NCG030134_DMR_20210324 (2)

ThermoRsher
S C I E N T I F I C
March 24, 2021
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Stormwater Analytical Monitoring Results for Thermo Fisher Scientific, LLC
I have attached the analytical monitoring results from stormwater sampling that was collected
on February 26, 2021 at Thermo Fisher Scientific, LLC's four outfalls.
Per our General Storm Water Permit No. NCG03000 requirements of monthly monitoring for
applicable parameters during a storm event, I have sampled each outfall for copper, zinc, pH,
lead, TSS, and Non -Polar Oil/Grease/TPH. Results show that TSS at one outfall, copper at two
outfalls, and zinc at all four outfalls were above the benchmark values, as noted in Table 3 of the
general storm water permit. All other results were below the benchmark values. We have
implemented a Tier Three response for the site and Thermo Fisher Scientific, LLC has notified
the Asheville Regional Office. Thermo Fisher Scientific, LLC is currently working with an
environmental consultant to help achieve compliance with the benchmark values set forth in
the facility's storm water permit. I have attached the completed Monitoring Report containing
the monitoring results from the four outfalls.
If you have any questions, please feel free to contact me at 828-658-2845.
Jeremy Putnam
Sr. EHS Manager
Attachments: 1

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted: 03/24/2021
CERTIFICATE OF COVERAGE NO. N00030134
FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS
LABORATORY: Pace Analytical Lab Cert. ff
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR
SAMPLE PERIOD —Jan-June_July-Dec
p roc Or X Monthly: February
RECEII/ HARGINGTOCLASS R1 ❑HQW "rout ❑PNA
❑Zero -flow ❑Hater Supply ❑SA
APR 05 2021 ❑other
CENTRAL FILES
DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3
F—Wo discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organics
Benchmarks
_
-
100 mg/L or 50 mg/O
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Outfalll
2/26/2021
0.3
19.0
6.75
10.0057
<0.005
0.150
<5
N/A
Outfall2
2/26/2021
0.3
40.8
5.6
0.0411
0.005
0.241
<5
N/A
Outfall3
2/26/2021
0.3
117.0
5.45
0.0556
0.0117
0.254
<5
N/A
Outfall4
2/26/2021
0.3
11.9
5.4
0.005
0.005
0.189
<5
N/A
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO
monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the
General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),
I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent
management plan included in the Stormwater Pollution Prev tion Plan."
i
Name (Print name)
Tie tint title)
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
FlNo discharge this period?2
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/O
Parameter Code
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?
YES X NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert
(Asheville Regional Office)
Mail an original copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitorina period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aWpre that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
o3�a3 � a
Date
Permit Date: 11/1/2018-05/31/2021
11/1/2018
SWU-245, last revised

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted: 03/24/2021
CERTIFICATE OF COVERAGE NO. NCG030134
FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS
LABORATORY: Pace Analytical Lab Cert. ff
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR: 2020
SAMPLEPERIOD _Jan-JuneJuly-Dec
Or X Monthly: January
��/ * R�Sfi AGING TO CLASS n ORW F X❑Frout nPNA
1, P J i ❑Zero -flow ❑NaterSupply [:]SA
APR 0 5 2021 [_]Other
CENTFu\L FILES
DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -
nNo dischorcie this period?Z
Outfall No.
Date Sample
P
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
p H,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics'
Benchmarks
-
-
100 mg/L or 50 mg/L'
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Outfall 1
Outfall 2
Outfall 3
Outfall 4
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO
monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the
General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),
I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent
management plan included in the Stormwater Pollution P ion Plan."
Name (Print name)
itle (Print title)
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: !f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
Fl No discharge this period ?2
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/V
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: !f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?
YES X NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert
(Asheville Regional Office)
Mail an original copy of this DW including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
a ware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
o a-,�C)�"
Signature of Permittee
Date
Permit Date: 11/1/2018-05/31/2021
11/1/2018
SWU-245, last revised

aceAna1j6ca1
www.pmis6p.com
1
March 09, 2021
Mr. Jeremy Putnam
Thermo Electron Corp.
275 Aiken Road
Asheville, NC 28804
RE: Project: Feb.2021 SW 2/26
Pace Project No.: 92524538
Dear Mr. Putnam:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 26, 2021. The results relate only
to the samples included In this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, LLC.
Page 1 of 13

aceAnalocal
/ www.pacalabscom
Project: Feb.2021 SW 2/26
Pace Project No.: 92524538
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification M 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification M 84
Virginia/VELAP Certification M 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification M 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 13

