WQ0032723_Renewal Application_20210528

Initial Review
Reviewer Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Permit Number (IR)* WQ0032723
Applicant/Permittee City of Reidsville
Applicant/Permittee Address 1100 Vance Street, Reidsville, NC 27320
Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No
Owner Type Municipal
Facility Name City of Reidsville DCAR
County Rockingham
Fee Category Minor
Is this a complete
application?*
c Yes r No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review bythe hydrogeologist?* r Yes r No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount $0
Complete App Date 05/28/2021
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Kendall
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by NI3 Staff
Name * Brent Collins
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ....................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
336-751-1441
O Modification - Minor
G Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00032723
Fbs Current Existing permt number
Applicant/Permittee * City of Reidsville
Applicant/Permittee Address* 1100 Vance Street, Reidsville, NC 27320
Facility Name * City of Reidsville DCAR
Please provide comments/notes on your current submittal below.
The PDF was put together and the plant vicinity map was left out. Once the document is
signed it cannot be edited. I will provide the vicinity map as soon as someone receives the
permit renewal. Thank you.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Rc.)
City of Reidsville WTP Permit Renewal - W00032723.pdf 5.36MB
upload only 1 RCFdocurrent (less than 250 W). NLfliple documents rust be corrbined into one PDF file unless file is larger than
upload limit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
06' &o ¢

Submission Date 5/28/2021

g
Inc.
Permit Renewal Application
For
City of Reidsville WTP
WQ0032723
Distribution of Residual Solids
(503 Exempt)
Prepared By:
EMA Resources Inc.
755 Yadkinville Road
Mocksville, NC 27028
336-751-1441
May 26, 2021
Phone [phone] — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27028

May 26, 2021
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1617 Mail Services Center
Raleigh, NC 27699-1617
RE: Permit Renewal — WQ0032723
To Whom it May Concern:
EMA Resources is submitting the included permit renewal for the Reidsville WTP permit
- WQ0032723. There are no modifications included in this renewal. The process has not
changed and there are no dry ton changes requested.
If you have any questions concerning this renewal, please contact Brent Collins —
Director of Technical Services
Respectfully,
Brent Collins
Director of Technical Services
brent.collinsgemaresourcesinc.com
[phone]
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

Table of Contents
1) DCAR Form
a) Current Permit
2) Program Information
3) RSC Form
a) Vicinity Map
b) Process Flow Diagram & Process Summary
c) Quantitative Justification
d) Sampling Plan
4) Residuals Quality Information
a) Laboratory Analytical Reports
b) Residuals Information Sheet
5) Operation & Maintenance Plan

1) DCAR Form

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
L APPLICANT INFORMATION:
1. Applicant's name: City of Reidsville
Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership E:1 Privately -Owned Public Utility
❑ Federal ❑ State ® Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Jerry Rothrock Title: Interim Public Works Director
Applicant's mailing address: 1100 Vance Street
City: Reidsville State: NC Zip: 27320-
Telephone number: [phone] Email Address: irothrock&reidsvillenc.gov
2. Consultant's name: Brent Collins License Number (for P.E.):
Affiliation: ❑ On Staff ® Retained (Firm: EMA Resources Inc.)
Consultant's mailing address: 755 Yadkinville Rd
City: Mocksville State: NC Zip: 27028-
Telephone number: [phone] Email Address: brent.collinsA_emaresourcesinc.com
3. Fee submitted: $0 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00032723
Date of most -recently issued permit: 09/23/2016
Date of most -recently certified Attachment A (if different than the permit): 09/23/2016
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Reidsville WTP
City: Reidsville State: NC Zip: 27320-
Coordinates: Latitude: 36' 17' 02" Longitude: 79. 39' 36"
Datum: NAD83 Level of accuracy: nearest second
Method of measurement: GPS
County where facility is located: Rockingham
2. Facility contact (person familiar with residuals preparation):
Name: Scott Jewell Title: WWTP Superintendent
Mailing address: 278 Reid Lake Rd.
City: Reidsville State: NC Zip: 27320-
Telephone number: (L36) 342-4001 E-mail address: siewellgci.reidsville.nc.us
FORM: DCAR 06-16 Page 1 of 3

