1
NO3 as N
N/A
mg/I
Pb — Lead N/A
mg/I
Coliform: MF Total
<1 /100m1
Phosphorus: Total as P
0.254
mg/I
Zn — Zinc N/A
mg/I
Dissolved Solids: Total
538 mg/I
Al — Aluminum
N/A
mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.0 units
Ba — Barium
N/A
mg/I
ug/I
TOC
3.3 mg/I
Ca — Calcium
N/A
mg/1
ug/1
Chloride
84.7 mg/I
Cd — Cadmium <0.001
mg/I
ug/1
Arsenic
N/A mg/1
Chromium: Total <0.001
mg/1
Other FLUORIDE 0.50
mg/1
Grease and Oils
N/A mg/I
Cu — Copper
N/A
mg/1
Other MIBK N/A
ug/1
Hardness: Total
N/A mg/1
Fe — Iron
N/A
mg/I
Other Ag — Silver N/A
mg/I
Phenol
N/A mg/I
Iig — Mercury
N/A
mg/1
Other Se — Selenium N/A
mg/1
Sulfate
<10 mg/I
K — Potassium
N/A
mg/I
ug/I
Specific Conductance
N/A uMohs
Mg — Magnesium
N/A
mg/I
ug/I
Total Ammonia(NI14 + NI13)
N/A mg/I
Mn — Manganese
0.17
mg/1
TKN as N
N/A mg/1
Na — Sodium
N/A
mg/1
Note: Micro —Purge System used for Sampling
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
jetZt4.44,741-‘-g--)/
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
er
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COMPLIANCE MONITORING DIVISION OFENVIRONMENTALMANAGEM13Nf
GROUNDWATER QUALITY MONITORIf :3 3 f£ 011 J P.U.14oX29535
COMPLIANCE REPORT FORM
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071- WO-0005
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
Spray Field Subsurface Low —Pressure
_ Land Appl of Sludge
Well Location : Tank Farm
Rotary Distributor _x_Otl
179.0 Well Depth:
Well I.D. Number: INJ. SUPPLY Well Depth:
Well Diameter 6" Sample(Screened) Interval N/A Ft. to N/A Ft.
Depth to Water Level N/A Ft. below meas. pt.(before sampling) or N/A Ft. (MSL)
Measuring Point is 1.00 Ft. above land surface or N/A Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pit 7.tif Specific Conductance 825 uMhos Temp 21.5 oC Odor
NONE
Date Sample Collected 10/26/94 Date Lab Sample Analyzed 10/26-11/08 1994 Appearance:
CLEAR
Laboratory Name TEXASGULF INC. Certification No. 330 AND 102 (TOC ONLY)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED X YES
NO
COD N/A mg/1
NO2 as N N/A mg/I
Ni — Nickel
N/A mg/1
Coliform: MI' Fecal N/A /100nil
NO3 as N N/A mg/I
Pb — Lead
N/A mg/1
Coliform: MFTotal N/A /100m1
'Z.n — Zinc
N/A mg/1
Phosphorus: Total as P 0.036 mg/I
Dissolved Solids: Total 560 mg/to
Al — Aluminum N/A mg/I
Pesticides/l lerbicidcs (Specify)
pH (when analyzed) 7.1 units
Ba — Barium N/A mg/I
ug/1
TOC 5.5 mg/1
Ca — Calcium N/A mg/I
ug/I
bride 95.1 mg/1
Cd — Cadmium N/A mg/I
ug/1
Chromium: Total N/A mg/1
Other FLUORIDE
0.57 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/1
Cu — Copper N/A mg/I
Other MIRK
N/A ug/1
I ardness: Total N/A mg/1
Fe -• Iron N/A mg/1
Other Ag — Silver
N/A mg/1
Phenol N/A mg/I
Ilg — Mercury N/A mg/1
Other Se — Selenium
N/A mg/1
Sulfate <10 mg/1
K — Potassium N/A mg/1
ug/1
Specific Conductance N/A uMohs
Mg — Magnesium N/A mg/I
ug/I
Total Ammonia(NI14 + NII3) N/A mg/I
Mn — Manganese N/A mg/I
TKN as N N/A mg/I
Na — Sodium NIA mg/I
_
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
f?.1 /s4
SIGNATU OF PERMITTE,J(OR AUTHORIZED AGENT)
er
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back).
C - 1 k4N i2•7p.1.
/-Li-�f
DATE

A#1)(/L4�Li?
SIGNATURE OF PERMITTEE(OR AUTHORIZED AGENT)
COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
3
(1j)IVISION OF ENVIRONMENTAL MANAGI:MENF,
911 3 Li V Li { l P.o. BOX 29535
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
PERMIT NO.: 06-007 1 —WO-0005
Non —Discharge Tank Farm Remedial System
Lagoon Septic Tank/Drain Field
_Spray Field Subsurface Low —Pressure
_Land Appl of Sludge
Address P.O. BOX 48 AURORA, NC 27806
Well Location :
Tank Farm
Rotary Distributor _x_Ott
Well I.D. Number:
WLCT
Well Depth: n/a
Well Diameter
n/a
Sample (Screened) Interval
n/a
Ft. to n/a Ft.
Depth to Water Level
n/a
Ft. below meas. pt.(before sampling) or
n/a
Ft. (MSL)
Measuring Point is
n/a
Ft. above land surface or
n/a
Ft. (MSL)
Gallons of water pumped/bailed before sampling
CONTINUOUS
field Analysis: pH 7.1t
Specific Conductance
775 uMhos Temp 20.5 oC Odor
NONE
Date Sample Collected
10/26/94
Date Lab Sample Analyzed
10/26-11/08
1994 Appearance: CLEAR
Laboratory Name
TEXASGULF INC. Certification No.
330 (Tg Env. Lab). 102 (TOC and Metals), 78 ( Coliform Only)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD
N/A
mg/I
NO2 as N
N/A
mg/l
Ni — Nickel
N/A
mg/I
Coliform: MI? Fecal
N/A
/100m1
NO3 as N
N/A
nig/I
Pb — Lead
N/A
mg/I
Coliform: MFTotal
<1
/100m1
Phosphorus: Total as P
0.021
mg/I
Zit — Zinc
N/A
mg/I
Dissolved Solids: Total
500
mg/4
Al — Aluminum
N/A
mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.1
units
Ba — Barium
N/A
mg/I
ug/I
TOC
5.16
mg/lo
Ca — Calcium
N/A
ntg/I
ug/l
Chloride
85.7
mg/I
Cd — Cadmium
<0.001
mg/1
ug/I
Arsenic
N/A
mg/1
Chromium: Total
<0.02
mg/I
Other FLUORIDE
0.53
mg/I
Grease and Oils
N/A
mg/I
Cu — Copper
N/A
mg/I
Other MIBK
N/A
ug/1
Hardness: Total
N/A
mg/I
Fe — Iron
N/A
mg/1
Other Ag — Silver
N/A
mg/I
Phenol
N/A
mg/I
Hg — Mercury
N/A
mg/I
Other Se — Selenium
N/A
mg/1
Sulfate
<10
mg/1
K — Potassium
N/A
mg/1
ug/l
Specific Conductance
N/A
uMolts
Mg — Magnesium
N/A
mg/1
ug/1
Total Anunonia(N114 + NH3)
N/A
mg/I
Mn — Manganese
<0.01
mg/I
TKN as N
N/A
mg/1
Na — Sodium
N/A
mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
DATE
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W

COMPLIANCE MONITORING GROUNDWATER QUALITY MONITORII 3 3 Ii Q 3 P.O.BOX 29535
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MANAGENIENF
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071- WO-0005
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
_Spray Field _Subsurface Low —Pressure
_Land Appl of Sludge
Well Location :
Tank Farm
Rotary Distributor
x Otf
Well I.D. Number:
CIW-7 Well,Depth: . 48.00 Well Depth:
Well Diameter
4" Sample (Screened) Interval
31.00 Ft. to 45.25 Ft.
Depth to Water Level
Na Ft. below meas. pt.(before sampling) or
n/a Ft. (MSL)
Measuring Point is
3.33 Ft. above land surface or
13.13 Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 7.1 # Specific Conductance
825 uMhos Temp 21.5 oC Odor
NONE
Date Sample Collected
1026/94 Date Lab Sample Analyzed 10/26-11/08 1994 Appearance: CLEAR
Laboratory Name
TEXASGULF INC. Certification No. 330 (Tg Env Lab). 102 (TOC and METALS) and 78 (Coliform Only)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD
N/A mg/I
NO2 as N
N/A mg/I
Ni — Nickel
N/A
mg/1
Coliform: MF Fecal
N/A /100m1
NO3 as N
N/A mg/1
Pb — Lead
N/A
mg/1
Coliform: MF Total
<1 /100m1
Phosphorus: Total as P
0.024 mg/I
Zit — Zinc
N/A
mg/1
Dissolved Solids: Total
528 mg/1 1
Al — Aluminum
N/A mg/I
Pesticides/I lerbkides (Specify)
pl I (when analyzed)
7.0 units
Ba — Barium
N/A mg/1
ug 1
.,TOC
5.05 mg/1
Ca — Calcium
NIA mg/I
ug/I
Chloride
94.9 mg11
Cd — Cadmium
<0.001 mg/I
ug/I
Arsenic
N/A mg/1
Chromium: Total
<0.02 mg/I
Other FLUORIDE
0.71
mg/I
Grease and Oils
N/A mg/I
Cu — Copper
N/A mg/1
Other MIIIK
N/A
ug/1
I ardness: Total
N/A mg/1
Fe — Iron
N/A mg/1
Other Ag — Silver
N/A
mg/1
Phenol
N/A mg/1
lig — Mercury
N/A mg/1
Other Se — Selenium
N/A
mg/1
Sulfate
<10 mg/I
K — Potassium
N/A mg/I
ug/I
Specific Conductance
N/A uMohs
Mg — Magnesium
N/A mg/I
ug/1
Total Ammonia(NI14 + NI13)
N/A mg/1
Mn — Manganese
<0.01 mg/1
TKN as N
N/A mg/1
Na — Sodium
N/A mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE CSF PERMITTEE
AUTHORIZED AGENT)
er
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
DATE
MIN

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
1)wlslON OF ENVIRONMENTAL MANAGEMENT
P.O. BOX 29535
RAI.FIGl1, NC 27626-0535
(919) 733 -3221
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
91,13 3 '1 0 r.} 8
PERMIT NO.: 06-0071— WI-0238
Non -Discharge Tank Farm Remedial System
Lagoon _Septic Tank/Drain Field
_Spray Field Subsurface Low -Pressure
_Land Appl of Sludge
Well Location : Tank Farm
-J Rotary Distributor
_x_Oth
Well I.D. Number: MWFF1-C
Well Depth: 41.20 Ft.
Well Diameter 2"
Sample(Screened) Interval 38.70
Ft.
to 40.70Ft.
Depth to Water Level
6.00 Ft. below meas. pi(before sampling) or
4.49 Ft. (MSL)
Measuring Point is 0.00 Ft. above land surface or 10.49
Ft. (MSL)
Milliliters of water purged before sampling
2200
Field Analysis: p1I 6.9
Specific Conductance
625 uMhos Temp 22.0 oC Odor
NONE
Date Sample Collected
10/26/94
Date Lab Sample Analyzed 10/26-11/08
1994 Appearance: VY LT RST BRWN
Laboratory Name TEXASGULF INC. Certification No. 330 (Tg Env Lab). 102 (TOC and METALS) and 102 (Metals and Coliform)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD
N/A
mg/I
NO2 as N
N/A
mg/I
Ni - Nickel
N/A
mg/I
Coliform: MF Fecal
N/A
/100m1
NO3 as N
N/A
mg/1
Pb - Lead
WA
mg/I
Coliform: MF Total
<1
/100m1
i torus: 'Total as P
0.29
mg/I
Zn - Zinc
NIA
mg/1
Dissolved Solids: Total
• 460
mg/I
Al - Aluminum
N/A
mg/1
Pesticides/Ilerbicides (Specify)
'r'"
pl I (when analyzed)
7.3
units
Ha - Barium
N/A
mg/I
ug/I C3"
TOC
3.32
mg/1
Ca - Calcium
N/A
mg/I
ug/1 W
Cd - Cadmium <0.001
mg/I
ugnC')
IIIIW
662
mg/y
Chromium: Total <0.02
mg/I
Other FLUORIDE
0.51
mg/I -13
Arsenic
N/A
mgn
Grease and Oils
N/A
mg/I
Cu - Copper
N/A
mg/I
Other MIRK
NIA
ugn_,.,,
llardness: Total
N/A
mg/I
Fe - Iron
N/A
mg/1
Other Ag - Silver
N/A
mg/Ito
Phenol
N/A
mg/I
lig - Mercury
N/A
mg/I
Other Se - Selenium
N/A
mg/I
Sulfate
10.6
mg/I
K - Potassium
N/A
mg/I
ugn
Specific Conductance
N/A
uMohs
l
Total Ammonia(N114 + NII3)
N/A
mg/I
Mn - Manganese
0.05
mg/I
TKN as N
N/A
mg/1
Na - Sodium
N/A
n1g 1
Note: Micro —Purge System used for Sampling
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
%tero: ��
SIGNATUROF PERMITT,E (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
//'z9
DATE
er

4
`;COMPUANCE MONITORIN
pROUNOWATER QUA:UTY MONITORI
COMPLIANCE REPORTIORM
IVISCOI fJF ONX Ok: 11.0f6 StMA'AM
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location : Tank Farm
Well I.D. Number
Well Diameter
Depth to Water Level
Measuring Point is
PERMIT NO.: 06-0071— W O — 0005
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
_Spray Field Subsurface Low —Pressure
Land Appl of Sludge
Rotary Distributor 'Oth.t"'f'
60,
WLCT Well Depth: n/a �i p
n/a Sample (Screened) Interval n/a
Ft. to n/a Pt. �/t
n/a Ft. below meas. pt.(before sampling) or n/a Ft. (MSL) ' a t4
n/a Ft. above land surface or n/a Ft. (MSL) -E�
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH
Date Sample Collected
7.1 Specific Conductance
800 uMoos 1'emp
59.5'oCbdor NONE
07/29/94 Date Lab Sample Analyzed 07/29-8/18 1994 Appearance: CLEAR
Laboratory Name TEXASGULF INC. Certification No. 330 (Tg Env. Lab), 102 (TOC ONLY)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES NO
COD N/A mg/I
NO2 as N N/A mg/I
Ni — Nickel N/A mg/1
Cotiform: MF Fecal N/A /100m1
NO3 as N N/A mg/I
Pb — Lead N/A mg/I
Coliform: MA Total <1 /100m1
Dissolved Solids: Total 314 mg/1
Phosphorus: Total as P 0.071 mg/I
Al — Aluminum N/A mg/I
Zn — Zinc N/A mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed) 7.6 units
TOC 5.2 mg/1
Ba — Barium N/A mg/I
Ca — Calcium N/A mg/1
ug/1
ug/I
Chloride 45.6 mg/I
Cd — Cadmium 0.00131 mg/I
ug/1
Arsenic N/A mg/1
Chromium: Total 0.00198 mg/1
Other FLUORIDE 0.28 mg/1
Grease and Oils N/A mg/1
Hardness: Total N/A mg/I
Phenol N/A mg/1
Sulfate' <10 mg/1
Cu — Copper N/A mg/1
Fe — Iron N/A mg/1
Hg — Mercury N/A mg/I
K — Potassium N/A mg/1
Other MIRK N/A ug/I
Other Ag — Silver N/A mg/I
Other Se — Selenium N/A mg/I
ug/l
Specific Conductance N/A uMohs
Total Ammonia(NH4 + NH3) N/A mg/I
TKN as N N/A mg/1
Mg — Magnesium
N/A mg/I
ug/1
Mn — Manganese
<0.00001 mg/I
Na — Sodium N/A mg/I
TOC RECHECK VALUES
Contract Lab
Tezasgutf Lab
7.0 mg/
3.0 mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
•
. SIC TU • E OF PERMITTE(OR AUTHORIZEC ENT) , , _ MATE
c2 402_.1 k 4rf l'!crgy

