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HomeMy WebLinkAboutWQ0004972_Monitoring - 05-2021_20210630Monitoring Report Submittal ............................................................................................................................................ Permit Number #* WQ0004972 Name of Facility:* Month:* May Report Information Forest Lakes Preserve ELS Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter:* Signature: Date of submittal: Initial Review Year:* 2021 Upload Document* Forest Lake_May.pdf 1.68MB FDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-t, NDAR-2, NDMLR, GW-59). Jessica. Mize@pacelabs.com Jessica Mize jus l oil Reviewer: Saunders, Erickson G 6/30/2021 This will be filled in automatically Is the project number correct? * WQ0004972 Is the monitoring report r Yes r No accepted?* Regional Office * Winston-Salem Accepted Date: 7/7/2021 Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W 0004972 MONTH: Mav YEAR: 2021 FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie Flow Monitoring Point: Effluent: El Influent: Parameter Monitoring Point: Effluent: W Influent: I Surface Water SW SW Code/Name: LJ Was There Effluent Flow for this Month Generated At This Facility: Yes: No: Operator 50050 00400 50060 00310 1 00610 00530 31616 00665 00625 00630 00600 00620 70300 00949 D Arrival Daily Rate Fecal A Time Operator ORC (Flow}Into C.1iforin Total Total T 2400 Time W on Treatment Residual BOP-5 (Geometric Taal I:jcldhal Total Nitrate Dissolved @ Clock Site Site? System Pit CMoriae 20C NH-3-N TSS Mean`) P1ms Nitrogen NO2+NO3 Nitrogen NO3-N Solids Chlotidc I1RS Y1N GPD NITS G:L AIG'L MG,L 71 Q I -I I I 00ILIL h11i M&L Iv110i MG!L h1G'L M&L h1G,L Continuous +Y .ant y unt v a,t y on[ ont y oni _. ont e Monthly y ortv . f .,yd, 1 9.999 9,999 3 1140 0.50 Y 9.999 6.50 <10 4 0755 0.25 S' 8.066 6.40 <10 s 1159 0.5U Y 7,952 6.541 <10 <2.0 82.5 C3.0 2421) 12.5 66.7 0.11 66.8 0.86 6 1141 0.25 Y 7,981 6.311 <10 7 0911 0.25 Y 7,888 1 6.10 <10 $ 8,173 9 8,173 10 0918 (1.25 13 8.173 5,911 <10 It 1030 050 Y 7,434 5.90 <10 12 1232 0.25 Y 10,997 5.80 <10 13 0808 0.25 Y 19,651 5.90 <10 14 0826 0.25 1' 18,038 6.00 <10 ` 10,261 16 10,261 17 0947 0.25 Y 10,261 6.10 <to 1R 1353 li 1 9,876 6,00 <10 19 1100 0.25 N' 9,041 1 6.10 <10 20 1312 0.511 1S 9,094 6.10 <t0 21 0944 0.25 It 8,633 6.01) <10 22 10,333 2,3 10,333 24 I O18 0.25 1 10,333 6.00 <10 25 1352 0.25 5 8.055 5.90 <10 261 1216 1 0.50 1' 7.873 5.90 <10 Z71 0730 050 Y 7.111 6.00 <10 28 1010 0.25 B 7,657 6.40 <10 29 9.442 .to 9,442 �1 H 9.442 6.30 --to Average 9.676 <10 <-• <.Il 24241 I_'.� 6t,J 11.11 66.3 4.B6 Daily Maximum 19,651 6.50 <10 .0 2420 12.n 4,6.7 II.I 1 66,4 I1.86 Daily Minimum 7,111 5.80 <10 <2.0 82.5 <3.0 242U 12.5 66.7 11.11 hh.8 I1l,86 Monthly Limits (s) 244UU Composite D 1 Grab (G) Operator in Responsible Charge (ORC); CTenn Price Genic II Phone; 336-996-2841 Check Box if ORC Has Changed 11 ORC Certification Number: 987931/20771 Certified Laboratories (1): Pace Analytical Serivees (2): PersOn(s) Collecting Samples: Glenn Price l Mail ORIGINAL and Two COPIES to; \. ATTN-. Non -Discharge Compliance Unit X DENR (SIGNATtiRE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best or my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Co�(Y,N ) 1. Does all monitoring data and sampling frequencies meet permit requirements? ``TT If the facility is non-comp-Hant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." -3cp - (Signature of Permitee)* Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza Suite 800 Chicago, Il 60606 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivi 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel - Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31/21 (Permit Exp. Date) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W009 PAN Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 idity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. * If signed by other than the Perrnittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W 004972 MONTH: May YEAR: 2021 FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie Formulas: Daily Leading (inches) = (Volume Applied (gallons) x 0.1336 (cubic feellgallon) x 12 (incheadoot)] I (Area Sprayed (acres) x 43,660 (square feetlacre) or = (Volume Applied (gallons) I (Area Sprayed (acres) x 27,152 (gallons)ecre-inch). Maximum Hourly Loading (inches) = Daily Loading (inches) I (rime imgated (minutes)) 60 (minutes/hour)) Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of this months Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = (Monthly Loading (lncneslmonth)I Number of days in the month (dayslmonth )] x 7 (days/weak) n, Irrigation Occur oE • • IMMM11. "MEN •. Occur On - D. Inig9tion Occur On ■ ■ Permitted Hourly Rate CinchesF Rate (�nches) MEN '!Feather Coda: C-elrar, PC -partly cloudy, Ci-cloudy. R-rain, S"new, SWIM Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931120771 Check Box if ORC Has Changed: Mail ORIGINAL and Two COPIES to: C ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quafity By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Farm NDAR-9 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) I. The application rate(s) did not exceed the limit(s) specified in the permit. 4 Z Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit.` 4. All buffer zones as specified in the permit were maintained during each application. C� S. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for s mitting false information, including the possibility of fines and imprisonment for knowing violations." 3 v a Baron Neal McDuffie (Signature Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N. Riverside Plaza. Suite 800 Chicago. Il 60606 (Permittee Address) Field Services Director (Pace Analytical Services) (Position or Title) 3/31 /2021 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). aceAnalytrcal www.pacelabs.com May 17, 2021 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lakes Pace Project No.: 92536950 Dear Tracy Overdurf: Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Enclosed are the analytical results for sample(s) received by the laboratory on May 05, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures �Q PCCR�r�. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in V1, without the written consent of Pace Analytical Services, LLC. Page 1 of 16 aceAnalytical " www.pacelabs.com Project: Forest Lakes Pace Project No.: 92536950 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977.0981 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in foil, without the written consent of Pace Analytical Services, LLC. Page 2 of 16 1�5a'neAnaljftal oaarva.pacelabs.com f SAMPLE ANALYTE COUNT Project: Forest Lakes Pace Project No.: 92536950 Pace Analytical Services, LLC 1377 South Park Drive Kemersvitle, NC 27284 (704)977-0981 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92536950001 Effluent SM 254OD-2011 LRB 1 PASI-E EPA 353.2 Rev 2.0 1993 AMI 1 PASI-E SM 521OB-2011 MWF 1 PASI-E Colilert-18 MLS1 1 PASI-E TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 350.1 Rev 2.0 1993 NGP 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 NGP 1 PASI-A EPA 365.1 Rev 2.0 1993 KDF1 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 aceAnalj6cal t www.pacelabs.com ANALYTICAL RESULTS Project: Forest Lakes Pace Project No.: 92536950 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 aampie: tTriuent Lab ID: 92536950001 Collected: 05/05/21 12:03 Received: 05/05/21 14:14 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Eden Total Suspended Solids ND mg/L 3.0 1 05/06/21 09:17 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 0.86 mg/L 0.040 1 05/O6/21 16:21 14797-55-8 5210E BOD, 5 day EDN Analytical Method: SM 521 OB-2011 Preparation Method: SM 5210B-2011 Pace Analytical Services - Eden BOD, 5 day ND mg/L 2.0 1 05/06/21 15:12 05/11/21 10:48 132 Colilert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-16 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100mL 1.0 1 05/05/21 18:11 05/06/21 12:37 1g,El Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 66.8 mg/L 0.52 1 05/14/21 16:52 