3. Is the residual process facility also the generator? ® Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: 700 days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other (explain); Land applied at agronomic rates per this permit — W00032723
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials Amounts to be added
Der 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: 200 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 200 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): Two — 1.25 MG sludge lagoons with an average storage time of 12 months and
a maximum of 27 months.
6. Does the facility have a stormwater management plan? ❑ Yes; ® No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled:
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
e
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes L] No, Explain;
I, Jerry Rothrock — Interim Public Works Director
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for City of Reidsville WTP
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature.
cJY4 W Mai/ 28 2021
Jerry W. lzothrock (May 28, 202111:05 EDT) J
Date:
FORM: DCAR 06-16 Page 3 of 3

la) Current Permit

PAT MCCRORY
Water Resources
ENVIRONMENTAL Ot1AL11 Y
September 23, 2016
KEVIN E. EASON, PE — PUBLIC WORKS DIRECTOR
CITY OF REIDSVILLE
l 100 VANCE STREET
REIDSVILLE, NORTH CAROLINA 27320
Dear Mr. Eason:
❑ONALD R. VAN DER VAART
S..IAY ZIMMERMAN
Subject: Permit No. WQ0032723
Reidsville WTP
Distribution of Class A Water
Treatment Plant Residuals
Rockingham County
In accordance with your permit renewal request received July 29, 2016, and subsequent additional
information received September 6, 2016, we are forwarding herewith Permit No. WQ0032723 dated
September 23, 2016, to the City of Reidsville for the continued operation of the subject residuals
management program. Please note that this renewed permit shall become effective on January 1, 2017 (i.e.
the day after the expiration date of the existing permit).
This permit shall be effective from January 1, 2017 until December 31, 2021, shall void Permit No.
WQ0032723 issued May 1, 2008, and shall be subject to the conditions and limitations as specified therein.
Please pay particular attention to the monitoring requirements listed in Attachment A for they may differ
from the previous permit issuance. Failure to establish an adequate system for collecting and maintaining
the required operational information shall result in future compliance problems.
Please note the following permit conditions have been removed since the last permit issuance
dated May 1, 2008:
➢ Old Condition II.S., [1.10., 11.14. and II.15. — Not applicable to distribution permits.
➢ Old Condition I1.12. — Compliance Boundaries do not apply to distribution permits.
➢ Old Condition I1.13. — Review Boundaries do not apply to distribution permits.
➢ Old Condition 111.4. — Other sites can be found if soils fail to assimilate the residuals, so no
need to void the permit.
➢ OId Condition III.7. -- Redundant since covered by Old Condition 111.6.
➢ Old Condition 111.11. — Superseded by Conditions 1I1.9. and I11.10. for Utilization Agreement.
Read carefully.
➢ OId Condition 111.12. -- Superseded by Conditions 111.9. and IIl.10. for Utilization Agreement.
Read carefully.
State of North Carolina 1 Environmental Quality I Water Resources j Water Quality Permitting I Non -Discharge Permitting
1617 Mail Service Centet I Raleigt4 North Carolina 27699-1617
919 807 6464

Mr. Kevin E. Eason
September 23, 2016
Page 2 of 3
➢ Old Condition IV.8. — Record keeping duration requirements are part of each individual record
keeping requirement.
Please note the following permit conditions are new since the last permit issuance dated May
1, 2008:
➢ Condition II1.2. —Operations and Maintenance (O&M) Plan requirements are set out.
➢ Condition II1.4. — Similar to Old Condition 111.5., but now the O&M Plan shall be kept on site
as well.
➢ Condition III.7. — Vegetative cover requirement.
Condition I11.9. — Requirement for Utilization Agreement. Read carefully.
➢ Condition 111.10. -- Requirements of terms of Utilization Agreement. Read carefully.
➢ Condition III.13. — No distribution to those who over -apply residuals. Reporting requirement
if Permittee knows others are over -applying residuals.
Condition V1.6. — Similar to Old Condition V1.6., but 60-day notification now required prior
to revocation or modification.
Condition VI.7. — Expansion of existing facility not allowed without variance if Permittee
exhibits behavior detrimental to environment.
If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Troy Doby at (919) 807-
6336 or troy.dobv�i�nedeni goy.
Sincerely,
S. Jay Zimmerman, P.G., Director
Division of Water Resources
cc: Rockingham County Health Department (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Beth Buffington — Protection and Enforcement Branch (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Files

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
1117161�4I"II
DISTRIBUTION OF CLASS A WATER TREATMENT PLANT RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
City of Reidsville
Rockingham County
FOR THE
continued operation of a residuals management program for the City of Reidsville and consisting of the
distribution of Class A Water Treatment Plant residuals generated by the approved facility listed in
Attachment A with no discharge of wastes to surface waters, pursuant to the application received July 29,
2016, and subsequent additional information received by the Division of Water Resources, and in
conformity with other supporting data subsequently Fled and approved by the Department of
Environmental Quality and considered a part of this permit. The use and disposal of residuals are regulated
under Title 40 Code of Federal Regulations Part 257. This permit does not exempt the Permittee from
complying with the federal regulations.
This permit shall he effective from January 1, 2017 until December 31, 2021, shall void Permit No.
WQ0032723 issued May 1, 2008, and shall be subject to the following specified conditions and limitations:
I. SCHEDULES
I . No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application.
[15A NCAC 02T .0108(bX2), 02T .0105(d), 02T .01091
[I. PERFORMANCE STANDARDS
The subject residuals management program shall be effectively maintained and operated at all times so
there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distribution of residuals, contact the Winston-Salem Regional Office supervisor, and take any
immediate corrective actions. [G.S. 143-215.1 ]
WQ0032723 Version 2.0 Shell Version 160210 Pang I + 11

2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02B .0200,
02L .0100]
3. Only residuals generated by the facilities listed in Attachment A are approved for distribution in
accordance with this permit. [G.S. 143-215.1]
4. PoIlutant concentrations in residuals distributed or applied to any land application site shall not exceed
the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis):
Parameter
Ceiling Concentration
(milligrams per kilogram)
Monthly Average
Concentration
(milligrams per kilogram)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
nla
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
[15A NCAC 02T. 11051
5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T
.1106 (b)(2). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1106]
6. Setbacks for treatment and storage facilities shall be as follows:
Setback Description
Setback
feet
Habitable residence or place of public assembly under separate ownership or not to
be maintained as part of the project site
100
Property lines
50
Private or public water supply
100
Surface waters (streams — intermittent and perennial, perennial waterbodies, and
wetlands)
50
Wells with exception to monitoring wells
100
[15A NCAC 02T. 11081
WQ0032723 Version 2.0 Shell Version 160210 Paap I of 1

7. Setbacks for Class A land applied bulk residuals shall be as follows:
Setback by residual type
Setback Description
(feet)
Liquid
Cake
Private or public water supply
100
100
Surface waters (streams — intermittent and perennial,
100
25
perennial waterbodies, and wetlands)
Surface water diversions (ephemeral streams,
25
0
waterways, ditches)
Groundwater lowering ditches (where the bottom of
25
0
the ditch intersects the SHW
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported and
spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast spreader or
other equipment designed for handling solid materials) without leaving any significant liquid
fraction behind.
[I 5A NCAC 02T .1108]
8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance
of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen
requirements based on the determined Realistic Yield Expectations (RYE) using any of the following
methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (lttt:Iliiutrients.soil.nesu.edu! ields/index. h ). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the Iocal Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter I
(http://www.iicagr.gov/SWC/tech/documents/9th Guidance Doc 100109, df).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(ftp://ft-fc.sc.egov.usda.yov/NHQ/practice-standards/standards/590.pdf).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[ 15A NCAC 02T . i 109(bx l)(k)]
WQ0032723 Version 2.0 Shell Version 160210 Pace 'i of 1 1

Ill
4. The Permittee shall not distribute Class A Water Treatment Plant residuals that have a sodium
adsorption ratio (SAR) of 10 or higher without prior written Division approval. The Permittee may
seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high
SAR content; has agreed on proper residual application rates; and has agreed to operational
considerations to ensure that the high SAR content will not adversely impact the receiving sites.
Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a
mechanism for maintaining site integrity and conditions conducive to crop growth, can be obtained
from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services,
the Natural Resource Conservation Service, a North Carolina Licensed Sail Scientist, or an agronomist.
[15A NCAC 02T .0108(b)(1)]
OPERATION AND MAINTENANCE RE UI REM ENTS
The residuals management program shall be properly maintained and operated at all times. The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water or groundwater standards. [ 15A NCAC 02T . 1110]
2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications
to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan,
at the minimum, shall include:
a. Operational functions;
b. Maintenance schedules;
c. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions to be taken
by the inspector in the event that noncompliance is observed pursuant to the noncompliance
notification requirements under the monitoring and reporting section of the permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen reduction requirements (e.g. facilities that distribute multiple times per year but
have an annual sampling frequency, may need to sample during winter months when pathogen
reduction is most likely to be negatively affected by cold temperatures).
[ 15A NCAC 02T. I 1001
W00032723 Version 2.0 Shell Version 160210 Page 4 of I ]

3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in responsible
charge (ORC) and one or more certified operators as back-up ❑RCs in accordance with 15A NCAC
08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204,
or as specified in the most recently approved O&M plan (i.e., see Condition III.2.), and shall comply
with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and
designation requirements, please contact the Division of Water Resources' Protection and Enforcement
Branch at [phone]. [ 15A NCAC 02T A 117]
4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be
maintained at the land application sites during land application activities. [ I5A NCAC 02T
.0108(b)(1)]
When the Permittee transports or land applies bulk residuals, the spill control provisions shall be
maintained in all residuals transport and application vehicles. [ 15A NCAC 02T .1 l 10]
6. When the Permittee land applies bulls residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals from the land application sites onto adjacent
properties or into surface waters. [G.S. 143-215.1]
7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land
application sites onto which residuals are applied, or application shall be in accordance with the crop
management plan outlined by the local Cooperative Extension Office, the Department of Agriculture
and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved
by the Division. [ 15A NCAC 02T .1109(b)(1)]
H. Bulk residuals shall not be land applied under the following conditions:
a. If the residuals are IikeIy to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the
residuals would occur;
e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a
24-hour period following a residuals land application event;
f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
18% for injected or incorporated bulk liquid residuals;
h. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to
achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the
pH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved variations
to the acceptable soil pH (6.0) will be noted in this permit;
i. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in a
USDA no -till program shall be exempted from meeting this vegetative cover requirement;
j. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
k. If the vertical separation of bedrock and the depth of residuals application is less than one foot:
W00032723 Version 2.0 Shell Version 160210 Pave s of i i

1. Application exceeds agronomic rates.
[15A NCAC 02T. 11091
9. A dated Utilization Agreement between the Permittee, his subcontractor distributing and applying the
residuals, and the entity agreeing to accept Class A bulk residuals shall be in place prior to distribution
of the bulk residuals. The agreement shall specify the subcontractors and the agreeing entity's
responsibilities. The Permittee, the subcontractor, and the entity accepting the Class A bulk residuals
shall sign the Utilization Agreement. 'The Utilization Agreement shall have a clause allowing the
recipient of the residuals to end the Utilization Agreement at any time by notifying the Permittee in
writing. if the recipient ofthe residuals sells the property, the Utilization Agreement shall automatically
terminate. If the permit is rescinded, the Utilization Agreement shall automatically terminate. The
duration of the Utilization Agreement shall be one to which the Permittee, the subcontractor, and the
recipient of the residuals agree. Any changes in the agreement that are necessitated by changes in the
permit shall be mailed to the subcontractor and the recipient of the residuals by certified mail with
return receipt. The Permittee shall keep these records on file for inspection by the Division for each
Utilization Agreement while that Utilization Agreement is in force. [ 15A NCAC 02T .0108(b)(1), 02T
.1104]
10. At a minimum, the Utilization Agreement shall stipulate the following:
a. By agreeing to accept the bulk Class A residuals, it is recognized that the application of these
residuals is allowed under the conditions of this agreement including the prohibitions contained in
Condition II1.8. Land application of Class A residuals is considered the beneficial reuse of a waste
under 15A NCAC 02T .I 100, and has been deemed permitted under 15A NCAC 02T .1103(4)
provided the conditions of this agreement are met. Any action resulting in damages to surface water
or groundwater, caused by failure to follow the conditions of this agreement, is subject to Division
enforcement action;
b. The person or entity accepting the bulk Class A residuals shalt to the best of his knowledge meet
the following application requirements:
i. Class A Water Treatment Plant Residuals shall not be stockpiled for more than 60 days (after
the delivery of the last load) prior to land application unless the permittee notifies the Winston-
Salem Regional Office and receives approval to exceed the 60-day limit. At a minimum, the
information provided shall be the location, the date that the last load was delivered, the quantity
of residuals stockpiled, the percent solids of the residuals stockpiled, measures taken to prevent
stockpile runoff (e.g. placement, perimeter berms, etc.) and the anticipated date the residuals
will be spread.;
ii. Application of bulk residuals shall not occur within 100 feet of a public or private water supply
source;
iii. Application of bulk residuals shall not occur within 100 feet of any well, with the exception of
Division approved monitoring wells;
iv. Application of bulk residuals shall not occur within 25 feet of surface waters.
c. The generator of the Class A bulk residuals shall provide information on the proper use of the
residuals, including information on the nutrient quantities within the residuals and recommended
application rates. A copy of the label or information sheet attached to bags or other containers, as
specified in the labeling requirements under Condition IIl.12., is sufficient;
d. The applicator or party accepting bulk residuals from the Permittee shall supply all third parties
receiving bulk residuals with documentation specifying that application shall occur consistent with
the utilization agreement;
e. Instructions, including contact information for key personnel, shall be provided to the applicator or
party receiving bulk residuals in the event that any requirements specified in the utilization
agreement are not met.
WQ0032723 Version 2.0 Shell Version 160210 Page 6 of f 1

f. A copy of the Utilization Agreement shall be maintained at the land application sites when bulk
residuals are being applied.
f 15A NCAC 02T .0108(b)(1), 02T. 1104]
11, All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may
be placed on a concrete pad, placed under shelter or physically covered until it is distributed to the
buyer. If an alternate storage site is used, approval must be obtained from the Division. [15A NCAC
02T .0108(b)(1)]
12. A label shall be affixed to the bag or other container in which residuals are sold or given away for land
application, or an information sheet shall be provided to the person who receives Class A residuals. At
a minimum, the label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
b. A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet;
c. A statement identifying that this material shall be prevented from entering any public or private
water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.);
d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
[15A NCAC 02T .1109(a)]
13. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals
contrary to the condition of the signed Utilization Agreement. The Permittee shall report to the
Winston-Salem Regional Office as per reporting conditions under Condition IV.8. any person or entity
known to be applying residuals contrary to the condition of the signed Utilization Agreement. [I SA
NCAC 02T .1103(a)]
WQ0032723 Version 2.0 Shell Version 160210 Ncre 7 of 11

