WQ0019960_More Information (Received)_20210618

Legend
Propery Line
Field Boundary
Perennial Stream
Surface Water
® Unused Area
Dairy Dr.
o Well
House
Field F1
9.9 acres
y � v
Buffers
Property Line (50')
Perennial Stream (33')
House (400')
Well (100')
he Compli Tance Boundary is established either 250 feet from the perimeter of the residuals application area or 50 feet within
1 the property boundary. whichever is closer. The Review Boundary is established midway between the Compliance foundary
and the perimeter of the residuals application area.
Fisher, John Buffer Map
Parcels: 1658004330035, 165800433035, 165800525658
McDowell County, NC 0 375 750
t _I_ 1 t f I 1
135.5936.-81.8462 _ . North Carolina Stateplane, NAD83
Field F4
6.7 acres
common parcol line
+ i
•
1
tit.•
ap GeVraphic Information and 'An"alysi's,.N'C 9
•a^�r..�.w
1,500 Feet
Produced November 2015
Shaffer Soil Services, Inc.

The Compliance Boundary is established either 250 feet from the perimeter of the residuals application area or 50 feet within
the property boundary, whichever is closer. The Review Boundary is established midway between the Compliance Boundary
and the perimeter of the residuals application area. , A
Buffers
Property Line (50')
Perennial Stream (33')
House (400')
Well (100')
Legend
Propery Line
Field Boundary o Well
Perennial Stream House
iskiptit Surface Water
•
Nc: L ® Unused Area
Kay, Brian: Buffer Map
Parcel 1657001 8 1637
McDowell County, NC
n 175 71
^ 1 500 Feet
E { 1 L 1 t
35.5805,-81.8569 North Carolina Stateplane NAD83

Operation and Maintenance Plan
City of Marion, WWTP
Permit No. WQ0019960
In accordance with the requirements as issued by the North Carolina Department of Environmental
Quality using NCGS 143-215.1 and 143-215.3(a) based on 15A NCAC 02T .110, the City of Marion and U.S
Biosolids, Inc. is implementing this Operation and Maintenance Plan.
The Land Application of Non -Dedicated Class B Residuals from the City of Marion WWTP will be
conducted from the Wastewater Treatment facility, located at 3892 Highway 226 South Marion, NC
28752. Residuals will be removed and given away to farmers to be used as a soil amendment. The
residuals will be removed on as needed bases as fluctuation in the output of the plant will vary with
changing economic conditions. The day-to-day operation of the running of the Wastewater Treatment
will be conducted by Tim Horton, Wastewater Superintendent of the City of Marion WWTP or his/her
designee. The operations of the land application program will be conducted by Dennis Key of U.S
Biosolids, Inc. or his/her designee.
Land application of residuals will be determined once enough residuals have been produced from
processing of biological residuals to fill the 700,000-gallon residual digester. The land application event
is initiated by the Marion Wastewater Treatment plant contacting U.S. Biosolids, Inc. U.S. Biosolids, Inc.
will contact the farmers in listed in the permit to arrange for a land application event to occur. This my
take up to 45 days to arrange due to crop and animal rotations and weather conditions, so a land
application event must be planned enough in advance, so enough freeboard is maintained in the
residual digester.
Prior to land applying these residuals to permitted sites, the following sampling conditions must be met
(as is outlined in greater detail in the sampling plan attached to this Operation and Maintenance Plan).
Toxicity Characteristics Leaching Procedure (TCLP) will be conducted once per
year, if a land application event takes place.
A metals and nutrients analysis, pathogen and vector attraction, and soil analysis will be conducted
annually if a land application event takes place.
These samples will be collected by Tim Horton or his/her designee and transported to an approved lab
the same day the samples are taken, as in accordance with 15A NCAC 02B .0505. The samples must be
taken in a matter to ensure a representative sample of the residuals has been taken.
An inspection will be conducted daily while a land application event is taking place. This inspection will
confirm that all requirements of permit WQ0019960 are complying with regulations. The fields should
be inspected daily for compliance with the conditions that is outline in then permit. The inspection
should consist of (but not limited to):
1. All required setbacks and buffers are complying.
2. All required record keeping of truck and fields sheets are maintained and properly filled out so
accurate records of the volume and locate of residuals are keep.
3. All public access points are controlled (signs posted, gates closed)

4. Make sure all fields' records are turned over to the ORC so records can be reviewed by NCDEQ,
and an annual report can be constructed.
The daily land application inspection will be conducted by the following personal:
Dennis Key, ORC U.S. Biosolids, Inc.
Zach Key, BORC U.S. Biosolids, Inc.
If any issues or violations are discovered, the ORC of Land Application, the City of Marion WWTP and the
Asheville Regional Office should be contacted as soon as safely possible.
o ORC of Land Application, US Biosolids, Inc. 336-957-7878
o Marion WWTP 828-652-8843
o Asheville Regional Office 828-296-4500
To prevent any spills and or safety issues from occurring the flowing will take place during a land
application event. In the unlikely event of a spill consult the spill control plan immediately.
1. Access to the facility will be controlled with a locked gates and fences and signs to prevent any
unauthorized entry into the complex.
2. All pumps and hose will be checked at the start of each day for leaks or loose fittings.
3. All tanker valves are closed prior to loading and lids are closed prior to transport.
4. All dump trailers or dump trucks gates are tightly fastened and do not leak prior to transport.
5. All on road equipment is check as per DOT regulations for any safety or mechanical hazards or
issues.
6. All equipment is secured at the end of each working day to prevent any tampering or
unauthorized use.
7. Enough freeboard is maintained in the residual digesters so to prevent overflowing. This can be
accomplished by maintaining the levels of residuals to an acceptable level by planning adequate
land application events to keep up with residuals production.

City of Marion, WWTP
Permit No. WQ0019960
SAMPLING PLAN
Annually, if a land application event occurs, grab samples are collected from the digester.
Samples from the digester will be combined to form individual grab samples to be sent to a laboratory for
analysis.
These individual grab samples are collected and tested for fecal coliform analysis, vector
attraction reduction, nutrient analysis, and a TCLP test. These tests will be taken by the Tim Horton from
City of Marion or his/her designee. All samples apart from the vector attraction sample will be taken to a
state certified laboratory. The vector attraction sample will be analyzed in house at the City of Marion,
WWTP.
The vector attraction reduction will first be attempted to be achieved using option 4
[503.33(b)(1)]; Specific Oxygen uptake know as a SOUR test. This sample will be taken from the
digester.
Fecal Coliform is gathered in seven (7) individual samples and tested to meet the requirements of
[503.32(b)(2)]. This requirement is for the geometric mean fecal coliform density of the samples be less
than two million (2,000,000) MPN per gram. These samples will be placed in 250m1 containers and
placed on ice, in a cooler for transport to the laboratory before 1600 hours (4pm) the same day the
samples are obtained.
Annually, if land application occurs, a composite residual sample will be analyzed, prior to a land
application event for: Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, Zinc,
Aluminum, Ammonia Nitrogen, Calcium, Nitrate Nitrogen, Magnesium, % total Solids, pH, Phosphorus,
Potassium, TKN, Sodium. From this information, the Plant Available Nitrogen (PAN) and a Sodium
Absorption Ratio (SAR) will be calculated. This sample will be collected in a non -breakable container, at
least one quart in size. This sample will be taken from the digester.
A full TCLP test, including corrosivity, ignitability, and reactivity will be taken in two (2) gallon
containers from the aerobic digester. This test will be run annually unless prior approval is granted from
the division to reduce this requirement to once per permit cycle.

