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HomeMy WebLinkAboutNCG060414_DMR_20210114 (2)STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 Date submitted 01-14-2021 CERTIFICATE OF COVERAGE NO. NCGO6 0 4 1 4 FACILITY NAME Amazon.com Services LLC. - DRT4 COUNTY Henderson PERSON COLLECTING SAMPLES Duncan Quinn LABORATORY Eurofins Test America Lab Cert. # 269 r F FB 0 1 "�fi_1 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2020 SAMPLE PERIOD ❑ Jan -June ❑■ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA ❑Zero -flow [—]Watersupply [_]SA ❑■ Other e FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ❑ use animal fats/byproducts PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall20.8 or ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, ni Oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0-9.0 120 30 10001 500' Parameter Code - C0530 00400 00340 00556 31616 61211 Sample Point 01 12/24/2020 28 8.15 9.0 2.5 N/A N/A Sample Point 02 12/24/2020 18 8.53 <5.0 <0.69 N/A N/A Sample Point 03 12/24/2020 <5.0 8.02 <5.0 <0.67 N/A N/A Sample Point 04 12/24/2020 13 7.52 27 <0.66 N/A N/A 1 Only applies to facilities that use/process meats. 1The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 45ee General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes ❑■ no (if ves, complete Part B) Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/S/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, IncheS2 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO 0 IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO rl REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR, includina all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing Signature of Permittee Permit Date:11/1/2018-05/31/2021 Date ZC SWU-249, Last Revised 11/5/2018 Page 2 of 2 eurofins Environment Testing America ANALYTICAL REPORT Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel:(912)354-7858 Laboratory Job ID: 680-193354-1 Client Project/Site: Storm Water - Amazon Warehouses (DRT4) For: ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade Authorized for release by. 111212021 9:12:45 AM Lauren Evans, Project Manager 1 (615)301-5034 Lauren. Evans@Eurofinset.com The test results in this report meet all 2003 NELAC, 2009 TNi, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Qualifiers General Chemistry Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. o Listed under the "D" column to designate that the result Is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re -extraction, or additional Initial metalslanion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DODIDOE) LOO Limit of Quantitation (DoDIDOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated NO Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative I Absent POS Positive I Present PQL Practical Quantitation Limit PRIES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins TestAmerica, Savannah Page 2 of 17 1/12/2021 Sample Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Lab Sample ID Client Sample ID Matrix Collected Received 680-193354-1 DRT4 SAMPLE POINT 01 20201224 Water 12/24/20 09:54 12/29/20 10:00 680-193354-2 DRT4_SAMPLE_POINT 02 20201224 Water 12/24/20 09:37 12/29/20 10:00 680-193354-3 DRT4 SAMPLE POINT 03 20201224 Water 12/2412010:41 12/29/20 10:00 680-193354-4 DRT4 SAMPLE POINT 04 20201224 Water 12/24/20 08:42 12/29/20 10:00 Job ID: 680-193354-1 Asset ID Eurofins TestAmerica, Savannah Page 3 of 17 1 /12/2021 Case Narrative Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Job ID: 680-193354-1 Laboratory: Eurofins TestAmerica, Savannah Narrative Job Narrative 680-193364-1 Comments No additional