NCG030145_DMR_20210603

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Z77,z
neral Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGENO. NCG030145 SAMPLE COLLECTION YEAR: 2021
FACILITY NAME: Newton Instruments i ,t �CSMPLE PERIOD ❑ Jan -June ❑ July -Dec
COUNTY: Granville ,;�ECE V or ®Monthly' May 2021
PERSON COLLECTING SAMPLES: Geoffrey Murphrey DISCHARGING TO CLASS ❑ORW ®HQW ❑Trout ❑PNA
LABORATORY: : Pace Analytical Lab Cert. ##: 40 jum 14 NZ ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: Monthly samplifflq7RAL FILES ❑Other
JWR SECTION
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 34
Part A: Stormwater Benchmarks and Monitoring Results
❑ No discharge this period?'
pH'
Non -Polar
Outfall No.
Date Sample
24-hour rainfall
Total Suspended
Standard
Copper
Lead
Zinc
O&G/ Total
Total Toxic
Collected'
amount,
Solids
Petroleum
Organics'
(mo/dd/yr)
Inches'
units
Hydrocarbons
Benchmarks
-
-
100 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
001
05/12/21
0.2
15.2 mg/L
7.2
0.0056 mg/L
<0.005 mg/L
0.0171 rrg/L
8.4 mg/L
Not Detected
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
Permit Date: 11/1/2017-10/31/2022 SWU-245, last revised 10/25/2012
Page 1 of 3

stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or others imi I a r non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L', where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2017-10/31/2022 SWU-245, last revised 10/25/2012
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?YES ® No ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE?YES ® NO ❑
REGIONAL OFFICE CONTACT" NAME: John Holley
Mail an original and one copy of this DMR, including all "No Discharge" reportsLwithin 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports] to:
Division of Water Quality
Attn: DWQ Central Files
1517 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature o
(Date)
Permit Date: 11/1/2017-10/31/2022 SWU-245, last revised 10/25/2012
Page 3 of 3

ace Analytical
www.pacelabs.com
May 28, 2021
Mr. Pete Dressel
Piedmont Geologic
6003 Chapel Hill Road
Suite 109
Raleigh, NC 27607
RE: Project: Newton Instruments/ 2112
Pace Project No.: 92538713
Dear Mr. Dressel:
Pace Analytical Services, LLC
9800 KinceyAve- Suite 100
Huntersville, NC 28078
(704 )875-90 92
Enciosed are the analytical results for sample(s) received by the laboratory on May 13, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
Revision 1 - This report replaces the May 26, 2021 report This report was reissued on May 28, 2021 to update collectors
name per client's request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Jonathan Murphrey, Piedmont Geologic
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.L.C.
Page 1 of 30

aceAnalytical
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r
E
Project: Newton Instruments 12112
Pace Project No.: 92538713
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
(704 )878-9092
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia[VELAP Certification M 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiafVELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shah not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 30

Pace Analytical Services, LLC
3
aceAnalytrcal 9844 untey Ave, Suite 144
Hurstersville, NC 26078
www.pacelabs.com [phone]
SAMPLE SUMMARY
Project: Newton Instruments 12112
Pace Project No.: 92538713
Lab ID Sample ID Matrix pate Collected pate Received
92538713001 Outfall-001 Water 0511212110:05 05/13/2115:18
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 30

_ ?ceAnalytical_'
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SAMPLE ANAL.YTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Project:
Pace Project No.:
Newton Instruments ! 2112
92538713
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92538713001
Outfall-001
SM 254OD-2011
LRB
1
PASI-E
EPA 1664B
TEG
1
PASI-C
EPA 608.3
SEM
30
PASI-C
EPA 200.7 Rev 4.4 1994
IDS
12
PASI-A
EPA 245.1 Rev 3.0 1994
SOO
1
PASI-A
EPA 625.1
PKS
62
PASI-C
EPA624.1
SAS
31
PASI-C
EPA420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
PAS[ -A= Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC Page 4 of 30

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ANALYTICAL RESULTS
Project: Newton Instruments / 2112
Pace Project No.: 92538713
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall-001
Lab ID:
92538713001
Collected:
05/12/21 10:05
Received: 05/13/21 15:18 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical
Method: SM 254OD-2011
Pace Analytical Services
- Eden
Total Suspended Solids
15.2
mg/L
2.6
2.6
1
05/17121 09:08
Field Data
Analytical
Method:
Pace Analytical
Services
- Charlotte
Perforated by
Piedmont
1
05/12/21 10:05
Geologic
Collected By
Geoffrey
1
05/12121 10:05
Murphrey
Collected Date
06112/21
1
05/1221 10:05
Collected Time
10:05
1
0511221 10:05
pH
7.2
Std. Units
1
05/12/21 10:05
HEM, Oil and Grease
Analytical
Method: EPA 1664E
Pace Analytical
Services
- Charlotte
Oil and Grease
8.4
mg/L
4.9
1.1
1
05/2521 18:53
608 PCB Pest RVE
Analytical
Method: EPA608.3 Preparation Method: EPA608.3
Pace Analytical Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.026
1
0&18/2106:25
05/212104:26 309-00-2
alpha-BHC
ND
ug/L
0.050
0.026
1
05/182106:25
05/212104:26 319-84-6
beta-BHC
ND
ug/L
0.050
0.022
1
05/182106:25
05/212104:26 319-85-7
delta-BHC
ND
ug/L
0.050
0,018
1
051182106:25
051212104:26 319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.020
1
05/1821 06:25
05/2121 04:26 58-89-9
Chlordane (Technical)
ND
ug/L
0.50
0.21
1
0511M 106:25
05/2121 04:26 57-74-9
alpha -Chlordane
ND
ug/L
0.050
0.015
1
05/182106:25
051212104:26 5103-71-9
gamma -Chlordane
ND
ug/L
0.050
0.035
1
05/182106:25
051212104:26 5103-74-2
4.4'-DDD
ND
ug/L
0.050
0,012
1
05/182106:25
05/212104:26 72-54-8
4.4'-DOE
ND
ug/L
0.050
0.016
1
05/182106:25
05/212104:26 72-55-9
4.4'-DDT
ND
ug/L
0.050
0.048
1
05/182106:25
05/212104:26 50-29-3
Dieldrin
ND
ug/L
0.050
0.013
1
05/1821 06:25
0512121 04:26 60-57-1
Endosulfan I
ND
ug/L
0.050
0.014
1
05/1821 06:25
05/2121 04:26 959-98-8
Endosulfan 11
ND
ug/L
0.050
0.017
1
05/1821 06:25
05121M 04:26 33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.014
1
05/1821 06:25
0512121 04:26 1031-07-8
Endrin
ND
ug/L
0.050
0.014
1
05/1821 06:25
0512121 04:26 72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.028
1
05/1821 06:25
05/2121 04:26 7421-93-4
Heptachlor
ND
ug/L
0.050
0.036
1
05/1821 06:25
0512121 04:26 76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.015
1
0&1821 06:25
0512121 04:26 1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.47
1
0511IM1 06:25
0512121 04:26 12674-11-2
PCB-1221 (Arodor 1221)
ND
ug/L
0.50
0.45
1
05/1821 06-.25
05/2121 04:26 11104-28-2
PCB-1232 (Arodor 1232)
ND
ug/L
0.50
0.36
1
05/1821 06:25
052121 04:26 11141-16-5
PCB-1242 (Arodor 1242)
ND
ug/L
0.50
0.26
1
05/1821 06:25
0512121 04:26 53469-21-9
PCB-1248 (Arodor 1248)
NO
ug/L
0.50
0.40
1
0511821 06:25
052121 04:26 12672-29-6
PCB-1254 (Arodor 1254)
NO
ug/L
0.50
0.25
1
05/1821 06:25
052121 04:26 11097-69-1
PCB-1260 (Arodor 1260)
ND
ug/L
0.50
0.42
1
0511821 06:25
0512121 04:26 11096-82-5
PCB, Total
ND
ug/L
0.50
0.50
1
05/1821 06:25
05/2121 04:26 1336-36-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/282021 10:52 AM without the written consent of Pace Analytical Services, LLC, Page 5 of 30

aceAnalytrcal
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(7p4)875-9092
Project: Newton Instruments 12112
Pace Project No.. 92538713
Sample: Outfall-001
Lab ID:
92538713001
Collected:
05112/21 10:05
Received: 05/13/21 15:18 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared
Anaiyzed CAS No.
Qual
608 PCB Pest RVE
Analytical
Method: EPA608.3
Preparation Method: EPA608.3
Pace Analytical
Services
- Charlotte
Toxaphene
ND
ug/L
050
0.27 1
05/18/21 06:25
05/21/21 04:26 8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
113
%
10-154
1
05/18/21 06:25
05/21/21 04:26 877-09-8
Decachlorobiphenyl (S)
106
%
10-184
1
05/18/21 06:25
05/21/21 04:26 2051-24-3
200.7 MET ICP
Analytical Method: EPA200
7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical
Services
- Asheville
Antimony
ND
uglL
5.0
3.0 1
05/22/21 09:50
05/22/21 23:06 7440-36-0
Arsenic
ND
ug1L
10.0
4.7 1
05/22/21 09:50
05/22/21 23:06 7440-38-2
Beryllium
Nil
ug/L
1.0
0.70 1
0512212109:50
0512212123:06 7440-41-7
Cadmium
ND
ug/L
1.0
0.40 1
0512212109:50
0512212123:06 7440-43-9
Chromium
ND
ug1L
5.0
3.7 1
05/22/21 09:50
05/22/21 23:06 744047-3
Copper
5.6
ug/L
5.0
4.3 1
05/22/21 09:50
05/22/21 2106 7440-50-8
Lead
NO
ug1L
5.0
4.5 1
05/22/21 09:50
05/22/21 23:06 7439-92-1
Nickel
3.5J
ug/L
5.0
3.5 1
05/22/21 09:50
0512212123:06 7440-02-0
Selenium
ND
ug/L
10.0
4.7 1
05/22/21 09:50
0512212123:06 7782-49-2
Silver
ND
ug1L
5.0
2.5 1
05/2212109:50
05/22/21 23:06 7440-22-4
Thallium
ND
ug1L
10.0
8.1 1
0512212109:50
05/22/21 23:06 7440-28-0
Zinc
17-1
ug/L
10.0
9.5 1
05/22/21 09:50
05/22/21 23:06 7440-66-6
245.1 Mercury
Analytical
Method: EPA245
1 Rev 3.0
1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical
Services
-Asheville
Mercury
ND
ug1L
0.20
0.12 t
05/24/2113:55
0512512113:01 7439-97-6
625 RVE
Analytical
Method: EPA 625.1
Preparation Method: EPA625.1
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/L
5.0
2.0 1
05118/21 11:12
05119/2121:44 83-32-9
Acenaphthyiene
ND
ug/t_
5.0
2.0 1
0511812111A2
0511912121:44 208-96-8
Anthracene
ND
ug1L
5.0
2 3 1
05/18/21 11:12
05/19/21 21:44 120-12-7
Benzidine
ND
ug1L
50.0
13.4 1
05/18/21 11:12
05/19/21 21:44 92-87-5
IL
Benzo(a)anthracene
ND
ug1L
5.0
2.7 1
05/18/21 11:12
05/19/2121:44 56-55-3
Benzo(a)pyrene
ND
ug1L
5.0
2.8 1
05118/2111:12
05/19/2121:44 50-32-8
Benzo(b)fluoranthene
ND
ug1L
5.0
2.6 1
0511812111:12
05119/2121:44 205-99-2
Benzo(g.h,i)perylene
ND
ug1L
5.0
2.8 1
M1812111:12
0511912121:44 191-24-2
Benzo(k)fluoranthene
ND
ug1L
5.0
2.7 1
0511812111:12
05/19/2121:44 207-08-9
4-Bromophenylphenyl ether
ND
ug1L
5.0
1.8 1
05/18/21 11712
05/19/21 21:44 101-55-3
L1
Butyl benzylphtha late
ND
ugIL
5.0
3.1 1
M1812111:12
0511912121:44 85-68-7
L1
4-Chloro-3-methyl phenol
ND
ug1L
5.0
3.3 1
05/18/21 11:12
05119/2121:44 59-50-7
bis(2-Chloroethoxy)methane
ND
ug1L
10.0
1.8 1
0511812111:12
05119/2121:44 111-91.1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.9 1
05/18/21 11:12
05/19/21 21:44 111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1.7 1
05/18/21 11:12
05/19/21 21:44 91-58-7
2-Chlorophenol
ND
ug/L
5.0
1.2 1
05/18/21 11:12
05/19/21 21:44 95-57-8
4-Chlorophenylphenyl ether
ND
ug1L
5.0
2.0 1
05/18/21 11:12
05/19/21 21:44 7005-72-3
Chrysene
ND
ug1L
5.0
2.8 1
0511812111:12
0511912121:44 218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
3.0 1
05/18/21 11:12
05/19/21 21:44 5370-3
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except in full,
Date: 05/28/2021 10:52 AM
without the written consent of Pace Analytical Services,
LLC.
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ANALYTICAL RESULTS
Project: Newton Instruments / 2112
Pace Project No.: 92538713
Pace Analytical Services, LLC
9800 Kincey Ave_ Suite 100
Huntersviile. NC 28078
[phone]
Sample: Outfall-001 Lab 1D: 92538713001 Collected: 05/12/21 10:05 Received: 05/13/21 15:18 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 RVE
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobe nzidine
2,4-❑ichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylptie nol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphth a late
1,2-Diphenylhydrazine
bis(2-Ethylhexyl)phlhalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitropheno!
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorcbiphenyl(S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Analytical Method: FPA625.1 Preparation Method: EPA625.1
Pace Analytical Services - Charlotte
ND
ug/L
5.0
1.8
1
05/1812111:12
0511912121:44
95-50-1
ND
ug/L
5.0
1.5
1
05118/2111:12
05/1912121:44
541-73-1
ND
ug/L
5.0
1.7
1
0511812111:12
0511912121:44
106-46-7
ND
ug1L
10.0
8.1
1
0511812111:12
05/19/21 21:44
91-94-1
ND
ug/L
5.0
1.4
1
05/1812111:12
05/1912121:44
120-83-2
ND
ug/L
5.0
2.0
1
05118/2111:12
0511912121:44
84-66-2
ND
ug/L
10.0
1.7
1
05/1812111:12
0511912121:44
105-67-9
ND
ug/L
5.0
2.1
1
05/18/21 11:12
0511912121:44
131-11-3
ND
ug/L
5.0
2.2
1
05/18/21 11:12
05/19/21 21:44
84-74-2
ND
ug/L
10.0
3.4
1
05/1812111:12
05/19/21 21:44
534-52-1
ND
ug/L
50.0
25.0
1
05/18/21 11:12
05/19/21 21:44
51-28-5
ND
ug1L
5.0
1.6
1
05/18/21 11:12
05/19/21 21:44
121-14-2
ND
ug/L
5.0
1.7
1
05/18/21 11:12
05/19/21 21:44
606-20-2
ND
ug/L
5.0
3.9
1
0511812111:12
05119/2121:44
117-84-0
ND
ug/L
5.0
1.6
1
05/18/21 11:12
05/1912121:44
122-66-7
ND
ug/L
5.0
3.7
1
05/18/21 11:12
05/19/21 21:44
117-81-7
ND
ug/L
5.0
2.2
1
05/18/21 11:12
05/19/21 21:44
206-44-0
ND
ug/L
5.0
2.1
1
05/18/21 11:12
0511912121:44
86-73-7
ND
ug/L
5.0
1.8
1
05/113/21 11:12
05119/2121:44
87-68-3
ND
ug/L
5.0
2.2
1
05/18/2111:12
0511912121:44
118-74-1
ND
ug/L
10.0
1.6
1
05/18/21 11:12
05/19/21 21:44
77-47-4
ND
ug/L
5.0
1.4
1
05/18/21 11:12
05/19/21 21:44
67-72-1
ND
ug/L
5.0
2.9
1
05/18/21 11:12
05119/2121:44
193-39-5
ND
ug/L
10.0
1.7
1
05/113/21 11:12
05119/2121:44
78-59-1
ND
ug/L
5-0
2.1
1
05/18/21 11:12
05119/2121:44
91-20-3
ND
ug/L
5.0
1.9
1
05/18/21 11:12
0511912121:44
98-95-3
ND
ug/L
5.0
1.4
1
05/18/21 11:12
05/19/21 21:44
88-75-5
ND
ug/L
10.0
6.6
1
05118/2111:12
05/19/2121:44
100-02-7
ND
ug/L
5.0
1.9
1
05/18/21 11:12
05/19/21 21:44
62-75-9
ND
ug/L
5.0
1.3
1
05/16/21 11:12
05/19/21 21:44
621-64-7
ND
ug/L
10.0
3A
1
05/18/21 11:12
05/19/21 21:44
86-30-6
ND
ug/L
10.0
3.8
1
05/18/21 11:12
05/19/21 21:44
87-86-5
ND
ug/L
5.0
2.0
1
05/18/21 11:12
05/19/21 21:44
85-01-8
ND
ug/L
5.0
1.4
1
05/1812111:12
05119/2121:44
108-95-2
ND
ug/L
5.0
2.2
1
0511812111:12
05119/2121:44
129-00-0
ND
ug/L
5.0
1.7
1
05/18/21 11:12
05/19/21 21:44
120-82-1
ND
ug/L
10.0
1.6
1
05/18/21 11:12
05/19/21 21:44
88-06-2
103
%
10-120
1
05/18/21 11:12
05/19/21 21:44
4165-60-0
91
%
15-120
1
05118/2111:12
05/19/21 21:44
321-60-8
124
%
11-131
1
05/18/21 11:12
05/19/21 21:44
1718-51-0
58
%
10-120
1
05/1812111:12
0511912121:44
13127-88-3
70
%
10-120
1
05/18/21 11:12
05/19/21 21:44
367-12-4
119
%
10-137
1
05/1812111:12
05/19/21 21:44
118-79-6
REPORT OF LABORATORY ANALYSIS
L1
L1
L1
L1
L1
L1
L1
L1
L1
L1
L1
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Date: 05128/2021 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 30