SPILL CONTROL PLAN- U.S. Biosolids, Inc.
City of Marion, NC -Permit No. WQ0019960
In the event of a spill, the following should be taken IMMEDITALY.
1. Make sure all personal and bystanders are safe- if not contact emergency services
2. Halt the source of the spill- overturned truck, leaking valve, ruptured tank.
3. Contain the spill. Use straw bales or earthen barrier to form a dike to contain the spill.
4. Cleanup. Employ vacuum trucks, dump trucks, and loaders to remove as much of the spilled
material as possible. Use straw to soak -up the remaining material. Dispose of the same in a
landfill.
5. Flush the roadways with water if needed. If the spill occurred on a tillable area, till the same into
the soil and spread lime if necessary. If a spill occurs on private property, final clean-up should be
to the satisfaction of the owner.
6. Notification. (This should be done as soon as safely possible.)
A. U.S. Biosolids, Inc. Main Office [phone]
B. City of Marion, WWTP- Tim Horton [phone]

C. NCDEQ-Asheville Regional Office [phone]
D. County Emergency Services (Sheriff, Fire Dept.) 911
7. Reporting:
The Permittee shall report by telephone to the Asheville Regional Office, telephone number (828)
296-4500, as soon as possible, but in no case more than 24 hours or on the next working day
following the occurrence or first knowledge of the occurrence of any of the following:
A. Surface disposal of residuals abnormal in quantity or characteristic.
B. Any failure of the surface disposal program resulting in a release of material to surface
waters.
C. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
D. Any process unit failure, due to known or unknown reasons, rendering the facility
incapable of adequate residual treatment.
E. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent
failure of a storage structure, etc.) outside of normal business hours shall be reported to the
Division's Emergency Response personnel at telephone number [phone], [phone],
or [phone]. Persons reporting such occurrences by telephone shall also file a written
report in letter form within five days following first knowledge of the occurrence. This report
shall outline the actions taken or proposed to be taken to ensure that the problem does not recur.
8. Spill Prevention. The easiest way to clean a spill is to prevent one.
A. Ensure loading personal watch the vehicle being loaded.
B. Ensure all valves and lids are closed.
C. Inspect all seals and replace if necessary.

Environmental Testing Sohn., Inc.
Certificate of Analysis
PO Box7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project name: Marion WWTP Project number: 200602.537
Collection date: 2-1un-20
Date received: 24un-20
Sample identification: Sludge 1- Grab Sample number: 199953
Parameter Method Result RL Units Analyad Dale Analyst Footnotes
Total Solids SM 2540 G 1.75 0.100 % ANB
Mercury 7471B 1.5 1.1 mg/kg TLT
Aluminum 6010 D 20800 282 mg/kg MLR
Arsenic 6010 D <28.2 28.2 mg/kg MLR
Cadmium 6010 D <11.3 11.3 mg/kg MLR
Calcium 6010 D 15300 563 mg/kg MLR
Copper 6010 D 422 11.3 mg/kg MLR
Lead 6010 D 47.5 28.2 mg/kg MLR
Magnesium 6010 D 5700 282 mg/kg MLR
Molybdenum 6010 D 39.0 28.2 mg/kg MLR
Nickel 6010 D 20.2 11.3 mg/kg MLR
Potassium 6010 D 5570 19.3 56.3 MLR
Selenium 6010 D <28.2 28.2 mg/kg MLR
Sodium 6010 D 2810 563 mg/kg MLR
Zinc 6010 D 1020 28.2 mg/kg MLR
Nitrate + Nitrite as 300.0 511 60.0 mg/kg ANB
Total Phosphorus 6010 D 23000 282 mg/kg MLR
Total Kjeldahl Nitrogen 351.2 58400 3690 mg/kg LKH
Total Nitrogen Calculation 58900 573 mg/kg LKH
Ammonia Nitrogen SIN 4500 NM 13 2800 220 mg/kg KEK
pH SW846 9040 C 6.2 0.1 S.U. MS
Percent Solids SM 2540 G 1.8 0.10 % KEK
N-PAV Calculation 18600 KEK
Sodium Absorption Rate Calculation Y/A KEK
FapLwt es.RL =Reporting Limit. Values are reported down to the Reposing Limit only.
I. Sample analyzed by Rogers & Callcotr Environmental.
2. Sample maimed pmaide holding time.
Date wed:
Data reviewed by:
Signature:
Kelley E. Keenan
2
NC Certification Number. 600
SC Certification Number: 99053
NC Drinking Water Certification Number 37786
'[Lis report should not be repmdured, eaept in in entirety, wIthoul the 0Xnen consent of Environmental Testing$olutioN, Inc.
The results in this report relate only to the sm pia submmed for analysis.

Environmental Testing Solutions, Inc.. Certificate of Analysis
Project name: City of Marion
Collection date: 15-Feb-21
Date received ... 15-Feb-21
Sample identification: FS TCLP - Grab
PO Box 7565
Asheville, NC 28802
Phone: [phone].
Fax: [phone];
Project mintier: . `.:20215.507.:.
Sample number 209872
..Parameter .
Date
Method Result RL ' Units Analyst Footnotes
Analyzed .......
<0.25 0.25 m :.
Arsenic - TCLP ... 6010 D ::. mg/L s-mar-zt MLR 1
Barium - TCLP 6010 D <2.50 2.50 mg/L 3-Mar-v. MLR 1
Cadmium -TCLP 6010 D <0.05 0.05 mg/L 3-Mar-21 MLR 1
<0.10 0.10 m
Chromium. - TCLP 6010 D g/.-
3-Mar-21 MLR 1
Lead - TCLP <0.25 0.25 m 3-Mar-21 MLR 1
6010 D :...... �
Selenium - TCLP 6010 D . <0.25 0.25 mg/L 3-Mar-2 MLR - 1
Silver - TCLP 6010 D <0.10 0.10 mg/L 3-Mar-21 MLR 1
Mercury - TCLP 7470A <0.0020 0.0020 mg/L 3-Feb-21 MLR 1
Full Scan TCLP Organics Seeattached sheets 1, 2 .'
Reactive Cyanide 335.4 1.70 0.05 mg/kg 22-Feb-21 ECHEM 2
Reactive Sulfide SM 4500 S D 2.70 : 0.1 mg/kg 22-Feb-21 ECHEM 2
Ignitability SW 846 1010 >190 190 °F 4-Mar-21 ECHEM 2
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit .only..
1. Sample analzyed by Rogers & Callcott Environmental.
2: Sample analyzed by Enviro Chemists, Inc:
Date reviewed:
Data reviewed by:
Signature:
Kelley E. Keenan
tA—e
NC Certification Number:: 600. . .
SC Certification Number: 99053
NC Drinking Water Certification Number:. 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