comments. Job ID:680-193354-1 Receipt The samples were received on 12/29/2020 10:00 AM; the samples arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 4.1° C. General Chemistry Method SM 254OD: The sample duplicate precision for the following sample associated with analytical batch 680-650893 was outside control limits: (680-193357-A-1 DU). The associated Laboratory Control Sample / Laboratory Control Sample Duplicate (LCS/LCSD) precision met acceptance criteria. Method SM 254OD: Insufficient sample volume was provided to produce results within the specifications of SM 2540D which requires at least 2.5 mg dried residue with a sample volume not to exceed 1 L. A sample volume less than 1 L, that yielded less than 2.5 mg dried residue, was provided for the following sample: DRT4_SAMPLE_POINT_03_20201224 (680-193354-3). Methods 1664B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 680-651693. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 4 of 17 1/12/2021 Client Sample Results Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Client Sample ID: DRT4_ SAMPLE_POINT_01_20201224 Lab Sample ID: 680-193354-1 Date Collected: 12/24/20 09:54 Matrix: Water Date Received: 12/29/20 10:00 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac Oil & Grease (HEM) 2.5 2.4 0.67 mg/L 01/11/21 07:55 01/11/21 10:48 1 Chemical Oxygen Demand 9.0 J 10 5.0 mg/L 01/07/21 10:54 1 Total Suspended Solids 28 6.5 6.5 mg/L 12/30/20 14:43 1 Eurofins TestAmerica. Savannah Page 5 of 17 1/12/2021 Client Sample Results Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Client Sample ID: DRT4_ SAMPLE_POINT_02_20201224 Lab Sample ID: 680-193354-2 Date Collected: 12/24/20 09:37 Matrix: Water Date Received: 12/29/20 10:00 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Oil & Grease (HEM) <0.69 2.5 0.69 mg/L 01/11/21 07:55 01/11/21 1048 1 Chemical Oxygen Demand <5.0 10 5.0 mg/L 01/07/21 10:54 1 Total Suspended Solids 18 5.0 5.0 mg/L 12/30/20 14:43 1 Eurofins TestAmerica, Savannah Page 6 of 17 1/12/2021 Client Sample Results Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Client Sample ID: DRT4_ SAMPLE_POINT_03_20201224 Lab Sample ID: 680-193354-3 Date Collected: 12/24/20 10:41 Matrix: Water Date Received: 12/29/20 10:00 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fae Oil & Grease (HEM) <0.67 2.4 0.67 mg/L 01/11/21 07:55 01/11/21 10:48 1 Chemical Oxygen Demand <5.0 10 5.0 mg/l. 01/07/21 10:54 1 Total Suspended Solids <5.0 5.0 5.0 mg/L 12/30/20 14:43 1 Eurofins TestAmerica, Savannah Page 7 of 17 1/12/2021 Client Sample Results Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water -Amazon Warehouses (DRT4) Client Sample ID: DRT4 SAMPLE_POINT_04_20201224 Lab Sample ID: 680-193354-4 Date Collected: 12/24/20 08:42 Matrix: Water Date Received: 12/29/20 10:00 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac Oil & Grease (HEM) <0.66 2.4 0.66 mg/L 01/11/21 07:55 01/11/21 10:48 1 Chemical Oxygen Demand 27 10 5.0 mg/L 01/07/21 10:54 1 Total Suspended Solids 13 5.7 5.7 mg/L 12/30/20 14:43 1 Eurofins TestAmerica, Savannah Page 8 of 17 1/12/2021 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Method: 1664B - HEM and SGT-HEM Lab Sample ID: MB 680-65169311-A Matrix: Water Analysis Batch: 651719 MB MB Analyte Result Qualifier Oil & Grease (HEM) <1.4 Lab Sample ID: LCS 680-651693/2-A Matrix: Water Analysis Batch: 651719 Job ID:680-193354-1 Client Sample ID: Method Blank Prep Type: TotalINA Prep Batch: 651693 RL MDL Unit D Prepared Analyzed oil Fac 5.0 1.4 mg/L 01111/2107:55 01/11/2110:48 1 �. Spike Los LCS Analyte Added Result Qualifier Oil & Grease (HEM) 40.0 33.20 Lab Sample ID: LCSD 680-65169313-A Matrix: Water Analysis Batch: 651719 Analyte LOil & Grease (HEM) Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch:651693 %Rec. Unit D %Rec Limits mg/L 83 78-114 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch:651693 Spike LCSD LCSD %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 40.0 34.40 mg/L 88 78-114 4 18 Method: 5220D-2011 - Chemical Oxygen Demand Lab Sample ID: MB 680-65157413 Matrix: Water Analysis Batch: 651574 MB MB Analyte Result Qualifier Chemical Oxygen Demand 15.0 Client Sample ID: Method Blank Prep Type: Total/NA RL MDL Unit D Prepared Analyzed Dil Fac 10 5.0 mg/L 61/07/2110:54 1 Lab Sample ID: LCS 680-651574/4 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 651574 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 50.0 52.1 mg/L 104 90-110 Method: SM 2540D - Solids, Total Suspended (TSS) Lab Sample ID: MB 680-650893/1 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 650893 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac Total Suspended Solids <2.5 2.5 2.5 mg/L 12/30/20 14:43 1 FLab Sample ID: LCS 680-650893/2 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 650893 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 951 926 mg/L 97 80 - 120 Eurofins TestAmerica, Savannah Page 9 of 17 1/12/2021 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Job ID:680-193354-1 Method: SM 2540D - Solids, Total Suspended (TSS) (Continued) Lab Sample ID: LCSD 680-650893/3 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch:650893 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 951 964 mg/L 101 80-120 4 25 Eurofins TestAmerica, Savannah Page 10 of 17 1/12/2021 QC Association Summary Client: ERNI-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) General Chemistry Analysis Batch: 650893 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-193354-1 DRT4_SAMPLE_POINT_01_20201224 - TotatINA Water SM 25400 680-193354-2 DRT4_SAMPLE_POINT_02_20201224 TotaVNA Water SM 2540D - 680-193354-3 DRT4_SAMPLE_POINT_03_20201224 Total/NA Water SM 2540D 680-193354-4 DRT4_SAMPLE_POINT_04_20201224 Total/NA Water SM 2540D MB 680-650893/1 Method Blank Total/NA Water SM 2540D LCS 680-650893/2 Lab Control Sample Total/NA Water SM 2540D LCSD 680-650893/3 Lab Control Sample Dup TotaVNA Water SM 2540D Analysis Batch: 651574 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch _ _ 680-193354-1 ORT4_SAMPLE_POINT_O1_20201224 TotaVNA Water 5220D-2011 - 680-193354-2 DRT4_SAMPLE_POINT_02_20201224 Total/NA Water 5220D-2011 680-193354-3 DRT4_SAMPLE_POINT 03_20201224 Total/NA Water 5220D-2011 680-193354-4 DRT4_SAMPLE_POINT_04_20201224 Total/NA Water 5220D-2011 MB 680-651574/3 Method Blank TotaVNA Water 5220D-2011 LCS 680-651574/4 Lab Control Sample TotaVNA Water 5220D-2011 Prep Batch: 651693 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-193354-1 DRT4_SAMPLE_POINT_01_20201224 TotaVNA Water 1664E 680-193354-2 DRT4_SAMPLE_POINT_02_20201224 TbtaVNA Water 1664E 680-193354-3 DRT4_SAMPLE_POINT_03_20201224 Total/NA Water 1664E 680-193354-4 DRT4_SAMPLE_POINT_04_20201224 Total/NA Water 1664E MB 680-651693/1-A Method Blank TotaVNA Water 1664E LCS 680-65169312-A Lab Control Sample TotaVNA Water 1664B LCSD 680-65169313-A Lab Control Sample Dup TotaVNA Water 1664E Analysis Batch: 651719 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-193354-1 DRT4_SAMPLE_POINT_01_20201224 TotaVNA Water 1664B 651693 680-193354-2 DRT4_SAMPLE_POINT_02_20201224 Total/NA Water 16646 651693 680-193354-3 DRT4_SAMPLE_POINT 03_20201224 TotaVNA Water 1664E 651693 680-193354.4 DRT4_SAMPLE_POINT_04_20201224 TotaVNA Water 16643 651693 MB 680-651693/1-A Method Blank Total/NA Water 16648 651693 LCS 680-651693/2-A Lab Control Sample Total/NA Water 1664E 651693 LCSD 680-651693/3-A Lab Control Sample Dup Total/NA Water 1664E 651693 Eurofins TestAmerica, Savannah Page 11 of 17 1/12/2021 Lab Chronicle Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Client Sample ID: DRT4_SAMPLE_POINT_01_20201224 Lab Sample ID: 680-193354-1 Date Collected: 12/24/20 09:54 Matrix: Water Date Received: 12/29/20 10:00 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 1664E 1050mL 500ML 651693 01/11/2107:55 JAS TALSAV TotaVNA Analysis 1664E 1 651719 01/1112110:48 JAS TALSAV Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL 2 mL 651574 01/07/21 10:54 ALG TALSAV Instrument ID: SPC7 TbtaVNA Analysis SM 2540D 1 384 mL 1000 mL 650893 12/30/20 14:43 MS TAL SAV Instrument ID: NOEQUIP Client Sample ID: DRT4_ SAMPLE_POINT_02_20201224 Lab Sample ID: 680-193354-2 Date Collected: 12/24/20 09:37 Matrix: Water Date Received: 12/29/20 10:00 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount ­mL Number or Analyzed - Analyst Lab Total/NA Prep 16648 1016 mL 500 6516 33 1111121 07:55 JAS TALSAV TotaVNA Analysis 16648 1 651719 01111/2110:48 JAS TALSAV Instrument ID: NOEQUIP TbtaVNA Analysis 5220D-2011 1 2mL 2ml- 651574 01/07/21 10:54 ALG TALSAV Instrument ID: SPC7 TotaVNA Analysis SM 2540D 1 500 mL 1000 mL 650893 12/30/20 14:43 MS TALSAV InstrumentlD: NOEQUIP Client Sample ID: DRT4_ SAMPLE_POINT_03_20201224 Lab Sample ID: 680-193354-3 Date Collected: 12/24/20 10:41 Matrix: Water Date Received: 12/29/20 10:00 Batch Batch oil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab TotaVNA Prep 1664E 1048mL 500­mL 651-6 33 01/11/2107:55 JAS TALSAV TotaVNA Analysis 1664B 1 651719 01/11/2110:48 JAS TALSAV Instrument ID: NOEQUIP TotaUNA Analysis 5220D-2011 1 2 mL 2 mL 651574 01/07/21 10:54 ALG TAL SAV Instrument ID: SPC7 TotaUNA Analysis SM 2540D 1 500 mL 1000 mL 650893 12/30/20 14:43 MS TAL SAV Instrument ID: NOEQUIP Client Sample ID: DRT4_ SAMPLE_POINT_04_20201224 Lab Sample ID: 680-193354-4 Date Collected: 12/24/20 08:42 Matrix: Water Date Received: 12/29/20 10:00 Prep Type Batch Batch Type Method DII Run Factor Initial Amount Final Amount Batch Number Prepared or Analyzed Analyst Lab TotsVNA Prep 16646 1053 mL 500 mL 6516 33 - 1111121 07:55 JAS TAL SAV TotaVNA Analysis 1664B 1 651719 0111112110:48 JAS TALSAV Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL 2 mL 651574 01/07/21 10:54 ALG TALSAV Instrument ID: SPC7 Total/NA Analysis SM 2540D 1 440 mL 1000 mL 650893 12/30/20 14:43 MS TALSAV Instrument ID: NOEQUIP Eurofins TestAmerica, Savannah Page 12 of 17 1/12/2021 Lab Chronicle Client: ERM-West Job ID: 680-193354-1 ProjectlSite: Storm Water - Amazon Warehouses (DRT4) Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 13 of 17 1 /12/2021 Accreditation/Certification Summary Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Laboratory: Eurofins TestAmerica, Savannah The accreditation/certifications listed below are applicable to this report. [Authority Program Identification Number Expiration Date North Carolina(WW/SPV) State 269 12 1-21 0 Eurofins TestAmerica, Savannah Page 14 of 17 1/12/2021 Method Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Method Method Description 1664B HEM and SGT-HEM 5220D-2011 Chemical Oxygen Demand SM 2540D Solids, Total Suspended (TSS) 1664E -HEM and SGT-HEM (Aqueous) Protocol References: 1664B = EPA-821-98-002 SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Job ID: 680-193354-1 Protocol Laboratory 1664E TAL SAV SM TAL SAV SM TAL SAV 1 1664B TAL SAV �. Eurofins TestAmerica, Savannah Page 15 of 17 1/12/2021 LZOZ/Z6/6 L6 JO 96 abed S D• y� gg $gg ; Z U? tl %% ? J- O F .. y ; O 7 A -i �.0 o N J � O y 0 o fG u IQ) n 1 7 u A „Z 3 33 i aJ Ri i.l N� 3 aII s 3 4 J C ry y )J S 5 G n o 7 '^ S iIWrW w 3 Z 2 2> 0616000 y _ D )J }1 AU 148N_NP-XEY IDi16 Grw�) � m J A dig { y VMD-COD m � ci of A �I� N H 4 6 1 3 i 2 s .t �. � i 11h1t1umMro/owblwn N IIII IIIIII itIII II!IItl� ; .2 OF<cgNnovoz. $ m n n 3 680-193354 Cnam of Cusiooy e§pBY= n S Df 0 0 c 0 c. ID O Q f:.; Login Sample Receipt Checklist Client: ERM-West Job Number: 680-193354-1 Login Number: 193354 List Source: Eurofins TestAmerica, Savannah List Number: 1 Creator: Mooken, DarmalIL ' Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey NIA meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins TestAmerica, Savannah Page 17 of 17 1/12/2021 January 14,2021 Wastewater Branch Water Quality Permitting Section Division of Water Resources 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Delegation of Signature Authority AMAZON.COM SERVICES LLC. - DRT4 NPDES Permit Number NCG060414 To Whom It May Concern: By notice of this letter, I hereby delegate signatory authority to each of the following individuals for all permit applications, discharge monitoring reports, and other information relating to the operations at the subject facility as required by all applicable federal, state, and local environmental agencies specifically with the requirements for signatory authority as specified in 15A NCAC 213.0506. Individual #1 Individual #2 (ifapplicable) Name: Michael Boese Title: Business Environmental Leader Mailing Address: Na Environmental Dept Po Box 80842 Seattle, Wa 98108 Physical Address: (if different) Email Address: boese@amazon.com Office Phone: 484 - 252 - 1748 Mobile Phone: - If you have any questions regarding this letter, please feel free to contact me at 951-445-7785. Sincerely, see attached delegation authority Michael D. Deal President, Treasurer And Secretary cc: Asheville Regional Office, Water Quality Permitting Section DocuSign Envelope ID: 110ECCCC-4COB-4164-917A-E418C922A295 AMAZON.COM SERVICES LLC DELEGATION OF AUTHORITY (Boese, Nickens, Wilson, Vijaykumar, Sanches) I, Michael D. Deal, being the duly elected, qualified and acting President, Treasurer and Secretary of Amazon.com Services LLC (the "Company"), and having been authorized by resolutions duly adopted by the Board of the Company, do hereby sub -delegate my authority as follows: DELEGATION OF AUTHORITY 1. Effective September 10, 2020, authority is hereby delegated to Michael Boese, Amber Nickens, Paul Wilson, Vimal Vijaykumar, and Debora Sanches ("Authorized Representatives") to act on behalf of the Company and in its name and place to execute and file environmental and permitting applications, and related documents with government authorities. This Delegation of Authority shall not include any authority to commit spend on behalf of the Company. SUBDELEGATION 2. The Authorized Representatives are not authorized to subdelegate the authority granted to them in this delegation. TERM OF DELEGATION 3. The authority delegated hereby shall terminate upon the earlier of: (i) when revoked by the Company, the undersigned, any successor in responsibility to the undersigned, or any person to whom the undersigned reports; or (ii) immediately upon the cessation of the Authorized Representative's employment by Amazon.com, Inc. ("Amazon"), the Company, and Amazon's affiliates. 4. The authority delegated herein shall remain in full force and effect until terminated in accordance with Section 3 of this Delegation of Authority regardless of the appointment status of the undersigned with the Company. DATED: September 10, 2020 VLr A/ Michael D. Deal President, Treasurer and Secretary