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i
ANALYTICAL RESULTS
Project: Newton Instruments 12112
Pace Project No.: 92538713
Pace Analytical Services, LLC
9800 Klncey Ave Suite 100
Huntersville, NC 28078
(704 )875-9092
Sample: Outfall-001 Lab ID: 92538713001 Collected: 05/12/21 10:05 Received: 05/13/21 15:18 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. (Dual
624 Volatile Organics Acrolein
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochiorometha ne
1,1-Dichloroethane
1,2-Dichloroethane
trans- l,2-Dichloroethene
1.2-Dichloropropane
cis-1,3-Dichloropro pene
trans- l,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trlchloroethane
1,1,2-Tri ch loroetha ne
Trichloroethene
Vinyl chloride
Surrogates
4-Bromoffuorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
420.4 Phenolics, Total
Phenolics, Total Recoverable
450OCNE Cyanide, Total
Cyanide
Date: 05/28/2021 10:52 AM
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
ND
ug/L
5.0
3.6
1
05/14/21 14:59
107-02-8
ND
ug/L
5.0
2.3
1
05/14/21 14:59
107-13-1
ND
ug/L
1.0
0.42
1
05/14/21 14:59
71-43-2
ND
ug/L
2.0
0.41
1
05/14/21 14:59
75-27-4
ND
ug/L
2.0
0.59
1
05/14/21 14:59
75-25-2
ND
ug/L
2.0
1.5
1
05/14/21 14:59
74-83-9
ND
ug/L
2.0
0.47
1
05/14/21 14:59
56-23-5
ND
ug/L
2.0
0.39
1
05/1412114:59
108-90-7
ND
ug/L
2.0
0.71
1
05/14/21 14:59
75-00-3
ND
ug/L
5.0
0.94
1
05/1412114;59
110-75-8
ND
ug1L
2.0
0,49
1
05/14/21 14:59
67-66-3
ND
ug/L
2.0
0.60
1
05/14/21 14:59
74-87-3
NO
ug/L
2.0
0.39
1
D511412114:59
124-48-1
ND
ug/L
2.0
0.47
1
05/14/21 14:59
75-34-3
ND
ug/L
2.0
0.42
1
05/1412114:59
107-06-2
ND
ug/L
2.0
0.48
1
05/14/21 14:59
156-60-5
ND
ug/L
2.0
0.44
1
05114/2114:59
78-87-5
ND
ug1L
2.0
0.35
1
05/14/21 14:59
10061-01-5
ND
ug1L
2.0
0.34
1
05114/2114:59
10061-02-6
ND
ug/L
1.0
0.35
1
05/14/21 14:59
100-41-4
ND
ug/L
2.0
0.91
1
05/14/21 14:59
75-09-2
ND
ug/t_
2.0
0.30
1
05/14/21 14:59
79-34-5
ND
ug1L
2.0
0.38
1
05/14/21 14:59
127-18-4
ND
uglL
1.0
041
1
D5114121 14:59
108-88-3
ND
uglL
2.0
0.43
1
05/14/21 14:59
71-55-6
ND
uglL
2.0
0,38
1
05114/2114:59
79-00-5
ND
uglL
2.0
0.41
1
05114/21 14:59
79-01-6
ND
uglL
2.0
0.41
1
05/14/21 14:59
75-01-4
103
%
70-130
1
05/14/21 14:59
460-00-4
102
%
70-130
1
05/14/21 14:59
2037-26-5
98
%
70-130
1
05/14/21 14:59
17060-07-0
Analytical Method: EPA420.4 Rev 1.0 1993 Preparation Method: EPA420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
ND mg/L 0.020 0.0076 1 05/18/21 08:15 05/18/2112:57 64743-03-9
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
ND mg/L 0.0080 0.0060 1 05/19/21 21:32 06/20/21 20:26 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
without the written consent of Pace Analytical Services. l
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QUALITY CONTROL DATA
Project: Newton Instruments 12112
Pace Project No.: 92538713
QC Batch: 620784 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92538713001
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersvilie. NC 28078
[phone]
METHOD BLANK: 3266172 Matrix: Water
Associated Lab Samples: 92538713001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 2.5 05/17121 09:00
LABORATORY CONTROL SAMPLE: 3266173
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 238 95 90-110
SAMPLE DUPLICATE: 3266174
92538710001
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Total Suspended Solids
mg/L
150
155
3 25
SAMPLE DUPLICATE: 3266175
92538710002
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Total Suspended Solids
mg/L
1010
653
43 25 D6
Results presented on this page are in the units indlcated by the "units" column except whore an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/28/2021 10:52 AM without the written consent of Pace Analytical Services, LLG. Page 9 of 30

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QUALITY CONTROL DATA
Project: Newton Instruments 12112
Pace Project No.: 92538713
QC Batch: 622846 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92538713001
METHOD BLANK: 3276679
Associated Lab Samples: 92538713001
Parameter Units
Oil and Grease mg1L
LABORATORY CONTROL SAMPLE: 3276680
Parameter Units
Oil and Grease mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Matrix: Water
Blank Reporting
Result Limit MDL Analyzed Qualifiers
ND 5.0 1.1 05/25/2118:50
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 31.3 78 78-114
MATRIX SPIKE SAMPLE: 3276681
35633068001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 1.8J 39.2 35.9 87 78-114
SAMPLE DUPLICATE: 3276682
92539234002 Dup
Parameter Units Result Result
Oil and Grease mg1L 6.8 6.1
Max
RPD RPD Qualifiers
11 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/2812021 10:52 AM without the written consent of Pace Analytical Services, LLC, Page 10 of 30

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Project: Newton Instruments / 2112
Pace Project No.: 92538713
QC Batch: 622447
QC Batch Method: EPA 245.1 Rev 3.0 1994
Associated Lab Samples: 92538713001
METHOD BLANK: 3274974
Associated Lab Samples: 92538713001
Parameter Units
Mercury ug/L
LABORATORY CONTROL SAMPLE: 3274975
Parameter Units
Mercury ug/L
QUALITY CONTROL DATA
Analysis Method: EPA 245.1 Rev 3.0 1994
Analysis Description: 245.1 Mercury
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit
ND 0.20
Spike LCS
Conc. Result
2.5 2.3
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
HuMersville, NC 28078
[phone]
MDL Analyzed Qualifiers
0.12 05/25/2112:50
LCS % Rec
% Rec Limits Qualifiers
92 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3274976 3274977
MS MSD
92538634001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2.5 2 3 2.3 93 93 70-130 0 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3274978 3274979
MS MSD
92538713001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conic. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2 5 2.3 2.4 92 94 70-130 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the resuM.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 30

