NCG030134_DMR_20210112 (2)

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted: 01/12/2021
CERTIFICATE OF COVERAGE NO. NCG030134
FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS
LABORATORY: Pace Analytical Lab Cert. #
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR
SAMPLE PERIOD — Jan -June _July -Dec
OrXMonthly: December
DISCHARGING TO CLASS ❑ ORW ❑ HQW "rout ❑PNA
❑Zero -flow ❑NaterSupply ❑SA
❑Other
JAN 2 5 2021PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -
„ f E3
DNliR
F—UVo discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
PH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
TotalToxic
Organics'
Benchmarks
-
-
100 mg/L or 50 mg/V
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Outfall 1
12/24/2020
0.6
23.2
6.4
0.011
<0.005
0.302
<5
N/A
Outfall2
12/24/2020
0.6
14.1
6.6
0.0126
0.005
1102
<5
N/A
Outfall3
12/24/2020
.6
37.2
6.4
0.0253
0.005
1168
<5
N/A
Outfall4
12/24/2020
0.6
10.3
6.5
<0.005
0.005
3.317
<5
N/A
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO
monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the
General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),
I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent
management plan included in the Stormwater Pollution Prev i Plan."
Name (Print name)
%ient title)
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
F--]No discharge this period ?2
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/O
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?
YES X NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert
(Asheville Regional Office)
Mail an original copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
tho=hat
ns directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am therpre significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of
Date
Permit Date: 11/1/2018-05/31/2021
11/1/2018
SWU-245, last revised

Thermo Posher
S C I E N T I F I C
January 12, 2021
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Stormwater Analytical Monitorine Results for Thermo Fisher Scientific, LLC
I have attached the analytical monitoring results from stormwater sampling that was collected
on December 24, 2020 at Thermo Fisher Scientific, LLC's four outfalls.
Per our General Storm Water Permit No. NCG03000 requirements of monthly monitoring for
applicable parameters during a storm event, I have sampled each outfall for copper, zinc, pH,
lead, TSS, and Non -Polar Oil/Grease/TPH. Results show that both copper and zinc were above
the benchmark values at three of the four outfalls, as noted in Table 3 of the general storm
water permit. All other results were below the benchmark values. We have implemented a Tier
Three response for the site and Thermo Fisher Scientific, LLC has notified the Asheville Regional
Office. Thermo Fisher Scientific, LLC is currently working with an environmental consultant to
help achieve compliance with the benchmark values set forth in the facility's storm water
permit. I have attached the completed Monitoring Report containing the monitoring results
from the four outfalls.
If you have any questions, please feel free to contact me at 828-658-2845.
Jeremy Putnam
Sr. EHS Manager
Attachments: 1

( ace Analytical
www.pecelehs.cam
January 11, 2021
Mr. Jeremy Putnam
Thermo Electron Corp.
275 Aiken Road
Asheville, NC 28804
RE: Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Dear Mr. Putnam:
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 24, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, -LC.
Page 1 of 12

aceAnalytical
www.pacelelu cm
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Flodda/NELAP Certification #: E87648
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
South Carolina Certification M 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification M 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 12

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SAMPLE ANALYTE COUNT
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92513743001
1
EPA 1664B
CJM
1
PASI-C
EPA 1664E
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
DS
3
PASI-A
SM 2540D-2011
ALP
1
PASI-A
92513743002
2
EPA 1664B
CJM
1
PASI-C
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 2540D-2011
ALP
1
PASI-A
92513743003
3
EPA 1664B
CJM
1
PASI-C
EPA 1664E
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH 1
3
PASI-A
SM 254OD-2011
ALP
1
PASI-A
92513743004
4
EPA 1664B
CJM
1
PASI-C
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH 1
3
PASI-A
SM 254OD-2011
ALP
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 12

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ANALYTICAL RESULTS
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: 1
Lab ID: 92513743001 Collected:
12/24/20 11:00
Received: 12/24/20 12:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
01/08/21 11:22
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
01/08/21 11:22
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
11.0 ug/L
5.0
1
01/06/2100:56 01/06/2120:32 7440-50-8
Lead
ND ug/L
5.0
1
01/06/2100:56 01/06/2120:32 7439-92-1
Zinc
302 ug/L
10.0
1
01/06/2100:56 01/0612120:32 7440-66-6
2640D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
23.2 mg/L
2.5
1
12/29/20 11:28
Sample: 2
Parameters
Lab ID: 92513743002 Collected: 12/24/20 11:15
Results Units Report Limit DF
Received: 12/24/20 12:24 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
01/08/21 11:22
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
01/08/21 11:22
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
12.6 ug/L
5.0
1
01/06/2100:56 01/0612120,48 7440-50-8
Lead
ND ug/L
5.0
1
01/06/2100:56 01/0612120:48 7439-92-1
Zinc
102 ug/L
10.0
1
01/06/2100:56 01/0612120:48 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
14.1 mg/L
3.0
1
12/29/20 11:28
Date: 01 /11/2021 07:30 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, LLC.
Page 4 of 12

