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AN M-W�
Stormwater Discharge Dutfall (SDD)
Qualitative Monitoring Report
For guidance onfilling out this form, please visit: httu://uortal ncdenr org web/wq/wSu npdessw#ta 4
Permit, No.: N
Facility Name:
County: Ma
Date of Inspection:
Time of Inspection:
or Certificate of Coverage No.:
-ARC
f4aI e -#-V & % &2 'T�
Total Event Precipitation (inches):
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
2' Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
I
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
l ' and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
1 prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter 3
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
Pagel of 2

Ck
1. Outfall Description:
Outfall No. A IStructure
Receiving Stream:
,De�sscribe the industrial
UP. t
ditch, etc.),
occur within the outfall drainage area:
TNA AA&
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): MV n .0
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
C 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 1D 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 0 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes Ce
9. is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2

am, MA :
MWORD
qpl-
Qualitative MonitoringReport
For guidance on filling out this form, please visit. hM2://12ortal ncdenr or /web/""`w!gJws/su, clessw#tab 4
Permit No.: g/ _g1_3101NI&1.0/ or Certificate of Coverage No.: Facility Name: 1's c�c�n 'P`A� �, s r �,.�& e .M e . --%- -JA/-V
County; L Phone No. 70Y—''�',
Date of inspection:"/3
Time of Inspection: ID , it D f :n
Total Event Precipitation inches
Was this a "Representative_ Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event"or "measureablestorm event" (requirements vary, depending on the permit).
' Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
j performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
j 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
Prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office. j
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Page 1 of 2

1. Outfall Description:
Outfall No. --AAL2—_ Structure (pipe, ditch, etc.) 7; Q r.
Receiving Stream-:"' �(}�;,.\ �, P'1JL _ 1--V
Describe the industrial activities at occur within the outfall drainage area:. ,moo _: t
J
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (he., smells strongly of oil,
weak chlorine odor, etc.): A3 in
4. Clarity: Choose the number which best describes the clarityof the
clear and 5 is very cloudy: discharge, where 1 is
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
C'N 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2

SWPPP Form 3: Rain Event Data
This form will be used to document any rainfall data starting at least 72 hours before the
expected representative storm event.
Personnel
(�a-jey
Date/Time/Rainfall
y Z Z-! J
�c ! 0. 00
Date/Time/Rainfall
j2121
: 3 a J Q• p
Date/Time/Rainfall
gI25 /zl
j o ' 3J 0 0 J
Date/Time/Rainfall
r
0 C�
Date/Time/Rainfal(
Date/Time/Rainfall
Date/Time/Rainfall
Stormwater Pollution Prevention Plan Appendices

X)! aceAnalj6cal
www.pacelabs.com
May 17, 2021
Mr. Gary Hames
American Truetzschler, Inc.
PO Box 669228
5315 Heavy Equipment School Rd
Charlotte, NC 28266
RE: Project: Al & A2
Pace Project No.: 92536420
Dear Mr. Harries:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 03, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNIlNELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 33

aceAnalyticalr.
WWW.pacalahs.cmn
Project: Al & A2
Pace Project No.: 92536420
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100. Huntersville. NC 28078
LouisianalNELAP Certification* LA170028
North Carolina Drinking Water Certification #' 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Ashevilie
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 2 of 33

aceAnalXical V
www.pacelab.carm
SAMPLE ANALYTE COUNT
Pace Ana lyticat Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Al & A2
Pace Project No: 92536420
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92536420001 Al
EPA 1664E
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
11
PASI-A
EPA 245.1 Rev 3.0 1994
Soo
1
PASI-A
EPA625.1
PKS
58
PASI-C
EPA 624.1
SAS
34
PASI-C
SM 254OD-2011
RED
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 9040C
SMK
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92536420002 A2
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SHi
11
PASI-A
EPA 245.1 Rev 3.0 1994
Soo
1
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
34
PASI-C
SM 2540D-2011
RED
1
PASI-A
SM 4500-S2D-201 t
JP1
1
PASI-A
EPA 9040C
SMK
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
PASI-A = Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC.
Page 3 of 33

Pace Analytical Services, LLC
aceAnalXical c 9800 KinceyAve. Suite 100
Huntersville, NC 28078
www.pacctabs.cam [phone]
ANALYTICAL RESULTS
Project: Al & A2
Pace Project No.: 92536420
Sample: All LabID: 92536420001 Collected: 05/03/21 10:15 Received: 05/03/21 13:25 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analyfical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
NO
mg1L
4.9
1
05/15121 11:35
200.7 MET lCP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Antimony
NO
ug/L
5.0
1
05/0412116:23
0510612101:08 7440-36-0
Arsenic
NO
ug1L
10.0
1
05104/2116:23
0510612101:08 7440-38-2
Cadmium
ND
ug/L
1.0
1
05/0412116:23
05/06/2101:08 7440-43-9
Chromium
ND
uglL
5.0
1
05/04/2116:23
0510612101:08 7440-47-3
Copper
19.6
ug1L
5.0
1
05104/21 16:23
0510612101:08 7440-50-8
Lead
ND
ug/L
5.0
1
05/04/2116:23
0510612101:08 7439.92-1
Nickel
ND
ug/L
5.0
1
05/04/2116:23
05106/2101:08 7440-02-0
Selenium
ND
ug1L
10.0
1
05104/2116:23
0510612101:08 7782-49-2
Silver
ND
ug/L
5.0
1
05/04/211623
05106/2101:08 7440-22-4
Thallium
ND
ug/L
10.0
1
05/04/21 16:23
05/06/21 01:08 7440-28-0
Zinc
85.4
ug/L
10.0
1
05/04/2116:23
05106/2101:08 7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services - Asheville
Mercury
NO
ug/L
0.20
1
05/04/21 13:42
05/04/21 17:53 7439-97-6
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA
625.1
Pace Analytical Services - Charlotte
Acenaphthylene
NO
ug/L
5.0
1
05104/21 06:02
05105/21 21:44 208-96-8
Anthracene
NO
ug/L
5.0
1
05/04/21 06:02
05105/21 21:44 120-12-7
Benzidine
NO
ug/L
50.0
1
0510412106:02
05105/21 21:44 92-87-5 IL
Benzo(a)anthracene
NO
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44 56-55-3
Benzo(a)pyrene
NO
ug/L
5.0
1
05104/2106:02
05/05/21 21:44 50-32-8
Benzo(b)fluoranthene
NO
ug/L
5.0
1
05/0412106:02
05105/21 21:44 205-99-2
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
05/04/21 06:02
05/0512121:44 191-24-2
Benzo(k)fluoranthene
NO
ug/L
5.0
1
05104/2106:02
05/05/21 21:44 207-08-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
1
05/04/21 06:02
05/05/21 21 A4 101-55-3
Butylbenzylphthalate
NO
ug/L
5.0
1
05104/2106:02
05/05/21 21:44 85-68-7
4-Chlor0-3-methylphenol
ND
ug/L
5.0
1
05104/2106:02
05105/2121A4 59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
05104/2106:02
05/05/21 21:44 111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44 11144-4
2-Chloronaphthalene
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44 91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44 95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44 7005-72-3
Chrysene
N❑
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44 218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
05/04121 06:02
05105121 21 A4 53-70-3
3,3'-Dichlorohenzidine
ND
ug/L
10.0
1
05/04/21 06:02
05105/2121A4 91-94-1
2.4-Dichlorophenol
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 21 A4 120-83-2
Diethyl phtha late
ND
ug1L
5.0
1
05/04/21 06:02
05105/21 21:44 84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
05/04/21 06:02
05/05/21 21:44 105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 21 A4 131-11-3
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
Date: 05/17/2021 03:04 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 33

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Al & A2
Pace Project No.: 92536420
Sample: Al Lab ID: 92536420001 Collected: 05/03/21 10:15 Received: 05/03/21 13:25 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Di-n-butylphthalate
NO
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44
84-74-2
4,6-Dinitro-2-methylphenol
NO
ug/L
10.0
1
05/0412106:02
05/05121 21:44
534-52-1
2,4-Dinitrophenol
NO
ug/L
50.0
1
05/04/21 06:02
05/05/21 21:44
51-28-5
2,4-Dinitrotoluene
NO
ug/L
&0
1
05104/2106:02
0510512121:44
121-14-2
2.6-Dinitrotoluene
NO
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44
606-20-2
Di-n-octytphthalate
NO
ug/L
5.0
1
05104/2106:02
05/05/21 21:44
117-84-0
1,2-Diphenylhydrazine
NO
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44
122-66-7
bis(2-Ethylhexyl)phthalate
NO
ug1L
5.0
1
0510412106:02
0510512121:44
117-81-7
Fluoranthene
NO
ug/L
5.0
1
0510412106:02
05/05/21 21:44
206-44-0
Fluorene
ND
ug/L
5.0
1
05104/2106:02
0510512121:44
86-73-7
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
05104/2106:02
05105/2121:44
87-68-3
Hexachlorobenzene
NO
ug/L
5.0
1
05104/2106:02
0510512121:44
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
05104/2106:02
05/05/21 21:44
77-47-4
Hexachloroethane
NO
ug/L
5.0
1
05/04/21 06:02
05/05/21 21:44
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug/L
5.0
1
05104/2106:02
05/0512121:44
193-39-5
Isophorone
NO
ug/L
10.0
1
05/04/21 06:02
05/05/21 21:44
78-59-1
Naphthalene
NO
ug/L
5.0
1
05104/2106:02
05/05/21 21:44
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
06/04/2106:02
0510512121:44
98-95-3
2-Nitrophenol
NO
ug/L
5.0
1
05/04/21 06:02
05/0512121:44
88-75-5
4-Nitrophenol
NO
ug/L
10.0
1
0510412106:02
05/0512121:44
100-02-7
N-Nitrosod imethyla mine
NO
ug1L
5.0
1
05/04/21 06:02
05/05/21 21:44
62-75-9
N-Nitroso-di-n-pro pyla mine
NO
ug/L
5.0
1
0510412106:02
05/05/21 21:44
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
05/04/2106:02
05/05/21 21:44
86-30-6
Pentachlorophenol
ND
ug/L
10.0
1
05/04/2106:02
0510512121:44
87-86-5
Phenanthrene
NO
ug/L
5.0
1
05104/2106:02
05/05/21 21:44
85-01-8
Phenol
ND
ug/L
&0
1
05/04/21 06:02
0510512121:44
108-95-2
Pyrene
NO
ug/L
5.0
1
05104/2106:02
0510512121:44
129-00-0
1,2,4-Trichlorabenzene
ND
ug/L
5.0
1
0510412106i02
0510512121:44
120-82-1
2,4,6-Trichlorophenol
NO
ug/L
10.0
1
05/04/21 06:02
0510512121:44
88-06-2
Surrogates
Nitrobenzene-d5 (S)
24
%
10-120
1
05/04/21 06:02
05/05/21 21:44
4165-60-0
2-Fluorobiphenyl (S)
18
%
15-120
1
05/04/21 06:02
05105/21 21:44
321-60-8
Terphenyl-d14 (S)
46
%
11-131
1
05/04/21 06:02
05/05/21 21:44
1718-51-0
Phenol-d6 (S)
16
%
10-120
1
05/04/21 06:02
05/05/21 21:44
13127-88-3
2-Fluorophenal (S)
14
%
10-120
1
05/04/21 06:02
05/05/21 21:44
367-12-4
2.4,6-Tribromophenol (S)
40
%
10-137
1
05/04/21 06:02
05/05/21 21:44
118-79-6
624 Volatile Organics
Analytical Method:
EPA 624.1
Pace Analytical
Services - Charlotte
Benzene
NO
uglL
1.0
1
05/04/2113:51
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1
05104/2113:51
75-27-4
Bromoform
NO
ug/L
2.0
1
0510412113:51
75-25-2
Bromomethane
NO
ug/L
2.0
1
0510412113:51
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
05/04121 13:51
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
05/04/2113:51
108-90-7
Chloroethane
ND
ug/L
2.0
1
0510412113:51
75-00-3
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full.
Date: 05117/2021 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 33

accAnalyticale
www.pacelabs.tom
ANALYTICAL RESULTS
Project: Al & A2
Pace Project No.: 92536420
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersv Ile, NC 28078
[phone]
Sample: Al Lab ID: 92536420001 Collected: 05/03/21 10:15 Received: 05/03/21 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics
Analytical Method: EPA624.1
Pace Analytical Services - Charlotte
Chloroform
ND uglL
2.0
1
05/04/21 13:51
67-66-3
Chloromethane
ND ug1L
2.0
1
05/04/21 13:51
74-87-3
Dibromochloromethane
ND ug1L
2.0
1
05/0412113:51
124-48-1
1,2-Dichlorobenzene
ND uglL
2.0
1
0510412113:51
95-50-1
1,3-Dichlorobenzene
ND ug1L
2.0
1
05/04/21 13:51
541-73-1
1.4-Dichlorobenzene
ND uglL
2.0
1
05/04/21 13:51
106-46-7
1,1-Dichloroethane
ND uglL
2.0
1
05104/2113:51
75-34-3
1.2-Dichloroethane
ND uglL
2.0
1
05104/2113:51
107-06-2
1,1-Dichloroethene
ND uglL
2.0
1
05/04/2113:51
75-35-4
cis- 1,2-Dichloroethene
ND ug/L
2.0
1
05/04/21 13:51
156-59-2
trans- 1,2-Dichtoroethene
ND uglL
2.0
1
05/04/21 13:51
156-60-5
1,2-Dichloropropane
ND uglL
2.0
1
05/04/21 13:51
78-87-5
cis-1,3-Dichloropropene
ND uglL
2.0
1
05/04/21 13:51
10061-01-5
trans- 1,3-Dichloropropene
ND uglL
2.0
1
05/04/21 13:51
10061-02-6
Ethylbenzene
ND uglL
1.0
1
05104/2113:51
100-41-4
Methylene Chloride
ND uglL
2.0
1
05/04/21 13:51
75-09-2
1,1,2,2-Tetrachloroethane
ND uglL
2.0
1
05104/2113:51
79-34-5
Tetrachloroethene
ND uglL
2.0
1
05/0412113:51
127-18-4
Toluene
ND uglL
1.0
1
0510412113:61
108-88-3
1,1,1-Trichioroethane
ND uglL
2.0
1
05/04/21 13:51
71-55-6
1,1,2-Trichloroethane
ND uglL
2.0
1
0510412113:51
79-00-5
Trichloroethene
ND ug1L
2.0
1
0510412113:51
79-01-6
Trichlorofluoromethane
ND ug1L
2.0
1
05104/2113:51
75-69-4
Vinyl chloride
ND ug1L
2.0
1
05/04/21 13:51
75-01-4
Surrogates
4-Bramofluorobenzene (S)
107 %
70-130
1
05/04121 13:51
460-004
Toluene-d8 (S)
11l %
70-130
1
05/04/21 13:51
2037-26-5
1.2-Dichloroethane-d4 (S)
102 %
70-130
1
05/04/21 13:51
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services -Asheville
Total Suspended Solids
46.8 mg1L
9.4
1
05/06/21 22:08
4500S2D Sulfide Water
Analytical Method: SM. 4500-S2D-2011
Pace Analytical Services - Asheville
Sulfide
ND mglL
0.10
1
05/05/2106:08
18496-25-8
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.1 Std. Units
0.10
1
05/09/21 16:01
30D.0 IC Anions 28 Days
Analytical Method. EPA 300.0 Rev 2.1
1993
Pace Analytical Services - Asheville
Sulfate
13.1 mg1L
1.0
1
05/06/2115:21
14808-79-8
Date: 05/17/2021 03:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC.
H3
Page 6 of 33

aceAnalytical L
www.pacelahsxom
ANALYTICAL RESULTS
Project: Al & A2
Pace Project No.: 92536420
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Al Lab ID: 92536420001 Collected: 05/03/21 10:15 Received: 05/03/21 13:25 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
420.4 Phenolics, Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
Phenolics, Total Recoverable ND mg/L 0,020 1 05/05/21 10:17 05/05/21 14:01 64743-03-9
450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
Cyanide NO mg/L 0.0080 1 05/06/21 20:48 05/07/21 00:58 57-12-5
Sample: A2 Lad ID: 92536420002 Collected: 05103/21 10:30 Received: 05/03/21 13:25 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
4.9
1
05/15/21 11:35
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7
Rev 4.4 1994
Pace Analytical Services - Asheville
Antimony
NO ug/L
5.0
1
05/04/2116:23
05/06/21 01:11
7440-36-0
Arsenic
ND ug/L
10.0
1
05/04/2116:23
05/06/21 01:11
7440-38-2
Cadmium
NO ug/L
1.0
1
05/04121 16:23
05/06/21 01:11
7440-43-9
Chromium
NO ug/L
5.0
1
05/04/2116:23
05/06/21 01:11
7440-47-3
Copper
6.2 ug/L
5.0
1
05/04/2116:23
05/06/21 01:11
7440-50-8
Lead
ND ug/L
5.0
1
05/04/2116:23
05/06/21 01:11
7439-92-1
Nickel
NO ug/L
5.0
1
05/0412116:23
05/06/21 01:11
7440-02-0
Selenium
NO ug/L
10.0
1
05/04/2116:23
05/06/21 01:11
7782-49-2
Silver
ND ug/L
5.0
1
0510412116:23
05/06/21 01:11
7440-22-4
Thallium
NO ug/L
10.0
1
05/04/2116:23
05/06/21 01:11
7440-28-0
Zinc
50.6 ug/L
10.0
1
05/0412116:23
05/06/21 01:11
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation Method: EPA 245.1
Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
ND ug/L
0.20
1
05104/2113A2
0510412117:55
7439-97-6
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625A
Pace Analytical Services - Charlotte
Acenaphthylene
NO ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13
208-96-8
Anthracene
NO ug/L
5.0
1
05104/2106:02
05/05/21 22:13
120-12-7
Benzidine
NO ug/L
50.0
1
05/04/2106:02
05/05/21 22:13
92-87-5 IL
Benzo(a)anthracene
NO ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13
56-55-3
Benzo(a)pyrene
ND ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13
50-32-8
Benzo(b)fluoranthene
ND ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13
205-99-2
Benzo(g,h.i)perylene
ND ug/L
5.0
1
05/04/21 06:02
05/0512122:13
191-24-2
Benzo(k)fluoranihene
NO ug1L
5.0
1
05/04/21 06:02
05/05/21 22:13
207-08-9
4-Bromophenylphenyl ether
NO ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13
101-55-3
Butylbenzylphthalate
ND ug/L
5.0
1
05104/21 06:02
05/05121 22:13
85-68-7
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced,
except
in full,
Date: 05/17/2021 03:04 PM
without the written consent of Pace
Analytical Services.
LLC-
Page 7 of 33

aceAnalytical
www.pacolabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Al & A2
Pace Project No.: 92536420
Sample: A2 Lab ID: 92536420002 Collected: 05/03/21 10:30 Received: 05/03/21 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
4-Chloro-3-methylphenol
ND
ug1L
5.0
1
05104/2106:02
0510512122:13 59-50-7
bis(2-Chlaroethoxy)methane
ND
ug/L
10.0
1
05/0412106:02
05105/2122:13 111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
05104/21 06:02
05/05/21 22:13 111-44-4
2-Chlorortaphthalene
N❑
ug/L
5.0
1
05/04/21 06:02
0510512122:13 91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
05/04/21 06:02
05105/21 22:13 7005-72-3
Chrysene
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
05/04/21 06:02
05105/2122:13 53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
05/04/21 06:02
05/05/21 22:13 91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
05104/2106:02
05105/2122:13 120-83-2
Diethylphthalate
ND
ug/L
5.0
1
05/04/21 06:02
05/06/21 22:13 84-66-2
2.4-Dimethylphenol
ND
ug/L
10.0
1
05/04/21 06:02
05/05/21 22:13 105-67-9
Di methylphtha late
ND
ug/L
5.0
1
05104/2106:02
05/0512122:13 131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
10.0
1
05/04/21 06:02
05/05/21 22:13 534-52-1
2.4-Dinitrophenol
ND
ug/L
50.0
1
05/04/21 06:02
05/05/21 22:13 51-28-5
2.4-Dinitrotoluene
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 121-14-2
2.6-Dinitrotoluene
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
05104/2106:02
05/05/21 22:13 117-84-0
1,2-Diphenylhydrazine
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 122-66-7
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 117-81-7
Fluoranthene
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 206-44-0
Fluorene
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
05/04/2106:02
05/05/21 22:13 87-68-3
Hexachloro benzene
ND
ug/L
5.0
1
05104/2106:02
05/0512122:13 118-74-1
Hexachlorocyclopentadiene
N❑
ug/L
10.0
1
05104/21 06:02
05/05/21 22:13 77-47-4
Hexachloroethane
ND
ug/L
5.0
1
05/04/21 06:02
0510512122:13 67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
05/04/21 06:02
0510512122:13 193-39-5
Isophorone
ND
ug/L
10.0
1
0510412106:02
0510512122:13 78-59-1
Naphthalene
ND
ug/L
5.0
1
05104/2106:02
05105/2122:13 91-20-3
Nitrobenzene
ND
ug/L
5.0
1
05104/2106:02
0510512122:13 98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
05104/2106:02
05/0512122:13 88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
05/04/21 06:02
0510512122:13 100-02-7
N-N itrosod imethylam ine
ND
ug/L
5.0
1
05/04/21 06:02
0510512122:13 62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
&0
1
05/04/21 06:02
05/05/21 22:13 621-64-7
N-N itrosod iphe nyla m ine
ND
ug/L
10.0
1
05/04/21 06:02
0510512122:13 86-30-6
Pentachlorophenol
ND
ug/L
10.0
1
05/04/21 06:02
05105/2122:13 87-86-5
Phenanthrene
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 85-01-8
Phenol
ND
ug/L
5.0
1
05/04/2106:02
05/05/21 22:13 108-95-2
Pyrene
ND
ug/L
5.0
1
05104/2106:02
05105/2122:13 129-00-0
1.2 4-Trichlorobenzene
ND
ug/L
5.0
1
05/04/21 06:02
05/05/21 22:13 120-82-1
2.4,6-Trichlorophenol
ND
ug/L
10.0
1
05/04/21 06:02
05105/2122:13 88-06-2
Surrogates
Nitrobenzene-d5 (S)
47
%
10-120
1
05/04/21 06:02
05/05/21 22:13 4165-60-0
2-Fluorobipheny) (S)
35
%
15-120
1
05/04/21 06:02
05/05/21 22:13 321-60-8
Terphenyl-d14 (S)
48
%
11-131
1
05/04/21 06:02
05/05121 22:13 1718-51-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/1712021 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 33

a
aceAnalyticai
www,pacolabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersy0e, NC 28078
[phone]
Project: Al & A2
Pace Project No.: 92536420
Sample: A2 Lab ID: 92536420002 Collected: 05/03/21 10:30 Received: 05/03/21 13:25 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA625.1 Preparation Method: EPA625.1
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
29
%
10-120
1 05/04/21 06:02
05/05/21 22:13
13127-88-3
2-Fluoraphenol (S)
35
%
10-120
1 05/04/21 06:02
05/05/21 22A3
367-12-4
2,4,6-Tribromophenol (S)
57
%
10-137
1 05/04/21 06:02
05/05/21 22:13
118-79-6
624 Volatile Organics
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
Benzene
NO
ug/L
1.0
1
05104/2114:09
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
05/04/21 14:09
75-27-4
Bromoform
NO
uglL
2.0
1
05/04/21 14:09
75-25-2
Bromomethane
ND
ug/L
2.0
1
05/04/21 14:09
74-83-9
Carbon tetrachloride
ND
uglL
2.0
1
05/04/21 14:09
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
05/0412114:09
108-90-7
Chloroethane
ND
ug/L
2.0
1
05/04/21 14:09
75-00-3
Chloroform
ND
ug/L
2.0
1
05/04/21 14:09
67-66-3
Chloromethane
ND
ug/L
2.0
1
05/0412114:09
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
05/04/21 14:09
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2A
1
05/04/21 14:09
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
05/04/21 14:09
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
05/04/21 14:09
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
05/04/21 14:09
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
05104/2114:09
107-06.2
1,1-Dichloroethene
ND
ug/L
2.0
1
05/04/21 14:09
75-35-4
cis-1,2-Dichloroethene
NO
ug/L
2.0
1
05/04/21 14:09
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1
05/04/21 14:09
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
05/04/21 14:09
78-87-5
cis-1.3-Dichloropropene
NO
ug/L
2.0
1
05/04/21 14:09
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
0510412114:09
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
05/04/21 14:09
100-41-4
Methylene Chloride
NO
ug/L
2.0
1
05/04/21 14:09
75-09-2
1.1,2,2-Tetrachloroethane
ND
ug1L
2.0
1
05/04/21 14:09
79-34-5
Tetrachloroethene
NO
ug1L
2.0
1
05/04/21 14:09
127-18-4
Toluene
NO
ug/L
1.0
1
05/04/2114:09
108-88-3
1,1,1-Trichloroethane
NO
uglL
2.0
1
05/04/21 14:09
71-55-6
1,1,2-Trichloroethane
ND
uglL
2.0
1
05/04/21 14:09
79-00-5
Trichloroethene
ND
ug1L
2.0
1
05/0412114:09
79-01.6
Trichlorofluoromethane
ND
ug/L
2.0
1
05/04/21 14:09
75-69-4
Vinyl chloride
ND
uglL
2.0
1
05/04/21 14:09
75-01-4
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
05/04/21 14:09
460-00-4
Toluene-d8 (S)
108
%
70-130
1
05/04/21 14:09
2037-26-5
1.2-Dichloroethane-d4 (S)
108
%
70-130
1
05/04/21 14:09
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services - Asheville
Total Suspended Solids
34.7
mg/L
3.7
1
05/06/21 22:08
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 05/17/2021 03:04 PM
without the written consent of Pace Analytical Services, LLC,
Page 9 of 33

aceAnalyfical
www.pacelsbs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Al & A2
Pace Project No.: 92536420
Sample: A2
Lab ID: 92536420002 Collected: 05/03/21 10:30
Received: 05/03/21 13:25 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
450OS20 Sulfide Water
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
Sulfide
ND mg/L 0.10 1
05105/2106:09 18496-25-8
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.1 Std. Units 0.10 1
05/09/21 16:07 H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
2.0 mg/L 1.0 1
05/05/2121:03 14808-79-8
420.4 Phenolics, Total
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation
Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
Phenolics, Total Recoverable
ND mg/L 0.020 1
05/05/21 10:17 05/05/21 14:02 64743-03-9
450OCNE Cyanide, Total
Analytical Method: SM 4500-CN-E-2011 Preparation Method:
SM 4500-CN-E-2011
Pace Analytical Services - Asheville
Cyanide
ND mg/L 0.0080 1
05/11/21 00:25 05/12/21 00:24 57-12-5
Date: 05/17/2021 03:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 33

ZacAnalyticaf�
www.pacelahs.com
QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersmile, NC 28078
[phone]
QC Batch: 620717
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664B
Analysis Description:
1664 HEM, Oil and
Grease
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92536420001, 92536420002
METHOD BLANK: 3265990
Matrix: Water
Associated Lab Samples: 92536420001, 92536420002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Oil and Grease
mg/L
ND 5.0
05/15/21 11:35
LABORATORY CONTROL SAMPLE:
3265991
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
40 33.0
82
78-114
MATRIX SPIKE SAMPLE:
3265992
92537669002 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 39.2
26.9
64
78-114 M1
MATRIX SPIKE SAMPLE:
3265993
92537669004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
25.5
57
78-114 M1
SAMPLE DUPLICATE: 3265994
92537669004 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Oil and Grease
mg/L
ND 1 7J
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the resuit
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 05/1712021 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 33

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 618032 Analysis Method: EPA 245.1 Rev 3.0 1994
QC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92536420001, 92536420002
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
METHOD BLANK: 3251514
Matrix: Water
Associated Lab Samples: 92536420001, 92536420002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
uglL
ND 0.20
0510412116:49
LABORATORY CONTROL. SAMPLE:
3251515
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Mercury
uglL
2.5 2.8
110 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3251516 3251517
MS MSD
92536174001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.7 101 109 70-130 7
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3251618 3251519
MS MSD
92536178001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.7 2 5 107 102 70-130 5
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 33

acEAnalyiical
www.pacelab3.com
QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
OC Hatch: 618115
QC Batch Method: EPA 2003 Rev 4.4 1994
Associated Lab Samples: 92536420001, 92536420002
Analysis Method:
Analysis Description:
Laboratory:
EPA 200.7 Rev 4.4 1994
200.7 MET
Pace Analytical Services - Asheville
METHOD BLANK: 3252170
Matrix: Water
Associated Lab Samples:
92536420001, 92536420002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Antimony
ug/L
ND
5.0
05106/2117:57
Arsenic
ug/L
ND
10.0
05/0612117:57
Cadmium
ug/L
ND
1.0
05/0612117:57
Chromium
ug/L
ND
5.0
05/0612117:57
Copper
ug/L
ND
5.0
05/06/2117:57
Lead
ug/L
ND
5.0
05/0612117:57
Nickel
ug/L
ND
5.0
05/06/2117:57
Selenium
ug/L
ND
10.0
05106/2117:57
Silver
ug/L
ND
5.0
05/06/2117:57
Thallium
ug/L
ND
10.0
05/06/2117:57
Zinc
ug/L
ND
10.0
05106/2117:57
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville. NC 2807E
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
3252171
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
494
99
85-115
Arsenic
ug/L
500
496
99
85-115
Cadmium
ug/L
500
488
98
85-115
Chromium
ug1L
500
507
101
85-115
Copper
ug/L
500
519
104
85-115
Lead
ug/L
500
483
97
85-115
Nickel
ug/L
500
498
100
85-115
Selenium
ug1L
500
483
97
85-115
Silver
ug/L
250
247
99
85-115
Thallium
uglL
500
491
98
85.115
Zinc
ug1L
500
478
96
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3252172
3252173
MS
MSD
92535735001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
47.3
500
500
529
543
96
99
70-130
3
Arsenic
ug/L
ND
500
500
548
565
108
111
70-130
3
Cadmium
ug1L
ND
500
500
546
558
109
112
70-130
2
Chromium
ug/L
10.5
500
500
444
443
87
86
70-130
0
Copper
ug/L
ND
500
500
560
572
111
114
70-130
2
Lead
ug1L
ND
500
500
387
390
77
77
70-130
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC,
Page 13 of 33