I e
aceAnalytical
www.pacelebLcom
f
SAMPLE ANALYTE COUNT
Project: Feb.2021 SW 2126
Pace Project No.: 92524538
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92524538001
1
EPA 1664B
CJM
1
PASI-C
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
SM 254OD-2011
RED
1
PASI-A
92524538002
2
EPA 1664B
CJM
1
PASI-C
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
SM 254OD-2011
RED
1
PASI-A
92524538003
3
EPA 1664B
CJM
1
PASI-C
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
SM 254OD-2011
RED
1
PASI-A
92524538004
4
EPA 1664E
CJM
1
PASI-C
EPA 1664E
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
SM 254OD-2011
RED
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

/�5aan'c('%. en Analytical
www.paceleb.com
iI
ANALYTICAL RESULTS
Project: Feb.2021 SW 2/26
Pace Project No.: 92524538
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: 1
Lab ID: 92524538001 Collected:
02/26/21 12:45
Received: 02/26/21 13:45 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
03/09/21 10:17
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
03/09/21 10:17
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
5.7 ug/L
5.0
1
03/07/21 17:20 03/08/21 12:25 7440-50-8
Lead
ND ug/L
5.0
1
03/07/21 17:20 03/08/21 12:25 7439-92-1
Zinc
150 ug/L
10.0
1
03/07/21 17:20 03/08/21 12:25 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
19.0 mg/L
6.1
1
03/03/21 22:33
Sample: 2 Lab ID: 92524538002 Collected: 02/26/21 13:00 Received: 02/26/21 13:45 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No.
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
03/09/21 10:17
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
03/09/21 10:17
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
41.1 ug/L
5.0
1
03/07/21 17:20 03/08/21 12:35 7440-50-8
Lead
ND ug/L
5.0
1
03/07/21 17:20 03/08/21 12:35 7439-92-1
Zinc
241 ug/L
10.0
1
03/07/21 17:20 03/08/21 12:35 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
40.8 mg/L
6.2
1
03/03/21 22:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/09/2021 04:16 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 4 of 13

a Analytical
www.pacelabscom
i
ANALYTICAL RESULTS
Project: Feb.2021 SW 2/26
Pace Project No.: 92524538
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: 3
Lab ID: 92524538003 Collected:
02/26/21 13:15
Received: 02/26/21 13:45 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
03/09/21 10:17
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
03/09/21 10:17
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
55.6 ug/L
5.0
1
03/07/21 17:20 03/08/21 12:38 7440-50-8
Lead
11.7 ug/L
5.0
1
03/07/21 17:20 03/08/21 12:38 7439-92-1
Zinc
254 ug/L
10.0
1
03/07/21 17:20 03/08/21 12:38 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
117 mg/L
25.0
1
03/03/21 22:34
Sample: 4 Lab ID: 92524538004 Collected: 02/26/21 13:30 Received: 02/26/21 13:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease ND mg/L 5.0 1 03/09/21 10:17
1664 SGT-HEM, TPH Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons ND mg/L 5.0 1 03/09/21 10:17
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper ND ug/L 5.0 1 03/07/21 17:20 03/08/21 12:42 7440-50-8
Lead ND ug/L 5.0 1 03/07/21 17:20 03/08/21 12:42 7439-92-1
Zinc 189 ug/L 10.0 1 03/07/21 17:20 03/08/2112:42 7440-66-6
2540D Total Suspended Solids Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids 11.9 mg/L 3.5 1 03/03/21 22:35
Date: 03/09/2021 04:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 13

aceAnalytical
www.pacelebs.com
QUALITY CONTROL DATA
Project: Feb.2021 SW 2/26
Pace Project No.: 92524538
QC Batch: 604994 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples. 92524538001, 92524538002, 92524538003, 92524538004
METHOD BLANK: 3187522 Matrix: Water
Associated Lab Samples: 92524538001, 92524538002, 92524538003, 92524538004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 03/09/21 10:17
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 3187523
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 40 32.0 80 78-114
MATRIX SPIKE SAMPLE:
Parameter
Oil and Grease
3187524
92525094001 Spike MS MS
Units Result Conc. Result % Rec
mg/L ND 40 34.1
o/ Ran
82 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/09/2021 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

an Analytical
t+nww.pa>:efafu.eom
1
QUALITY CONTROL DATA
Project: Feb.2021 SW 2126
Pace Project No.: 92524538
QC Batch: 604999 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92524538001, 92524538002, 92524538003, 92524538004
METHOD BLANK: 3187550 Matrix: Water
Associated Lab Samples: 92524538001, 92524538002, 92524538003, 92524538004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.0 03/09/21 10:17
LABORATORY CONTROL SAMPLE: 3187551
Spike LCS LCS
Parameter Units Conc. Result % Rec
Total Petroleum Hydrocarbons mg/L 20 12.9
MATRIX SPIKE SAMPLE:
Parameter
Total Petroleum Hydrocarbons
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
% Rec
Limits Qualifiers
64 64-132
3187552
92525094001 Spike MS MS
Units Result Conc. Result % Rec
mg/L ND 20 13.8
% Rec
Limits Qualifiers
63 64-132 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 03/09/2021 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

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QUALITY CONTROL DATA
Project: Feb.2021 SW 2126
Pace Project No.: 92524538
QC Batch: 604799 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92524538001, 92524538002, 92524538003, 92524538004
METHOD BLANK: 3186433
Matrix: Water
Associated Lab Samples:
92524538001, 92524538002, 92524538003, 92524538004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Copper
ug/L
ND 5.0
03/08/2117:57
Lead
ug/L
ND 5.0
03/08/2117:57
Zinc
ug/L
ND 10.0
03/08/2117:57
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
3186434
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Copper
ug/L
500 526
105 85-115
Lead
ug/L
500 502
100 85-115
Zinc
ug/L
500 497
99 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3186435
3186436
MS
MSD
92524538001
Spike
Spike
MS
Parameter Units
Result
Conc.
Conc.
Result
Copper ug/L
5.7
500
500
411
Lead ug/L
ND
500
500
401
Zinc ug/L
150
500
500
548
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3186437
3186438
MS
MSD
92525328001
Spike
Spike
MS
Parameter Units
Result
Conc.
Conc.
Result
Copper ug1L
117
500
500
532
Lead ug/L
ND
500
500
393
Zinc ug/L
ND
500
500
450
MSD
MS
MSD
% Rec
Result
% Rec
% Rec
Limits RPD Qual
422
81
83
70-130 3
412
80
82
70-130 3
566
80
83
70-130 3
MSD MS MSD % Rec
Result % Rec % Rec Limits RPD Qual
617 83 100 70-130 15
449 79 90 70-130 13
527 81 97 70-130 16
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/09/2021 04:16 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

;a'tc.%tai AnalXical
www.paselsl P M 14
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QUALITY CONTROL DATA
Project: Feb.2021 SW 2/26
Pace Project No.: 92524538
QC Batch: 604031 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92524538001, 92524538002, 92524538003, 92524538004
METHOD BLANK: 3182324 Matrix: Water
Associated Lab Samples: 92524538001, 92524538002, 92524538003, 92524538004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 03/03/21 22:27
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 3182325
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L 250 248 99 90-110
SAMPLE DUPLICATE: 3182588
92524582006 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids
mg/L 1420 1080 27 D6
SAMPLE DUPLICATE: 3182589
92524582007 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids
mg/L 6200 6750 8
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 03/09/2021 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

I el
a^Amalytical
www.pacclabs.com
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QUALIFIERS
Project: Feb.2021 SW 2126
Pace Project No.: 92524538
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/09/2021 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 13

aceAnalyr'cal
www.pacelabs.com
Project: Feb.2021 SW 2/26
Pace Project No.: 92524538
Lab ID
92524538001
92524538002
92524538003
92524538004
92524538001
92524538002
92524538003
92524538004
92524538001
92524538002
92524538003
92524538004
92524538001
92524538002
92524538003
92524538004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Sample ID QC Batch Method QC Batch Analytical Method
1 EPA 1664E
604994
2 EPA 1664E
604994
3 EPA 1664B
604994
4 EPA 1664E
604994
1 EPA 1664E
604999
2 EPA 1664B
604999
3 EPA 1664E
604999
4 EPA 1664B
604999
1 EPA 200.7 Rev 4.4 1994
604799
2 EPA 200.7 Rev 4.4 1994
604799
3 EPA 200.7 Rev 4.4 1994
604799
4 EPA 200.7 Rev 4.4 1994
604799
1 SM 2540D-2011
604031
2 SM 2540D-2011
604031
3 SM 2540D-2011
604031
4 SM 2540D-2011
604031
Date: 03/09/2021 04:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
EPA 200.7 Rev 4.4 1994 604802
EPA 200.7 Rev 4.4 1994 604802
EPA 200.7 Rev 4.4 1994 604802
EPA 200.7 Rev 4.4 1994 604802
Page 11 of 13

W0# •9Z5Z4b " rkorder Number or r
�CHAIN-OF-CUSTODY Analytical Request Document
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Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields
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Company:Billing
Information:
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92524538
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Address'.
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Report To. Put
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Email To: amV 1 f1�m0 s�1 � ��'✓i
•' Preservative Types: (1) nitric acid, (2) sulfuric acid, (31 hydrochloric acid, (4) sodium hytlroxiste, (5) tint acetate.
(6) methanol, (7) sodium bisulfate, (8) sodium thiasulfate,191 hexane, (A) ascorbic acid, (ii) ammonium sulfate,
(C) ammonium hydroxide, ID) TSP, (U) Unpreserved, (0) Other
Copy To:'Site
Colle . ion lefo/Address:
Analyses
Lab Profile/Line:
i 5
Customer Project Name/Number:
Stale: County/City: Time Zone Collected:
( (PT[ (MT( I CT (Aj ET
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Lab Sample Receipt Checklist:
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Custody Seals Present/Intact G) NA
Gu atody Signatures Present N HA
Collector Signature present 14 NA
Phone: gZ,�.• IDS�''2. S
Site/Facility ID it;
Compliance Monitoring
Email:
I Yes ( I No
T
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bottles Intact Y H NA
Correct Bottles N NA
SuLf icient volume N NA
Samples Received on Ice tJ N
VOA — Headspace Acceptable Y tJ
USDA Regulated Soilss ,i, iJ A
Collected By (print
YV r 1 0 kftoj ' �
Purchase Order H:
Quote li:
DW PWS ID It:
DW Location Code:
Ile ed By gnaturej:
Turnaround Date Required:
hnme( Gate y Pac ed on Ice:
Yes ( ]No
to
Samples in 11old.ing Time N RA
Residual Chtor. inu Yrenent Y Fr iA>
�/
Cl Strips:
Sample Disposal
Rush:
I•ield Filtered (if applicable):
( I Dispose as appropriate ( ! Return
Archive:
( ) Same Day I I Next Day
I) 2 Da I ) 3 Day ( I4 Day ( ) S Day
( 1 Yes I ]NoW-V
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Sample pH Acceptable f Y N NA
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(Expedite Charges APPIY)
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Sulfide present Y N
Lead Acetate strips: ...........
LAB USE ONLY:
• Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Lab Sample # / Comments:
Comp /
Collected (or
Res
if of
Customer Sample ID
Matrix '
Grab
Composite Start)
Composite End
Cl
CtnsV
kq
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Date
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Customer Remarks / Special Conditions / Possible I la:ards: Type of Ice Used: Wet Blue Dry None SHORT HOLDS PRESENT (c72 hours); Y N N/A
Lab Sample Temperature Info:
Y NA
Packing Material Used: "'• c:• Lab Tracking ft:
1'� ,"
> "�`' 2427024
Temp Blank Received:
Therm IDtt: % t
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7
Cooler 1 Temp Upon Receipt: �..,� oC
()
Samples received via:
Y N fA
Cooler 1 Therm Corr. Factor: oC
Radchem sample(s) screened (<SOU cpm):
FEDEX UPS Client Courier Pace Courier
Cooler 1 Corrected Temp: �_ aC
Ralir quisIed by/Company: (Signature) Date/Time: Receivpo" /Company, (Sign)attire) `' Date/Time: MTJL LAB USE ONLY
\��'.�- Table p:Lf
Comments:
_
Acctnum.
Relinquished by/Company: (Signature) Date/lime: Ret:elved by/Company: (Signature) Date/Time: Template:
p Tri Blank Received: Y N NA
Prclogirt:
HCL McOH TSP Other
Relinquished by/Con►pany: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: PM:
Non Conforru ce(s):
YES / t
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