Client
ogee &Cattcott
ENVIRONMENTAL
Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Laboratory Report:
Project: iMarion.wW'rP
Work Order: 1020875
Received; 07/16/2021.12:30...:.
Dear Client:
Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of
custody for samples that were received on February 16 2021. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all
analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence
interval for each test methodunless otherwise qualified. Estimated uncertainty is available upon request.
Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Lauren Hollister, your Project Manager, at [e-mail]
(864)-232-1556 if you have any questions about this report.
Report Approved By:
:.Lauren Hollister.
Project Manager
This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.
x 5655.I Greenville, SC 29606 ` 426 Fairforest Way Greenville, SC 29607 ;main 64.232.1556 i fax 564_232.6140 rogersandcallcott com
. an employee -owned company:'
Page 1 of 21

Environmental Testing Solutions
Kelley E. Keenan
351. Depot St,
Asheville, NC 28801-4310
South Carolina Greenville Laboratory Identification
South Carolina Columbia Laboratory Identification 40572
North Carolina Laboratory Certification Number27
North Carolina. Drinking Water Lab Number 45710
NELAP Utah Certificate Number SC000042014-1
Georgia Drinking WaterLab ID 880
Project Marion WWTP
Work Orders 1020875
Received: 02/16/2021 12:30
Sample Number Sample Description: ; Matrix Sumpied
1020875-01 .. Marion WWTP Sludge - Grab.
:Solid 02115/21 07:40 Grab
x 5655 I Greenville, SC 29606 ' 426 Fairforest Way 1 Greenville,. SC 29607 i main 864.232.1556 ; fax [phone] roger sandca lcott.corn
4..m an employee -owned company
03/23/2021 09:49
This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.'

Roge s & Caticott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Project: Marion WWTP
Work Order: 1020875
Reported: 03/23/21 09:49
Revised Report
Revised to update the project name to Marion WWTP. This report replaces the one generated on 3/23/21 at 14:53.
PO Box 5655 Greenville, SC 29606 ' 426 Fairloreat Way Gr eenv€Ile SC 29607 main 864 232 1556 fax [phone] i0 t'O @1"san C1lCO .GOtYI
an employee -owned company
03/23/2021 09:49 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc; age 3 Of 21
I..

Rogers
oTAi.fi
ENV:IR0N:MEN
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Project: Marion W WTP
Work Order: 1020875
Reported: 03/23/21 09:49
Sample Number
Sample Description
Parameter
Sample Data
1020875-01
Marion WWTP Sludge- Grab collected on:02/15/21 07:40:..
Result..."
Reporting,
Limit:
Units DF Analyzed:::: Method `.
:Flag Analyst '.Butch
TCLP Metals
Mercury ND..:. 0.0020 nig/i, ..100 03/03/21 13:06 EPA7470A.
Arsenic ND 0,25.: mg/L 5.00 03/03/21 04:43 EPA60101).
Barium ND 2.50. mg/1, 5.00 03/03/21 04:43 EPA 6010D
Cadmium ND .. 0.05 mg/L 5.00 03/03/21 04:43 EPA 601mu
Chromium . ND 0.10. mg/L 5.00 03/03/21 04:43 EPA 6010D
Lead ND 0.25 mg/L 5.00 03/03/21 04:43 EPA 6010D
Selenium ND 0.25 mg/L 5.00 03/03/21 04:43 EPA6010D
Silver ND 0.10 mg/L 5.00 03/03/21 04:43 EPA 6010D
TCLP Volatile Organics
Benzene ND 0.100 mg2 50.0 03/01/21 18:09 EPA8260D
2-Butanone (MEK) ND 0.200 mg/L 50.0 03/01/21 18:09 EPA8260D' .'
Carbon tetrachloride ND : 0.100 mg/L 50.0 03/01/21 18:09 EPA8260D
Chlorobenzene ND ` 0.100 mg/L 50.0 03/01/21 18:09 EPA8260D
Chloroform ND 0.100 mg/L 50.0 03/01/21 18:09 EPA 8260D
1,2-Dichloroethane ND ' 0.100 mg/L 50.0 03/01/21 18:09 EPA 82601)
1,4-Dichlorobenzene ND 0.100 mg/L 50.0 03/01/21 18:09 EPA8260D'
1,1-Dichloroethene ND 0.100 mg/L 50.0 03/01/21 18:09 EPA 8260D
Tetrachloroethene ND 0.100 mg/I, 50.0 03/01/21 18:09 EPA8260D
Trichloroethene ND 0.100 mgL 50.0 03/01/21 18:09 EPA8260D
Vinyl chloride ND 0.100 mg/L 50.0 03/01/21 18:09 EPA"8260D
Surrogates
%REC •%%REC Limits' Flag
MLR B1C0126
MLR . RIC0080
MLR B1C0080'
MLR B;1G0080
MLR • " .BiC0080
MLR 13-1C0080
MLR 131C0080
MLR BIC0080
AMF B1C0582
AMF BC0582
AMF B1C0582
AMF 111C0582
AMF 131C0582
AMF 131C0582
AMF BIC0582
AMF B1C0582
AMF 131C0582
AMF B1C0582 :.:
AMF BC0582:.:.,
1.2-Dichlo►oethane-D4 104 .... 70 130 ..:.
TolueneD8. 111 70-130':".
4-Bromo,(luorobcn:ene :: 124 ' 70-130
TCLP Seinf-Volatile Organics
2-Methylphenol (o-Cresol)
3/4-Methylphenol (m,p-Cresol)
total Cresol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene.....
ND. 0.100 ....mg/L . 10.0 :03/09/21, 15:00... ...EPA8270E : ...RJM.. B110071
RBIr0071ND `. 0.100. m$L 10.0 03/09/21 15:00 • EPA 827OE . M Nu.... 0.200 .mg/L 100 .03/09/21 15:00 EPA827OE' RJM . B1C0071 -
ND 0.1.00. mg/L 10.0 03l09/21' 15:00 EPA$270B:' > ; B1.00071
ND'.. 0.100 mg L 10.0 03/09f21 .15;00 ...EPA827OE`, RANI • "B'1.0007i
ND 0:100 . ma L 10.0 03/09/21
15:00..EPA 8270E
: RJ1VI B1C0071
•.. .
ND 0.100. ing'L 10.0 03/09/2115:00 EPA827OE. RM B1C0071
.
ND .• 0..1.00. " ..m�8/L.. ' 10.0 03i09/21. 15:00 .EPA 827OE.:
RJM B.1C0071
PO Box 5655 I Greenville; SC 29606 ..426 Fairforest lNay 1 Greenie, SC 29607 I ma" 864.2321556 1 fax [phone] rogersandcallcott.COm
.... an employee; owned romp},3ry
03/23/2021 09:49.
This report may not be reproduced, except in full, :without written permission from Rogers 4 Cgllcott, Fncnc.:l:
Page 4 of 21 I

