Loading...
HomeMy WebLinkAboutNC0037508_Pretreatment Compliance_20121130ATA NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Charles Wakild, P. E. Dee Freeniafl Governor Director Secretary November 30, 2012 Janna Scherer Pretreatment Coordinator/Lab Supervisor 1094 Addor Road . Aberdeen, NC 28315 SUBJECT: Pretreatment Compliance Inspection (PCI) Moore County Water Pollution Control Plant NPDES Permit No. NC0037508 Moore County Dear Ms. Scherer: Enclosed you will find a copy of the Pretreatment Compliance Inspection Report for the November 16, 2012 inspection of the pretreatment records, Erico (IUP #A005) files, CIU a site visit and tour of Erico. Since you had performed an Industrial Inspection on October 10, 2012, understandablyyou did not perform another Inspection during this PCI. This report indicates that Moore County Water Pollution Control Plant meets the pretreatment requirements as outlined in 15A NCAC 2H .0900. I appreciated your co-operation and your continued efforts with the pretreatment program. Your excellent record keeping and your organization of the Pretreatment files were outstanding. Please keep up the good work. If you have any questions concerning this report, please do not hesitate to contact me at (910) 433-3312. U Dale Lopez Environmental Specialist Enclosures: Pretreatment Compliance Inspection Report EPA Water Compliance Inspection Report SIU Inspection Form Effluent Flow Meter and Recorder Calibration report cc: PERCS _ Pretreatment Unit (Monti Hassan) FRO files,(Dale=Lopez) 225 Green Street -Suite 714 —Fayetteville, North Carolina 28301-5043 Phone: 910-433.33001 FAX: 910-486-07071 Customer Service: 1-877-623-6748 Internet: www.ncwaterquality.orq An Equal Opportunity \ Affirmative Action Employer • thCarolina h1\-Onatitra1Iy United States Environmental Protection Agency EPA Washington, D.C. 20460 Water Compllanne Inspection Report Form Approved. OMB No. 2040-0057 Approval expires 8-31-98 Section A: National Data System Coding (i.e., PCS) Transaction Code NPDES yr/mo/day Inspection 1 I N I 2 15I 31 NC0037508 111 121 12/11/16 117 Type Inspector FacType 18I P I 19I S I 20I I I I I I I I I I I I I I I I I 166 • Remarks 21 I III I I I I I I I I I I I I I I I I I I I I I I I. I 1 I I Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 QA---- 671 2.0 169 70I 41 711 I 72I N I 731 1 174 751 I I I I I I 180 Section B: Facility Data Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include POTW name and NPDES permit Number) Moore County WPCF 1094 Addor Rd Aberdeen NC 28315 Entry Time/Date 10:30 AM 12/11/16 Permit Effective Date 10/12/01 Exit Time/Date 03:00 PM 12/11/16 Permit Expiration Date 14/07/31 Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s) /// George R Yankay/ORC/910-789-2658/ Other Facility Data Name, Address of Responsible Official/Title/Phone and Fax Number Contacted George Yankay,1094 Adder Rd Aberdeen NC 28315//910-281-3146/ No Section C: Areas Evaluated During Inspection (Check only those areas evaluated) Pretreatment Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary) (See attachment summary) Name(s) and nature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date Dale Lopez �� I� FRO WQ//910-433-3300 Ext.712/ / t 30 JaPU/ l Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers Date J. 9 LA /140•10 i V.".3 /12 EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete. Page # 1 NPDES yr/mo/day Inspection Type (cont .) 1 NC0037508 12/11/16 1 17 181 PI Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary) Enclosed you will find a copy of the Pretreatment Compliance Inspection Report for the November 16, 2012 inspection of thepretreatment records, Erico (IUP #A005) files, CIU a site visit and tour of Erico. Since you had performed an Industrial Inspection on October 10, 2012, understandably you did not perform another Inspection during this PCI. This report indicates that Moore County Water Pollution Control Plant meets the pretreatment requirements as outlined in 15A NCAC 2H .0900. I appreciated your co-operation and your continued efforts with the pretreatment program. Your excellent record keeping and your organization of the Pretreatment files were outstanding. Please keep up the good work. If you have any questions concerning this report, please do not hesitate to contact me at (910) 433-3312. (Please see question #17, in the PCI checklist attached with this report). The Fecal Coliform violation during May 2012 for a monthly average of 223 col/100 mL due to a spill at a splitter box on May 17, 2012 that was caused by a leak when soil was removed during construction. Two Godwin pumps were set up as a temporary pumping system to distribute the hydraulic load to each aeration basin. This shortcircuiting might have caused the exceedence. The leak repair has been completed, and no additional non -compliances are expected to occur. Page # 2 NORTH CAROLINA DIVISION OF WATER QUALITY PRETREATMENT COMPLIANCE INSPECTION (PCI) REPORT BACKGROUND INFORMATION (Complete Prior To PCI; Review Program Info Database Sheet(s)1 1. Control Authority (POTW) Name: Moore County WPCP 2. Control Authority Representative(s): Janna Scherer 3. Title(s): Chemist/PT Coordinator/FOG Coordinator 4. Last Inspection Date: 04/27/2012 Inspection Type (Check One): ® PCI ❑ Audit 5. Has Program Completed All Requirements from the Previous Inspection and Program Info Sheet(s)? ® YES ❑ NO 6. Is POTW under an Order That Includes Pretreatment Conditions? ❑ YES ® NO Order Type, Number, Parameters: Are Milestone Dates Being Met? ❑ YES ❑ NO PCS CODING Trans.Code Main Program Permit Number f N f C 101013171510181 MM/DD/YY f 111161121 (DTIA) Inspec.Type Inspector Fac. Type P (TYPI f SI 11! INSP) (FACC 7. Current Number Of Significant Industrial Users (SIUs)? 3 SIUS 8. Current Number Of Categorical Industrial Users (CIUs)? 3 CIUS 9. Number of SIUs Not Inspected By POTW in the Last Calendar Year? 0 10. Number of SIUs Not Sampled By POTW in the Last Calendar Year? 0 11. Enter the Higher Number of 9 or 10 0 _ NOIN 12. Number of SIUs With No IUP, or With an Expired IUP 0 NOCM 13. Number of SIUs in SNC for Either Reporting or Limits Violations During Either of the Last 2 Semi -Annual Periods (Total Number of SIUs in SNC) 0 PSNC - .14. Number of SIUs in SNC For Reporting During Either of the Last 2 Semi -Annual Periods 0 MSNC 15. Number of SIUs In SNC For Limits Violations During Either of the Last 2 Semi -Annual Periods 0 SNPS 16. Number of SIUs In SNC For Both Reporting and Limits Violations During Either of the Last 2 Semi-annual Periods 0 POTW INTERVIEW 17. Since the Last PCI, has the POTW had any NPDES Limits Violations? If Yes, What are the Parameters and how are these Problems Being Addressed? Please see File Review Comment #1 18. Since the Last PCI, has the POTW had any Problems Related to an Industrial Discharge (Interference, Pass -Through, Blockage, Citizens' Complaints, Increased Sludge Production, Etc.)? If Yes, How are these Problems Being Addressed? 19. Which Industries have been in SNC for Limits or Reporting during either of the Last 2 Semi -Annual Periods? Not Been Published for Public Notice?(May refer to PAR if Excessive SIUs in SNC) SNC for SNC for Not Put 20. Which Industries are on Compliance Schedules or Orders? For all SIUs on an Order, Has a Signed Copy of the Order been sent to the Division? 21. Are Any Permits Or Civil Penalties Currently Under Adjudication? If Yes, Which Ones? LTMP/STMP FILE REVIEW: YES ❑ NO ❑ YES .... NO Limits: Reporting: dished: 0 0 0 0 ❑YES /1NO 22. Is LTMP/STMP Monitoring Being Conducted at Appropriate Locations and Frequencies? 23. Are Correct Detection Levels being used for all LTMP/STMP Monitoring? r Y ES YES ❑ NO i1 ❑ NO always on quarterly monitoring schedule 24. Is LTMP/STMP Data Maintained in a Table or Equivalent? YES ❑ NO Is Table Adequate? 25. All LTMP.-STMP effluent data reported on Discharge :Monitoring Report? ® YES ❑ NO DWQ Inspector, please verify yourself! 26. If NO to 23 - 26, list violations ® YES ❑ NO 27. Should any Pollutants of Concern be Eliminated from or Added to LTMP/STMP? ❑ YES ® NO NC DWQ Pretreatment Compliance Inspection (PCI) Form Updated 7/25/07 Page 1 • 28. PRETREATMENT PROGRAM ELEMENTS REVIEW— Please review POTW tiles. verify POTW has copy of Program Element in their files, complete with supporting documents and copy of PERCS Approval Letter, and dates consistent with Program Info: Program Element Last Submittal Date In file? Last Approval Date In file Date Next Due, If Applicable Headworks Analysis (HWA) 11/08/100 Yes ❑ No 02/22/11 4 Yes ❑ No 11/01/2015 Industrial Waste Survey (IWS) 08/26/08 E/ Yes ❑ No 11/05/08 _ r Yes ❑ No 09/01/2013 Sewer Use Ordinance (SUO) 05/31/07 Li Yes ❑ No 10/16/07 /Z1 Yes ❑ No 12/31/2012 Enforcement Response Plan (ERP) 10/16/2012 '1 Yes ❑ No 10/22/2012 0 Yes ❑ No Long Term Monitoring Plan (LTMP) 06/28/04 4 Yes ❑ No 07/13/04 Yes ❑ No INDUSTRIAL USER PERMIT (IUP) FILE REVIEW (3 IUP FILE REVIEWS OR 1 FILE REVIEW AND 1 IU INSPECTION) 29. User Name I. Erico, Inc 30. IUP Number A005 31. Does File Contain Current Permit? ►X1 Yes, eff. 07/01/08 32. Permit Expiration Date 06/30/13 33. Categorical Standard Applied (I.E. 40 CFR, Etc.) Or N/A 433 34. Does File Contain Permit Application Completed Within One Year Prior to Permit Issue Date? / / Yes ❑ No 12/20/07 35. Does File Contain an Inspection Completed Within Last Calendar Year? Yes 10/10/2012 36. a. Does the File Contain a Slug/Spill Control Plan? b. If No, is One Needed? (See Inspection Form from POTW) Cs Yes ■No 10/19/10 37. For 40 CFR 413 and 433 TTO Certification, Does File Contain a Toxic Organic Management Plan (TOMP)? ®Yes❑No❑N/A 38. a. Does File Contain Original Permit Review Letter from the Division? b. All Issues Resolved? a. _Yes No 07/03/2008 b.®Yes❑No❑N/A 39. During the Most Recent Semi -Annual Period, Did the POTW Complete its Sampling as Required by IUP, including flow? /1 Yes ❑ No 40. Does File Contain POTW Sampling Chain -Of -Custody Forms? // Yes ❑ No 41. During the Most Recent Semi -Annual Period, Did the SIU Complete its Sampling as Required by IUP, including flow? ®Yes❑No❑N/A 41b. During. the Most Recent Semi -Annual Period, Did SIU submit all reports on time? ®Yes❑No❑N/A 42a. For categorical !Us with Combined Wastestream Formula (CWF), does file include process/dilution flows as Required by IUP? ❑Yes❑No®N/A 42b. For categorical lUs with Production based limits. does tile include production rates and/or flows as Required by fUP? ❑Yes❑No®N/A 43a. During the Most Recent Semi -Annual Period, Did the POTW Identify All Limits Non- Compliance from Both POTW and SIU Sampling? /1 Yes ❑ No No violations 43b. During the Most Recent Semi -Annual Period, Did the POTW Identify All Reporting ❑Yes❑No®NiA None Non -Compliance from SIU Sampling? 44. a. Was the POTW Notified by SIU (Within 24 Hours) of All Self- Monitoring Violations? b. Did Industry Resample and submit results to POTW Within 30 Days? c. Ifapplicable, Did POTW resample within 30 days of becoming aware of SiU limit violations in the POTW's sampling of the SIU? a.❑Yes❑No®N/A b.❑Yes❑No®N/A c.❑Yes❑No®N/A 46. During the Most Recent Semi -Annual Period, Was the SIU in SNC? ❑ Yes /i1 No 47. During the Most Recent Semi -Annual Period, Was Enforcement Taken as Specified in the POTW's ERP (NOVs, Penalties, timing, etc.)? ❑Yes❑No®N/A 48.. Does the File Contain Penalty Assessment Notices? ❑Yes❑No®N/A 49. Does The File Contain Proof Of Penalty Collection? ❑Yes❑NoEIN/A 50. a. Does the File Contain Any Current Enforcement Orders? b. Is SIU in Compliance with Order? a.❑Yes❑No®N/A b.❑Yes❑No® N/A 51. Did the POTW Representative Have Difficulty in Obtaining Any of This Requested Information For You? ❑ Yes No NC DWQ Pretreatment Compliance Inspection (PCI) Form Updated 7/25/07 Page 2 FILE REVIEW COMMENTS: 1. (Please see question #17, above). Fecal Coliforms during May 2012 for a monthly average of 223 col/100 mL due to a spill at a splitter box on May 17, 2012 that was caused by a leak when soil was removed during construction. Two Godwin pumps were set up as a temporaryy pumping system to distribute the hydraulic load to each aeration basin. This shortcircuiting might have caused the exceedence. The leak repair has been completed, and no additional non -compliances are expected to occur. INDUSTRY INSPECTION PCS CODING: Trans.Code Main Program Permit Number MM/DD/YY Inspec.Type Inspector Fac. Type N C101013 I715I 0 J8J J111.16112J J I 1 J S J 12 (DTIA) (TYPI) (INSP) (FACC) 1. Industry Inspected: Erico, Inc 2. Industry Address: 188 Carolina Road, Aberdeen, NC 28315 3. Type of Industry/Product: Ground rod manufacturing and metal electroplating with Nickel,. Zinc, and/or Copper 4. Industry Contact: Joe Holt - Title: Wastewater/Pretreatment Operator Phone: (910) 944-4126 Fax: (910) 944-2648 5. Does the POTW Use the Division Model Inspection Form or Equivalent? ® YES ❑ NO 6. Did the POTW Contact Conduct the Following Parts of the Industrial Inspection Thoroughly? Comments: A. Initial Interview ® YES ❑ NO B. Plant Tour YES ❑ NO C. Pretreatment Tour ® YES ❑ NO D. Sampling Review ® YES ❑ NO E. Exit Interview ® YES ❑ NO Industrial Inspection Comments: Please see the enclosed SIU Inspection Form for the inspection performed by the POTW on October 10, 2012. Erico started sending their effluent samples to MicroBac approximately two years ago. The ultrasonic flow meter checked the flow out of an open 4-inch PVC line. (Mr. Holt had calculated that no greater than 54.45 gallon was able to flow out of a 4-inch line). This secondary flow measuring device was calibrated by Chris Siler (ISI Instrumentation Services, Inc) on 10/03/2012 (please see the two attached calibration report sheets). NC DWQ Pretreatment Compliance Inspection (PCI) Form Updated 7/25/07 Page 3 OVERALL SUMMARY AND COMMENTS: Comments: We appreciate your co-operation and your continued efforts with the pretreatment program. Your excellent record keeping and your organization of the Pretreatment files were outstanding. Please keep up the good work with your pretreatment program. Requirements: None Recommendations: Please keep up the good work. NOD: ❑ YES ® NO NOV: ❑ YES ® NO QNCR: ❑YES A NO POTW Rating: Satisfactory Marginal UnS; isfactory PCI COMPLETED BY: Dale Lopez \'`-/CL(,L DATE: November 30, 2012 REVIEWED BY: Belinda Henson i%j 7 G��ZD��'l� DATE: j a -3- I eL NC DWQ Pretreatment Compliance Inspection (PCI) Form Updated 7/25/07 Page 4 SHJ INSPECTION FORM Product Raw materials used Manufacturing processes Categorical, if applicable Production rate Number of employees Number of shifts Comments: Name of Industry: Erico, Inc. Address Of Industry: 188 Carolina Road Aberdeen, NC 28315 Industry Representatives: Joe Holt Frank Bryant _POTW Representatives: Janna Scherer IUP # A005 IUP Expiration Date: June 30, 2013 Title Wastewater/Pretreatment Operator Wastewater/Pretreatment Operator -Backup Title: Chemist/IPP Coordinator Date of Inspection: October 10, 2012 Time Of Inspection: 11:00 am/pm Purpose oflnspection: Annual X Other (Describe) POTW to which IU discharges Moore County WPCP NPDES # NC0037508 Is SIU currently in SNC? No If yes, for what? PART I - INITIAL INTERVIEW Has anything changed since the last inspection or 1-UP application in the following: COMMENTS YES l NO YES / NO YES / NO YES / NO 433 YES / NO Production about the same YES INO about 80 YES / NO 4 shifts in plating (24 hr/day run) PART II - PLANT TOUR - Visit all areas where wastewater is generated or where there are drains to the POTW. Plant Tour Section A - PRODUCTION AND STORAGE AREAS 1. Are there floor drains in the production area? YES / NO Where do they go? Waste from the production areas go to the equalization tank. 2. Are production areas diked, contained, or otherwise constructed in such a way as to prevent harm to the WWTP, especially from spills or slugs? YES / NO Comments: There are either containment or pit sumps. 3. Are there floor drains in the storage area? YES / NO Where do they go? There are sumps in the chemical storage area. In case of a spill or leak, the chemicals are contained until they can be pumped into another storage drum. 4. Are storage tanks and areas diked, contained, or otherwise constructed in such a way as to prevent harm to the WWTP, especially from spills or slugs? YES / NO Comments: 5. Are process and storage tanks and pipes labeled? YES / NO 6. How are off -spec raw materials, and products disposed of? Off spec materials are re -worked, scraped, or sent back to the manufacturer A&D Environmental is recycler used. 7. When is the production area cleaned? Once per shift/ continuously 8. Is the wastewater from cleaning the production area discharged to the POTW? YES l NO The wastewater from cleaning goes to the Pretreatment system before being discharged to the POTW. 9. What non -process wastewaters are discharged to POTW? Domestic sewage is discharged via a separate line. Comments: Line 3 will be shut down starting in November for a complete tear down and replacement of all parts. Title: SIU Inspection Form File name: COMP.INSP App 7-D Revision data: August I, 1994 Page 1 SW. INSPECTION FORM PART II - Plant Tour Section B - PRETREATMENT SYSTEM Ask the operator to describe pretreatment system. 1. Does operator seem knowledgeable about the system? YES / NO Comments: Mr. Holt holds a NC Grade II WW Operator license and his back-up holds a NC Grade I Operator license. Both operators are extremely knowledgeable about the treatment process and maintain it well. 2. Are all units operational? YES / NO 3. How often does operator/maintenance person check system? Hourly 4. Is there an operator for each shift? YES / NO Joe Holt is responsible but several different employees have been trained to monitor the Memtech system during their respective shifts. 5. How and when is sludge disposed of? The sludge is picked up by A&D Environmental about once every 90 days (or when 10 bps accumulate) and recycled. The status of the waste is non -hazardous 6. Is there a schedule for preventative maintenance? YES / NO Comments: Preventative and corrective maintenance is conducted by plant maintenance department and the system operators and is ongoing. PART II - Plant Tour Section C - SAMPLING POINT(S) AND FLOW MEASUREMENT (Collect a sample if desired.) 1. Does an outside lab complete sampling? YES / NO If yes, name of lab. Microbac, Meritech Labs and the Moore County WPCP Laboratory. 2. If industry completes sampling, ask the industry representative to describe sampling procedures. Comments: The sample is collected in the composite sampler. The industry representative collects the samples and chills them until the lab arrives. Samples are then signed over. 3. Is flow measurement equipment operational? YES / NO Comments: Flow meter is calibrated by ISI Systems twice per year. 4. Is there a calibration log for the flow meter? YES / NO Comments: The sticker on the instrument indicated the instrument was last calibrated on October 3, 2012.. Comments: They are using an ISCO 3010 ultrasonic flow transmitter. The sticker showed the next calibration due was April 2013. PART III - EXIT INTERVIEW Review monitoring records and other SIU records required by IUP. 1. Are files well organised? YES / NO Comments: Files are very well organised. Current permit is filed. 2. Are sample collection / chain -of -custody forms filled out properly? YES / NO Comments: 3. Do results in files agree with reports sent to POTW? YES / NO Comments: February 2012 flow log and lab results were compared and were in order. 4. Who has authority to shut down production should a spill or slug discharge occur? Joe Holt, Emad Girgis, and/or Frank Bryant, or any lead man on any shift. 5. How does SIU inform employees of whom to call at POTW in case of spill/slug? Employees notify the above listed personnel. The above personnel then contact the POTW. Emergency numbers are posted throughout the plant. If slug/spill plan is already required by POTW, review procedures. 6. Is SIU implementing slug/spill plan? YES I NO Comments: Plan was last revised on October 19, 2010. Comments: The plant permit and lab results were reviewed. Files are in order and complete. INSPECTION RESULTS Slug/Spill Control Plan Needed? YES / NO Plan is already in place. Revise as necessary. See above note. Comments, Required or Recommended Actions: Pretreatment areas were clean and in order. Files were neat and complete. Signature of Inspector(s) (1.444 Axil,li(rPi(- Date: Date: / O -1 - Title: SN Inspection Form File name: COMP.INSP App 7-D Revision data: August 1, 1994 Page 2 CERTIFICATE OF CALIBRATION Certification Number: 10.03.12 .603404068 ERICO, INC. 188 CAROLINAROAD ABERDEEN , NC 28315 EMAD GIRGIS ISI Form: 1150-12/16/09 a A 111 Instrumentation Services, Inc. 3436 Toringdon Way, Suite 105 Charlotte, North Carolina 28277 800-532-0415 FAX:888-367-3571 www.ISlservesYOUcom EQUIPMENT INFORMATION: Instrument ID 603404068 Description EFFLUENT FLOW METER Location Manufacturer Model Number Serial Number ISCO 3010 603404068 SERVICE INFORMATION: Frequency SEMI-ANNUALLY Classification ISO9001 Calibration Type ROUTINE Sop Number ISI-WI-1100 Environmental Conditions Calibrated Next Calibration Due Date As Found Status As Left Results Acceptable Parameters 10/3/2012 04/30/2013 In Tolerance In Tolerance ISI certifies that the above listed Instrument(s) meets or exceeds specifications as stated in the service agreement or purchase order unless stated otherwise. The Calibration Standards used to perform the calibration of the instrument(s) above are traceable through the National Institute of Standards and Technology (MST) or other National Metrology Institute (NMI) to the International System of Units (SI units). ISI is registered to IS09001:2008 and accredited to ISO/IEC 17025:2005 for calibration. ISI's systems, processes, procedures, and work performed conform to the requirements of IS09001:2008, ISO17025:2005, M L-STD-45662A, ANSI/NCSL Z540-I-1994, 21 CFR Part 11, ISO 10012 part 1, and AMS2750 as applicable and referenced in the service agreement and/or purchase order. The the standard referenced is indicated in the Classification Type Above. The "pass/fail" indication provided on this report is for your convenience and is an opinion and/or interpretation of the compliance/noncompliance of the results of the measurements. It is the end -users responsibility to evaluate the compliance/noncompliance of the Instrument(s) based on the usage of the instrument and the measurement requirements. The responsibilities of ISI shall, in no event, exceed the cost of the service performed. This calibration certificate applies only to the Instruments) listed above and shall not be reproduced except in full without the vninen permission of the Quality Manager of ISI. CALIBRATION RESULTS Calibration Type: FLOW Applied Expected Range Units 0.00 to 0.25 FEET 0.00 to 54.45 GPM Applied Expected 0.24 50.48 Tolerance Specification: 2.00 % of Output Full Range Low Tolerance High Tolerance As Found 49.39 51.57 50.45 As Left 50.45 Pass / Fail Pass Adjusted NO Test Instruments Used During the Calibration Test Instrument ID SG-002 Manufacturer Stevens Water Monitoring Systems Serial Number 2 Last Cal Date 3/14/2012 Next Cal Date 3/14/2015 Notes about this Calibration Calibrated By: Chris Siler ISI utilises Electronic Signature in compliance with 21 CFR part 11 Job No. / Service:1024-000 / PM S/A Page I of I ISO 140.. osistmr croup Inc. LABORATORY ACCREDITATION BUREAU Certificate 0 L1139-1 Callratinn CERTIFICATE OF CALIBRATION Certification Number: 10.03.12 .114378 ERICO, INC. 188 CAROLINA ROAD ABERDEEN , NC 28315 EMAD GIRGIS ISl Form: 1150-12/16/09 MOO 'tL Instrumentation Services, Inc. 3436 Toringdon Way, Suite 105 Charlotte, North Carolina 28277 800-532-0415 FAX:888-367-3571 wvw.ISlservesYOU.cam EQUIPMENT INFORMATION: Instrument ID 114378 Description EFFLUENT FLOW RECORDER Location Manufacturer CHESSELL Model Number Serial Number 114378 SERVICE INFORMATION: Frequency SEMI-ANNUALLY Classification IS09001 Calibration Type ROUTINE Sop Number ISI-WI-1100 Environmental Conditions Calibrated Next Calibration Due Date As Found Status As Left Results Acceptable Parameters 10/3/2012 04/30/2013 In Tolerance In Tolerance ISI certifies that the above listed Instrument(s) meets or exceeds specifications as stated in the service agreement or purchase order unless stated otherwise. The Calibration Standards used to perform the calibration of the instrument(s) above are traceable through the National Institute of Standards and Technology (MST) or other National Metrology Institute (NMI) to the International System of Units (SI units). ISI is registered to IS09001:2008 and accredited to IS0/IEC 17025:2005 for calibration. ISI's systems, processes, procedures, and work performed conform to the requirements of 1S09001:2008, IS017025:2005, MIL-STD-45662A, ANSI/NCSL Z540-1-1994, 21CFR Part 11, ISO 10012 part 1, and AMS2750 as applicable and referenced in the service agreement and/or purchase order. The the standard referenced is indicated in the Classification Type Above. The "pass/fail" indication provided on this report is for your convenience and is an opinion and/or interpretation of the compliance/noncompliance of the results of the measurements. It is the end -users responsibility to evaluate the compliance/noncompliance of the Instrument(s) based on the usage of the instrument and the measurement requirements. The responsibilities of ISI shall, in no event, exceed the cost of the service performed. This calibration certificate applies only to the Instrument(s) listed above and shall not be reproduced except in full without the written permission of the Quality Manager of ISI. CALIBRATION RESULTS Calibration Type: FLOW - DIGITAL DISPLAY Tolerance Specification: Range Units Applied Expected 4.00 to 20.00 mA 0.00 to 54.45 GPM 1.00 % of Output Full Range Applied Expected Low Tolerance High Tolerance As Found As Left Pass / Fail Adjusted 4.00 0.00 -0.54 0.54 0.01 0.01 Pass NO 12.00 27.23 26.69 27.77 27.25 27.25 Pass NO 20.00 54.45 53.91 54.99 54.50 54.50 Pass NO Calibration Type: FLOW - CHART Range Units Applied Expected 4.00 to 20.00 me, 0.00 to 54.45 GPM Applied, 4.00 12.00 20.00 Tolerance Specification: 1.00 (+/-) Output Reading Expected Low Tolerance High Tolerance As Found As Left Pass / Fail Adjusted 0.00 -1.00 1.00 0.00 0.00 Pass NO 27.23 26.23 28.23 27.00 27.00 Pass NO 54.45 53.45 55.45 54.00 54.00 Pass NO Test Instruments Used During the Calibration Test Instrument ID Manufacturer 7281617 FLUKE Serial Number 7281617 Last Cal Date 12/6/2011 Next Cal Date 12/6/2012, Notes about this Calibration Calibrated By: Chris Siler ISI utilizes Electronic Signature in compliance with 21 CFR parr 11 Job No. / Service:1024-000 / PM S/A Page l of l pistmr Group Inc. LABORATORY ACCREDITATION BUREAU Certificate 18 L1139-1 Call6ration