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ANALYTICAL RESULTS
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: 3 Lab ID: 92513743003 Collected: 12/24/20 11:30 Received: 12/24/20 12:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
01/08/21 11:22
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
01/08/21 11:22
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
25.3 ug/L
5.0
1
01/06/2100:56
01106/2120:52 7440-50-8
Lead
ND ug/L
5.0
1
01/06/2100:56
01/06/2120:52 7439-92-1
Zinc
168 ug/L
10.0
1
01/05/2100:56
01/06/21 20:52 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
37.2 mg/L
5.0
1
12/29/20 11:28
Sample: 4
Lab ID: 92513743004 Collected:
12/24/20 11:45
Received: 12/24/20 12:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
01/08/21 11:22
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
01/08/21 11:22
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
ND ug/L
5.0
1
01/06/2100:56 01/0612120:55 7440-50-8
Lead
ND ug/L
5.0
1
01/06/2100:56 01/0612120:55 7439-92-1
Zinc
317 ug/L
10.0
1
01/06/2100:56 01/06/2120:55 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
10.3 mg/L
2.5
1
12/29/20 11:28
Date: 01 /11/2021 07:30 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 12

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QUALITY CONTROL DATA
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
QC Batch: 591513 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
METHOD BLANK: 3122727 Matrix: Water
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 01/08/21 11:22
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
3122728
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 33.6
84
78-114
MATRIX SPIKE SAMPLE:
3122729
92514150004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
26.2
64
78-114 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 07:30 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 12

acewww.patelabs.comAnalytical
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QUALITY -CONTROL DATA
Project: Dec. 2020 SW 12/24
Pace Project No.: 92613743
QC Batch: 591515 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
METHOD BLANK: 3122742 Matrix: Water
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.0 01/08/21 11:22
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
3122743
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 15.7
78
64-132
MATRIX SPIKE SAMPLE:
3122744
92514328001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 20
ND
10
64-132 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11/2021 07:30 AM without the written consent of Pace Analytical Services, I.I.C. Page 7 of 12

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QUALITY CONTROL DATA
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: 590825
Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
METHOD BLANK: 3119311
Matrix: Water
Associated Lab Samples: 92513743001, 92513743002,
92513743003, 92513743004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Copper
ug/L
ND 5.0
01/06/2120:10
Lead
ug/L
ND 5.0
01/06/2120:10
Zinc
ug/L
ND 10.0
01/06/2120:10
LABORATORY CONTROL SAMPLE:
3119312
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Copper
ug/L
500 462
92 85-115
Lead
ug/L
500 459
92 85-115
Zinc
ug/L
500 464
93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3119313 3119314
MS MSD
92513663001
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Copper
ug/L 0.039
500 500 524
517 97 96
70-130
1
mg/L
Lead
ug/L 0.015
500 500 482
475 93 92
70-130
1
mg/L
Zinc
ug/L 0.072
500 500 555
549 97 95
70-130
1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3119315 3119316
MS MSD
92514237002
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Copper
ug/L 0.016
500 500 506
507 98 98
70-130
0
mg/L
Lead
ug/L <0.0050
500 500 463
460 92 92
70-130
1
mg/L
Zinc
ug/L 0.12
500 500 595
592 95 94
70-130
0
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11/2021 07:30 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 12

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QUALITY CONTROL DATA
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
QC Batch: 589742 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
METHOD BLANK: 3114565 Matrix: Water
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 12/29/20 11:26
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 3114566 3114711
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Total Suspended Solids mg/L 250 246 238 99 95 90-110 3 25
SAMPLE DUPLICATE: 3114712
Parameter
Total Suspended Solids
Units
mg/L
92513899001 Dup
Result Result RPD Qualifiers
208 210 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 07:30 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 12

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QUALIFIERS
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 U7:30 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 12