�COMC�LlANGC.» MQNlTORCNGI
GROIJNDWATERQUAUTY MONITOR(
COMPLIANCE REPORT FORM
_W.t15
-IOC. �.
rieia
h.ue.r
40.i.
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071-WO-0005
Non -Discharge Tank Farm Remedial System
Lagoon _Septic Tank/Drain Field
— _Spray Field _Subsurface Low -Pressure
_Land Appl of Sludge
Well Location : Tank Perm
j__FUIarY IJI•lI1VulM
- "
k.'
Well I.D. Number: CI W -7
Well Depth: 48.00 Well Depth:
Well Diameter 4"
Sample (Screened) Interval
31.00 Ft.
10 45.25 Pt.
�A`,
Depth to Water Level
n/a
Ft. below meas. pt.(before sampling) or
n/a Ft. (MSL) `
Measuring Point is
3.33 Ft. above land surface or
13.13 Ft. (MSL) `}
Gallons of water pumped/bailed before sampling
CONTINUOUS
,-:`
Meld Analysis: pH 7.2
Specific Conductance
575 uMhos Temp 341k dor
NONE
Date Sample Collected
07/29/94
Date Lab Sample Analyzed 7/29-8/18
1994 Appearance: - ---CLEAR
Laboratory Name TEXASGULF INC.
Certification No. 330 AND 102 (TOC ONLY) r
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD N/A mg/I
NO2 as N
N/A
mg/1
Ni - Nickel
N/A
mg/l
Coliform: MF Fecal
N/A
/100m1
NO3 as N
N/A
mg/I
Pb - Lead
N/A
mg/I
Coliform: MF Total
<1
/100m1
Phosphorus: Total as P
0.050
mg/l
Zn - Zinc
N/A
mg/I
Dissolved Solids: Total
396
mg/1
Al - Aluminum
N/A
mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.6
units
Ba - Barium
N/A
mg/I
ug/1
TOC 4 L •L.
tA.44 S.1
mg/I
Ca{Calcium
N/A
mg/I
ng/I
'Chloride
47.7
mg/l
IJ
cal"- Caddy s f., . ,
; v�U DA0907 ,
:,t
r = "
ug/1
Arsenic
N/A
mg/I
Chromium: Total
0.00192
mg/1
Other FLUORIDE
0.31
mg/I
Grease and Oils
N/A
mg/I
Cu - Copper
N/A
mg/I
Other MIBK
N/A
ug/l
Hardness: Total
N/A
mg/I
Fe - Iron
N/A
mg/1
Other Ag - Silver
N/A
mg/I
Phenol
N/A
mg/l
Hg - Mercury
N/A
mg/I
Other Se - Selenium
N/A
mg/1
Sulfate
<10
mg/1
K - Potassium
N/A
mg/)
ug/1
Specific Conductance
N/A
uMobs
Mg - Magnesium
N/A
mg/l
ug/I
Total Ammonia(NH4 + NH3)
N/A
mg/1
Mn - Manganese
0.0001
mg/1
TOC RECHECK VALUES
Contract Lab
Texasgulf Lab
5.0 mg/1
3:: mg/1
TKN as N
N/A
mg/1
Na - Sodium
• N/A
mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIC TU E OF PERMI E (OR AUTHORIZED ENT)
.r
O
Note: Values should reflect dissolvedndi
colloidal concentrations. (see #3 on back)
f-3/- Cif
411ATE
L h : l Wd Z - d3S +6
KAIf q • 750'
/,f -A. Du .,n of -NI 70(1 rii /I -1

OMi uANcg >NONITORirvi
GROUNDWATER QUALITY MONITORIN
COMPLIANCE REPORT FORM
wisl N OI;! BN'VYI IONMENTA46.:$60gMA
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071- WO -0005
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tank/Drain Field
_Spray Field Subsurface Low —Pressure
_ Land Appl of Sledge
Well Location : Tank Farm
Rotary Distributor _x_Oth
Well I.D. Number. INJ. SUPPLY Well Depth: 179.0 Well Depth:
jl
Well Diameter 6"
Sample (Screened) Interval N/A
Ft. to N/A Ft.
Depth to Water Level
N/A Ft. below meas. pt.(before sampling) or N/A Pt. (MSL)
Measuring Point is
1.00 Ft. above land surface or N/A PI. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.8 Specific Conductance
790 uMhos Temp 19.5 oC Odor
NONE
Date Sample Collected
07/29/94 Date Lab Sample Analyzed 7/29-8/18
1994 Appearance: CLEAR
Laboratory Name TEXASGULF INC. Certification No. 330 AND 102 (TOC ONLY) t
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD
N/A mg/1
NO2 as N
N/A mg/I
Ni — Nickel
N/A mg/1
Coliform: MP Fecal
N/A /100m1
NO3 as N
N/A mg/I
Pb — Lead
N/A mg/I
Coliform: MF Total
N/A /100m1
Phosphorus: Total as P
0.034 mg/1
Zn — Zinc
N/A mg/I
`Dissolved Solids: Total
586 mg/I
Al — Aluminum
N/A mg/1
Pesticides/Herbicides (Specify)
/
pH (when analyzed)
7.4 units
Ba — Barium
N/A mg/1
tig/1
/ TUC
6.1 mg/1
Ca — Calcium
N/A mg/1
ug/I
Chloride
91.8 mg/1
Cd — Cadmium
N/A mg/)
ug/I
Arsenic
N/A mg/1
Chromium: Total
N/A mg/I
Other FLUORIDE
0.57 mg/1
Grease and Oils
N/A mg/1
Cu — Copper
N/A mg/I
Other MIBK
N/A ug/I
Hardness: Total
N/A mg/I
Fe — Iron
N/A mg/I
Other Ag — Silver
N/A mg/I
Phenol
N/A mg/1
Hg — Mercury
N/A mg/I
Other Se — Selenium
N/A mg/I
Sulfate
<10 mg/1
K — Potassium
N/A mg/1
ug/I
Specific Conductance
N/A uMohs
Mg — Magnesium
N/A mg/1
ug/I
Total Ammonia(NH4 + NH3)
N/A mg/I
Mn — Manganese
N/A mg/1
TOC RECHECK VALUES
Contract Lab
Texasgulf Lab
7.0 mg/I
5.0 . mail
TKN as N
N/A mg/1
Na — Sodium
N/A mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
Note:
Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
•TE
SIC FUI E OF PERMIT E (OR AUTHORIZED ENT)
c.%.-c. J bit/ `f•/r•cici

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL MANAOEMBN 1'
p.a. BOX 29535
RALEIGH, NC 27626-0533
(9I9) 733-322I
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 40 AURORA, NC 27806
PERMIT NO.: 06-0071- WI-0238
Non —Discharge Tank Farm Ramsdial System
Lagoon _Septic Tank/Drab Field
_spray Plaid _Subsurlacs Low —Pressure
_Land Appl of Sludge
Well Location :
Tank Farm
Rotary Distributor _x va
WelI.D. Number.
MWTF1—C Well Depth: 41.20 Ft.
Well Diameter
2" Sample (Screened) Interval
38.70 Ft. to 40.70 Pt.
Depth to Water Level
4.34 Ft. below meas. pt.(before sampling) or
6.15 Ft. (MSL)
Measuring Point is
0.00 Ft. above land surface or
10.49 Ft. (MSL)
Milliliters of water purged before sampling 2100
Field Analysis: pH 6.8 Specific Conductance
750 uMbos Temp 22.5 oC Odor
NONE
Date Sample Collected
07/29/94 Date Lab Sample Analyzed 7/29-8/18 1994 Appearance: CLEAR
Laboratory Name
TEXASGULF INC. Certification No. 330 AND 102 (TOC ONLY)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED X
YES
NO
N/A mg/1
COD
N/A mg/I
NO2 as N
N/A mg/1
Ni — Nickel
Coliform: MF Fecal
N/A /100m1
NO3 as N
N/A mg/1
Pb — Lead
N/A mg/I
Coliform: MF Total
<1 /100m1
Phosphorus: Total as P
0.213 mg/1 .
Zn — Zinc
N/A mg/I
DimoIved Solids: Total
534 mg/I
Al — Aluminum
N/A mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.0 units
Ba — Barium
N/A mg/I
ug/I
TOC —
h 7....14.61.0 mg/1
Ca — Calcium
N/A mg/l
ug/I
_J1
Chloride
76.8 mg/1
Cd — Cadmium
0.00246 mg/1
ug/1
Arsenic
N/A mg/I
Chromium: Total
0.00434 mg/I
Other FLUORIDE
0.47 mg/I
Grease and Oils
N/A mg/1
Cu — Copper
N/A mg/I
Other MIBK
N/A ug/I
Hardness: Total
N/A mg/1
Fe — Iron
N/A mg/I
Other Ag — Silver
N/A mg/1
Phenol
N/A mg/1
Hg — Mercury
N/A mg/I
Other Se — Selenium
N/A mg/I
Sulfate
9.1 mg/I
K — Potassium
N/A mg/I
ug/1
Specific Conductance
N/A uMohs
Mg — Magnesium
N/A mg/I
ug/l
Total Ammonia(NH4 + NH3)
N/A mg/1
Mn — Manganese
<0.00001 mg/I
TOC RECHECK VALUES
Contract Lab
Texaagulf Lab
N/A mg/I
4.0 mg/I
TKN as N
N/A mg/I
Na — Sodium
N/A mg/l
kr...e. to:....._D.....n C,ctam „cars fro- Camnlino
Note:
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
er

C01_ L.ECTION AID kNALYSIS OF GROUNDWAT' SAMPLES
1 S,riiit-i s siroulcl be analyzed a:; soon as possible alter collection. SAMPLES WHICH ARE HOT ANALYSED WITHIN THE HOLDIIIG 1IME SPECI-
FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
('i ialyscs: Use Staidard L1ell►od 3030C for sample preparation (rne►cury excluded). DO NOT FILTER METALS SAMPLES III THE FIELD i!_!
'!r ! H;r';r1 sarnples must be collected for metals, then field acidified with 5 rnl concentrated nitric acid per liter of sample, and should be submitted I(J rl�
lab • ',ithin 2.1 Bern-.
Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
3 A1In1 'ISES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
Gil:`1111DWATEFI, NOT THOSE THAT ARE A PART CIF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As poi Title 15. iloitli Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
tin following publications, or by other methods approved beforehand by the Director, Division of Environmental
Moiragemerit:
(a) Standard Methods for the Exarnination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA-600/4.79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equiprnent must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above)
10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents.

COMPLIANCE MONITORING
REPORT
Facility Name:
TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
PERMIT NO.: 06- 0071- W O -0005
Non —Discharge Tank Farm Remedial System
Lagoon _SepticTank/Drain Field
_Spray Field _Subsurface Low —Pressure
Land Appl of Sludge
Address P.O. BOX 48 AURORA, NC 27806
Well Location :
Tank Farm
Rotary Distributor _x_Othe:
Well I.D. Number:
INJ. SUPPLY Well Dept. 179.0 Ft.
Well Diameter
6" Sample (Screened) Interval
N/A
FT to N/A FT
Depth to Water Level
N/A ft. below meas. pt.(before sampling) or
N/A (MSL)
Measuring Point is
1.00 feet above land surface or
N/A
ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH )( 7.1 19 Specific Conductance
675 uMhos Temp 19.0 oC Odor
NONE
Date Sample Collected
04/14/94 Date Lab Sample Analyzed
4/14-4/26
1994 Appearance: CLEAR
Laboratory Name
TEXASGULF INC. Certification No.
330 AND 102 (TOC ONLY)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD
N/A mg/I
NO2 as N
N/A mg/I
Ni — Nickel
N/A mg/I
Coliform: MF Fecal
N/A /100m1
NO3 as N
N/A mg/1
Pb - Lead
N/A mg/I
Coliform: MF Total
)( N/A /l0onij
Phosphorus: Total as P
✓
0.038 mg/I
Zn — Zinc
N/A mg/1
Dissolved Solids: Total
X 494 mg/I
Al — Aluminum
N/A mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.1 units
Ba — Barium
N/A mg/I
ug/I
TOC
3.84 mg/I
Ca — Calcium
N/A mg/I
ug/I
Chloride
X 67.6 mg/I
Cd — Cadmium
X
N/A mg/I
ug/1
Arsenic
N/A mg/I
Chromium: Total
k
N/A mg/I
Other FLUORIDE
0.60 mg/I
Grease and Oils
N/A mg/I
Cu — Copper
N/A mg/I
Other MIBK
N/A ug/1
Hardness: Total
N/A mg/I
Fe — Iron
N/A mg/I
Other Ag — Silver
N/A mg/I
Phenol
N/A mg/1
Hg — Mercury
N/A mg/1
Other Se — Selenium
N/A mg/I
Sulfate
we/ <10 mg/I
K — Potassium
N/A mg/1
ug/I
Specific Conductance
N/A uMohs
Mg — Magnesium
N/A mg/1
ug/I
Total Ammonia(NH4 + NH3)
N/A mg/I
Mn — Manganese
Y
N/A mg/I
Note: Values should reflect total concentrations
TKN as N
N/A mg/1
Na — Sodium
N/A mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
CiefASPM/14"
SIGNAT RE OF PERMITTEE, R AUTHORIZED AGENT)
;1
/r //i/
DATE
•
>/to t
or not
ekna4/2-e4(,

