WQ0006101_Renewal Application_20210621

Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional
information.)*
r Yes r No
Permit Number (IR)*
WQ0006101
Applicant/Permittee
City of Dunn
Applicant/Permittee Address
PO Box 1065 Dunn, NC 28335
Is the owner in BIMS? r Yes r No
Is the facility in BIMS? r Yes r No
Owner Type
Municipal
Facility Name
City of Dunn RLAP
County
Harnett
Fee Category Major
Fee Amount $0
Is this a complete
application?*
r Yes r No
Complete App Date 06/21/2021
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review bythe hydrogeologist?* r Yes r No
Regional Office
CO Reviewer
Admin Reviewer
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other
.......................................................... electronic surece, aner correspondence.
_ -
Name * Drew Matthews
Email Address*
[e-mail]
Project Information
........ .................................................................................................................................................. .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
2528839301
O Modification - Minor
G Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
r Wastewater Irrigation
r High -Rate Infiltration
r Other Wastewater
r Reclaimed Water
r Closed -Loop Recycle
r Residuals
r Single -Family Residence Wastewater
r Other
Irrigation
Permit Number:*
W00006101
Fbs Current Existing permt number
Applicant/Permittee *
City of Dunn
Applicant/Permittee Address*
PO Box 1065 Dunn, NC 28335
Facility Name *
City of Dunn RLAP
Please provide comments/notes
on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Spec'rfications, Calculations, Rc.)
2021 City of Dunn RLAP Permit Renewal.pdf 30.5MB
upload only 1 RCF docurrent (less than 250 M3). Matiple documents nest be combined into one RDF file unless file is larger than
upload limit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Ot w e3'/Ga&Ai mv
Submission Date 6/21/2021

CITY OF DUNN
2021 PERMIT RENEWAL
CLASS B PROGRAM
WQ0006101
Submitted by:
Soil Plus
PO Box 1396
Oxford, North Carolina 27565
June 21, 2021
SOIL PLUS

SOIL PLUS
June 21, 2021
NCDEQ-DWR
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attention: Mr. Nathaniel Thornburg
Reference: PERMIT RENEWAL
City of Dunn Residual Biosolids "Class B" Program
Permit # WQ0006101
Mr. Thornburg:
Soil Plus, LLC (Soil Plus) is submitting one electronic copy of this permit renewal
application package for the City of Dunn (WQ0006101). This package includes:
1. Completed Residual Land Application Program Application (RLAP)
• Weighted PAN Calculations
• O&M Plan
2. Completed Residual Source Certification Attachments (RSCA)
• Field Loading Calculation Sheet
• Analytical
3. Completed Land Application Site Certification Attachment (LASCA)
• RENEW Sites CU-34 and HA-08
• DELETE Sites CU-10/HA-201/HA-307/SA-19
Soil Plus will be responsible for completing this permit renewal for the City of Dunn. If
there is any further information required or questions regarding this permit application,
please do not hesitate to contact me for assistance.
Respectfully,
Drew Matthews, Soil Plus
cc: Heather Adams, City of Dunn
Jason Smith, Granville Farms
PO Box 1396
Oxford, NC 27565
[phone]
dmatthewsgsoilplus. ne t
www.soilplus.net

City of Dunn
2021 Class B
Permit Renewal
WQ0006101
Dunn, NC
Residual Land
Application Program
Weighted Source PAN Calculations
O&M Plan
Residual Source
Certification
Field Loading Calculations
Analytical Data
Land Application Site
Certification
Land Owner Agreement Forms
Maps
Biosolid Utilization
CPLR Summary

APPENDIX 1
2021 PERMIT RENEWAL
City of Dunn (VQ0006101)
Weighted PAN Calculations
O&M Plan

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM
FORM: RLAP 06-16
L APPLICANT INFORMATION:
1. Applicant's name: City of Dunn
Applicant type: ❑ Individual Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal 17I State ® Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Heather Adams Title: Public Utilities Director
Applicant's mailing address: PO Box 1065
City: Dunn State: NC Zip: 28335-
Telephone number: [phone] Email Address: hadamskdunn-nc.org
2. Consultant's name: Drew Matthews License Number (for P.E.):
Affiliation: ❑ On Staff ® Retained (Firm: Soil Plus, LLC)
Consultant's mailing address: PO Box 1396
City: Oxford State: NC Zip: 27565-
Telephone number: [phone] Email Address: dmatthewsksoilplus.net
3. Agronomist's name: License Number:
Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: )
Agronomist's mailing address:
City: State: Zip: -
Telephone number: (_) _- Email Address:
4. Soil Scientist's name: License Number:
Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: )
Soil Scientist's mailing address:
City: State: Zip: -
Telephone number: (_) _- Email Address:
5. Fee submitted: $0.00 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00006101
Date of most -recently issued permit: October 13, 2016
Date of most -recently certified Attachment A (if different than the permit):
Date of most -recently certified Attachment B (if different than the permit): July 8, 2020
FORM: RLAP 06-16 Page 1 of 5

III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: Multiple Facilities/See O&M Plan
City:
Coordinates: Latitude: °
Datum:
Method of measurement:
State: Zip:.
Longitude:
Level of accuracy:
2. County where residuals land application program is headquartered: Harnett
3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Jason A. Smith
Granville Farms, Inc.
13266
Back -Up ORC
Drew A. Matthews
Soil Plus, LLC
1003075
Additional Back -Up
ORCs
(if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the
candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school
and certification test:
4. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in the
following table:
Maximum amount of residuals to be certified: 650 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
21.71
24.70
14,114
16,058
Five -Year Maximum Adjusted
32.51
34.76
21,131
22,595
b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and
proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
Row Crops
Hay
67.0
Pasture
67.0
Total:
67.0
Methods
Surface
67.0
Incorporation or Injection
Total:
67.0
FORM: RLAP 06-16 Page 2 of 4

c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Application Rate
(lbs PAN/ac yr)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
50
282.28
321.15
422.61
451.89
100
141.14
160.58
211.31
225.95
150
94.09
107.05
140.87
150.63
200
70.57
80.29
105.65
112.97
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction
practices not in place, etc.): The City of Dunn's WTP and WWTP are also listed sources on Granville Farms, Inc. Class B
Permit W00002890 should additional acreage be required for land application
7. Specify type of residuals program (See Instruction F): 0 Non -dedicated ❑ Dedicated
If Dedicated, specify the following (check all that apply):
❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic
rates, explain;
❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain;
❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation
facilities fed through a fixed supply system, explain;
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the following Residuals Source Certification and all associated documentation.
L
i
Residuals Source
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land Applications Site Certification and all associated documentation.
RA
Land Application Siite
Certification.doc
FORM: RLAP 06-16 Page 3 of 4

Applicant's Certification (signing authority roust he in compliance with 15A NCAC 02T .0106):
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ❑ No, Explain;
I, Heather Adams Public Utilities Director
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for City of Dunn
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if ail required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: Date: F 4
FORM: RLAP 06-16 Page 4 of 4

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CITY OF DUNN
OPERATION AND MAINTENANCE PLAN
LAND APPLICATION OF CLASS B RESIDUAL BIOSIOLIDS
WQ#0006101
Revised June 2021

1.0 ANALYTICAL REQUIREMENTS
Prior to the hauling and land application event being schedule the generator must provide analytical results
documenting that all parameters listed in Condition IV. 2 — 4 and at the frequency listed in most recent copy of this
permit. The City of Dunn will collect the sample prior to land application and will be done in the following manner:
Four factors that may ultimately affect the integrity of reported data include: 1) obtaining a representative sample, 2)
preventing contamination of the sample, 3) providing legal documentation of the sampling event, and 4) protecting
the sample from chemical, physical or biological change prior to analysis.
A sample will be collected according to the schedule provided in the most recent copy of the Attachment of this
permit and prior to land application one composite sample should be pulled from a designated location from the
generating source. The City of Dunn has identified Meritech, Inc. in Reidsville, NC to be used as the Certified
Laboratory. The composite sample should be analyzed for:
• % Solids,
• Nitrogen Series (TKN, Ammonia, Nitrate, Nitrite, and Organic Nitrogen),
• Phosphorus,
• Potassium,
• Sulfur,
• Calcium,
• Magnesium,
• Sodium,
• Iron,
• Aluminum,
• Manganese,
• Copper,
• Zinc,
• and Remaining 503 Metals (i.e. Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel,
Selenium)
Approximately 2 quarts of residual should be collected. The sample containers should be clean and sterile. They
should also be labeled so that they are easily identifiable in the lab. The samples should be pulled using the method
listed below:
❖ Collect one sample from each holding tank(s) from which the material will be land applied using a "swing
sampler"
o The swing sampler must be used with a sterile, plastic 960 ml container
❖ Combine each sample in a stainless steel bucket
❖ Mix thoroughly using a fiberglass rod
❖ Collect each sample from the top of the access point at each holding tank. This access point is obtained by
climbing the installed ladder on the side of the holding tank.
Once the sample is pulled, it should be placed in medium size cooler packed with ice. The sample should be collected
with an enough time so that it can be delivered to the laboratory.
Revised 06/21 OCity of Dunn Operation and Maintenance Plan

Once per calendar year a sample should be collected and submitted to Meritech, Inc. in Reidsville, NC. This sample
should be analyzed for:
• Full TCLP
• Ignitability, Corrositivity, and Reactivity
• Requires 5 Liters (In Opac Glass Bottles)
A third should be submitted to Meritech, Inc. for Fecal Coliform Density Test to meet Pathogen Compliance (WWTP
ONLY). This sample would be analyzed for:
• Fecal Coliform Density Test (seven pint samples)
The City of Dunn will use 38% Volatile Solids Reduction to meet Vector Attraction Reduction (WWTP ONLY).
These samples will be performed in house at City of Dunn's WWTP Laboratory.
The contact information for the labs is:
Mailing Address
Meritech, Inc.
642 Tamco Road
Reidsville, NC 27320
[phone] (phone)
[phone] (fax)
Sampling frequency will be conducted in accordance with the Table listed in the most recent Attachment A of this
permit. The sample will be collected by a representative of Soil Plus, LLC. For further information please contact:
Drew Matthews
PO Box 1396
Oxford, NC 27565
252-883-9301
Revised 06/21 OCity of Dunn Operation and Maintenance Plan

2.0 BIOSOLIDS REMOVAL, TRANSPORT, AND APPLICATION
Biosolids will be transported from the generators to suitable, permitted land application sites. Transport equipment
will be inspected, licensed and appropriately marked, as required, for the purpose of transporting biosolids. Biosolids
will be delivered to the application sites between sunrise to sunset.
Both liquid and dewatered biosolids distribution on the land application sites will be uniform throughout the
application area. To ensure adequate control of the application rate for each site, the equipment used for spreading
the sludge will be calibrated by measuring the amount handled on a known square footage. While the rate of discharge
from the application vehicle is fixed, the speed of the equipment can be adjusted to maintain the flow rate needed to
achieve specific application rates. Spreading operations will be discontinued during periods of inclement weather and
will not be resumed until sufficient drying of the fields has occurred. This allows equipment access without causing
excessive soil compaction or rutting. To prevent adherence of the biosolids, transport vehicles will be equipped with
rear mud flaps, thereby preventing biosolids from being tracked onto roadways. Biosolids adhering to the mud flap
will be scraped off in the field before the truck returns to the roadway. Examples of our application tracking and
summary form/reports can be provided upon request.
3.0 SITE OPERATION
Biosolids will be surface applied at the properly -calculated agronomic rate and in strict accordance with any state and
federal regulations for the land application of the biosolids. Buffer zone distances will be observed in accordance with
applicable state and federal regulations. Buffer zones will be flagged and no biosolids will be applied within those
areas. The most restrictive buffer will apply in combined situations. Operational provisions will be taken to prevent
soil loss through erosion. Provisions will include contour application and avoidance of areas where surface drainage
patterns result in concentrated flow of runoff from rainfall. In accordance with sound, industry standard agronomic
practice, areas which are unseasonably wet (and would produce rutting or damage to the field) will not be utilized for
biosolids application operations during those periods. Operations will be discontinued when soils are saturated and
will not be resumed until the field has sufficient dried. The amount of biosolids applied will not exceed the hydraulic
capacity of the soil at the time of each application. If a subsequent pass across a field is necessary to achieve the
desired application rate, sufficient drying time will be allowed between passes.
4.0 PROJECT CONTROL
To ensure biosolids are continuously applied at the correct application rate and in a manner consistent with the
Operations Plan, a Field Manager (provided by the contracted land application company) will be in direct charge of
the field operations, controlling the amount of biosolids delivered to each field, and conducting daily field inspections.
Field inspections will include ensuring that flags are in place, biosolids are applied uniformly at the designated
application rate, setbacks are observed, trucks are unloading at best location, trucks are not driving over biosolids,
trucks are cleaned before leaving the field and the land application equipment is maintained in working condition.
5.0 TRANSPORTATION SYSTEM ROUTING
Per the specifications, transportation vehicles will be equipped with GPS devices that will guide drivers to the land
application sites. Transportation routes will follow primary highways and avoid residential areas where possible.
Designated routes are followed unless a detour is specified. In the event of a detour route, it shall be taken as specified
by the detour authority. There shall be no unscheduled stops when loaded. Transportation vehicles will be inspected,
licensed and appropriately marked as required with identification numbers for the purpose of this contract. All units
will be equipped with spill guards and full mud flaps. This will prevent the biosolids from adhering to the tires and
undercarriage of the transport vehicle, thereby preventing biosolids from being tracked onto roadways. Biosolids
adhering to the mud flap will be scraped off in the field before the truck returns to the roadway. All federal OSHA
Revised 06/21 OCity of Dunn Operation and Maintenance Plan

and DOT laws and regulations are complied with for the protection of our clients, the community and our drivers.
Examples of vehicle and driver transportation logs and inspection forms can be provided upon request.
6.0 DEWATERED BIOSOLIDS
Dewatered biosolids will be transported in standard end dump trailers. The tankers will be loaded per the generator's
specifications and standard protocols. The aluminum dump trailers used for transportation of dewatered cake
biosolids will be equipped with sealed tailgates and will be completely sealed to prevent leakage. All trucks will be fully
covered and will be fitted with positive lock tailgates.
7.0 LIQUID BIOSOLIDS
Liquid biosolids will be transported using liquid tankers pulled by standard road tractors, or pumper trucks. The
tankers and pumper trucks will be loaded per the generator's specifications and standard protocols. The
tractor/tanker unit will transport its load to a designated staging area inside the buffered area of a permitted land
application site.
8.0 APPLICATION (SPREADING) — DEWATERED BIOSOLIDS
At the staging area each load will be unloaded in a designated area within the land application site. Biosolids will be
loaded into our Side Slinger cake box by a front-end loader. This unit is capable of delivering an accurate, calibrated
application of dewatered biosolids over the application site. The uniform spread pattern ensures that biosolids are
applied at proper agronomic (nutrient) and hydraulic loading rates. The application rates for each site, and its
corresponding crop, will be determined based on the Plant Available Nitrogen (PAN) content of the biosolids, or
other limiting factors. Typical applications will deliver between 75 and 100 percent of a crop's annual PAN
requirement.
9.0 APPLICATION (SPREADING) — LIQUID BIOSOLIDS
At the staging area each load will be transferred into a 4,000 gallon capacity pull behind subsequent land application.
This unit is capable of delivering an accurate, calibrated application of liquid biosolids over the application site. The
uniform spread pattern ensures that biosolids are applied at proper agronomic (nutrient) and hydraulic loading rates.
The application rates for each site, and its corresponding crop, will be determined based on the Plant Available
Nitrogen (PAN) content of the biosolids, or other limiting factors. Typical applications will deliver between 75 and
100 percent of a crop's annual PAN requirement.
10.0 SPILL AND EMERGENCY RESPONSE PROGRAM
In the unlikely event of a spill, the City of Dunn will take the following actions immediately.
• Halt Source of Spill. Use of any leaking or damaged unit which is causing the spill will cease immediately. The
unit will be repaired before resuming its use.
• Contain Spill. In the event large quantities of biosolids have been spilled, straw bales will be used where
available and as necessary to either form a barrier or absorb biosolids.
• Clean -Up. Depending on the type and amount of biosolids spilled, a variety of equipment may be used to
remove the biosolids: front-end loader, shovels and brooms and vacuum equipment of a liquid biosolids
applicator. Any biosolids removed from the spill site will be spread on an approved application site, returned
to the WWTP, or disposed of in an approved landfill.
Revised 06/21 ©City of Dunn Operation and Maintenance Plan

• Final Clean -Up. Flush roadways with water or sweep as necessary to clean. Allow to dry and incorporate if
spill occurs on non -paved and tillable area. In the event a spill occurs on private property, final clean-up
should be completed immediately to the satisfaction of the owner.
• Management of Clean -Up Efforts. The Operations Manager will take immediate charge and initiate clean-up
activities. The Contract Land Applier along with the City of Dunn labor will be used, with additional labor
secured as needed. The Operations Manager will also communicate with the public on the scene, answering
questions and advising of clean-up activities.
• Reporting. All spills will be reported immediately to the City of Dunn officials. State and local agencies will
be notified in accordance with their notification requirements. Within 24 hours of the spill, the Operations
Manager will send the City of Dunn a written report detailing how the spill occurred and remedial action
taken. This report will be provided using the enclosed Spill Report form.
• Spill Prevention. The Operations Manager will implement the following spill prevention measures:
o Ensure truck drivers watch trailer while loading and do not overload;
o Ensure trailer hatches are closed and latched while transporting;
o Ensure trailer seals are inspected on a daily basis and replaced as necessary; and
o Ensure unloading operations in the field are conducted to minimize any potential runoff or tracking.
The City of Dunn require that the Contract Land Applier shall ensure that all employees receive safety and spill
response training as part to their new hire training and thereafter participate in our monthly safety and spill response
training program. In addition to their internal training and protocols, they must also contract with a regional
emergency response firm - HEPACO - available to respond to an incident in the Central and Eastern North Carolina
area within two hours. A copy of our agreement with HEPACO can be provided upon request.
Names and Titles of Inspection Personnel
Andy Smith, Area Supervisor
Jason Smith, Area Supervisor
JT Bryant, Regional Supervisor
Jay Bryant, Project Supervisor
Matt Foster, Project Supervisor
Jeff Bumpass, Field operators
Curtis Riggs, Field operators
Mark Hurley, Field operators
11.0 PREVENTION
The goal of a compliance assurance system is to prevent compliance issues from occurring. Prevention involves:
• Ensuring personnel understand their role in assuring compliance;
• Identifying compliance requirements at the federal, state and local levels;
• Implementing a system where compliance tasks are scheduled, assigned and tracked to completion;
• Developing standard operating procedures where appropriate; and
• Reviewing the compliance task list and standard operating procedures on an ongoing basis and modifying
them as appropriate to account for changes in regulations/requirements and operating methods, and to
address compliance deficiencies.
Revised 06/21 OCity of Dunn Operation and Maintenance Plan

12.0 STANDARD OPERATING PROCEDURES (SOP's)
The City of Dunn will direct the Contract Land Applier to develop and implements SOPS to ensure compliance tasks
are completed consistently across the company. The SOP provides standard forms to use, approved biosolids
analytical methods, frequency of monitoring information, etc. Another key SOP relative to preventing compliance
issues from occurring is the use of a "Pre -Operating and Buffer Checklist".
The Pre -Operating and Buffer Checklist ensures federal, state and local regulations and permit requirements are met
prior to initiating biosolids applications at field sites. Compliance items on the Checklist include:
• The field is permitted and suitable for the biosolids/residuals type being applied;
• Pre -application requirements are met;
• Farmer and landowner agreements are current and the crop to be grown has been verified;
• The field is flagged to prevent applications in buffer zones and restricted areas;
• The appropriate application rate and field capacity is calculated; and
• Any special permit or local requirements are met.
• A listing of the buffer zones and restricted areas where biosolids/residuals cannot be applied
• A listing of operating requirements including notification requirements,
• application method requirements, and inclement weather operating requirements
13.0 ASSESMENT
To help ensure compliance requirements are being met and the compliance assurance system is implemented and
working, periodic, consistent, objective and documented assessments of the project/facility's compliance status are
conducted.
14.0 CORRECTIVE ACTION
Once compliance issues have been identified during the course of day to day business and through internal audits and
inspections a system must be in place which ensures that appropriate and timely corrective action is taken, the cause
of the compliance issue is identified and actions are taken to prevent recurrence of the issue.
The City of Dunn's goal is to have no instances of non-compliance. However, issues and incidents may occur and
when this happens employees work to correct the incident in a timely and thorough manner. When compliance issues
are identified, the situation is examined to determine the root cause of the problem and the corrective and preventive
action that must be taken. The preventive action must address the root cause with the goal of preventing a recurrence.
Depending on the nature of the compliance issue, it is assigned to one or more responsible parties to ensure that the
corrective and preventive actions are implemented. A deadline for completion of the task is assigned and the issue is
tracked to completion by regional and corporate compliance personnel.
15.0 TRAINING
An effective compliance training program involves:
• Identifying training needs and requirements;
• Assigning personnel to provide training and providing them the resources they need to conduct training;
• Documenting and tracking that mandatory t raining has occurred; and
• An employee's training needs and requirements, as well as their training responsibilities, are based on
his/her position within the company.
Revised 06/21 ©City of Dunn Operation and Maintenance Plan