03/23/2021 09:49
Ro e s &Calicott
ENVIRONMENTAL
Environmental Testing Solutions.. Project: Marion WWTP
351 Depot St Work Order: 1020875
Asheville, NC 288014310 Reported: 03/23/21 09 49`
Sample Number
Sample Description Marion W WTP:Sludge Grab collected on 02/15/2I 07:40
Parameter
1020875-01
Result
Reporting.
Limit
p
F Analyzed .: Method :. Flag Analyst Batch .:.
Units
TCLP Semi -Volatile Organics
Pentachlorophenol ND . 0.200 mg/L 10.0 03/09/21 15:00 EPA8270E RJM B1.00071
Pyridine ND . 0.100 mg/L " 10.0 03/09/21 15:00 EPA 8270E RIM B1C0071
2,4,5-Trichlorophenol ND 0.1.00; mg/L 10.0 03/09/21 15:00 EPA8270E .RJM B1C0071
2,4,6-Trichlorophenol ND 0.100 mg/L , 10.0 03/09/21 15:00 EPA 8270E RJM :. 131 coo71
Surrogates.
%REC %REC Limits
Nitrobenzene-DS
2-Fluorobipbenyl
2-Fluorophenol
Phenol-D5
2, 4.6-Tribromophenol
Terphenyl-D14
69 15-314
61 32-118
47 20-110
35 8-424
75 39-130
85 26-173
TCLP Pesticides
Gamma-BHC (Lindane) ND 0.00050 mg/L 10.0 03/10/21 02:55 EPA8081B
Chlordane ND . 0.0050 mg/L 10.0 03/10/21 02:55 EPA8081B
Endrin ND 0.00050 mg/L 10.0 03/10/21 02:55 EPA8081B
Heptachlor, ND : 0.00050 mg/L 10.0 03/10/21 02.55 EPA808IB
Heptachlor: epoxide ND 0.00050 mg/L 10.0 03/10/21 02:55 EPA8o8IB..
Toxaphene ND . 0.0050 mg/L 10.0 03/10/21 02:55 EPA8o81B.,
Methoxychlor . ND 0.00050 mg/L 10.0 03/10/21 02:55 EPA808113
Surrogates. %REC %REC Limits
: Flag
RKH B1C0171
RKH B1C0171
RKH BIC0171`::
RKH BIC0171:
RICH 131C0171
RKH B1C0171
RICH Bt.00J,71
2.4.5,6-Tetrachloro.m-xylene 25 60-130
DecachlorobiphenyJ 23 30450
R..
PO Box 5655 i Greenville, SC 29606 1 426 Fairforest V'day = Greenville, SC 29607 main 864.232.1556 864.232.6140 rogerSandcallcott.com
an employee -owned company
I Page-5of21
This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.

ogers tot
LNViR0NMENTAL
Environmental Testing Solutions ..
351 Depot St..
Asheville,: NC 28801-43.10
Batch BICOO80: - EPA:3005A
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Blank (131C0080-BLK3)
Arsenic'
Barium
Cadmium
Chromium
Lead
Selenium
Silver.
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium:
Silver
LCS (B1C0080-BS2)
Arsenic
Barium
Cadmium
Chroiniuin
Lead..
Selenium
Silver .
Project:.: Marion WWTP
Work Order, 1020$75
Reported 03/23/21 •09 49
TCLP.'Metals
•Quality Contro•l Summary •
Spike
Level
ND 0,05
ND 0.50 mg/L.
ND 0.01 mg/L
ND 0.02
ND 0.05 mg/L
ND 0:05 mg/L
ND 0.02 mg/L
ND 0.25 mg/L
ND 2.50 mg/L
ND 0.05 mg/L
ND 0.10 mg/L
ND 0.25 mg/L"
ND 0.25 mg/L
010 mg/L
Source %REC:.:
Result %REC IAmliia RED Limit..,
0.48 0.05 mgL: 0.500 97 80-120
ND 0.50. mg/L 0.500 95 80-120
0.47 0.01 mg/10.500 94 80120
0.48 0.02. mg/L 0.500 95 80-120
0.48 0.05 mg/I., 0.500 ': 96 80-120
0,48 0.05 mg/L 0.500 96 • 80-120 , ....
0,47 0.02 mg9I 0.500 95 80-120
2,45 0.05 mg/L 2.50 98 ':80-110
:2.45 0:50 mg/L 2.50 98 80.120
2.37 0:01 , mg/L 2,:50 95 ' " 80-120
2,41 .. 0:02: mg/L., ...:.. .,2.50:,::. 96...'. 80-120
2.43. 0.05 ' mgIL 2:50 97 80-120
2,50 0:05 mg/L 2:50 : '. `. 100 80-120
2,46 0.02 mg/L . :::230 .. 98 80-120
PO BoxSEr55 Greenville, SC 29606 426 Fairforest Way s Greenville, 5C 29607 main 864.23?.IS56 fax 864_232.6140-COgersanf Cal_cat. o n
an employee -awned company
03/23/2021 09:49
This report may not be reproduced. except in full, without written permission from Rogers & Callcott. Inc.