aceARalytical a
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
(704�875-9092
Project: Al & A2
Pace Project No.: 92536420
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3252172
3252173
MS
MSD
92535735001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nickel
uglL
431
500
500
816
828
77
79
70-130
1
Selenium
ug/L
ND
500
500
61.9
70-0
12
13
70-130
12 M1
Silver
uglL
ND
250
250
290
293
116
117
70-130
1
Thallium
uglL
ND
500
500
344
347
69
69
70-130
1 Mi
Zinc
uglL
ND
500
500
464
464
92
92
70-130
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3252174
3252175
MS
MSD
92536378001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
uglL
ND
500
500
501
498
100
100
70.130
1
Arsenic
ug1L
ND
500
500
507
506
101
101
70-130
0
Cadmium
ug1L
ND
500
500
498
495
100
99
70-130
1
Chromium
ug1L
ND
500
500
499
491
100
98
70.130
2
Capper
ug1L
ND
500
500
512
502
101
100
70-130
2
Lead
uglL
ND
500
500
482
478
96
96
70-130
1
Nickel
ug1L
ND
500
500
498
495
100
99
70-130
1
Selenium
ug1L
ND
500
500
518
509
104
102
70-130
2
Silver
ug/L
ND
250
250
248
244
99
98
70-130
2
Thallium
ug/L
ND
500
500
488
485
97
97
70.130
1
Zinc
ug/L
11.6
500
500
487
483
95
94
70-130
1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 33

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 618052
QC Batch Method: EPA 624.1
Associated Lab Samples: 92536420001, 92536420002
Analysis Method: EPA 624.1
Analysis Description: 624 MSV
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 3251766
Matrix:
Water
Associated Lab Samples: 92536420001, 92536420002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
uglL
ND
2.0
05/04/21 12:41
1.1.2.2-Tetrachloroethane
uglL
ND
2.0
05/04/21 12:41
1,1,2-Trichloroethane
uglL
ND
2.0
0510412112:41
1,1-Dichloroethane
uglL
ND
2.0
05/04/21 12:41
1,1-Dichioroethene
uglL
ND
2.0
05/04/21 12:41
1,2-Dichlorobenzene
uglL
ND
2.0
05/04/21 12:41
1,2-Dichforoethane
uglL
ND
2.0
05/04/2112:41
1.2-Dichloropropane
uglL
ND
2.0
05/04/2112A1
1,3-Dichlorobenzene
uglL
ND
2.0
05/04/21 12:41
1,4-Dichlorobenzene
uglL
ND
2.0
05/0412112A1
Benzene
uglL
ND
1.0
05/04/2112A1
Bromodichloromelhane
ug1L
ND
2.0
05/04/2112A1
Bromoform
uglL
ND
2.0
0510412112A1
Bromomethane
uglL
ND
2.0
0510412112:41
Carbon tetrachloride
uglL
ND
2.0
05/04/21 12Al
Chlorobenzene
uglL
ND
2.0
0510412112A1
Chloroethane
uglL
ND
2.0
05/04/2112A1
Chloroform
uglL
ND
2.0
0510412112A1
Chloromethane
uglL
ND
2.0
05/0412112:41
cis- 1,2-Dichloroethene
uglL
ND
2.0
05/04/21 12:41
cis-1,3-Dichtoropropene
uglL
ND
2.0
05/04/21 12:41
Dibromochloromethane
uglL
ND
2.0
05104/2112:41
Ethylbenzene
ug1L
ND
1.0
05/04/21 12:41
Methylene Chloride
uglL
ND
2.0
05/04/21 12:41
Tetra chloroethene
uglL
ND
2.0
05/04/21 12:41
Toluene
uglL
ND
1.0
05/04/21 12:41
trans-1.2-Dichloroethene
uglL
ND
2.0
05/0412112A1
trans- l,3-Dichloropropene
uglL
ND
2.0
05104/2112:41
Trichtoroethene
ug/L
ND
2.0
0510412112:41
Trichlorofluoromethane
uglL
ND
2.0
0510412112:41
Vinyl chloride
ug/L
ND
2.0
05/04/21 12:41
1,2-Dichloroethane-d4 (S)
%
101
70-130
05104/21 12:41
4-Bromofluorabenzene (S)
°!
103
70-130
05/04/21 12:41
Toluene-d8 (S)
%
105
70-130
05/04/21 12:41
LABORATORY CONTROL SAMPLE: 3251767
Pace Analytical Services, LLC
9800 KinceyAve- Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug1L 20 20.5 102 70.130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, U.C. Page 15 of 33

aceAnalyiical
www.pacolahs.com
QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
LABORATORY CONTROL SAMPLE:
3251767
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,1.2,2-Tetrachlaroethane
uglL
20
16.8
84
70-130
1.1,2-Trichloroethane
uglL
20
19.5
98
70-130
1,1-Dichloroethane
uglL
20
18.4
92
70-130
1,1-Dichloroethene
uglL
20
20.5
103
70-132
1,2-Dichlorobe nzene
uglL
20
19.3
97
70-130
1,2-Dichloroethane
uglL
20
21.3
106
70-130
1.2-Dichloropropane
uglL
20
18.1
90
70-130
1,3-Dichlorobenzene
uglL
20
197
99
70-130
1.4-Dichlorobenzene
uglL
20
203
101
70-130
Benzene
uglL
20
188
94
70-130
Bromodichloromethane
uglL
20
210
105
70-130
Bromoform
uglL
20
200
100
70-130
Bromomethane
uglL
20
26.8
134
30-177
Carbon tetrachloride
uglL
20
23.7
118
70-130
Chlorobenzene
uglL
20
20.2
101
70-130
Chloroethane
uglL
20
22.5
112
46-131
Chloroform
uglL
20
19.8
99
70-130
Chloromethane
ug/L
20
17.6
88
49-130
cis-1,2-Dichloroethene
ug1L
20
18.9
95
70-130
cis-1,3-Dichloropropene
uglL
20
19.5
97
70-130
Dibromochloromethane
ug1L
20
20.1
100
70-130
Ethylbenzene
uglL
20
19.9
99
70-130
Methylene Chloride
ug1L
20
14.5
73
68-130
Tetra chloroethene
ug/L
20
19.8
99
70-130
Toluene
uglL
20
19.7
99
70-130
trans-1.2-Dichloroethene
uglL
20
19.8
99
70-130
trans-1,3-Dichloropropene
uglL
20
20.0
100
70-130
Trichloroethene
uglL
20
20.7
103
70-130
Trichlorofluoromethane
uglL
20
21.2
106
61-130
Vinyl chloride
uglL
20
17.7
88
59-142
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(704}875-9092
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3251768
3251769
MS
MSD
92536256001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc,
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
24.8
24.7
124
123
70-148
1
1,1,2,2-Tetrachloroethane
ug1L
ND
20
20
17.3
17.2
87
86
70-131
0
1,1,2-Trichloroethane
uglL
ND
20
20
21.7
20.3
108
101
70-136
7
1,1-Dichloroethane
ug1L
ND
20
20
19.0
19.7
95
98
71-143
3
1.1-Dichloroethene
uglL
ND
20
20
25.1
24.3
126
121
70-158
4
1,2-Dichlorobenzene
uglL
ND
20
20
19.7
20.8
98
104
70-133
6
1,2-Dichloroethane
uglL
ND
20
20
24.2
24.2
121
121
72-137
0
Results presented on this page are in the units indicated by the" Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 33