Spill Response/Clean Up
THE FOLLOWING ACTIONS MUST BE TAKEN IN THE EVENT OF A SPILL
Halt the source of the spill: Ruptured line or valve, or damaged tank unit.
Contain spill: Use straw bales to form a barrier. Straw or hay bales can be obtained
from several sources for this purpose. Soil near the site can also be used to form a
barrier for containment.
Clean up: Use application equipment to recover as much of the material as possible.
After the application equipment has recovered as much material as possible, it will
be land applied as per the management plan. A temporary sump pit may be dug in
the containment area and spilled material washed into it to enhance recovery.
Final Clean up: Any unrecoverable material will be washed from road surfaces and
incorporated into an adjacent tillable area.
Notification: As soon as possible after a spill occurs notify:
City of Dunn
[phone]
Jason Smith, GFI -Vice President
[phone]
Department of Environmental Quality
Division of Water Resources
Fayetteville Regional Office
[phone]
Fire Department if assistance is required for wash down "911"
Highway Patrol if accident is on a public road "911"
Management of cleanup efforts: The field superintendent will take immediate
charge of the cleanup activities. Additional labor will be requested from the
groundwater recovery site and other departments as needed.
Reporting: Within 24 hours of a spill, the field superintendent will present a written
report detailing the cause of the spill and all actions taken in response to the spill.
The report will be sent to the NCDEQ Regional office having jurisdiction at the
location in which the release occurred.

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DUNN WATER TREATMENT PLANT
Quantitative Justification
YEAR DRY TONS
2017 131.15
2018 234.69
2019 134.72
2020 208.52
AVG DRY TONS 177.27

DUNN WWTP
Quantitative Justification
YEAR DRY TONS
2018 118.13
2019 118.30
2020 139.47
AVG DRY TONS 125.30

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SOURCE LOCATION MAP
Figure
Drawn by: DM
SOIL
PLUS
WQ0002890 O&M PLAN
Reviewed by:
Dunn, North Carolina
Date: Sept 2020
Soil Plus Project # 201702.A10

APPENDIX 2
2021 PERMIT RENEWAL
City of Dunn (VQ0006101)
RS CA
Field Loading Calculations
Analytical

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State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
l?ivision of hater Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: City of Dunn WT> f
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: IL Div. of Water Resources, Div. of Environmental Health,
or p Other (explain: PPM).
3. Facility contact person and title: Ian Stroud, Superintendent
Complete mailing address: PO Box 1065
City: = State: NC Zip: 28334-
Telephone number: M) 897-5129 E-mail address: dunnM �p dune-nc.org
4. Facility physical address: 805 West E Street
City: Erwin' State: IL Zip: 28339-
Coordinates: Latitude: b° 19' 27.2" Longitude: 78. 41' 17.9"
Datum: � Level of accuracy: Sub -Meter
Method of measurement: GIS
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes ® No
7. Facility permitted/design flow: 8_0 MGD and facility average daily flow: Wastewater Discharge — 0.349 MGD
8. Average amount of residuals being generated at this facility E dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Conventional WTP Process
Type and volume of residuals storage (i.e., outside of residuals treatment units): Uprox. 1.0 MG Lagoon
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological ® Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ® no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: P yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Summit Environmental Technologies, Inc. and Date of analysis: 8/21/2019
Passed corrosivity test: ;�j yes ❑ no. pH: 7.3 s.u. (2 < pH < 12.5)
Passed ignitability test: 0 yes F,1 no. Flashpoint: = OF (> 140°F)
Passed reactivity test: Eyes Mno. HCN: < 0.481 mg/kg (<250) & H2S: < 25.0 mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mg17)
Result
(mg17)
Arsenic
5.0
< 0.500
Hexachlorobenzene
0.13
< 0.100
Barium
100.0
<5.00
Hexachloro-1,3-Butadiene
0.5
<0.0400
Benzene
0.5
< 0.125
Hexachloroethane
3.0
< 0.200
Cadmium
1.0
< 0.100
Lead
5.0
< 0.500
Carbon Tetrachloride
0.5
< 0.125
Lindane
0.4
< 0.00500
Chlordane
0.03
< 0.0250
Mercury
0.2
< 0.00200
Chlorobenzene
100.0
< 1.25
Methoxychlor
10.0
< 0.00500
Chloroform
6.0
< 0.125
Methyl Ethyl Ketone
200.0
< 2.50
Chromium
5.0
< 0.200
Nitrobenzene
2.0
< 0.200
m-Cresol
200.0
< 10.0
Pentachlorophenol
100.0
< 0.500
o-Cresol
200.0
< 10.0
Pyridine
5.0
< 0.500
p-Cresol
200.0
< 10.0
Selenium
1.0
< 0.0500
Cresol
200.0
< 10.0
Silver
5.0
< 0.500
2,4-D
10.0
< 0.0100
Tetrachloroethylene
0.7
< 0.125
1,4-Dichlorobenzene
7.5
< 0.200
Toxaphene
0.5
< 0.0500
1,2-Dichloroethane
0.5
< 0.125
Trichloroethylene
0.5
< 0.125
1,1-Dichloroethylene
0.7
< 0.125
2,4,5-Trichlorophenol
400.0
< 0.500
2,4-Dinitrotoluene
0.13
< 0.100
2,4,6-Trichlorophenol
2.0
< 0.500
Endrin
0.02
< 0.00500
2,4,5-TP (Silvex)
1.0
< 0.00500
Heptachlor and its Hydroxide
0.008
< 0.00500
Vinyl Chloride
0.2
< 0.0500
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: hce Analytic and Date of analysis:
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
9.4
Cadmium
85
39
< 0.48
Copper
4,300
1,500
48
Lead
840
300
15
Mercury
57
17
< 0.4
Molybdenum
75
n/a
5.3
Nickel
420
420
16
Selenium
100
100
3.3
Zinc
7,500
2,800
77
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
W > 0 but < 25
30
200
210
19 > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: bee Analytical and Date of analysis: 4/6/2020
Parameter
Result
(mg1kg)
Aluminum
130,000
Ammonia -Nitrogen
230
Calcium
1,100
Magnesium
1,700
Nitrate -Nitrite Nitrogen
15.1
pH (Standard Unit)
6.0
Phosphorus
1,500
Potassium
1,600
Sodium
1,100
Total Kjeldahl Nitrogen
6,500
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available in
en (PAN) of the residuals: %. This rate
is a (check one): default value, or iW actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ia
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (11) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
130
130
Injection/Incorporation
245
245
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: None Kno
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
C1 A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
id A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
14 Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
EJ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment.
Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
E] Alternative 4 [15A NCAC 02T. 1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, A heat drying, 71 heat treatment,
thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
q Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
EJ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, I
air drying, ❑ anaerobic digestion,
El composting, or lime stabilization.
c. For Surface Disposal:
rl Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
El Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
El Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
E] Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
E] Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
E] Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
E] Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
E] Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
El Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
El Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

AGMAN
FIELD LOADING ESTIMATES
Facility Dunn WTP
Sampling Date 4/6/2020
Solids 4.29
Mineralization Rate 0
Gallons per DT 5,589.93
pH 6
Sodium Absorpotion 1.00 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 6,500 lbs./1,000 gal 2.33
Ammonia Nitrogen (mg/Kg) 230.00 lbs./1,000 gal 0.08
Nitrate -Nitrite (mg/Kg) 15.10 lbs./1,000 gal 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 130 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 245 lbs./1,000 gal 0.09
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./1,000 gal
0.57
Phosphorus lbs./1,000 gal
0.54
Calcium lbs./1,000 gal
0.39
Magnesium lbs./1,000 gal
0.61
Manganese lbs./1,000 gal
0.54
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
9.40
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.48
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
48.00
Copper lbs./1,000 gal
0.02
Lead (mg/Kg)
15.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.40
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
16.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
3.30
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
77.00
Zinc lbs./1,000 gal
0.03
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
61500
130 0.26
6,370
6,500
245 0.49
6,255
6,370
0 0.00
6,370
6,255
0 0.00
6,255
6,370
0 0.00
6,370
6,255
0 0.00
6,255
6,370
0 0.00
6,370
6,255
0 0.00
6,255
6,370
0 0.00
6,370
6,255
0 0.00
6,255
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 130 0.26
Total 245 0.49

aceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Melvin Goad
Project Name: Dunn 1NTP NC
Project Number: #2188
Lot Number:VD07020
Date Completed:04/14/2020
I
04/17/2020 12:54 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
ANSI M�GmrlAn�rOlHuor Aovd
A C C R E O 17 E 0
3ESTING L4"M10AY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: V©07020
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Phosphorus
The method blank for analytical batch 50964 contained the phosphorus greater than the acceptance
criteria. The associated sample contained detections for this analyte at concentrations greater than 10X
the value found in the method blank; therefore sample results are not impacted. The data has been
reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SG 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 7