1V. MONITORING AND REPORTING REQUIREMENTS
Any Division -required monitoring (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)]
Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA), Residuals that tests or is classified as a hazardous or toxic waste under 40
C1 R Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability,
reactivity, and toxicity characteristic leaching procedure (TCLP)i shall be performed at the
frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of
five years. Any exceptions from the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,I-Dichloroethylene (0.7)
Pyridine (5,0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Heptachlor (and its hydroxide)
0.008
Toxaphene (0.5)
Chloroform (5.0)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (5ilvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[15A NCAC 13A .0102(b), 02T .l 101, 02T .1105]
WM032721 Vercinn 7 0 Chril 'If prV;n" Irn )1A

3. An analysis shall be conducted on the Class A residuals at the frequency specified in Attachment A,
and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the
following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[I5A NCAC 02T .I 101]
4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency
specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the
approved O&M plan. The required data shall be specific to the stabilization process utilized, and
sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC
02T .1106 (b)(2), and one vector attraction reduction requirement in 15A NCAC 02T .1107 (a) shall be
met. Any exceptions from the requirements in this condition shall be specified in Attachment A. [15A
NCAC 02T .1106, 02T .l 107, 02T .1111(c)]
5. Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be
in accordance with the monitoring requirements in 15A NCAC 02B .0505. [ 15A NCAC 02B .0505]
6. The Permittee shall maintain records tracking all bulk residual distribution or land application events
performed by the Permittee. At a minimum, these records shall include the following:
a, Source of residuals;
b. Date of distribution/land application;
c. Name and address of recipient of residuals;
d. Volume of residuals distributed to each recipient;
e. Intended use of residuals;
f. If land application events performed by the Permittee - Nitrogen Application Rate based on RYEs
(if using data obtained from the North Carolina State University Department of Soil Science
Website, the printout page shall be kept on file and reprinted every five years).
[I 5A NCAC 02T .0I 09(a)]
7. Three copies of an annual report shall be submitted on or before March V. The annual report shall
meet the requirements described in the Instructions for Residuals Application Annual Reporting Forms.
Instructions for reporting and annual report forms are available at
http•Hl2ortal.iicdenr.orglweb/wq/gps/laulreUg ing, or can be obtained by contacting the Land
Application Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
WQ0032723 Version 2.0 Shell Version 160210 Paae 9 of 11

[ 1 SA NCAC 02T . l 1 l 1(a)]
8. Noncompliance Notification
The Permittee shall report by telephone to the Winston-Salem Regional Office, telephone number (336)
776-9800, as soon as possible, but in no case more than 24 hours or on the next working day following
the occurrence or first knowledge of the occurrence of any of the following:
a. Distribution of residuals abnormal in quantity or characteristic.
b. Any failure of the distribution program resulting in a release of material to surface waters.
c. Any time self -monitoring indicates the facility ,has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone].Persons
reporting such occurrences by telephone shall also file a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
betaken to ensure that the problem does not recur. [15A NCAC 02T .0I05(1), 02T .0108(b)(1)]
V. INSPECTIONS
The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [ 15A NCAC 02T ,0108(b)]
Prior to each bulk residuals distribution event, the Permittee or his designee shall inspect the residuals
processing, storage, transport and distribution facilities to identify malfunctions, facility deterioration
and operator errors that could result in discharges to the environment, pose a threat to human health or
be a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the
date and time of inspection, observations made, and any maintenance, repairs, or corrective actions
taken. The Permittee shall maintain this inspection log for a period of five years from the date of
inspection, and this log shall be made available to the Division upon request. [15A NCAC 02T
.0108(b)]
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the distribution facilities permitted herein at any
reasonable time for the purpose of determining compliance with this permit; may inspect or copy any
records required to be maintained under the terms and conditions of this permit; and may collect
groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)]
VI. GENERAL CONDITIONS
I. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an
enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to
143-215.6C. fG.S. 143-215.6A to 143-215.6C]
2. This permit shall become voidable if the residuals distribution events are not carried out in accordance
with the conditions of this permit. [ 15A NCAC 02T .01 l0]
3. This permit is effective only with respect to the nature and volume of residuals described in the permit
application and other supporting documentation. [G.S. 143-215.1 ]
W00032723 Version 2.0 Choll Vorcinn 1 Am 10