aceAnalytical
www.paceilhs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2807E
[phone]
Project: Al & A2
Pace Project No.: 92536420
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3251768
3251769
MS
MSD
92536256001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,2-Dichloropropane
ug/L
NO
20
20
19.6
19.3
98
97
70-138
1
1,3-Dichlorobenzene
ug1L
NO
20
20
20A
21.6
102
108
75-133
5
1,4-Dichlorobenzene
ug1L
NO
20
20
20.4
21.4
102
107
70-133
5
Benzene
ug1L
ND
20
20
19.6
19.9
98
99
75-125
2
Bromodichloromethane
ug1L
NO
20
20
22.9
22.6
115
113
70-138
1
Bromoform
ug1L
ND
20
20
20.9
21.0
105
105
57-138
0
Bromomethane
ug/L
ND
20
20
28.2
29.6
141
148
10-200
5
Carbon tetrachloride
ug/L
ND
20
20
26.2
26.9
131
134
70-125
2 M1
Chlorobenzene
ug1L
ND
20
20
21.7
21.5
108
107
82-137
1
Chtoroethane
ug/L
ND
20
20
25.3
27.7
126
138
51-166
9
Chloroform
ug/L
NO
20
20
22.7
20.5
112
101
70-121
10
Chloromethane
ug1L
ND
20
20
20.0
20.6
100
103
24-161
3
cis-1,2-Dichloroethene
ug/L
ND
20
20
21A
20.6
106
103
67-148
2
cis- 1,3-Dichlorop ropene
ug/L
ND
20
20
20.6
19.3
103
97
70-142
7
Dibrom och lorom ethane
ug1L
ND
20
20
21.7
20.9
109
104
69-133
4
Ethylbenzene
ug/L
NO
20
20
21.2
21.2
106
106
75-134
0
Methylene Chloride
ug/L
ND
20
20
16.2
17.7
81
89
64-148
9
Tetrachloroethene
ug/L
ND
20
20
22.3
21.6
112
108
70-133
3
Toluene
ug/L
NO
20
20
22.0
21.0
110
105
75-134
4
trans-1,2-Dichloroethene
ug/L
NO
20
20
21.8
22.6
109
113
70-143
4
trans-1,3-Dichloropropene
ug/L
NO
20
20
21.3
20.2
106
101
70-138
5
Trichloroethene
ug/L
NO
20
20
23.2
22.1
116
110
75-138
5
Trichlorofluoromethane
ug/L
ND
20
20
25.7
26.4
129
132
61-154
3
Vinyl chloride
uglL
ND
20
20
20.5
21.3
102
106
55-172
4
1,2-Dichloroethane-d4 (S)
%
105
112
70-130
4-Bromofluorobenzene (S)
%
99
99
70-130
Toluene-d8 (S)
%
102
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shatl not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 33

e;
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QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 617823 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Laboratory: Pace Analytical Services -Charlotte
Associated Lab Samples: 92536420001. 92536420002
METHOD BLANK: 3250649
Associated Lab Samples: 92536420001. 92536420002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichlorobenzene
uglL
NO
5.0
05/04/2108:34
1,2-Diphenylhydrazine
ug/L
NO
5.0
05104/2108:34
2,4.6-Trichlorophenol
ug/L
NO
10.0
05/04/2108:34
2,4-Dichlorophenol
ug/L
NO
5.0
05/0412108:34
2.4-Dimethyl phenol
ug/L
NO
10.0
05/04/2108:34
2,4-Dinitrophenol
ug/L
NO
50.0
05/0412108:34
2,4-Dinitrotoluene
ug/L
NO
5.0
05/0412108:34
2,6-Dinitrotoluene
ug/L
NO
5.0
05/0412108:34
2-Chloronaphthalene
ug/L
NO
5.0
05/0412108:34
2-Chlorophenol
ug/L
NO
5.0
0510412108:34
2-Nitrophenol
ug/L
NO
5.0
051041210&34
3.3'-Dichlorobenzidine
ug/L
NO
10.0
05104/2108:34
4,6-Dinitro-2-methylphenol
ug/L
NO
10.0
05/0412108:34
4-Bromophenylphenyl ether
ug/L
NO
5.0
05/04/21 08:34
4-Chloro-3-methylphenol
ug/L
NO
5.0
05104/2108:34
4-Chlorophenylphenyl ether
ug/L
NO
5.0
05104/21 08:34
4-Nitrophenol
ug/L
NO
10.0
05/04/2108:34
Acenaphthylene
ug/L
NO
5.0
05/04/2108:34
Anthracene
ug/L
NO
5.0
05104/2108:34
Benzidine
ug/L
NO
50.0
0510412108:34
Benzo(a)anthracene
ug/L
NO
5.0
05/04/2108:34
Benzo(a)pyrene
ug/L
NO
5.0
06/04/2108:34
Benzo(b)fluoranthene
ug/L
NO
5.0
05/04/2108:34
Benzo(g,h,i)perylene
ug/L
NO
5.0
05/04/2108:34
Benzo(k)fluoranthene
ug/L
NO
5.0
05104/2108:34
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
05/04/2108:34
bis(2-Chloroethyl) ether
ug/L
NO
5.0
05104/21 08:34
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
05/0412108:34
Butylbenzytphthalate
ug/L
ND
5.0
05/0412108:34
Chrysene
ug/L
ND
5.0
05/04/2108:34
Di-n-butylphthalate
ug/L
ND
5.0
05104/2108:34
Di-n-octylphthalate
ug/L
ND
5.0
05104/2108:34
Dibenz(a,h)anthracene
ug/L
ND
5.0
05104/2108:34
Diethylphthalate
ug/L
ND
5.0
05104/2108:34
Dimethytphthalate
ug/L
ND
5.0
05104/2108:34
Ftuoranthene
ug/L
ND
5.0
05/04/2108:34
Fluorene
ug/L
ND
5.0
05/04/2108:34
Hexachloro-1,3-butadiene
ug/L
ND
5.0
05/04/21 08:34
Hexachlorobenzene
ug/L
ND
5.0
06/04/2108:34
Hexachlorocyclopentadiene
ug/L
ND
10.0
05/04/2108:34
IL
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 33