Roy s &Cattcott
ENVIRONMENTAL
Environmental Testing Solutions
351 DepotSt.
Asheville, NC 28801-4310
Project: Marion WWTP
Work Order: 1020875
Reported: 03/23/21 09:49 -'
Parameter
LCS Dup (B1C0080-BSD1)
Arsenic
Barium Cadmium
Chromium
Lead
Selenium
Silver
LCS Dup (B1C0080-BSD2)
Result
TCLP Metals
Quality Control Summary
Reporting
Limit
Spike Source %REC RPD
Units Level Result %REC Limits RPD Limit Flags
0.48 0.05 mg/L 0.500 96 80-120 0.9 20
ND 0.50 mg/L 0.500 95 80-120 20
0.47 0.01 mg/L 0.500 94 80-120 0.7 20
0.48 0.02 mg/L 0.500 95 80-120 0.2 20
0.48 0.05 mg/L 0.500 96 80-120 0.2 20
0.48 0.05 ing/L 0.500 97 80-120 0.5 20
0.47 0.02 mg/L. 0.500 95 80-120 01. 20
Arsenic 2.45 0.05
Barium 2.44 0.50
Cadmium 2.36 0.01
Chromium 2.40 0.02
Lead ` 2.44 0.05
Selenium 2.49 0.05
Silver 2.44 0.02
Matrix Spike (B1C0080-MS5) Source:1020875-01
Arsenic 2.44
Barium 2.58
Cadmium
Chromium
Lead ...
Selenium
Silver
Batch B1C0126 - EPA 7470A
Blank (B1C0126-BLK1)...
Mercury
Blank (B1C0126-BLK3)
20
20
20
20
•
20
20
2.41 0.05
2.42 0.10
2.44 . 0.25
2.55 0.25
2A4 0.10
0.25 mg/L
2.50 mg/L
mg/L
mg/L
mg/L
mg/L
2.50 98 80-120 0.2.
2.50 98 80-120 0.6
2.50 95 80-120 0.4
2.50 96 80-120 0.2
2.50 98 80-120 0.6
2.50 100 80-120. 0.4
2.50 98 80-120 0.7 20
2.50 75-125
2.50 ND 96 75-125
2.50 ND 96 . 75-125
2.50 ND 97 75-125
2.50 ND 97 75-125
2.50 ND 102 ... 75-125
2.50
ND
98
PO Box 5655 i Greenville, SC 29606 s 426 Fairforest Way Greenville, SC 296©7 ' main 864,232.1556 ; fax $64.232.6140 rogerSandcaltcott.com
an employee -horned company
03/23/2021 09:49
This report may not be reproduced, except in full, without written permission from Rogers & Calkott, Inc.

Rogers &Ca[kat
ENVIRONMENTAL
Environmental Testing Solutions
351.Depot St.
Asheville, NC 28801.-4310
Batch B1C0126 EPA 7470A
LCS (B.1C0126-.BS1)
LCS (B1C0126-BS2)
Mercury
LCS Dup (B1C0126-BSD1).
Project: Marion WWTP
Work Order: 1020875
Reported 03/23/21 09:49
TCLP Metals
Quality Control Summary :.
. aeportitig ... Spike Source %REG" RPD
Limit 1luits Level $exult %REC LimitE 1tPD Limit'
0.0051 0.0002 - ..: mg/L. 0.00500 102 85.115 :..:
0;0507 o.00z0 mgiL'. ` .
0.0500
Mercury 0.0051 0.0002 , ukg/L 0.005011
LCS Dup (B1C0126-BSD2)
Mercury 0.0508 0.0020
Matrix Spike (B1C0126-MS3)
L 0.0500
Mercury 0.0509 0.0020 mg/L 0.0500
101 , 85 115 .
85-115 : 1 20
102 85-115
102 ` 75-125
20
PO Sox 5655 i GI eenvU!e, SC 29606 426 Fairforest Way l G,reenvile, SC 29607 i main 864.232.1556 fax [phone] rogers lndcatcott.com
m _ an employee -owned company
03/23/2021.09:49 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.

Environmental Testing Solutions Project: Marion WWTP
351 Depot St
Work Order: 1020875
Asheville, NC 288014310 Reported:..: 03/23/21 09:49
TCLP Volatile Organics
Quality Control Summary
Batch BiC05.82 :EPA 5030•
.:Blank (B1C0582-31,1(1:) • .:. .
Benzene ... ND 0.00200
2-Butanone (MEK) ND .. 0.00400 tng/L::
Carbon tetrachloride ND 0.00200
Chlorobenzene ND 0.00200 mg/L.;
Chloroform . ND 0.00200 .. mg/L
1,2-Dichloroethane ND 0.00200 mg/L
1,4-Dichlorobenzene ND 0.00200 mg/L
1,1-Dichloroethene ND 0.00200 mg/L,
Tetrachloroethene ND 0.00200 mg/L.
Trichloroethene ND 0.00200 mg/L
Vinyl chloride ND 0.00200 mg/L
Surrogate: 1,2-Dichloroethane-D4
Surrogate: Toluene D8
Surrogate: 4-Bromofluoiobenzene
Blank (B1C0582-BLK3)
Benzene ND 0.100 . mg/L
2-Butanone (MEK) ND 0.200 mg/L
Carbon tetrachloride ND 0.100 :: mg/L
Chlorobenzene ND 0.100. mg/L
Chloroform ND 0,100 mg/L
1.2-Dichloroethane ND 0.100 ..: mg/L
1,4-Dichlorobenzene ND. 0.100 mg/L.
1,1-Dichloroethene ' ND 0.100 mg/L
Tetrachloroethene ND .. 0.100. •:.:.. ....mg/L:
Trichloroethene ND 0.100 mg/L.
Vinyl chloride ND .. 0.100 -::..
ICED:
Source : . `' ' :..::'/. BBC
:
Resalt %RBC: ,. Limits.... RPD Limit: ::
107 70-130
109 70-130
123 70-130
Surrogate: 1, 2Dichloroetliane=D4
Surrogate: Toluene D8 112
Surr»gate: 4-Bromof luorobenzene
. 113 :::.. . 70-130' :....
':LCS (B1C0582=BSI)
Benzene ` 0.0233 0 00200' mg/l; 0.0200 116' 70-130
2-Butanone.(MEK) . 0.0212 0,00400' mg/L! 0.0200' 106 60-140 ,
Carbon tetrachloride . 0.0244 0.00200 mg/L., 0.0200, 122 70-130
Chlorobenzene 0.0226 0.00200 :: mg/L 0.0200 113 : 70-130
FGz Box 5655 Greenville, SC.29606 1426 Fairforest Way : Greenville SC 29607 I main ii64.2321556 !Fax [phone] rtigerSandtaliCOttg0lY1'
..•:-.. anemployee-ownedOtnp<any.
This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.::

Cattcott
;V i0P NMENTA.L
Environmental Testing Solutions Project: Marion WWTP
351 Depot St. Work Order: 1020875
Asheville, NC 28801-4310 Reported: 03/23/21 09:49
TCLP Volatile Organics
Quality Control Summary
Reporting
Limit Units'
Spike Source
Level Result %REC
Chloroform 0.0217 0.00200 mg/L 0.0200 109 70-130
1,2-Dichloroethane 0.0222 0.00200 - mg/L 0.0200 111 70-130
1,4-Dichlorobenzene 0.0215 0_00200: mg/L 0.0200 107 70-130 ;
1,1-Dichloroethene 0.0245 0.00200 mg/L0.0200 I22 70-130
Tetrachloroethene 0.0211 0.00200 mg/L 0.0200 106 70-130
Trichloroethene 0.0235 0.00200 mg/L, 0.0200 118 70-130
Vinyl chloride 0.0245 0.00200 mg/L 0.0200 123 60-140
Surrogate: 1,1-Dichloroethane-D4
Surrogate: Toluene-D8
Surrogate: 4 Bromofluorobenzene
127 70-130
127 70-130 113 70-130
Benzene 0.0227 : 0.00200 mg/L 0.0200 114 70-130 2 20
2-Butanone (MEIO 0.0211 0.00400 mg/L 0.0200 105 60-140 0.6 20
Carbon tetrachloride 0.0238 - 0.00200 mg/L 0.0200 119 70-130 2 20
Chlorobenzene 0.0230 0.00200 mg/L 0,0200 115 70-130 2 20
Chloroform 0.0216 0.00200 mg/L 0.0200 108 70-130:.. 0.7 20
1,2-Dichloroethane 0.0220 0.00200. mg/L 0.0200 110 70-130 • 1 20
1,4-Dichlorobenzene 0.0225 0.00200 mg/L 0.0200 1I2 70-130 4 20
1,1-Dichloroethene 0.0240 0.00200 mg/L 0.0200 120 70-130 2 20
Tetrachloroethene 0.0212 0.00200 ntglL 0.0200 106 70-130 0.2 20
Trichloroethene 0.0234 0.00200 mg/L 0.0200 117 70-130 .r 0.6 20
Vinyl chloride 0.0236 0.00200 mg/L 0.0200 118 60-140 4 20
Surrogate: 1,2-Dichloroethane-D4
Surrogate: Toluene-D8
Surrogate: 4-Bromofluorobenzene
Matrix Spike (B1C0582-MS3) .. Source: 1020875-01
126 70-130:..
128 70-130
112 70-130
Benzene 1.16 0.100 mg/L T.00 ND I16 70-130
2-Butanone (MEK) 0.924 0.200 mg/L 1:00 ND 92 60-140
Carbon tetrachloride 1.24 0.100 mg/L 1.00 ND 124 70-130
Chlorobenzene 1.08 0.100 mg/L 100 ND 108 70-130
Chloroform 1.07 0.100 mg/L 1.00 ND 107 70-130
1,2-Dichloroethane 1.04 0.100 mg/L 1.00 ND 104 70-130
1,4-Dichlorobenzene 1.09 0.100 mg/L 1.00 ND 109 70-130
1,1-Dichloroethene 1.33 0.100 mg/L 1.00 ND 133 70-130 8
PC7 Box 5655 1 Greenville, SC 29606 , 426 fairforest VVay ? Greenville, SC 29607 = main 864,232i556 ' fax [phone](1 I'O,gersandcaUcott.com
an employee -owned company
03/23/202i 09:49
This report may not be reproduced, except in full, without written permission from Rogers & Callcatt, Inc.

Callcott
NVIRONMENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Project: Marion WWTP
Work Order: 1020875
Reported: 03/23/21 09:49
TCLP Volatile Organics
Quality Control Summary
Spike Source %REC ; RPD°
Units Level Result %REC Limits RPI) Limit- Flags
Batch B1C0582 - EPA 5030
Matrix Spike (B1C0582-MS3)
Tetrachloroethene 1.11 0.100 mg/L 1.00 ND 111 70-I30.
Trichloroethene 1.19 0.100 - mg/L 1,00 ND 119 70-130
Vinyl chloride . 1.08 0.100 mg/L 1.00 ND 108 60-140
Surrogate: 1, 2-Dichloroethane-D4
Surrogate: Toluene-D8
Surrogate: 4-Bromofluorobenzene
122 70-130
130 70-130
117 70-130
PO Box 5655 = Greenville; SC 29606 ' 426 Fairforest Way ? Greenvitle, SC 29607 mam $64,232,1556 ? fasc 864.2 2.6140 rogersandcal cott.com
an employee -owned company
03/23/2021 09:49
This report may not be reproduced, except in full, without written permission from Rogers &Callcott; Inc:

e s &Ca cat
ENViR0 Nil ENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Project: Marion WWTP
Work Order: 1020875
Reported: 03/23/21 09:49
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting
Result Limit
Spike
Level
Source
Result %REC
%REC - RPD
Limits RPD Limit
Batch B1C0071 - EPA 3510C - GCMS
Blank (B1C0071-BLK1)
2-Methylphenol (o-Cresol)
3/4-Methylphenol (m,p-Cresol)
total Cresol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Blank (B1C0071-BLK2)
2-Methylphenol (o-Cresol)
3/4-Methylphenol (m,p-Cresol)
total Cresol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
PO Box 5655 Gieenvl
03/23/2021 09:49
Surrogate: Nitrobenzene-D5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Phenol-D5
Surrogate: 2, 4. 6-Tribromophenol
Surrogate: Terphenyl-D14
ND
ND
0.0100 mg/L
0.0100 mg/L
0.0200 mg/L
0.0100 mg/L
0.0100 mg/L
0.0100 mg/L
0.0100 mg/L
0.0100 mg/L
0.0200 mg/L
0.0100 mg/L
0.0100 mg/L
0.0100 mg/L
0.100 mg/L
0.100 mg/L
0.200
0.100
ND 0.100
ND 0.100
ND 0.100
ND 0.100
ND 0.200
ND 0.100
ND 0.100
ND 0.100
ND
ND
Surrogate: Nitrobenzene-D5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate • Phenol-D5
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
63 15-314'
69 32-118
61 20-110
45 8-424
71 39-130
98 26-173
SC 29606 i 426 Fairforest Way i Greenville, SC 29607 main 864.232,1556 fax
37 15-314 '-
54 32-118
33 20-110
26 8-424
64.232.6140 rogersandcallcott.corri
- an employee -owned company
This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.

Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Project: Marion WWTP
Work Order: 1020875
Reported: 03/23/21 09:49
Parameter
Batch B1C0071 - EPA 3510C - GCMS
Blank (B1C0071-BLK2)
LCS (B1C0071-BS1)
2-Methylphenol (o-Cresol)
3/4-Methylphenol (m,p-Cresol)
2,4-Dinitrotoluene Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting
Result Limit Units
Surrogate: 2, 4.6-Tribromophenol
Surrogate: Terphenyl-D14
0.433 0.100
0.831 0.100
0.549 0.100
0.602 0.100
0.520 0.100
0.382 0.100
0.436 0.100
0.554 0.200
0.359 0.100
0.698 0.100
0.625 0.100
Surrogate: Nitrobenzene-D5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2 Fluorophenol
Surrogate: Phenol-D5
Surrogate: 2, 4, 6-Tribromophenol
Surrogate: Terphenyl-D14
Matrix Spike (B1C0071-MS3)
2-Methylphenol (o-Cresol)
3/4-Methylphenol (m,p-Cresol)
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Triehlorophenol
Spike
Level
mg/L 0.800
mg/L 1.60
mg/L 0.800
mg/L 0.800
mg/L 0.800
mg/L 0.800
mg/L 0.800
mg/L 0.800
mg/L 0.800
mg/L 0.800
ing/L 0.800
Source %REC
Result %RFC Limits RPD
54
52
69
75
65
48
55
69
45
87
78
39-130
26-173
40-110
40-110
52-110
52-121
30-110
24-110
36-110
43-125
24-110
53-115
53-110
57 15-314
69 32-118
47 20-110
34 8-424
85 39-130
80 26-173
0.366 0.100 mg/L 0.800 ND 46 30-110
0.495 0.I00 mg/L 1.60 ND 31 26-110
0.357 0.100 mg/L 0.800 ND 45 43-120
0.476 0.100 - mg/L 0.800 ND 60 45-120
0.300 0.100 mg/L 0.800 ND 37 12-110
0.217 0.100 mg/L 0.800 ND 27 15-110
0.283 0.100 mg/L 0.800 ND 35 25-112
0.558 0.200 mg/L 0.800 ND 70 30-140
0.251 0.100 mg/L 0.800 ND 31 17-110
0.457 0.100 mg/L 0.800 ND 57 46-125
0.434 0.100 mg/L 0.800 ND 54 43-120
Surrogate: Nitrobenzene-D5
Surrogate: 2-Fluorobiphenyl
x 5655 i GreeiaviEle,'SC 29606 ? 426 Fairfores
03/23/2021 09:49
15-314
32-118
ay i Greenville, SC 29607 main 864.232,1556 fax 864_232.6140 rogersandcallcott.com
an employee -owned company
Page13of21
This report may not be reproduced, except in full, without written permission from Rogers 8c Callcott, Inc.

Rogers Ca cat
ENViRONMENTAL
Environmental Testing Solutions Project: Marion WWTP
351 Depot St. Work Order: 1020875
Asheville, NC 28801-4310 Reported: 03/23/21 09:49
TCLP Semi -Volatile Organics
Quality Control Summary
Spike Source *AMC RPD
Units Level Result %REC Limits RPD Limit
Batch BIC0071- EPA 3510C - GCMS
Matrix Spike (B1C0071-MS3) Source: 1020875-01
Surrogate_ 2 Fluorophenol
Surrogate: Phenol-D5
Surrogate: 2, 4, 6-Tribromophenol
Surrogate: Terphenyl-D14
PO Box 5655 I Greenville, SC29606'i 426 Fairforest Way Greenvi}Ie, SC 29607 i2
03/23/2021 09:49
'33 20-110
24 8-424
67 39-130.
73 26-173 `.
64.232IS56 864.232.6140 rogersandcallcc tt.corn
an employee -owned company
This report may not be repr duced, except in full, without written permission from Rogers & Callcott, Inc..

Environmental Testing Solutions Project: Marion W WTP`
351 Depot St. Work Order: 1020875
Asheville, NC 28801-4310 Reported: 03/23/21 09:49
TCLP Pesticides
Quality Control Summary ...
Spike
Level Result
Black (B1C0171-BLK1)
Gamma-BHC (Lindane) . ND 0,000050.. mg/L
Chlordane ND 0.00050 `. me-
Endrin ND 0.000050 mg/L
Heptachlor ND 0,000050 mg/L
Heptachlor epoxide ND 0.000050 mg/L
Toxaphene ND 0.00050 mg/L
Methoxychlor ND 0.000050 mg/L
Surrogate: 2,4,5,6-Tetrachloro-m-xylene 63 60-130
Surrogate: Decachlorobiphenyl 51 30-150
Gamma-BHC (Lindane) ND 0.00050 mg/L
Chlordane ND 0.0050 mg/L
Endrin ND 0.00050 mg/L
Heptachlor ND 0.00050 ` mg/L
Heptachlor epoxide, ND 0.00050 mg/L
Toxaphene ND 0.0050 mg/L
Methoxychlor ND 0.00050. mg/L
Surrogate: 2,4.5,6-Tetrachloro-m-xylene 55 60-130
Surrogate: Decachlorobiphenyl 68 30-150 :`•
LCS {B1C0171-BSI)
Gamma-BHC (Lindane) 0.0031 0.00050 mg/L 0.00400 7770-130
Endrin 0:0034 0.00050 mg/L 0.00400 85 70-130 ::
Heptachlor 0.0030 0.00050 . mglL 0,00400 74 70-130 :.
Heptachlorepoxide 0.0032 0.00050 . mg/L 0.00400 % 80 • 70-130
0: 003
Methoxxychlor 2 0,00050' mg/L 0.00400 79 70-130 :,
Surrogate: 2.4, 5, 6Telrachlbro-m-xylene
Surrogate: Decachlorobiphenyl : ..
61 :...
7..::
. 30,150
Matrix S ike.(1CO171-MS1) : : Source:1020875=01
Gamma-BHC (Lindane) 0.0035 0.00050 mglL 0.00400 ND 87 .: 60-140
Endrin.. 0.0037 0.00050 mg/L 0.00400 ND 92 60-140
Heptachlor 0.0035 0.00050 mg/L 0.00400 `. ND 1 88 60-140
Heptachlorepoxide 0.0035 0.00050 mg/L 0.00400 Ni) 86 60-140
Methoxychlor 0.0034 0.00050 mg/L 000400 ND 85 60-140
x 5655 :l Greenville, SC
03/2312021 09:49
96{ib ! 426 Fairiorest Way ' Greetivik(e. SC 29607 , main 864.232.1556 ;fax 864_232.6140 rogersandca Hcott_com
an employee -owned company
This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. I Pane 5 ©f 21

Environmental Testing Solutions Project: MarionWWTP
351 Depot St. Work Order: 1020875
Asheville,NC 28801-4310 Reported 03/23/21 09:49
TCLPPesticides'
Quality Control Summary
Reporting Spike Source "/rREC ..: RPD
Limit. Units ; Level Result %REC Limits RPD Lionit .' Flags
Batch 131CO171- EPA 3510C - GC.
Matrix Spike (B1C0171-MS1) Source;1020875-D1
Surrogate: 2,4:5,6•Tetrachloro-m xylene
Surrogate: Decachlorobiphenyl
Matrix Spike Dup (B1C0171-MSD1) Source:1020875-01'..
Gamma-BHC (Lindane) 0.0034 0.00050 mg/L 0.00400 ND 84 60-140 : 4 20
Endrin 0,0035 0.00050 . mg/L 0.00400 ND 89 60-140 4 20
Heptachlor 0.0034 0.00050 mg/L 0.00400 ND 84 60-140 4 • 20
Heptachlor epoxide 0.0033 0.00050 mg/L 0.00400 ND 83 60-140 4 20
Methoxychlor 0.0031 0.00050 mg/L 0.00400 ND 78 60-140 10. 20
Surrogate: 2,4,5i6-Tetrachloro-m xylene 67 60-130
Surrogate: Decachlorobiphenyl 67 30-150
PO Box 5655 ., Greenville, SC 29606 426 Fa€rforest Way 1 Greenville, SC 29607 -main 864.232,1556 ` £ax 864.232.6140 roger sandcal cott.corn
mm - an employee -owned company
03/23/2021 09.-49
This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.

Environmental Testing. Solutions.
351 Depot St.
Asheville, NC 28801-4310
Project: Marion WWTP
Work Order: 1020875
Reported: 03/23/21 09:49
TCLP Bottle Extraction
Quality Control Summary
Reporting Spike Source %REC RPD
Result
Limit Unitp ...- I.evet Result "7oRkC LfuN6 RPD Limit Flags
Complete.
PO Box 5655 I Greenville, SC 29606 426 Fairforest Way .1 Greenville, SC 29607 main 864.232,1556 ' tax 864_232,6140 rogerSandCai1COtt.CC►R1
..n,, an employee --owned company
03/23/2021 09:49 This report may not be reproduced, except in full, without written permission from Rogers & Callcott. Inc-

Ro erg &Caticott
ENVIRONMENTAL
Environmental Testing Solutions
35.1 Depot, St,
Asheville; NC 28801-4310
roject: ` Marion WWTP
Work Order 1020875
Reported 03/23/21 09:49.:
Batt h B1:B1�249: -EPA 13I1 ..ZHE
::Blank (B10.249-BLK1)
TCLPZHE Extraction
EPA 3005A ICP Digestion
EPA 3005A
EPA 3510 Extraction . .
EPA 3510C-GC
EPA 3510 Extraction
EPA 3510C - GCMS
EPA 7470A Mercury Digestion
EPA 7470A
Parameter
EPA 1311 TCLP Extraction :
EPA 1311
EPA 1311- TCLP ZHE,
EPA 1311- ZHE
TCLP ZHE Extraction ..
Quality Control Summary
Spike Source;....:.:. ,
'traits :• Level Result %REC Limits
Sample Preparation Data
Batch Sample ID Prepared
B1C0080 1020875-01 03/02/2021 09:57
B1C0171.. 1020875-01 03/03/2021 09:15
'131C0071 1020875-01 03/02/2021 09:00
B 1 C0126 1020875-01 . 03/02/2021 16:39
Batch • Sample ID ` Started Finished
B1C0412 1020875-01 2/28/2021 at 1141 3/1/2021 at 0715
B1B1249 ..: 1020875=01: 2125/2021 at 1700 2/26/2021 at 0940 '..
PO Box 56r551 Greenville; SC 29606 ! 426 Fairfore
Extraction..
:Fluid # on
ay ( Greenville, SC 29607 ! main 864,232,1556 ;fax [phone]i40 rogersandcallcott:-Com
an employee -owned company
This report may not be reproduced, except in full, without written permission from.Rogers & Cancan, Inc.
Ige 18 of 21

Rogers ott
EN\i1RONi ENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Project: Marion WWTP
Work Order: 1020875
Reported: 03/23/21 09:49
Data Qualifiers and Definitions
ND Analyte NOT DETECTED at or above the reportinglimit
Nlt Not reported
RPD Relative Percent Difference
R The surrogate was not within quality control limits.
S The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits. The Laboratory Control Sample
(LCS) was within control limits.
Sample extracted and analyzed in hold time and results were non -detect with low surrogate recoveries. Sample re -extracted and
reanalyzed out of hold time on 3/17/21 and surrogate recovenes were within limits. Non -detect results were confirmed.
03/23/2021 09:49
SC 29606 i 426 Fairforest
Greenville, SC 29607 t main 864.232.1556 i fax [phone] rogersandcal(Cott.coi
�._� . an employee -owned company
This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.
Page 19 of 21

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Rogers &Cattcott
ENVIRONMENTAL
Client: ETS
Sample Receipt Verification
Date
Received:
Carrier Name: Client
02/16/21
Work
Order: 1020875
FedEx UPS US Mail Courier Field Services Other:
Tracking Number: 462235129446
N
e
s
N
A
Shipping container / cooler intact?
X
amaged
Leaking Other:
Custody seals intact?
X
COC included with samples?
X
COC signed when relinquished and received?
X
Sample bottles intact?
X
Damaged Leaking Other:
Sample ID on COC agree with label on bottle(s)?
X's
Date / time on COC agree with label on bottle(s)?
X`
Number of bottles on COC agrees with number of bottles received?
X
Samples received within holding time?
X
Sample volume sufficient for analysis?
X'
VOA vials free of headspace (<6mm bubble)?
X
Temp at receipt recorded on COC
Samples cooled? Temp measured with IR thermometer - SN: 97050067
Samples requiring pH preservation at proper pH?
Note: Samples for metals analysis may be preserved upon receipt in the lab.
Note: Samples for O&G and VOA analysis `preservation checked at bench.
Samples dechlorinated for parameters requiring chlorine removal at
the time of sample collection?
Note: Chlorine checked at bench for samples requiring Bacterial, VOA, and HAA
analysis.
X
X
X
Cold Packs Dry Ice None
If in-house preservation used — record Lot
HCL
H3PO4
H2SO4
NaOH
HNO3
Other '!
Were non-conformance issues noted at sample receipt?
Yes
or
Non -Conformance issue other than noted above:

ANALYTICAL 8, CONSULTING CHEMISTS
Environmental Testing Solutions, Inc.
Post Office Box 7565
Asheville NC 28802
Attention: Kelley Keenan (ETS)
Lab ID Sample ID:
21-06871 Site: Sludge 002
2,4,5-TP (TCLP)
2,4-D (TCLP)
RCI
Cyanide
Sulfide
Ignitability
Report #:: 2021-02848
nvironmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.02_23 Lab : 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Mar 04, 2021
Customer PO #:
Customer ID: 08100055
Report #: 2021-02848
Project ID: Marion VWVTP
Collect Date/Time
2/15/2021 7:40 AM
SW846 Method 8151A
SW846 Method 8151A
SM4500CND.
SM 4500 S D
SW 846 method 1010
Matrix Sampled by
Solid/Sludge Client
Results
1.70 mg/kg
2.70 mg/kg ..
>190 °F
02/26/2021
02/26/2021
02/22/2021
02/22/2021
03/04/2021

Sample Number
EIS Ilse Only
atria; Waier, Solid,
Liquid
Date Collected
(MM/DD/YY)
Unpreserved
H2SO4
NaOH + Ascorbic
Na2S20

PJ
0
'd6. a
c a
Q
(P
.c
CS-
4\
r
Item Number..
1••
.
1:3
G= Grab, C = Composite ..
Sample Number
ETS Use Only
Maui%: Water, Sand,
Liquid
Date Collected
(MM/DD/YY)
Time Collected
(HH:MM)
# Containers
Unpreserved
H2SO4
HNO3
HCI
NaOH + Ascorbic