Client: Sy nagro Laboratory ID:VD07020-001
Description: Dunn NC WTP Matrix: Solid
Date Sampled:0410612020 0900 % Solids: 4.29 04/0812020 0043
Date Received:0410712020
Run Prep Method
1
1 350.1
1
1
1
1
1 351.4
Inorganic
non-metals
_
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
(% Solids) SM 2540G
1
04/08/2020 0043 MOM
50147
(Ammonia - N ) 350.1
1
04/13/2020 1310 SLC
50851
(Nitrate - N) 9056A
1
04/09/2020 1911 HKL
50610
(Nitrite - N) 9056A
1
04/09/2020 1911 HKL
50611
(Phosphorus) 365.1
2
04/13/2020 1631 DMA
04/13/2020 1215 50872
(Soil pH meas) 9045D
1
04/09/2020 2129 SRB
50573
(TKN) 351.2
1
04/14/2020 1429 DMA
04/14/2020 0940 50881
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
4.29
%
1
Ammonia - N (gas diffusion)
350.1
230
23
12
mglkg
1
Nitrate - N (soluble)
9056A
13
12
0.57
mglkg
1
Nitrite - N (soluble)
9056A
2.1 J
4.7
0.45
mglkg
1
Phosphorus
7723-14-0 365.1
1500
230
47
mglkg
1
Soil pH measured In water @
21.5 ° C 9045D
6.0
su
1
TKN
351.2
6500
580
580
mglkg
1
CVAA
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
74719 1 04110120201210 KSH2
04110120200300 50363
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471E
ND
1.7
0.40
mglkg
1
1CP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD 1 04/09/2020 1746 KSH2
O410812020 1523 50361
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
130000
150
57
mglkg
1
Arsenic
7440-38-2 601OD
9.4
5.7
1.9
mglkg
1
Cadmium
7440-43-9 6010D
ND
1.9
0.48
mglkg
1
Calcium
7440-70-2 60100
1100 J
1900
240
mglkg
1
Chromium
7440-47-3 60100
42
3.8
0.95
mglkg
1
Copper
7440-50-8 601OD
48
3.8
1,7
mglkg
1
Iron
7439-89-6 601OD
31000
38
17
mglkg
1
Lead
7439-92-1 6010D
15
3.8
1.7
mglkg
1
Magnesium
7439-95-4 6010D
1700 J
1900
240
mg/kg
1
Manganese
7439-96-5 6010D
1500
5.7
2.2
mglkg
1
Molybdenum
7439-98-7 6010D
5.3 J
15
3.8
mglkg
1
Nickel
7440-02-0 6010D
16
15
4.0
mglkg
1
LOO = Limit of Quantitation
H = Detected in the method blank E = Quantitation of compound exceeded the
catibration range
DL = Detection limit
ND = Not detected at or above the OL
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOU and > DL
H = Out of holding time
W = Reported on wet weight basis
ice Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
J6 Vantage Point Drive West Columbia,
SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VD07020-001
Description: Dunn NC WTP Matrix: Solid
Date Sampled:0410612020 0900 % Solids: 4.29 04108/2020 0043
Rate Received:04/0712020
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/09/2020 1746 KSH2 O4/08/2020 1523 50361
CAS
Analytical
Parameter
Number
Method
Result
Q LOQ
DL
Units
Run
Potassium
7440-09.7
601OD
1600
J 1900
240
mglkg
1
Selenium
7782-49.2
601OD
3.3
J 7.6
3.1
mglkg
1
Sodium
7440-23-5
6010D
1100
J 1900
240
mglkg
1
Zinc
7440-66-6
601OD
77
19
4.7
mglkg
1
LOCI = Limit of Quantitalion 8 = Detected in the method blank F = Quantilation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N - Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H - Out of holding time W = Reported an wet weight basis
'ace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Envimnmenlal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] fax [phone] www.pacelabs.com
Page 5 of 7

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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax {803) 791-9111 www.pacetabs.com
Page 6 of 7
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Shral� G9V1r0nn%9nrat Sarvfcea, lnrn
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Clfont: 5ynagrc� Cooler InpecleJ by/daty 3MO / 44,107/200 Lc Cti: STC7OM20
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l� No S, Were Proper on."dy procedurrs (relingt�lsitetllieceiilcd)%!lowed?
— No 6. wore sumpte IDs listed on the COC2
NO 7. Were sample Iris listed an all sanlplc contalrFers7
© Z+ln 8, W as cnllcetiott dke & fime ilslcd nn the coC?
�i Nn $, 4Vas cr3llection date Ai time listed cart all Murple cntttauters7
© No 10. Did all conutiner Jat>rl infatmation (Ill, date, tirtre) a fee with thr C[]C?
] 1Va 1 i. Were fasts to b: pertornted listed nit the COC'�
Na 12• Did all santples ar:lte in tis� proper cttntaintrS fi5r each tcNt Pradfar in good co�tdit;o„
(uttlat4l:ctt, lids on, etc.)7 _
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14. Wete a]I samples Mwivcd wkhln 3z Ilte
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d sulfide yampies received at a trH x 97
Q Yes Q No O NA 20. Were ciic+nt retnaticsfrcgttaslS (1,e.:rsgnesfed dilutions, MS( MSD doslgtaltion.%
cetrrnctty ""Scrtltad frcrn, tits GOC in,ca the eotnment section in 1.ItvI i?
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!ample lE'resert+atioo (Vital be crnnplc�tcd For any samples) incorrectly preserved or n ith headspw .)
Satnplr(s) Nit._._ were rzceivcxl lncorrectiy preserv[sd a,td weri3 trusted accardingl3� in sample n�ccivljlg »'itlt Nil tnL of circle onc: I-I2804, HNC3, HCL Na0l•t iming SR !/ NA
Time,0f pre9cmtlnn NAA _ Iftnerc th€� nne prosarvadve is nce-ded, please note in the commttls1belmy,
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ere received with bubbles >fr lnnt in diarnet� er.
SrOtiptas(s) MA_ �vzre received witFa TRG> t?.� mglL {If#19 ix fin) xnd �v ark 411Stcxl accordingly in sample l v svingwB Sodium tlll05ulF0e (NMA,03) with .Shealy ID: NA
R barcode lallola applied, by: 1]Mi3 Date_ 0dit}TfZp$fl
t,'Oritrtlratts: -
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs,cam
Page 7 of 7

MY0 Um" li
EI,IInOi4M€MiaL pia tlranL[1t;il s, INC,
�? �,alyrflr7al L�r�e�ralvf'lg+s
September 11, 2019
Melvin Goad
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Duren, NC WTP
Dear Melvin Goad:
Summit Eftwiromnenfal Technologies, Inc.
3310 97in St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FIX.' [phone]
FYebslle: hfty://isltrin.setfek.com
Order No.: 19081720
Summit Environmental Tecluiologics, Inc. received I sample(s) on 8/22/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance Iimits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
Iaboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, Califonua 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas. E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39105 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OHM001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OH009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 33

Summil Environmental Technologies, Ine.
' jprib 3310 Win St. Case Narrative
LLJEiV011DtVALtJT4L �xC�} C�I_n:9i��, NG Cuyahoga Falls, Ohio44223 Wo#: 19081720
AnR.VYUcal TEL. (330J 253-8211 FAX [phone]
Dat
ATebsite: httn://ivir7v.settek.cw7r e: 911112019
CLIENT: Synagro
Project: Dunn, NC WTP
WorkOrder Narrative:
19081720: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chant -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc, and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19081720-00 IA TCLP-SVOC_8270E: Possible low bias for Pyridine due to low recovery in the LCS.
19081720-001A TCLP-svoc-herb_TCLP(8IS 1): The CCV exhibits high recoveries for 2,4-D. All
reported samples are ND for 2,4-D.
Original
Page 2 of 33

=rrn raw Sutnadt Environmental Technologies, lit Qualifiers and Acronyms
3310 Win 5
t NOITOWOL WTAL rui INOI LIGIFS, lNr Cuyahoga Falls, Ohio 442i WO#: 19081720
Rat;aly0cal tnboralortes TEL: [phone] FAY (330) 253-445
Websile: htro://tir�iu.settek.co. Date: 911I/2619
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
In Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:I response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low () or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The 1CV recovery failed low (-) or high (+).
s The spilce result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level ofDetection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvi
Regulatory Limit
AISD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextractiou
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 33

l U - �.-i Sanmrltl trnirormrerrtalTechrrologies, Inc. Workorder
MMOA3310 Win St.
ITEPA MONMENTdL r u ni nm a, or. Cuyahoga Falls, Ohto 44223 Sample Summary
—1AjTafy0ca1 L4bora1u v!-L TEL: [phone] FAX:- [phone] woft: 19081720
Websiie: htM.-11 ww.settelr.conr 11-3ep 19
CLIENT: Synagro
Project: Dunn, NC WTP
Lab Samplell) Client Sample ID Tag No Date Collected Date Received Matrix
19081720-001 Dunn, NC WTP 9/21/2019 11:15:00 AM 8/22/2019 I0:20:00 AM Sludge
Page 4 of 33

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Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
Ilt_tlULWAL r1oimtl7nE 1nr Cuyahoga Falls. Ohio44223 (base report)
r' _ r'! rll,f`c�1 ��t�nrail�r+et TEL: [phone] FkY..• [phone] WO#: 19081720
r^Yebsile; htla;/hvrvrv.settek.can Date Reported: 9/11/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/21/2019 11:15:00 AM
Lab ID: 19081720-OOIA
Project: Dunn, NC WTP
Client Sample ID Dunn, NC WTP
Analyses Result RI., Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As)
ND
TCLP Barium(13a)
RD
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
N❑
TCLP Siiver(Ag)
ND
FLASHPOINT DETERMINATION (1010)
Flashpoint (140°F) >140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachioro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr; 2-Fluorophenol
39.0
Surr: PhenolA6
43.2
Surr: Nitrobenzene-d5
30.7
SW7470A SW7470A Analyst: DNS
0.00200
mg1L 1
8/26/2019 3:55:00 PM
SW601OD
SW3010A Analyst; EAM
0,500
mglL 1
812612019 5:5926 PM
5.00
mg1L 1
8/2612019 5:59:28 PM
0.100
rnglL 1
8/26/2019 5:59:26 PM
0.200
mglL 1
8126/2019 5:59:26 PM
0.500
mglL 1
8/2612019 6:59:26 PM
0.0500
mglL 1
8126/2019 5:59:26 PM
0.500
mglL 1
8/26/2019 5:59:26 PM
SW1010 Analyst: TAH
°F
1
8/3012019 12:31:30 PM
SW8270
SW3610C Analyst: MES
0.200
mglL
2
8/28/2019 7:28:00 PM
0.600
mglL
2
8/28/2019 7:28:00 PM
0.500
mglL
2
8/28/2019 7:28:00 PM
0.100
mglL
2
8/28/2019 7:28:00 PM
10.0
mglL
2
8128/2019 7:28:00 PM
0.0400
mg1L
2
8/28/2019 7:28:00 PM
0.100
mglL
2
8/28/2019 7:28:00 PM
0.200
mglL
2
8/28/20 f 9 7:28:00 PM
0.200
mg1L
2
8/28/2019 7:28:00 PM
0.500
mglL
2
8/28/2019 7:28:00 PM
0.500
QL- mg1L
2
8/28/2019 7:28:00 PM
10 - 109
in %Rec
2
8/2812019 7:28:00 PM
10 - 109
%Rec
2
8/2812019 7:28:00 PM
19 - 120
%Rec
2
8/28/2019 7:28:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding tithes for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit r..imit
RL Reporting Detection Limit
H Value above quantitation range
M Manual Integration used to detennine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 6 of 33

L Suitirtsil Ettvirotattte>ztal Technologies, Inc. Analytical Report
=, �� I Sril�� 3310 Win Sr.
4'IIY_3rlM_UTb.L ri_ RJiil n„ - , 1" CupahogaFalls, Ohio 44223 (base report)
5lytfic7lt�Lbor�IfooE-_ TEL: [phone] FAX. [phone] WO#: 19081720
Ifebsite: h1in:/hniviv.setrek.cont Date Reported: 9/11/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/21/2019 11:15:00 AM
Lab ED: 19081720-OOIA
Project: Dunn, NC WTP
Client Sample ID Dunn, NC WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
Surr: 2,4,6-Tribromophenol 4T3 10 - 120 %Rec
Suer: 2-Flucrobiphenyl 42.1 22 - 117 %Rec
Surr: p-Terphenyl-d14 56.3 34 - 116 %Rec
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
71.7
Surr: DCB
75.9
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SWI 311181 51)-SOLID
2,4-D ND
2,4,5-TP ND
Surr: DCAA 94.6
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
N❑
Tetrachloroeihene
ND
SW8270 SW3610C Analyst: MES
2 8/28/2019 7:28:00 PM
2 8/2812019 T28:00 PM
2 8/2812019 7:28:00 PM
SW8081 SW3510C Analyst: MES
0.0250
mg/L
10
8/2812019 9:17:00 AM
0.0500
mg/L
10
8/2812019 9:17:00 AM
0.00500
mg/L
10
8/28/2019 9:17:00 AM
0.00600
mg/L
10
8/28/2019 9:17:00 AM
0.00500
mg/L
10
8/28/2019 9:17:00 AM
0.00500
mg/L
10
8/2812019 0:17:00 AM
0.00500
d mg/L
10
8/2812019 9:17:00 AM
10 - 119
%Rec
10
8/28/2019 9:17:00 AM
10 - 119
%Rec
10
8/2812019 9:17:00 AM
SW8151A SW8151A Analyst: MES
0.0100 QC+ mglL 1 8/30/2019 5:2B:00 PM
0.00500 mg/L 1 8/3012019 5:28:00 PM
20 - 140 m %Rec 1 8/3012019 5:28:00 PM
SW8260 Analyst: CTB
0.125
mg/L
25
812612019 3:04:00 PM
0.125
mg/L
25
8/2612019 3:04:00 PM
2.50
mg/L
25
8/26/2019 3:04:00 PM
0.125
mg/L
25
8/26/2019 3:04:00 PM
0.125
mg/L
25
8/26/2019 3:04:00 PM
1.25
mg1L
25
8/2612019 3:04:00 PM
0,125
mg/L
25
812612019 3:04:00 PM
0,125
mg/L
25
8/26/2019 3:04:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
PL
Permit Limit
RL
Reporting Detection Lunit
E Value abovo quantitation rango
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column continuation exceeds
R RPD outside accepted recovery hmits Original
* Samples with CalcVal < MDL
Page 7 Of 33

SwounifEnvironmental Technologies, hm. Analytical Report
3310 Brit St.
Ft�'Jlii4ihJtnu€1Tts4 r,�G7fnCilt��i=_s,:Pt Cuyahoga Falls, Ohio 44223 (base report)
P r;ilyflC7.i iicra7r�flE% TEL: [phone] FAX: [phone] WD#: 19081720
TFebsim: hflm:lhaww.sellek.coLn Date Reported: 9/11/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection hate: 8/21/2019 11:15:00 AM
Lab ID: 19081720-001A
Project: Dunn, NC WTP
Client Sample ID Dunn, NC WTP
Analyses
Result
RL
Qua] Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB
-SOLID
SW8260
Analyst: CTI3
TCLP VOLAT[LES ANALYSIS
Trichlorcethene
ND
0.125
mg1L
25
8/26/2019 3:04:00 PM
Vinyl chloride
ND
0.0500
mglL
25
8/26/2019 3:04:00 PM
Surr: 4-Bromofluorobenzene
89.4
70 - 130
%Rec
25
8/26/2019 3:04:00 PM
Surr. Dibromofluoromethane
88.1
70 - 130
%Roc
25
8/26/2019 3:04:00 PM
Surr: Toluene-d8
94.9
70 - 130
%Rec
25
8/2612019 3:04:00 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9014 Analyst: MS
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive ND 0.481 mg/Kg 1 8/2712019 5:11:00 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9045D Analyst: DHC
PH (SW9045D)
pH 7.3 s.u.@19.5C 1 9/6/2019 10:53:00 AM
RCI-SOLID-WI IGNITABIL[TY1030 SW9034 Analyst: MS
REACTIVE SULFIDE (9034)17,3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 8/27/2019 5:11:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL PwnitLifnit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to detennine area response
N Tentatively identified compounds
P Second column conl"mnation exceeds
R RPD outside accepted recovery limits Original
U Samples witli C*Val < MDL
Page 8 of 33

Sunanit5m,honmerrtalTechnologies,Inc. Accreditation Program
3310 Win St. Anal tes Report
ENVIII0J.J at i,iTA,L trItH(Mal GGI 5, Ec CuyaltagaFalls, Ohio 44223
Arrafy0ral Uboralorla-� TEL: [phone] FAX.- [phone] WO#: 19081720
Webstle: httn:/htnryseltek.corn II-Sep-19
Client: Synagro State: NW
Project: Dunn, NC WTP Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19081720-OOlA Sludge
Flashp6intDetennination(1010)
Flasbpoint(140°F)
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3,3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)17.3.4.2
Sulfide, Reactive
U
Sludge
TCLP herbicides Analysis (SW13111815l)-solid
2,4,5-TP
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)-solid
2,4-D
A
Sludge
TCLP Mercury Analysis (SWI31117470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8091)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW131118081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Aualysis (SW1311/8081)
Heptaclilor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SWI 311/808 1)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/9270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotolueno
A
Sludge
TCLP Sean-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlornbenzene
A
Sludge
TCLP Semi Volatiles Analysis (SW1311/8270)
Hexachlorobutediene
A
Sludge
TCLP Semi-Volatiles Analysis (SW131119270)
hexachlorcethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentacblorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original #1
Page 9 of 33

t:001� SUi. L __ Suuunit Emironntental Technologies, Inc. Accreditation Program
` 6�� i' ';'i 1 U 3310Win St. Anal tes Report
F_PtS+ifMIAMEWAL tEellojnt n 3 G, ',;r, Cuyahoga Falls, Ohio 44223
Analy tfcal Laboraxones TEL: [phone] FAX.' [phone] WO#: 19081720
Website. htto;1Ayww.settek.coni 1-sep-19
Client: Synagro State: NW
Project: Dunn, NC WTP Program Name: NC_WW_SCM
Sample ID Matrix Test Name Aaalpte Status
19081720-OOIA
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
NC WW SCM A Accredited
TCLP Volatiles Analysis
1,1-Dichloroethene A
TCLP Volatiles Analysis
1,2-Dichloroetliane A
TCLP Volatiles Analysis
2-Butanone A
TCLP Volatiles Analysis
Benzene A
TCLP Volatiles Analysis
Carbon tetrachloride A
TCLP Volatiles Analysis
Chlorobenzene A
TCLP Volatiles Analysis
Chloroform A
TCLP Volatiles Analysis
Tetrachloroethene A
TCLP Volatiles Analysis
Trichloroethene A
TCLP Volatiles Analysis
Vinyl chloride A
NC WW SCM U Unavailable
Original #1
Page 10 of 33

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Srann it Environniental Technologies, Inc.
3310 lVin St,
t'blfiL+tJI1�61YAL r��li4'•i]f lfl�" ih Cuyahoga Falls, Ohio44223 Sample Log -In Check List
TEL: [phone] FAX.- [phone]
JEebsile: http:/hvaviv.settelr.cvm
Client Name: SYN-NC-27028 Work Order Number: 19081720 RcptNo: 1
Logged by: John A.Semonik
Completed By: Jacqueline Rasile
Reviewed By: Jan nifer Woolf
812212019 10:20:00 AM
812212019 1:37:08 PM
812212019 2:53:33 PM
Chain of Custody
1. Is Chain of Custody complete? Yes 0 No ❑ Not Present ❑
2, How was the sample delivered? UPS
Log In,
3. Coolers are present? Yes k No ❑ NA ❑
4. Shipping containerlcouler in good condition? Yes Q No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑d
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes Q No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes 91 No ❑ NA ❑
7. Sample(s) in proper container(s)?
Yes 0
No ❑
8. Sufficient sample volume for indicated test(s)?
Yes 0
No ❑
g. Are samples (except VOA and ONG) properly preserved?
Yes ®
No ❑
10, Was preservative added to bottles?
Yes ❑
No NA ❑
11, Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes ❑
No ❑ No VOA Vials 0
12. Were any sample containers received broken?
Yes ❑
No ❑J
13. Does paperwork match bottle labels?
Yes
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes ®
No ❑
15. Is it clear what analyses were requested?
Yes ©
No ❑
16, Were all holding times able to be met?
Yes W
No ❑
(If no, notify customer for authorizatlon.)
Special Handling (if applicable}
17. Was client notified of all discrepancies with this order?
Yes ❑
No ❑ NA d❑
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding: � -- - - ----- ----- -- --.
Client fnstructions:
18. Additional remarks:
Cooler Information
Cooler No Temp °C Condition I Seal Intact I Seal Na I Seal Date Signed C3
1 3.7 Good Nat Present
Page 33 of 33

