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(�5a'neAnaljdical' ANALYTICAL REPORT May 18, 202 i Piedmont Geologic Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: L1347963 05/05/2021 1751 ABB Inc. PINETOPS, NC Pete Dressel 6003 Chapel Hill Rd Ste 145 Raleigh, NC 27607 Entire Report Reviewed By: Heather J Wagner Project Manager Results relate only to the items tested of calibrated and are reported as rounded values. This test report shall not be reproduced. except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0057 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided. and as the samples are recewed. sRh` u 1 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Piedmont Geologic 1751 L1347963 05l18l21 1153 1 of 12 TABLE OF CONTENTS Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 I-SIS OUTFALL-001 L1347963-01 5 Qc: Quality Control Summary 6 Fn] Gravimetric Analysis by Method 2540 D-2011 6 SI Wet Chemistry by Method 1664E 7 Metals (ICP) by Method 200.7 8 Metals (ICPMSI by Method 200.8 9 GI GI: Glossary of Terms 10 Al: Aecreditations & Locations 11 Sc: Sample Chain of Custody 12 Sc ACCOUNT. PROJECT: SDG: DATEMM E: PAGE: Piedmont Geologic 1751 L1347963 05/18/21 13:53 2 of 12 OL-Im SAMPLE SUMMARY OUTFALL-001 L1347963-01 WW NILA;)! Y Method Gravimetric Analysis by Method 2540 0-2011 Wei Chemistry by Method 1664E Metals (ICPI by Method 200.7 Metals IICPMS) by Method 200.8 Batch Dilution Preparation Analysis Afi,flytil Location date/time dateltime WG1667670 1 0511012713:23 0511012113:29 CAT Mt Juliet, TIN WGI666022 1 05106/210951 05107/2105:40 LTC MI, Juliet. 7N WGI669599 1 05113121 08:32 05r3/21 23'56 CCE Mt. Juliet, TN WG1668227 I 051I5121 01!26 05/1512118:28 JPD Mt Juliet, TN ACCOUNT: PROJECT: SDG: DATE(TIME: PAGE: Piedmont Geologic t751 L1347963 05/180113:53 3 of 12 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the Ll appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control El are vdit'nin established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my q knowledge, all prot�lemslanomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. Sr f L� GI Feather J Wagner Project Manager I qC ACCOUNT: PROJECT: SDG: DATEITIM E: PAGE: Piedmont Geologic 1751 L1347963 05/18/21 13:53 4 of 12 OUTFALL-001 SAMPLE RESULTS - 01 Collected date/time: 05103121 14:08 L1347963 Additional information - Results for field not �1Ccredited to 150 17025 Result Units Analyte I PH (On Site) 7.7 su Gravimetric Anal1 -;is by I'vlet'iioc 2540 D-2,311 Fs] Result Oualifier RDL Dilution _ Analysis Batch Analyte mgll mgll date 1 time Cn Suspended Sclids 8.27 3.33 1 05110'202113 29 WG15616 Wet Chemistry by Method 1664B Result Qualifier RDL Dilution Analysis Batch Analyte ugll ugll date 1 time Ell TPH -Oil & Grease ND 5880 1 051071202105A0 tiVGi666022 Sample Narrative: E L1347963-01 WG1666022, Total Oil&Grease is non -detect. Extract vras not processed through silica gel I El Metals (ICP) by Method 200.7 Result Qualifier RDL Dilution Analysis Batch SC Analyte ugll ugll date 1 time Lead NO 500 1 05/13/202123:56 WG1669599 Zinc ND 50.0 1 051131202123756 WG1669599 Metals (ICPMS) by Method 200.8 Result Qualifier RDL Dilution Analysis Batch Analyte ugll ugll date 1 time Copper 4.25 1.00 1 05115/202118:28 WG1666227 ACCOUNT: PROJECT: SDG: DATEMM E: PAGE: Piedmont Geologic 1751 L1347963 05/18/21 13:53 5 of12 m m 2 E Ili lz 15 0 E u Cu El F.9 E cr e 00 rn E oo 0 v, E O Ln 0 00 0 04 6 to Ln to �'D u w CL f i E-1 Fw] FA a n� Cy G ,D V ! I O_� m LL � F� zo r OJ U F— `..D V J Q t7 m 4 Ln E u J e n D 0 z 0 u 0 4 E Ln to 40 cz �R co co �-) Lr) rn u ;-o Ln 0 E-1-11 F-I m F-I m m m z W 0 O O t _ CO N � � 00 g c IL QD to V v O i z a N O: N m c N N N 0 m 0 m m a : U E �n u o d N m 3" n _ O Q C? M X O vni Ln N 0 N A CD 0 It to +n ir eo V? a U d o d v I J a C 3e O N Ln �i a 0 N CA00 O M m LO (fl N m tn cc N N 0 0 L m mm J :. CK a v O '.J Mo v J iJ Y Co i U7 �y G O cll fV C O 0 C� Q0 O 00 cq J IS J n CL C e 0 9 0 Ln o 7W GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report. include Permit Limits. Project Name, Sample ID. Sample Matrix. Sample Preservation. Field Blanks, Field Spikes, Field Duplicates On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy ofthis information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec. Recovery, RPD Relative Percent Difference. SDG Sample Delivery Group. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes In the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field. the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful OC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result In this column may state "ND" (Not Detected) or "SDL" Result (Below Detectable Levels). The Information In the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results. Including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Oc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG. ACCOUNT: PROJECT, SOG: DATEITIME: PAGE: Piedmont Geologic 1751 L1347963 05A8121 13'53 10 of 12 ACCREDITATIONS & LOCATIONS Pace An,*ticed National 12065 l- n. ; r l i Pd n^C_II It Julia. TN 371212 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TNOOD032021-1 Arizona AZO612 New Hampshire 2975 Arkansas 68-0469 New Jersey—NELAP TNO02 California 2932 New Mexico TNODO03 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E97497 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-I40 Idaho TN00003 Ohio—VAP CLOO69 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA0003S6 Kentucky'6 KY90010 South Carolina 84004002 Kentucky 16 South Dakota nla Louisiana AI30792 Tennessee' ` 2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas s LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TNO03 Vermont VT20D6 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERTOD86 Wyoming A2LA A2LA— ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA — ISO 17025 s 1461,02 DOD 1461.01 Canada 1461,01 USDA P330-15-00234 EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks ' Aquatic Toxicity ° ChemicallMicrobiologlcal 'Mold "Wastewater nla Accreditation not applicable Not all certifications held by the laboratory are applicable to the results reported in the attached report. 'Accreditation is only applicable to the test methods specified an each scope of accreditation held by Pace Analytical. ACCOUNT: PROJECT: Si DATEMME: PAGE: Piedmont Geologic 1751 L1347963 05/18/2113:53 11 of 12 ca 4 r� rV ODO \ tr ar x w 41 o A u c •, a' ee N @ N c 0 0 0ti �m 3 _0 - I a Y n saJdON 3d4H-31 SSI x �J r �1 9'80 dH X3H9OHd1 x '7 EONH-3dOHiLudSZ gn]'d9INZ'd7igd x F U V i l A � N n a d _ R c m co .Y - O kA cu n m 4� O a n = to o ur (U o rfl e N T ry °_ a 0 't p ? N b A W O 7 YS E pq a a a O n Y m m m F 1^ ti m p Q 'y rF d ^t p q ` O r v = r rp O o a � �M l � V V tt Ll Z � �' > r � y re � •.1 m a O E o 3 e t7 141 CL �rl.-i na U0 4ai l 0 flJ oC r -- c. I E h c Z a ° n Q) � O 2 '.' � ce m c a V1 CO z Ql cn { v K 3 a x c A o p y n � ❑. win a ec a G 0 I