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 82.5 mg/L 1.0 10 05/14/2112:47 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 66.7 mg/L 2.5 5 05111/21 22:02 05/13/21 05:03 7727-37-9 353.2 Nitrogen, NO2JN03 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 0.11 mg/L 0.040 1 05/13/21 12:49 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 12.5 mg/L 0.25 5 05/13/21 18:32 05/1412112:32 7723-14-0 Date: 05/17/2021 03:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 4 of 16 aceAnalytical www.pacelaDs.ecm { QUALITY CONTROL DATA Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Forest Lakes Pace Project No.: 92536950 QC Batch: 618636 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92536950001 METHOD BLANK: 3254811 Matrix: Water Associated Lab Samples: 92536950001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 05/06/21 09:09 LABORATORY CONTROL SAMPLE: 3254812 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 236 94 90-110 SAMPLE DUPLICATE: 3254813 92536941001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 13.0 14.0 7 SAMPLE DUPLICATE: 3254814 92537022001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 252 238 6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/17/2021 03:13 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16 QD acmnalytical www.pacelabs.com 1 I QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92536950 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977.0981 QC Batch: 618679 Analysis Method: EPA 353.2 Rev 2.01993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92536950001 METHOD BLANK: 3255098 Matrix: Water Associated Lab Samples: 92536950001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 05/06/21 16:18 LABORATORY CONTROL SAMPLE: 3255099 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3255100 3255101 MS MSD 92536950001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 0.86 1.5 1.5 2.4 2.4 103 99 90-110 3 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/17/2021 03.13 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16 aceAnalytical www.pacolabs.com QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92536950 Pace Analytical Services, LLC 1377 South Park Drive Kemersvilie, NC 27284 (704)977-0981 QC Batch: 618742 Analysis Method: SM 521OB-2011 QC Batch Method: SM 521 OB-2011 Analysis Description: 521013 BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92536950001 METHOD BLANK: 3255537 Matrix: Water Associated Lab Samples: 92536950001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 05/11/21 10:12 LABORATORY CONTROL SAMPLE: 3255538 Spike LCS LCS % Rec Parameter Units Conc. Result % Rao Limits Qualifiers BOD, 5 day mg/L 198 206 104 84.6-116.4 SAMPLE DUPLICATE: 3255540 92537248002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 97.5 97.5 0 R6 Results presented on this page are In the units indicated by the'Untis' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/17/2021 03:13 PM without the written consent of Pace Analytical Services, I.I.C. Page 7 of 16 /�5a'vce Ana/Xicai� tnmr.pacelabseam t t QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92536950 %At, maicn: bldb40 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN Associated Lab Samples: 92536950001 laboratory: Pace Analytical Services - Eden SAMPLE DUPLICATE: 3254820 92536950001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms MPN/100mL 2420 2420 0 19,El Pace Analytical Services, LLC 1377 South Park Drive Kemersviile, NC 27284 (704)977-0981 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/17/2021 03:13 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16 aceft ytical 1 www.pacelabo.com QUALITY CONTROL DATA Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Forest Lakes Pace Project No.: 92536950 QC Batch: 620337 Analysis Method: EPA 350.1 Rev 2.01993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated lab Samples: 92536950001 METHOD BLANK: 3263877 Matrix: Water Associated Lab Samples: 92536950001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 05/14/21 11:51 LABORATORY CONTROL SAMPLE: 3263878 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.0 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3263879 3263880 MS MSD 92538146002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 4.9 4.9 98 97 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3263881 3263882 MS MSD 92538146003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 4.9 4.9 98 98 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05117/2021 03:13 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16 10001111 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92536950 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 619667 Analysis Method: EPA 351.2 Rev 2.0 1993 OC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92536950001 METHOD BLANK: 3259941 Matrix: Water Associated Lab Samples: 92536950001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 05/13/21 02:53 LABORATORY CONTROL SAMPLE: 3259942 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.4 94 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3259943 3259944 MS MSD 92537483004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 52.6 10 10 56.2 59.9 36 74 90-110 7 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3259945 3259946 MS MSD 92537483005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L NO 10 10 11.6 9.9 115 98 90-110 15 M1,R1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Date: 05/17/2021 03:13 PM without the written consent of Pace Analytical Services, I.I.C. Page 10 of 16 1�5a'ceAnalj6cal www.pacelabs.eom QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92536950 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 620117 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.01993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92536950001 METHOD BLANK: 3262556 Matrix: Water Associated Lab Samples: 92536950001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L NO 0.040 05/13/21 12:25 LABORATORY CONTROL SAMPLE: 3262557 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3262558 3262559 MS MSD 92537597005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 1.2 2.5 2.5 3.7 3.6 99 97 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3262560 3262561 MS MSD 92537611001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.61 2.5 2.5 2.8 2.8 68 88 90-110 0 M1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/1712021 03:13 PM without the written consent of Pace Analytical Services, I.L.C. Page 11 of 16 aceAnalytical www.pacelala.eom I QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92536950 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 620175 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92536950001 METHOD BLANK: 3262793 Matrix: Water Associated Lab Samples: 92536950001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 05/1412112:25 LABORATORY CONTROL SAMPLE: 3262794 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3262795 3262796 MS MSD 92536748001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Phosphorus mg/L 12.9 2.5 2.5 15.4 15.4 100 103 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3262797 3262798 MS MSD 92536750001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 7.0 2.5 2.5 9.6 9.4 103 94 90-110 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the resulL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/17/2021 03:13 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16 aceaAnalytical r f www.pacolabs.com t i i QUALIFIERS Project: Forest Lakes Pace Project No.: 92536950 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS 1g >2419.6 B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated for the dilution using the most amount of sample. El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. R6 The RPD between valid sample dilutions exceeded 30%. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/17/2021 03:13 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 16 ace Analyticall www.pacelabs.ccm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lakes Pace Project No.: 92536950 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92536960001 Effluent SM 254OD-2011 618636 92536950001 Effluent EPA 353.2 Rev 2.0 1993 618679 92536950001 Effluent SM 521 OB-2011 618742 SM 521OB-2011 618874 92536950001 Effluent Coiilert-18 618640 Colilert-18 618641 92536950001 Effluent TKN+NO3+NO2 620670 Calculation 92536960001 Effluent EPA 350.1 Rev 2.0 1993 620337 92536950001 Effluent EPA 351.2 Rev 2.0 1993 619667 EPA 351.2 Rev 2.0 1993 620086 92536950001 Effluent EPA 353.2 Rev 2.0 1993 620117 92536950001 Effluent EPA 365.1 Rev 2.0 1993 620175 EPA 365.1 Rev 2.0 1993 620454 Date: 05/17/2021 03:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 16 CHAIN -OF -CUSTODY Analytical Request LAB USE ONLY- Affix Workord,-^-s - aeA,a,>�»l i WO# 9253C950 Chain -of -Custody is a LEGAL DOCUMENT •Complete all retevent fields 0 ALL SHADEC II I III_IIIiI I m Company: Forest Lakes Billing Information:e- .I , Container Preservative Type ` 92569$0 ' Address: u 2 8 " Preservative Types: (1) nitric add, (2) sulfuric acid, (3) hydrochloric acid, (4► sodium hydroxide, (5) zinc acetate, ReportTo: Email To: (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (8) ammonium sulfate, (C) ammonium hydroxide. (D) TSP, (U) Unpreserved, (o) other Copy To: Site Collection Info/Address: Analyses lLab Profile Line: Customer Project Name/Number: State: County/City: Time Zone Collected: Lab Sample Receipt Checklist: J t JPTJ JMTI JCT I JET Custody Beals Present/Intacf14A Custody Signatures PresentEmail: Phone: Site/Facility ID b: Compliance Monitoring? (/Yes ( ]No Collector Signature PresentBottles Intact Correct Bottles Collected B (p 'nt): Purchase Order 4: DW PWS ID 4: Quote a: DW Location Code: Z Sufficient volume Samples Received cn Ice Y N NA VOA - Headepace Acceptable Y A Collected By (signature) Turnaround Date Required: immediately Packed on Ice: _ t )Yes [ ]No CL USDA Regulated Soils Y rA ` Samples in Holding Time Yam. NA Residual Chlorine cFs W NA Sample Disposal: Rush: Field Filtered (if applicable): ( J Dispose as appropriate I J Return ( ] Same Day I J Next Day ( ) Yes [ ]No Cl Stripe r I J Archive: I J 2 Day I) 3 Day ( J 4 Day I 15 Day o H Sample pH Acce t�i N NA ( J Hold: lExpedite Charges Apply) Analysis: Z Cl)' pit Stripe: t Sulfide PresentY HA Lead Acetate Strips: • Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) O f Z LAB USE ONLY: Lab Sample H ( Comments: Comp/ Collected (or Composite End Res kof Customer Sample ID Matrix Grab Composite Start) CI Ctns p ro to m IZ IU. D le Time Dale Time Effluent WW Customer Remarks J Sperial Conditions / Possible Hazards Type of Ice Used: Wet Blue Dry None SHORT HOLDS PRESENT (<72 hours): Y N N/A Lab Sample Temperature Info: Packing Material Used: Lab Tracking #: Temp Blank ReceivedL Y N NA Therm 1011; Cooler l Temp Upon eceipt:2—.Loc Radchem sample(s) screened (<500 cpm): Y N NA Samples received via: Cooler 1 Therm Corr. Factor: --Q--oC FEDEX UPS Client Courier Pace Courier Cooler 1 Corrected Temp:oC Relinquished by/Company. Signature) D im Received by omp ny: ( ign ur Date/Time: MTJL LAB USE ONLY Comments: Table it: Acctnum. Relinquished by/Company: (Signature) Date/Time: Received by/Company: [Signature) Date/Time: t Tri f Blank Received: Y N NA Template: Prelogin• HCL McOH TSP Other Relinquished by/Company: (Signature) �Date/Time: Received by/Company: (Signature) Date/Time: PM: l Non Conformance(s): Page: PB: ____ YES / NO___ of: �_ i7 i:..L e"S, t.., r.,`�t f .r rY.e ♦CeN.IJ\V:1) � I'3_��ll1i L C In ,. _ . t _ `•�r�•G•C3, a•r.Q7 - h 'c.^.ter n!I ..3:1]rt IS Frc:'�- •z `: I ve--Hie a1v L':l;h t t ,? c�]�2^:3i C@ ra^�? for i_ i r samp!e5. "D:)"Or^ h3", C'I LCx i] tL Nist ills';'•-.r p{ bottjas In t^, } �IIIIII it �IIIIIIII� llllllll\i II_iIill�i pN Adjustment Loa for Pr ;ampid 10 Tyre of Preservative ( pH upon recei t p d e D atz preserv,,tion adjusted i t?: �i,i2 r?',?r I't8'? IS 3 d�sCra^a^c' a°'ar•: J ... ,. c n C served Samples Time preservation Amount of Preservative adjusted added Lot" rd ..r C,r'-:.,..Jrre ;ar._ Ci?�. a t of hcld, irc,3ceC. ,rra ? �, ser:3' . opt ar te^ p, ,otorrec: tcr.ta nzr, ' t err C3r.!ir. CCer:rf:c�:.on Ofr,ca ; A Page 16 of 16