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State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
l?ivision of hater Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: bunn WWTP
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: IL Div. of Water Resources, Div. of Environmental Health,
or p Other (explain: W).
3. Facility contact person and title: Donrie Dukes, Supenntenden'i
Complete mailing address: PO Box 1065
City: = State: NC Zip: 28334-
Telephone number: 10) 892-2935 E-mail address: wastewater&dunn-nc.org
4. Facility physical address: 580 J.W. Edwards Lani
City: Dunn State: NC Zip: 28334-
Coordinates: Latitude: b° 17' 48" Longitude: 78' 38' 14.6"
Datum: � Level of accuracy: Sub -Meter
Method of measurement: GIS
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes ® No
7. Facility permitted/design flow: M MGD and facility average daily flow: 0 MGD
8. Average amount of residuals being generated at this facility E dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Extended Aeration Basin (4 Cells)
Type and volume of residuals storage (i.e., outside of residuals treatment units): 130.000 Gallon Aerobic Digester &
600,000 Gallon Sludge Holding Tank
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 0 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Summit Environmental Tecbno ogi and Date of analysis: /15/2020
Passed corrosivity test: ® yes Ejj no. pH: 6.2 s.u. (2 < pH < 12.5)
Passed ignitability test: yes LA no. Flashpoint: - OF (> 140°F)
Passed reactivity test: Eyes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
Arsenic
5.0
< 1.25
Hexachlorobenzene
0.13
< 0.1
Barium
100.0
< 12.5
Hexachloro-1,3-Butadiene
0.5
< 0.04
Benzene
0.5
< 0.25
Hexachloroethane
3.0
< 0.2
Cadmium
1.0
< 0.25
Lead
5.0
< 1.25
Carbon Tetrachloride
0.5
< 0.25
Lindane
0.4
< 0.0125
Chlordane
0.03
< 0.125
Mercury
0.2
< 0.005
Chlorobenzene
100.0
< 2.5
Methoxychlor
10.0
< 0.0125
Chloroform
6.0
< 0.25
Methyl Ethyl Ketone
200.0
< 5.0
Chromium
5.0
< 0.5
Nitrobenzene
2.0
< 0.2
m-Cresol
200.0
< 10.0
Pentachlorophenol
100.0
< 0.5
o-Cresol
200.0
< 10.0
Pyridine
5.0
< 0.5
p-Cresol
200.0
< 10.0
Selenium
1.0
< 0.125
Cresol
200.0
< 10.0
Silver
5.0
< 1.25
2,4-D
10.0
< 0.5
Tetrachloroethylene
0.7
< 0.25
1,4-Dichlorobenzene
7.5
< 0.2
Toxaphene
0.5
< 0.25
112-Dichloroethane
0.5
< 0.25
Trichloroethylene
0.5
< 0.25
1,1-Dichloroethylene
0.7
< 0.25
2,4,5-Trichlorophenol
400.0
< 0.5
2,4-Dinitrotoluene
0.13
< 0.1
2,4,6-Trichlorophenol
2.0
< 0.5
Endrin
0.02
< 0.0125
2,4,5-TP (Silvex)
1.0
< 0.5
Heptachlor and its Hydroxide
0.008
< 0.0125
Vinyl Chloride
0.2
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytica and Date of analysis: 1/15/2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
< 20.8
Cadmium
85
39
< 4.17
Copper
4,300
1,500
294
Lead
840
300
55
Mercury
57
17
1.55
Molybdenum
75
n/a
< 10.4
Nickel
420
420
16.5
Selenium
100
100
< 20.8
Zinc
7,500
2,800
613
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
17 > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Kaypoint Analtical and Date of analysis: 1/15/2020
Parameter
Result
(mg1kg)
Aluminum
15,000
Ammonia -Nitrogen
6,210
Calcium
9,290
Magnesium
2,890
Nitrate -Nitrite Nitrogen
1,490
pH (Standard Unit)
5.9
Phosphorus
21,500
Potassium
4,460
Sodium
2,000
Total Kjeldahl Nitrogen
68,800
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): �.
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): JW default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ia
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (11) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
23,372
35,066
Injection/Incorporation
26,477
37,372
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: None Kno
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
C1 A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
id A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
14 Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
EJ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment.
Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
E] Alternative 4 [15A NCAC 02T. 1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, A heat drying, 71 heat treatment,
thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, I
air drying, ❑ anaerobic digestion,
El composting, or lime stabilization.
c. For Surface Disposal:
rl Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
71 Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
E] Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
E] Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
E] Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
E] Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
E] Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
El Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
El Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
q Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
id Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

AGMAN
FIELD LOADING ESTIMATES
Facility Dunn WWTP
Sampling Date 1/15/2020
Solids 2.43
Mineralization Rate 0.30
Gallons per DT 9,868.65
pH 5.9
Sodium Absorpotion 0.72 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 68,800 lbs./1,000 gal 13.94
Ammonia Nitrogen (mg/Kg) 6,210.00 lbs./1,000 gal 1.26
Nitrate -Nitrite (mg/Kg) 1,490.00 lbs./1,000 gal 0.30
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 23,372 lbs./1,000 gal 4.74
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 26,477 lbs./1,000 gal 5.37
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./1,000 gal
0.90
Phosphorus lbs./1,000 gal
4.36
Calcium lbs./1,000 gal
1.88
Magnesium lbs./1,000 gal
0.59
Manganese lbs./1,000 gal
0.05
Sulfur lbs./1,000 gal
2.17
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
20.80
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
4.17
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
294.00
Copper lbs./1,000 gal
0.06
Lead (mg/Kg)
55.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
1.55
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
16.50
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
20.80
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
613.00
Zinc lbs./1,000 gal
0.12
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
68,800
23,372 46.74
45,428
68,800
26,477 52.95
42,323
45,428
6,814 13.63
38,614
42,323
6,348 12.70
35,975
38,614
2,896 5.79
35,718
35,975
2,698 5.40
33,276
35,718
1,339 2.68
34,378
33,276
1,248 2.50
32,029
34,378
645 1.29
33,734
32,029
601 1.20
31,428
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 35,066 70.13
Total 37,372 74.74

Waypoint,(D
ANALYTICAL:
1 /2412020
Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref. Analytical Testing
Report Number; 20-016-0008
Project Description: Dunn WVVTP
7621 White pine Road, Richrv►i�ndf VA 23237
Main 804-743-9401 ° Fox 804,��I r64
wwwi,way"16toalydcal.Cbm'
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/16/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable,
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated_ This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
p­�- r'
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

a
Waympo
t
.
ANALYTICAL
7621 Whifepine Road, Richmond, VA 23237
Main 804-743-9401 ° i;ax 804-271-6446
www.waypointanal*ai.com
Sample Summary Table
Report Number:
20-016-0008
Client Project Description:
Dunn WWTP
Lab No Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
70186 Dunn WWTP
Solids
01/15/2020
01/16/2020
70186 Dunn WWTP
Solids
01/15/2020
01/16/2020
SM-4500-NH3C
WP MTN
7C186 Dunn WWTP
Solids
01/15/2020
01/16/2D20
9045D
WP MTN
70186 Dunn WWTP
Solids
01/15/2020
01/16/2020
4500NO3F-2011
WP MTN
70186 Dunn WWTP
Solids
01/15/2020
01/16/2020
6010D
WP MTN
70186 Dunn WWTP
Solids
01/15/2020
01/16/2020
SW-74719
WP MTN
70186 Dunn WWTP
Solids
01/15/2020
01/16/2020
SM-4500-NH3C TKN
WP MTN
70186 Dunn WWTP
Solids
01/15/2020
01/16/2020
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

a
7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-940.1 ° FaX [phone]
46789 ANALYTICAL www.wOpo[ntanalyliCal.com
Synagro Central LLC/ Dunn
Mary Brewer Project Dunn WWTP Report Date : 01/24/2020
284 Boger Road Information ; Received : 01/16/2020
Macksville , NC 27028
Report Number: 20-016-0008 REPORTOFANALYSIS Paudc McGroary
Agronomist
Lab No : 70186
Matrix: Solids
Sample ED.- Dunn WWTP Sampled; 1/15/2020 0:00
Test
Results
Units
MQL
OF
Date I Time
By
Analytical
Analyzed
Method
Moisture
97.6
%
0.010
1
01/21/2016:44
ADM
SM-254OG
Test
Results
Units
MQL
DF
Date I Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
6210
mg/Kg - dry
4170
1
01/23/20 13:00
JP]
5M-4500-NH3C
Nitrate+Nitrite-N
1490
mg/Kg - dry
199
1
01/23/20 13:37
ZED
4500NO3F-2011
Organic N
62500
mg/Kg - dry
10400
1
01/23/20 10:00
CALCULATION
pH
5.9
s,u.
1
01122/2006:20
]SL
9045D
Total Solids
2.43
°7°
0.010
1
01/21/20 16:44
ADM
5M-254OG
Total Kjeldahl Nitrogen
68800
mg/Kg - dry
10400
1
01/23/20 10:00
JP]
iM-4500-NH3C TKP
Phosphorus
21500
mg/Kg - dry
208
1
01/21/20 16:45
BKN
6010D
Aluminum
15000
mg/Kg - dry
208
1
01/21/20 WAS
BKN
60i0D
Arsenic
<20.8
mg/Kg - dry
20.8
1
01/21/20 16:45
BKN
6010D
Calcium
9290
mg/Kg - dry
1040
1
01/21/20 16:45
KKM
6010D
Cadmium
<4.17
mg/Kg - dry
4.17
1
01/21/20 16:45
BKN
6010D
Chromium
36.5
mg/Kg - dry
10.4
1
01/21/20 16:45
BKN
6010D
Copper
294
mg/Kg - dry
10.4
1
01/21/20 16:45
BKN
6010D
Iron
28400
mg/Kg - dry
208
1
01/21/20 16:45
BKN
6010D
Lead
55.0
mg/Kg - dry
12.5
1
01/21/20 16:45
BKN
6010D
Magnesium
2890
mg/Kg - dry
208
1
01/21/20 16:45
BKN
6010D
Manganese
261
mg/Kg - dry
20.8
1
01/21/20 16:45
BKN
6010D
Qualifiers/ DF
Definitions
Dilution Factor
L
Limit Exceeded
MQLMethod
Quantitation Limit
Page 3 of 6

Waypoint,
ANALYTICAL
46789
Synagro Central LLC/ Dunn
M
76211i hitepine Road,. Richmond, VA Z3237
AAai.n 804-743-9401 ° fax [phone]
wWw waypointanalytical.com
ary Brewer Project Dunn WWTP Report Date : Ol/24/2020
284 Boger Road Information ; Received : 41/16/202D
Mocdksville , NC 27028
Report Number; 20-016-0008 REPORT OFANAL )ISIS Pauric McGroary
Agronomist
Lab No : 70186
Sample ID :Dunn WWTP Matrix: Solids
Sampled: 1/15/2020 0:00
Test
Results
Units
MQL
DE
Date I Time
By
Analytical
Analyzed
Method
Mercury
1.55
mg/Kg - dry
0.633
1
01/20/20 13:24
TJS
SW-7471B
Molybdenum
<10.4
mg/Kg - dry
10.4
1
01/21/20 16:45
BKN
60101)
Nickel
16.5
mg/Kg - dry
10.4
1
01/21/20' 16:45
BKN
6010D
Potassium
4460
mg/Kg - dry
208
1
01/21/2016:45
BKN
6010D
Selenium
<20.8
mg/Kg - dry
20.8
1
01/21/20 16:45
BKN
6010D
Sodium
2000
mg/Kg - dry
W40
1
01/21/20 16:45
BKN
6010D
Zinc
613
mg/Kg - dry .
52.1
1
01/21/20 16:45
BKN
6010D
Sulfur
10700
mg/Kg - dry
208
1
01/21/20 16:45
BKN
6010D
Qualifiers/ DE Dilution Factor
Definitians L Limit Exceeded
MQL Method Quantitation Limit
Page 4 of 6

Waypoin.
ANALYTICAL
7522 Whitepine Road, Richmond, VA Z3237
Main 804.743-9401 0 Fax [phone]
www,waypiointanalvecal.com
Shipment Receipt Form
Customer Number: 46789
Customer Name: Synagro Central LLCI Dunn
Report Number: 20-016-0008
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F . 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
() No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
9 Yes
C) No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
* N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
NIA
F_ High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes
No
Signature: Brandi Watson _ Date & Time: L1/16/2020 12:09:2
Page 5 of 6

��1ilJ T I
5yna�uaCa:uSruLLC;Guni
". outinwvvTP
�14rmu inurnt
Page :.'6 of 6 - - .
pkkk

SUMM111
ENVIRONMENTAL TECHNOLOMZ3. INC
ArrzrJy0ca1 Laboralorfas
February 07, 2020
Melvin Goad
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: DUNN WWTP
Dear Melvin Goad:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 20010926
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/16/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho 01100923, Illinois
200061, Indiana C-011-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OH00923201 1 -1, Virginia VELAP 9456, Washington C891
Page 1 of 32

mm' y Summit Environmental Technologies, Inc. Case Narrative
su3310 Win St.
ENVIRONMENTAL rEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 WO#: 20010926
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 2/7/2020
CLIENT: Synagro
Project: DUNN WWTP
WorkOrder Narrative:
20010926: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20010926-OOIA TCLP-SVOC-CPEST(8081B): Bracketing CCVs were out of range for some analytes.
All samples within the sequence are non -detect for all analytes.
20010926-OOIA TCLP-SVOC_8270E: Possible low bias for 1,4-Dichlorobenzene and
Hexachloroethane due to low recovery in LCS-41607.
20010926-OOIA F1ashPt_S(1010): Z = Method deviation, due to instrument limitations could not stir to
250 RPM as required by the method.
Analytical Sequence QC Notes:
CCV-108374 VOC-MSTR_NPW(8260): The VOC CCV (Batch R108374) exhibited high recovery fo
Chlorobenzene and Tetrachloroethene; All samples were ND.
Original
Page 2 of 32

mm' y Summit Environmental Technologies, Inc. Case Narrative
su3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 WO#: 20010926
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 2/7/2020
CLIENT: Synagro
Project: DUNN WWTP
LCS-41570 TCLP-SVOC-CPEST_TCLP(8081): LCS-41570 demonstrated high recovery for analyte
Endrin, suggesting a potential high bias for recovery of this analyte. All samples in this batch are non -
detect for Endrin.
LCS TCLP-SVOC-Herb_TCLP: LCS exhibited high recovery, associated samples are ND for all
analytes of interest.
LCS-R108707 F1ashPt_S(1010): Z = Method deviation, due to instrument limitations could not stir to
250 RPM as required by the method.
Original
Page 3 of 32

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
Ekiwlt OMM@N-rALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� WO#: 20010926
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: httn:11www.settek.co Date: 2/7/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low () or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low () or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low () or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low () or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 32

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
EkNVIROMMEWAL reCHNO ijULES. INC. Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
CLIENT: Synagro
Project: DUNN WWTP
Lab SampleID Client Sample ID
20010926-001 DUNN WWTP
Tag No Date Collected
1/15/2020 10:00:00 AM
Workorder
Sample Summary
WO#: 20010926
07-Feb-20
Date Received Matrix
1/16/2020 9:55:00 AM Sludge
Page 5 of 32

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SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVITtONMENTALTECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 20010926
Date Reported: 2/7/2020
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/15/2020 10:00:00 AM
Lab ID:
20010926-OOIA
Project:
DUNN WWTP
Client Sample ID DUNN WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
RCI
FLASHPOINT DETERMINATION (1010)
Flashpoint (140°F) >140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
31.2
Surr: Phenol-d6
34.2
Surr: Nitrobenzene-d5
48.0
SW7470A SW7470A Analyst: MJM
0.00500 mg/L 1 1/23/2020 3:25:00 PM
SW6010D SW301OA Analyst: EAM
1.25
mg/L
1
1/22/2020 1:30:02 PM
12.5
mg/L
1
1/22/2020 1:30:02 PM
0.250
mg/L
1
1/22/2020 1:30:02 PM
0.500
mg/L
1
1/22/2020 1:30:02 PM
1.25
mg/L
1
1/22/2020 1:30:02 PM
0.125
mg/L
1
1/22/2020 1:30:02 PM
1.25
mg/L
1
1/22/2020 1:30:02 PM
SW1010
Analyst: TAH
Z °F
1
1/30/2020 11:50:49 AM
SW8270 SW351OC Analyst: SFG
0.200
QL- mg/L
2
1/24/2020 7:47:00 PM
0.500
mg/L
2
1/24/2020 7:47:00 PM
0.500
mg/L
2
1/24/2020 7:47:00 PM
0.100
mg/L
2
1/24/2020 7:47:00 PM
10.0
mg/L
2
1/24/2020 7:47:00 PM
0.0400
mg/L
2
1/24/2020 7:47:00 PM
0.100
mg/L
2
1/24/2020 7:47:00 PM
0.200
QL- mg/L
2
1/24/2020 7:47:00 PM
0.200
mg/L
2
1/24/2020 7:47:00 PM
0.500
mg/L
2
1/24/2020 7:47:00 PM
0.500
mg/L
2
1/24/2020 7:47:00 PM
10 - 109
%Rec
2
1/24/2020 7:47:00 PM
10 - 109
m %Rec
2
1/24/2020 7:47:00 PM
19 - 120
%Rec
2
1/24/2020 7:47:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Origin
U Samples with CalcVal <MDL
Page 7 of 32

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVITtONMENTALTECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 20010926
Date Reported: 2/7/2020
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/15/2020 10:00:00 AM
Lab ID:
20010926-OOIA
Project:
DUNN WWTP
Client Sample ID DUNN WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: 2,4,6-Tribromophenol 54.1 10 - 120 %Rec 2
Surr: 2-Fluorobiphenyl 44.7 22 - 117 %Rec 2
Surr: p-Terphenyl-d14 82.4 34 - 116 %Rec 2
NOTES:
Possible low bias for 1,4-Dichlorobenzene and Hexachloroethane due to low recovery in LCS-41607.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
75.3
Surr: DCB
102
TCLP HERBICIDES BY EPA 8321B
2,4-D ND
2,4,5-TP ND
Surr: 2,4-Dichlorophenylacetic aci 76.5
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
SW351OC Analyst: SFG
1/24/2020 7:47:00 PM
1/24/2020 7:47:00 PM
1/24/2020 7:47:00 PM
SW8081 Analyst: SEK
0.125
mg/L
5
1/23/2020 11:40:00 PM
0.250
mg/L
5
1/23/2020 11:40:00 PM
0.0125iQC+(QDmg/L
5
1/23/2020 11:40:00 PM
0.0125
dQC+
mg/L
5
1/23/2020 11:40:00 PM
0.0125
dQC+
mg/L
5
1/23/2020 11:40:00 PM
0.0125
dQC+
mg/L
5
1/23/2020 11:40:00 PM
0.0125
dQC+
mg/L
5
1/23/2020 11:40:00 PM
10 - 119
%Rec
5
1/23/2020 11:40:00 PM
10 - 119
%Rec
5
1/23/2020 11:40:00 PM
SW8321A SW1311M Analyst: BJH
0.500 mg/L 50 1/24/2020 3:19:00 AM
0.500 mg/L 50 1/24/2020 3:19:00 AM
70 - 130 %Rec 50 1/24/2020 3:19:00 AM
SW8260 SW1311M Analyst: RMT
0.250
mg/L
50
1/22/2020 6:00:00 PM
0.250
mg/L
50
1/22/2020 6:00:00 PM
5.00
mg/L
50
1/22/2020 6:00:00 PM
0.250
mg/L
50
1/22/2020 6:00:00 PM
0.250
mg/L
50
1/22/2020 6:00:00 PM
2.50
QC+ mg/L
50
1/22/2020 6:00:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Origin
U Samples with CalcVal <MDL
Page 8 of 32

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 20010926
Date Reported: 2/7/2020
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/15/2020 10:00:00 AM
Lab ID:
20010926-OOIA
Project:
DUNN WWTP
Client Sample ID DUNN WWTP
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M
Analyst: RMT
TCLP VOLATILES ANALYSIS
Chloroform
ND
0.250
mg/L
50
1/22/2020 6:00:00 PM
Tetrachloroethene
ND
0.250
QC+ mg/L
50
1/22/2020 6:00:00 PM
Trichloroethene
ND
0.250
mg/L
50
1/22/2020 6:00:00 PM
Vinyl chloride
ND
0.100
mg/L
50
1/22/2020 6:00:00 PM
Surr: 4-Bromofluorobenzene
101
70 - 130
%Rec
50
1/22/2020 6:00:00 PM
Surr: Di brom oft uorom ethane
97.9
70 - 130
%Rec
50
1/22/2020 6:00:00 PM
Surr: Toluene-d8
94.1
70 - 130
%Rec
50
1/22/2020 6:00:00 PM
RCI
SW9014
Analyst: CXS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.495
mg/Kg
1
2/3/2020 5:24:00 PM
RCI
SW9045D
Analyst: VVK
PH (SW9045D)
pH
6.2
s.u.@20.00
1
2/3/2020 3:53:37 PM
RCI
SW9034
Analyst: CXS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0
mg/Kg
1
2/3/2020 5:24:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Origin
U Samples with CalcVal <MDL
Page 9 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Anal tes Report
Y
ENwIROMMEWALIrECHNOL.OG{r,S,INC,
Cuyahoga Falls, Ohio44223
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
20010926
Website: http://www.settek.com
07-Feb-20
Client: Synagro
State: NW
Project: DUNN WWTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20010926-OOIA Sludge
Flashpoint Determination (1010)
Flashpoint (140°F)
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.32)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.42
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 832113
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 832113
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Original # 1
Page 10 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Anal tes Report
Y
ENVIROMMEWAL YECHNOWGIES,
INC, Cuyahoga Falls, Ohio 44223
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
20010926
Website: http://www.settek.com
07-Feb-20
Client: Synagro
State: NW
Project: DUNN WWTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20010926-OOIA Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
Original # 1
Page 11 of 32

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Page 31 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGa1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 20010926 RcptNo: 1
Logged by: Jacqueline Rasile 1/16/2020 9:55:00 AM
1.f•
Completed By: Jesseca E. Westfall 1/19/2020 7:11:35 PM �{G
Reviewed By:
Chain of Custody
1. Is Chain of Custody complete? Yes d❑ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑ No ❑d NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑d
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes V No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑ No ❑0 NA ❑
7. Sample(s) in proper container(s)?
Yes
V
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
V
No
❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
V
No
❑
10. Was preservative added to bottles?
Yes
❑
No
V NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
V
13. Does paperwork match bottle labels?
Yes
V
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
V
No
❑
15. Is it clear what analyses were requested?
Yes
0
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
melted ice
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
18.7
Goodl
Not Present
Page 32 of 32

Cameron Testing Services, Inc. Laboratory Report
lied Synagro CT8 Prnje
Projec ; Dunn WV"iP Regutatary
Sample Information
Sarrti fad'-T M. Goad 03117120 Recal red
Analyses and Results
2003-121
yus
J. Cameron apt,
CL
Lab ID Sample 10 x a M
Anafyle
ROSUIt
iY
2003-121 -01
Fee. Coliiarm-S
<35500
cru4
355co
=18nO ERf
e 02
<30100
CFUIQ
MI00
-03
<35500
1;Fuio
myco
-04
<35500
CFU19
35500
-05
<35500
cFwg
m5oo
-06
<35600
CM11;
361500
-o7
<35500
C uIQ
35500
Geoman
<34700
2003-121 -01 3ludof Gr
TS (%)
2,82%
O.G1
03117120 ERR
-02
3-32%
a.at
-03
2,82%
001
-04
Z 82%
c.0,
-05
2.82%
OV
«06
2,82%
0,01
-07
2.82%
0.01
Report -
Review IV c

e
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CAMERON TESTING SERVICES
Sample Preservation Check -In Sheet
Project # 061)3 --/
Checked In By:
Date:
Temp ,9, `j °C
Ti .
Driver:
Client
Delivered
CTS
arnpled
CTS
Pickup
US Mail
I
FedEx
General
Courier
UPS
Sample No
Matrix
Grab,
Container
Checked for Preservative by p
No Change
Red H<2
p (Red)
DW I W 15
C G
P G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / W W / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / W W / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / W W / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
p / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
COMMENTS:

Black River Wastewater Treatment Plant
City of Dunn
2020
Sept. 2020 Vector Attraction
Rec.—.81
Holding Tank—.66
.81 - .66 = 53.5
81 - (.81x.66)

APPENDIX 3
2021 PERMIT RENEWAL
City of Dunn (VQ0006101)
LAS CA
Land Owner Agreement Forms
Maps
Biosolid Utilization
CPLR Summary

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DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
15A NCAC 02T .1100 — LAND OWNER AGREEMENT
FORM: LOA 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted. the Applicant shall submit one original and two conies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting
General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of
Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit
this agreement for review without a corresponding application form (FORM: RLAP 06-16).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Land Owner Agreement (FORM: LOA 06-16):
❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the
Applicant.
❑ A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND
The undersigned landowner or his representative hereby permits:
Applicant's name: City of Dunn
hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land
application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this
Agreement:
Site/Field ID
Lease
(yes/no)
Land Use or
Cropping Patterns
Intended Use of Crops
Residuals Source
(optional)
Special note
(no-till/over-seed/
pasture)
CU-34 Fields 1-5
No
Bermuda Hay
Animal Consumption
The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the
Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and
shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and
stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement.
FORM: LOA 06-16 Page 1 of 3

L STIPULATIONS:
1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted
entity for the site(s) specified by this Agreement.
2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall
be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement.
3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met.
4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail
Service Center, Raleigh, NC 27699-1617.
5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new
landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land
application site(s).
6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program,
including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the
equipment used by the Permittee.
7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land
application event and a copy of the results of each soil analysis.
8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil
pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the
specified crop.
9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of
soil samples, and the permitted application limits.
10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients
(e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s).
11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for
the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application
events at appropriate periods.
12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or
his representative prior to and during a residuals land application event.
13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and
inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining
compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records
that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the
term of, and 12 months after termination of, this Agreement.
H. RESTRICTIONS:
1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application
site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of
signs that indicate the activities being conducted at the land application site(s).
2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application
sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application
events.
3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event.
4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month
period following a residuals land application event.
5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application
event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil.
6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application
event when the residuals remain on the land surface for less than four months prior to incorporation into the soil.
7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event.
HLALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one)
15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the compliance
boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided
the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following;
❑ A re -defined compliance boundary is needed for field(s) ID:
(Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance
boundary to the application package)
❑ A re -defined compliance boundary is not needed for this site.
IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed)
❑ The land application field(s) ID: is currently permitted under another
residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this
agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred
into the new program;
(Name of the new program)
FORM: LOA 06-16 Page 2 of 3

Landowner's Certification:
I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions
regarding the use of the land application site(s) on behalf of other deeded landowners OR that 1 am otherwise authorized, through
a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the
deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or
agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement,
understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of
field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified
herein.
Landowner name: Harold Lee Eldridge
Address: 8373 Rhodes Pond Road
City: Dunn
Phone: 1jy 72 3 /9),?6
Signature:
State: NC
Zip: 28334
Date: 4 !
NORTH CAROLINA, G ' G COUNTY 1 �/ Q
I, the undersigned Notary Public do hereby certify that 'q e tic 1`l�e-
personally appeared before me this day and acknowledged the due execution of the forgoing instrument.
..ne6geeeeeao..
WITNESS my hand and official seal this the
day of Jvne
Signature and seal:
My commission
Lessee's/Operator's Certification:
-as-- a o'2
17
/gyp 4]
1` A �Ca 44
1 certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Lessee/operator name:
Address:
City:
Phone:
Signature:
Permittee's Certification:
State:
E-mail
Date:
Zip:
I certify that 1 have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Signing afficial name: Heather Adams, Public Utilities Director
63
Date: A e1y/
FORM: LOA 06-16 Page 3 of 3

. APPLICATION MAP
LEGEND
APPLICATION AREA UNSUITABLE AREA
PRIVATE ROAD
STREAM
DRAIN
-x 9 N FENCE
PROPERTY LINE
WATER
ONSITE HOUSE
OFFSITE HOUSE
OUTBUILDING
0
WELL
The compliance boundary is established either 250 ft from the residuals application area or 50 feet within
in the property boundary, whichever is closest to the application area. The review boundary is established
midway between the compliance boundary and the perimeter of the residuals application area. All
locations are approximate.
GRAPHIC SCALE
1" = 660'
ss o sW
Figure 2
NC-CU-34
Fields 1-5

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT
FORM: LOA 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted. the Applicant shall submit one original and two conies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting
General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of
Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit
this agreement for review without a corresponding application form (FORM: RLAP 06-16).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Land Owner Agreement (FORM: LOA 06-16):
❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the
Applicant.
❑ A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND
The undersigned landowner or his representative hereby permits:
Applicant's name: City of Dunn
hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land
application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this
Agreement:
Site/Field ID
Lease
(yes/no)
Land Use or
Cropping Patterns
Intended Use of Crops
Residuals Source
(optional)
Special note
(no-till/over-seed/
pasture)
HA-08 Fields 8-9
No
Bermuda Hay
Animal Consumption
The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the
Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and
shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and
stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement.
FORM: LOA 06-16 Page 1 of 3

L STIPULATIONS:
1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted
entity for the site(s) specified by this Agreement.
2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall
be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement.
3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met.
4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail
Service Center, Raleigh, NC 27699-1617.
5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new
landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land
application site(s).
6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program,
including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the
equipment used by the Permittee.
7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land
application event and a copy of the results of each soil analysis.
8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil
pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the
specified crop.
9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of
soil samples, and the permitted application limits.
10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients
(e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s).
11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for
the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application
events at appropriate periods.
12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or
his representative prior to and during a residuals land application event.
13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and
inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining
compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records
that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the
term of, and 12 months after termination of, this Agreement.
H. RESTRICTIONS:
1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application
site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of
signs that indicate the activities being conducted at the land application site(s).
2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application
sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application
events.
3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event.
4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month
period following a residuals land application event.
5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application
event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil.
6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application
event when the residuals remain on the land surface for less than four months prior to incorporation into the soil.
7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event.
HLALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one)
15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the compliance
boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided
the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following;
❑ A re -defined compliance boundary is needed for field(s) ID:
(Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance
boundary to the application package)
❑ A re -defined compliance boundary is not needed for this site.
IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed)
❑ The land application field(s) ID: is currently permitted under another
residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this
agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred
into the new program;
(Name of the new program)
FORM: LOA 06-16 Page 2 of 3

Landowner's Certification:
I certify that I am a deeded landowner of the above -referenced land application sites) and am authorized to make decisions
regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through
a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the
deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or
agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement,
understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of
field transfer, and do hereby grant permission to the Perinittee to land apply residuals to the land application site(s) as specified
herein.
Landowner name: R. Harold Dixon
Address: PO Box 849
city: Coats State: NC Zip: 27521
✓ J 1
Phone: �- 9 E-mail address: i }hex ! d; t,(r�K�0-� V'AC rD t Ct+iiz
f�
Signature: Date: 6 �` i - Z4
NORTH CAROLINA, g-a 1'{''t L /t 1 COUNTY
I, the undersigned Notary Public do hereby certify that A. fla'rw Id on
personally appeared before me this day and acknowledged the due execution of the forgoing instrumQebtntl"@ Y�+eb
i
WITNESS my hand and official seal this the
�-0 Mom,
day of S,».e ,20 01
Signature and seal:
J
v t�
My commission expires: Q y-4,5 d4a3 ®, 1 �t
tiruc�u�e�
Lessee's/Operator's Certification:
I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Lessee/operator name:
Address:
city:
Phone:
Signature:
Permittee's Certification:
State:
E-mail
Date:
Zip:
I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Signing official name:
Signature:
Heather Adams, Public Utilities Director
Date:
FORM: LOA 06-1 G Page 3 of 3

APPLICATION MAP
LEGEND
APPLICATION AREA
UNSUITABLE AREA
— — — — — — PRIVATE ROAD
Q
WATER
— — — --- STREAM
ONSITE HOUSE
— DRAIN
.
OFFSITE HOUSE
X X FENCE
❑
OUTBUILDING
PROPERTY LINE
0
WELL
The compliance boundary is established either 250 ft from the residuals application area or 50 feet within
in the property boundary, whichever is closest to the application area. The review boundary is established
midway between the compliance boundary and the perimeter of the residuals application area. All
locations are approximate.
GRAPHIC SCALE
lit =660'
66U 0 660'
Figure 3
NC-HA-08
Fields 8-9

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