COMPLIANCE MONITORING
REPORT
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071- WO - 0005
Non —Discharge Tank Farm Remedial System
Lagoon _SeptkTanWDrain Field
_Spray Field _Subsurface Low—PreDaure
Laud Appl of Sludge
Well Location :
Tank Farm
Rotary Diatributcr
t Other
Well I.D. Number:
CI W-7 Well Dept 48.00 Well Depth:
Well Diameter
4" Sample (Screened) Interval
31.00 FT to 45.25 FT
Depth to Water Level
n/a ft. below meas. pt.(before sampling) or n/a
(MSL)
Measuring Point is
3.33 feet above land surface or
13.13 ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analvei: pl1 6.9t«* Specific Conductance
525
uMhos Temp 19.0 oC Odor
NONE
Date Sample Collected
04/14/94 Date Lab Sample Analyzed 4/14-4/26
1994 Appearance: CLEAR
Laboratory Name
TEXASGULF INC. Certification No. 330 AND 102 (TOC ONLY)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD
N/A mg/1
NO2 as N
N/A
mg/1
Ni — Nickel
N/A
mg/I
Coliform: MF Fecal
N/A /100m1
NO3 as N
N/A
mg/I
Pb — Lead
N/A
mgfl
Coliform: MF Total
<1 /100m1
Phosphorus: Total as P
0.497
mg/1
Zn — Zinc
N/A
mg/1
Dissolved Solids: Total
384 mg/I
Al — Aluminum
N/A
mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.3 units
Ba — Barium
N/A
mg/I
ug/I
TOC
3.86 mg/I
Ca — Calcium
NIA
mg/I
ug/1
Chloride
54.6 mg/I
Cd — Cadmium
<0.01
mg/I
ug/1
Arsenic
N/A mg/I
Chromium: Total
0.34
mg/1
Other FLUORIDE
0.48
mg/1
Grease and Oils
N/A mg/1
Cu — Copper
N/A
mg/I
Other MIBK
N/A
ug/I
Hardness: Total
N/A mg/I
Fe — Iron
N/A
mg/I
Other Ag — Silver
N/A
mg/I
Phenol
N/A mg/I
Hg — Mercury
N/A
mg/I
Other Se — Selenium
N/A
mg/1
Sulfate
<10 mg/I
K — Potassium
N/A
mg/I
net
Specific Conductance
N/A uMohs
Mg — Magnesium
N/A
mg/1
ug/1
Total Ammonia(NH4 + NH3)
N/A mg/1
Mn — Manganese
0.1
mg/I
Note: Values should reflect total concentrations
TKN as N
N/A mg/1
Na — Sodium
N/A
mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
aria
SIGNAT RE OF PERMIT E (OR AUTHORIZED AGENT)
' ,7
ammo
GJ

r
COMPLIANCE MONITORING
REPORT
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
PERMIT NO.: 06-0071- WO-0005
Non —Discharge Tank Farm Remedbl System
_Lagoon _Septic Tank/Draln Field
_Spray Field Subsurface Low —Pressure
_Land Appl of Sludge
Address P.O. BOX 48 AURORA, NC 27806
Well Location :
Tank Farm
_Rotary Distributer
x_Otber
We1I I.D. Number.
WLCT Well Dept n/a Well Depth:
Well Diameter
nla Sample (Screened) Interval n/a
FT to n/a FT
Depth to Water Level
n/a ft. below meas. pt.(before sampling) or n/a
(MSL)
Measuring Point is
n/a feet above land surface or n/a
ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 7.0 Specific Conductance
675 uMhos Temp 20.0 oC Odor
NONE
Date Sample Collected
04/14/94 Date Lab Sample Analyzed 04/14-4/26
1994 Appearance: CLEAR
Laboratory Name
TEXASGULF INC. Certification No. 330 AND 102 (TOC ONLY)
SAMPLES FOR METALS WERE
AND FIELD ACIDIFIED
X YES
NO
COLLECTED UNFILTERED
COD
N/A mg/I
NO2 as N
N/A mg/I
Ni — Nickel
N/A mg/I
Coliform: MP Fecal
N/A /100m1
NO3 as N
N/A mg/1
Pb — Lead
N/A mg/I
Coliform: MF Total
<1 /100m1
Phosphorus: Total as P
0.042 mg/I
Zn — Zinc
N/A mg/1
Dissolved Solids: Total
484 mg/I
Al — Aluminum
N/A mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.0 units
Ba — Barium
N/A mg/I
ug/I
TOC
3.8 mg/1
Ca — Calcium
N/A mg/I
ug/I
Chloride
65.1 mg/I
Cd — Cadmium
<0.01 mg/I
ug/I
Arsenic
N/A mg/I
Chromium: Total
0.25 mg/1
Other FLUORIDE
0.59 mg/I
Grease and Oils
N/A mg/I
Cu — Copper
N/A mg/1
Other MIBK
N/A ug/I
Hardness: Total
N/A mgfl
Fe — Iron
N/A mg/1
Other Ag — Silver
N/A mg/I
Phenol
N/A mg/I
Hg — Mercury
N/A mg/I
Other Se — Selenium
N/A mg/I
Sulfate
<10 mg/I
K — Potassium
N/A mg/1
ug/I
Specific Conductance
N/A uMohs
Mg — Magnesium
N/A mg/I
net
Total Ammonia(NH4 + NH3)
N/A mg/I
Mn — Manganese
<0.01 mg/1
Note: Values should reflect total concentrations
TKN as N
N/A mg/I
Na — Sodium
N/A mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
TORE OF
PER R11 T'TEE (OR AUTHORIZED AGENT)

Co
1
tti
i

„viPLIANCE MONITORING
REPORT
Facility Name:
TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071— W I —0238
Noe —Discharge Tank Farm Remedial System
__Lagoon Sepik Tank/Drabs Field
_Spray Field __Subsurface Low —Pressure
_land Appl of Sludge
Well Location :
Tank Fann
Rotary DletrIbuIcv
x Otba
WellI.D. Number:
MWTF1—C
Well Dept 41.20 Pt.
Well Diameter
2”
Sample (Screened) Interval
38.70 FT to 40.70 FT
Depth to Water Level
8.20 ft. below meas. pl.(before sampling) or
2.29 (MSL)
Measuring Point is
0.00 feet above land surface or
10.49 ft. (MSL)
Milliliters of water purged before sampling
900
Field Analysis: pH
6.5
Specific Conductance
700 uMhos
Temp 21.5 oC Odor
NONE
Date Sample Collected
04/14/94
Dale Lab Sample Analyzed 4/14-4/26
1994 Appearance: VRY LT YLLW
Laboratory Name
TEXASGULF INC. Certification No. 330 AND 102 (TOC ONLY)
SAMPLES FOR METALS WERII COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD
N/A
nig/I
NO2 as N
N/A
ntg/1
Ni — Nickel
N/A
mg/I
Coliform: MF Fecal
N/A
/100m1
NO3 as N
N/A
ntg/l
Pb — Lead
N/A
mg/I
Coliform: MF Total
<l
/100m1
N/A
Zn — Zinc
N/A
mg/I
-504
mg/I ',
Al — Aluminum
nig/I
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.0
units
Ra — Barium
N/A
tng/I
ug/I
TOC
3.37
nig/I
Ca — Calcium
N/A
mg/I
ug/1
Arsenic
98;
N/A
ing/I
told — Ca
<0.010
0.51
N/A
mg/I
ug/I
Curoutiuna: Total ram'°
mg/I /
Other FLUORIDE
0.53
mg/1
Grease and Oils
N/A
mg/1
Cu — Copper
mg/I
Other MIRK
N/A
ug/I
Hardness: Total
N/A
tng/I
Fe — Iron
N/A
mg/I
Other Ag — Silver
N/A
mg/1
Phenol
N/A
ing/I
llg — Mercury
N/A
mg/I
Other Se — Selenium
N/A
mg/I
Sulfate
<10
mg/I
K — Potassium
N/A
mg/1
ug/I
Specific Conductance
N/A
uMohs
Mg — Magnesium
N/A
0.12
mg/I
ug/I
Total Ammonia(NI-14 + NH3)
N/A
mg/I
MI
Note: Values should reflect total concentrations
TKN as N
N/A
mg/I
Na — Sodium
N/A
mg/I
Note: Micro —Purge System used for sampling
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
c-4111,714;:r
RE OF PERMITT
SIGNATU FOR AUTHORIZED AGENT)

COMPLIANCE MONITORING
REPORT
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071-WO-0005
Noo—DIscbarge Tank Fenn HemedIsISyetesu
lagoon —Rook Took/Drain Flo Id
.__Spray Feld _Svburfece Low -Pressure
_ Land Appl of Studge
Farm
Rotary Distributer _x_utaer
Well Location : Tank
WeII LD. Number: IN]. SUPPLY Well Dept 179.0 Ft.
Well Diameter 6" Sample (Screened) Interval N/A FT to N/A FT
Depth to Water Level N/A ft. below meas. pt.(before sampling) or N/A (MSL)
Measuring Point is 1.00 feet above land surface or N/A ft. (MSL)
before sampling CON11NLJOUS
Gallons of water pumped/bailed
Analysis: 7.24 Specific Conductance 775 uMhos Temp 17.5 oC Odor NONE
!;Field pH
Date Sample Collected 01/10/94
Dale 1.ab Sample Analyzed 1/10-1/20 1994 Appearance: CLEAR
Laboratory Name TEXASGULF INC. Certification No. 330 AND 102 (TOC ONLY)
SAMPLES FOR METALS WERE COLLECTED 1INPILTERIiD ANI) FIELD ACIDIFIED X YES NO
— — COD N/A nrg/1
NO2 as N N/A mgA
Ni - Nickel N/A mg/I
Coliform: MP Pecal N/A /100m1
Coliform: MP Total ' N/A >
NO3 as N N/A mgA
Ph - Lead N/A - mg/1
Phosphorus: Total as P 0.035 mg/I
Zn - Zinc N/A mg/I
AI - Aluminum N/A mg/I
Pesticides/Ilerbicides (Specify)
Dissolved Solids: Total 562 m•
Ba - Barium N/A mg/I
ug/I
(when analyzed) 7.3 units
pH
TOC 4.09 mg/I
('a - Calcium N/A ntg/I
ug/l
ug/I
NIA mg/10
Chloride 84.I _
4111111111111W
Bit
Other FLUORIDE 0.59 mg/I
Arsenic N/A ntg/I
Cu - Copper N/A mg/I
Other MIBK N/A ug/l
Grease and Oils N/A mg/I
Hardness: Total N/A mg/I
Pe - Iron N/A mg/I
Other Ag - Silver N/A mg/I
Phenol N/A mg/I
IIg - Mercury N/A mg/I
Other Se - Selenium N/A mg/I
Sulfate <10 tng/1
K - Potassium N/A mg/I
ug/I
Mg - Magnesium N/A mg/I
ug/I
Specific Conductance N/A uMohs
Total Ammonia(NI14 + N113) N/A mg/I
1111100zapnese N/A na
Note: Values should reflect total concentrations
Na - Sodium N/A mg/I
TKN as N N/A rng/I
I CERTIFY THAT THIS RREPORT-IS TRUE AND ACCURATE
1 J. J
SIGNATU E OF I MI T (bF AUTitIORIZED AGENT)
DAT E
ako,,AP41 S?/q

COMPLIANCE MONITORING
REPORT
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071—WI —0238
Non— Discharge Tank Farm Remedial System
__lagoon ___Septic Tank:Theta Field
_Spray Field _Subsurface Low—Preuure
lend Appl of Sludge
Well Location :
Tank Farm
KNIT/ Uutrtuurrr
_:-anuar
41.20 Ft.
WeII I.D. Number:
MWTFI—C Well Dept
Interval
38.70 FT to 40.70 FT
Well Diameter
2" Sample (Screened)
Depth 10 Water Level
7.94 ft. below meas. pt.(before sampling) or
2.55 (MST.)
Measuring Point is
0.00 feet above land surface or
10.49 ft. (MSL)
Gallons of water before sampling 28.3
pumped/bailed
Field Analysis: pil 6.7 Specific
Conductance
725 uMhoe Temp 20.0 oC Odor
NONE
1994 Appearance: CLEAR
Date Sample Collected
01/10/94 Date Lab Sample Analyzed 1/10-1/20
Laboratory Name
TEXASGULF INC.
Ceslineation No. 330 AND 102 (TOC ONLY)
X YES
NO
SAMPLES FOR METALS WERE COI.I.IEC7EI) UNFILTERI: t) AND FIELD ACIDIFIED
COD
N/A mg/1
NO2 as N
N/A mgA
Ni — Nickel
N/A mg/1
N/A mgA
Pb — Lead
N/A mgA
Coliform: MF Fecal
N/A /100ns1
NO3 as N
Coliform: MF Total
<1 /100n1
oapborus: Total as P
0.319 min
Zn — Zinc
N/A mgA
N/A mg/I
Pesticides/Ilerbicidea (Specify)
Dissolved Solids: Total
540 map
Al — Aluminum
(when analyzed)
6.7 units
Ba — Barium
N/A mgA
ug/1
p11
TOC
3.81 mg/1
Ca — Calcium
N/A mgA
ug/I
Chloride
79.1
, s<
<o.olt
ug/1
Arsenic
N/A mgA
Chromium Total
<0.02 mgA
Other FLUORIDE
0.48 mgA
N/A mg/I
Other M1BK
N/A ug/I
Grease and Oik
N/A mgA
Cu — Copper
hardness: Total
N/A mgA
Fe — Iron
N/A mgA
Other Ag — Silver
N/A mgA
Phenol
N/A mg/I
lig — Mercury
N/A mgA
Other Se — Selenium
N/A mgA
Sulfate
<10 mg/I
K — Potassium
N/A mgA
ug/1
N/A mgA
ug/l
Specific Conductance
N/A uMohs
Mg — Magnesium
Total Ammonia(N114 + N113)
N/A mgA
1111144anganese
0.12 mgA i
Note: Values should reflect total concentrations
TKN as N
N/A mg/1
Na — Sodium
N/A mg/I
I CERTIFY THAT TNjtp I PART IS TRUE AND ACCURATE
9 _
SIGNATURE OF PERMITT OR -AUTHORIZED AGENT)
2/Y94/'
.
# X

COMPLIANCE MONITORING
REPORT
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071-W0-0005
Non -Discharge Taok Farm Remedial System
__Lagoon Sep.kTank/DralnMold
_Spray Feld _Subsurface Low -Pressure
Land Appl of Sludge
Well Location : Tank Farm
Well1.D. Number: CIW-7 Well Dept 48.00 Well Depth:
4e Sample (Screened) interval 31.00 PT to 45.25 FT
Well Diameter
Water Level n/a ft. below meas. pt.(before sampling) or n/a (MSL)
Depth to
Point is 3.33 feet above land surface or 13.13 ft. (MSL)
Measuring
before sampling CONTINUOUS
Gallons of water pumped/bailed
Field Analysis: 7.0 Specific Conductance 700 uMhos
Temp 16.0 oC
Odor NONE
pHI
Collected 01/10/94 Date Lab Sample Analyzed 1/10-1/20 1994 Appearance: CLEAR
Dale Sample
TEXASGULF INC. Certification No. 330 AND 102 (TOC ONLY)
Laboratory Name
NO
UNFILTERED AND FIELD ACIDIFIED X YES
SAMPLES FOR METALS WERE COLLECTED
N/A
NO2 as N N/A mg/1
Ni — Nickel N/A mg/1
COD mg/1
N/A
N/A /100m1
N( )3 as N N/A mg/I
Pb — I.cad mgA
Coliform: MP Fecal
<1 /100m1
Phosphorus: Total as I' 0.039 mg/I
Zn — Zinc N/A mg/1
Coliform: MF Total
540 mg/1
Al — Aluminum N/A mg/I
Pesticides/Ilerbicides (Specify)
Dissolved Solids: Total
(when analyzed) 7.3 units
lla — Barium N/A mg/1
ugll
p11
4.22 mg/I
(a — Calcium N/A mg/I
ug/I
TOC
Cd — Caehninnn 0.01 mg/1
ug/1
Chloride 82.2 mg/I
Arsenic N/A mg/I
Chromium: Total <0.02 mg/I
Other FLUORIDE 0.58 mg/I
Grease and Oils N/A mg/I
Cu — Copper N/A mg/I
Other MIRK N/A ug/
Hardness: Total N/A tng/1
Fe — Iron N/A mg/1
Other Ag — Silver N/A mg/I
Phenol N/A mg/1
I Ig — Mercury N/A mg/I
Other Se — Selenium N/A mg/1
<10 mg/1
K — Potassium N/A mg/I
ug/I
Sulfate
Specific Conductance N/A uMohs
Mg — Magnesium N/A mg/I
u�
Total Ammonia(N114 + N113) N/A mg/1
Mn — Manganese <0.01( mg/I
TKN as N N/A mg/I
Ns — Sodium N/A mg/I
Note: Values should reflect total concentrations
I CERTIFY THAT THIStiBEPQRT:jIT. TRUE AND ACCURATE
J .,.4 - J
SIGNATUF E OF PERMIT) E (OR AUTI-IORIZED AGENT)
11II4L
U7
v(j 1't1

eCTa3
COMPLIANCE MONITORING
REPORT
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071- WO-0005
Non —Discharge Tank Farm Remedial System
_Lagoon _Septic Tenk/Dralu Field
_Spray Field _Subsurface Low —Pressure
_Land Appl d Sludge
Well Location :
Tank Farm
jRotary Dlnrlbutor c Othrr
Well I.D. Number:
INJ. SUPPLY
Well Dept 179.0 Ft.
Well Diameter
6" Sample
(Screened) Interval
N/A
FT to N/A F1'
Depth to Water Level
N/A ft.
below nteas. pl.(before sampling) or
N/A
(MSL)
Measuring Point is
1.00 feet above land surface or
N/A
ft. (MSL)
Gallons of water pumped/bailed before sampling
CONTINUOUS
Field Analysis: pit 6.9
Specific Conductance
775
uMhos Temp 1/ 19.0 oC Odor
NONE
Date Sample Collected
10/28/93
Date Lab Sample Analyzed
10/28-11/19
1993 Appearance: CLEAR
Laboratory Name
TEXASGULF INC.
Certification No.
330 AND 102 (TOC ONLY)
N/A
mg/1
Ni - Nickel
N/A mg/1
COD
-.. zt.Pi rr
b11;_J
NO2 as N
Colifortn: MI' Fecal
N/A
/100rn1
NO3 as N
N/A
mg/I
Pb - Lead
N/A mg/I
Coliform: MFTotal
Dissolved Solids: Total
— r.N/A
/I00m1
Phosphorus: 'Total as P
✓0.032
mg/I
Zn - Zinc
N/A mg/I
y „492
mg/1 p
Al - Alunaintut
N/A
mg/I
Pesticides/llerbicidea (Specify)
pH (when analyzed)
7.3
units
Ila - Barium
N/A
mg/I
ug/1
TOC
/<1.0
mg/I
Ca - Calcium
0- Cadmium
N/A
mg/I
ug/I
*ride
—
idameskitraw
Y(4011111110
ug/I
Arsenic
N/A mg/Iprromium:
'Total
Cu - Copper
Fe - Iron
X.1111111/11
Other FLUORIDE
0.59 mg/I
Grease and Oils
N/A
mg/I
N/A
rng/l
Other MIRK
N/A ug/I
Ilardness: Total
N/A
ntg/I
N/A
mg/1
Other Ag - Silver
N/A mg/1
Phenol
N/A
mg/1
1fg - Mercury
N/A
mg/1
Other Se - Selenium
N/A mg/I
Sulfate
1/ <10
mg/1
K - Polassiuut
N/A
mg/I
ugfl
Specific Conductance
N/A
uMohs
Mg - Magnesium
N/A
mg/I
ug/I
Total Ammonia(N114 + N113)
N/A
mg/I
ilk! - Manganese
ki g•1
Note: Values should reflect total concentrations
TKN as N
N/A
mg/I
Na - Sodium
N/A
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURAIE
SIGNATl7R OF PERMITTEE R AUTHORIZED AGENT)
T E
C•'
C'7
1
• ,) i•
.'J I • 1
Cam - --- 6--b t(
S.la •Q

COMPLIANCE MONITORING
REPORT
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071- W I -0238
Non—DIscherge Took Fern RemedYi System
tallow _Sepik TeeklDn In Meld
_Spray Field Subsurface Low —Pressure
Laud Appl of Sludge
Well Location :
Tank Farm
LRoger/ Distributor
• Other
Well I.D. Number:
MWTFI —C
Well Dept 41.20
F1.
Ir
Well Diameter
2"
Sample (Screened) Interval
38.70 FT to 40.70 FT
Depth to Water Level
6.68 ft. below meas. pt.(before sampling) or
3.81 (MSL)
Measuring Point is
0.00 feel above land surface or
10.49 ft. (MSL)
Gallons of water pumped/bailed before sampling
39.0in
Field Analysis: pi!
s/ 6.9
Specific Conductance
725
uMhos Temp jr-20.0 oC Odor
NONE
Date Sample Collected
10/28/93
Date Lab Sample Analyzed
10/28-11/19
1993 Appearance: CLEAR
Laboratory Name
TEXASGUI.F INC. Certification No.
330 AND 102 (TOC ONLY)
COD
N/A
mg/I
NO2 as N
N/A
mg/I
Ni — Nickel
N/A
mg/1
Coliform: MF Fecal
N/A
/1 t0m1
NO3 as N
N/A
mg/I
Pb — Lead
N/A
mg/1
Coliform: MF Total
'I/ <1
/100m1
AlliplegrinWas P
Al — Alnntintim
•OIW
Zn — Zinc
N/A
mg/1
Dissolved Solids: Total
4/468
mg/I
N/A
mg/I
Pesticides/Ilerbicides (Specify)
p11 (when analyzed)
7.6
units
Ba — barium
N/A
mg/I
ugA
TOC
/
V 1.2
mg/1
Ca — Calcium
N/A
mg/I
WI
Chloride
mg/1
Cd — Cadmium
<0.10
mg/1
ug/I
Arsenic
N/A
Chromium: Total
4 <0.0.
I mg/I
Other FLUORIDE ✓
0.47
mg/I
Grease and Oils
N/A
mg/I
Cu — Copper
N/A
mg/I
Other MIRK
N/A
ug/I
Hardness: Total
N/A
mg/1
Fe — Iron
N/A
mg/I
Other Ag — Silver
N/A
mg/1
Phenol
N/A
mg/1
Fig — Mercury
N/A
mg/1
Other Se — Selenium
N/A
mg/I
Sulfate
✓ <10
mgfl
K — Potassium
N/A
mg/1
ugfl
Specific Conductance
N/A
uMohs
Mg — Magnesium
/A
mg/1
u�
Total Ammonia(N114 + NFI3)
N/A
mg/1
Mn — Manganese
)<0.10
mg/I
Note: Values should reflect total concentrations
TKN as N
N/A
mg/I
Na — Sodium
N/A
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
!` ,J<Z!% / 6/W
SIGNATU E OF PERMITT,E (OR AUTHORIZED AGENT)
///Jc)/
DATE
tt�
O
'.7
ry
:1
r .)
04
(5-' IO.9-7

COMPLIANCE MONITORING
REPORT
Facility Name: TEXASGULF INC. PHOSPHATE OPERATIONS County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Tank Farm
Well Location :
PERMIT NO.: 06-0071- WO-0005
Nos— Dlschsrge Tank Farm Re medial System
_Lassos __Sept lc Tank/Ihaln Field
_Spray Field Subsurface 1.mr—Reuure
_land Appl of Sludge
_ .Rotary Distributor z Other
IWen LD. Number:
Well Diameter
C'1 W-7
4"
wen wept ��•w
Sample (Screened) Interval
31.00 FT to
45.25 FT
Depth to Water Level
n/a
ft. below meas. pt.(before sampling) or
n/a
(MSL)
Measuring Point is
3.33 feet above land surface or
13.13 ft. (MST.)
-
Gallons of water pumped/baile
before sampling
CONTINUOUS
NONE
Conductance
750
uMohs Temp
.� 24.5 oC Odor
Field Analysis: pl1
6.9
Specific
Date Sample Collected
10128/93
Date Lab Sample Analyzed
10/28-11/19
1993 Appearance: CLEAR
Laboratory Name
TEXASGUI.F INC.
Certification No.
330 AND 102 (TOC ONLY)
N/A mg/I
Ni — Nickel
N/A
mg/1
COD
:k4Offtng/14
NO2 as N
/100mt
NO3 as N
N/A
mg/1
Pb — Lead
N/A
mg/I
Coliform: MF Fecal
N/A
Coliform: MF Total
✓ <1
/100m1
Phosphorus: Total as P
/ 0.038
mg/I
Zn — Zinc
NIA
mg/1
intalyed Solids: Total
x
Al — Aluminum
N/A
ntg/1
Pesticides/Iterbicides (Specify)
n
Ba — Barium
N/A
mg/Iu�
(w a
pH
TOC
s// 1.04
mg/1
Ca — Calcium
N/A
mg/I
ug/1
ug/I
<0.02
mg/1
/
Other FLUORIDE ✓
0.51
mg/1
Arsenic
N/A
tngt
Chromium: Total
V
N/A
mg/1
Other MIRK
WA
ugfl
Grease and Oils
N/A
mg/I
Cu — Copper
Ilardness: Total
N/A
mg/1
Fe — Iron
N/A
mg/1
Other Ag — Silver
N/A
mg/I
Phenol
mg/1
IIg — Mercury
N/A
mgA
Other Se — Selenium
N/A
mg
Sulfate
�N/A
r <10
mg/l
K — Potassium
N/A
mg/I
uJI
Specific Conductance
N/A
uMohs
Mg — Magnesium
N/A
1,0..0
mgA
ugf
ntg/i ;.
Note: Values should reflect total concentrations
Total Ammonia(N114 + N113)
N/A
mg/1 _
IN Manganese
mg/I
TKN as N
N/A
mg/I
N.t — Sodium
N/A
I CERTIFY THAT THIS REPORT IS TRUF AND ACCURATE
SIGNATURE OF PERMITTEE, OR AUTH(IRIZED AGENT)
DATE
1)
C.1
I ri
�Rf
5
-II- i�f

Tub 4,5
,,dlCE MONITORING
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: 06-0071-WO-0005
Well Location Tank Farm Non -Discharge TANK FARM REMEDIAL SYSTEM
Well I.D. Number INJ. SUPPLY Well Depth 179.00 Ft. NPDES
Well Diameter 6" Sample (Screened) Interval N/A Ft. to N/A Ft. _Lagoon Septic Tank/Drain Field
Depth to Water Level N/A ft. below meas. pt.(before sampling) or N/A MSL _Spray Field Subsurface Low -Pressure
_
Measuring Point is 1.00 feet above land surface or N/A ft. (MSL) _Land Appl of Sludge ---Piping (LPP)
Gallons of water pumped/bailed before sampling CONTINUOUS _Rotary Distributor _x_Other
Field Analysis: pH 6.8 Specific Conductance 790 uMhos Temp 20.5 oC Odor NONE Appearance CLEAR
Date Sample Collected 07/28/93 Date Lab Sample Analyzed 7/28-8/06 1993
Laboratory Name
TEXASGULF INC. Certification No. 330
COO N/A mg/l
NO2 as N
N/A mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/l
Coliform: MF Total <1 /100ml
Oftsotved Solids: Total 574 mg/l
Phosphorus: Total as P* 0.022 mg/l
Ni - Nickel N/A mg/l
Pb - Lead N/A mg/l
Zn - Zinc
Al - Aluminum
N/A mg/1
pH (when analyzed) 7.3 units
Ba - Barium N/A mg/l
N/A mg/l
Pesticides/Heribicides (Specify)
TOC 4.00 mg/t
Ca - Calcium N/A mg/l
Chloride 90.3 mg/l
Cd - Cadmium N/A mg/l
Arsenic N/A mg/t
Chromium: Total
Grease and Oils N/A mg/t
Hardness: Total N/A mg/l
Fe - Iron
N/A mg/t
ug/l
us
(mil
Other FLUORIDE 0.53 mg/l
ug/L
N/A mg/l
Phenol
N/A mg/l
Hg - Mercury N/A mg/l
Sulfate
<10 mg/l
K - Potassium
N/A mg/l
Specific Conductance N/A uMohs
Mg - Magnesium
N/A mg/l
Total Ammonia(NH4 + NH3) N/A mg/l
Mn - Manganese
N/A mg/l
TKN as N
N/A mg/t
Na - Sodium
N/A mg/t
Note:
Values should reflect total
concentrations.
ug/1
ug/l
ug/t
ug/l
IFY T T THIS REP,
e/li{il n+N1
tLNMITuE
RT IS TRUE
ND ACCURATE
(UR AUTHORIZED Al
* Resampled 11/30/92 and
analyzed 12/02/92.

