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NCG030657_2021 DMR_20210623
NCDEQ Division of Energy, Mineral and Land Resources StormwatenDischarge Monitoring Report (DMR) Form for NCG030000 Metal Fabrication Click here for instructions Complete sign scan and submit the DW1Rvia the within 3Odays ufreceiving sampling results. Mail the original, signed hard copy ufthe DIVIRtothe appropriate DEMLR Regional Office. Certificate of Coverage No. NCG03�6 �57 Person Collecting Samples: Paul W. Spangenberg, B.E.E. Facility Name: Matlab, Inc. - Plant 14 Laboratory Name: Con -Test Facility County: Randolph Laboratory Cert. No.: 652 Discharge during this period: N Yes E] No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions for any benchmark exceeclances? M Yes RNNo Analytical Monitoring Requirements for OutHa|bwith Industrial Activities — Benchmarks \n(Red) Code N/A Receiving Stream Class C C N/A Date Sample Collected MM/DD/YYYY 06/03/2021 06/03/2021 NCOIL New Motor/Hydraulic Oil Usage in N/A N/A gal/month 01051 Lead, total recoverable in mg/ L 78141 Total Toxic Organics (TTO) in mg/L(l) N/A N/A * Outfalls to Outstanding Resource Waters (ORW),High Quality Waters (HQW), Trout Waters (Tr)and Primary Nursery Areas(PNA) have a benchmark TSS limit of 50 mg/L All other water classifications have a benchmark of 100 mg/L. I Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachmentswere prepared under mydirection or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing vio}abonx."'~---_^~/~-�~~^ '� 7-:Z- Z1 Signature of PermitteeprDelegated Authprii-edkndividua| Date STORMWATER DISCHARGE OUTFALL (SDO) QUALITATIVE MONITORING REPORT Certification of Coverage No.: Facility Name: County: Permit No: NCG030657 Matlab, Inc. — Plant #14 Randolph Expires: 5/31/2021 Asheboro, North Carolina Inspector Name: Date of Inspection: Paul S an enber 11/12/20 OUTFALLDESCRIPTION` Outfall No.: Structure (pipe, ditch, etc.): Receiving Stream: 1 Ditch I Hasketts Creek Describe the industrial activities that occur within the outfall drainage area: Painting & Coating Manufacturing Color Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Lite Brown Odor Describe any distinct odors that the discharge may have (i.e. smells strongly of oil, weak chlorine odor, etc.): None Clarity Choose the number which best describes the clarity of the discharge where 1 is clear and 10 is very cloudy (circle one): 1 0 3 4 5 6 7 8 9 10 Floating Solids Choose the number which best describes the amount of floating solids in the stormwater discharge where 1 is no solids and 10 is the surface is covered in floating solids (circle one): 2 3 4 5 6 7 8 9 10 Suspended ended Solids Choose the number which best describes the amount of suspended solids in the stormwater discharge where 1 is no solids and 10 is extremely muddy (circle one): 1 3 4 -5 6 7 8 9 10 Foam Is there any foam in the stormwater discharge (circle one)?: Yes o Oil Sheen Is there an oil sheen in the stormwater discharge (circle one)?: Yes o Erosion Deposition ' Is there evidence of erosion or deposition at the outfall? (circle one): Yes a If yes, list and describe: Other . Is there other obvious indicators of stormwater pollution in the stormwater discharge (circle one): Yes o If yes, list and describe: Rain Event Was this a Representative Storm Event? X Yes _ No Total Event Precipitation (Inches}: 1.5 A measurable storm event is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. Certification By this signature I certify that this report is accurate and complete to the best of my