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Late ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92513743001
1
EPA 1664E
591513
92513743002
2
EPA 1664B
591513
92513743003
3
EPA1664B
591513
92513743004
4
EPA1664E
591513
92513743001
1
EPA 1664E
591515
92513743002
2
EPA 1664E
591515
92513743003
3
EPA1664B
591515
92513743004
4
EPA1664B
591515
92513743001
1
EPA 200.7 Rev 4.4 1994
590825
EPA 200.7
Rev 4.4 1994
590851
92513743002
2
EPA 200.7 Rev 4.4 1994
590825
EPA 200.7
Rev 4.4 1994
590851
92513743003
3
EPA 200.7 Rev 4.4 1994
590825
EPA 200.7
Rev 4.4 1994
590851
92513743004
4
EPA 200.7 Rev 4.4 1994
590825
EPA 200.7
Rev 4.4 1994
590851
92513743001
1
SM 254OD-2011
589742
92513743002
2
SM 254OD-2011
589742
92513743003
3
SM 254OD-2011
589742
92513743004
4
SM 254OD-2011
589742
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 07:30 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 12

v' CHAIN -OF -CUSTODY Analytical Request Document LAB USE WO : 925 13743 Aber or c
N
PaceAnalyticaJ `
Chain-of-C istody is a LEGAL DOCUMENT - Complete all relevent fields rn
Company: Billin. Information: I I� I� �) ns
I lbe&WtoS !r P.Vt C.
ra�t,✓�f`3 n��C�.. 925137A3 n-
AddS 1�0A�. Container ..... ...�.....e.+...,b�..
Re ort To: Email To: r s t -� •' Qreservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
�, Vyj �t,/f<,' ) a•11/1 C jr p 7iC (6) methanol, (7) sodium bisulfate, (8) sor lum thiostdfate, (9) hexane, (A) ascorbic acid, (B) ammoniumn sulfate,
Copy To; Ate Collection nfo/Address: (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other
Analyses Lab Profile/Line:
Customer Project Name/Number: State: County/City: Time Zone Collected: Lab Sample ttece.ipt Chacklist:
b� be ?�� S1N �G /�s1�f'iV11l.e- [ j PT ( j MT ( j CT (ET Q
lU Custody Sear Present/Intact Y Na
t7A
Phone:82I6 S8 2$ Site/Facility ID It: Compliance Monitoring? l custody Signatures Present N NA
.9 Collector Signature Present N NAEmail: (xj Yes ( ) Na
eottlea intact Y N NA
Collected By (print): Purchase Order If DW PWS ID tl: Correct Bottles N IIA
p 'h�►am Quote If: DW Location Code: sufficient volume N 14A
--LL Samples Received on Ice N NA
:llecte - ;
(nature): Turnaround Dale teyuired: tmmedrate y Pace on Ice: i VOA - nendspace Acceptable Y 14
USDA Regulated Sails Y N(B
�.. _ _ �► Yes [ j No Samplenn in holding 714mo ® N ton
Sample Disposal: Rush: Field Filtered (if applicable]. `� Residual Chlorine Present Y N
( I Dispose as appropriate I )Return ( ) Same Day ( ) Next Day ( ( Yes ( ]No ` .(r6 Cl Strips:
I I Archive: ( ) 2 Day ( ( Day ( j 4 Day [ j 5 Day O Sample pH Acc tab lJ N NA
( J Hold:_ {Eap ite Charges Apply) Analysis: 'D pit strips: .Zj�
Sulfide Present Y :t
Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Lead Acetate Strips:
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air I AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)%S1LAB USE ONLY:
q
C mp / Collected (or Res If of f S; Lab Sample # / Comments:
Customer Sample ID Matrix Grab Composite Start} Composite End Cl Ctns O
Date Time Date Time
Customer Remarks / Special Conditions / Possible
(Signature)
Relinquished by/Company: (Signature)
Type of Ice Used: �Wet), Blue Dry None
Packing Material Used:
Radchem sample(s) screened (<500 epm): Y N { 1
Date/Time: Receive y ompany: (Signs tire)
Date/Time: Received by/Company: (Signature)
Relinquished by/Company: (Signature) I !Date/Time: Received by/Company: (Signature)
SHORT HOLDS PRESENT (<72 hours): Y UN N/A
Lab Tracking tt: 2427023
Samples received via:
FEDEX UPS Client Courier Pace Courier
Date/Time: MTJL LAB USE ONLY
ram. "q Table 11:
Acctnum:
Lab Sample Temperature into:
Temp Blank Received: Y N NA
Therm IDtt: �- i _' 7 /
Cooler 1 Temp Upon Recelpt: � oC
Cooler 1 Therm Corr. Factor: Q_oC
Cooler 1 Corrected Temp: oC
Comments:
Template: Trip Blank Received: Y W NA
Prelogin: HCL McOH TSP Other
Date/Time: PM: Non Conformance(s): Page:
PB: YES / (1(15) 1 of: