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Home My WebLink AboutNCG030134_DMR_20210409Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted: 04/09/2021 CERTIFICATE OF COVERAGE NO. NCG030134 FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC COUNTY: Buncombe PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS LABORATORY: Pace Analytical Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR SAMPLE PERIOD —Jan-June July -Dec Or X Monthly: March RECEI Th ARGING TO CLASS ❑ ORW ❑ HQW X❑frout ❑ PNA '" ❑Zero -flow ❑Water Supply ❑SA APR 2 6 2021 ❑other CENTRAL FILE a PWR uIECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 - No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches' Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics' Benchmarks - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 Outfall1 03/25/2021 0.8 45.4 6.8 0.0075 <0.005 0.145 <5 N/A Outfall2 03/25/2021 0.8 48.0 6.2 0.0291 <0.005 0.214 <5 N/A Outfall3 03/25/2021 0.8 141 6.3 0.0353 0.0152 0.143 <5 N/A Outfall4 03/25/2021 0.8 2.5 6.2 <0.005 0.005 0.0894 <5 N/A Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. = For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Section 13, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Pr ve do Plan." Name (Print name) 'tle (Print title) Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier z, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. nNo discharge this period?' Outfall No. Rate Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/O Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FORTH E SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES X NO IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert (Asheville Regional Office) Mail an on final copV of this DMR includingall "No Discharge" reports, within 30 days a recei t o the lab results or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I aqx aXare that th e a ignificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee V J J Date Permit Date: 11/1/2018-05/31/2021 11/1/2018 SWU-245, last revised (�IaceAnalytical www.pacelabi.com April 07, 2021 Mr. Jeremy Putnam Thermo Electron Corp. 275 Aiken Road Asheville, NC 28804 RE: Project: March 2021 SW Pace Project No.: 92529821 Dear Mr. Putnam: Pace Analytical Services, LLC 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on March 25, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 f �ceAnalytical www.pacelahs.com Project: March 2021 SW Pace Project No.: 92529821 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification M 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification M 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not 6e reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 2 of 12 11ce Analytical � I www.pacelabs.com Project: March 2021 SW Pace Project No.: 92529821 Lab ID Sample ID 92529821001 1 92529821002 2 92529821003 3 92529821004 4 PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 j8281254-7176 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 1664E CJM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 2540D-2011 ZMC 1 PASI-A EPA 1664B CJM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 254OD-2011 ZMC 1 PASI-A EPA 1664E CJM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 25400-2011 ZMC 1 PASI-A EPA 1664B CJM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 26400-2011 ZMC 1 PASI-A REPORT- OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC. Page 3 of 12 IeAnalytical e www.pacelabs.com ANALYTICAL RESULTS Project: March 2021 SW Pace Project No.: 92529821 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: 1 Lab ID: 92529821001 Collected: 03/25/21 14:15 Received: 03/25/21 15AI Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 04/07/21 11:03 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4A 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper 7.5 ug/L 5.0 1 04/01121 01:49 04/05/21 23:37 7440-50-8 Lead ND ug/L 5.0 1 04/01/2101:49 04105/2123:37 7439-92-1 Zinc 145 ug/L 10.0 1 04/0112101:49 04/05/2123:37 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 26400-2011 Pace Analytical Services - Asheville Total Suspended Solids 45.4 mg/L 3.3 1 03/28/21 11:16 Sample: 2 Lab ID: 92529821002 Collected: 03/25/21 15:00 Received: 03/25/21 15:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg1L 5.0 1 04/07/21 11:03 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper 29.1 ug/L 5.0 1 04/01/2101.49 04/06/2100:00 7440-50-8 Lead ND ug/L 5.0 1 04/01/2101*49 04/06/2100:00 7439-92-1 Zinc 214 ug/L 10.0 1 04/01121 01:49 04/06/2100:00 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Asheville Total Suspended Solids 48.0 mg/L 7.1 1 03/28/21 11:15 Sample: 3 Lab ID: 92529821003 Collected: 03/25/21 15:15 Received: 03/25/21 15:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 04/07/21 11:03 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4A 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper 35.3 ug/L 5.0 1 04/01/2101:49 04106/2100:04 7440-50-8 Lead 15.2 ug/L 5.0 1 04/01121 01:49 04106/2100:04 7439-92-1 Zinc 143 ug/L 10.0 1 04/01/2101:49 04106/2100:04 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/07/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 12 1�;a'ne Analytical www.paeelabs.eom ANALYTICAL RESULTS Project: March 2021 SW Pace Project No.: 92529821 Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Sample: 3 Lab ID: 92529821003 Collected: 03/25/21 15:15 Received: 03/25/21 15:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services -Asheville Total Suspended Solids 141 mg/L 25.0 1 03/28121 11:16 Sample: 4 Parameters Lab ID: 92529821004 Collected: 03/25/21 15:30 Results Units Report Limit DF Received: 03/25/21 15:41 Matrix: Water Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg1L 5.0 1 04/07/21 11:03 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper ND ug1L 5.0 1 04/01121 01:49 04/06/2100:07 7440-50-8 Lead ND ug1L 5.0 1 04/01121 01:49 04/0612100:07 7439-92-1 Zinc 89.4 ug1L 10.0 1 04/01121 01:49 04/06/2100:07 7440.66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services -Asheville Total Suspended Solids ND mg1L 2.6 1 03/28/21 11:16 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/07/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 (—'!1aceAna1j6ca16 www.pacelabs.com QUALITY CONTROL DATA Project: March 2021 SW Pace Project No.: 92529821 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QC Batch: 611861 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92529821001, 92529821002, 92529821003, 92529821004 METHOD BLANK: 3220892 Matrix: Water Associated Lab Samples: 92529821001, 92529821002, 92529821003, 92529821004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 04/07/21 11:03 LABORATORY CONTROL SAMPLE: 3220893 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 14.9 74 64-132 MATRIX SPIKE SAMPLE: 3220894 92530737001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 ND 18 64-132 M1 Results presented on this page are in the units Indicated by the "Units" column except where an aftemate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/07/2021 03:06 PM without the written consent of Pace Analytical Services, I.I.C. Page 6 of 12 Iac ( eAnalil ical www.patelabs com QUALITY CONTROL DATA Project: March 2021 SW Pace Project No.: 92529821 QC Batch: 610650 Analysis Method: EPA 200.7 Rev 4.4 1994 OC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92529821001, 92529821002, 92529821003, 92529821004 METHOD BLANK: 3215568 Matrix: Water Associated Lab Samples: 92529821001, 92529821002, 92529821003, 92529821004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L NO 5.0 04/05/2123:21 Lead ug/L NO 5.0 04/05/2123:21 Zinc ug/L ND 10.0 04/05/2123:21 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 3215569 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 517 103 85-115 Lead ug/L 500 471 94 85-115 Zinc ug/L 500 457 91 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3215570 3215571 MS MSD 92529821001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 7.5 500 500 534 539 105 106 70-130 1 Lead ug/L ND 500 500 491 492 98 98 70-130 0 Zinc ug/L 145 500 500 625 630 96 97 70-130 1 Results presented on this page are in the units indicated by the "Unite" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/07/2021 03:06 PM without the written consent of Pace Analytical Services, L-C. Page 7 of 12 1�;a'ceAnalyfical' www.pacelabsxom QUALITY CONTROL DATA Project: March 2021 SW Pace Project No.: 92529821 QC Batch: 609823 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92529821001, 92529821002, 92529821003, 92529821004 METHOD BLANK: 3211790 Matrix: Water Associated Lab Samples: 92529821001, 92529821002, 92529821003, 92529821004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 03/28/21 11:12 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 3211791 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 248 99 90-110 SAMPLE DUPLICATE: 3211806 92529776002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 535 545 2 SAMPLE DUPLICATE: 3211807 92529961001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 2760 2740 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fun, Date: 04/07/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 m (�IaneAnalyfical www.pacelabs.com QUALIFIERS Project: March 2021 SW Pace Project No.: 92529821 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Retative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/07/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 12 aceAnalytical www.pacelaGs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: March 2021 SW 92529821 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92529821001 1 EPA1664B 611861 92529821002 2 EPA 1664B 611861 92529821003 3 EPA1664B 611861 92529821004 4 EPA1664B 611861 92529821001 1 EPA 200.7 Rev 4.4 1994 610650 EPA 200.7 Rev 4.4 1994 610681 92529821002 2 EPA 200.7 Rev 4.4 1994 610650 EPA 200.7 Rev 4.4 1994 610681 92529821003 3 EPA 200.7 Rev 4.4 1994 610650 EPA 200.7 Rev 4.4 1994 610681 92529821004 4 EPA 200.7 Rev 4.4 1994 610650 EPA 200.7 Rev 4.4 1994 610681 92529821001 1 SM 254OD-2011 609823 92529821002 2 SM 254OD-2011 609823 92529821003 3 SM 2540D-2011 609823 92529821004 4 SM 254OD-2011 609823 Date: 04/07/2021 03:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 12 CHAIN -OF -CUSTODY Analytical Request Document LAB USE ONLY- Affix Workordr � �/ 9252M8 /r1 f. i PaceAnalytical 1 w�� Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevent fields II � III II III III () I II III Company; Billing Information: , ' `� P!G a 1-�. ALLSHADED Container Preservative Type •` 92529821 -- Address: u Rep rt T0: Ejnail To: ' • Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hsdrochloric acid, (4) sodium hydroxide, (5) zinc acetate, I? a ¢ rLtnot4ten to (6) methana1,17j sodium bisutfate,l8j sodium thiosutfate, f9j hexane, (A) ascorbic acid, (B) ammonium sulfate, (C) ammonium hydroxide, ID) TSP, (U) Unpreserved, (0) Other Copy To: e C Og n oJAddre s: Analyses Lab Prof! Upe: Customer Project Name/Number: f State: County/City: Time Zone Collected: rok 202-1 SU+I NC, /A.16eVl I i e [ [ PT [ [ MT [ [ CT (�(ET J '` x Lab S pie Receipt Checklist: P F .�+ •�•• - Custody Seals PresentlIntact YNA Phone: % - $-2$ $ Site/Facility ID #: Compliance Monitoring? Email: Yes [ ]No -S S +� A w Custody Signatures Present H NA Collector Signature Present N NA V1 _ Q 1✓1 Bottles Intast'l ; N HA correct Bottles nt H HA Collected By (print): Purchase Order #: QW PWS ID #: 4nyn ri ctYY1 Quote #: OW Location Code: ,rt 1U nt cvolume N HA sufficieReeived once Samples VOA - Headspace AcceptableiY tNt ilected By signature): Turnaround Date Required: Immediately ace on Ice: [(Yes I )No t Y USDA Regulated Soils Y N r Samples in Holding Time 0 H NA Residual Chlorine Present Y H ID Sample Disposal: Rush: Field Filtered (if applicable): ( I Dispose as appropriate I I Return [ I Archive: ( ]Same Day ( )Next Day I ) 2 Day 3 Day 4 Day S Day ( ) Yes ( ) No i Cl Stripe: �- Sample pH Acceptable V n NA[ [ ) ( ) ( ) Analysis: ♦ A- pH Strips: 3�ia A� I Hold: (Expedite Charges Apply) 4 4-1 iN Sulfide Present x tt • Matrix Codes (insert in Matrix box below): Drinking Water (OW), Ground Water (GW), Wastewater [WW), Lead Acetate Stripst Product (P), Soil/Solid [SL), Oil (OL), Wipe [WP), Air (AR), Tissue (TS), Bioassay (8), Vapor (V), Other (OT) r LAB USE ONLY: Lab Sample 6 I Comments Comp / Collected (or Res # Customer Sample ID Matrix ' Grab Composite Start) Composite End Cl of Ctns i!: .5 Q I Date Time Date Time aka qua tTt ' C79A0 o *5 t oo o S r. S 3 1 1 ► t �3t. 0 3t, t5 U09- Customer Remarks J Special Conditions / Possible Hazards: Type of Ice Used: et Blue Dry None SHORT HOLDS PRESENT (02 hours): Y CN N/A Lab Sample Temperature Info: Temp Blank Recelved: Y (� NA Packing Material Used: Lab Tracking #: 2427025 Therm ID#: _ Cooler 1 Temp Upon Receipt:-fi5 oC [R.dchern sample(s) screened (c500 cpm): Y N NA Samples received via: Cooler i Therm Corr. Factor: �2_oC FEDEX UPS Clien Courier Pace Courier Cooler 1 Corrected Temp: q'.'a oC Comments: Reli q ' hed by/Company: ISignature) Date/fime: C Recei y/Comps y: (Signature) Date/Time: MTJL LAB USE ONLY ) 6&Acctnum: x Z� JSqT Table#: Template: Relinquished by/Company: (Signature) Oate/Time: a by/Company: [Signature) Date/Time: _ Trip Blank Received: Y N NA Prelogin: PM: HCL McOH TSP Other Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: on Crsnformance(s): Page: PaBa 11 Of ; PB: YES / NO of: Document Name, Sample Condition Upon Rec ICeAnaMkal' Document No.: F-CAR-05-033-Rev.1 *Check marls top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, MC, Oil and Grease, DRO/8015 (water) DOC, LLH6 **Bottom half of box is to list number of bottles pecwment Revised: October 28, 2020 Paee 2 of 2 -- Issuing Authority: pace Carolinas Quality Office Project N 1 Ij' # * 9i 2529VQ 21 ph: CDl Due Date: 04/O8/21 CLIENT: 93—Therm0 t I I I u.ten roof M y V 53 A °' = a =' "1+' n m n M m C D a .o a� C O 2 V o = a N O m V m T C z ¢ ,�� =• a p = a c c o �: E ? 0 I u' _ a C M a. E LA O. E o a E o 0 a i i E ,n o c o R i G ,n i E in o E: 9 E d ; E 4 `w d o q i O O O 0 o j E a J > > > E E E E m E E E E I > i n o uoi o N Qo voi O CLA e. c O. to tL 9 n. O. to .e Q. o Nv 6. tl v Q. M �S i l9 Q '+ V' d m r� m m m m 0 w a n I:J V' t4 13 l? t7 0 > i G m Q > S d 4 d > > --- - tv 1e1 ' --1 3 5 ^� i �r 9 11 12 pH Adjustment Lag for Preserved Samples Lott sample ID Type of Preservative pH upon receipt Date preservation adµsted Time preservation adjusted Amount Preservative added compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification offia Note: Whenever there is a discrepancy affectin8 North Carolina Out of hold, Incorrect preservative, out of temp, incorrect containers. N O E Thermo Rsher S C I E N T I F I C Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Stormwater Analytical Monitoring Results for Thermo Fisher Scientific, LLC I have attached the analytical monitoring results from stormwater sampling that was collected on March 25, 2021 at Thermo Fisher Scientific, LLC's four outfalls. Per our General Storm Water Permit No. NCG03000 requirements of monthly monitoring for applicable parameters during a storm event, I have sampled each outfall for copper, zinc, pH, lead, TSS, and Non -Polar Oil/Grease/TPH. Results show that TSS at one outfall, copper at two outfalls, and zinc at three of the four outfalls were above the benchmark values, as noted in Table 3 of the general storm water permit. All other results were below the benchmark values. We have implemented a Tier Three response for the site and Thermo Fisher Scientific, LLC has notified the Asheville Regional Office. Thermo Fisher Scientific, LLC is currently working with an environmental consultant to help achieve compliance with the benchmark values set forth in the facility's storm water permit. I have attached the completed Monitoring Report containing the monitoring results from the four outfalls. If you have any questions, please feel free to contact me at 828-658-2845. Jeremy Putnam Sr. EHS Manager Attachments: 1