knowledge: Inspector's Signature: ;vaae y 9ZI 613121 STORMWATER FACILITY INSPECTION FORM Facility Name: Location: Certification of Coverage No.:NCG030657 Matlab, Inc. — Plant #14 Asheboro, North Carolina Expires: 5/31/2021 Number of Inspector's Name: Date: Outfalls: 6/3/21 2 Paul Spangenberg Con$!Lb4t!ng Areas Evidence of pollutants entering system (circle one): Yes kNjo If yes, describe: Areas of potential pollutants entering system: Describe: Chemical and Waste storage buildings. Control measures present (circle one): Yeo No If yes, describe: Secondary containment Additional control measures needed (circle one): Yes No If yes, describe: Sediment and erosion control measures present (circle one): es No If yes, describe: Rip -Rap at discharge and drainages ditches Describe any new structural stormwater management measures: None Potential Pollutant Areas Describe any loading/unloading operations: Trucking, Tank Truck Describe any outdoor storage activities: Wood pallets, scrap metal, waste storage piles, municipal waste dumpsters, used equipment, used machinery, and painted equipment. Describe any outdoor manufacturing or processing activities: None Describe and dust or particulate generating areas: Dust collector area Describe any onsite waste disposal activities: None Significant s or Spills Any reportable spills or leaks in the past year (circle one): Yes No If yes, date: Impact on stormwater system(s): Certification By this signature I certify that this report is accurate and complete to the best of my knowledge: Inspector's Signature: ;yawe 7P.5A�_613121 ... .......... FACILITY:.Matiab, Inc. — Plant #14 ADDRESS: 1623 North Fayetteville Street Asheboro, NC 27203 CONTACT PERSON: Press Bower TELEPHONE: 336- 629-4161 YEAR MONTH DAY DATE 2021 6 3 HOURS MINUTES DURATION 24 0 PRECIP. AMOUNT (IN.) 1.50 RUNOFF VOL. (GAL.) 0.083 DAYS HOURS PRECEDING EVENT 6 0 PRINT I SIGNATURE I DATE Paul W. Spangenberg A r WO IV/ A;p VW I 3 Acres - Sq. Ft. 89775 x 1.5 = 134662.5 x 0.0833 =1 1217.3 x 7.48 = 83906.0 / 1000000 = 0.083 mg Boyer Enterprises East, LLC June 17, 2021 NCDEQ/DWR Attention: Central Files 450 West Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 Subject: STORMWATER SAMPLING RESULTS MATLAB, INC. - PLANT 14 1623 NORTH FAYETTEVILLE STREET ASHEBORO, RANDOLPH COUNTY, NORTH CAROLINA PERMIT NCG030657 Dear Sir/Madam: Attached please find the Stormwater Discharge Monitoring Reports (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 and 002 on June 3, 2021 and analyzed for total suspended solids (TSS) pH, lead (Pb), copper (Cu), zinc, (Zn), and oil and grease (O&G). As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at (919) 624-0630. Sincerely, BOYER ENTERPRISES EAST, LLC Paul W. Spangenberg EH&S Compliance DIRECTOR Attachments: Stormwater Discharge Monitoring Report Laboratory Report 127 Red Hill Church Road 919-971-0415 (24 Hrs.) Dunn, NC 28208 NCDEQ Division of Energy, Mineral and Land Resources rM&.. r • Metal Fabrication Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG03 0 6 5 7 Person Collecting Samples: Paul W. Spangenberg, B.E.E. Facility Name: Matlab, Inc. - Plant 14 Laboratory Name: Con -Test Facility County: Randolph Laboratory Cert. No.: 652 Discharge during this period: X Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes ❑ No If so, which Tier (I, II, or III)? Analytical Monitoring Requirements for Outfalls with industrial Activities — Benchmarks in (Red) Parameter Code Parameter Outfall 1 Outfall2 Outfall Outfall Outfall N/A Receiving Stream Class C C N/A Date Sample Collected MM/DD/YYYY 06/03/2021 06/03/2021 46529 24-Hour Rainfall in inches 1.5 1.5 00552 Non -Polar Oil & Grease in mg/L (15) <0.33 0.70 C0530 TSS in mg/L (100 or 50*) 25 26 00400 pH in standard units (6.0-9.0) 6.3 7.0 NCOIL New Motor/Hydraulic Oil Usage in N/A N/A gal/month 01119 Copper, total recoverable in mg/L 0.0094 0.013 (0.010 FW, 0.005 SW) 01051 Lead, total recoverable in mg/ L t}.�QQ7g �.��7 (0.075 FW, 0.220 SW) 01094 Zinc, total recoverable in mg/ L (0.126 a.o42 �.L142 FW, 0.095 SW) 78141 Total Toxic Organics (TTO) in mg/L(1) N/A NIA * Qutfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L. Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee or Delegat—ed Authorized Individual Date Boyer Enterprises East, LLC MEC June 17, 2021 Attention: Central Files 450 West Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 Subject: STORMWATER SAMPLING RESULTS MATLAB, INC. - PLANT 14 1623 NORTH FAYETTEVILLE STREET ASHEBORO, RANDOLPH COUNTY, NORTH CAROLINA PERMIT NCG030657 Dear Sir/Madam: Attached please find the Stormwater Discharge Monitoring Reports (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 and 002 on June 3, 2021 and analyzed for total suspended solids (TSS) pH, lead (Pb), copper (Cu), zinc, (Zn), and oil and grease (O&G). As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at (919) 624-0630. Sincerely, BOYER ENTERPRISES EAST, LLC Paul W. Spangenberg EH&S Compliance DIRECTOR Attachments: Stormwater Discharge Monitoring Report Laboratory Report 127 Red Hill Church Road 919-971-0415 (24 Hrs.) Dunn, NC 28208 NCDEQ, division of Energy, Mineral and Land Resources Metal Fabrication Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG03 0 6 5 7 Person Collecting Samples: Paul W. Spangenberg, B.E.E. Facility Name: Matlab, Inc. - Plant 14 Laboratory Name: Con -Test Facility County: Randolph Laboratory Cert. No.: 652 Discharge during this period: M Yes ❑ No (if no, skip to signature and dote) Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes R No If so, which Tier (I, II, or III)? Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Code parameter Outfall 1 Outfall2 Outfall Outfall Outfall N/A Receiving Stream Class C C N/A Date Sample Collected MM/DD/YYYY 06/03/2021 06/03/2021 46529 24-Hour Rainfall in inches 1.5 1.5 00552 Non -Polar Oil & Grease in mg/L (15) <0.33 0.70 C0530 TSS in mg/L (100 or 50*) 25 26 00400 pH in standard units (6.0-9.0) 6.3 7.0 NCOIL New Motor/Hydraulic Oil Usage in NIA NIA gal/month 01119 Copper, total recoverable in mg/L 0.0094 0.013 (0.010 FW, 0.005 SW) 01051 Lead, total recoverable in mg/ L O.a007g O.pp16 (0.075 FW, 0.220 SW) 01094 Zinc, total recoverable in mg/ L (0.126 0.02 0.042 FW, 0.095 SW) 78141 Total Toxic Organics (TI-O) in mg/L(1) N/A N/A * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L. Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee or Delegated Authorized Individual 2.Z Date con-test(3 A Pace Analytical® Laboratory 39 Spruce Street * East Longmeadow, MA 01028 * FAX 4131525-6405 * TEL, 413/525-2332 June 17, 2021 Paul Spangenberg Boyer Enterprises East, LLC PO Box 550 Dunn, NC 28208 Project Location: Plant 14- Asheboro, NC Client Job Number: Project Number: R2943. 10 Laboratory Work Order Number: 2 IF0250 Enclosed are results of analyses for samples received by the laboratory on June 3, 2021. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Table of Contents I Page 1 of 16 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 21F0250-01 21F0250-02 Sample Preparation Information QC Data Metals Analyses (Total) B283398 Conventional Chemistry Parameters by EPAJAPHAJSW-846 Methods (Total) B283390 B283438 B283886 F1agJQualifier Summary Certifications Chain of CustodyJSaraple Receipt 3 4 5 5 7 9 10 10 10 11 11 11 11 12 13 14 I Page 2 of 16 Table of Contents OPAm colrtest'9 A Pace AnalyticalO Laboratory 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Boyer Enterprises East, LLC PO Box 550 Dunn, NC 28208 ATTN: Paul Spangenberg PURCHASE ORDER NUMBER: PROJECT NUMBER: R2943.10 ANALYTICAL SUMMARY REPORT DATE: 6/17/2021 WORK ORDER NUMBER: 21F0250 The results of analyses performed on the following samples submitted to CON -TEST, a Pace Analytical Laboratory, are found in this report PROJECT LOCATION: Plant 14- Asheboro, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB 21F0250-01 Water EPA 1664B SM21-22 2540D SM21-22 4500 H B SW-846 6020B 2 21F0250-02 Water EPA 1664B SM21-22 2540D SM21-22 4500 H B SW-846 6020B I Page 3 of �16 co n -te 7 fit© A Pace AnalyticalO Laboratory Table of Contents 39 Spruce Street * East Longmeadow, MA 01026 * FAX 413t525-6405 * TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. SM21-22 4500 H B Qualifications: H-05 Holding time was exceeded. pH analysis should be performed immediately at time of sampling. Nominal 15 minute holding time was exceeded Analyte & Sainples(s) Qualified: PH 2IF0250-01[l], 2 1 F0250-02[21, B283390-DUP1 The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Technical Representative Page 4 of 16 Table of Contents con -test A Pace AnalyticaP Laboratory 39 Spruce Street . East Longmeadow, MA 01028 . FAX 413/525-6405 ' TEL. 413/525-2332 Project Location: Plant 14- Asheboro, NC Sample Description: Work Order: 21F0250 Date Received: 6/3/2021 Field Sample #: 1 Sampled: 6/3/2021 13:00 Sample ID: 21F0250-01 Sample Matrix: Water Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Copper 0.0094 0.0010 0.00027 mg/L I SW-846 6020B 6/4/21 6/8/21 13:22 QNW Lead 0.00079 0.00050 0.00014 mg/L 1 SW-8466020B 6/4/21 6/8/2113:22 QNW Zinc 0.042 0,010 0.0034 mg/L 1 SW-8466020B 6/4/21 6/8/2113:22 QNW Page 5 of 16 Table of Contents con-testo A Pace Analytical® Laboratory 39 Spruce Street * East Longmeadow, MA 01028 * FAX 4131525-6405 * TEL. 413/525-2332 Project Location: Plant 14- Asheboro, NC Sample Description: Work Order: 21F0250 Date Received: 6/3/2021 Field Sample k 1 Sampled: 6/3/2021 13:00 Sample ID: 21F0250-01 Sample Matrix: Water Conventional Chemistry Parameters by EPA/AP1IA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst PH @19.2°C 6.3 pH Units 1 H-05 SM21-22 4500 H B 6/4/21 6/4/21 18:00 ALG Total Suspended Solids 25 2.0 0.64 mg/L I SM21-22 2540D 6/7/21 6/7/21 12:45 LL Oil & Grease (HEM) ND 1.4 0.33 mg/L 1 EPA 1664B 6/14/21 6/14/21 13:00 LL Page 6 of 16� Table of Contents con -test@ A Face Anaty#icaP Laboratory 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Plant 14- Asheboro, NC Sample Description: Work Order: 21F0250 Date Received: 6/3/2021 Field Sample #: 2 Sampled: 6/3/2021 13:00 Sample ID: 21F0250-02 Sample Matrix: Water Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Copper 0.013 0.0010 0.00027 mg/L 1 SW-846 6020B 6/4/21 6/8/21 13:25 QNW Lead 0.0016 0.00050 0.00014 mg/L 1 SW-846 6020B 6/4/21 6/8/21 13:25 QNW Zinc 0.042 0.010 0.0034 m9/L 1 SW-846 6020E 6/4/21 618/21 13:25 QNW Page 7 of 16 1 Table of Contents con -testa A Pace AnatyficaP Laboratory 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-8405 * TEL. 413/525-2332 Project Location: Plant 14- Asheboro, NC Sample Description: Work Order: 21F0250 Date Received: 6/3/2021 Field Sample #P: 2 Sampled: 6/3/2021 13:00 Samale ID: 21F0250-02 Samale Matrix: Water Conventional Chemistry Parameters by EPA/APHA/SW--846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst pH@19.1°C 7.0 pH Units 1 H-05 SM21-224500HB 6/4/21 6/4/2118:00 ALG Total Suspended Solids 26 2.0 0,64 mg/L 1 SM21-22 2540D 6n121 6/7/21 12:45 LL Oil & Grease (HEM) 0.70 1.4 0.33 mg/L 1 J EPA 1664B 6/14/21 6/14/21 13:00 LL Page 8 of 16 Table of Contents con -test A Pace AnatyticalO Laboratory 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Sample Extraction Data EPA 1664B Lab Number [Field ID] Batch Initial [mL] Date 21F0250-01 [1] B283886 1000 06/14/21 21F0250-02 [21 B283886 1000 06/14/21 SM21-22 2540D Lab Number [Field ID] Batch Initial [mL] Date 21F0250-01 [11 B283438 250 06/07/21 21FO250-02 [2] B283438 250 06/07/21 SM21-22 4500 H B Lab Number [Field ID] Batch Initial [mL] Date 21FO250-01[11 B283390 50.0 06/04/21 21F0250-02 [21 B283390 50.0 06/04/21 Prep Method: SW-846 3005A Analytical Method: SW-846 6020E Lab Number [Field ID] Batch Initial [mL] Final [mL1 Date 21F0250-01[1] B283398 50.0 50.0 06/04/21 21F0250-02 [2] B283398 50.0 %0 06/04/21 Page 9 of 16� Table of Contents 00 n-testa A Pace Anafytical® Laboratory 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413l525-6405 * TEL. 413l525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B283398 - SW-846 3005A Blank(B283398-BLKI) Prepared: 06/04/21 Analyzed: 06/08/21 Copper ND 0.0010 mg/L Lead ND 0.00050 mg/L Zinc ND 0.010 mg/L LCS (B283398-BSI) Prepared: 06/04/21 Analyzed: 06/08/21 Copper 1.00 0.010 mg/L 1.00 100 80-120 Lead 0.535 0.0050 mg/L 0.500 107 80-120 Zinc 1.07 0.10 mg/L 1.00 107 80-120 LCS Dup (B283398-BSDI) Prepared: 06/04/21 Analyzed: 06/08/21 Copper 1.00 0.010 mg/L 1.00 Lead 0.533 0.0050 mg/L 0.500 Zinc 1.06 0.10 mg/L 1.00 100 80-120 0.282 20 107 80-120 0.431 20 106 80-120 1.15 20 Page 10 of 16 Table of Contents con -test° A face AnalyticaP Laboratory 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) .. Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B283390 - SM21-22 4500 H B LCS (B283390-BSI) Prepared & Analyzed: 06/04/21 PH Duplicate (B283390-DUPI) 6.00 pH Units Source: 21FO250-02 6.00 99.9 90-110 Prepared & Analyzed: 06/04/21 pH Batch B283438 - SM21-22 2540D 7.0 pH Units 7,0 0.158 5 H-05 Blank (B283438-BLKI) Prepared & Analyzed: 06/07/21 Total Suspended Solids LCS (B283438-BSI) 1.5 2.5 mg/L ,1 Prepared&Analyzed: 06/07/21 Total Suspended Solids Batch 11283886 - EPA 1664B 192 10 1119/1, 200 96.0 53.8-124 Blank (B283886-BLKl) Prepared & Analyzed: 06/14/21 Oil & Grease (ITEM) LCS (B283886-BS1) ND 1.4 mg/L Prepared & Analyzed: 06/14/21 Oil & Grease (HEM) 22 mg/L 20.0 110 78-114 Page 11 of 16 Table of Contents con"" test A Pace Analytical' Laboratory 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALrPIER SUMMARY QC result is outside of established limits. fi Wide recovery limits established for difficult compound. Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quarnitation (LOQ) DL Detection Limit is the lower Emit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. H-05 Holding time was exceeded. PH analysis should be performed immediately at time of sampling. Nominal 15 minute holding time was exceeded. I Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). I Page 12 of 16 Table of Contents con#testio A Pace AnalyticalO Laboratory 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included In this Report Analyte Certifications EPA 1664E in Water Oil & Grease (HEM) SM21-22 2540D in Water Total Suspended Solids SM21-22 4500 HB in Water PH SW-846 6020B in Water C T,MA,NH,NY,RI,NC,ME, VA CT,MA,NH,NY,RI,NC,ME, VA CT,MA,RI Copper CYNH,NY,ME, VA,NC Lead CT,NH NY,ME,VA,NC Zinc CTNH,NY,ME,VA,NC Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2017 100033 03/1/2022 MA Massachusetts DEP M-MA100 06/30/2022 CT Connecticut Department of Publilc Health PH-0165 12/31/2022 NY New York State Department of Health 10899 NELAP 04/l/2022 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2022 RI Rhode Island Department of Health LA000112 12/30/2021 NC North Carolina Div. of Water Quality 652 12/31/2021 NJ New Jersey DEP MA007 NELAP 06/30/2021 FL Florida Department of Health E871027 NFLAP 06/30/2021 VT Vermont Department of Health Lead Laboratory LL720741 07/30/2022 ME State of Maine MA00100 06/9/2023 VA Commonwealth of. Virginia 460217 12/14/2021 NH-P New Hampshire Environmental Lab 2557 NELAP 09/&2021 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2021 NC-DW North Carolina Department of Health 25703 07/31/2021 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2022 MI Dept. of Env, Great Lakes, and Energy 9100 0916/2021 Page 13 of 16 1 Table of Contents 4r: x E S! 10 0 vIi It 0 r " -j it 01 a j S U" L-7 — E Z, 60 9 It 16 In IA 0 K I— v W 15 —1 -T g El in J29 E D -Oc to uz X vt -o 0 c a; qd z z -Z- SSI x rs x ;B 0 JL11 11 11 rn D 13 0 x u 14 x . . . . . . . . . . w -j 421 ID El F7 ED Ip X X X >1 CD 4CI O In 01 !:4 10 10 kd a 0 F� 7 in Q a 8 8 8 1: W& aw. 0 IN OIE� 0. 0. 0. I TOM 41 E E .9 � a .5 Am 14 of 16 Table of Contents Travel History TIME Z0"9 Local Scan Time Friday, June 4,2021 9:38 AM 8:33 AM 8:25 AM 7:00 AM 3:53 AM TRACK ANOTHER SHIPMENT 411359783416 ADD NICKNAME . Delivered Friday, June 4) 2021 at 9.38 am WINDSOR LOCKS, CT WINDSOR LOCKS, CT FAST GRANBY, CT MEMPHIS, TN Thursday, June 3,2021 11:13 PM MEMPHIS. TN 5:06 PM GREENSBORO, NC 4D0 PM ASHEBORO, NC Shipment Facts TRACKING NUMBER 411359783416 DELIVERED Signed for by: R.PIETRAS GET STATUS UPDATES OBTAIN PROOF OF DELIVERY Delivered On FedEx vehicle for delivery At local FedEx facility At destination sort facility Departed FedEx location Arrived at FedEx location Picked up Picked up Tendered at FedEx office SERVICE FedEx Priority Overnight WEIGHT 33.4 Ibs / 15.15 kgs M SS/ I Page 15 of 16 Table of Contents I % I Have Not Confirmed Sample Container Numbers With Lab Staff Before Relinquishing Over Samples All= . . . . . . . . . . . . . . . . . . . . . ............. .11-7:06i -7 ...... . ....... .. ....... ... Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client Q Received � it Date 14-2,1 Time AN On Ice I No Ice Ambient Melted Ice Were samples within By Gun # Actual Temil:!::, Temperature? 2-60C Y By Blank # Actual Temp - Was Custody Seat Intact? PJ Pt Were Samples Tampered with? Was COC Relinquished ? M - Does Chain Agree With Samples? 7 Are there broken/leaking/loose caps on any samples? F Is COC in ink/ Legible? I Were samples received within holding time? T- Did COC include sit Client 1 Analysis Sampler Name pertinent Information? Project 7- ID's Collection Dates/Times Are Sample labels filled out and legible? T- Are there Lab to Filters? f: Who was notified? Are there Rushes? Are there Short Holds? Is there enough Volume? Is there Headspace where applicable? Proper Media/Containers Used? Were trip blanks received? Do all samples have the proper pH? How were the samples In Cooler -r No Cooler received? Direct from Sampling F Who was notified? Who was notified? MS/MSD?— ',r- Is splitting samples required? On COC? 1; Acid 3: Base Page 16 of 16