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QUALITY CONTROL DATA
Project: Newton Instruments 12112
Pace Project No.: 92538713
QC Batch: 622085 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 2D0.7 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92538713001
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
METHOD BLANK: 3272875
Associated Lab Samples: 92538713001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
MDL
Analyzed Qualifiers
Antimony
ug1L
ND
5.0
3.0
05/2212121:39
Arsenic
ug1L
ND
10.0
4.7
0512212121:39
Beryllium
ug1L
ND
1.0
0.70
05122/2121:39
Cadmium
ug1L
ND
1.0
0.40
05122/2121:39
Chromium
ug1L
ND
5.0
3.7
05122/2121:39
Copper
ug1L
ND
5.0
4.3
0512212121:39
Lead
ug1L
ND
5.0
4.5
0512212121:39
Nickel
ug1L
ND
5.0
3.5
05/2212121:39
Selenium
ug1L
ND
10.0
4.7
05122/2121:39
Silver
ug1L
ND
5.0
2.5
05122/2121:39
Thallium
ug1L
ND
10.0
8.1
05122/2121:39
Zinc
ug1L
ND
10.0
9.5
05/22/2121:39
LABORATORY CONTROL SAMPLE:
Parameter
3272876
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug1L
500
474
95
85-115
Arsenic
ug1L
500
478
96
85-115
Beryllium
uglL
500
493
99
85-115
Cadmium
ug1L
500
491
96
85-115
Chromium
ug1L
500
484
97
85-115
Copper
ug1L
500
490
98
85-115
Lead
ug1L
500
480
96
85-115
Nickel
ug1L
500
482
96
85-115
Selenium
ug1L
5D0
466
93
85-115
Silver
ug1L
250
242
97
85-115
Thallium
ug1L
500
477
95
85-115
Zinc
ug1L
500
478
96
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3272877
3272878
MS
MSD
92538551001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Cone.
Result
Result
% Rec
% Rec
Limits RPD
RPD Qual
Antimony
uglL
ND
500
500
476
483
95
96
70-130 1
20
Arsenic
ug1L
ND
500
500
479
484
95
96
70-130 1
20
Beryllium
ug1L
ND
500
500
488
496
98
99
70-130 2
20
Cadmium
uglL
ND
500
500
488
495
98
99
70-130 1
20
Results presented on this page
are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result -
REPORT OF LABORATORY ANALYSIS
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Date: 05128/2021 10:52 AM without the written consent of Pace Analytical Services. LLC
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersvi1e. NC 28078
[phone]
Project:
Pace Project No.:
Newton Instruments 12112
92538713
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3272877
3272878
MS
MSD
92538551001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Chromium
ug/L
0.0052
500
500
497
503
98
100
70-130
1
20
mg/L
Copper
ug/L
0.015
500
500
510
516
99
100
70-130
1
20
mg/L
Lead
ug/L
ND
500
500
479
485
95
96
70-130
1
20
Nickel
ug/L
ND
500
500
483
489
96
98
70-130
1
20
Selenium
ug/L
ND
500
500
485
492
97
98
70-130
1
20
Silver
ug/L
ND
250
250
242
244
97
98
70-130
1
20
Thallium
ug/L
ND
500
500
466
475
93
95
70-130
2
20
Zinc
ug/L
0,073
500
500
565
571
98
100
70-130
1
20
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3272879
MS
92538803002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3272880
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
Antimony
ug/L
ND
500
500
469
472
94
94
70-130
1
20
Arsenic
ug1L
ND
500
500
470
468
94
93
70-130
0
20
Beryllium
ug/L
ND
500
500
483
483
97
97
70-130
0
20
Cadmium
ug/L
ND
500
500
476
478
95
96
70-130
1
20
Chromium
ug/L
ND
500
500
479
432
96
96
70-130
1
20
Copper
ug/L
ND
500
500
478
484
95
96
70-130
1
20
Lead
uglL
ND
500
500
467
471
93
94
70-130
1
20
Nickel
ug/L
ND
500
500
471
474
94
95
70-130
1
20
Selenium
ug/L
ND
500
500
481
486
96
97
70-130
1
20
Silver
ug/L
ND
250
250
235
237
94
95
70-130
1
20
Thallium
ug/L
ND
500
500
454
455
90
91
70-130
0
20
Zinc
ug/L
16.3
500
500
502
504
97
98
70-130
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report sha11 not be reproduced, except in full,
Date: 05128/2021 10:52 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Newton Instruments 12112
Pace Project No.: 92538713
QC Batch: 620596
QC Batch Method: EPA 624 1
Associated Lab Samples: 92538713001
Analysis Method:
Analysis Description:
Laboratory:
EPA624.1
624 MSV with Acrolein
Pace Analytical Services - Charlotte
METHOD BLANK: 3265338
Matrix: Water
Associated Lab Samples- 92538713001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
1,11-Trichloroethane
ug1L
NO
2.0
0.43
0511412114:06
1,1,2,2-Tetrachloroethane
ug1L
NO
2.0
0.30
0511412114:06
1,1,2-Trichloroethane
ug1L
ND
2.0
0.38
0511412114:06
1,1-Dichloroethane
uglL
ND
2.0
0.47
05/14/21 14:06
1,2-Dichloroethane
ug1L
ND
2.0
0.42
05114/2114:06
1.2-Dichloropropane
uglL
NO
2.0
0.44
05114/2114:06
2-Chloroethylvinyl ether
uglL
ND
5.0
0.94
05114/21 14:06
Acrolein
uglL
ND
5.0
3.6
05114/2114:06
Acrylonitdle
ug1L
ND
5.0
2.3
0511412114:06
Benzene
uglL
ND
1.0
0.42
05114/2114:06
BromOdiGhloromethane
ug1L
NO
2.0
0.41
05/14/21 14:06
Bromoform
ug1L
ND
2.0
0.59
05114/2114:06
Bromomethane
uglL
ND
2.0
1.5
05114/2114:06
Carbon tetrachloride
ug1L
ND
2.0
0.47
05/14/21 14:06
Chlorobenzene
uglL
ND
2.0
0.39
05/14/21 14:06
Chloroethane
ug1L
ND
2.0
0.71
05114/2114:06
Chloroform
uglL
ND
2.0
0.49
05/14/21 14:06
Chloromethane
ug1L
ND
2.0
0.60
05114/2114:06
cis-1,3-Dichloropropene
ug1L
ND
2.0
0.35
0511412114:06
Di b romochloro methane
ug1L
ND
2.0
0.39
05/14/21 14:06
Ethylbenzene
uglL
N❑
1.0
0.35
05/14/21 14:06
Methylene Chloride
uglL
NO
2.0
0.91
05/14/21 14:06
Tetrachloroethene
uglL
ND
2 0
0.38
05/14/21 14:06
Toluene
uglL
ND
1.0
0.41
05/14/21 14:06
trans-12-Dichloroethene
uglL
ND
2.0
0.48
05/14/2114:06
trans- 1.3-Dichloropropene
uglL
ND
2.0
0.34
05/14/21 14:06
Trichloroethene
uglL
NO
2.0
0.41
05/14/21 14:06
Vinyl chloride
uglL
ND
2.0
0.41
05/14/21 14:06
1,2-Dichloroethane-d4 (S)
%
98
70-130
05/14/21 14:06
4-Bromofluorobenzene (S)
%
101
70-130
05/14/21 14:06
Toluene-d8 (S)
%
98
70-130
05/14/21 14:06
LABORATORY CONTROL SAMPLE: 3265339
Pace Analytical Services, LLC
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,11-Trichloroethane
uglL
20
19.9
99
70-130
1,1,2,2-Tetrachloroethane
uglL
20
19.1
96
70-130
1,1,2-Trichloroethane
uglL
20
20.2
101
70-130
1,1-Dichloroethane
uglL
20
19.4
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05128/2021 10:52 AM without the written consent of Pace Analytical Services. LLC
Page 14 of 30

aceAnalytical "
wwtrpacetatucom
QUALITY CONTROL DATA
Project: Newton Instruments / 2112
Pace Project No.: 92538713
LABORATORY CONTROL SAMPLE: 3265339
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,2-Dichloroethane
ug/L
20
19.3
96
70-130
1,2-Dichloropropane
ug/L
20
20.2
101
70-130
2-Chloroethylvinyl ether
ug/L
40
30.7
77
67-130
Acrolein
ug/L
100
123
123
60-M
Acrylonitrile
ug/L
100
94.2
94
70-130
Benzene
ug/L
20
20.6
103
70-130
Bromodichloromethane
ug/L
20
18.9
95
70-130
Bromoform
ug/L
20
18.9
94
70-130
Bromomethane
ug/L
20
25.8
129
30-177
Carbon tetrachloride
ug/L
20
21.8
109
70-130
Chlorobenzene
ug/L
20
20.8
104
70-130
Chloroethane
ug/L
20
19.1
95
46-131
Chloroform
ug/L
20
20.1
101
70-130
Chloromethane
ug/L
20
19.1
95
49-130
cis-1,3-Dichloropropene
ug/L
20
18.9
95
70-130
Dibromochloromethane
ug/L
20
19.7
99
70-130
Ethylbenzene
ug/L
20
20.8
104
70-130
Methylene Chloride
ug/L
20
19.1
96
68-130
Tetrachloroethene
ug/L
20
20.8
104
70-130
Toluene
ug/L
20
19.6
98
70-130
trans-1.2-Dichloroethene
ug/L
20
20.2
101
70-130
trans-1,3-Dichloropropene
ug/L
20
17.8
89
70-130
Tichloroethene
ug/L
20
21.3
107
70-130
Vinyl chloride
ug/L
20
18.7
93
59-142
1,2-Dichloroethane-d4 (S)
%
94
70-130
4-Bromoftuorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3265340
3265341
MS
MSD
92538568001
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc. Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Quai
1,1,1-Tdchloroethane
ug/L
ND
20
20
23.9
22.4
119
112
70-148
7
21
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.6
20.1
113
101
70-131
12
30
1,1,2-Tdchloroethane
ug/L
ND
20
20
23.1
21.6
116
108
70-136
7
27
1, 1 -DicHoroethane
ug/L
ND
20
20
22.9
21.7
114
108
71-143
5
30
1,2-Dichloroethane
ug/L
ND
20
20
22.0
21.3
110
106
72-137
3
29
1,2-Dichloropropane
ug/L
ND
20
20
23.9
22.2
120
111
70-138
8
30
2-Chtoroethylvinyl ether
ug/L
ND
40
40
34.0
32.5
85
81
10-200
5
32
Acrolein
ug/L
ND
100
100
65.8
76.0
66
76
50-150
14
30
Acrylonitdle
ug/L
ND
100
100
108
97.4
108
97
68-140
11
30
Benzene
ug/L
ND
20
20
24.3
22.7
121
114
75-125
6
30
Bromodichloromethane
ug/L
ND
20
20
23.1
21.1
115
106
70-138
9
30
Bromoform
ug/L
ND
20
20
22.5
20.0
112
100
57-138
12
25
Bromomethane
ug/L
ND
20
20
21.2
23.1
106
115
10-200
9
35
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 30

_ _ ?ceAnaVical'
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9B00 KinceyAve. Suite 100
Huntersville. NC 28078
[phone]
Project: Newton Instruments 12112
Pace Project No.: 92538713
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3265340
3265341
MS
MSD
92538568001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Cone.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Carbon tetrachloride
ug/L
ND
20
20
25.8
24.4
129
122
70-125
6
26 M1
Chlorobenzene
ug/L
ND
20
20
24.7
22.3
124
111
82-137
10
29
Chloroethane
ug/L
ND
20
20
22.8
22.4
114
112
51-166
2
30
Chloroform
ug/L
ND
20
20
24.2
22.6
119
111
70-121
7
30
Chloromethane
ug1L
ND
20
20
20.3
19.0
101
95
24-161
6
30
cis- 1,3-Dichloropropene
ug1L
ND
20
20
22.0
20.3
110
101
70-142
8
30
Di b romochloro methane
ug/L
ND
20
20
24.1
21.4
121
107
69-133
12
30
Ethylbenzene
ug/L
ND
20
20
24.9
22.4
125
112
75-134
11
30
Methylene Chloride
ug1L
ND
20
20
21.6
20.0
108
100
64-148
8
30
Tetrachloroethene
ug1L
ND
20
20
25.0
22A
125
112
70-133
11
23
Toluene
ug/t_
ND
20
20
23.7
22.1
117
109
75-134
7
22
trans- l.2-Dichloroethene
ug1L
ND
20
20
23.9
22.3
120
111
70-143
7
27
trans- 1,3-Dichloropropene
ug1L
ND
20
20
20.6
19.6
103
98
70-13B
5
30
Tfichloroethene
ug1L
ND
20
20
25.5
23.5
127
117
75-138
8
29
Vinyl chloride
ug1L
ND
20
20
22.6
21.0
113
105
55-172
7
30
1,2-❑ichloroethane-d4(S)
%
97
93
70-130
4-Bromofluorobenzene (S)
%
100
97
70-130
Toluene-0 (S)
%
98
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full.
Date: 05/2812021 10:52 AM without the written consent of Pace Analytical Services, LLC
Page 16 of 30

1�?ceAnalyfical
www.pacelaKeom
QUALITY CONTROL DATA
Project: Newton Instruments 12112
Pace Project No.: 92538713
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 620767
OC Batch Method: EPA608.3
Associated Lab Samples: 92538713001
Analysis Method: EPA608 3
Analysis Description 608 PCB Pest Red Vol
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK 3266119
Matrix:
Water
Associated Lab Samples: 92538713001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
4,4'-DDD
ug/L
ND
0.050
0.012
05/19/2116-53
4,4'-DOE
ug/L
ND
0.050
0.016
0511912116:53
4.4'-DDT
ug/L
ND
0.050
0.048
05/19/21 16:53
Aldrin
ug/L
ND
O.D50
0.026
05/1912116:53
alpha-BHC
ug/L
ND
0,050
0.026
05/19/21 16:53
alpha -Chlordane
ug/L
ND
0.050
0.015
05/19/2116-53
beta-BHC
ug/L
ND
0.050
0.022
05/1912116:53
Chlordane (Technical)
ug/L
ND
0.50
0.21
05/19/21 16:53
delta-BHC
ug/L
ND
0.050
0.018
05/19/21 16:53
Dieldrin
ug/L
ND
0.050
0.013
05/1912116:53
Endosulfan I
ug/L
ND
0.050
0.014
05/19/21 16:53
Endosulfan II
ug/L
ND
0,050
0.017
05/19/21 16:53
Endosulfan sulfate
ug/L
ND
0,050
0.014
05/19/21 16:53
Endrin
ug/L
ND
0,050
0.014
05/1912116:53
Endrin aldehyde
ug/L
ND
0.050
0.028
05/19/21 16:53
gamma-BHC (Lindane)
ug/L
ND
0.050
0.020
05/19121 16:53
gamma -Chlordane
ug/L
ND
0,050
0.035
0511912116:53
Heptachlor
ug/L
ND
0.050
0.036
05/19/21 16:53
Heptachlor epoxide
ug/L
ND
0.050
0.015
05/19/21 16:53
PCB-1016 (Arodor 1016)
ug/L
ND
0.50
0.47
05/19121 16:53
PCB-1221 (Arodor 1221)
ug/L
ND
0,50
0.45
05/19/21 16:53
PCB-1232 (Arodor 1232)
ug/L
ND
0.50
0.36
05/19/21 16:53
PCB-1242 (Arodor 1242)
ug/L
ND
0.50
0.26
05/19/21 16:53
PCB-1248 (Arodor 1248)
ug/L
ND
0.50
0.40
05/19/21 16:53
PCB-1254 (Arodor 1254)
ug/L
ND
0.50
0.25
05/19121 16:53
PCB-1260 (Arodor 1260)
ug/L
ND
0.50
0.42
05/19/21 16:53
Toxaphene
ug/L
ND
0.50
0.27
0511912116:53
Decachlorobiphenyl IS)
%
B6
10-184
05/19/21 16:53
Tetrachloro-m-xylene (S)
%
84
10-154
05/19/21 16:53
LABORATORY CONTROL SAMPLE:
Parameter
3266120
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4.4'-DDD
ug/L
0,25
0.25
100
45-141
4,4'-DDE
ug/L
0.25
0.22
87
37-141
4,4'-DDT
ug/L
0,25
0.16
66
52-160
Aldrin
ug/L
0,25
0.16
65
42-130
alpha-BHC
ug/L
0.25
0.20
79
37-139
alpha -Chlordane
ug/L
025
0.21
84
45-139
Results presented on this
page are in the units indicated by the "Units"
column except
where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:52 AM without the written consent of Pace Aralytical Services, LLC.
Page 17 of 30

w
aceAnaIXical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Newton Instruments/ 2112
Pace Project No.: 92538713
LABORATORY CONTROL SAMPLE:
Parameter
3266120
Units
Spike
Conc.
LCS
Result
beta-BHC
ug/L
0.25
0.25
delta-BHC
ug/L
0.25
0.22
Dieldrin
ug/L
0.25
0.22
Endosulfan I
ug/L
0.25
0.20
Endosulfan 11
ug/L
0.25
0.21
Endosulfan sulfate
ug/L
0.25
0.22
Endrin
uglL
0.25
0.23
Endrin aldehyde
ug/L
0.25
0.17
gamma-BHC (Lindane)
ug/L
0.25
0.20
gamma -Chlordane
ug/L
0.25
0.22
Heptachlor
ug/L
0.25
0.21
Heptachlor epoxide
ug/L
0.25
0.21
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
LCS
% Rec
%u Rec
Limits
100 39-147
87 39-140
86 40-146
79 45-145
85 47-153
88 48-144
90 41-147
67 45-146
82 42-140
88 45-140
83 34-135
85 39-142
93 10-184
82 10-154
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE:
3266121
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
5 3.8 76
50-137
PCB-1260 (Aroclor 1260)
ug/L
5 4.3 85
42-140
Decachlorobiphenyl (S)
%
85
10-184
Tetrachloro-m-xylene (S)
%
70
10-154
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3266122 3266123
MS
MSD
92538041001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
4,4'-DDD
ug1L
ND
0.25
0.25
0.25
0.27
100
107
36-141
6
39
4,4'-DDF
ug/L
ND
0.25
0.25
0.17
0.17
68
69
31-145
1
35
4,4'-DDT
ug/L
ND
0.25
0.25
0.27
0.24
it()
96
25-160
13
42
Aidrin
ug1L
ND
0.25
0.25
0.25
0.24
99
96
42-140
3
35
aipha-BHC
ug/L
ND
0.25
0.25
0.18
0.18
71
71
37-140
0
36
alpha -Chlordane
ug1L
ND
0.25
0.25
0.19
0.20
76
79
45-140
3
35
beta-BHC
ug/L
ND
0.25
0.25
0.24
0.25
95
101
30-147
6
44
delta-BHC
ug/L
ND
0.25
0.25
0.16
0.18
66
73
32-140
10
52
Dieldrin
ug/L
ND
0.25
0.25
0.18
0.18
70
72
36-146
3
49
Endosulfan I
ug/L
ND
0.25
0.25
0.16
0.16
62
65
45-153
4
28
Endosulfan II
ug/L
ND
0.25
0.25
0.16
0.17
66
68
27-176
3
53
Endosulfan sulfate
ug/L
ND
0.25
0.25
0.16
D.15
62
61
31-144
2
38
Endrin
ug/L
ND
0.25
0.25
0.18
0.18
73
72
30-147
1
48
Endrin aldehyde
ug/L
ND
0.25
0.25
ND
ND
11
6
16-177
30 M1
gamma-BHC (Lindane)
ug/L
ND
0.25
0.25
0.18
D.19
71
74
32-140
4
39
gamma -Chlordane
ug1L
ND
0.25
0.25
0.32
0.33
129
134
45-140
3
35
Heptachlor
ug/L
ND
0.25
0.25
0.17
0.23
66
91
34-140
31
43
Results presented on this page
are in the units indicaled 4y the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:52 AM without the written consent of Pace Analytical Services. LLC.
Page 18 of 30

aceAnalXical
WWw.pdtala63.cUm
QUALITY CONTROL DATA
Project: Newton Instruments 12112
Pace Project No.: 92538713
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 3266122
3266123
MS
MSD
92538041001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc
Conc
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Heptachlor epoxide
ug/L
ND
0.25
0.25
0.18
0.19
71
75
37-142
5 26
Decachlorobiphenyl (S)
%
64
67
10-184
Tetrachloro-m-xylene (S)
%
68
71
10-154
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3266124
3266125
MS
MSD
92538041001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
PC8-1016 (Arodor 1016)
ug/L
ND
5
5
6.6
4.7
133
94
50.140
34 36
PCB-1260 (Arodor 1260)
ug/L
ND
5
5
3.8
3.5
76
70
42-140
8 38
Decachlorobiphenyl (S)
%
101
70
10-184
Tetrachloro-m-xylene (S)
%
84
71
10-154
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05128/2021 10:52 AM without the written consent of Pace Analytical Services. LLC
Page 19 of 30

acmnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Newton Instruments 12112
Pace Project No.: 92538713
QC Batch: 621048
Analysis Method:
EPA625.1
QC Batch Method: EPA625.1
Analysis Description:
625 MSS
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92538713001
METHOD BLANK( 3267555
Matrix Water
Associated Lab Samples: 92538713001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
1.7
05118/2117:07
1,2-Dichlorabenzene
ug/L
NO
5.0
1.8
05/1812117:07
1,2-Diphenylhydrazine
ug/L
ND
5.0
1.6
05/1812117:07
1,3-Diohlorobenzene
ug/L
ND
5.0
1.6
D511812117.07
1,4-DicNorobenzene
ug/L
ND
5.0
1.7
0511812117:07
2.4.6-Trtchlorophenol
ug/L
ND
10.0
1.6
05/18/21 17:07
2,4-Dichlorophenol
ug/L
NO
5.0
1.4
0511812117:07
2.4-Dimethylphenol
ug/L
NO
10.0
1.7
0511812117:07
2,4-Di nitro phenol
uglL
NO
5D 0
26.0
05/18/21 17:07
2,4-Dinitrotoluene
ug/L
ND
5.0
1.6
05118/2117:07
2,6-Dinitrotoluene
ug/L
ND
5.0
1.7
05/1812117:07
2-Chloronaphihalene
ug/L
ND
5.0
1.7
05/18/21 17:07
2-Chlorophenol
ug/L
ND
5.0
1.2
0511812117:07
2-Nitrophenol
ug/L
ND
5.0
1.4
0511812117:07
3,3'-DichIorobenzidine
ug/L
ND
10.0
8.1
05/18/21 17:07
4,6-Dinitro-2-methy IphenaI
ug/L
ND
100
3A
05/18/21 17-07
4-Bromophenylphenyl ether
ug/L
ND
5.0
1.8
05118/21 17:07
4-Chloro-3-methylphenol
ug/L
NO
5.0
3.3
05/1812117:07
4-Chlorophenylphenyl ether
ug/L
ND
5.0
2.0
05/18/21 17:07
4-Nitrophenol
ug/L
ND
100
6.6
05118/21 17:07
Acenaphthene
ug/L
NO
5.0
2.0
05/18/21 17:07
Acenaphthylene
ug/L
ND
5.0
2.0
05/18/21 17:07
Anthracene
ug/L
ND
5.0
2.3
05/1812117:07
Benzidine
ug/L
NO
50.0
13.4
0511812117.07
Benzo(a)anthracene
uglL
ND
5.0
2.7
05118/2117:07
Benzo(a)pyrene
ug/L
ND
5.0
2.8
0511812117:07
Benzo(k)fluoranthene
ug/L
ND
5.0
2.6
05/1812l 17:07
Benzo(g.h.i)perylene
ug/L
ND
5.0
2.8
05/18/21 17:07
Benzo(k)fluoranthene
ug/L
ND
5.0
2.7
05118/2117:07
bis(2-Chloroethoxy)melhane
ug/L
NO
10.0
1.8
05/1812117:07
bis(2-Chloroethyl) ether
ug/L
NO
5 0
1.9
05/18/21 17:07
bi s(2-Ethylhexyl) phthal ate
ug/L
NO
5.0
3.7
05/1812117:07
Butyl benzylphthalate
ug/L
NO
5.0
3.1
05/1812117:07
Chrysene
ug/L
ND
5.0
2.8
0511812117:07
Di-n-butylphthalate
ug/L
ND
5.0
2.2
0511812117:07
Di-n-octylphth a late
ug/L
ND
5.0
3.9
05/18/21 17:07
Dibenz(a,h)anthracene
ug/L
ND
5.0
3.0
05/18/2117:07
Diethyl phthalate
ug/L
NO
5.0
2.0
0511812117:07
Dimethylphthalate
ug/L
NO
5.0
2.1
0511812117:07
Fluoranthene
ug/L
NO
5 0
2.2
05/18/21 17:07
Pace Analytical Services, LLC
9800 KinceyAve_ Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05128/2021 10:52 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 30

Pace Analytical Services, LLC
aceAnalytical
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
www.pacelabsxom
[phone]
QUALITY CONTROL DATA
Project: Newton Instruments / 2112
Pace Project No.: 92538713
METHOD BLANK: 3267555
Matrix: Water
Associated Lab Samples: 92538713001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Fluorene
ug/L
ND
5.0
2.1
05/1812117:07
Hexachloro-1,3-butadiene
ug/L
ND
5.0
1.8
0511812117:07
Hexachlorobenzene
ug/L
ND
5.0
2.2
05118/2117:07
Hexachlorocyclopentadiene
ug/L
ND
10.0
1.6
05118/2117:07
Hexachloroethane
ug/L
ND
5.0
1.4
05118/2117:07
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
2.9
05118/2117:07
Isophorone
ug/L
ND
10.0
1.7
05118/2117:07
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
1.3
05/18/2117:07
N-Nitrosodimethylamine
ug/L
ND
5.0
1.9
05118/2117:07
N-Nitrosodiphenylamine
ug/L
ND
10.0
3.0
05/18/2117:07
Naphthalene
ug/L
ND
5.0
2.1
05/18/2117:07
Nitrobenzene
ug/L
ND
5.0
1.9
05/18/2117:07
Pentachlorophenol
ug/L
ND
10.0
3.8
05/18/2117:07
Phenanthrene
ug/L
ND
5.0
2.0
05/18/2117:07
Phenol
ug/L
ND
5.0
1.4
05/18/2117:07
Pyrene
ug/L
ND
5.0
2.2
05/1842117:07
2,4,6-Tdbromophenol (S)
%
142
10-137
05/1821 17:07 S3
2-Fluorobiphenyl (S)
%
107
15-120
0511821 17:07
2-Fluorophenol (S)
%
94
10-120
05/1821 17:07
Nitrobenzene-d5 (S)
%
119
10-120
0511821 17:07
Phenol-d6 (S)
%
76
10-120
05/1821 17:07
Terphenyl-d14 (S)
%
114
11-131
05/1821 17:07
LABORATORY CONTROL SAMPLE: 3267556
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
1,2,4-Tdchlorobenzene
ug/L
50
46.1
92
44-142
1,2-Dichlorobenzene
ug/L
50
42.7
85
32-129
1,2-Diphenylhydrazine
ug/L
50
64.9
130
25-150
1,3-Dichlorobenzene
ug/L
50
41.5
83
1-172
1,4-Dichlorobenzene
ug/L
50
42.6
85
20-124
2,4,6-Tdchlorophenol
ug/L
50
74.5
149
37-144 L1
2,4-Dichlorophenol
ug/L
50
74.0
148
1-191
2,4-Dimethylphenol
ug/L
50
75.9
152
32-119 L1
2,4-Dinitrophenol
ug/L
250
367
147
1-181
2,4-Dinitrotoluene
ug/L
50
65.9
132
39-139
2,6-Dinitrotoluene
ug/L
50
69.1
138
50-158
2-Chtoronaphthalene
ug/L
50
57.8
116
60-118
2-Chlorophenol
ug/L
50
65.7
131
23-134
2-Nitrophenol
ug/L
50
76.0
152
29-182
3,3'-Dichtorobenzidine
ug/L
100
139
139
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
153
153
1-181
4-Bromophenylphenyl ether
ug/L
50
68.6
137
53-127 L1
4-Chloro-3-rttethylphenol
ug/L
100
142
142
22-147
Results presented on this page are in the units
Indicated by the "units"
column except where an alternate
unit Is
presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05128/2021 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 30

aceAnaV cal
www.paceiabs.com
QUALITY CONTROL DATA
Project: Newton instruments 12112
Pace Project No.: 92538713
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
3267556
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4-Chlorophenylphenyl ether
uglL
50
63.8
128
25-158
4-Nitrophenol
uglL
250
247
99
1-132
Acenaphthene
ug1L
50
63.0
126
47-145
Acenaphthylene
ug1L
50
64.9
130
33-145
Anthracene
ug1L
50
69.0
138
1-166
Benzidine
ug1L
100
15.2J
15
10-130
Senzo(a)anthracene
ug1L
50
70.9
142
33-143
Benzo(a)pyrene
uglL
50
68.3
137
17-163
Benzo(b)fluoranthene
uglL
50
66.8
134
24-159
Benzo(g,h,i)perylene
ug1L
50
74.7
149
1-219
Benzo(k)fluoranthene
ug1L
50
67.6
135
11-162
bis(2-Chloroethoxy)methane
ug1L
50
64.8
130
33-184
bis(2-Chloroethyl) ether
ug1L
50
65.6
131
12-158
bis(2-Ethylhexyl) phthal ate
ug1L
50
80.1
160
8-158 L1
Butylbenzylphthalate
ug1L
50
77.4
155
1-152 L1
Chrysene
ug1L
50
68.7
137
17-168
Di-n-butylphthalate
ug1L
50
73.0
146
1-118 L1
Di-n-octylphthalate
ug1L
50
85.8
172
4-146 L1
Dibenz(a,h)anthracene
ug1L
50
76.3
153
1-227
Diethyl phlhalate
ug1L
50
64.1
128
1-114 L1
Dimethylphthalate
ug1L
50
63.2
126
1-112 L1
Fluoranthene
ug1L
50
71.3
143
26-137 L1
Fluorene
ug1L
50
66.1
132
59-121 L1
Hexachloro-1,3-1)utadiene
ug1L
50
41.1
82
24-116
Hexachlorobenzene
ug1L
50
63.2
126
1-152
Hexachlorocyclopentadiene
ug1L
50
41.6
83
25-150
Hexachloroethane
ug1L
50
39.9
80
40-113
Indeno(1,2,3-cd)pyrene
ug1L
50
75,6
151
1-171
Isophorone
ug1L
50
61.0
122
21-196
N-Nitroso-di-n-propylamine
ug1L
50
59.3
119
1-230
N-Nitrosodimethylamine
ug1L
50
55.5
111
25-150
N-Nitrosodiphenylamine
uglL
50
69.2
138
25-150
Naphthalene
uglL
50
53.1
106
21-133
Nitrobenzene
ug1L
50
62.6
125
35-180
Pentachlorophenol
uglL
100
164
164
14-176
Phenanthrene
ug1L
50
67.8
136
54-120 L1
Phenol
ug1L
50
49.5
99
5-112
Pyrene
ug11-
50
66.3
133
52-115 L1
2,4,5-Tribromophenol (S)
%
142
10-137 SO
2-Fluorobiphenyl (S)
%
106
15-120
2-Fluorophenol (S)
%
96
10-120
Nitrobenzene-d5 (S)
%
119
10-120
Phenol-d6 (S)
%
78
10-120
Terphenyl-d14 (S)
%
120
11-131
Resutts presented an this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 30

aceAnalytrcal
- www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments 12112
Pace Project No.: 92538713
MATRIX SPIKE & MATRIX SPIKE DUPLICATE. 3267557
3267558
MS
MSD
35632710001
Spike
Spike
MS
MSD MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits
RPD
RPD Qual
12,4-Trichlorobenzene
ug/L
8.6U
50
50
19.1J
15.8J
38
32
44-142
30 M1
1,2-Dichlorobenzene
ug/L
9.01-1
50
50
18,4J
15.6J
37
31
32-129
30 M1
1,2-Diphenylhydrazine
ug/L
8.01-1
50
50
23 9J
23.8J
48
48
25-150
30
1.3-Dichlorobenzene
ug/L
8AU
50
50
16.9J
15.3J
34
31
1-172
30
1,4-Dichlorobenzene
ug/L
8AU
50
50
18.11
15.13J
36
32
20-124
30
2,4,6-Trichlorophenol
ug/L
7.81-1
50
50
27AJ
26.7J
54
53
37-144
30
2,4-Dichlorophenol
uglL
7.OU
50
50
27.7
25.8
55
52
1-191
7
30
2.4-Dimethylphenol
ug/L
8.51-1
50
50
27.8J
25.6J
56
51
32-119
30
2.4-Dinitrophenol
ug/L
130U
250
250
ND
NO
0
12
1-181
30 M1
2,4-Dinitrotoluene
ug/L
8.1U
50
50
24.7J
24.OJ
49
48
39-139
30
2,6-Dinitrotoluene
ug/L
8.6U
50
50
22.5J
23.3J
45
47
50-158
30 M1
2-Chloronaphthalene
ug/L
8.6U
50
50
23 7J
21.OJ
47
42
60-118
30 M1
2-Chlorophenol
ug/L
6.OU
50
50
25.6
23.1J
51
46
23-134
30
2-Nitrophenol
ug/L
7.OU
50
50
29.0
24.21
58
48
29-182
30
3,3'-Dichlorobenzidine
ug/L
40.6U
100
100
ND
NO
16
20
1-262
30
4,6-Dinitro-2-methylphenol
ug/L
17.OU
100
100
ND
21.OJ
16
21
1-181
30
4-Bromophenylphenyl ether
ug/L
8.8U
50
50
24AJ
24.5J
49
49
53-127
30 MO
4-Chlaro-3-methylphenol
ug/L
16 7U
100
100
49.4
50.8
49
51
22-147
3
30
4-Chlorophenylphenyl ether
ug/L
10.0U
50
50
24.5J
23.6J
49
47
25-158
30
4-Nitrophenol
ug/L
33.OU
250
250
77,8
82.3
31
33
1-132
6
30
Acenaphthene
ug/L
10.0U
50
50
24.8J
22.7J
50
45
47-145
30 M1
Acenaphthylene
ug/L
9.8U
50
50
25.0
22.8J
50
46
33-145
30
Anthracene
ug/L
11.61-1
50
50
24 9J
25.7
50
51
1-166
30
Benzidine
ug/L
67.OU
100
100
ND
NO
0
0
10-130
30 M1
Benzo(a)anthracene
ug]L
13AU
50
50
24.9J
26.2
50
52
33-143
30
Benzo(a)pyrene
ug/L
13.9U
50
50
23AJ
25.5
46
51
17-163
30
Benzo(b)nuoranihene
ug/L
13.OU
50
50
22.5J
24.7J
45
49
24-159
30
Benzo(g,h,i)perylene
ug/L
14.2U
50
50
25.0
27.7
50
55
1-219
10
30
Benzo(k)Ruo(anthene
ug/L
13.6U
50
50
22.8J
24.1J
46
48
11-162
30
bis(2-
ug]L
9.1U
50
50
25AJ
22.2J
50
44
33-184
30
Chloroethoxy)methane
bis(2-Chloroethyl) ether
ugJL
9.61-11
50
50
27.7
24.3J
55
49
12-158
30
bis(2-Ethylhexyl) p hthal ate
ug/L
18.6U
50
50
24.8J
25.6
50
51
8-158
30
Butyibenzylphthalate
ug/L
15.7U
50
50
25.8
27.9
52
56
1-152
8
30
Chrysene
ug/L
13.8U
50
50
23.7J
26.2
47
52
17-168
30
Di-n-butylphthalate
ug/L
11.0U
50
50
22.7J
24.9J
45
50
1-118
30
Di-n-octylphthalate
ug]L
19.6U
50
50
26.0
29.0
52
58
4-146
11
30
Dibenz(a,h)anthracene
ug/L
14.81J
50
50
252
27.5
50
55
1.227
9
30
Diethyl phthalate
ug/L
10.2U
50
50
23.OJ
23.7J
46
47
1-114
30
Dimethylphthalate
ug/L
10.61-11
50
50
22.8J
22.5J
46
45
1-112
30
Fiuoranthene
ug/L
11.0U
50
50
24 5J
26.1
49
52
26-137
30
Fluorene
ug/L
10.41-1
50
50
25.0
24.2J
50
48
59-121
30 MO
Hexachloro-1.3-butadiene
ug/L
8.8U
50
50
17.3J
14.7J
35
29
24-116
30
Hexachlorobenzene
ug/L
10.81-11
50
50
23.OJ
23.5J
46
47
1-152
30
Hexachlorocyclopentadiene
ug/L
8 OU
50
50
11.5J
10.01
23
20
25-150
30 M1
Hexachloroethane
ug/L
6.9U
50
50
16.6J
14.3J
33
29
40-113
30 M1
Results presented
on this page are in the units
indicated by the "Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 05128/2021 10:52 AM
without the written
consent of Pace
Analytical
Services, LLC,
Page 23 of 30

aceAnalytfical
www.pat:alabs.cam
QUALITY CONTROL DATA
Project: Newton Instruments 12112
Pace Project No.: 92538713
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3267557
MS
35632710001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
Indeno(1,2,3-cd)pyrene
ug/L
14.41-1
50
50
Isophorone
ug/L
8.3U
50
50
N-Nitroso-di-n-propylamine
ug/L
6.6U
50
50
N-Nitrosodimethylamine
ug/L
9AU
50
50
N-Nitrasodiphenylamine
ug/L
15.OU
50
50
Naphthalene
ug/L
10AU
50
50
Nitrobenzene
ug/L
9AU
50
50
Pentachlorophenol
ug/L
18.8U
100
100
Phenanthrene
ug/L
10.0U
50
50
Phenol
ug/L
6.8U
50
50
Pyrene
ug/L
11.0U
50
50
2,4,6-Tribromophenal(S)
%
2-Fluorobiphenyl(S)
%
2-Fluorophenol(S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
3267558
MS
Result
25.4
23.3J
24.2J
22.3J
23.6J
21.8J
27.4
34.9J
24.8J
20.11J
23AJ
Pace Analytical Services, LLC
9800 Kincey Ave_ Suite 100
Huntersville, NC 28078
(704 )875-90 92
MSD
MS
MSD
% Rec
Max
Result
% Rec
% Rec
Limits RPD
RPD Qual
27.7
51
55
1-171 9
30
20.1J
47
40
21-196
30
21.OJ
48
42
1-230
30
19.91
45
4D
25-150
30
24.2J
47
413
25-150
30
18.5J
44
37
21-133
30
24.3J
55
49
35-180
30
42.3J
35
42
14-176
30
26.1
50
52
54-120
30 MO
16.4J
40
33
5-112
30
25.OJ
47
50
52-115
30 MO
43
46
10-137
41
37
15-120
35
30
10-120
50
43
10-120
D3
29
25
10-120
38
42
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:52AM without the written consent of Pace Analytical Services, LLC.
Page 24 of 30

aceAnalytical
www.paeelabs.com
1
Project: Newton Instruments / 2112
Pace Project No.: 92538713
QC Batch: 620922
QC Batch Method: EPA420.4 Rev 1.0 1993
Associated Lab Samples 92538713001
METHOD BLANK: 3267065
Associated Lab Samples: 92538713001
Parameter Units
Phenolics. Total Recoverable mg/L
QUALITY CONTROL DATA
Analysis Method: EPA420.4 Rev 1.0 1993
Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit MDL Analyzed
ND 0,020 0.0076 05/18/2112:27
Pace Analytical Services, t_LC
9800 Kincey Ave, Suite 100
Huntersville. NC 28078
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE: 3267066
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phenolics, Total Recoverable mg/L 0.05 0 051 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3267067 3267068
MS MSD
92538819001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec %fl Rec Limits RPD RPD Quail
Phenolics, Total mg/L ND 0.05 0.05 0.050 0.057 68 83 90-110 14 10 M1,R1
Recoverable
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full.
Date: 05/28/2021 10:52 AM without the written consent of Pace Analytical Services. LLC,
Page 25 of 30

aceAnaIXical"
www.pacelabs.com
QUALITY CONTROL DATA
Project: Newton Instruments 12112
Pace Project No.: 92538713
QC Batch: 621281 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92538713001
Pace Analytical Services, LLC
9800 Kinoey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 3269128 Matrix: Water
Associated Lab Samples: 92538713001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Cyanide mg/L ND 0.0080 0.0060 05/20/2120:05
LABORATORY CONTROL SAMPLE: 3269129
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Cyanide mg/L 0.1 0.10 103 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3269154 3269155
MS MSD
92539018004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide mg/L ND 0.1 0.1 0.10 0.10 102 101 80-120 1 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3269156 3269157
MS MSD
92539018011 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide mg/L ND 0.1 0.1 0.088 0.091 88 91 80-120 3 10
Results presented on this page are to the units Indicated by the "Units" column except where an alternate unit is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:52 AM without the written consent of Pace Analytical Services, I.I.C.
Page 26 of 30

1�;a'ceAnalytical'
WWW.pacalabstam
QUALIFIERS
Project: Newton Instruments / 2112
Pace Project No.: 92538713
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-90 92
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
Aseparate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonilrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits
IL This analyte exceeded secondary source verification criteria low for the initial Calibration. The reported results should be
considered an estimated value.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M0 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 30

1�;a'ceAnalXical'
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Newton Instruments 12112
92538713
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92538713001
Outfall-001
SM 2540D-2011
620784
92538713001
O utfal I-001
92538713001
Outfall-001
EPA 1664E
622846
92538713001
Outfall-001
EPA608.3
620767
EPA608.3
621019
92538713001
Outfall-001
EPA200.7 Rev 4.4 1994
622085
EPA200.7 Rev 4.4 1994
622302
92538713001
Outfall-001
EPA245.1 Rev 3.01994
622447
EPA245.1 Rev 3.01994
622486
92538713001
Outfall-001
EPA625.1
621048
EPA625A
621329
92538713001
Outfall-001
EPA 624.1
620596
92538713001
Outfall-001
EPA420.4 Rev 1.0 1993
620922
EPA420.4 Rev 1.0 1993
621042
92538713001
Outfall-001
SM 4500-CN-E-2011
621281
SM 4500-CN-E-2011
621609
Date: 05128/2021 10:52 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC,
Page 28 of 30

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Page 29 of 30

Name: �Oocument Revised: October 28, 2020
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Document No.:
'Check nhark top half of box If pH and/or dechlorinaton Is
verified and within the acceptance range for preservation
samples.
Ee;egtfons: VOA,Coliform, MC, Oil and Grease, DRO/Bois (water) Doc, Wig
Pace carounas Ouanty Office 1
Prole WO# : 92538713
PM: TIH Due Date: 05/27/21
CLIENT: 82—PIED GEOL
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Page 30 of 30