NCG030134_DMR_20210112

Stormwater Discharge MonitoringReport
eport
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted: 01/12/2021
CERTIFICATE OF COVERAGE NO. NCG030134
FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS
LABORATORY: Pace Analytical Lab Cert. #
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR
SAMPLE PERIOD —Jan-June July -Dec
Or X Monthly: December
DISCHARGING TO CLASS n ORW n HQW Trout n PNA
Zero -flow QNater Supply DA
Other
JAN 2 J Z021PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -
l]WR 5�Gi•f^'N
nNo discharge this period?'
Outfall No.
Date Sample
Collected;
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organics5
Benchmarks
-
-
100 mg/L or 50 mg/L°
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Outfall 1
12/24/2020
0.6
23.2
6.4
0.011
<0.005
0.302
<5
N/A
Outfall 2
12/24/2020
0.6
14.1
6.6
0.0126
<0.005
0.102
<5
N/A
Outfall 3
12/24/2020
0.6
37.2
6.4
0.0253
<0.005
0.168
<5
N/A
Outfall4
12/24/2020
0.6
10.3
6.5
<0.005
<0.005
0.317
<5
N/A
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
s See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO
monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the
General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),
I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent
management plan included in the Stormwater Pollution Prev i°�Plan."
�c :P
Name (Print name)
Ti a (Print title)
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
F7No discharge this period?2
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/O
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?
YES X NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert
(Asheville Regional Office)
Mail an original copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the
case of "No Discharae" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am a ar that therpre significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of
Date
Permit Date:11/1/2018-05/31/2021
11/1/2018
SWU-245, last revised

Thermo Rsher
S C. I E N T I F I C
January 12, 2021
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Stormwater Analytical Monitoring Results for Thermo Fisher Scientific, LLC
I have attached the analytical monitoring results from stormwater sampling that was collected
on December 24, 2020 at Thermo Fisher Scientific, LLC's four outfalls.
Per our General Storm Water Permit No. NCG03000 requirements of monthly monitoring for
applicable parameters during a storm event, I have sampled each outfall for copper, zinc, pH,
lead, TSS, and Non -Polar Oil/Grease/TPH. Results show that both copper and zinc were above
the benchmark values at three of the four outfalls, as noted in Table 3 of the general storm
water permit. All other results were below the benchmark values. We have implemented a Tier
Three response for the site and Thermo Fisher Scientific, LLC has notified the Asheville Regional
Office. Thermo Fisher Scientific, LLC is currently working with an environmental consultant to
help achieve compliance with the benchmark values set forth in the facility's storm water
permit. I have attached the completed Monitoring Report containing the monitoring results
from the four outfalls.
If you have any questions, please feel free to contact me at 828-658-2845.
Jeremy Putnam
Sr. EHS Manager
Attachments: 1

__ aceAnalytical
www.pacalabs.com
January 11, 2021
Mr. Jeremy Putnam
Thermo Electron Corp.
275 Aiken Road
Asheville, NC 28804
RE: Project: Dec. 2020 SW 12124
Pace Project No.: 92513743
Dear Mr. Putnam:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 24, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
lL-z-- _,�.-.�_.
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
"Nr
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification M 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification M 37706
Kentucky UST Certification M 84
North Carolina Field Services Certification M 5342
Virginia/VELAP Certification M 460221
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Fiorida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification M 40
South Carolina Certification M 99030001
VirginiaNELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C. Page 2 of 12

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SAMPLE ANALYTE COUNT
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
Method
Analysts
Analyses
Reported
Laboratory
92513743001
1
EPA 1664B
CJM
1
PASI-C
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
DS
3
PASI-A
SM 254OD-2011
ALP
1
PASI-A
92513743002
2
EPA1664B
CJM
1
PASI-C
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 2540D-2011
ALP
1
PASI-A
92513743003
3
EPA 1664B
CJM
1
PASI-C
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 2540D-2011
ALP
1
PASI-A
92513743004
4
EPA 1664E
CJM
1
PASI-C
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 2540D-2011
ALP
1
PASI-A
PASI-A= Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Dec. 2D20 SW 12/24
Pace Project No.: 92513743
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: 1
Parameters
Lab ID: 925137430D1 Collected: 12/24120 11:00
Results Units Report Limit DF
Received: 12124/20 12:24 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
01/08121 11:22
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
01/08/21 11:22
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
11.0 ug/L
5.0
1
01/0612100:56 01/06/2120:32 7440-50-8
Lead
ND ug/L
5.0
1
D1/0612100:56 01/0612120:32 7439-92-1
Zinc
302 ug/L
10.0
1
01/0612100:56 01/06/2120:32 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
23.2 mg/L
2.5
1
12/29/20 11:28
Sample: 2 Lab ID: 92513743002 Collected: 12/24120 11:15 Received: 12/24/20 12:24 Matrix: Water
Parameters
HEM, Oil and Grease
Oil and Grease
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
200.7 MET ICP
Copper
Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
Date: 01/11/2021 07:30 AM
Results Units Report Limit DF Prepared Analyzed GAS No. Qual
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
NO mg/L 5.0 1 01/08/2111:22
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
ND mg/L 5.0 1 01/08/2111:22
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
12.6 ug/L 5.0 1 01/06/2100:56 01/0612120:48 7440-5D-8
ND ug/L 5.0 1 01/06/2100:56 01/0612120:48 7439-92-1
102 ug/L 10.0 1 01/06/2100;56 01/06/2120:48 7440-66-6
Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
14.1 mg/L 3.0 1 12/2912011:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 12

Pace Analytical Services, LLC
2225 Riverside Dr.
aceMalXicai 0 Asheville, NC 28804
www.pacelabs.com [phone]
i
i
ANALYTICAL RESULTS
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
Sample: 3 Lab ID: 92513743003 Collected: 12/24/20 11:30 Received: 12/24/20 12:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
01/08/21 11:22
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg1L
5.0
1
01/08/21 11:22
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
25.3 ug/L
5.0
1
01/06/2100:56 0110612120:52 7440-50-8
Lead
ND ug/L
5.0
1
01106/2100:56 01/06/2120:52 7439-92-1
Zinc
168 ug/L
10.0
1
01/06/2100:56 01/06/2120:52 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
37.2 mg/L
5.0
1
12/29120 11:28
Sample: 4
Parameters
HEM, Oil and Grease
Oil and Grease
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
200.7 MET ICP
Copper
Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
Date: 01 /11/202107:30 AM
Lab ID: 92513743004 Collected: 12/24/20 11:45 Received: 12/24120 12:24 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
ND mg/L 5.0 1 01/0812111:22
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
ND mg/L 5.0 1 01/08/2111:22
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
ND ug/L
5.0
1
01106/2100:56 0110612120:55 7440-50-8
ND ug/L
5.0
1
01/06/2100:56 01/0612120:55 7439-92-1
317 ug/L
10.0
1
01/06/2100:56 01 /06121 20:55 7440-66-6
Analytical Method: SM 2540D-2011
Pace Analytical Services - Asheville
10.3 mg/L
2.5
1
1212912011:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
QC Batch: 591513 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
METHOD BLANK: 3122727 Matrix: Water
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 01/0B/21 11:22
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(B28)254-7176
LABORATORY CONTROL SAMPLE:
3122728
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 33.6
84
78-114
MATRIX SPIKE SAMPLE:
3122729
92514150004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
26.2
64
78-114 M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11 /2021 07:30 AM without the written consent of Pace Analytical Services, LLC.
Page 6 of 12

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QUALITY•CONTROL DATA
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
QC Batch: 591515 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
METHOD BLANK: 3122742 Matrix: Water
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.0 01/08/21 11:22
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 3122743
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L 20 15.7 78 64-132
MATRIX SPIKE SAMPLE: 3122744
92514328001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L ND 20 ND 10 64-132 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 07:30 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 12

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QUALITY CONTROL DATA
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
QC Batch: 590825 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
METHOD BLANK: 3119311 Matrix: Water
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper ug/L ND 5.0 01/06/2120:10
Lead ug/L ND 5.0 01/06/2120:10
Zinc ug/L ND 10.0 01/0612120:10
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
3119312
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Copper
ug/L
500
462 92 85-115
Lead
ug/L
500
459 92 85-115
Zinc
ug/L
500
464 93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3119313
3119314
MS
MSD
92513663001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper
ug/L
0.039
500
500
524
517
97
96
70-130
1
mg/L
Lead
ug/L
0.015
500
500
482
475
93
92
70-130
1
mg/L
Zinc
ug/L
0.072
500
500
555
549
97
95
70-130
1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3119315
3119316
MS
MSD
92514237002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper
ug/L
0.016
500
500
506
507
98
98
70-130
0
mg1L
Lead
ug/L
<0.0050
500
500
463
460
92
92
70-130
1
mg/L
Zinc
ug/L
0.12
500
500
595
592
95
94
70-130
0
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 07:30 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 12

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QUALITY CONTROL DATA
Project: Dec. 2020 SW 12/24
Pace Project No.: 92513743
QC Batch: 589742 Analysis Method: SM 254OD-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
METHOD BLANK: 3114565 Matrix: Water
Associated Lab Samples: 92513743001, 92513743002, 92513743003, 92513743004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 12/29/20 11:26
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 3114566 3114711
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Total Suspended Solids mg/L 250 246 238 99 95 90-110 3 25
SAMPLE DUPLICATE: 3114712
Parameter Units
Total Suspended Solids mg/L
92513899001 Dup
Result Result RPD Qualifiers
208 210 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 07:30 AM without the written consent of Pace Analytical Services, I.L.C.
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QUALIFIERS
Project: Dec. 2020 SW 12124
Pace Project No.: 92513743
I , G.
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(628}254-7176
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific anatyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylarnine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11/2021 07:30 AM without the written consent of Pace Analytical Services, L.L.C. Page 10 of 12

ZaceAnalXical"
www.pacelabs.com
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Dec. 2020 SW 12124
Pace Project No.: 92513743
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92513743001
1
EPA 1664E
591513
92513743002
2
EPA 1664E
591513
92513743003
3
EPA 1664B
591513
92513743004
4
EPA 1664B
591513
92513743001
1
EPA 1664E
591515
92513743002
2
EPA 1664B
591515
92513743003
3
EPA 1664E
591515
92513743004
4
EPA 1664E
591515
92513743001
1
EPA 200.7 Rev 4.4
1994
590825
92513743002
2
EPA 200.7 Rev 4.4
1994
590825
92513743003
3
EPA 200.7 Rev 4.4
1994
590825
92513743004
4
EPA 200.7 Rev 4.4
1994
590825
92513743001
1
SM 2540D-2011
589742
92513743002
2
SM 2540D-2011
589742
92513743003
3
SM 2540D-2011
589742
92513743004
4
SM 2540D-2011
589742
Date: 01/11/2021 07:30 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
EPA 200.7 Rev 4.4 1994 590851
EPA 200.7 Rev 4.4 1994 590851
EPA 200.7 Rev 4.4 1994 590851
EPA 200.7 Rev 4.4 1994 590851
Page 11 of 12

LASUSE 1 WOE# : 92513743 'nberor
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CHAIN -OF
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•' Prc�servauve Types: (1) nitric acid, (2) sulfuric a rid, 13) hydrochloric acid, (4) sodium hydroxide,15) zinc. acetate,
W(' t�tA, A.i!Y't
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(6) methanol, (7) sodium likulfate, (A) sodium thiusullale, (9) hexane,
(CI ammonium hydroxide, (D) TSP, (U) Unpreserved, ID}
(A) ascorbic acid, IS) amrnuniurn sulfate,
Copy To:
rite Collection nfo/Address:
Analyses
Lab Profile/Line:
Customer Project Name/Number: {-`''
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Slate: County/City: Time Zone Collected:
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Custody Seals Present/Intact Y©N NA
custody signatures Present 11 NA
Collector signature PresentN ttA
N NA
Bottles Intact all t1A
Phone:62-8d'8-2.8
Email:
Site/Facility ID N:
Compliance Monitoring?
Yes ( ! No
Collected By (print):
tD
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Purchase Order
Quote It:
It
DW PWS ID It:
DW Location Code:
t
Correct Bottles
stiff icient volume N NA
Samples Received on Ice N NA
VaA - naadesPnee Acceptable Y p
USDA Regulated. Soils Y No
ullecter+�nature):
7urnaruunel Date
ertulrecl:
lmme late y ac r, on Ice:
Yes ( j No
y
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Samplat, in Holding 7'imo CD N NA
Residual Chlorine Present Y N
Rush:
Field Filtered (if applicable):
Sample Disposal:
( ) Dispose as appropriate ( I Return
( I Archive: ___-__
[ ) Same
[ 12 Day I
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) Day I ] 4 Day ( ) 5 Day
( ) Yes ( ] No
Analysis:
(
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Cl strips:
Sample pit Ab �Y N NA
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pit Strips:.2
( IHold:_
(Eapr
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%
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Sulfide Present Y t !
Lead Acetate Strips:
• Matrix Codes (Insert in Matrix box below): Drinking
Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air
I AR), Tissue (TS), Bioassay (B), vapor (V), Other (OT)
�
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LAB USE ONLY:
Lab Samle b`.f Comments:
P
Camp/
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Customer Sample ID
Matrix "
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Composite End
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Date
Time
Date
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Customer Remarks / Special Conditions / Possible Hai
lyds:
Type of Ice Used: Wet.) Blue Dry None
SHORT
HOLDS PRESENT (<72 hours): Y UN N/A
Lab Sample Temperature Info:
Q
Packing Material Used:
Lab
Tracking If:
2427023
Temp Blank Received: �Y NA
Therm IDR:
Cooler 1 Tem6 Upon Receipt: <.. oC
Radchem sample(s) screened (<500 cpm): Y N ti W/
.�.,
Samples received via:
FEDEX UPS Client Courier Pace Courier
Cooler 1 Therm Corr. Factor: _{ZoC
Cooler l Corrected Temp:
Re jnc fished b npany: (Signature)
Date``/Time: Receive o y mpany: (Signs ore)
/
Date/Time! M71L LAB USE ONLY
Table
_ _ac
Comments;
n:
Date/Time: Received by/Company: (Signature)
Acctnum:
Daie/Tinte:
Relinquished by/Company: (Signature)
_
Trip 0
Template-
Blank Received: Y NA
Date/Time: Received by/Company: (Signature)
Prelogin:
Date/Time: PM:
HCL McOH TSP Other
Relinquished by/Company: (Signature)
Non Conformance(s):
Pace:
PB:
YES /'
of: