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HomeMy WebLinkAboutNC0037508_NPDES Permit Renewal_20140205ATADEN®FRC' _ FEB 1 1 2014 NCDENR North Carolina Department of Environment and Natural Resources Division of Water Resources Pat McCrory Thomas A. Reeder John E. Skvarla, III Governor Director Secretary February 05, 2014 Attn: Larry Caddell -Chairman Moore Co. Board of Commissioners PO Box 905 Carthage, NC 28327 Subject: Receipt of permit renewal Permit NC0037508 Moore County Dear Mr. Caddell: The NPDES Unit received your permit renewal application on February 02, 2014. A member of the NPDES Unit will review your application. They will contact you if additional information is required to complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days before your existing permit expires. If you have any additional questions concerning renewal of the subject permit, please, contact Tom Belnick (919) 807-6390. Sincerely, Wren Thedford Wastewater Branch cc: Central Files • Fayetteville Regional Office NPDES Unit 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Location: 512 N. Salisbury St. Raleigh, North Carolina 27604 Phone: 919-807-63001 Fax: 919-807-6492/Customer Service: 1-877-623-6748 Internet:: www.ncwater.orq An Equal OpportunityAAffirmative Action Employer Public Works )4'a.ter PoOCution Control 7094 . ddor Road Aberdeen, NC 28315 County of _Moore January 27, 2014 Re: NPDES Permit Application NPDES Permit No. NC0037508 Moore County Water Pollution Control Plant Mr. Matt Matthews NC DENR/DWR/ Surface Water Protection 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Mr. Matthews: (91o) 281-3146- Phone (910) 281-2047- J'ax ICE 1- 0 2 2014 F—KGEems FRO FEB2014 Moore County's NPDES Permit expires 'July 31, 2014. In compliance with Federal (40 CFR 122) and State (15A NCAC 2H.0105 (e)) regulations, we are required to submit a Permit Renewal Application at least 180 days prior to the expiration date. The Permit Renewal Application is enclosed, in triplicate, with correspondence. The County of Moore requests that their existing Permit be renewed at the 10MGD effluent limits and requirements. Construction at the facility is complete at this time. The following are changes made at the facility since the last issuance of the permit: 1. A third train was added to the plant including a new primary clarifier, intermediate clarifier, final clarifier, and two new basins at both first and second stage aeration tanks. 2. Sand filters were added prior to UV. 3. UV disinfection was installed and chlorination/dechlorination systems were removed from operation. 4. New generators were installed; three total. 5. A second primary digester was constructed. 6. Sludge presses were added for thickening and dewatering purposes; two total. 7. Drying beds are used for stockpile only at this time. All effluent testing concentrations were calculated from 2013 lab data. All toxicity data is included for the years of 2010, 2011, 2012, and 2013 and PPA results for four scans for the same years. Also included are the upstream low level mercury (1631) results for twelve months required on the current NPDES permit. Public -Works Water Pollution ControCP(ant 1094 .Addor Road .Aberdeen, NC 28315 County of .Moore (9io) 281-3146- Phone (910) 281-2047- fax If additional information is needed, please do not hesitate to contact me at (910) 281- 3146. Sincerely, George R. Yankay, System Superintendent GRY/j is Enclosures Cc: Ms. Belinda Henson, Fayetteville Regional Office, Director Mr. J. Wayne Vest, County of Moore, Manager Mr. Randy Gould, County of Moore, Public Utilities Director PERMIT ACTION REQUESTED: Renewal FAc.ILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 FORM 2A NPDES Form 2A has'_been developed in a modular format and consists of a "Basle Apj and a "Supplemental Application; Information'•' packet The Basic Application l into two parts All applicants must complete Parts A and C Applicants with a equal to 01 mgd must also complete Part B Some applicants must also comp " plication Information packet The following items explain which parts of Fo RIVER BASIN: Lumber BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. B. Additional Application Information for Applicants with a Design Flow >_ 0.1 mgd. All treatment works that have design flows greater than or equal to 0.1 million gallons per day must complete questions 6.1 through 6.6. C. Certification. All applicants must complete Part C (Certification). SUPPLEMENTAL APPLICATION INFORMATION: D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets one or more of the following criteria must complete Part D (Expanded Effluent Testing Data): 1. Has a design flow rate greater than or equal to lmgd, 2. Is required to have a pretreatment program (or has one in place), or - 3. Is otherwise required by the permitting authority to provide the information. E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing Data): 1. Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. F. Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users (SlUs) or receives RCRA or CERCLAwastes must complete Part F (Industrial User Discharges and RCRA/CERCLA Wastes). SlUs are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that: a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain exclusions); or b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant; or c. Is designated as an SIU by the control authority. G Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer Systems). EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 1 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Watery Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber .Cea .B t 4 �.. 4!"'F 'J� L - R.9, Y T i �►I II 1 Pp 61F?P' GA 5' �. All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet. A.1. Facility Information. • Facility Name Moore County Water Pollution Control Plant Mailing Address 1094 Addor Road • Aberdeen, NC 28315 Contact Person George Yankav Title System Superintendent Telephone Number (910) 281-3146 Facility Address same as above (not P.O. Box) A.2. Applicant Information. If the applicant is different from the above, provide the following: Applicant Name Moore County Board of Commissioners Mailing Address PO Box 905 Carthage, NC 28327 Contact Person Larry Caddell Title Chairman Telephone Number (910) 947-6403 Is the applicant the owner or operator (or both) of the treatment works? ® owner 0 operator Indicate whether correspondence regarding this'permit should be directed to the facility or the applicant. ❑ facility ® applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state -issued permits). - NPDES NC 0037508 PSD UIC Other RCRA Other A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Population Served Type of Collection System Ownership Town of Aberdeen 6350 separate town Town of Southem Pines 12334 separate town Village of Pinehurst 13124 separate municipal Town of Carthage 2205 separate town Town of Pinebluff 1337 separate town Town of Vass 720 separate municipal Tourism/seasonal/resort 8000 separate town Total population served 44070 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 2 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber A.5. Indian Country. a. Is the treatment works located in Indian Country? ❑ Yes ® No b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through) Indian Country? ® Yes ❑ No A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12th month of "this year" occurring no more than three months prior to this application submittal. a. Design flow rate 10 mgd b. Annual average daily flow rate Two Years Aqo 4.132mgd Last Year This Year 4.193mqd 4.889mqd c. Maximum daily flow rate 5.993mqd 8.156mqd 9.531mgd A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent contribution (by miles) of each. ® Separate sanitary sewer 100 ❑ Combined storm and sanitary sewer A.8. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? ® Yes ❑ No If yes, list how many of each of the following types of discharge points the treatment works uses: i. Discharges of treated effluent 1 ii. Discharges of untreated or partially treated effluent 0 iii. Combined sewer overflow points iv. Constructed emergency overflows (prior to the headworks) v. Other b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments that do not have outlets for discharge to waters of the U.S.? 0 Yes If yes, provide the following for each surface impoundment: Location: 0 0 ® No Annual average daily volume discharge to surface impoundment(s) Is discharge ❑ continuous or ❑ intermittent? c. Does the treatment works land -apply treated wastewater? If yes, provide the following for each land application site: Location: Number of acres: mgd ❑ Yes ® No Annual average daily volume applied to site: mgd Is land application ❑ continuous or ❑ intermittent? d. Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? ❑ Yes ® No EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 3 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control; NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber e. If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). If transport is by a party other than the applicant, provide: Transporter Name Mailing Address Contact Person Title Telephone Number ( ) For each treatment works that receives this discharge, provide the following: Name Mailing Address Contact Person Title Telephone Number ( ) If known, provide the NPDES permit number of the treatment works Provide the average daily flow rate from the treatment works into Does the treatment works discharge or dispose of its wastewater in A.8. through A.8.d above (e.g., underground percolation, well injection): If yes, provide the following for each disposal method: that receives this discharge the receiving facility. mgd in a manner not included ❑ Yes 0 No Description of method (including location and size of site(s) if applicable): Annual daily volume disposed by this method: Is disposal through this method 0 continuous or 0 intermittent? EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 4 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber WASTEWATER DISCHARGES:. If you answered "Yes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question A.8.a, go to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Outfall. a. Outfall number 001 b. Location Aberdeen 28315 (City or town, if applicable) Moore County (Zip Code) North Carolina (County) (State) 35°04'04" N 78°28'07" W (Latitude) (Longitude) c. Distance from shore (if applicable) ft. d. Depth below surface (if applicable) - ft. e. Average daily flow rate 4.982 mgd f. Does this outfall have either an intermittent or a periodic discharge? ❑ Yes ® No (go to A.9.g.) If yes, provide the following information: Number f times per year discharge occurs: Average duration of each discharge: Average flow per discharge: mgd Months in which discharge occurs: g. Is outfall equipped with a diffuser? 0 Yes ® No A.10. Description of Receiving Waters. a. Name of receiving water Aberdeen Creek b. Name of watershed (if known) United States Soil Conservation Service 14-digit watershed code (if known): c. Name of State Management/River Basin (if known): United States Geological Survey 8-digit hydrologic cataloging unit code (if known): d. Critical low flow of receiving stream (if applicable) acute cfs chronic cfs e. Total hardness of receiving stream at critical low flow (if applicable): mg/I of CaCO3 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 5 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber A.11. Description of Treatment a. What level of treatment are provided? Check all that apply. ® Primary ® Secondary ❑ Advanced 0 Other. Describe: b. Indicate the following removal rates (as applicable): Design BOD5 removal or Design CBOD5 removal 90 Design SS removal 90 % Design P removal 0 Design N removal 75 % Other i c. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe: UV disinfection If disinfection is by chlorination is dechlorination used for this outfall? 0 Yes ❑ No Does the treatment plant have post aeration? 0 Yes ® No A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combinedsewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart. Outfall number: 001 '6" ?._ "` '.. • IY)vMtLi%L1i� 4 �i . �J om, 3 # �r4Q.i��ll�t 'V "1 GE D -( ki k. 'k fi- * {x'..z ii Ti 34L'r-^F �k'S h r s., ...• alu.jyfa �' .�` i�fi��Q -- } +' d'Y +-"" - r .+ "' tea' ; , c� � n �. '3 pH (Minimum) 6.02 s.u. C eF i i 4 „ .K ys S i1 pH (Maximum) 7.80 s.u.. ` , Flow Rate 9.531. mgd 4.889 mgd 365 Temperature (Winter) 18.1 °C 15.4 °C 181 Temperature (Summer) 24.2 °C 21.7 °C 184 For pH please report a minimum and a maximum daily value �# :f ,.; t ..::a'`.r!'�r "�+ DISCHARGE {� S+�i€tit'- VERA DI ILA} ISCH ►l E ,. 4E *j am $rz. rL �t 7 3 .n. T +t<✓`...t-{ 1, lc t# E�yi ,r Y NT... . H 3�sst' 3'�♦<'�.+ �''i!".3.3yaC3 '�^^-,-- > -3'= 't.+T:Y' s���`$- - .3 �t '�"�' Con ' Uri ; . ' a: =s i cc- Unit> eta e CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BIOCHEMICAL OXYGEN DEMAND (Report one) BOD5 35.5 mg/L 5.1 mg/L 249 SM5210B CBOD5 FECAL COLIFORM >900 #/100mL 5.4 #/100mL 249 SM922D TOTAL SUSPENDED SOLIDS (TSS) 24 mg/L 8.2 mg/L 249 SM2540D .• ¢.,x,y c`.-;t:�a_�},. � = '� y} �'" FE 1CAlp s sd �+§» � �� `.:')'as• ... �:'.a „- +�i. ''_ `� .C..N 'G ice. �' °ss�f�,�fat,«-�c--;ti: rx " qA` `e sY'2 t�h `: '5.z.� i�o-�' ' � 'vim:-X 1" IOyN .w).5'yi F FORM .F:'i"�`.ii�.5�'�.T?.s'+ •L y�iA - '-J "5 - 'i `k#`{'.,`3�- ,a ss„'.�,.' GE ) T TLL� RMI HICH T R �4�T £ r=M+ S's(-'. Y'+uk w'? gi'Y1L 4 t:.. . to -� k 3i* 2A Y®_ , T�G`O P'LE'> E� 'ri ��. �"tt ��s `� ��-7a: _.. �k 5".»�'�w s.. SG EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 6 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber AS C-APPt' ATIONLINE0 MATiIOM q� . .: .......e;;��i-.�i.i—,.iFi,6`...;^•i.�n'"S +-=<1-2F'` ta, r�34c''.. 'per .'.� ., �� .n ••�*u'�'° 'X6?£+z.,�.i•iii3�.1a £..iir".§v.=e, , "e a +ate . r,ia 3- JM- "�.:- , Se. .r... '),"�' ;,, 4 'L t+Y =''S •R s??-' P- €pw 1 I TialeA A►; F�10+„J N °�NIF4aMAT� t;7�+i Q , ►P--- L CA T 11�1((1Tkl ;Ai Ala OW t3Rl; It THA §,, .. rn 4i fr• "S'€"�m4z . AtF + `+t' I nJP A .. f $L �.i'R �},. Q 9 Jiw`t y }'„KrS' Y* AL,. 01 D 100 0 t0 Was ` ia �; � � .; � . � � may: ��,�.. All applicants with a design flow rate >_ 0.1 mgd must answer questions B.1 through B.6. All others go to Part C (Certification). B.1. Inflow and Infiltration. Estimate the average number of gallons per day 798,613 gpd that flow into the treatment works from inflow and/or infiltration. 2013. Rehab of 5 stations was completed in 2010. Rehab on Briefly explain any steps underway or planned to minimize inflow and infiltration. Rehab of Old Town Pinehurst sewer lines was completed in the interceptor began January 2014. The sewer lines around Pinehurst Lake were lined- cure in place. Camp Mackall line will be inspected in 2014. B.2. Topographic Map. Attach to this application a topographic map of the map must show the outline of the facility and the following information. area.) a. The area surrounding the treatment plant, including all unit processes. b. The major pipes or other structures through which wastewater enters treated wastewater is discharged from the treatment plant. Include c. Each well where wastewater from the treatment plant is injected underground. d. Wells, springs, other surface water bodies, and drinking water wells works, and 2) listed in public record or otherwise known to the applicant. e. Any areas where the sewage sludge produced by the treatment works f. If the treatment works receives waste that is classified as hazardous or special pipe, show on the map where the hazardous waste enters B.3. Process Flow Diagram or Schematic. Provide a diagram showing the backup power sources or redundancy in the system. Also provide a water chlorination and dechlorination). The water balance must show daily average rates between treatment units. Include a brief narrative description of the B.4. OperationlMaintenance Performed by Contractor(s). Are any operational or maintenance aspects (related to wastewater treatment area extending at least one mile beyond facility property boundaries. This (You may submit more than one map if one map does not show the entire the treatment works and the pipes or other structures through which outfalls from bypass piping, if applicable. that are: 1) within 'A mile of the property boundaries of the treatment is stored, treated, or disposed. under the Resource Conservation and Recovery Act (RCRA) by truck, rail, the treatment works and where it is treated, stored, and/or disposed. processes of the treatment plant, including all bypass piping and all balance showing all treatment units, including disinfection (e.g., flow rates at influent and discharge points and approximate daily flow diagram. and effluent quality) of the treatment works the responsibility of a and describe the contractor's responsibilities (attach additional contractor? 0 Yes "4 No If yes, list the name, address, telephone number, and status of each contractor pages if necessary). Name: Mailing Address: Telephone Number: ( ) • Responsibilities of Contractor: B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule. None b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. ❑ Yes ❑ No EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 7 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber c. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable). d. Provide dates imposed applicable. For improvements applicable. Indicate Implementation Stage - Begin Construction - End Construction - Begin Discharge - Attain Operational e. Have appropriate Describe briefly: by any compliance schedule planned independently dates as accurately as possible. Level permits/clearances conceming other or any actual dates of completion for the implementation steps listed of local, State, or Federal agencies, indicate planned or actual completion Schedule Actual Completion MM/DD/YYYY MM/DD/YYYY below, as dates, as 0 No / / / / / / / / / / / / Federal/State requirements been obtained? 0 Yes B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD Applicants that discharge to waters of the US must effluent testing required by the permitting authority on combine sewer overflows in this section. All information using 40 CFR Part 136 methods. In addition, this data QA/QC requirements for standard methods for analytes based on at least three pollutant scans and must be Outfall Number: 001 ONLY). provide effluent testing data for the following parameters. Provide for each outfall through which effluent is discharged. Do not include the indicated information conducted other appropriate data must be reported must be based on data collected through analysis must comply with QA/QC requirements of 40 CFR Part 136 and not addressed by 40 CFR Part 136. At a minimum effluent testing no more than four and on -half years old. 'xy TACJIYIUM 'F �iISCHARG s. IDAI1/EE1)`DAl lgIGHAE _ t - #a` ] "k_ 7 "„ �„ .i+=l. �. 4�3. � L.�#*- »« a A#J I A> p1):LUTi11`� - F�''q,�YS ss. ! yx 3' + ' 1: 2 3 b - .. 'h � ' V-t 3-aT— �.:� ,-�-w 3 #' M � , i ).���Y ��:. a } i- i�5 •� "a' 4, j �tk � : ��.... rx -t i y„ �"{.may, Ila lx = i f :'r�s may{.. ": 3 Y�_} ia�"�1, ,.3 L " }i' 4 I't`3 }G x,y � -L 3 h'4..u� "��' ..r> V�it�`� � 'C n . r x� � +'?ci.,ari; � _ e '� 7S8".,�.-1a ample{., ice. +:u..:^ ST' ...r.1-'a. CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA (as N) 29.3 mglL 1.60 mg/L 249 SM4500NH3D CHLORINE (TOTAL RESIDUAL, TRC) 27.0 uglL 25.0 uglL 25 SM4500CI-G DISSOLVED OXYGEN 11.79 mglL 8.38 mglL 365 SM45000-G TOTAL KJELDAHL NITROGEN (TKN) 6.34 mglL 2.25 mg/L 13 SM450ONH3 F , NITRATE PLUS NITRITE NITROGEN 19.5 mg/L 14.7 mglL 13 SM4500 NO3 E OIL and GREASE 6.35 mg/L 2.12 mglL 3 EPA 1664 PHOSPHORUS (Total) 5.84 mg/L 3.20 mg/L 13 SM4500 PE TOTAL DISSOLVED SOLIDS (TDS) 380 mglL 349 mg/L 3 SM2540C OTHER ��ND .n:51-'k+�s6s�.'"�':_ VON Ei 1(IEW a-, O»►RT 11 ' CE B'`� �n" �5=� '�.�:-z z) r0 D 'ERMIN y T H OTHEJ 'AR NW' iu',4L .,, � �i�''z;�:.��*,�'x��r,4u2�'""�:� y.K'�Si.�x,,S,o.�t?x`"� EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 8 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber ;4" �. t� `�{'._y�µ ID4 4Y l e Kam•' ire • US: MAT ,-- d�+h{�. b y }1}:l 4 ., . 3+ ^X`ih i41i5 }a+:. `. 'nkr. h 4y� \.J. e�4'tt.�Z- •,._.a .?S�w�`�r`:f {l :,T."'u ._ .� �; k4., •i`� ... .= .m 4�'�,`��� .. ��� :s, �• All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application is submitted. Indicate which parts of Form 2A you have completed and are submitting: ® Basic Application Information packet Supplemental Application Information packet: ® Part D (Expanded Effluent Testing Data) ® Part E (Toxicity Testing: Biomonitoring Data) ® Part F (Industrial User Discharges and RCRA/CERCLA Wastes) 0 Part G (Combined Sewer Systems) it lGi11 QMPE 1iF�,�t�„ ,ICAO I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name and official title Larry Caddell- Chairman Signature G4liZALIA.K. Telephone number (910) 947-6403 Date signed 'e-24'1-01 + Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment works or identify appropriate permitting requirements. SEND COMPLETEDFORMS TO: NCDENR/ DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 9 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County.Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber ¢r.l oAPPLICAT ON INFORMATIONg PalitT D. EXPANDED DMA � Pis Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these_data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMITJM DAILY,DISCHARGEr,, P.NERAGE EtAi V ISCHARGE ,s OLLUTANT Conc. [ Conc. :. 3 ir)- umber : -; of s � ANALY ICAL METHOD M M DLL .,_ b.e .`1 a _..., , ._ .,:�4 _v.. .� _ ��._ Samples: � METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. - ANTIMONY <0.025 mg/L <0.025 mg/L 4 EPA 200.7 ARSENIC <0.010 mg/L <0.010 mg/L 4 EPA 200.7 BERYLLIUM <0.001 mg/L -" <0.001 mg/L 3 EPA 200.7 CADMIUM <0.002 mg/L <0.002 mg/L 4 EPA 200.7 CHROMIUM <0.005 mg/L <0.005 mg/L . 4 EPA 200.7 COPPER 0.017 mg/L 0.011 mg/L 4 EPA 218.2 LEAD 0.053 mg/L 0.018 " mg/L 4 EPA 200.7 MERCURY 4.63 ng/L 1.930 ng/L 12 EPA 1631 NICKEL 0.006 mg/L 0.008 mg/L 4 EPA 200.7 SELENIUM <0.010 mg/L <0.010 mg/L 4 EPA 200.7 SILVER <0.005 mg/L <0.005 mg/L 4 EPA 200.7 THALLIUM" <0.005 mg/L <0.005 mg/L 3 EPA 200.7 ZINC 0.089 mg/L 0.073 mg/L 4 EPA 200.7 CYANIDE <0.005 mg/L <0.005 mg/L 4 SM 4500 CN E TOTAL PHENOLIC COMPOUNDS 0.064 mg/L 0.020 mg/L 4 EPA 420.1 HARDNESS (as , CaCO3) , 121 mg/L 108 mg/L 4 SM 2340C Use this space (or a separate sheet) o provide information on other metals requested by the permit writer EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 10 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Outfall number: 001- Results Attached (Complete once for each outfall discharging effluent to waters of the United States.) ivri s i `" # ii LIf D1SC 1 = 7 ti ' 1 R%K0 �A L3 i31SCHP ' -atAI `s.i --- ,, r �;-,{,.. � ���� �� V� � y� j ..=g•tiii _ , g�+s Mass`^s•iz.. r€w-'='-.Y-�3t ._ _�::iy' �` 4, � .} .a.. "r .. 'c'.2-.•=:GY;"1` i€'. ^.*fF-fir. Mc� E .. aF� �� Y, \F..t:'-w-r,.v�e , +v�-1 `•�'+ a-�,. -5-"£� VOLATILE ORGANIC COMPOUNDS ACROLEIN ACRYLONITRILE BENZENE BROMOFORM CARBON TETRACHLORIDE CHLOROBENZENE CHLORODIBROMO- METHANE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM DICHLOROBROMO- METHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE TRANS-1,2-DICHLORO- ETHYLENE 1,1-DICHLORO- ETHYLENE 1,2-DICHLOROPROPANE 1,3-DICHLORO- PROPYLENE , ETHYLBENZENE METHYL BROMIDE METHYL CHLORIDE METHYLENE CHLORIDE 1,1,2,2-TETRA- CHLOROETHANE TETRACHLORO- ETHYLENE TOLUENE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 11 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Outfall number: 001- Results Attached (Complete once for each outfall discharging effluent to waters of the United States.) �,y:i 'Y*FF4'+�"`�r �'li"3?mt v sry IOC l�T Nt1' '.'.._ Vl- AiZ1ME�MD (L I�t 'G �1kn, _ i GE : t{c ;'�T'� nERAGE AtCX , tii'x N .�: ;^� DISC ARCS - l cs_z e�'�$: 4 t^.+�„ -- 7n .{.��Se ' , 3, M "3 i.- '4, ,, -T r k � 'T �" c nctin�, 4 - Hr F' ' ;{.�:•__k�,� av p asUtits 3� r ?T .� V` its., � CQrt' r'{+ .L$ t: 4 i� tinlM a 9 s k - a�`!�. =- t - _ '�..s f7 U�.t r- - ra `��'. _' Ff yJ* „ . " f- 1,1,1- TRICHLOROETHANE -T .�,:[ ....�,.x:t Ev.�.i:-; .. .�._3-,-t' _ __: ��..x5ia� .'"Y... _ 112 . TRICHLOROETHANE TRICHLOROETHYLENE VINYL CHLORIDE Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID -EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL 2-CHLOROPHENOL 2,4-DICHLOROPHENOL 2,4-DIMETHYLPHENOL 4, 6-D I N I T R O-O-C R ES O L 2,4-DINITROPHENOL 2-NITROPHENOL 4-NITROPHENOL PENTACHLOROPHENOL PHENOL 2,4,6- TRICHLOROPHENOL Use this space (or a separate sheet) to provide information on other acid -extractable compounds reques ed by the permit writer BASE -NEUTRAL COMPOUNDS ACENAPHTHENE ACENAPHTHYLENE ANTHRACENE BENZIDINE BENZO(A)ANTHRACENE BENZO(A)PYRENE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 12 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Outfall number: 001-Results Attached (Complete once for each outfall discharging effluent to waters of the United States.) z 'MAXIMUM DAll Y p,„ „_ _GE `x A /ERAG D 1 Y D SGFIARG - { ti h � w,; C rfc al a, : xfMass units f = Conc 3 1111 ,, t�n� u of samples trier " ANIiL' t AL HAD £ 3,4 BENZO- FLUORANTHENE BENZO(GHI)PERYLENE BENZO(K) FLUORANTHENE BIS (2-CHLOROETHOXY) METHANE BIS (2-CHLOROETHYL)- ETHER BIS (2-CHLOROISO- PROPYL) ETHER BIS (2-ETHYLHEXYL) PHTHALATE 4-BROMOPHENYL PHENYL ETHER BUTYL BENZYL PHTHALATE 2-CHLORO- NAPHTHALENE 4-CHLORPHENYL PHENYL ETHER CHRYSENE DI-N-BUTYL PHTHALATE DI-N-OCTYL PHTHALATE DIBENZO(A,H) ANTHRACENE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 3,3-DICHLORO- BENZIDINE DIETHYL PHTHALATE DIMETHYL PHTHALATE 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE • 1,2-DIPHENYL- HYDRAZINE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 13 of 22 c FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Outfall number: 001-Results Attached (Complete once for each outfall discharging effluent to waters of the United States.) . - t' l M CIII ei. tlI�C.DA1LV D H RG '4, i ..;A Y fls ^.�' f �4 � ERAS „ .Gfh/1LiE..DACL.X -� �az.._..trr SCHA� q CsSCrtIAR�i` S a"t„sz , c x -4, k Un Is -- -^ v. �. ..b..r-iY e ,, f , 'lr� a''S- .,Samilptf ,..�c- mow' L.UT IT Y = ;.- , —_ -,+ ,,. ,.," ti a�� �;�- A � . -. �u :.�,• �7 T* -._�r - ;w.lh,'� �- � �.-_.Tn X�! _ , p S`.,. - F . '� F�� - ' YHIW .-e ' �i's.-a:. r r.:a 34;, j+^ Conn � .f f�+ , Units p -7 ,-�"� -1N+<<' 't l-.. + �7x, Ma im -i, � 3 y HOP - . = +f a._Y - - r- - 7 3 °. -.�. id $.., FLUORANTHENE FLUORENE _ HEXACHLOROBENZENE HEXACHLORO- BUTADIENE HEXACHLOROCYCLO- PENTADIENE HEXACHLOROETHANE INDENO(1,2,3-CD) PYRENE ISOPHORONE NAPHTHALENE NITROBENZENE N-NITROSODI-N- PROPYLAMINE N-NITROSODI- METHYLAMINE N-NITROSODI- PHENYLAMINE PHENANTHRENE PYRENE 124 TRICHLOROBENZENE Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer Use this space (or a separate sheet) to provide information on other pollutants (e.g , pesticides) requested by the permit writer :�`.3c.-�`3'yx:�::•: ,�� �. '��'E �" .�'4 R O vvs.cq .: ' y. :.x:vz„ a k'..� a;s 5 x. x� �� ,', a ter• •�.. f' `"ia - . t .#�y1y+.i TH, P A 9 o Ei I '1 E��41I E 1l H OTHE , z .frtom:-ss'�.�_',�.; EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page14of22 - FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control,NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber •�}^.r k_s 7l.. v. s� APLGQ Q ,5e•'t.;datt> PPLEiM .:rb7 \ '..4++?3'^ a. . . A 1^d H�' �y"•F.ksz'-�sn.rsJ �_ -`¢ i+YF� 3 . ..$. gr. •9£`3^+�,`.F"y'u�v�F,? p� �;t� exn �s-; R} RrLp.eNRwf@XF',+'°--vS7ef ah ''Y.e i3 ml ti3"'�'i �+"'i +7 $ix°`.9xiaYs..:k. L' y� i1lJE3'3a."�S� i'�s,"C+ �+w .�;e.� v>k' kw.�? r..+�- x �' =i�v. i � +t. F i5'�eAY.t_u �.a _.., POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.1. Required Tests. Indicate the number of whole effluent ❑ chronic ❑ acute E.2. Individual Test Data. Complete the column per test (where each species - toxicity tests conducted in the past four and one-half years. following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one constitutes a test). Copy this page Test number: if more than three tests are being reported. Test number. Test number. a. Test information. Results Attached Test Species & test method number Age at initiation of test Outfall number Dates sample collected Date test started Duration b. Give toxicity test methods followed. Manual title Edition number and year of publication Page number(s) c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 15 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution •Control,NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Test number: Test number: Test number: e. Describe the point in the treatment process at which the sample was collected. Sample was collected: f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity Acute toxicity g. Provide the type of test performed. Static Static -renewal Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Receiving water i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water Salt water j. Give the percentage effluent used for all concentrations in the test series. "" w^ .i .:"w n, .t,„. ;' '+4 �ji.'ti"t �y k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Salinity Temperature Ammonia Dissolved oxygen I. Test Results. Acute: Percent survival in 100% effluent LC50 95% C.I. % % % Control percent survival % % Other (describe) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 16 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Chronic: NOEC % % % IC25 - % % Control percent survival % % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? Was reference toxicant test within acceptable bounds? What date was reference toxicant test run (MM/DD/YYYY)? / / / / / / Other (describe) E.3. Toxicity Reduction Evaluation. ❑ Yes ® No Is the treatment works involved in a Toxicity Reduction Evaluation? If yes, describe: E.4. Summary. of Submitted Biomonitoring Test Information. If you have cause of toxicity, within the past four and one-half years, provide the dates of the results. Date submitted: / / (MM/DD/YYYY) submitted biomonitoring test information, or information regarding the the information was submitted to the permitting authority and a summary Summary of results: (see instructions) All results are attached. �� Ems, *� ,` , � �Fo-�es.e� -:ram � 'fix sr +' � w3 ..E."T� Y_.�` w� ^fy`.v» ti . 4,- A:-....»..?. "f. i.".,'?F zc ,a. G>Fe, .�«r r-^a.'#'•.^'R., .+..:^�521..;s EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 17 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: • Lumber t-1-3- �} 'a,�''a '" OP PMEN E R A,7 3 kit '�tx+Y;NF' j} ,x iF,., -- € a §'� "-"'":._� wr '33 ! - .,[•'S"' . ''NRE'x€`;�% 41SRD)!`s?` G+ 1r'C . G-1'^?CF RIE� %�., - .:. Y t •�F n st "'� �.}3.: �,�?i All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have, or is subject to, an approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number industrial users that discharge to the treatment works. a. Number of non -categorical SIUs. 0 or other remedial wastes must - of each of the following types of questions F.3 through F.8 and b. Number of CIUs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: to the treatment works, copy Supply the following information for each SIU. If more than one SIU discharges provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Erico, Inc Mailing Address: 188 Carolina Road Aberdeen, NC 28315 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Electroplating. of grounding rods with copper and nickel F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Grounding Rods - Raw material(s): Steel rod and coil F.6. -Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into day (gpd) and whether the discharge is continuous or intermittent. 9233 gpd (100% continuous or intermittent) the collection system in gallons per into the collection system b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits . ® Yes 0 No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 433- Electroplating and Metal Finishing EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 18 of 22 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe? ❑ Yes ® No (go to F.12) F.10. Waste transport. Method by which RCRA waste is received (check all that apply): ❑ Truck ❑ Rail 0 Dedicated Pipe F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units). EPA Hazardous Waste Number Amount Units CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? ❑ Yes (complete F.13 through F.15.) ® No F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or isexcepted to origniate in the next five years). F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets if necessary.) F.15. Waste Treatment. a. Is this waste treated (or will be treated) prior to entering the treatment works? ❑ Yes ❑ No If yes, describe the treatment (provide information about the removal efficiency): b. Is the discharge (or will the discharge be) continuous or intermittent? ❑ Continuous 0 Intermittent If intermittent, describe discharge schedule. EFER ` EaA P GATt(� 01lERV Elit1 bAGIE. TU E 'ERMINE 11dIII� CH RS P RT t Y `jam fi ca- '±�"i#SF 3 } t R { ,fps #4� ,t?Rt l 2�0. YO►U • ST t1A CpiVtPLET .�^v:.ft .'�.. �� i �A X .�5�f :_`„ c... n..,4 _..x'Sf:.. . �...R _ _ .. ,,7. .:•v.s - � .-k+,?..;i EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 19 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: • RIVER BASIN: .. ,, 1aYi �. �� `k ' �.�SYS '�f'y}y'"ai` lPPLEME L kPPLt f `I 1 fil . I n � _ - ms_ �..w.. _: t _ f �s,t ?ma`s;•- .i't u^e-s?s',P}"+°3swl:9;vv.,"S<.K.Ysa`i �. : {f "ems){ _`�'" fi„ ED' Et2 STEMS , ' z _ k ,4 If the treatment works has a combined sewer system, complete Part G. G.1. System Map. Provide a map indicating the following: (may be included with Basic Application Information) a. All CSO discharge points. b. Sensitive use areas potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, outstanding natural resource waters). c. Waters that support threatened and endangered species potentially affected by CSOs. G.2. System Diagram. Provide a diagram, either in the map provided in G.1 or on a separate drawing, of the combined includes the following information. a. Location of major sewer trunk lines, both combined and separate sanitary. b. Locations of points where separate sanitary sewers feed into the combined sewer system. c. Locations of in -line and off-line storage structures. d. Locations of flow -regulating devices. e. Locations of pump stations. CSO OUTFALLS: sensitive aquatic ecosystems, and sewer collection system that Complete questions G.3 through G.6 once for each CSO discharge point. G.3. Description of Outfall. a. Outfall number - b. Location • (City or town, if applicable) (Zip Code) (County) (State) (Latitude) (Longitude) c. Distance from shore (if applicable) ft. d. Depth below surface (if applicable) ft. e. Which of the following were monitored during the last year for this CSO? 0 Rainfall 0 CSO pollutant concentrations 0 CSO frequency ❑ CSO flow volume 0 Receiving water quality f. How many storm events were monitored during the last year? G.4. CSO Events. a. Give the number of CSO events in the last year. events (❑ actual or 0 approx.) b. Give the average duration per CSO event. hours (0 actual or ❑ approx.) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 20 of 22 FACILITY NAME AND PERMIT NUMBER: I PERMIT ACTION REQUESTED: RIVER BASIN: G.S. G.6. c. Give the average volume per CSO event. million gallons (0 actual or 0 approx.) d. Give the minimum rainfall that caused a CSO event in the last year Inches of rainfall Description of Receiving Waters. a. Name of receiving water: b. Name of watershed/river/stream system: United State Soil Conservation Service 14-digit watershed code (if known): c. Name of State Management/River Basin: United States Geological Survey 8-digit hydrologic cataloging unit code (if known): CSO Operations. Describe any known water quality impacts on the receiving water caused by this CSO intermittent shell fish bed closings; fish kills, fish advisories, other recreational loss, (e.g., permanent or intermittent beach closings, permanent or or violation of any applicable State water quality standard). & .�e e 7 ti 1T EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 21 of 22 Additional information, if provided, will appear on the following pages. FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber. ro" ' �'� y.� �.: �' � a � +, r � rx { '' +., F:'. ".r :e°..,i'v;s.;°. �.F d::frs51' --{'�`^'{�-� � ^'fir •S .42 . ; a�ti "fi ' :'y A� s tl' � a 3' _ �'' • ; ",', `a SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. • Name: Pinnacle Furnishings, Inc Mailing Address: 10570 NC Hwy 211 East Aberdeen, NC 28315 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Electroplating and anodizing of aluminum metal F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Furniture for hotels, casinos and restaurants Raw material(s): Aluminum metal F.6. Flow Rate. c. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the day (gpd) and whether the discharge is continuous or intermittent. 1550 gpd ( continuous or 100% intermittent) collection system in gallons per into the collection system _ d. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( - continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes 0 No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 433- Electroplating and Metal Finishing F.S. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused -or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? 0 Yes ® No If yes, describe each episode. NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control, NC0037508 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber _. J air €N >i, OF 't' i h �i'Yzre �S`4 wi dl� 1�iS �,4i: It S D + , +G S l �Gfi #1 lE� . b 5 � � `� ,• �` . questions F.3 through F.8 and SIGNIFICANT INDUSTRIAL USER INFORMATION: to the treatment works, copy Supply the following information for each SIU. If more than one SIU discharges provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Thermal Metal Treating, Inc Mailing Address: PO Box 367 Aberdeen, NC 28315 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Electroplating and metal heat treating F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Residential and commercial door hardware, industrial tools and automotive components Raw material(s): Brass, steel, and nickel parts F.6. Flow Rate. e. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into day (gpd) and whether the discharge is continuous or intermittent. 540 gpd ( continuous or 100% intermittent) the collection system in gallons per discharged into the collection system f. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 433- Electroplating and Metal Finishing F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. NPDES FORM 2A Additional Information NPDES Permit No. NC0037508 Moore County WWTP Hereivinc Stteutru AberdeenCteak Drainage &situ bitrber River Latitude! 35.04 ' 03"H Lmicitude: 79 28' 08"W Sub-Baahu 03-07-50 Permitted Plow: 6.7 /10.0 MGD State Grid USCS Quad: G 2IS W/ Nub lufgN.C. Stream Clatr: C NPDES Permit NC0037508 Moore COunty Moore County Water Pollution Control Plant Process Narrative Moore County Water Pollution Control Plant is an activated sludge treatment facility with two stages of aeration and three stages of sedimentation. Anaerobic digestion is utilized to reduce the volume of sludge. Sludge is subsequently pressed and stockpiled before disposal. Raw sewage enters the wet well of the Raw Sewage Pump Station by gravity and is screened and pumped to the Grit Removal Unit where grit is separated from the raw flow. The sewage then flows to the primary clarifiers (three) from which the primary sludge flows to the digesters. Flow then goes into the First Stage Aeration Basin where diffused aeration is employed to reduce the BOD of the wastewater. The Intermediate Clarifiers (three) receive the flow, and the settled sludge is returned to the aeration basin with excess going to the digester. The wastewater then enters the Second Stage Aeration Basin where diffused aeration further reduces the BOD and also accomplishes nitrification. The Final Clarifiers (three) then provide final sedimentation of the activated sludge which is returned to the aeration basin with excess to the digesters. The liquid flowing over the wier of the Final Clarifier then flows to a sand filter which further reduces the TSS/BOD and turbidity. UV bulbs disinfect the water prior to discharge. The fmal step in treatment is the Cascade Aerator which allows the remaining elevation to be employed to increase the oxygen content of the treated effluent. The primary sludge is pumped to one of two Anaerobic Digesters. The waste activated sludge from the Intermediate Clarifiers and the Final Clarifiers is thickened prior to going into the other Anaerobic Digester. Digested sludge from both primary digesters is sent to the Secondary Digester for further treatment and is periodically withdrawn and pressed on a Belt Press to form a cake. The cake is stockpiled on covered beds prior to final disposition at either a landfill or composting facility. The following section provides a brief description of each process unit. Raw Sewage Pump Station The Raw Sewage Pumping Station wet well receives the raw flow and the in -plant waste flow through a mechanically cleaned bar screen. The purpose of these units is to remove rags, sticks, and other debris that may, interfere with the equipment and treatment units that follow. Bar screening is also done at the pump stations ahead of the pumps. The screenings are landfilled. The wet well has a small volume to prevent septicity of the sewage during low flow. Four dry pit submersible pumps take suction from the wet well and maintain the wet well level in a narrow range as the inflow varies. Grit Removal Unit The effluent from the Raw Sewage Pump Station enters the parshall flume at the Grit Unit where the total waste flow measurement is made. The dischargefrom the parshall flume is routed through control gates to two grit chambers where sand and other heavy particulate matter settle from the wastewater. The settled grit is pumped from the bottom of each chamber by two grit pumps discharging into the grit washer where the grit slurry is washed. A screw conveyor carries the grit at an incline (to allow dewatering) to a container located outside the Grit Unit. The grit thus collected is landfilled. Wastewater in the Grit Unit flows over a wier into the effluent line ensuring a grit free discharge to the Primary Clarifiers. Primary Clarifiers Three 75.0 ft. diameter settling tanks receive the wastewater from the Grit Unit. Settled solids (sludge) from the clarifiers are mechanically collected for pumping to the anaerobic digesters. Sewage enters the clarifier at the center and flows through ports in the top of the central vertical pipe, then radially to a peripheral effluent wier. A very slowly rotating collector arm plows settled solids to the sludge draw off pit at the center of the tank. A skimmer attached to the arm collects scum from the surface and drops it into a scum box that drains outside the tank wall. Both primary sludge and scum are allowed to flow into a pit located beside the clarifier. This primary sludge in the pit is then pumped directly to the anaerobic digesters by pumps located in the Grit Unit. First Stage Aeration Basin The First Stage Aeration Basin is, separated into six rectangular compartments with diffused air. The effluent from the Primary Clarifiers flows into each compartment at three points for a step feed process. Return activated sludge from the Intermediate Clarifiers is pumped into each compartment at three locations further enhancing nutrient equalization. Wastewater flowing into the First Stage Aeration Basin contains organic matter (BOD) as a food supply. Bacteria metabolize the waste solids, producing new growth while taking in dissolved oxygen and releasing carbon dioxide. Protozoa graze on bacteria for energy to reproduce. Some of the new microbialgrowth dies releasing cell contents to solution for re -synthesis. After the addition of a large population of microorganisms, aerating raw wastewater for a few hours removes organic matter from solution by synthesis into microbial cells. Mixed liquor is continuously transferred to the Intermediate Clarifier for gravity separation of the biological floc. Settled floc (activated sludge) is returned continuously from the sludge hoppers at the Intermediate Clarifiers to the First Stage Aeration Basin for mixing with entering wastewater. Intermediate Clarifiers Three 90 ft. diameter settling tanks receive the flow of mixed liquor from the First Stage Aeration Basin. The purpose of the Intermediate Clarifiers is gravity separation of the biological growth suspended in the mixed liquor effluent from the aeration basin. The liquid flow pattern is the same as that of the Primary Clarifiers except that the sludge is collected with suction tubes that pick up sludge at several radii in the tank. The sludge collection system provides rapid withdrawal of sludge across the entire bottom of the tank. The retention time of solids that settle near the tank periphery is not greater than those that land near the center, thus, aging of the biological floc and subsequent floating solids due to gas production is eliminated. Settling sludge flows by gravity into the wet well in the Return Activated Pump Station #1 where it is then pumped into the First Stage Aeration Basin. Excess sludge is wasted to the Solid Handling Unit. Second Stage Aeration Basin The Second Stage Aeration Basin provides carbonaceous BOD removal and nitrification. The basin is subdivided into six compartments with baffles for plug flow. Each compartment is aerated with diffused air. The influent is split in control structure #4 and flows to the head of each of the six compartments. Activated sludge from the Final Clarifier is returned to the. head of each compartment. The process of nitrification involves oxidation of ammonia to nitrate. The important parameters in bacterial nitrification kinetics are temperature, pH, and dissolved oxygen concentration. Reaction rate is decreased markedly at reduced temperatures with about 80°F being the minimum reasonable value. Optimum pH in near 8.4 s.u. and the dissolved oxygen level should be greater than 1.0 mg/1. The system requires a long sludge retention time to preventexcessive loss of viable nitrifying bacteria. Since biological nitrification destroys alkalinity, lime slurry is added to the Second Stage Aeration Basin to raise the pH to the optimum level. Final Clarifiers Three 105 ft. diameter settling tanks receive the flow of mixed liquor from the Second Stage Aeration Basin. The purpose of the Final Clarifier is gravity separation of the biological growths suspended in the mixed liquor effluent from the aeration basin. Sludge is collected and returned to the aeration basin to maintain a supply of nitrifying organisms. The Final Clarifiers are, except for a greater volume, identical to the intermediate clarifiers. Sand Filter Flow from the Final Clarifiers is diverted to the Sand Filter into up to six individual compartments. Water enters and filters through a layer of sand, or media, removing fine suspended particles. By removing the fine particles, TSS and BOD are reduced as well as turbidity. Reduced turbidity is vital for UV disinfection to work properly. Polished effluent flows through an underdrain system beneath the media. UV Disinfection Ultraviolet light is used for disinfection to sterilize pathogens and control nuisance microorganisms. Eight banks, each containing thirty-two bulbs, are controlled based on the effluent flow. Cascade Aerator The treated wastewater leaves the UV banks and then flows over the Cascade Aerator. Water turbulence caused by the slats and steps increase the dissolved oxygen content of the water entering the receiving streams. Primary Anaerobic Digester The Primary Anaerobic Digesters (two) function to reduce the volume of sludge by providing an oxygen free environment for sludge digestion and gas formation. The purpose of sludge digestion is to convert bulky, odorous, raw sludge to a relatively inert material that can be rapidly dewatered in the absence of obnoxious odors. The bacterial process consists of two successive processes that occur simultaneously in digesting sludge. The first stage consists of breaking down large organic compounds and converting them to organic acids along with gaseous by-products of carbon dioxide, methane and trace amounts of hydrogen sulfide. In order for digestion to occur, second stage gasification is needed to convert the organic acids to methane and carbon dioxide. This stage is very sensitive to environmental conditions of temperature and pH. The primary Anaerobic Digesters are completely mixed by a gas compressor that forces the sludge gas collected under the floating cover down to the bottom of the digestion tank. The rising gas bubbles provide complete mixing of the digested contents. Two sludge heaters are provided to maintain the temperature at an optimum 95°F for best digestion. The gas collected in the digester is used to fuel the sludge heaters and heat the Solid Handling Unit. Excess gas is allowed to bum in the waste gas burner. Secondary Anaerobic Digester Since the contents of the Primary Anaerobic Digester are completely mixed, no sludge thickening is possible in this unit. The purpose of the Secondary Digester is to provide an environment where anaerobic digestion can continue under minimum hydraulic disturbances which result in a dense sludge at the bottom of the digester and a clear supernate above the sludge. Gravity Belt Press/Thickener Waste activated sludge from the Intermediate Clarifiers and Final Clarifiers is thickened prior to entering the primary digester. Periodically, sludge is withdrawn from the secondary digester and sent to the belt presses (two) to be de -watered. Polymer is added to increase efficiency. Dewatered sludge is stockpiled on covered beds prior to disposal. Moore County Water Pollution Control Plant Flow Schematic Raw Sewage Pump Station 1.0-2Q mgd Grit Removal Unit Raw Sewage Influent 4.889mgd Avg ,. rr Grit to Disposal mgd Primary Clarifier Primary Sludge 1st Stage Aeration Basin Intermediate Clarifier 1.0-300 mgd mgd fRetum Activated 0216ityl BOD Make-up 0-1.4mgd Anaerobic Digesters 2nd Stage Aeration Basin Return Activated 0-10m Final Clarifier mgd Waste Activated Sludge— to thickener WAS— thickened Sludge to be "Pressed Secondary Digester -v Gravity Thickener/ Belt Press 1.0-?`0 mgd UV Disinfection Cascade Aeration Effluent Discharge 001 10 MGD 4.982mgd Avg Sludge to Disposal 3 Generators for Back up Power ADDENDUM 2 NPDES PERMIT #NC0037508 REQUEST FOR RENEWAL January 10, 2014 Whole Effluent Toxicity: Moore County Water Pollution Control Plant had one failed toxicity test which occurred. in September 2010. Our quarterly chronic pass/fail Ceriodaphnia testing resulted in a fail. In October 2010, we split the sample between our commercial lab and a second lab. Both tests resulted in >100%. In November 2010, the result was 57.98%. The result for the quarter was a pass. All testing since September 2010 has resulted in `pass' results, including four second species tests in 2013. Our commercial lab changed in July 2011. The following toxicity procedures are still followed each time toxicity tests are conducted: New tubing is installed prior to the beginning of collection. Cleaning procedures for tubing and collection jugs are performed prior to the first use and every toxicity collection day following. Procedures for pouring samples into containers allow proper mixing and allow split samples to be split properly. The location of toxicity sample collection is at the effluent composite sample location at the bottom of the cascade. Chains -of -custody are filled out properly with all signatures needed and anyone who assisted in the sample collection or handling is noted. Any plant process changes during the week prior and the week of toxicity testing are to be made only by the ORC. There is no cleaning of clarifiers or basins during the week prior to and the week of toxicity testing. Attached are all toxicity test results for the years of 2010, 2011, 2012,.and 2013. If you have any questions concerning our past toxicity results, please do not hesitate to contact George Yankay at (910) 281-3146. Facility: Moore County Ty: Research & Apalysical Laboratories NCOO 37508 Pipe #: 001 County: Moore Comments Final Effluent Signa x I r, R = .63sible Ch- ge Sigr(aturdof Labors ''ry Supervisor RAL#767183,767521.767654 MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time Sept 11,2013/ 1408pm % Eff. Repl. Contro . Surviving # Original # Wt/original (mg) 25 Surviving # Original # Wt/original (mg) I 37.51 Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) 50 lb Surviving # Original # Wt/original (mg) 1001 Surviving # Original # Wt/original (mg) water uuality uata Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin HIE Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mglL) Conductivity (umhos/cm) Chlorine(mg/L) Temp. at Receipt (IC) Dilution H2O Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) 2 3 . 4 Avg WtlSurv. Control 15 , 15 15 15 15 15 15 15 0.9087 0.9460 0.8960 . 0.8280 15 15 15 15 15 15 15 15 0.8073 . 0.9053 0.9133 0.8720 15 -15 15 15 15 15 15 15 0.8913 0.8200 0.9153 0.9727 15 15 15 15 15 15 15 15 0.9587 0.8760 0.9367 0.8633 15 15 15 15 15 15 15 15 0.9193 0.9627 - 0.8980 0.9433 15 15 15 15 15 15 15 15 0.8640 0.9387. 0.9447 0.8680 !Jay % Survival Avg Wt (mg) % Survival Avg Wt (mg) Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) 0.8947 100.0 1 l 0.8947 100.0 0.8745 100.0 0.8998 100.0 0.9087 100.0 0.9308 ( I 100.0 0.9039 b ti Test Organisms Outside Supplier Hatch Date: 09/09/2013 Hatch Time: after 1600 6.92 7.06 6.94 7.07 6.93 7.07 6.91 7.08 6.93 7.08 6.93 7.07 6.98 . 7.05 8.60 / 7.10 8.60 6.60 8.50 5.50 8.60 5.30 8.60 5.70 8.60 5.30 8.60 5.40 24.5 / 24.4 24.6 24.7 24.7 24.7 24.5 24.4 24.6 24.7 24.4 24.5 24.6 24.6 4 b ti 7.01 / 7.15 • 7.02 7.16 7.02 7.15 7.02 7.21 7.03 7.28 7.08 7.21 6.98 7.22 8.60 / 7.30 8.60 6.80 8.60 5.40 8.50 5.40 8.50 ' 5.30 8.50 5.20 8.30 5.20 24.5 / 24.4 24.6 24.7 24.7 24.7 24.5 24.4 24.6 24.7 24.4 24.5 24.6 24.6 2 3 9-Sep-13 12-Sep-13 , 15-Sep-13 24.00 23.00 24.00 67 . 60 54 46 41 43 462 482 468 0.04 0.06 0.04_ 1.4 3.2 1.4 48 38 193 Survival Growth Normal >rl 171 Overall Result Horn. Var. fl I✓ I ChV >100% NOEC 100% 100% LOEC 100% 100% ChV >100% >100% Method Steel's Dunnett's Stats Survival Growth Conc. Critical Calculated Critica Calculated 25 10 16 2.41 0.6 37.5 10 18 2.41 -0.153 50 10 19 2.41 -0.415 75 .10 , 22 ._ ..2,41_.____ 100 10 18 2.41 -0.2725 DWQ Form AT-5 (1/04) acli : Moore County NC00 37508 Pipe #: 001 County: Moore orates/ Research & Analytical Laboratories Signature of Q erator • Re ?o Si. =.Charge x Signature-6f Lab6ratory u.ervisor Comments l! Final Effluent RAL #759440,759759,759841 MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation DatefTime % Eff. Repl. Contro Surviving # Original # Wt/original (mg) 25 Surviving # Original # Wt/original (mg) .b Surviving # Original # Wt/original (mg) 5U Surviving # Original # Wt/original (mg) b Surviving # Original # Wt/original (mg) 00 Surviving # Original # Wt/original (mg) water uuallty uata Control pH (SU) init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin HIE Concentration pH (SU) Init/Fin DO (mg/L) 'nit/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) conductivity (umhos/cm) Chlorine(mg/L) Temp. at Receipt (IC) Dilution H2O Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) June 5,2013 / 1456pm 2 Avg Wt/Surv. Control 15 . 15 15 15 - : - 15 - 15 15 15 0.8480 0.7067 0.7933 0.8853 15 15 15 15 15 - 15 15 15 0.8780 0.7220 . 0.8247 0.8633 15 15 15 15 15 15 -15 15 0.8140 0.8567 0.9227 0.8527 15 15 .15 15 1515 - 15 15 0.8587 0.8333 0.9607 0.8673 15 15 15 15 15 15 15 - . 15 0.8913- 0.8633 0.7600 0.8393 15 15 15 15 15 '15 15 15 0.7787 0.8947 0.8667 0.7873 uay % Survival • Avg Wt (mg) Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt(mg) % Survival Avg Wt (mg) - % Survival Avg Wt.(mg) 0.8083 100.0 0.8083 100.0 0.8220 100.0 0.8615 100.0 0.8805 100.0 0.8385 100.0 0.8318 Test Organisms 11' Outside Supplier Hatch Date: 06/03/2013 Hatch Time: after 1600 1 2 6 6.94 7.07 6.95 7.28 6.96 7.06 6.93 7.12 6.97 - 7.10 6.96 7.11 6.95 7.04 8.60 / 8.10 8.50 6.70 8.40 5.60 8.60 5.40 , .8.60 5.60 8.60 6.40 8.60 -- 5.30 24.4 / 24.4 24.6 24.5 24.4 24.5 24.6 24.5 24.6 . 24.6 24.6 24.6- 24.4 24.6 2 b 7.16 / 7.17 7.04 7.05 7.33 7.08 7.22 7.18 7.40 7.17 7.35 . 7.17 7.17 7.15 8.60 / 7.20 8.60 5.70 8.60 5.40 8.60 5.50 8.60 -'6.20 8.60 6.00 - 8.60 - 5.60 24.4 / 24.4 24.6 24.5 24.4 24.5 24.6 24.5 24.6 - 24.6 24.6 24.6 24.4 24.6 2 3-Jun-13 6-Jun-13 9-Jun-13 23.00 : 24.00 . 24.00 46 - . 44 68 87 . 83 - 80 - 484 . 426 324 0.07 0.03 0.03 2.0 0.7 3.1 48 38 189 Survival Normal Hom. Var. VI NOEC - - 100% LOEC 100% ChV >100% Growth 171 If 100% 100% >100% Method . Steel's . Dunnett's Stats Conc. 25 37.5 10 50 Survival Critical . 10 10 • 75 - 10 100 10 Calculated 19 22 . Overall Result ChV >100% Growth Critical Calculated 2.41 - -0.3154 2.41 -1.2271 22- , 2.41-1.6647 20 19 . 2.41-0.6954 2.41 -0.5426 - DWQ Form AT-5.(1/04) [C,N 0..// Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:03/13/13 • Facility: Moore County -.,.Labpatory: Research.4 Analytical Laboratories ix i:.i• �;i Signature of eratoril1Pon Charge x NC00 37508 Pipe #: 001 County: Moore Signatur{'of Laboratory Supervisor . Comments 1 Final Effluent RAL #, 752501,752797,752886 MAIL ORIGINAL TO:. Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/me 6-Mar-13 / 3:28 PM % Eff. Repl. CContro Surviving # Original # Wt/original (mg) Surviving # Original # Wt/originat-(rng). 2b 3 /.b Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) 50 ib Surviving # Original # Wt/original (mg) 100 Surviving # Original # Wt/original (mg) water 6tualrty uata Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Hig Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin . Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Term. at Receipt (IC) Dilution H2O Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) 2 4 Avg WtlSurv_ Control 15 15 15 15 15 15 15 15 0.9713 0.9433 0.9560 0.9753 15 15 15 15 15 '15 15 15 . 0.9567 0.9247 0.9160 1.1580 15 15 15 15 15 15 15 15 0.9247 1.0347 0.9100 1.0740 15 15 15 15 15 15 15 15 1.1000 1.0040 0.9573 . 0.8513 15 15 15 15 15 15 15 15 1.0120 0.8867 1.0127 0.9253 15 15 15 15 15 15 15 15 0.9680 0.9073 - 0.9967 0.9713 nay 0.9615 Test Organisms r Cultured In -House % Survival' 100.0 Outside Supplier Avg Wt (mg)'. 0.9615 1 Hatch Date: 3/4/2013 Survival' 100.0 Hatch Time: after1600 Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) 0.9888 100.0 0.9859 100.0 0.9782 100.0 0.9592 100.0 0.9608 2 4 6.93 7.23 6.94 7.08 6.92 7.23 6.99 . 7.29 6.98 7.16 6.94 7.14 6.94 7.10 8.60 / 8.10 8.60 .. 8.20 8.60 5.40 8.40 6.40 8.40 6.70 8.40 7.20 8.60 6.00 24.5 / 24.7 24.4 .24.7 24.4 24.8 24.4 24.8 24.5 24.7 24.6 - 24.8 24.6 24.8 2 5 6 7.63 / 7.27 7.52 7.41 7.29 7.38 7.20 . 7.06 7.20 7.35 7.43 7.47 7.29 7.46 8.50 / 8.00 8.50 7.90 8.40 5.90 8.40 6.40 8.50 7.90 8.60 6.90 8.50 5.90 24.5 / 24.7 24.4 24.7 24.4 24.8 24.4 24.8 24.5. 24.7 24.6 24.8 24.6 24.8 2 3 4-Mar-13 7-Mar-13 10-Mar-13 24.00 23.00 24.00 111 107 103 142 123 : 125 506 480 463 0.06 <0.01 0.03 0.5 0.7 1.8 48 38 198 Survival Normal d I` Hom. Var. 11. NOEC 100% Growth Overall Result EI ChV • 100% LOEC 100% 100% -ChV >100% >100% Method Steel's Dunnett's >100%. Stats Survival Growth Conc. Critical Calculated Critical Calculated 25 10 , 16 2.41 -0.5003 37.5 10 18 2.41 -0.4455 50 10 20 2.41 -0.3048 75 10 18 2.41 0.0422 100 10 18.5 2.41 0.0119 -- Effluent Tc.xicity Report Form -Chronic Fathead Minnow Multi -Concentration Test 4 Facility'Moore County NCOO 37508 Pipe #: 001 County: Moore Laboratory: Research & Analytical Laboratories J. Signature of Oper fin Re'sp'or}¢j`b x Signature o orat Supervis Comments 1 Final Effluent RAL # 74595874�2 MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 h BY: Test Initiation Date/Time Dec 05,12 / 1445pm . % Eff. Repl. Contro Surviving # Original # Wt/original (mg) 251 Surviving # Original # Wt/original (mg) 37.5 Surviving # Original # Wt/original (mg) 50 Surviving # Original # Wt/original (mg) 75 Surviving # Original # Wt/original (mg) 100 Surviving # Original # Wt/original (mg) Water Quality uata Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Hic Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Terrp. at Receipt (iC) Dilution H2O Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) 2 3 4 Avg Wt/Surv. Control 15 15 15 15 15 15 15 15 0.9173 0.9627 0.9547 0.8593 15 15 15 15 15 15 15 15 0.8813 0.8620 0.9527 0.9507 15 15 . 15 15 15 15 15 15 0.9893 0.9320 0.9527 1.0433 15 15 15 15 15 15 15 - 15 0.8533 0.8940 0.8927 0.9286 15 15 15 .15 15 15 15 15 0.9987 1.1053 0.9573 0.9440 15 15 15 15 15 15 . 15 15 0.9093 0.9567 0.8927 0.7527 Day % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) 0.9235 100.0 0.9235 100.0 0.9117 100.0 0.9793 100.0 0.8922 100.0 1.0013 100.0 0.8779 Test Organisms I_ Cultured In -House j+ Outside Supplier. Hatch Date: 12/3/2012 Hatch Time: after1600 1 2 3 5 6.94 7.15 7.04 6.98 6.98 6.75 7.02 6.67 7.12 6.97 6.99 6.84 7.06 7.09 8.60 / 6.40 8.50 6.60 8.50 .6.40 8.60 6.30 8.50 6.00 8.60 5.80 8.60 6.10 24.5 / 24.8 24.6 24.8 24.7 24.6 24.6 24.6 24.7 24.5 24.6 24.8 24.7 24.6 1 4 5 b 7.25 / 7.20 7.16 6.93 7.39 6.82 7.44 6.80 7.26 6.91 7.14 6.93 7.21 6.99 8.60 / 6.00 8.50 6.30 8.50 6.30 8.60 5.40 8.40 5.70 8.50 5.30 8.50 5.40 24.5 / 24.8 . 24.6 24.8 24.7 24.6 24.6 24.6 24.7 24.5 24.5 24.8 24.7 24.6 2 3-Dec-12 6-Dec-12 9-Dec-12 23.25 23.50 23.00 106 . 105 94 147 139 143 532 501 401 0.03 <0.01 <0.01 2.4 2.1 2.6 48 38 207 Survival Normal F"k Hom. Var. Irk NOEC 100% Growth Overall Result 1115I; ChV qr 100% LOEC 100% 100% ChV >100% >100% Method Steel's Dunnett's >100% Stats Survival Growth Conc. Critical Calculated Critical Calculated 25 10 16 2.41 0.2841 37.5 10 22 2.41 -1.3411 50 10 14 2.41 0.7531 75 10 23 2.41 -1.8696 100 10 15 2.41 1.0966 DWQ Form AT-5 (1/04) x ( ` •� ,� lgn u� Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Facility: MOORE CO. WWTP Laboratory Perfor ing Test: f ./ ram. S'- o rOperator- n Responsible Charge NPDES#: NC003750B Pipe#: R & A LABORATORIES, INC. eo Laboratory Supervisor e-aodd,, Date: tar Date: 001 Count cn Comments: Fin BYav------ee.o...moe... * PASSED: 2.87% Reduction * Work Order: 773726/77389 MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 21 25 23 24 22 25 23 22 24 25 22 23 Adult (L)ive (D)ead L Effluent t: 50% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 24 20 23 25 21 25 20 22 23 23 24' 21 Adult (L) ive (D) ead Chronic Test Results Calculated t = 1.031 Tabular t = •2.508 Reduction = 2.87 % Mortality Avg.Reprod. 0.00 Control 23.25 Control 0.00 Treatment 2 22.58 Treatment 2 Control CV' 5.836% % control orgs producing 3rd brood 100% PASS X FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 6.95. 7.02 7.22 7.30 s t a r t 1st 6.93 7.02 6.98 7.06 s t a r t sample 1st e n d 8.6 8.4 8.6 8.4 e n d sample 8.6 8.3 8.6 8.3 2nd sample 6.96 7.04 6.98 7.06 s t e a n r d t 2nd sample 8.6 8.4 8.5 8.3 LC50/Acute Toxicity Test (Mortality expressed as Complete This For Either Test Test Start Date: 12/04/13 Collection (Start) Date Sample 1: 12/02/13 Sample 2: 12/04/13 Sample Type/Duration Sample 1 Sample 2 Sample Grab Comp. Duration X 23.3 hrs X 23.3 hrs D I L U T 1st S A M P 2nd P/F S A M P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) temp. at receipt(°C) 48 196 496 499 0.02 0.04 1.7 3.5 combining replicates) % % % % % % % Concentration Mortality start/end LC50 = 95t Confidence Limits Method of Determination Moving Average Probit Spearman Karber _ Other Note: Please Complete This Section Also start/end Control pH Organism Tested: Ceriodaphnia dubia Duration(hrs): High Conc. D.O. Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) 1 Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/19/13 Facility: MOORE CO. WWTP NPDES#: NC0037508 Pipe#: 001 County: MOORE LaY2Qratory Performer Test: R & A LABORATORIES, INC. :, / . gna } re' rat -Or ill Responsible Charge X Sim atfre'o' oratory Supervisor * PASSED: 0.36% Reduction * Work Order: 767183/76752 MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 22 25 21 23 21 25 24 22 23 21 25 22 Adult (L)ive (D)ead Effluent %: 50% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 25 24 23 23 21 21 25 21 22 24 23 21 Adult (L) ive (D) ead L Chronic Test Results Calculated t = Tabular t = % Reduction = 0.36 % Mortality Avg.Reprod. 0.00 Control 22.83 Control 0.00 Treatment 2 22.75 Treatment 2 Control CV 6.946% control orgs producing 3rd brood 100% PASS FAIL X Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 6.92 7.00 7.01 7.10 6.95 7.02 6.95 7.03 6.94 7.02 6.94 7.03 s s s t e t e t e a n a n a n ✓ d r d r d t t t 1st sample 1st sample 2nd sample 8.6 8.4 8.6 8.4 8.6 8.4 8.6 8.3 8.6 8.4 8.6 8.3 LC50/Acute Toxicity Test• (Mortality expressed as % Complete This For Either Test Test Start Date: 09/11/13 Collection (Start) Date Sample 1: 09/09/13 Sample 2: 09/12/13 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D. I S S Sample 1 X 24.1 hrs L A A U M M Sample 2 X 23 hrs T P P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 48 193 462 482 0.04 0.06 1.4 3.2 combining replicates) % % % % % % . % % Concentration Mortality LC50 = 95% Confidence Limits Method of Determination Moving Average _ Probit _ Spearman Karber _ Other Note: Please Complete This Section Also start/end start/end Control High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 06/13/13. Facility: MOORE CO. WWTP NPDES#: NC0037508 Pipe#: 001 County: MOORE Laboratory Performing/Testy R & A LABORATORIES, INC. Comments: Final Effluent \Signa're- r=0• rator in,jRespons Sig at e'er :•oratory Supervisor * PASSED: 1.77% Reduction * Work Order: 759440/75975 MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 25 22 24 25 23 21 25 22 23 24 25 24 Adult (L) ive (D) ead L L Effluent a: 50% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 .# Young Produced 23 25 21 25 23 24 22 23 24 21 22 25 Adult (L) ive (D) ead Chronic Test Results Calculated t = 0.717 Tabular t = 2.508 Reduction = 1.77 's Mortality Avg.Reprod. 0.00 Control 23.58 Control 0.00 Treatment 2 23.17 Treatment 2 Control CV 5.847% control orgs producing 3rd brood 1000 PASS FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 6.94 7.02 7.16 7.24 t e a n ✓ d t 1st sample 8.6 8.4 8.6 8.4 6.95 7.04 6.97 7.06 6.96 7.03 6.98 7.07 s s t e t e a n a n ✓ d r d t t 1st sample 2nd sample 8.6 8.3 8.6 8.3 8.5 8.2 8.5 8 •. 2 LC50/Acute Toxicity Test (Mortality expressed as %., combining replicates Complete This For Either Test Test Start Date: 06/05/13 Collection (Start) Date Sample 1: 06/03/13 Sample 2: 06/06/13 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X 23.1 hrs L A A U M M Sample 2 X 23.8 hrs T P P Hardness(mg/1) Spec. Cond.(Amhos) Chlorine(mg/1) Sample temp. at receipt(°C) 48 189 484 426 0.07 0.03 2.0 0.7 96 O 0 96 0 0 0 96 96 Concentration Mortality LC50 = 95% Confidence Limits • -- o Method of Determination Moving Average Probit Spearman Karber _ Other Note: Please Complete This Section Also start/end start/end Control High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/14/13 Facility: MOORE CO. WWTP NPDES#: NC0037508 Pipe#: 001 County: MOORE Laborato y PerforRing:.'Test: R & A LABORATORIES, INC. f r f" , '-g g " u,r �O er� in Responsible Charge x a oratory Supervisor Comments: Final Effluent * PASSED: 0.37% Reduction * Work Order: 752501/75279 MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 23 21 24 22 22 21 25 23 22 24 25 21 Adult (L) ive (D) ead L Effluent %: 50% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 .10 11 12 # Young Produced 24 23 21 25 23 23 21 21 24 23 21 23 Adult (L)ive (D)ead L L, L Chronic Test Results Calculated t = 0.143 Tabular t = 2.508 % Reduction = 0.37 % Mortality Avg.Reprod. 0.00 Control 22.75 Control 0.00 Treatment 2 22.67 Treatment 2 Control CV 6.526% control orgs producing 3rd brood 100 % PASS FAIL X Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 6.93 7.02 7.33 7.40 s t e a n ✓ d t 1st sample 8.6 8.4 8.5 8.4 6.96 7.04 7.05 7.13 s t e a n ✓ d t 1st sample 2nd sample 6.94 7.03 7.04 7.12 8.5 8.2 8.5 8.2 s t a r t e n d 8.5 8.3 8.5 8.3 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Complete This For Either Test Test Start Date: 03/06/13 Collection (Start) Date Sample 1: 03/04/13 Sample 2: 03/07/13 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X 24 hrs L A .A U M M Sample 2 X 22.8 hrs T P P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 48 198 506 480 0.06 0.01 0.5 0.7 % % % % % % % Concentration Mortality LC50 = 95% Confidence Limits Method of Determination Moving Average Probit Spearman Karber _ Other start/end Note: Please Complete This Section Also start/end Control High r.,,, n • pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/13/12 Facility: MOORE CO. WWTP NPDES#: NC0037508 Pipe#: 0017.0 Laboratory Performing Test: R & A LABORATORIES, ure f Op or Re ponsible Charge X S: natire o:/ boratory Supervisor INC. Torgu' Comments: Fin telliW 2012 v BY: ........... PASSED: -0.37% Reduction * Work Order: 745958/74629 MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 21 23 22 21 23 24 21 25 24 22 25 21 Adult (L)ive (D)ead L L Effluent %: 50% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 9 10 11 12 # Young Produced 24 23 21 24 24 22 21 22 24 21 24 23 Adult (L)ive (D)ead Chronic Test Results Calculated t = -0.143 Tabular t = 2.508 % Reduction = -0.37 % Mortality Avg.Reprod. 0.00 Control 22.67 Control 0.00 Treatment 2 22.75 Treatment 2 Control CV 6.869% % control orgs producing 3rd brood 100% PASS FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 6.94 7.02 7.25 7.33 s t e a n ✓ d t 1st sample 8.6 8.4 8.6 8.4 1st sample 7.01 7.08 6.99 7.06 s t a r t 1st 2nd sample 6.98 7.05 6.98 7.06 s e t n a d r t sample 2nd sample 8:6 8.3 8.6 8.3 e n d 8.6 8.4 8.6 8.3 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Complete This For Either Test Test Start Date: 12/05/12 Collection (Start) Date Sample 1: 12/03/12 Sample 2: 12/06/12 Sample Type/Duration Sample 1 Sample 2 Grab Comp. Duration X 23.3 hrs X 23.4 hrs D I L -U T 1st S A M P 2nd P/F S A M P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 48 207 532 501 0.03 �.01 2:4 2.1 % % Concentration Mortality start/end LC50 = 95% Confidence Limits % - o Method of Determination Moving Average Probit _ Spearman Karber _ Other Note: Please Complete This Section Also Control start/end pH Organism Tested: Ceriodaphnia dubia Duration (hrs) : High Conc. D.O. Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) A d 0)* Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Facility: MOORE CO. WWTP Cl/ECITC117gUril Date Dv2110 . NPDES#: NC0037508 Pipe#: 001 County: MOORE BY:...............omooe Laboratory Performin Test: R & A LABORATORIES, INC. (e._ O % / Sign�lue ; ��era 6r i�RespCharge eoaboratory Supervisor Comments: Final Effluent * PASSED: -0.72% Reduction * Work Order: 739899/74020 MAIL ORIGINAL TO: Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 24 23 22 24 21 25 22 25 24 23 23 21 Adult (L)ive (D)ead L Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 22 24 24 22 23 25 24 21 23 23 24 24 Adult (L)ive (D)ead Chronic Test Results Calculated t = -0.323 Tabular t = 2.508 % Reduction = -0.72 % Mortality Avg.Reprod. 0.00 Control 23.08 Control 0.00 Treatment 2 23.25 Treatment 2 Control CV 5.974% % control orgs producing 3rd brood. 100% PASS FAIL Check One pH. Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 6.93 7.01 7.27 7.34 6.93 7.02 7.28 7.37 6.94 7.02 7.30 7.38 s s s t e t e t a n a n a ✓ d r d r t t t 1st sample 1st sample 2nd sample 8.6 8.4 8.6 8.4 8.6 8.3 8.6 8.3 e n d 8.6 8.4 8.6 8.3 LC50/Acute Toxicity Test (Mortality expressed as Complete This For Either Test Test Start Date: 09/12/12 Collection (Start) Date Sample 1: 09/10/12 Sample 2: 09/12/12 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X 22.8 hrs L A A U M M Sample 2 X 24 hrs T P P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 48 194. 442 431 0.03 0.04 1.7 0.8 combining replicates) Concentration Mortality LC50 = 95% Confidence Limits Method of Determination Moving Average Probit Spearman Karber Other Note: Please Complete This Section Also start/end start/end Control High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Da e AiA3%4 )2 Facility: MOORE CO. WWTP NPDES#: N00037508 Pipe#: Laboratory` Performing Test:_R & A LABORATORIES, INC. - ! i f / / Si atu •' Operator in Regponss.ble Charge X gn t re ►f' Laboratory Supervisor 001 Cotetyr,; g oeeve_evo Comments: Final Effluent * PASSED: 0.75% Reduction * Work Order: 734059/73434 MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 22 20 28 20 24 23 21 19 24 20 24 23 Adult (L) ive (D) ead L• Effluent %: 50% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 23 23 21 20 23 23 22 24 20 23 23 21 Adult (L)ive (D)ead Chronic Test Results Calculated t = 0.201 Tabular t = 2.508 % Reduction = 0.75 % Mortality Avg.Reprod. 0.00 Control 22.33 Control 0.00 Treatment 2 22.17 Treatment 2 Control CV 11.349% % control orgs producing 3rd brood 1000 PASS FAIL Check One pH Control Treatment 2 D.O. .Control Treatment 2 1st sample 1st sample 2nd sample 6.96 7.04 6.92 7.01 s t a r t 1st 6.94 7.04 6.83 6.92 s e t e n a n d r d t sample 1st sample 8.5 8.3 8.5 8.3 8.6 8.1 8.6 8.2 6.99 7.16 7.08 7.37 s t a r t 2nd sample e n d 8.5 8.0 8.1 8.1 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Complete This For Either Test Test Start Date: 06/20/12 Collection (Start) Date Sample 1: 06/18/12 Sample 2: 06/20/12 Sample Type/Duration Sample 1 Sample 2 Grab Comp. Duration X 23.8 hrs X 23.5 hrs D I L U T 1st S A M P 2nd P/F s A M P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 117 194 479 544 0.04 0.04 1.5 2.9 Concentration Mortality LC50 = 95% Confidence Limits Method of Determination Moving Average _ Probit - Spearman Karber _ Other start/end Note: Please Complete This Section Also Control start/end pH Organism Tested: Ceriodaphnia dubia Duration(hrs): High Conc. D.O. Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Dattutm e/� U MOORE CO. WWTP NPDES#: NC0037508 Pipe#: 001 Count iL r . Fa cility: Laboratory Performing Test: R & A LABORATORIES, INC. ri pe atoi n Responsible Charge na e o Laboratory Supervisor Comments: Final Eff.ynt * PASSED: 1.09% Reduction * Work Order: 726029/72632 MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 23 22 24 21 25 21 22 25 21 24 24 22 Adult (L)ive (D)ead L L L Effluent 50% TREATMENT 2 ORGANISMS 1 2 - 3 4 5 6 7 8 9 10 11 12 # Young Produced 23 22 24 21 22 22 23 21 22 24 25 22 Adult (L)ive (D)ead Chronic Test Results Calculated t = 0.440 Tabular t = 2.508 % Reduction = 1.09 Mortality Avg.Reprod. 0.00 Control 22.83 Control 0.00 Treatment 2 22.58 Treatment 2 Control CV 6.690% % control orgs producing 3rd brood 100% PASS . FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 6.94 7.03 6.88 6.96 6.93 7.03 6.95 7.04 6.94 7.02 6.96 7.05 s s s t e t e t e a n a n a n ✓ d r d r d t t t 1st sample 1st sample 2nd sample 8.6 8.4 8.6 8.3 8.5 8.2 8.5 8.2 8.6 8.4 8.6 8.4 LC50/Acute Toxicity Test (Mortality expressed Complete This For Either Test Test Start Date: 03/07/12 Collection (Start) Date Sample 1: 03/05/12 Sample 2: 03/07/12 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X 21.6 hrs L A A U M M Sample 2 X 24.2 hrs T P P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 48 182 377 486 0.03 0.03 2.9 3.4 as %, combining replicates) % % % % % % 96 % % % % 96 % Concentration Mortality LC50 = 95% Confidence Limits Method of Determination Moving Average Probit Spearman Karber - Other Note: Please Complete This Section Also start/end start/end Control High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Effl▪ uent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/15/11 Facility: MOORE CO. WWTP Laboratory Performing Test: R & A LABORATORIES, INC. Sign-`0 r�n0_it�r_2i}esponsible Charge X S NPDES#: NC0037508 Pipe#: 001 County: MOORE natu4re`o%Laboratory Supervisor Comments: Final Effluent * PASSED: 1.80% Reduction * Work Order: 719437/71979 PY North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test -:CONTROL ORGANISMS MAIL ORIGINAL TO: Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 3 4 5 6 7 8 9 10 11 12 # Young Produced 24 21 24 22 22 25 23 24 21 24 25 23 Adult (L)ive (D)ead L L Effluent %: 50% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 21 25 24 22 24 21 22 22 25 22 24 21 Adult (L)ive (D)ead Chronic Test Results Calculated t = 0.692 Tabular t = 2.508 Reduction = 1.-80 % Mortality Avg.Reprod. 0.00 Control 23.17 Control 0:00 Treatment 2 22.75 Treatment 2 Control CV 6.058% % control orgs producing 3rd brood 100% PASS FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 6.93 7.01 6.99 7.08 6.94 7.03 7.03 7.12 s s t e t a n a ✓ d r t t 1st sample 1st 8.6 8.4 8.5 8.3 6.6 8.5 sample 8.3 8.2 6.92 7.01 7.02 7.10 s e t e n a n d r d t 2nd sample 8.5 8.3 6.4 8.2 LC50/Acute Toxicity. Test (Mortality expressed as % combining replicates Complete This For Either Test Test Start Date: 12/07/11 Collection (Start) Date Sample 1: 12/05/11 Sample 2: 12/07/11 d Sample Type/Duration 1st 2n2nP/d Grab Comp. Duration D I S S Sample 1 X 23.8 hrs L AU M M Sample 2 X 23.6 hrs T P P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 48 182 350 513 0.02 0.04 0.8 2.3 96 % % 96 96 96 % 96 % % Concentration Mortality LC50 = 95% Confidence Limits o Method of Determination Moving Average _ Probit Spearman Karber - Other Note: Please Complete This Section Also start/end start/end Control High Conc. pH D.O. organism Tested: Ceriodaphnia dubia Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Duration(hrs): Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/22/11 Facility: MOORE CO. WWTP NPDES# Laboratory. Performing Test: R & A LABORATO Si= r�Atre , ng'at Laboratory Supervisor as . ij:7508 Pipe#: 001 County: MOORE Comments: Final Effluent * PASSED: 1.82% Reduction.* Work Order: 712295/71260 MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 1621 Mail Service Ctr Raleigh, North Carolina 27699-1621 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 23 24 21 25 22 23 22 23 25 21 24 22 Adult (L)ive (D)ead L Effluent %: 50% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 21 25 24 22 22 24 23 23 21 22 21 22 Adult (L)ive (D)ead L Chronic Test Results Calculated t = 0.758 Tabular t = 2.508 % Reduction = 1.82 % Mortality Avg.Reprod. 0.00 Control 22.92 Control 0.00 Treatment 2 22.50 Treatment 2 Control CV 6:017% control orgs producing 3rd brood 100% PASS FAIL Check One 1st sample pH Control Treatment 2 D.O. Control Treatment 2 6.94 7.01 6.87 6.94 1st sample 2nd sample 6.93 7.03 7.01 7.10 6.93 7.01 7.02 7.10 s s s t e t e t e a n a n a n ✓ d •r d r d t t t 1st sample 1st sample 2nd sample 8.6 8.4 8.5 8.3 8.6 8.3 8.5 8.2 8.5 8.3 8.5 8.3 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Complete This For Either. Test Test Start Date: 09/14/11 Collection (Start) Date Sample 1: 09/12/11 Sample 2: 09/14/11 Sample Type/Duration 2nd 1st P/F Grab Comp Duration D I S S Sample 1 X 23.5 hrs L A A U M M Sample 2 X 22.5 hrs T P P Hardness(mg/1) Spec. Cond.(Amhos) Chlorine(mg/1) Sample temp. at receipt(°C) 48 182 368 370 0.04 0.08 3.6 4.0 96 96 96 % 96 % % % % 9-6 96 96 Concentration Mortality LC50 = 95% Confidence Limits Method of Determination Moving Average- Probit Spearman Karber - Other Note: Please Complete This Section Also start/end start/end Control High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) ir Effluent Toxicity Report Form - Chronic Pass/Fail an cut 50 : 06/23/11 Facility: MOORE CO. WPCP NPDES#: NC0037508 Pipe#: County: MOORE Laboratory Performing Test: MERITECH LABS, INC. Si•natur_ O,• t•`:�;5rs ons Signature of Laboratory Supervisor PASSED: 16.83% Reduction Comments: Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Environmental Sciences Branch Div. of Water. Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 CONTROL ORGANISMS 1 .2 3 4 5 6 7 8 9 10 11 12 # Young Produced 14 18 16 16 17. 18 15 21 22 16 18 17 Adult (L)ive (D)ead Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3- 4 5 6 7. 8 9 10 11 12 # Young Produced 15 7 17 16 14 10 19 17 18 16 5 19 Adult (L)ive (D)ead L Chronic Test Results Calculated t = 1.949 Tabular t = 2.508 Reduction = 16.83 % Mortality Avg.Reprod. 0.00 Control 17.33 Control 0.00 Treatment 2 14.42 Treatment 2 Control CV 13.323% % control orgs producing 3rd brood 100% PASS FAIL x Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 8.25 8.08 8.08 8.18 s t a r t 1st sample e n d 7.67 7.54 7.83. 7.47 1st sample 2nd sample 8.22 8.08 8.07 8.24 8.21 8.14 7.99 8.16 s s t e t e a n a n ✓ d r d t t 1st sample 2nd sample 7.40 7.29 7.35 7.31 7.40 7.30 7.56 7.19 LC50/Acute Toxicity Test (Mortality expressed as % combining replicates Complete This For Either Test Test Start Date: 06/15/11 Collection (Start) Date Sample 1: 06/13/11 Sample 2: 06/15/11 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X 22 hrs L A A U M M Sample 2 X 24.6 hrs T P P Hardness(mg/1) Spec. Cond.(pmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 46 182 439 492 <0.1 <0.1 1.3 0.7 % % % % % % % % % % 96 Concentration Mortality LC50 = 95% Confidence Limits %-- a Method of Determination Moving Average Probit Spearman Karber _ Other Note: Please Complete This Section Also start/end . start/end Control High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and A : 04/01/11 Facility: MOORE CO. WPCP NPDES#: NC0037508 Pipe#: Laboratory Performing Test MERI CH LABS, INC. Signature o 0le Charge X•"r ,s,:_ wf Signature of Laboratory Supervisor Comments: County: MOORE (71'I rl r_+e-.--1e-ac7nrrz% III� \!1 kPP (1 0 rzn rt .tBi . U V * PASSED: 7BVI_$educLioz-b -*--- Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 Environmental Sciences Branch Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 18 21 20 24 24 21 22 24 23 25 25 25 Adult (L) ive (D) ead L Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 22 20 18 20 22 25 22 19 15 24 27 18 Adult (L) ive (D) ead L Chronic Test Results Calculated t = 1.425 Tabular t = 2.508 % Reduction = 7.35 Mortality Avg.Reprod. 0.00 Control 22.67 Control 0.00 Treatment 2 21.00 Treatment 2 Control CV 10.013% % control orgs producing 3rd brood 100% PASS FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 8.20 8.13 7.91 8.06 s t e a n ✓ d t 1st sample 7.64 7.54 8.01 7.30 8.16 8.10 7.98 8.02 s t e a n ✓ d t 1st sample 7.74 7.48 7.80 7.40 2nd sample 8.21 7.97 7.97 8.08 s t a r t 2nd sample e n d 7.60 7.44 7.76 7.40 LC50/Acute Toxicity Test Complete This For Either Test Test Start Date: 03/23/11 Collection (Start) Date Sample 1: 03/21/11 Sample 2: 03/23/11 Sample Type/Duration Sample 1 Sample 2 Grab Comp. Duration X 23 hrs X 24.7 hrs D I L U T 1st S A M P 2nd P/F S A M P Hardness(mg/1) Spec. Cond.(pmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 44 180 432 436 <0.1 <0.1 0.5 0.5 (Mortality expressed as %, combining replicates) % % % % % % % % % % Concentration Mortality LC50 = 95% Confidence Limits Method of Determination Moving Average Probit Spearman Karber- _ Other start/end Note: Please Complete This Section Also start/end Control High- rnnr pH Organism Tested: Ceriodaphnia dubia Duration(hrs): D.O. Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver.. 4.41) 1M1, - Effluent Toxicity Report Form - Chronic ss;/Fa�lS,-• nd`l�cute LC50 , u,a.e r tr7 ,s •, r =- rm LL iw1?2 .2'2=/ 10 EJ (t 6 Facility: MOORE COUNTY NPDES#: NC0037508 Pipe#: 001 Coungy: MOORE �J 'I o-e.o-eomevo_--o--o Labor ryPig/formingTest: !' RITECH, INC. Signatu e o Ope -tor in syonsible Carge 7,7 X Signature of Laboratory Supervisor, Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Comments: dilution water batch number 847 and 848 used. * PASSED: -18.31% Reduction * Environmental Sciences Branch Div. of Water Quality NC DENR t 1621 Mail Service Center Raleigh, NC 27699-1621 445 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 20 27 25 27 22 28 27 26 11 24 24 23 Adult (L)ive (D)ead L Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 29 27 29 30 30 23 30 28 27 28 26 29 Adult (L) ive (D) ead Chronic Test Results Calculated t = Tabular t = % Reduction = -18.31 gEMENMETVEIET % Mortality Avg.Reprod. 0.00 Control 23.67 Control 0.00 Treatment 2 28.00 Treatment 2 Control CV 19.599% % control orgs producing 3rd brood 91.7% PASS FAIL Check One • pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 8.11 8.02 7.8.8 7.92 8.17 7.88 7.83 7.81 8.03 8.09 7.92 7.94 s s s t e t e t a n a n a ✓ d r d r t t t 1st sample 1st sample 2nd sample 7.65 7.58 7.64 7.50 7.67 7.54 7.87 7.74 e n d 7.85 7.42 7.89 7.40 - ;�.G 1•^ (i".v -T:y'S +ZP " fF:h::l',�1)}° t] Tn>`s'i. {'v.'t1,. ;. . ly+. (u Lri ; s MP[1.k i:; ICS1I...: LC50/Acute Toxicity Test (Mortality expressed as % combining replicates Complete This For Either Test Test Start Date: 12/15/10 Collection (Start) Date Sample 1: 12/13/10 Sample 2: 12/16/10 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X 24 hrs L A A U M M Sample 2 X 23.3 hrs T P P Hardness(mg/1) Spec. Cond.(pmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 42 180 460 472 <0.1 <0.1 0.6 0.3 Concentration Mortality LC50 = % 95% Confidence Limits o Method of Determination Moving Average _ Probit Spearman Karber _ Other start/end Note: Please Complete This Section Also start/end Control High r.,,,,,, pH Organism Tested: Ceriodaphnia dubia Duration(hrs): • D.O. Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Facility Effluent Aquatic T ' E LabRrato-Perforrrying Tests �t= t " t (j) r `� LJ V Phase El Chronic Cer!odar hnia NPDES#: NC )0374 0"d" Pipe# oci County Signature of Lab Supervisor Sample Information Collection Start Date Grab Composite (Duration) Hardness(mg/I Spec.Cond.(i.lmhos/c Chlorine(mg/I Sample temp. at receip Control Effluent% Effluent% Effluent% L1I Effluent% Effluent% (op 1 # Young Organism# 2 3 4 5 6 7 8 9 10 11 12 mean LL V 2010 v J. (t!\c,,}gY:o.®. ee_ Comments Test Information* Start Date HH/34o Start End Date ft44/iD Renews Renew2 Start Time / tpp- Start End Time Renews Renew Treatment pH Initial pH Final D.O. Initial D.O. Final Temp. Initial Temp. Final °Id '7.519 7, al 7.1 1t e} r Control 7.,47 'P Control tYt 797 Control %.[if) 7eC1 24.1 7,13 7Le r�Ct! p7` ,. r 20 Adult (L)ive (D)ead # Young Adult (L)ive (D)ead, L L- "lam L_ 1 3 4 L-- LI L 7 L- 1211 L- L 9 10 11 12 L.y-- ;3 L< Mean # Young 1 )- it-- L. l_._-- L— U-- ,. �.- ^ __ 1.___ %Red .T., s 6 #Young p V )1 2.4- ; ?..) .2.1 0 id, 2.,, CI %Red E3 Adult (L)ive (D)ead t— L__3 i__- L.- L " 1..-- L.— L L # Young Adult (L)ive (D)ead # Young Adult (L)ive (D)ead 1 2 f.1 3 L /34 % Red 7 1 fc� 2 3 4 5 6 7 8 9 10 Mean L. .D, f-3 �3 1 1-1 L. Mean Red iL. 7. 7.'7 7 7.is Li a 7.71 -1(4 --33 •ify Chronic Test Results Final Control Mortality ° L) % Control 3rd Brood ei Control Repro CV Cq 48 Hour Mortality Control IWC of /.f of /6'/I Significant? Final Mortality S' %I Reproduction Analysis: d� Repro. L OEC= %; NOEC= I / % Method: Normal Distrib? v Method: Statistic: /1.'7 Critical: / L- 5 Equal Variances? / 6 Method: Statistic: le .`t Critical:_ Non -Parametric Analysis (if applicable): Methodk7g Effluent d/e Rank'Sum Critical Sum 7`a.Z 75� / IOC ft- Overall Analysis: Result = PASS/FAIL or r Test LOEC= ¶- %; NOEC= / e/a t: Chronic Value= ,` �jg` MAIL TO: ATT: Environmental Sciences Branch Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, N.C. 27699-1621 *Should use highest test concentration or highest concentration with D.O. >5.0 mg/I t% Reduction from Control Reproduction Mean DWQ form AT-3 (8/91) Rev. 11/95 Effluent Aquatic Toxicity Report Form/Phase. II Chronic' i4 a Facility 11 �41 1 . ! -v Lt: r+mot Laboratory Performing Tex '.t1 `'1-c.1- 1'\e X ' ,,.� i' 1/4 Signature of Lab Supervisor gnature of O.R.C. NPDES#: NC CO,V1568 Pipe# WI County tuk c!i' Comments Wo..4- 3'- • Sample Information Sample 1 Sample 2 Control Collection Start Date. . Grab Composite (Duration) A % 23.E Hardness(mg/I Spec.Cond.(pmhos/c .._41. : - :. 50 4o 4c Chlorine(mg/I C°. $ t O. ! Sample temp. at receipt 0, y, °C (}, 5 °C Control Effluent% Effluent% .20.5 1 #YoUng Test Information* Treatment pH Initial pH Final D.O. Initial D.O. Final Temp. Initial Temp. Final Start Date End Date e E9/fit Start Time et 54:4. End Time 41:t5 Start Renewl Renew2 Start Renewl Renew2 IUD i007. Control Control Control 7. E. ✓ r 5 'C, 9 8,25 6:/6 '73E r7. f'7 8.83 21.2+ 24-4 '1. 54 25.t5 /1. 51 /1.Ai5 4 11.66 1. 2.4.5 103 25,6 24.2 25.1 "5.4 25. *1 Organism# 2 3 4 5 6 7 8 9 10 11 12 �I 14- 24 Jj Adult (L)ive (D)ead # Young L L L L L L. L L L Adult (L)ive (D)ead # Young Adult (L)ive (D)ead 1 2(6 2 24 L 1 2 21 L. L 3 L 4 25 L Mean r. Chronic Test Results Final Control Mortality % % Control 3rd Brooc Control Repro CV ' 60 5 6 7 8 9 10 11 12 Mean L L 3 4 5 6 25 L L 24 L ZS L 25 L L 2 L 7 8 9- 10 phi L L Ji L 1 L Mean 41,11 %Red Mean. Effluent% # Young, 1 1 L .., — " . — Z)_, �"'1,:. 41 (L)ive (D)ead L L L_ L L L L- L L ,L %Red it Effluent% #Young 92_ 24 1`i 1 z4.J i 2() E. 21-1 2✓ Adult (L)ive (D)ead L L 3 L !3 -. L L 1- L % t - Effluent% 100 # Young Adult (L) ive - (D)ead 1 19 L 2 2.5 L 3 28 L 4 25 L 5 25 L 6 8 L L Mean tio %Red 48 Hour Mortality Control IWC If of Significant? Final Mortality Si % Reproduction Analysis: Repro. LOEC=>/I = %; NOEC=11:D % Method: Normal d Distrib? :I Method:�ccr'v Statistic:1.f •2 Critical: 6: i Equal Variances? iti MethodAQickhli Statistic: ?'` • ` Critical: i.< Non-Parametric.Analysis (if applicable Method:t Effluent % Rank Sum EEC Critical Sum f-- :i Overall Analysis: Result PASS/FAPASS/FAR.or cl Test LOEC 00 %; NOEC= v' ' % Chronic Value= ,? fly.?Y % MAIL TO: ATT: Environmental Sciences Branch Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, N.C. 27699-1621 *Should use highest test concentration or highest concentration with D.O. >5.0 mg/I t% Reduction from Control Reproduction Mean DWQ form AT-3 (8/91) Rev. 11/95 Effluent Ai is tic#,'I' Ile urt\Ph .II Chronic Ceripodaphnia 10/27/10 Facility Moore County P Labor 1y rformin X Sihddtur•'of O.R. Research X NPDES#NC 0037508 7a bs c. tiatur� u perviso r Pipe# 001 County Moore Comments: Final Effluent 686662/687083 Sample Information Sample 1 Sample 2 Control Collection Start Date 10/18/10 10/21/10 'rR `fs Grab Reinai..g.. Composite rr (Duration) 24 hrs 23.9 hrs. ITS r . T;;,,, .' Hardness (mg/1) r' . a � ! .-,: 48 Spec.Cond. (umhos/cm) 414 440 182 Chlorine (mg/L) 0.06 0.03 ..iA';r 4 '° .,, 'tl - ns:. Sample temp. at receipt 2.9°C 2.4°C r.WW;;;::'' Control Effluent % 110.25 Effluent % 20.5 Effluent % 41 Effluent % 82 Effluent % 100 Organism# 2 3 4 5 6 7 8 Test Information* Start Date 10/20/10 • End Date 10 27/10 Start Time 14:34 PM End Time 9:37 AM Treatment pH Initial pH Final D.O. Initial D.O. Final Temp. Initial Temp. Final Start Renew 1 _ Renew 2 Start Renew 1 s Renew 2 100% 100.0% 100.0% Control Control Control 7.10 7.11 7.14 6.92 6.94 6.95 7.19 7.20 7.22 7.00 7.03 7.03 8.3 8.4 8.4 8.6 8.6 8.6 8.1 8.1 8.1 8.3 8.3 8.4 24.6 24.8 24.9 24.2 . 24.4 24.5 25.0 25.0 24.9 25.0 25.0 24.9 9 10 11 '12 Mean # Young 23 24 22 24 21 23 22 25 21 25 23.0 Adult . (L)ive (D)ead L L L L L L L L L L o rS f ?j ': 2 3 4 5 6 7 9 10 11 12 Mean # Young 22 25 26 23 21 24 24 21 24 22 23.2 Adult (L)ive (D)ead L L L L L L L L L L % Red t -0.87 2 3 5 6 7 8 9 10 Mean # Young 21 25 21 24 25 21 24 23 23 21 22.8 Adult % Red (L)ive (D)ead L L L L' L L L L L L 0.87 2 3 4 5 6 7 8 9 10 Mean # Young 24 21 25 22 .22 23 22 21 22 23 22.5 Adult % Red (L)ive (D)ead L L L L L L L L L L 2.17 2 3 4 5 6 7 8 9 10 Mean # Young 23 21 20 22 24 20 23 21 20 21 21.5 Adult % Red 6.52 (L)ive (D)ead L L L L L L L L L L 5 6 7 8 9 10 Mean # Young 20 22 19 20 21 22 20 18 19 20 20.1 Adult (L)ive (D)ead L L L L L L L L L L % Red 12.61 Chronic Test Results Final Control Mortality % % Control 3rd Brood Control Repro CV 0 100 6.48 48 Hour Mortality Control IWC 0 of 10 0 of 10 Significant Y Fiinal Mortality Significant % or No Conc. Reproduction Analysis: Repro. LOEC = 100% NOEC = 82 % Method: Dunnett's T-test Normal Distrib? yes Method: Kolmogorov Statistic: 0.726 Critical: 1.035 Equal Variances? yes Method: Bartlett's Statistic: 1.337 Critical: 15.086 Non -Parametric Analysis (if applicable) Method: Effluent% Rank Sum Critical Sum Overall Analysis: Result = PASS\FAIL or TestLOEC= >100 %: NOEC= 100 % Chronic Value= >100 0/0 ATT: Environmental Sciences Branch Div. Of Water Quality MAIL N.C. DENR TO 1621 Mail Service Center Raleigh, NC 27699-1621 * Should use highest test concentration or highest concentration with D.O. >5.0 mg/1 1% Reduction from Control Reproduction Mean Copy DWQ form AT-3 (8/91) Rev. 11/95 ail and Acute LC50 Date: 09/29/10 • i Effluent Toxicity Report F Facility: MOORE COUNTY NPDES#: NC0037508 Pipe*: 001 County: MOORE n c=.1 ra cwn Laborator r Perform ng Zest : MERITECH, INC. nat e of Operator in Responsible ChRrge Signature of Laboratory Supervisor Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS Environmental Sciences Branch Div. of Environmental Management N.C. Dept. of EHNR 4401 Reedy Creek Road Raleigh, North Carolina 27607-6445 3 4 5 6 7 8 9 10 11 12 # Young Produced 20 28 23 24 21 24 26 27 26 24 20 26 Adult (L)ive (D)ead Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 13 22 15 16 18 20 13 24 18 20 23 19 Adult (L)ive (D)ead Chronic Test Results Calculated "t = 4.332 Tabular t = 2.508 % Reduction = 23.53 % Mortality Avg.Reprod. 0.00 Conti.ol 24.08 Control 16.67 Treatment 2 18.42 Treatment 2 Control CV 11.122% % control orgs producing 3rd brood 100% PASS FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 8.00 7.90 7.78 7.86 8.06. 7.91 7.76 7.76 7.89, 7.83 7.66 7.76 s s s t e t e t e a n a n a n ✓ d r d r d t t t 1st sample 1st sample 2nd sample 7.44 7.34 7.42 7.34 7.70 7.35 7.85 7.25 7.59 7.39 7.61 7.39 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Complete This For Either Test Test Start Date: 09/22/10 Collection (Start) Date Sample 1: 09/20/10 Sample 2: 09/23/10.. Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X 23.4 hrs L A A U M M Sample 2 X 23.8 hrs T P P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 40 177 467 490 <0.1 <0.1 0.4 0.8 96. 96 % 96 Concentration Mortality LC50 = .% 95% Confidence Limits % -- Method of Determination Moving.Average - Probit Spearman Karber Other start/end Note: Please Complete This Section Also start/end Control High r,,, pH Organism Tested: Ceriodaphnia dubia Duration(hrs): D.O. Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Effluent Toxicity Report Form - Chronic Pass/Fail Acute / 1 and t LC50 Facility: MOORE COUNTY 1--I , c CC1 C 1 C7 C7 C7 C� Th U LL LI-, L{te:11�0}6/24/100j�� NPDES#: NC0037508 Pipe#: 001 County: 'OR 1�+9� Laboratory Performin est: MERITECH, INC. . X� Sig atur of Opera or in Responsible Charge X l� Signature of Laboratory Supervisor EN: Comments: Dilution Water Batch #813 & 814 Used Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 26 25 28 21 24 27 26 25 26 25 26 27 Adult (L)ive (D)ead Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 23 21 22 16 21 16 20 23 27 20 18 26 Adult (L)ive (D)ead PASSED: 17.32% Reduction * Rmeentall-Se-ienees-E-ranch Div. of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Chronic Test Results Calculated t = 3.939 Tabular t = 2.508 % Reduction = 17.32 145 % Mortality Avg.Reprod. 0.00 Control 25.50 Control 0.00 Treatment 2 21.08 Treatment 2 Control CV 6.995% % control orgs producing 3rd brood 100% PASS FAI Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 8.08 8.02 7.93 8.03 8.10 8.04 7.84 8.00 8.10 8.00 7.94 7.96 s s s t e t e t a n a n a ✓ d r d r t t t 1st sample 1st sample 2nd sample 7.40 7.38 7.45 7.40 7.54 7.30 7.64 7.26 e n d 7.55 7.27 7.56 7.21 LC50/Acute Toxicity Test (Mortality expressed as % combining. replicates Complete This For Either Test Test Start Date: 06/16/10 Collection (Start) Date Sample 1: 06/14/10 Sample 2: 06/17/10 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X 24.1 hrs L A A U M M Sample 2 X 23.4 hrs T P P Hardness(mg/1) Spec. Cond. (p.mhos) Chlorine(mg/1) Sample temp. at receipt(°C) 44 172 442 448 <0.1 <0.1 0.7 2.1 Concentration Mortality LC50 = 95% Confidence Limits Method of Determination Moving Average - Probit _ Spearman Karber _ Other start/end Note: Please Complete This Section Also start/end Control High Onn r+ pH Organism Tested: Ceriodaphnia dubia Duration(hrs): D.O. Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/25/10 Facility: MOORE COUNTY NPDES#: NO0037508 Pipe#: 001 County: MOORE Laboratory Performing ,re r`' : MERITECH, INC. Sign ture Ope sa or in Responsible Char Signature of Laboratory Supevi Work Order: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 Comments: Dilution Water Batch #795 & 796 Used * PASSED: -4.58% Reduction * Environmental Sciences Branch Div. of Water Quality MAIL ORIGINAL TO: ' NC DENR 1621 Mail Service Center Raleigh, N.C. 27699-1621 E45 Chronic Test Results Calculated t = -1.130 Tabular t = 2.508 6 7 8 9 10 11 12 % Reduction = -4.58 # Young Produced 16 22 23 23 22 21 22 21 23- 23 23 23 Adult (L) ive (D) ead L Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 27 23 22 19 20 25 23 21 25 24 24 21 Adult (L) ive (D) ead % Mortality Avg.Reprod. 0.00 Control 21.83 Control. 0.00 Treatment 2 22.83 Treatment 2 Control CV 9.126% % control orgs producing 3rd brood 91.7% PASS FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 7.97 7.80 7.32 7.72 s t a r t 1st 7.87: 7.85 7.51 7.88 a r t sample 1st e n d 7.73 7.88 8.12 7.96 e n d sample 7.80 7.62 8.12 7.52 7.96 7.88 7.68 7.80 s t a r t 2nd sample e d 7.53 7.38 7.72 7.23 LC50/Acute Toxicity Test (Mortality expressed as % combining replidates Complete This For Either Test Test Start Date: 03/17/10 Collection (Start) Date Sample 1: 03/15/10 Sample 2: 03/18/10 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X 24.2 hrs L A A U M M Sample 2 X 23.9 hrs T P P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine (mg/ 1) Sample temp. at receipt(°C) 42 170 398 429 <0.1 <0.1 0.5 0.2 Concentration Mortality LC50 = 95% Confidence Limits Method of Determination Moving Average - Probit Spearman Karber _ Other start/end Note: Please Complete This Section Also start/end Control High rnnr pH Organism Tested: Ceriodaphnia dubia Duration(hrs) : D.O. Copied from DEM form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.32) RESEARCH & ANAIytkCAE LABORATORIES? INCe Analytical/Process Consultations March.26, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer Chemical Analysis for Selected Parameters and Sampling Location (A Moore County WWTP Project, collected 08 March 2013) BY: PPA- I. Miscellaneous Method Detection Effluent Date Parameters Units Number Limit 0308055 Analyzed Analyst °Antimony, Total mg/L 200.7 0.025 BDL. 03/12/13 JC 'Arsenic, Total mg/L 200.7 0.010 BDL' 03/12/13 JC . Beryllium, Total mg/L 200.7 0.001 BDL• 03/12/13 JC • Cadmium, Total mg/L 200.7 0.002 BDL• 03/12/13 JC • Calcium, Total mg/L 200.7 N/A 31.0 • 03/15/13 JC ' Chromium,Total mg/L 200.7 0.005 BDL• 03/12/13 JC • Copper,Total mg/L 218.2 0.002 0.007• - 03/12/13 JC • Lead,Total mg/L 200.7 0.005 BDL• 03/12/13 JC • Nickel,Total mg/L 200.7 0.010 BDL' 03/12/13 JC - Selenium, Total mg/L 200.7 0.010 BDL' 03/12/13 JC • Silver,Total mg/L 200.7 0.005 BDL • 03/12/13 JC •Thallium, Total mg/L 200.7 0.005 BDL• 03/19/13 JC • Zinc, Total mg/L 200.7 0.010 0.062 • 03/12/13 JC —Nitrate (NO-3-N) mg/L SM 4500 NO3 E 0.050 0.710 03/08/13 DW — Nitrite (NO-2-N) mg/L SM 4500 NO2 B 0.010 0.013 03/08/13 DW Dissolved Solids mg/L SM 2540C 5.00 320 03/11/13 YJ • Hardness, Total mg/L SM 2340C 1.00 97.9 • 03/11/13 AP • Total Nitrogen mg/L N/A 1.00 BDL` 03/25/13 AA - TKN mg/L SM4500NH3 F 1.00 BDL• 03/25/13 ZP • NO2+NO3 mg/L SM4500NO3 E 0.050 0.723- 03/08/13 DW • Phosphorus,Total mg/L SM4500 PE 0.050 2.08 • 03/11/13 MS RAL Sample Number Collection Date Collection Time 752809 03/08/13 0845 mg/L = milligrams per Liter = parts per million (ppm) BDL = Below Detection Limit RESEARCh &.ANAtyT9Citi 0 LAbORATORkESP ONCO Analytical/Process Consultations March 26,2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer Chemical Analysis for Selected Parameters and Sampling Location (A Moore County WWTP Project, collected 08 March 2013) I. Miscellaneous Method Detection Effluent Date Parameters Units Number Limit 0308059 Analyzed Analyst Cyanide mg/L SM4500 CN E 0.005 BDL• 03/12/13 YJ RAL Sample Number 752810 Collection Date 03/08/13 Collection Time 0840 mg/L = milligrams per Liter = parts per million (ppm) BDL = Below Detection Limit RESEARCh & ANAEyTkkA[ LAb®RATORIES, Analytical/Process Consultations March 26, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer. Chemical Analysis for Selected Parameters and Sampling Location (A Moore County WWTP Project, collected 08 March 2013) I. Miscellaneous Parameters • Oil & Grease • Phenols RAL Sample Number Collection Date Collection Time BY Method Detection Effluent Date Units Number Limit 0308061 Analyzed . Analyst EPA 1664 EPA 420.1 5.0 6.35' 03/13/13 MS 0.005 BDL' 03/11/13 YJ 752812 03/08/13 0840 mg/L = milligrams per Liter = parts per million (ppm) BDL = Below Detection Limit R ES EARCII . . } NALyTBCAi LAbORATORkkSP I NC, Analytical/Process Consultations Chemical Analysis for Selected Parameters and Water Sample Identified as PPA (A Moore County WPCP Project, collected 08 March 2013) )(. Volatile Organics Quantitation PPA II, Semi -volatile Organics Quantitation PPA EPA Method 624 Limit Method 625 Limit Parameter (m¢/L) (mg/L) Parameter (m2./L) (mp/L) Methylene Chloride 0.010 BQL 4-Chloro-3-methylphenol 0.010 BQL Trichlorofluoromethane 0.010 BQL 2-Chlorophenol 0.010 BQL 1,1-Dichloroethene 0.010 BQL 2,4-Dichlorophenol 0.010 BQL 1,1-Dichloroethane 0.010 BQL 2,4-Dimethylphenol 0.010 BQL Chloroform . 0.010 BQL 2,4-Dinitrophenol 0.050 BQL Carbon Tetrachloride 0.010 BQL 2-Methyl-4,6-dinitrophenol 0.050 BQL 1,2-Dichloropropane 0.010 BQL 2-Nitrophenol 0.010 BQL Trichloroethene 0.010 BQL 4-Nitrophenol 0.050 BQL Dibromochloromethane 0.010 BQL Pentachlorophenol 0.050 BQL 1,1,2-Trichloroethane 0.010 BQL Phenol 0.010 BQL Tetrachloroethee 0.010 BQL 2,4,6-Trichlorophenol 0.010 BQL Chlorobenzene 0.010 BQL Acenaphthene 0.010 BQL Trans-1,2-Dichloroethene 0.010 BQL Acenaphthylene 0.010 BQL 1,2-Dichlorcethane 0.010 BQL Anthracene 0.010 BQL 1,1,1-Trichloroethane 0.010 BQL Benzidine 0.050 BQL Bromodichloromethane 0.010 BQL Benzo(a)anthracene 0.010 BQL Cis-1,3-Dichloropropene 0.010 BQL Benzo(a)pyrene 0.010 BQL Benzene 0.010 BQL Benzo(b)fluoranthene 0.010 BQL Trans-1,3-Dichloropropene 0.010 BQL Benzo(ghi)perylene 0.010 BQL Bromoform 0.010 BQL Benzo(k)fluoranthene 0.010 BQL 1,1,2,2-Tetrachloroethane 0.010 BQL Benzyl butyl phthalate 0.010 BQL Toluene 0.010 BQL Bis(2-chloroethoxy)methane 0.010 BQL Ethyl Benzene 0.010 BQL Bis(2-chloroethyl)ether 0.010 BQL Chloromethane 0.010 BQL Bis(2-chloroisopropyl)ether 0.010 BQL Bromomethane 0.010 BQL Bis(2-ethyl-hexyl)phthalate 0.010 0.013 Vinyl Chloride 0.010 BQL 4-Bromophenyl phenyl ether 0.010 BQL Chloroethane 0.010 BQL 2-Chloronaphthalene 0.010 BQL Total Xylenes 0.010 BQL 4-Chlorophenyl phenyl ether 0.010 BQL Acrolein 0.100 BQL Chrysene 0.010 BQL Acrylonitrile 0.100 BQL Dibenzo(a,h)anthracene 0.010 BQL 2-Chloroethyl vinyl ether 0.010 BQL 1,2-Dichlorobenzene 0.010 BQL 1,3-Dichlorobenzene 0.010 BQL Dilution Factor 1 1,4-Dichlorobenzene 0.010 BQL 3,3-Dichlorobenzidine 0.020 BQL Sample Number 752811 Di-N-Butyl phthalate 0.010 BQL Sample Date 03/08/13 2,4-Dinitrotoluene 0.010 BQL Sample Time (hrs) 0840 2,6-Dinitrotoluene 0.010 BQL Di-N-Octyl phthalate 0.010 BQL Fluoranthene 0.010 BQL Hexachlorobenzene 0.010 BQL Hexachlorobutadiene 0.010 BQL Hexachlorocyclopentadiene 0.010 BQL Hexachloroethane 0.010 BQL Indeno(1,2,3-cd) pyrene 0.010 BQL Isophorone . 0.010 BQL Naphthalene - 0.010 BQL Nitrobenzene 0.010 BQL N-Nitrosodimethylamine 0.010 BQL N-nitrosodi-n-propylamine 0.010 BQL N-Nitrosodiphenylamine 0.010 BQL Phenanthrene 0.010 BQL Pyrene 0.010 BQL 1,2,4-Trichlorobenzene 0.010 BQL Dilution Factor 1 BQL = Below Quantitation Limits mg/L = milligrams per Liter = parts per million (ppm) Sample Number 752809 Sample Date 03/08/13 Sample Time (hrs) 0845 RESEARCIii & ANAlyTic/l LABORATORIES, INC. Analytical/Process Consultations Chemical Analysis for Selected Parameters and Water Sample Identified as PPA (A Moore County WPCP Project, collected 21 June 2012) Quantitation PPA Quantitation PPA III. Miscellaneous Limit IV. Miscellaneous Limit Parameters (mg/L) (mg/L) Parameters (mg/L) (mg/L) Antimony,Total 0.025 BQL Phenols 0.005 BQL Arsenic,Total 0.005 BQL Oil & Grease 5.0 BQL Beryllium,Total 0.0010 BQL Cadmium,Total 0.002 BQL Sample Number 734362 Chronuum,Total 0.005 BQL Sample Date 06/21/12 Copper,Total 0.005 0.017 Sample Time (hrs) 0932 Lead,Total 0.005 0.053 Mercury,Total 0.0002 BQL Nickel,Total 0.005 BQL Quantitation PPA Selenium,Total 0.005 BQL V. Miscellaneous Limit Silver,Total 0.005 BQL Parameters (mg/L) (mg/L) Thallium,Total 0.005 BQL Zinc,Total 0.010 0.089 Cyanide 0.005 BQL NH-3-N 0.100 0.128 Nitrate 0.050 21.5 Nitrite 0.010 0.015 Sample Number . 734360 Total Nitrogen 0.010 24.6 Sample Date 06/21/12 TKN 0.010 3.07 Sample Time (hrs) 0932 Phos,Tot 0.050 3.54 Dissolved Solids 5.0 380 Hardness 1.00 121 Calcium 0.200 47.5 Sample Number 734359 Sample Date 06/21/12 Sample Time (hrs) 0932 RESEARch & ANAlyiicAL LAb®RAT®RIESp INC. Analytical/Process Consultations Chemical Analysis for Selected Parameters and Water Sample Identified as PPA (A Moore County WPCP Project, collected 21 June 2012) I. Volatile Organics Quantitation PPA II, Semi -volatile Organics Quantitation PPA EPA Method 624 Limit Method 625 Limit Parameter (mg/L) (mg/L) Parameter (mg/L) (mg/L) Methylene Chloride 0.010 BQL 4-Chloro-3-rnethylphenol 0.010 BQL Trichlorofluoromethane - 0.010 BQL 2-Chlorophenol 0.010 BQL 1,1-Dichloroethene 0.010 BQL 2,4-Dichlorophenol 0.010 BQL 1,1-Dichloroethane 0.010 BQL 2,4-Dimethylphenol 0.010 BQL Chloroform 0.010 BQL 2,4-Dinitrophenol 0.050 BQL Carbon Tetrachloride 0,010 BQL 2-Methyl-4,6-dinitrophenol 0.050 BQL 1,2-Dichloropropane 0.010 BQL 2-Nitrophenol 0.010 BQL Trichloroethene 0.010 BQL 4-Nitrophenol 0.050 BQL Dibromochloromethane 0.010 BQL Pentachlorophenol 0.050 BQL 1,1,2-Trichloroethane 0.010 BQL Phenol 0.010 BQL Tetrachloroethene 0.010 BQL 2,4,6-Trichlorophenol 0.010 SQL Chlorobenzene 0.010 BQL Acenaphthene 0.010 BQL Trans-1,2-Dicbloroethene 0.010 BQL Acenaphthylene 0.010 BQL 1,2-Dichloroethane 0.010 BQL Antbracene 0.010 BQL 1,1,1-Trichloroethane 0.010 BQL Benzidine 0.050 BQL Bromodichloromethane 0.010 BQL Benzo(a)anthracene 0.010 BQL Cis-1,3-Dichloropropene 0.010 BQL Benzo(a)pyrene 0.010 BQL Benzene 0.010 BQL Benzo(b)fluoranthene 0.010 BQL Trans-1,3-Dichloropropene 0.010 BQL Benzo(ghi)perylene 0.010 BQL Bromoform 0.010 BQL Benzo(k)fluoranthene 0.010 BQL 1,1,2,2-Tetrachloroethane 0.010 BQL Benzyl butyl phthalate 0.010 BQL Toluene 0.010 BQL Bis(2-chloroethoxy)methane 0.010 BQL Ethyl Benzene 0.010 BQL Bis(2-chloroethyl)ether 0.010 BQL Chloromethane 0.010 BQL Bis(2-chloroisopropyl)ether 0.010 BQL Bromomethane 0.010 BQL Bis(2-ethyl-hexyl)phthalate 0.010 BQL Vinyl Chloride 0.010 BQL 4-Bromophenyl phenyl ether 0.010 BQL Chloroethane 0.010 BQL 2-Chloronaphthalene 0.010 BQL Total Xylenes 0.010 BQL 4-Chlorophenyl phenyl ether 0.010 BQL Acrolein 0.100 BQL Cluysene 0.010 BQL Acrylonitrile 0.100 BQL Dibenzo(a,h)anthracene 0.010 BQL 2-Chloroethyl vinyl ether 0.010 BQL 1,2-Dichlorobenzene 0.010 BQL 1,3-Dichlorobenzene 0.010 BQL Dilution Factor 1 1,4-Dichlorobenzene 0.010 BQL 3,3-Dichlorobenzidine . 0.020 BQL Sample Number 734361 Di-N-Butyl phthalate 0.010 BQL Sample Date 06/21/12 2,4-Dinitrotoluene 0.010 BQL Sample Time (hrs) 0932 2,6-Dinitrotoluene 0.010 BQL Di-N-Octylphthalate 0.010 BQL Fluoranthene 0.010 BQL Hexachlorobenzene 0.010 BQL Hexachlorobutadiene . 0.010 BQL Hexachlorocyclopentadiene 0.010 BQL Hexachlorcethane 0.010 BQL Indeno(1,2,3-cd) pyrene 0.010 BQL Isophorone 0.010 BQL Naphthalene 0.010 BQL Nitrobenzene 0.010 BQL N-Nitrosodimethylamine 0.010 BQL N-nitrosodi-n-propylamine 0.010 BQL N-Nitrosodiphenylamine 0.010 BQL Phenanthrene 0.010 BQL Pyrene 0.010 BQL 1,2,4-Tichlorobenzene 0.010 BQL Dilution Factor 1 BQL = Below Quantitation Limits mg/L = milligrams per Liter = parts per million (ppm) Sample Number 734359 Sample Date 06/21/12 Sample Time (hrs) 0932 00 • RESEARCH & ANALy1icAL LAbORATORIES, INC. Analytical/Process Consultaflor>,s Chemical Analysis for Selected Parameters and Water Sample Identified as PPA (A Moore County WPCP Project; collected 15 September 2011)= L Volatile Organics EPA Method 624 Parameter Methylene Chloride 71tichlorofluotometl3ane l,l-DichloroeHxne 1,1-Dicblomethane Chloroform Carbon Tetrachloride 1,2-Dichlompmpane Trichloroethene Dribromochloromethane 1,1,2-Trichloroetl me Temchloroetheae Chlotobeozate Trans-L2-Dichloroerhene 1,2-Did 1oroetbane 1,1,1.-Triddomethme Bromodichlo ourthne Cia-1,3-Diehloraptopeae Benzene Trans-1,3-Dieblomprapene Brom:oh m 1,1,2,2-Tdrachloradhane Toluene Ethyl Benzene chlorometbane Bromomethane Vinyl Chloride Chlotoethane Tout Xyleoes Acrolein Acryloni(rilc 2-Chloroethyl vinyl ether Dilution Factor l- Miscellaneous Parameter Antimony,Total Arsenic,Total Betyllium,ToW Cadnium,Toul Chmmium,Total Copper,Tota1 Lead,Tbml Mercuy,Total • Nickel,Total Seleaium,Total Site ,Total 'Btallium,Tota1 Zine,Total CYlmide Phenols NH-3-N Nmate Nitrite Total Nitrogen TKN NO2+No3 Oil & Grease Pbos,Tot Dissolved Solids Hardness Calcium Sample Number Sample Date Sample Time (lira) Quantitation PPA Limit (MEMO) fmg(LI 0,010 BQL 0.010 BQL 0.010 BQL 0.010 SQL 0.010 BQL 0.010 .BQL 0.010 BQL 0.010 BQL 0.010 SQL 0.010 BQL, 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 SQL 0.010 BQL 0,010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL D.010 BQL 0.010 BQL 0.100 BQL 0.100 BQL 0.010 SQL Ouantitation PPA Limit (ntrJl.� (u (L) 0.025 0.005 0.0010 0.002 0.005 0.005 0.005 0.0002 0.005 0.005 0.005 0.005 0.010 0.005 0.005 0.100 0.050 0.010 0.010 0.010 0.050 5.0 0.050 5.0 1.00 0200 BQL BQL BQL BQL BQL 0.014 BQL SQL 0.006 SQL SQL SQL 0.066 BQL SQL SQL 20.2 SQL 222 2.02 20.2 BQL 139 348 115 90.1 712607 09/15/11 0803 in. Semi -volatile Organics Method 625 btu• der 4-Chloio-3-u hylphenol 2-Chloropbmol 2,4-Dichloropbenol 2,4-Diuethylphenol 2,4-Dinitrophenol 2-Methy1-4,6 dinitrophenol 2-Nitrophenol 4-Niuophmol Peouchlompbenol Phenol 2,4,6-Trich/omphenol Acenaplttbaw Acenaphthylene Aw Benadine Benm(a)anthtecene Bmzo(a)pyrene Beazo(b)flunrmthene Beozo(ghi)paylene Beazo(k)fumanttbare Benzyl butyl phthalate Bis(2-ohloroe0nxyhrethane Bis(2-chlomethyl)ether Bis(2-chloroisopropyl)ether Bis(2-ethythexyl)phtbalate • 443connphrsryl phenyl ether 2-Chlomn hthrde to 4-Chloropheayl phenyl Chr Claysene Dbenzo(a,h)mtbracene 1,2-Dichlombenzeae 1,3-Dichlombenmte 1,4-DichlombaIne 3,3-Dichlorobenudinc Di-N-Butyl phthalate 2,4-Dinitrotolume 2,6-Dinitrotoluene Di-N-Octyl phthalate Flunranthene Hexachkmbmie Hexacblorobuudiene Hetachbtocyclopmtadiene Hexachloroethane Irrdmo(1,2,3-cd) pyrem ):sophorone Naphthalene Nitrobenzene N-Nitrosodimethylamiae N nitrosodi-n-propylaanne N-Nitrosodiphenylamine Phcnant rene Pyreoe 1,2,4-Trichlorobenzene Dilution Factor Sample Number Sample Date Sample Time (hrs) Quantitation PIA Limit fmg/t ' fn+NL1 0.010 BQL 0.010 SQL 0.010 BQL 0.010 , SQL• 0.050 BQL 0.050 BQL 0,010 BQL 0.050 SQL 0.050 SQL 0.010 SQL 0.010 SQL 0.010 BQL 0.010 BQL 0.010 BQL 0.05(1 BQL 0.010 SQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 SQL 0.010 BQL 0.010 BQL 0.010 SQL 0.010 BQL Q010 BQL 0.010 SQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.010 BQL 0.020 SQL 0.010 BQL 0.010 BQL 0.010 SQL 0.010 BQL 0.010 SQL 0.010 BQL 0.010 SQL 0.010 BQL 0.010 BQL 0.010 SQL 0.010 SQL 0.010 SQL 0.010 SQL 0:010 BQL 0.010 BQL 0.010 BQL 0.010 SQL 0.010 BQL 0.010 BQL 712607 09/15/11 0803 BQL = Below Quantitation limits 'AWL = milligrams per Liter = parts pa• mil lion (ppm) Contact: Client: Janna Scherer Moore County WWTP 1094 AddorRoad Aberdeen, NC 28315 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: Revision Date: rw .tee-=wFL r. lam, �V R L CP L B. .. Date Sample Rcvd: 12/14/10 Meritech Work Order # Parameters Antimony, total Arsenic, total Beryllium, total Cadmium, total Calcium, total Chromium, total Copper, total Lead, total Mercury, total Nickel, total Selenium, total Silver, total Thallium, total Zinc, total Hardness, total EPA 625 BNA 12141055 Sample: 1214138 Effluent Composite - 12/13-14/10 Result Analysis Date Reporting Limit Method < 0.025 mg/L ' < 0.010 mg/L < 0.005 mg/L < 0.002 mg/L 32.8 mg/L < 0.005 mg/L 0.007 mg/L < 0.010 mg/L < 0.0002 mg/L < 0.010 mg/L < 0.010 mg/L < 0.005 mg/L < 0.020 mg/L 0.075 mg/L 100 mg eq CaCO3/L Attached 12/22/10 12/22/10 12/22/10 12/22/10 1/5/11 12/22/10 12/22/10 12/22/10 12/15/10 12/22/10 12/22/10 12/22/10 12/22/10 12/22/10 12/30/10 12/21/10 0.025 mg/L 0.010 mg/L 0.005 mg/L 0.002 mg/L 0.100 mg/L 0.005 mg/L 0.002 mg/L 0.010 mg/L 0.0002 mg/L 0.010 mg/L 0.010 mg/L 0.005 mg/L 0.020 mg/L 0.010 mg/L 1 mg eq CaCO3/L EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 245.1 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 SM 2340B Meritech Work Order # 12141056 Parameters Cyanide, total Phenols, total EPA 624 A+A Trip Blank Result < 0.005 mg/L 0.064 mg/L Attached Attached Sample: 1214138 Effluent Grab Analysis Date Reporting Limit 12/16/10 0.005 mg/L 12/22/10 0.010 mg/L 12/20/10 12/20/10 12/14/10 Method EPA 335.4 EPA 420.1 I hereby certify that 1 have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Contact: Janna Scherer Client: Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Report Date: n c—,rwc—,ra7 JI 7711 In Y"66 e it 2011 B Y: Date Sample Rcvd: Meritech Work Order # 12141055 Parameters Antimony, total Arsenic, total Beryllium, total Cadmium, total Calcium, total Chromium, total Copper, total Lead, total Mercury, total Nickel, total Selenium, total Silver, total Thallium, total Zinc, total Hardness, total EPA 625 BNA pP Sample: 1214138 Effluent Composite Result < 0.025 mg/L < 0.010 mg/L < 0.005 mg/L < 0.002 mg/L * mg/L < 0.005 mg/L 0.007 mg/L < 0.010 mg/L < 0.0002 mg/L < 0.010 mg/L < 0.010 mg/L < 0.005 mg/L < 0.020 mg/L 0.075 mg/L 100 mg eq CaCO3/L Attached Analysis Date 12/22/10 12/22/10 12/22/10 12/22/10 12/22/10 12/22/10 12/22/10 12/15/10 12/22/10 12/22/10 • 12/22/10 12/22/10 12/22/10 12/30/10 12/21/10 Reporting Limit 0.025 mg/L 0.010 mg/L 0.005 mg/L 0.002 mg/L 0.100 mg/L 0.005 mg/L 0.002 mg/L 0.010 mg/L 0.0002 mg/L 0.010 mg/L 0.010 mg/L 0.005 mg/L 0.020 mg/L 0.010 mg/L 1 mg eq CaCO3/L 12/13-14/10 Method EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 245.1 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 SM 2340B Meritech Work Order # 12141056 Parameters Cyanide, total Phenols, total EPA 624 A+A Trip Blank Result < 0.005 ing/L 0.064 mg/L Attached Attached Sample 1214138 Effluent Grab Analysis Date 12/16/10 12/22/10 12/20/10 12/20/10 Reporting Limit 0.005 mg/L 0.010 mg/L 12/14/10 Method EPA 335.4 EPA 420.1 * Will forward upon completion. I hereby certify that I have reviewed and approve these data. -2Q,0( Laboratory Representative 642 Tamco. Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Client: Project: Client Sample ID: Sample Collection: Parameter Acenaphthene Acenaphthylene Anthracene - Benzidine Benzo(a)anthracene Benzo(a)pyrene 3,4-Benzofluoranthene .Benzo(k)fluoranthene Benzo(g,h,i)perylene Benzyl butyl phthalate Bis(2-chloroethoxy)methane B is(2-chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-ethylhexyl)phthalate 4-Bromophenyl phenyl ether 2-Chloronaphthalene 4-Chlorophenyl phenyl ether Chrysene Dibenzo(a,h)anthracene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 3,3'-Dichlorobenzidine Diethyl phthalate Dimethyl phthalate Di-n-butyl phthalate 2,4-Dinitrotoluene 2,6-Dinitrotoluene - Di-n-octyl phthalate 1,2-Diphenylhydrazine MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Moore County WWTP PPA Effluent 1214138 12/14/10 Meritech ID#: 12141055 Analysis: 12/21/10 Extraction: 12/14/10 Analyst: MC Dilution Factor: 1 EPA 625 SEMIVOLATILE ORGANICS Result <10 ug/L <10 ug/L <10 ug/L <50 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L < 10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <50 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L Parameter Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene Naphthalene Nitrobenzene N-Nitrosodimethylamine N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine Phenanthrene Pyrene 1,2,4-Trichlorobenzene p-Chloro-m-cresol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 4,6-Dinitro-o-cresol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol I hereby certify that I have reviewed and approve these data. Result <10 ug/L <10 ug/L <10 ug/L <10 ug/L <50 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <50 ug/L <50 ug/L <10 ug/L <50 ug/L <50 ug/L <10 ug/L <10 ug/L Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax Client: Project: Client Sample ID: Sample Collection: MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Moore County WWTP 624 PPA Trip Blank 12/14/10 Meritech ID#: Analysis: Analyst: Dilution Factor: 1 EPA 624 VOLATILE ORGANICS Parameter - Result Benzene < 1.00 ug/L Dichlorobromomethane < 1.00 ug/L Bromoform < 1.00 ug/L Methyl Bromide < 5.00 ug/L Carbon Tetrachloride < 1.00 ug/L Chlorobenzene < 1.00 ug/L Chloroethane < 5.00 ug/L 2-Chloroethyl vinyl ether < 5.00 ug/L Chloroform < 1.00 ug/L Methyl Chloride <5.00 ug/L Chlorodibromomethane < 1.00 ug/L 1,2-Dibromoethane < 1.00 ug/L 1,1-Dichloroethane < 1.00 ug/L 1,2-Dichloroethane < 1.00 ug/L 1,4-Dichlorobenzene < 1.00 ug/L 1,2-Dichlorobenzene < 1.00 ug/L 1,3-Dichlorobenzene < 1.00 ug/L 1,1-Dichloroethylene < 1.00 ug/L trans-1,2-Dichloroethylene < 1.00 ug/L 1,2-Dichloropropane < 1.00 ug/L cis-1,3-Dichloropropylene < 1.00 ug/L trans-1,3-Dichloropropylene < 1.00 ug/L 1.00'' Ethyl benzene. � u ��'-' Methylene chloride • < 1.00 ug/L 1,1,2,2-Tetrachloroethane < 1.00 ug/L Tetrachloroethylene < 1.00 ug/L Toluene < 1.00 ug/L 1,1,1-Trichloroethane < 1.00 ug/L 1,1,2-Trichloroethane < 1.00 ug/L Trichloroethylene < 1.00 ug/L Trichlorofluoromethane < 5.00 ug/L Vinyl chloride < 5.00 ug/L Additional Compounds Acrolein <50.0 ug/L Acrylonitrile <10.0 ug/L I hereby certify that I have reviewed and approve these data. 12141056tb 12/20/10 VWV ge Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax Client: Project: Client Sample ID: Sample Collection: MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Moore County WWTP 624 PPA Effluent 1214152 12/14/10 Meritech ID#: Analysis: Analyst: Dilution Factor: EPA 624 VOLATILE ORGANICS Parameter Result Benzene < 1.00 ug/L Dichlorobromomethane <1.00 ug/L Bromoform <1.00 ug/L Methyl Bromide <5.00 ug/L Carbon Tetrachloride <1.00 ug/L Chlorobenzene < 1.00 ug/L Chloroethane < 5.00 ug/L 2-Chloroethyl vinyl ether < 5.00 ug/L Chloroform < 1.00 ug/L Methyl Chloride < 5.00 ug/L Chlorodibromomethane < 1.00 ug/L 1,2-Dibromoethane <1.00 ug/L 1,1-Dichloroethane < 1.00 ug/L 1,2-Dichloroethane < 1.00 ug/L 1,4-Dichlorobenzene < 1.00 ug/L 1,2-Dichlorobenzene <1.00 ug/L 1,3-Dichlorobenzene < 1.00 ug/L 1,1-Dichloroethylene < 1.00 ug/L trans-1,2-Dichloroethylene < 1.00 ug/L 1,2-Dichloropropane < 1.00 ug/L cis-1,3-Dichloropropylene < 1.00, ug/L trans-1;3-Dichloropropylene < 1.00 ug/L Ethyl benzene < 1.00 ugiL Methylene chloride < 1.00 ug/L 1,1 ,2,2-Tetrachl oroethane < 1.00 ug/L Tetrachloroethylene < 1.00 ug/L Toluene < 1.00 ug/L 1,1,1-Trichloroethane <1.00 ug/L 1,1,2-Trichloroethane <1.00 ug/L Trichloroethylene < 1.00 ug/L Trichlorofluoromethane < 5.00 ug/L Vinyl chloride < 5.00 ug/L Additional Compounds Acrolein Acrylonitrile 1 hereby certify that I have reviewed and approve these data. <50.0 ug/L <10.0 ug/L 12141056 12/20/10 VWV 1 Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax 4• ADDENDUM 1 NPDES PERMIT #NC0037508 REQUEST FOR RENEWAL January 10, 2014 Sludge Management Plan: The Sludge Management Plan for the Moore County Water Pollution Control Plant consists of two items: 1. Disposal of Sludge as compost from 2006 to the end of 2013. Compost ultimately was distributed as a soil amendment. 2. Disposal of Sludge at Anson County Landfill starting December 2013. The Land Application permit (Permit #WQ0018018) was rescinded January 2006. The permit was never used. If you have any questions concerning our Sludge Management Plan, please do not hesitate to contact George Yankay at (910) 281-3146. RESEARCIi ail ANAIyTicAI LAbORATORIES, INC. Analytical/Process Consultations January 22, 2014 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer Low Level Mercury Analysis RAL Low Level Sample Sample Sample Sample Mercury * Identification Number Date Time (ng/L) Upstream 776308 12/31/13 1245 1.27 Field Blank 776309 12/31/13 1247 1.23 * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per Liter < = Less than or below detection limit RESEARCII & ANAIyTICA[ LABORATORIES, INC. Analytical/Process Consultations December 17, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer Sample Identification Upstream Field Blank Low Level Mercury Analysis RAL Sample Sample Number Date 773897 11/21/13 1335 773898 11/21/13 1337 Sample Time ,Low Level Mercury •* (nulL) <0.500 <0.500 BY: o__---- * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per. Liter < = Less than or below detection limit RESEARCH & ANA(yTICAL LAbORATORI'ES, INC. Analytical/Process Consultations November 20, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer 1 SS! 9 di i.) Low Level Mercury Analysis RAL Low Level Sample Sample Sample Sample Mercury Identification Number Date Time (n&L) Upstream 772027 10/31/13 1435 <0.500 Field Blank 772026 10/31/13 1000 0.990 = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per Liter < = Less than or below detection limit RESEARCH & ANALyTi.CA1 LAbORATORIES,_ INC. Analytical/Process Consultations October 21, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer Low Level Mercury. Analysis RAL Low Level Sample Sample Sample Sample Mercury * Identification Number Date . Time (ng/L) Effluent 769511 .09/30/13 1110 . 2.34 Fie1d;B1ank 769512 09/30/13 , 1115 0.700 * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per Liter. < = Less than or below detection limit RESEARCh & ANALyTICAL LABORATORIES, INC. Analytical/Process Consultations September 23, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 283.15 Attention: Janna Scherer Low Level Mercury Analysis •�v. • r.r.ra 2 6 20,13 BY: --- ---- RAT Low Level Sample Sample Sample Sample Mercury Identification Number Date Time (n2/L) Effluent 767177 08/28/13 1508 1.57 Field Blank 767178 08/28/13 1505 <0.500 * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per Liter < = Less than or below detection limit RESEARCk & ANALyTICAL e LABORATORIES, INCe Analytical/Process Consultations August 23, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer AUGimcmawmr-1 la 2 7 2013 LI B Y: Low Level Mercury Analysis RAL Low Level Sample Sample Sample. Sample Mercury * Identification Number Date Time (n2/L) Effluent 764742 07/26/13 1245 1.60 Field Blank 764743 07/26/13 . 1248 1.20 * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per Liter < = Less than or below. detection limit RESEARCI1 & ANALyTicAL LABORATORIES, INC° Analytical/Process Consultations July 24, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer Low Level Mercury Analysis RAL Low Level Sample Sample Sample Sample Mercury * Identification Number Date Time (ns/L) Effluent 762035 06/28/13 1545 2.81 Field Blank 762036 06/28/13 1548 <0.500 * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW, Cert#39705) ng/L = nanograms per Liter < = Less than or below detection limit RESEARCH C ANALyTkAL LAbORATORiES, INC. Analytical/Process Consultations June 14, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer Low Level Mercury Analysis RAT . Low Level Sample Sample Sample Sample Mercury Identification Number Date Time ingLIL Upstream 759449 05/29/13 1425 1.55 Field Blank 759450 05/29/13 1430 <0.500 T = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per Liter < = Less than or below detection limit RESEARCII & ANALyTiCAL LAbORATORIESF INCe Analytical/Process Consultations April 17, 2013 Moore County WWTP 1094 Addor Road. Aberdeen, NC 28315 Attention: Janna Scherer Low Level Mercury Analysis RAL Low Level Sample Sample Sample Sample Mercury * Identification Number Date Time . (u /L) Effluent 754863 03/28/13 1430 1.44 Field Blank 754864 03/28/13 1427 1.00 * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per Liter < = Less than or below detection limit ,����llttifl���• + RESEARCIi & ANAlyTiCAl ,,,.� `.' •••.. LAboI To(t1E5 INC.- °`f° NC#34 = = s sli 1 Analytical/Process Consultations •.oigE�c ' A. -4,11100- April 25, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer Low Level Mercury Analysis RAL Low Level Sample Sample . Sample Sample - Mercury. * Identification Number Date Time (ns/L) Upstream . 752798 02/28/13 1435 1.49 Field Blank 752799 02/28/13 .1430 <0.500 * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW.Cert#39705) ng/L = nanograms per Liter < = -Less than or below detection limit R ESEARCII & ANALYTICAL L.AbORATORiESF INC. �,�,�,��� Analytical/Process Consultations g C METE V `- ' "1 f -..: 7 I V February 11, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer BY:------------- ------ Low Level Mercury Analysis IRAL Low Level Sample Sample Sample Sample Mercury * Identification Number Date Time (na/L) Upstream 748599 01/10/13 1355 0.320 Field Blank 748600 01/10/13 <0.5 * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per Liter < = Less than or below detection limit ossiumieta RESEARCH &. ANALyTICAL _ �� sote.4 -044 $ fU cV LAbORATORIES, INC. ! b o � NC ZSips v Analytical/Process Consultations 4 1 ,y,.•� January 29, 2013 Moore County WWTP 1094 Addor Road Aberdeen, NC 28315 Attention: Janna Scherer Low Level Mercury Analysis RAL Low Level Sample Sample Sample Sample Mercury * Identification Number Date - Time (ng/L) Upstream 748198 12/20/12 1400 <0.5 Field Blank 748199 12/20/12 <0.5 * = Sample analyzed by Summit Environmental Technologies, Inc. (NC WW Cert#39705) ng/L = nanograms per Liter < = Less than or below detection limit i#r