a;
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QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
METHOD BLANK: 3250649
Associated Lab Samples: 92536420001. 92536420002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
Hexachloroethane
ug1L
ND
5.0
05/0412108:34
Indenc(1,2,3-cd)pyrene
ug/L
ND
5.0
05/04/21 08:34
Isaphorone
ug/L
ND
10.0
05/0412108:34
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
05104/2108:34
N-Nitrosodimethyiamine
ug/L
ND
5.0
05/0412108:34
N-Nitrosodiphenylamine
ug/L
ND
10.0
05/0412108:34
Naphthalene
ug/L
ND
5.0
05/0412108:34
Nitrobenzene
ug/L
ND
5.0
05/0412108:34
Pentachlorophenol
ug/L
ND
10.0
05/04/21 08:34
Phenanthrene
ug/L
ND
5.0
05/0412108:34
Phenol
ug/L
ND
5.0
0510412108:34
Pyrene
ug/L
ND
5.0
05/04/21 08:34
2,4,6-Tribromophenol (S)
%
110
10-137
05/04/21 08:34
2-Fluorobiphenyl (S)
%
88
15-120
05/04/21 08:34
2-Fluorophenol (S)
%
70
10-120
05/04/21 08:34
Nitrobenzene-d5 (S)
%
94
10-120
05/04121 08:34
Phenol-d6 (S)
%
55
10-120
05/04/21 08:34
Terphenyl-d14 (S)
%
124
11-131
05/04/21 08:34
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersvi4e, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
3250650
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichtorobenzene
ug/L
50
31.1
62
44-142
1,2-Diphenylhydrazine
ug/L
50
40.4
81
25.150
2,4,6-Trichlorophenol
ug/L
50
39.8
80
37-144
2,4-Dichlorophenol
ug/L
50
37.7
75
1-191
2,4-Dimethylphenol
ug/L
50
37.7
75
32-119
2,4-Dinitrophenol
ug/L
250
223
89
1-181
2,4-Dinitrotoluene
ug/L
50
40.0
80
39-139
2,6-Dinitrotoluene
ug/L
50
38.8
78
50-158
2-Chloronaphthalene
ug/L
50
35.5
71
60-118
2-Chlorophenol
ug/L
50
33.8
68
23-134
2-Nitrophenol
ug/L
50
37,9
76
29-182
3,3'-Dichlorobenzidine
ug/L
100
85.8
86
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
92.0
92
1-181
4-Bromophenylphenyl ether
ug/L
50
45.4
91
53-127
4-Chloro-3-methylphenol
ug/L
100
76.1
76
22-147
4-Chlorophenylphenyl ether
ug/L
50
39.2
78
25-158
4-Nitrophenol
ug/L
250
130
52
1-132
Acenaphthylene
ug/L
50
37.8
76
33-145
Anthracene
ug1L
50
43.4
87
1-166
Benzidine
ug/L
100
35.9J
36
10-130 IL
Benzo(a)anthracene
ug/L
50
44.5
89
33-143
Benzo(a)pyrene
ug1L
50
46.1
92
17-163
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 33

aceAnalytica!s
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QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
LABORATORY CONTROL SAMPLE:
Parameter
3250650
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(b)fluoranthene
uglL
50
45.3
91
24-159
Benzo(g,h,i)perylene
uglL
50
45.2
90
1-219
Senzo(k)tluoranthene
uglL
50
46.6
93
11-162
bis(2-Chloroethaxy)methane
ug1L
50
36.0
72
33-184
bis(2-Chloroethyl) ether
ug1L
50
36.4
73
12-158
bis(2- Ethylhexyl)phtha late
ug1L
50
46.5
93
8-158
Butylbenzyl phtha late
ug/L
50
43.4
87
1-152
Chrysene
ug/L
50
43.8
88
17-168
Di-n-butylphihalate
ug1L
50
45.5
91
1-118
Di-n-octylphthalate
ug1L
50
44.3
89
4-146
Dibenz(a,h)anthracene
ug1L
50
45.8
92
1-227
Diethylphthalate
ug/L
50
39.8
80
1-114
Dimethytphthalate
ug1L
50
38.9
78
1-112
Ftuoranihene
ug1L
50
44.0
88
26-137
Fluorene
ug1L
50
39.7
79
59.121
Hexachloro-1,3-butadiene
ug1L
50
29.7
59
24-116
Hexachlo robe nze ne
ug/L
50
42.0
84
1-152
Hexachlorocyclopentadiene
ug1L
50
30.1
60
25-150
Hexachloroethane
ug/L
50
27.4
55
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
46.5
93
1-171
Isophorone
ug1L
50
34.8
70
21-196
N-Nitroso-di-n-propylamine
ug1L
50
33.8
68
1-230
N-Nitrosodimethylamine
ug1L
50
32.4
65
25-150
N-Nitrosodiphenylamine
ug/L
50
40.9
82
25-150
Naphthalene
ug/L
50
33.5
67
21-133
Nitrobenzene
ug/L
50
35.5
71
35-180
Pentachlorophenol
ug/L
100
90.4
90
14-176
Phenanthrene
ug/L
50
42.6
85
54-120
Phenol
ug/L
50
24,3
49
5-112
Pyrene
uglL
50
44.2
88
52-115
2,4,6-Tribromophenol (S)
%
100
10-137
2-Fluorobiphenyi (S)
%
68
15-120
2-Fluorophenol (S)
%
53
10-120
Nitrobenzene-d5 (S)
%
74
10-120
Phenol-d6 (S)
%
44
10-120
Terphenyl-d14 (S)
%
90
11-131
Pace Analytical Services, LLC
9800 KinceyAve, Suite too
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 05117/2021 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 33

aceAnalyticalc:
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 618816
Analysis Method:
SM 2540D-2011
QC Batch Method: SM 2540D-2011
Analysis Description:
2540D Total Suspended Solids
Laboratory:
Pace Analytical Services - Asheville
Associated Lab Samples: 92536420001.
92536420002
METHOD BLANK: 3256161
Matrix:
Water
Associated Lab Samples: 92536420001,
92536420002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mglL
ND
2.5 05106/21 22:05
LABORATORY CONTROL SAMPLE:
3256152
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mglL
250
258
103 90-110
SAMPLE DUPLICATE: 3256292
92536425001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mglL
235
239 2
SAMPLE DUPLICATE: 3256293
92536431001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mglL
203
203 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 33

aceAnalyfrcal
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 618249
Analysis Method: SM 4500-S2D-2011
QC Batch Method: SM 4500-S2D-2011
Analysis Description: 4500S2D Sulfide Water
Laboratory: Pace
Analytical Services -Asheville
Associated Lab Samples: 92536420001, 92536420002
METHOD BLANK: 3252970
Matrix: Water
Associated Lab Samples: 92536420001, 92536420002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Sulfide mg/L
ND 0.10
05105/2105:54
LABORATORY CONTROL SAMPLE: 3252971
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Sulfide mg/L
0.5 0.54
108 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3252974 3252975
MS MSD
92536434001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Sulfide mg/L ND
0.5 0.5 0.49
0.52 97 104
80-120 7
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3252985
3252986
MS MSD
92535951003
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Sulfide mg/L ND
0.5 0.5 0.56
0.57 112 114
80-120 2
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 33

aceAnalytical
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QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 619192 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92536420001, 92536420002
SAMPLE DUPLICATE: 3257845
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 3257846
Parameter
pH at 25 Degrees C
92535411001 Dup
Units Result Result
Std. Units 7.6 7.5
92536889002 Dup
Units Result Result
Std. Units 6.6 6.2
RPD Qualifiers
1 H3
RPD Qualifiers
5 D6,H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 33

,1!aceAna1ytical
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QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 618437 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92536420001
METHOD BLANK: 3253905
Associated Lab Samples: 92536420001
Parameter Units
Sulfate mg/L
LABORATORY CONTROL SAMPLE: 3253906
Parameter Units
Sulfate mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 05/06/21 07:39
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
50 51.6 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3253907 3253908
MS MSD
92535019002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 3.2 50 50 53.0 53.8 100 101 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3253909 3253910
MS MSD
92535019012 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/1 ND 50 50 49.8 51.6 99 103 90-110 4
Results presented on this page are in the units indicated by the "Units" column except when: an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 33

aceAnalylfical'
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QUALITY CONTROL DATA
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 618439 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92536420002
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2807B
{704)875-9092
METHOD BLANK: 3253920
Matrix: Water
Associated Lab Samples: 92536420002
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Sulfate mg1L
ND 1.0
0510512120:33
LABORATORY CONTROL SAMPLE: 3253921
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits
Qualifiers
Sulfate mg1L
50
52.4
105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3253922
3253923
MS
MSD
92536420002
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
Sulfate mglL 2.0
50
50 55.6
55.0 107
106
90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3253924
3253925
MS
MSD
92535190010
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
Sulfate mg/L 125
50
50 162
159 75
68
90-110 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
Date: 06/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 33

acmnalytical V
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i
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
hiuntersville, NC 28078
[phone]
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 618108
Analysis Method:
EPA 420.4 Rev i.0 1993
QC Balch Method: EPA 420.4 Rev 1.0 1993
Analysis Description:
420.4 Phenolics
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92536420001, 92536420002
METHOD BLANK: 3262121
Matrix: Water
Associated Lab Samples: 92536420001, 92536420002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Phenolics, Total Recoverable mglL
ND 0.020 05/05/21 13:26
LABORATORY CONTROL SAMPLE: 3252122
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Phenolics, Total Recoverable mglL
0.05 0.047
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3252123 3252124
MS MSD
92535972001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Cone. Cortc. Result
Result % Rec % Rec Limits RPD Qual
Phenolics, Total Recoverable mg1L ND
0.05 0.05 0.045 0.035 87 68 90-110 23 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3252125 3252126
MS MSD
92535972005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual
Phenolics. Total Recoverable mg1L ND 0.05 0.05 0.045 0.048 88 94 90-110 7 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 33

aceAnalytical
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Project: Al & A2
Pace Project No.: 92536420
QC Batch: 618558
QC Batch Method: SM 4500-CN-E-2011
Associated Lab Samples: 92536420001
METHOD BLANK: 3254652
Associated Lab Samples: 92536420001
Parameter Units
Cyanide mg/L
LABORATORY CONTROL SAMPLE: 3254653
Parameter Units
Cyanide mg1L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 4500-CN-E-2011
Analysis Description: 450OCNE Cyanide. Total
Laboratory: Pace Analytical Services - Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0080 05/07/2100:22
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
0.1 0.095 95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3256227 3256228
MS MSD
92535839002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RP❑ Qual
Cyanide mg/L ND 0.1 0.1 0.083 0.093 83 93 80-120 12 R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3256229 3256230
MS MSD
92535857002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Cyanide mg]L ND 0.1 0.1 0.092 0.091 88 86 80-120 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fui1.
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 33

aceAna1j4ica1
www.pat oJobs.corn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704i875.9092
Project: Al & A2
Pace Project No.: 92536420
QC Batch: 619478
Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011
Analysis Description: 450OCNE Cyanide, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92536420002
METHOD BLANK: 3259164
Matrix: Water
Associated Lab Samples: 92536420002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Cyanide mg1L
ND 0.0080
05112/2100:06
LABORATORY CONTROL SAMPLE: 3259165
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Cyanide mg1L
0.1 0.11
105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3259176 3259177
MS MSD
92536840001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Cyanide mglL ND
0.1 0.1 0.098
0.10 98 100
80-120 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3259178 3259179
MS MSD
92537651001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Cyanide mglL ND
0.1 0.1 0.063
0.029 63 29
80-120 73 M1,Rl
Result$ presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services. LLC.
Page 28 of 33

IX,i2aceAnalyfical":
www.pacela0sxem
QUALIFIERS
Project: Al & A2
Pace Project No.: 92536420
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyle in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acryionitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNi - The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/17/2021 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 33

1�aceAnalyfical'
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HvnlersviRe, NC 28078
[phone]
Project:
Pace Project No.:
Al & A2
92536420
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92536420001
Al
EPA1664B
620717
92536420002
A2
EPA1664B
620717
92536420001
Al
EPA 200.7 Rev 4.4 1994
618115
EPA 200.7 Rev 4.4 1994
618224
92536420002
A2
EPA 200.7 Rev 4.4 1994
618115
EPA 200.7 Rev 4.4 1994
618224
92536420001
Al
EPA 245.1 Rev 3.0 1994
618032
EPA 245.1 Rev 3.0 1994
618117
92536420002
A2
EPA 245.1 Rev 3.0 1994
618032
EPA 245.1 Rev 3.0 1994
618117
92536420001
Al
EPA 625.1
617823
EPA 625.1
617961
92536420002
A2
EPA 625.1
617823
EPA 625.1
617961
92536420001
Al
EPA 624.1
618052
92536420002
A2
EPA 624.1
618052
92536420001
Al
SM 254OD-2011
618816
92536420002
A2
SM 254OD-2011
618816
92536420001
Al
SM 4500-S2D-2011
618249
92536420002
A2
SM 4500-S2D-2011
618249
92536420001
Al
EPA 9040C
619192
92536420002
A2
EPA 9040C
619192
92636420001
Al
EPA 300.0 Rev 2.1 1993
618437
92536420002
A2
EPA 300.0 Rev 2.1 1993
618439
92536420001
Al
EPA420.4 Rev 1.0 1993
618108
EPA420.4 Rev 1.0 1993
618344
92536420002
A2
EPA 420.4 Rev 1.0 1993
618108
EPA 420.4 Rev 1.0 1993
618344
92536420001
Al
SM 4500-CN-E-2011
618558
SM 4500-CN-E-2011
618849
92536420002
A2
SM 4500-CN-E-2011
619478
SM 4500-CN-E-2011
619510
Date: 05/17/2021 03:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written Consent of Pace AnalyVcal Services, LLC.
Page 30 of 33

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ceAnalWical
.•w J..1. V•1�fA M.r
Sample Receivin Non -Conformance Form (NCF)
Date: - T2 Evaluated by:
Affix Workorder/Login Label Here or List Pace
Client: ,� f�, i(a � m oz Workorder Number or MTJL Log -in Number
t Here
I. If Chain -of -Custody (COC) is not received: contact client and if necessary, fill out a COC and indicate that it was filled out by
lab personnel. Note issues on this NCF.
2. If COC is incomplete check a licable Issues below and add details where appropriate:
Collection date/time �not
Analyses or analytes: missing or Samples listed on COC do not match samples
incorrectclarification needed received missin , additional, etc. Sample IN on COC
runjuiieu tr oianKs were
Comments/Details/Other Issues not listed above:
3. Sample ante ri issues: check a licable issues below and add details where appropriate:
Samples: Condition needs to be brought to ._ . ___
Samples: Past holding -limp— -- -i�h- ��.w: �.,= T= - r:. .. -------_-
Sam les: Not field filtered Containers: Broken or com romised Temperature: not within acceptance criteria (typically
Samples: in volume 0-6C
received Containers: Incorrect Temperature: Samples arrived frozen
Samples: Cooler damaged or Custody Seals: Missing or compromised on
-compromised romised sam les, tripblanks or coolers Vials received with improper heads ace
Samples: contain chlorine or
sulfides Packing Material:lnsufticienUlm ro er Other:
Comments/Details:
7Y yr Ok WK Afc-e i,e) tt� inn I719tf ���SF�s
P
D. _uenr contact: If client is contacted for any issue listed above, fill in details
PM Initials: I
Client Comments/Instructions:
F-ALL-C-011-rev.00, 05Jul2018
Page 33 of 33