N/A mg/t
Na - Sodium
N/A mg/L
Note:
Values should reflect total
concentrations.
.,rCE MONITORING
932. ti 3 i90
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number MWTF1-C Well Depth 41.20 Ft.
Well Diameter 2"
Sample (Screened) Interval 38.70 Ft. to 40.7 Ft.
Depth to Water Level 4.29 ft. below meas. pt.(before sampling) or 6.2 MSL
Measuring Point is 0.00 feet above land surface or 10.49 ft. (MSL)
Gallons of water pumped/bailed before sampling 37.00
Field Analysis: pH
PERMIT NO.:
Non -Discharge
NPDES
Lagoon
_Spray Field
_Land Appl of Sludge
Rotary Distributor _x_Other
6.5 Specific Conductance 750 uMhos Temp 20.5 oC Odor NONE
Date Sample Collected 07/28/93 Date Lab Sample Analyzed 7/28-8/06 1993
Laboratory Name TEXASGULF INC. Certification No. 330
Appearance CLEAR
COD
Coliform: MF fecal
N/A mg/l
N/A /100m1
NO2 as N N/A mg/l
NO3 as N N/A mg/1
Ni - Nickel
Pb - Lead
N/A mg/l
N/A mg/l
Coliform: MF Total
<1 /100m1
DA3soliya011sall;t4#1,0otsl.:�,
pH (when analyzed) 7 units
Chloride
Arsenic
80.8 mg/l
N/A mg/l
Pillsphorus: TO.teaL: 4s:if! <O r : 1/:t
Al - Aluminum N/A mg/l
Ba - Barium N/A mg/l
Zn - Zinc
N/A mg/L
Pesticides/Heribicides (Specify)
ug/t
Ca - Calcium N/A mg/l
Cd - Cadmium eu f,t2, t<0.01 mg/t ;?
Chromium: Total <0.02 mg/l
ug/L
Other FLUORIDE
ug/l
0.41 mg/l
Grease and Oils
Hardness: Total
Phenol
N/A mg/l
N/A mg/l
N/A mg/t
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/l
N/A mg/l
N/A mg/l
ug/l
ug/l
Sulfate
Specific Conductance
<10 mg/1
N/A uMohs
K - Potassium
Mg - Magnesium
N/A mg/l
N/A mg/t
ug/l
ug/l
ug/l
Total Ammonia(NH4 + NH3)
N/A mg/1
Mn - Manganese
0.01 mg/t
TKN as N
t CE
I GNA
THIS REPO•
NA
E OF'PERMIT It1:
T IS TRUE AN
ACCURATE
OR AUTHORIZED -AGE
9-3
06-0071-WI-0238
TANK FARM REMEDIAL SYSTEM
Septic Tank/Drain Field
Subsurface Low -Pressure
—Piping (LPP)
dvD)-6
' 1 iFi j r S a ?) Os 1.-.9 rISLI I \i.,/ r`
rAuiei 31 1ui93
GRO4INIMA i ER SECTION
RALCIGI-I: NG

APP43
***************************
COMPLIANCE MONITORING
REPORT
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number INJ. SUPPLY Well Depth 179.00 Ft.
Well Diameter 6" Sample (Screened) Interval N/A Ft. to N/A Ft.
Depth to Water Level N/A ft. below meas. pt.(before sampling) or N/A MSL
Measuring Point is 1.00 feet above land surface or N/A ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
PERMIT NO.: 06-0071-WO-0005
Non -Discharge TANK FARM REMEDIAL SYSTEM
NPDES
_Lagoon
_Spray Field ---Piping (LPP)
Land Appl of Sludge
Rotary Distributor x Other
_Septic Tank/Drain Field
Subsurface Low -Pressure
Field Analysis: pH
7.2 Specific Conductance 750 uMhos Temp 19.5 oC Odor NONE Appearance CLEAR
Date Sample Collected 04/26/93
Date Lab Sample Analyzed 4/26-5/17 1993
Laboratory Name
TEXASGULF INC. Certification No. 330
COD N/A mg/1
NO2 as N
N/A mg/l
Ni - Nickel N/A mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/1
Pb - Lead N/A mg/l
Coliform: MF Total <1 /100m1
Dissolved Solids: Total 532 mg/1
Phosphorus: Total as P
Al - Aluminum
0.062 mg/l
N/A mg/l
Zn - Zinc N/A mg/l
Pesticides/Heribicides (Specify)
pH (when analyzed) 7.1 units
Ba - Barium N/A mg/l
ug/l
TOC 3.92 mg/l
Ca - Calcium N/A mg/l
ug/l
Chloride 89.3 mg/l
Cd - Cadmium N/A mg/l
ug/l
Arsenic N/A mg/l
Chromium: Total
N/A mg/l
Other FLUORIDE 0.45 mg/1
Grease and Oils N/A mg/l
Cu - Copper N/A mg/l
ug/l
Hardness: Total N/A mg/l
Fe - Iron
Phenol N/A mg/1
N/A mg/1
ug/l
Hg - Mercury N/A mg/l
ug/t
Sulfate 0.9 mg/1
K - Potassium N/A mg/l
ug/l
Specific Conductance N/A uMohs
Mg - Magnesium N/A mg/1
ug/t
Total Ammonia(NH4 + NH3) N/A mg/l
Mn - Manganese
N/A mg/l
TKN as N N/A mg/l
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
1 CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
aiz` b' /��.��,
SUR�OF PtRMITTEE (OR AUFHII
ZED -Kali
g•/3•`q`1

13 1 ti50I3
COMPLIANCE MONITORING
REPORT
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number MWTF1-C Well Depth 41.20 Ft.
Well Diameter 2" Sample (Screened) Interval 38.70 Ft. to 40.7 Ft.
Depth to Water Level 2.63 ft. below meas. pt.(before sampling) or 7.86 MSL
Measuring Point is 0.00 feet above land surface or 10.49 ft. (MSL)
Gallons of water pumped/bailed before sampling 36.00
PERMIT NO.: 06-0071-WI-0238
Non -Discharge TANK FARM REMEDIAL SYSTEM
NPDES
_Lagoon _Septic Tank/Drain Field
_ Spray Field Subsurface Low -Pr
—Piping (LPP)
_Land Appl of Sludge
_Rotary Distributor x_0ther
Field Analysis: pH
7.0 Specific Conductance 750 uMhos Temp 21.0 oC Odor NONE Appearance CLEAR
Date Sample Collected 04/26/93
Date Lab Sample Analyzed 4/26-5/17 1993
Laboratory Name TEXASGULF INC.
Certification No. 330
COD N/A mg/l
Coliform: MF Fecal N/A /100ml
Coliform: MF Total <1 /100m1
NO2 as N
NO3 as N
ntaC
alaidinalliegilifttlitionedieSoastwow
Al - Aluminum
pH (when analyzed) 7 units
TOC 3.09 mg/1
Arsenic N/A mg/l
Grease and Oils N/A mg/l
Ba - Barium
Ca - Calcium
Cu - Copper N/A mg/l
Hardness: Total N/A mg/L
Phenol N/A mg/l
Hg - Mercury N/A mg/1
Sulfate 1.5 mg/l
Specific Conductance N/A uMohs
Total Ammonia(NH4 f NH3) N/A mg/1
TKN as N N/A mg/1
K - Potassium
Mg - Magnesium
- Sodium
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
7 �l/f n
y / , ✓� .GGiLyGLGu i(
31GNA1UHt OF P1:kMiTTEE (OR AUTHORIZED /,CENT)
{1 6 t& -
Ni - Nickel
N/A mg/l
Pb - Lead N/A mg/l
Zn - Zinc N/A mg/l
Pesticides/Heribicides (Specify)
ug/l
ug/1
ug/l
Other FLUORIDE 0.42 mg/l
ug/l
ug/l
ug/l
ug/l
ug/l
Note:
Values should reflect total
concentrations.
OK
NEW crv--A.
5.- /1-94.
T).
GDs nu
4_
Cd i (r1 Mco

COMPLIANCE MONITORING
REPORT
93146028
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number CIW-7 Well Depth 48.00 Ft.
Well Diameter
4" Sample (Screened) Interval 31.00 Ft. to 45.25 Ft.
Depth to Water Level N/A ft. below meas. pt.(before sampling) or N/A MSL
Measuring Point is 3.33 feet above land surface or 13.13 ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
aillmosemspilliammatemppecific Conductance
PERMIT NO.: 06-0071-WO-0005 C /
Non -Discharge TANK FARM REMEDIft Cap C r
NPDES
_Lagoon Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Appt of Sludge
_Rotary Distributor x Other
725 uMhos Temp 22.0 oC Odor NONE Appearance CLEAR
Date Sample Collected 04/26/93 Date Lab Sample Analyzed 4/26-5/17 1993
Laboratory Name
TEXASGULF INC. Certification No. 330
COD
N/A mg/l
NO2 as N
N/A mg/1
Coliform: MF Fecal
N/A /100m1
NO3 as N
N/A mg/l
Coliform: MF Total
<1 /100m1
Phosphorus: Total as P
0.046 mg/l
Al - Aluminum N/A mg/L
pH (when analyzed)
7.0 units
Be - Barium N/A mg/l
Ni - Nickel N/A mg/1
Pb - Lead N/A mg/L
Zn - Zinc N/A mg/t
Pesticides/Heribicides (Specify)
TOC
C
Arsenic
Grease and Oils
3.41 mg/l
N/A mg/L
N/A mg/l
Ca - Calcium N/A mg/L
ice; t Oicl mg t
ug/l
ug/l
ug/l
Ahroniva: 7ota4; r ,;O Ob r{'
Cu - Copper N/A mg/L
Other FLUORIDE 0.55 mg/L
Hardness: Total
N/A mg/l
Fe - Iron
N/A mg/l
Phenol
N/A mg/l
Hg - Mercury N/A mg/L
Sulfate
0.7 mg/l
K - Potassium
N/A mg/l
Specific Conductance N/A uMohs
Mg - Magnesium
N/A mg/l
Total Ammonia(NH4 + NH3) N/A mg/l
Mn - Manganese
0.05 mg/l
TKN as N N/A mg/1
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
ug/l
ug/L
ug/l
ug/l
ug/t
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
i RM T (/� . D AGENT
$1 ITAi NIiM TEL (UR UTHORILEITAGENx,
T]
U/(
CnA4A, .
X. )-/p..A.-yvt-ev‘. S. ((.'i

7 L )V.\I tAi11
TA ►J 13
***************************
COMPLIANCE MONITORING
REPORT
***************************
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number INJ. SUPPLY Well Depth 179.00 Ft.
Well Diameter 6" Sample (Screened) interval N/A Ft. to N/A Ft.
Depth to Water Level N/A ft. below meas. pt.(before sampling) or N/A MSL
Measuring Point is 1.00 feet above land surface or N/A ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.9 Specific Conductance 780 uMhos Temp 18.0 oC Odor
Date Sample Collected 01/07/93 Date Lab Sample Analyzed 1/7-1/27 1993
TEXASGULF INC. Certification No. 330
Laboratory Name
PERMIT NO.: 06-0071-W0-0005
Non -Discharge TANK FARM REMEDIAL SYSTEM
NPDES
Lagoon
Spray Field
Land Appl of Sludge
Septic Tank/Drain Field
Subsurface Low -Pressure
Piping (LPP)
Rotary Distributor _x_Other
NONE Appearance CLEAR
COD N/A mg/1
Coliform: MF Fecal N/A /100m1
NO2 as N
NO3 as N
N/A mg/1
N/A mg/l
Ni - Nickel N/A mg/l
Pb - Lead N/A mg/l
Coliform: MF Total <1 /100m1
Dissolved Solids: Total 520 mg/1
Phosphorus: Total as P
0.036 mg/l
Zn - Zinc N/A mg/1
Al - Aluminum
N/A mg/l
Pesticides/Heribicides (Specify)
pH (when analyzed) 7.1 units
TOC 3.90 mg/l
Chloride 88.1 mg/t
Arsenic N/A mg/l
Ba - Barium N/A mg/1
ug/t
Grease and Oils N/A mg/l
Ca - Calcium N/A mg/l
Cd - Cadmium <0.010 mg/l
Chromium: Total
<0.020 mg/1
Cu - Copper N/A mg/l
ug/l
ug/t
Other FLUORIDE 0.60 mg/l
ug/l
Hardness: Total N/A mg/l
Fe - Iron
N/A mg/1
ug/l
Phenol N/A mg/l
Hg - Mercury N/A mg/l
ug/l
Sulfate 0.5 mg/l
K - Potassium N/A mg/l
ug/l
Specific Conductance N/A uMohs
Total Anmonia(NH4 + NH3) N/A mg/l
TKN as N N/A mg/1
Mg - Magnesium N/A mg/l
ug/1
Mn - Manganese
<0.010 mg/l
Na - Sodium
I CERTIFY THA. THIS REPORT IS TRUE AND ACCURATE
u'ty/tf(Af
SIGNAL ORE Of PERMITTEE (O AUTHORIZED AGENT) uNIE
N/A mg/l
Note:
Values should reflect total
concentrations.
t

:OMPLIANCE MONITORING
1EPORT
11**************************
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: 06-0071-WI-0238
Well Location Tank Farm Non -Discharge TANK FARM REMEDIAL SYSTEM
Well I.D. Number MWTF1-C Well Depth 41.20 Ft. NPDES
Well Diameter 2" _ Sample (Screened) Interval 38.70 Ft. to 40.7 Ft. --- Lagoon Septic Tank/Drain Field
Depth to Water Level 5.48 ft. below meas. pt.(before sampling) or 5.01 MSL Spray Field Subsurface Low -Pressure
Piping (LPP)
MeasUMflg Point is 0.00 feet above land surface or 10.49 ft. (MSL) _Land Appl of Sludge
Gallons of water pumped/bailed before sampling 33.00bu
ROtery Distritor 7x=pther
Field Analysis: pH 6.9 Specific Conductance 750 uMhos Temp 20.0 oC Odor NONE Appearance CLEAR
_____________________
Date Sample Collected 01/12/93 Date Lab Sample Analyzed 1/12-1/27 1993
Laboratory Name TEXASGULF INC. Certification No. 330
COO NO2 as N N/A N/A mg/l. mg/l Ni - Nickel N/A mg/1
_______________
Coliform: MF Fecal N/A /100ml NO3 as N N/A mg/l Pb - Lead _ __ _ N/A mg/l
Coliform: MF Total >120 /100ml Phosporus: Total as P 0.231 mg/l Zn - Zinc N/A mg/l
Dissolved Solids: Total 535 mg/l Al - Aluminum N/A mg/l Pesticides/Heribicides (Specify)
pH (when analyzed) 6.8 units Ba - Barium N/A mg/l ug/l
______________________________
TOC 3.52 mg/1 Ca - Calcium N/A mg/I ug/1
_____________________________
Chloride 82.1 mg/I Cd - Cadmium BDL mg/l ug/l
______________________________________
Arsenic N/A mg/1 Chromium: Total BDL mg/l Other FLUORIDE 0.38 mg/l
Grease and Oils N/A mg/l Cu - Copper N/A mg/l ug/1
_____________ ___________________________
Hardness: Total N/A mg/l Fe - Iron N/A mg/1 ug/l
no
_____________________________
Phel N/A mg/1 Hg - Mercury N/A mg/1 ug/1
__________________________________
_______________________________
77: 9.14. ____ K
- 777 _____ NIA. _____ ____________________ 711.
Specific Conductance N/A uMohs Mg - Magnesium 0.1 mg/l ug/l
Total Ammonia(NH4 + NH3) N/A mg/l Mn - Manganese N/A mg/l Note:
Values should reflect total
_____
TKN as N N/A mg/l Na - Sodium N/A mg/1 concentrations.
Note: TOC analysis bias due to suspected propanol contamination. EPA cleaning method used.
1 CERTIFY T AT 'THIS REPORT IS TRUE AND ACCURATE
//

***************************
COMPLIANCE MONITORING
REPORT
***************************
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well 1.D. Number CIW-7 Well Depth 48.00 Ft.
Well Diameter 4" Sample (Screened) Interval 31.00 Ft. to 45.25 Ft.
Depth to Water Level N/A ft. below meas. pt.(before sampling) or N/A MSL
Measuring Point is 3.33 feet above land surface or 13.13 ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS 16.5 oC Odor NONE
Field Analysis- pH 6.7 Specific Conductance 750 uMhos Temp
Date Lab Sample Analyzed 1/7-1/27 1993
Date Sample Collected 01/07/93
TEXASGULF INC. Certification No. 330
PERMIT NO.: 06-0071-WO-0005
Non -Discharge TANK FARM REMEDIAL SYSTEM
NPDES
_Lagoon Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
—Piping (LPP)
Land Appl of Sludge
Rotary Distributor _x Other
Appearance CLEAR
Laboratory Name
COD
N/A mg/1
Coliform: MF Fecal N/A /100m1
Coliform: MF Total >120 /100m1
Dissolved Solids: Total 520 mg/L
NO2 as N
NO3 as N
N/A mg/1
N/A mg/l
Phosphorus: Total as P* 0.079 mg/l
N/A mg/l
Al - Aluminum
Ni - Nickel N/A mg/1
Pb - Lead N/A mg/L
Zn - Zinc N/A mg/1
Pesticides/Heribicides (Specify)
pH (when analyzed) 6.9 units
TOC
N/A mg/I
Chloride 87.1 mg/t
Arsenic N/A mg/l
Grease and Oils N/A mg/1
Hardness: Total N/A mg/l
Phenol
Sulfate
N/A mg/l
0.5 mg/1
Specific Conductance N/A uMohs
Total Ammonia(NH4 + N113) N/A mg/1
N/A mg/l
TKN as N
Ba - Barium N/A mg/l
Ca - Calcium N/A mg/1
Cd - Cadmium BDL mg/l
Chromium: Total
ug/l
ug/l
6.02 mg/1
Cu - Copper N/A mg/l
Fe - Iron N/A mg/l
Hg - Mercury N/A mg/l
K - Potassium N/A mg/1
Mg - Magnesium N/A mg/l
BDL mg/l
Mn - Manganese
ug/l
Other FLUORIDE 0.60 mg/l
ug/l
ug/l
ug/l
ug/l
Na - Sodium
ug/l
N/A mg/l
Note:
Values should reflect total
concentrations.
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE

6cT.q Z
COMPLIANCE MONITORING
REPORT
***************************
***AMENDED (TOTAL P)***
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number INJ. SUPPLY Well Depth 179.00 Ft.
Well Diameter
6" Sample (Screened) Interval N/A Ft. to N/A Ft.
Depth to Water Level N/A ft. below meas. pt.(before sampling) or N/A MSL
Measuring Point is 1.00 feet above land surface or N/A ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
PERMIT NO.:
Non -Discharge
NPDES
_Lagoon
_Spray Field
Land Appl of Sludge
Rotary Distributor
06-0071-Wo-0005
TANK FARM REMEDIAL SYSTEM
_Septic Tank/Drain Field
Subsurface Low -Pressure
—Piping (LPP)
x_Other
Field Analysis: pH 6.9 Specific Conductance 700 uMhos Temp 19.0 oC Odor NONE
Appearance CLEAR
Date Sample Collected 10/29/92 Date Lab Sample Analyzed 10/29-11/11 1992
Laboratory Name
TEXASGULF INC. Certification No. 330
COD N/A mg/1
NO2 as N N/A mg/1
Ni - Nickel
N/A mg/l
Coliform: MF Fecal N/A /100ml
NO3 as N N/A mg/l
Pb - Lead
N/A mg/l
Coliform: MF Total N/A /100ml
Phosphorus: Total as P* 0.017 mg/l
Zn - Zinc
N/A mg/l
Dissolved Solids: Total 540 mg/1
Al - Aluminum N/A mg/l
Pesticides/Heribicides (Specify)
pH (when analyzed) 7.0 units
Ba - Barium N/A mg/1
ug/l
TOC 6 mg/l
Ca - Calcium N/A mg/l
ug/l
Chloride 77.7 mg/l
Cd - Cadmium N/A mg/l
ug/l
Arsenic N/A mg/l
Chromium: Total N/A mg/l
Other FLUORIDE
0.58 mg/l
Grease and Oils N/A mg/l
Cu - Copper N/A mg/l
ug/l
Hardness: Total N/A mg/l
Fe - Iron N/A mg/l
ug/l
Phenol N/A mg/l
Hg - Mercury N/A mg/l
ug/l
Sulfate 1.1 mg/l
K - Potassium N/A mg/t
ug/l
Specific Conductance N/A uMohs
Mg - Magnesium N/A mg/l
ug/l
Total Ammonia(NH4 + NH3) N/A mg/l
Mn - Manganese
N/A mg/l
TKN as N N/A mg/l
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
siGNATURE OF NtRMA
IHURIItD A NT) DATE
* Resampled 11/30/92 and
analyzed 12/02/92.
iO

COMPLIANCE MONITORING
REPORT
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number MWTF1-C Well Depth 41.20 Ft.
Well Diameter
2" Sample (Screened) Interval 38.70 Ft. to 40.7 Ft.
Depth to Water Level 3.56 ft. below meas. pt.(before sampling) or 6.93 MSL
Measuring Point is 0.00 feet above land surface or 10.49 ft. (MSL)
Gallons of water pumped/bailed before sampling 38.75
PERMIT NO.: 06-0071-WI-0238
Non -Discharge TANK FARM REMEDIAL SYSTEM
NPDES
Lagoon
_Spray Field
_Land Appl of Sludge
_Rotary Distributor x_Other
_Septic Tank/Drain Field
Subsurface Low -Pressure
Piping (LPP)
Field Analysis: pH
6.7 Specific Conductance 700 uMhos Temp 20.5 oC Odor NONE Appearance VRY LT CLDY WHT
Date Sample Collected 10/29/92 Date lab Sample Analyzed 10/29-11/24 1992
Laboratory Name TEXASGULF INC. Certification No. 330
COD N/A mg/1
NO2 as N
N/A mg/l
Ni - Nickel N/A mg/t
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/l
Pb - Lead N/A mg/1
Con form: MF Total BDL /100mt
Phosphorus: Total as P 0.196 mg/l
Zn - Zinc N/A mg/1
Dissolved Solids: Total 490 mg/l
Al - Aluminum
N/A mg/1
Pesticides/Heribicides (Specify)
pH (when analyzed) 6.6 units
Ba - Barium N/A mg/1
ug/t
TOC 4 mg/l
Ca - Calcium N/A mg/1
ug/t
Chloride 66.1 mg/l
Arsenic N/A mg/1
Cd - Cadmium BDL mg/t
ug/l
Chromium: Total
BDL mg/t
Other FLUORIDE 0.350 mg/1
Grease and Oils N/A mg/l
Cu - Copper N/A mg/l
ug/l
Hardness: Total N/A mg/1
Fe - Iron
N/A mg/1
ug/l
Phenol N/A mg/L
Hg - Mercury N/A mg/1
Sulfate 9.6 mg/l
K - Potassium N/A mg/1
uI/t
ug/l
Specific Conductance N/A UMohs
Mg - Magnesium 0.01 mg/l
ug/l
Total Ammonia(NH4 + NH3) N/A mg/l
Mn - Manganese
N/A mg/1
TKN as N N/A mg/1
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
Note: TOC analysis bias due to suspected propanal contamination. EPA cleaning method used.
1 CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIG Al U���F PERMlTiEE (uK
9z

COMPLIANCE MONITORING
REPORT
15411)111
***AMENDED (TOTAL P)***
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well 1.D. Number CIW-7
Well Depth 48.00 Ft.
Well Diameter
4"
Sample (Screened) Interval 31.00 Ft. to 45.25 Ft.
Depth to Water Level N/A
ft. below meas. pt.(before sampling) or N/A MSL
Measuring Point is
3.33 feet above land surface or 13.13 ft. (MSL)
Gallons of water pumped/bailed before sampling
CONTINUOUS
PERMIT NO.:
Non -Discharge
NPDES
_Lagoon
_Spray Field
_Land Appl of Sludge
Rotary Distributor
06-0071-WO-0005
TANK FARM REMEDIAL SYSTEM
_Septic Tank/Drain Field
Subsurface Low -Pressure
---Piping (LPP)
_x_other
Field Analysis: pH
6.9 Specific Conductance 700 uMhos Temp 20.5 oC Odor NONE
Appearance CLEAR
Date Sample Collected 10/29/92
Date Lab Sample Analyzed 10/29-11/24 1992
Laboratory Name TEXASGULF INC.
Certification No. 330
COD
N/A mg/1
NO2 as N
N/A mg/L
Ni - Nickel
N/A mg/1
Coliform: MF Fecal
N/A /100ml
NO3 as N
N/A mg/l
Pb - Lead
N/A mg/l
Coliform: MF Total
BDL /100m1
Phosphorus: Total as P* 0.127 mg/l
Zn - Zinc
N/A mg/l
Dissolved Solids: Total
500 mg/l
Al - Aluminum
N/A mg/L
Pesticides/Heribicides (Specify)
pH (when analyzed)
TOC
7.1 units
Ba - Barium
N/A mg/t
ug/l
5 mg/l
Ca - Calcium
N/A mg/1
ug/l
Chloride
78.9 mg/1
Cd - Cadmium
BDL mg/1
ug/l
Arsenic
N/A mg/l
Chromium: Total
BDL mg/1
Other FLUORIDE
0.58 mg/I.
Grease and Oils
N/A mg/l
Cu - Copper
N/A mg/1
ug/l
Hardness: Total
N/A mg/l
Fe - Iron
N/A mg/l
ug/l
Phenol
N/A mg/l
Hg - Mercury
N/A mg/l
ug/l
Sulfate
0.0 mg/1
K - Potassium
N/A mg/1
ug/l
Specific Conductance
N/A uMohs
Mg - Magnesium
N/A mg/1
ug/l
Total Ammonia(NH4 + NH3)
N/A mg/1
Mn - Manganese
0.01 mg/l
TKN as N
N/A mg/l
Na - Sodium
N/A mg/1
Note:
Values should reflect total
concentrations.
I CERTIFY THAT THIS REP RT,IS TRUE AND ACCURATE
1GNATURE OF PMMIFIE (ii0R AUTHORIZED GENT)
DATE
* Resampled 11/30/92 and
analyzed 12/02/92.

T11L
qz_
********************** *****
COMPLIANCE MONITORING
REPORT
************* *********** ***
Facility Name TEXASGULF INC PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: N/A
Welt Location lank Farm Non -Discharge TANK FARM REMEDIAL SYSTEM
-------------------------------------------------------------------------------------------
Well 1.0. Number MWTF1-C Well Depth 41.20 Ft. NPDES
Well Diameter 2" Sample (Screenin
---Lagoon Septic Tank/Draed) Interval 38.70 Ft. to 40.7 Ft. Field
---
Depth _ to _ Water Level 10:74 ft. _ below _ meas. _ pt:(tefore sampling) or :0:25 _ pr
MSL Say Field
___ Subsurface Low -Pressure
Piping (LPP)
Measuring Point is 0 00 feet above land surface or 10.49 ft. (MSL) Land Appl of Sludge
Gallons of water pumped/bailed before sampling 21.50 _Rotary Distributor x Other
___________________
Field Analysis: pH 6.5 Specific Conductance 775 uMhos Temp 20.5 oC Odor NONE _ Appearance CLER
Date Sample Collected 07/15/92 Date Lab Sample Analyzed 07/15-07/23 1992
Laboratory _ Name TEXASGULF INC: Certification No. 330
_____________________________________________
COO iN/A mg/1 NO2 as N N/A mg/ l Ni - N_ ickel N/A mg/1
_________
Coliform: MF Fecal N/A /100ml NO3 as N N/A mg/l Pb - Lead N/A mg/1
_ .., ___________________
Coliform: MF Total 4,N/A /100ml Phosphorus: Total as P ___ 0.259 mg/1 Zn - Zinc N/A mg/l
Dissolved Solids: Total 540 mg/1 Al - Aluminum N/A mg/l Pesticides/Herides (Specify)
pH (when analyzed) 4/7.1 units _ Ba - Barium
______ NIA _ 7/t
N/A /1 ____________________________
ug/1
TOC vf 2 -mgil _ Ca _ = _ -Ca-l-ciuni mg ug/1
__________ r __________________________________
Chloride %./ 52.1 mg/l Cd - Cadmium 1 N/A mg/1 ug/1
_____________________________ _,.. ____________
Arsenic __________ N/Amg/1 Chromium: Total __ I ___ N/A _ mg/l __ Other FLUORIDE
___________________
,./ 0.300 mg/1
GreaSe and Oils N/A mg/l Cu - Copper N/A mg/l ug/1
___________________________________
A
Hardness: Total N/A mg/l Fe - Iron ug/1
_______ 111/_ _ 7/.1
Phenol N/A mg/l Hg - Mercury N/A mg/l ug/1
_______________________ -..... IIII _______________________________________________________________
N/A mg/l
Sulfate -mg/l K - Potassium N/A mg/l ug/1
Specific Conductance N/A uMohs Mg - Magnesium . ug/1
__ _ ;lip, _ .m.g.ii _______________________________
Values should reflect total
Total Ammonia(NH4 + NH3) N/A mg/l Mn - Manganese Note:
TKN as 14 N/A mg/1 Na - Sodium N/A mg/1 concentrations.
Note: TOC analysis bias due to suspected ACCURATE
___41041=It''
Cluzd2-4 -
91'a
lg -ILI

rtiq 2
***************************
COMPLIANCE MONITORING
REPORT
***************************
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806 PERMIT NO.: N/A
Well Location Tank Farm Non -Discharge TANK FARM REMEDIAL SYSTEM
Well I.D. Number MWTF1-C Well Depth 41.20 Ft. NPDES
Well Diameter 2" Sample (Screened) Interval 38.70 Ft. to 40.7 Ft. Water Use
Depth to Water Level 9.48 ft. below meas. pt.(before sampling) or 1.01 MSL Injection Well
Measuring Point is 0.00 feet above land surface or 10.49 ft. (MSL) Well Construction
Gallons of water pumped/bailed before sampling 35.00 Other
Field Analysis: pH 6.8 Specific Conductance 790 uMhos Temp 20.0 oC Odor NONE Appearance CLEAR
Date Sample Collected 04/22/92 Date Lab Sample Analyzed 04/22-04/28 1992
Laboratory Name TEXASGULF INC. Certification No. 330
COD N/A mg/l
NO2 as N
N/A mg/l
Ni - Nickel N/A mg/l
Coliform: MF Fecal N/A /100ml
NO3 as N
N/A mg/l
Pb - Lead N/A mg/l
Coliform: MF Total N/A /100m1
Dissolved Solids: Total 560 mg/l
Phosphorus: Total as P 0.289 mg/l
Zn - Zinc N/A mg/1
Al - Aluminum
N/A mg/l
Pesticides/Heribicides (Specify)
pH (when analyzed) 7 units
TOC 3 mg/l
Ba - Barium N/A mg/t
ug/l
Ca - Calcium N/A mg/l
ug/l
Chloride 49.5 mg/l
Arsenic N/A mg/l
Cd - Cadmium N/A mg/l
ug/l
Chromium: Total
N/A mg/l
Other FLUORIDE 0.312 mg/l
Grease and Oils N/A mg/l
Cu - Copper N/A mg/l
ug/l
Hardness: Total N/A mg/l
Fe - Iron
N/A mg/l
ug/l
Phenol N/A mg/l
Hg - Mercury N/A mg/1
ug/l
Sulfate 61.8 mg/t
K - Potassium N/A mg/l
ug/l
Specific Conductance N/A uMohs
Mg - Magnesium N/A mg/l
Total Ammonia(NH4 + NH3) N/A mg/l
Mn - Manganese
ug/l
N/A mg/l
TKN as N N/A mg/l
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
Note:CERIFaTHAT
OTC ntyisHbias REPORT
tsuspected
ted ACCURATE contamination. EPA cleaning method used.
SIGNATU E OF PERMITTEEj OR A[9HORIZED AGEN1)
it .Q. I s• r3 q o

.T4,0 RZ.
COMPLIANCE MONITORING
REPORT
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number
MWTF1-C Well Depth 41.20 Ft.
Well Diameter
2" Sample (Screened) interval 38.70 Ft. to 40.7 Ft.
Depth to Water Level 10.20 ft. below meas. pt.(before sampling) or 0.29 MSL
Measuring Point is 0.00 feet above land surface or 10.49 ft. (MSL)
Gallons of water pupped/bailed before sampling 30.00
PERMIT NO.:
Non -Discharge W00001105
NPDES
Water Use
Injection Well
Well Construction
Other
Field Analysis: pH
6.7 Specific Conductance 790 uMhos Temp 19.0 oC Odor NONE
Appearance CLEAR
Date Sample Collected 01/07/92 Date Lab Sample Analyzed 01/07-01/15 1991
Laboratory Name TEXASGULF INC.
Certification No. 330
COD N/A mg/l
NO2 as N
N/A mg/1
Ni - Nickel N/A mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/l
Pb - Lead N/A mg/l
Coliform: MF Total N/A /100m1
Phosphorus: Total as P
0.284 mg/1
Zn - Zinc N/A mg/1
Dissolved Solids: Total 594 mg/l
Al - Aluminum
N/A mg/l
Pesticides/Heribicides (Specify)
pH (when analyzed) 7.4 units
Ba - Barium N/A mg/1
ug/l
TOC 5 mg/t
Ca - Calcium N/A mg/l
ug/l
Chloride 52.1 mg/l
Cd - Cadmium N/A mg/t
ug/l
Arsenic N/A mg/l
Chromium: Total
N/A mg/l
Other FLUORIDE 0.301 mg/1
Grease and Oils N/A ng/l
Cu - Copper N/A mg/l
ug/l
Hardness: Total N/A mg/t
Fe - Iron
N/A mg/1
Phenol N/A mg/l
Hg - Mercury N/A mg/l
ug/t
ug/l
Sulfate 68.0 mg/l
Specific Conductance N/A uMohs
Total Ammonia(NH4 + NH3) N/A mg/l
K - Potassium N/A mg/1
Mg - Magnesium N/A mg/l
Mn - Manganese
N/A mg/l
TKN as N N/A mg/l
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
Note:
CEROC IFanatysisHbias
ISsEdueTue tISsuspecteed d ACropanol CURATE contamination. EPA cleaning method used.
16N7CIURE Ui• PERMTTTEE (UR AUTHORIZED AGENT)
DATE
ug/l
ug/l
•
t •, '
CA•II

**************************
COMPLIANCE MONITORING
REPORT
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well 1.D. Number MWTF1-C Well Depth 41.20 Ft.
Well Diameter 2" Sample (Screened) Interval 38.70 Ft. to 40.7 Ft.
Depth to Water Level 12.52 ft. below meas. pt.(before sampling) or -2.03 MSL
Measuring Point is 0.00 feet above land surface or 10.49 ft. (MSL)
Gallons of water pumped/bailed before sampling 27.00
PERMIT NO.:
Non -Discharge W00001105
NPDES
Water Use
Injection Well
Well Construction
Other
Field Analysis: pH
6.8 Specific Conductance 710 uMhos Temp 20.5 oC Odor NONE Appearance CLEAR
Date Sample Collected 10/02/91 Date Lab Sample Analyzed 10/02-10/30 1991
Laboratory Name
TEXASGULF INC. Certification No. 330
COD
N/A mg/l
NO2 as N
N/A mg/t
Ni - Nickel N/A mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/l
Pb - Lead N/A mg/l
Coliform: MF Total N/A /100m1
Phosphorus: Total as P
0.321 mg/1
Zn - Zinc N/A mg/l
Dissolved Solids: Total 586 mg/1
Al - Aluminum
N/A mg/1
Pesticides/Heribicides (Specify)
pH (when analyzed) 7.5 units
TOC
5 mg/t
Ba - Barium N/A mg/1
ug/l
Ca - Calcium N/A mg/l
ug/t
Chloride 53 mg/l
Arsenic N/A mg/l
Cd - Cadmium N/A mg/1
Chromium: Total
N/A mg/1
ug/l
Other FLUORIDE 0.369 mg/1
Grease and Oils N/A mg/l
Cu - Copper N/A mg/1
ug/l
Hardness: Total N/A mg/l
Fe - Iron
N/A mg/l
ug/t
Phenol
N/A mg/1
Hg - Mercury N/A mg/l
ug/l
Sulfate 71.35 mg/l
K - Potassium N/A mg/l
ug/l
Specific Conductance N/A uMohs
Total Ammonia(NH4 + NH3) N/A mg/1
Mg - Magnesium N/A mg/1
ug/l
Mn - Manganese
N/A mg/t
TKN as N N/A mg/l
Na - Sodium
N/A mg/1
Note:
Values should reflect total
concentrations.
Note: TOC analysis bias due to suspected propanol contamination. EPA cleaning method used.
1 CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
i
tt'4" %// //,' / -'6
7✓
SIGNATURE F PERMITTEE (OR I IIORIZED AGENT) DATE

COMPLIANCE MONITORING
REPORT
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
PERMIT NO.:
Non -Discharge W00001105
Well I.D. Number 41.20 Ft. NPOES
Well Diameter 2" Sample (Screened) Interval 38.70 Ft. to 40.7 Ft. Water Use
Depth to Water Level 11.68 ft. below meas. pt.(before sampling) or -1.19 MSL Injection Well
Measuring Point is 0.00 feet above land surface or 10.49 ft. (MSL) Well Construction
Gallons of water pumped/baited before sampling 27.75 Other
Field Analysis: pH 6.8 Specific Conductance 725 uMhos Temp 20.0 oC Odor NONE Appearance CLEAR
MWTF1-C Well Depth
Date Sample Collected 07/19/91
Date Lab Sample Analyzed 07/19-08/01 1991
Laboratory Name TEXASGULF INC.
Certification No. 330
COD
N/A mg/l
Coliform: MF Fecal N/A /100ml
NO2 as N
NO3 as N
N/A mg/l
N/A mg/1
Ni - Nickel N/A mg/1
Pb - Lead N/A mg/t
Coliform: MF Total N/A /100m1
Dissolved Solids: Total 606 mg/l
Phosphorus:: Total as P
0.296 mg/l
Zn - Zinc N/A mg/l
Al - Aluminum
N/A mg/l
Pesticides/Heribicides (Specify)
pH (when analyzed) 6.7 units
TOC
Chloride
Arsenic
5 mg/l
60.4 mg/t
Ba - Barium N/A mg/l
ug/l
N/A mg/l
Ca - Calcium N/A mg/l
Cd - Cadmium N/A mg/l
Chromium: Total
N/A mg/1
ug/l
ug/l
Other FLUORIDE 0.469 mg/l
Grease and Oils N/A mg/l
Cu - Copper N/A mg/l
ug/l
Hardness: Total N/A mg/l
Phenol
N/A mg/l
Fe - Iron
N/A mg/l
ug/l
Hg - Mercury N/A mg/l
ug/t
Sulfate
69.7 mg/l
K - Potassium N/A mg/t
ug/l
Specific Conductance N/A uMohs
Total Amnnonia(NH4 + NH3) N/A mg/l
Mg - Magnesium 'N/A mg/1
ug/l
Mn - Manganese
N/A mg/t
TKN as M
N/A mg/l
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
Note: TOC analysis bias due to suspected propanol contamination. EPA cleaning method used.
I CERTIFY THA THIS REPORT IS TRUE AND ACCURATE
A/A�1
SIGNAII)RE OF ERMITrEEd(OR AUrHORIZED AG4)

APR•R1
,..*************************
COMPLIANCE MONITORING
REPORT
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Welt I.D. Number
MWTF1-C Well Depth 41.20 Ft.
Well Diameter
211
Sample (Screened) interval 38.70 Ft. to 40.7 Ft.
Depth to Water Level, 10.00 ft. below meas. pt.(before sampling) or 0.49 MSL
Measuring Point is 0.00 feet above land surface or 10.49 ft. (MSL)
Gallons of water pumped/bailed before sampling 19.75
PERMIT NO.:
Non -Discharge W00001105
NPDES
Water Use
Injection Well
Well Construction
Other
Field Analysis: pH
6.6 Specific Conductance 725 uMhos Temp 19 oC Odor NONE Appearance CLEAR
Date Sample Collected 04/21/91 Date Lab Sample Analyzed 04/21-05/07 1991
Laboratory Name
TEXASGULF INC. Certification No. 330
COD
N/A mg/1
NO2 as N
N/A mg/l
Ni - Nickel N/A mg/t
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/1
Pb - Lead N/A mg/1
Coliform: MF Total N/A /100m1
Phosphorus: Total as P
0.279 mg/1
Zn - Zinc N/A mg/l
Dissolved Solids: Total 540 mg/l
Al - Aluminum
N/A mg/t
Pesticides/Heribicides (Specify)
pH (when analyzed) 7.3 units
Ba - Barium N/A mg/l
ug/l
TOC
3.45 mg/l
Ca - Calcium N/A mg/1
ug/l
Chloride
59.1 mg/l
Cd - Cadmium N/A mg/l
ug/t
Arsenic
N/A mg/t
Chromium: Total
N/A mg/l
Other FLUORIDE 0.252 mg/1
Grease and Oils N/A mg/l
Cu - Copper N/A mg/t
ug/l
Hardness: Total N/A mg/l
Fe - Iron
N/A mg/l
ug/l
Phenol
N/A mg/1
Hg - Mercury N/A mg/l
ug/l
Sulfate
65.8 mg/l
K - Potassium N/A mg/l
ug/t
Specific Conductance N/A uMohs
Total Ammonia(NH4 + NH3) N/A mg/1
Mg - Magnesium , N/A mg/1
ug/t
Mn - Manganese
N/A mg/l
TKN as N
N/A mg/t
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
Note: TOC analysis bias due to suspected propanol contamination. EPA cleaning method used.
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
31GNAIU
C �✓t�.
NM 11EE (UR
IZED AGENT)
44;70__
4.X s•/3-44

***********************
..OMPLIANCE MONITORING
REPORT
***************************
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number MWTF1-C Well Depth 41.20 Ft.
Well Diameter
2" Sample (Screened) Intervc.l 38.70 Ft. to 40.7 Ft.
Depth to Water Level 9.93 ft. below meas. pt.(befor sampling) or 0.56 MSL
Measuring Point is 0.00 feet above land surface cr 10.49 ft. (MSL)
Gallons of water pumped/bailed before sampling 15.00
PERMIT NO.:
Non -Discharge W00001105
NPDES
Water Use
Injection Well
Well Construction
Other
Field Analysis: pH
6.9 Specific Conductance 800 uMhos Temp 19 oC Odor NONE Appearance CLEAR
Date Sample Collected 01/09/91
Date Lab Sample Analyzed 01/09-01/22 1991
Laboratory Name
TEXASGULF INC. Certification No. NONE
COD N/A mg/l
NO2 as N
N/A mg/l
Ni - Nickel N/A mg/l
Coliform: MF Fecal N/A /100ml
NO3 as N
N/A mg/t
Pb - Lead N/A mg/l
Coliform: MF Totat N/A /100m1
Phosphorus: Total as P 0.262 mg/t
Zn - Zinc N/A mg/l
Dissolved Solids: Total 532 mg/t
Al - Aluminum
N/A mg/t
Pesticides/Heribicides (Specify)
pH (when analyzed) 7.3 units
Ba - Barium N/A mg/l
ug/l
TOC 4 mg/t
Ca - Calcium N/A mg/t
ug/l
Chloride 59.9 mg/t
Cd - Cadmium N/A mg/l
ug/l
Arsenic N/A mg/1
Chromium: Total
N/A mg/l
Other FLUORIDE 0.343 mg/l
Grease and Oils N/A mg/l
Cu - Copper N/A mg/l
Hardness: Total N/A mg/l
Phenol N/A mg/l
Sulfate 66.9 mg/1
Specific Conductance N/A uMohs
Fe - Iron N/A mg/l
Hg - Mercury N/A mg/t
K - Potassium N/A mg/t
Mg - Magnesium N/A mg/t
ug/l
ug/l
ug/l
ug/l
ug/t
Total Ammonia(NH4 + NH3) N/A mg/l
Mn - Manganese
N/A mg/l
TKN as N N/A mg/1
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
Note:
CETOIFanatysisHs biaTISsEdueTs due tISsuspected Ated Cropanol CURATE contamination. EPA cleaning method used.
I6NAIURE OF PERMITIEE (OR AUTHORIZED AGENT) DATE
/'C 4. 2I. S • /3.9`i

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��POKPHOSPHATE «vsnxT^ms County nsxoFom
Facility wo�T*xxsuuLF INC- _______
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pnuox4Dxonmm_wn_z/uvv
_��___�---------------------------
Address ____ ___________
-------------
/unx Farm -----------
Well Location -____
--'-----------Well »*Pt» n'zo m-----------------------------------
Well
� »' wwo�� nmFI'c ------------u� �O'7o m' �v *n'7 m' -__
-------'---------no�`�� (Screened) �r�rr»-------
,, ____----'-'-'----Rind)__~
measuring PO t.(before
Date Sample
NONE
-- --
--�-----------------'---
,"
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-' ------------- N/A mu/L \«i�w,cxwl -_______���_��_-
_�--/l
--^---. w*»
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'---o'.-�-----'--�--�--' "a, —Fecal -�-_'\.\\\'���-'-�-�-. ~. p V'3`Z1~ mg/
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�m4iform: "F Total, -�----'-----'\------
ioonl,=u_m~'`uy*�'"` ----------'-�
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COMPLIANCEMONITORIN
G
--�---
-
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om --�-'------
w/x/loomt\wn�oow -����___�---
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'cm(~=»~-----------c«'ou�c`«m___---_--
^----s -mn/
'\\\`'---'--'�' __w/a~.m--o~~/
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Tvc --'---'------n6'Cmmm��--______----
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--�----55'5 ��yi'�------'-_"`'^.11
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'----
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--'----w/* nm/t\nr ----------------------------
A
m/I
--
-
-
-
--
-
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,
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-
Chloride '----'\'--- � /
--------chrmu.�n�«
'
'------ N/A ng/l ...........^ a/L
mrow»i^ ��------'----w/» --~»/iCuu 'cvp�' --------_�
xa,dn�ao: Tctol --_--'-�____`___-,,/
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phenol ------\-ooimm --___C�
'---'---70'6 my/I o 'rota-------- _" ~'po
Sulfate --------°.""~"imn '-'�-
'--------'--'-- N/A U�oo|"y _���_��_--______
Specific cv~m�run:° �'___-_____.,~��
---'���'�-�-� Mn'��m���-----'--'���'�
-_-'-��w/« mg/ _- /c
Total ^«m»»imcwx^ - °"--'�-'���''��'�w���
_--'--- Sodium -_--�-'
-- -
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-----___. '~�� ,u suspect cro Q=E
Note* rnc m»m�S`, " is Txu `^
I CERTIFY Tp^T `"^" Rs'm-T
'
NO.;
Non -Discharge wo0001105
Use
-
Pb ' Lead '-_--_--___-__
---'----u/« mg/l
-------------
------------------
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other
------------------------------
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os reflectVa�ues should total:���t,����---__------'
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COMPLIANCE MONITORING
REPORT
Facility Name TEXASGULF INC. PHOSPHATE OPERATIONS County BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
Well Location Tank Farm
Well I.D. Number MWTF1-C Well Depth 41.20 Ft.
Well Diameter
2" Sample (Screened) Interval 38.70 Ft. to 40.7 Ft.
Depth to Water Level 11.48 ft. below measuring point.(before sampling)
Measuring Point is 0.00 feet above land surface.
Gallons of water pumped/bailed before sampling 20.00
Field Analysis: pH
PERMIT NO.:
Non -Discharge W0000110
NPDES �� .1 5 0 0 3
Water Use
Injection Well
Well Construction
Other
6.8 Specific Conductanc, 775 uMhos Temp 19 oC Odor NONE Appearance CLEAR
Date Sample Collected 04/18/90 Date Lab Sample Analyzed 04/18-04/23 1990
Laboratory Name
TEXASGULF INC. Certification No. NONE
COD N/A mg/l
NO2 as N
N/A mg/l
Ni - Nickel N/A mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/t
Pb - Lead N/A mg/l
Cotiform: MF Total N/A /100ml
Phosphorus: Total as P 0.298 mg/1
Zn - Zinc N/A mg/l
Dissolved Solids: Total 560 mg/l
Al - Aluminum
N/A mg/l
Pesticides/Heribicides (Specify)
pH (when analyzed) 7.4 units
Ba - Barium N/A mg/l
ug/l
TOC 4 mg/l
Ca - Calcium N/A mg/l
ug/l
Chloride 54.5 mg/l
Cd - Col'i w►-- N/A mg/l
ug/l
Arsenic N/A mg/l
Chromium: Total
N/A mg/l
Other FLUORIDE 0.604 mg/l
Grease and Oils N/A mg/l
Cu - Copper N/A mg/1
ug/l
Hardness: Total N/A mg/l
Fe - Iron
N/A mg/1
ug/l
Phenol N/A mg/l
Hg - Mercury N/A mg/l
ug/l
Sulfate
76.7 mg/t
K - Potassium N/A mg/l
ug/t
Specific Conductance N/A uMohs
Mg - Magnesium N/A mg/l
ug/l
Total Ammonia(NH4 + NH3) N/A mg/1
Mn - Manganese
N/A mg/1
TKN as N
N/A mg/l
Na - Sodium
N/A mg/l
Note:
Values should reflect total
concentrations.
1 CERTIFY, THAT THIS REPORT IS TRUE AND ACCURATE
Al( C(.'/ T L
ST6UATURE OF PERMIIIEE (OR THDRILED AGENT-)
j47-,r1-572
x4,/
S•/3• 1y

COMPLIANCE MONITORING
REPORT FORM
Facility Name
Address
Well Location
/ L-7 9iLL / -ZNc -
O . , - 9/8
/Arv/c ,C9/2/4/
62,4j, A%•C. 2 7
Well Identification Number /-1Gf1Tf=/-G
For additi,
Well Depth '// ZG Ft
Well Diameter 2/' Sample (Screened) Interval 3g?o Ft.
To 6f/ 2''Ft.
Depth to Water Level /lni •9 Z- ft below measuring point. (before sampling)
Measuring point is G' feet above land surface
Gallons of water pumped/bailed before sampling
/6,0
Field Analysis: pH 7 U Specific Conductance /7'9G
Date Sample Collected /O- Z5 - 39
Laboratory Name / (-=7?S2LG4f //4)c.
COD /1//n
Coliform: MF Fecal /0/4
Coliform: MF Total
Dissolved Solids: Total y�
pH (when analyzed) 7'/
TOC
Chloride
Arsenic
Grease and Oils
Hardness: Total
Phenol
Sulfate
Specific Conductance / /4
Total Ammonia(NH3 t NH 4) y/4
TKN as N /1)//9-
ll:
ocr
Division of Environmental Management
Groundwater Section
P.O. Box 27687
Raleigh, N.C. 2761 1
(91 )733-3221
County id:),471-e-fa2T'
Permit Number:
Non -Discharge
NPDES
893460E44
Water Use
Injection Well
Well Construction
Gther X1 C-i l&& /: L. /2c722)/J f.p,t)
uMhos Temp. 24" o C Odor 4 '" Appearance M/
Date Lab Sample Analyzed /0-27 -Z) 8j
Certification No. tiO ICJ
mg/I NO2 as N /0/9' mg/I
/100ml NO3 as N 42/73 mg/I
/100m1 Phosphorus: Total as P d 6/5mg/I
mg/I Al - Aluminum /!///i mg/I
units Ba - Barium /U/g mg/I
mg/I Ca - Calcium /2/// mg/I
535 mg/I Cd - Cadmium N/ mg/I
N//9- mg/I Chromium: Total /P/ft mg/I
/f//4 mg/I Cu - Copper /'�%//f mg/1
/1-)//4-- mg/I Fe - Iron /U/n mg/i
2)/4- mg/1 Hg - Mercury 41/4 mg/I
S7 z mg/1 K - Potassium /14,9 mg/1
uMhos Mg - Magnesium ' / mg/I
mg/I Mn - Manganese NM- mg/I
mg/I Na - Sodium /U/n mg/I
I CERTIFY THAT THIS REPORT IS TRUE
c444'114-7'
AND ACCURATE.
Ni - Nickel
Pb - Lead
Zn - Zinc
4/4
mg/1
mg/I
mg/1
Pesticides/Herbicides (Specify Compounds)
ug/1
ug/1
ug/I
Other (Specify) ug/I
tack / fit /-f rrglt—
ug/1
•
vg/I
Note:
�fr
1 tag c1 C
Values shoul< VOAbt
`mug/I
ug/I
•
tteoft-af ons3 t.(
* See back for instructions.
SIGNATURE OF PERMITTEE (OR AUT RIZED AGENT*) DATE
GW-59 Revised 6/88 '✓
* * Submit blue and green copies only to address above.

Tut. r
COMPLIANCE MONITORING
REPORT FORM
For additional forms please write or call:
Facility Name /6XJ"/S-9'e1L/�7 c_ - // /)/')7c 0/9e 'ziTi4 V-
Address t-C • &/
Well Location /Ai✓i- r/22r/
Well Identification Number N'l'TF /`G Well Depth
Well Diameter Z Sample (Screened) Interval 39.70 Ft.
Depth to Water Level /Z. 83
rf/ Z C Ft
To S"/Z0 Ft.
ft below measuring point. (before sampling)
Measuring point is feet above land surface
Gallons of water pumped/bailed before sampling /6% 5
Field Analysis: pH 9 Specific Conductance 85-O
Date Sample Collected
Laboratory Name
COD /1///i
Coliform: MF Fecal /11/n
Coliform: MF Total A)/R'
Dissolved Solids: Total
pH (when analyzed) 7./
TOC SZ
Chloride 53
Arsenic 4)//r
5'z e
Division of Environmental Management
Groundwater Section
P.O. Sox 27687
Raleigh, N.C. 27611
[phone]
County / ,'9Ze /0/CT
Permit Number: 89 3 If 6 Q 3 3
Non -Discharge
NPDES
Water Use
Injection Well
Well Construction
Other v`.'c d%/)G ,4 Z2 :'% /42 ,' j
uMhos Temp. 2/ o C Odor '/V44ic
Date Lab Sample Analyzed 7—/37/Vieet ,!"zo--55-
mg/I NO2 as N
/ 100m1 NO3 as N //in
/100m1 Phosphorus: Total as
mg/1 Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/1 Cd - Cadmium
mg/I Chromium: Total
mg/I Cu Copper
mg/I Fe - Iron
mg/1
mg/I
uMhos Mg - Magnesium
mg/1 Mn - Manganese
mg/I Na - Sodium
Grease and Oils
Hardness: Total
Phenol
Sulfate
%/A
Specific Conductance
/t)//)-
Sg. 3
Total Ammonia(NH3 t NH
TKN as N
4 ] N/q
N//J-
Certification No.
4,1,9.4.1
Appearance C2•69/
/l//4' mg/I Ni - Nickel 4/1/9- mg/I
mg/I Pb - Lead /tV4 mg/I
P C•C'Z.S77,� mg/I Zn - Zinc /1/� mg/I
tir/4 �C mg/I Pesticides/Herbicides (Specify Compounds)
/L/g mg/I ug/I
ug/I
ug/I
Other (Specify) ug/I
/Zoe/dam - Z e A./9/z, ug tt---,—
ug/I
N//} mg/I
/n mg/1
/1'/4 mg/I
////1 mg/I
Hg - Mercury
K - Potassium
I CERTIFY THAT THIS R PORT IS TRUE AND ACCURATE.
SIGNATURE OF PERMITTEE (OR
HORIZED AGENT*)
%///). mg/I
4t/n. mg/I
//°/mg/I
DATE
I** Submit blue and green copies only to address above.
Note � �•' 1'-�"
mg/I �
l a d e s
;..
shout reflect totalr�ertions
S13 `�
-' w`p/I
ug/I
•
* See back for instructions.
'�� 4•

COMPLIANCE MONITORING
REPORT FORM
For additional forms please write or call:
Facility Name �L�i Sy/GL Sc — A/fos2/i/aTe- C�nrx.?/1�s
Address /? �. 6.1/ 5/6 4c/2oi&j A C. 27 ,f
Well Location 7 N/ . //,?iy
Well Identification Number /1Ii) / = /-C Well Depth `//• ZC Ft.
Well Diameter 2.. Sample (Screened) Interval 38 '• Z'Ft. To 5/17.70 Ft.
Depth to Water Level // -3 ft below measuring point. (before sampling)
Measuring point is 0 feet above land surface
Gallons of water pumped/bailed before s‘impling
Division or tnvironmental Management
Groundwater Section
P.O. Box 27687
Raleigh, N.C. 27611
[phone]
County 15c79/G{c<?7-
Permit Number:
Non -Discharge
NPDES
89? 14 6020
Water Use
Injection Well
Well Construction.
A
Other !-f%'&C./// /,/i1n1
FieldAnalysis: pH 72 Specific Conductance PeC uMhos Temp. /9• D ° C Odor /11o4)C7- Appearance
Date Sample Collected 4/-/v-A4 Date Lab Sample Analyzed '`/-/e-d5 i,y/2,e- «-oe -0 j
Laboratory Name /c-x'/S9,, J- ,Z..t-c. Certification No. /LP/VC-
COD N/4 mg/I
Coliform: MF Fecal 4//A / 100ni1
Coliform: MF Total N//f /100m1
Dissolved Solids: Total 54, mg/I
pH (when analyzed) 6 •0 units
TOC 3 mg/I
Chloride -U. mg/1
Arsenic ti//9 mg/I
Grease and Oils /L%ff mg/I
Hardness: Total h/f% nig/1
Phenol /12//9" rng/I
Sulfate 50' 4. AuC mg/I
Specific Conductance /1//4 uMhos
Total Ammonia(NH3 t NH 4) /1//i4 mg/l
mg/1
TKN as N N/%�
NO2 as N
NO3 as N
Phosphorus: Total as
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd - Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K - Potassium
Mg - Magnesium
Mn - Manganese
Na - Sodium
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
/z4 -72��
SIGNATURE OF PERMITTEE (OR AUTHO
GW-59 Revised 6/88
N//)
N/4
mg/I Ni - Nickel /1)//7L mg/I
mg/I Pb - Lead /L'//} mg/I
P ©,/3/ mg/I Zn - Zinc /l'/%f mg/I
N//1J mg/I Pesticides/Herbicides (Specify Compounds)
N//9 mg/I ug/I
N//4 mg/I ug/I
ug/I
ug/1
N//9 mg/I
/U//1 mg/I
N//7 mg/I
N//L mg/I
/)//i- mg/I
mg/I
/v///
N/%f
D AGENT*) DATE
mg/I
mg/I
Other (Specify)
`/c cif/ -/e G, 2 17 ,4 -
l,r
u /I
Note: 5 (3. l/
Values should retl ,cfclC)]9%tl F irOwq'Yilrzations
11. :�
I* See back for instructions.
* * Submit blue and green copies only to address above.

COMPLIANCE MONITORING
REPORT FORM
Facility Name
Address
For additional forms please write or call:
/Lx4 9 /[f ivc• I )Y 7J4 TC li�4-7',<'�TS
Well Location /t`/N/c /Nr/y
Well Identification Number /U%GG'Tf= /-C
Well Depth
Well Diameter Z '' Sample (Screened) Interval 38.70 Ft.
// 2v
F t.
To 4/0-7C Ft.
Depth to Water Level /`1 6, ft below measuring point. (before sampling)
Measuring point is 0 feet above land surface
Gallons of water pumped/bailed before sampling /.5.
Division of Environmental Management
Groundwater Section
P.O. Sox 27687
Raleigh, N.C. 27611
[phone]
County .0c,9/ric,e7-
Permit Number:
Non -Discharge 89 3 !} 5 0 3 0
NPDES
Water Use
Injection Well
Well Construction
Other ' /c-o''//6 ,9cT/o,ti 7126,,/1,.
Field Analysis: pH 6.E Specific Conductance eex) uMhos Temp. /9.5 °C
Date Sample Collected / - 30-8 9 Date Lab Sample Analyzed 3 '/- 8`/
Laboratory Name /LXrr59u1 f ✓c -
COD /v//4 mg/I
Coliform: MF Fecal /'M /100m1
Conform: MF Total N//} /100m1
Dissolved Solids: Total 5JV mg/I
pH (when analyzed) '' 7 units
TOC oO mg/I
Chloride .74' mg/I
Arsenic N/// mg/I
Grease and Oils ti//4 mg/I
Hardness: Total 4//1 mg/I
Phenol /Li/-) mg/I
Sulfate G 9Z mg/I
Specific Conductance /1,//» uMhos
Total Ammorria(NH3 t NH 4) 4//7 mg/I
TKN as N AM' mg/I
Odor A-101)C Appearance (cc-/M_
r/ky--,`i
Certification No.
NO2 as N /7// mg/I Ni - Nickel
NO') as N /.,/4 mg/I Pb - Lead
Phosphorus: Total as P 0•149 mg/I Zn - Zinc
Al - Aluminum mg/I
Ba - Barium /i'1/ mg/I
N///
mg/I
mg/I
mg/I
Pesticides/Herbicides (Specify Compounds)
ug/1
Ca - Calcium /1%//i1 mg/1 ug/I
Cd - Cadmium '/7' mg/I ug/I
Chromium: Total /L0/0- mg/I Other (Specify) ug/I
Cu Copper N//i mg/I /Lien//&c%- 9 / /'f,'/'/
Fe - Iron /p//il mg/I ug/I
Hg - Mercury ///-1 mg/I ug/f, •
K - Potassium /t'// mg/I .:fig/I
Mg - Magnesium N//3 mg/I '':g/I
Mn - Manganese_ /1'//1 mg/I
Na - Sodium 47/g" mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
/ A
Note:
Values should
76 .
:'' 1.vi
reflect io''tal conc''g.rr`ii ions
—Z•/3•
c1�t'r,~
* See back for instructions.
SIGNATURE OF PERMITTEE/QOR AUTHORIZED AGENTit) DATE
GW-59 Revised 6/88
* * Submit blue and green copies only to address above.