4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in
I5A NCAC 02D .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and
under the Division's General Permit NCG010000; any requirements pertaining to wetlands under 15A
NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter
143 of the General Statutes. [15A NCAC 02T .0105(c)(6)]
In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [15A NCAC 02T .0110]
7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained
herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b).
[15A NCAC 02T .0120]
8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay
the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T
.0105(e)(3)]
Permit issued this the 23d day of September 2016
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
S. Jay Zimmerman, P.G., Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0032723
WQ0032723 Version 2.0 Shell Version 160210 PROP ► t of i i

ATTACHMENT A _ Approved Residual Sources
City of Reidsville
Owner
City of Reidsville
Total
Facility Name
Reidsville WTP
Maximum Monitoring
Permit Biological Fre uenc for
Cann q Y
County Number Residuals per Y arsi Non -hazardous
Characteristics 2
Rockingham I NCO046345 I No J 1.0o0
1,000
Annually
Certification Date: September 23, 2016
Permit Number: WQ0032723 Version: 2.0
Monitoring
Frequency for
Metals and
Nutrients s,s
See Table Below
1. Maximum Dry Tons per Year is the amount of residuals approved for distribution from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitahility, reactivity, and corrosivity) as stipulated under permit Condition iV.2.
3. Testing of metals and nutrients as stipulated under permit Condition fV.3.
4. Analyses of pathogen reductions as stipulated under permit Condition TVA.
5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above.
Dry Tons Distributed
short tons Per ear
Monitoring Frequency
Established in 40 CFR 503 and 15A NCAC 02T .1 I11
<319
)/Year
=>314 - <1.650
11 uarter (4 times per ear
-�1,650 - <16,500
1160 Days (6 times per ear)
=alb 500
I/month 12 times per ear)
Monitoring
Frequency for
Pathogen &
Vector Attraction
Reductions *, s, 6
None
Approved
Mineralization
Rate
6. Class A Water Treatment Plant residuals are exempt from meeting the pathogen & vector attraction reduction requirements in Condition IV.4., provided they are not mixed with residuals that have
been generated during the treatment of domestic wastewater, the treatment of animal processing wastewater, or the biological treatment of industrial wastewater. The Class A Water Treatment
Plant residuals must be treated and processed in a manner as to not meet the definition of "Biological Residuals" as defined in € 5A NCAC 02T . 11()2(6).
If no distribution events occur during a required sampling period (e.g. no distribution occurs during an entire year when annual monitoring is required), then no sampling
data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to
EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification.
WQ0032723 Version 2.0 Attachment A Page 1 of

2) Program Information

ADDITIONAL INFORMATION
1. Provide a narrative explaining the following:
a. How will the materials be handled and transported from where the residuals were produced
to where it will be treated?
The water plant residuals are strictly sediment which has settled in the sedimentation basin and
accumulated in the filters. The residuals are drawn off the bottom of the sedimentation basins
on a daily basis and pumped to one of the two storage lagoons. The filter wash water is
pumped to the lagoons on a daily basis where any residuals will settle.
b. How will the residuals be processed/treated?
The residuals are not actually processed or treated. See RSCA Form Attachment Order 2-b:
Process flow diagram and narrative.
c. How will leachate collection be handled?
There is no leachate in this system. The decant from the storage lagoon is discharged into
Troublesome Creek pursuant to NPDES Permit #NC0046345.
d. Where will the residuals be stored until processing?
The residuals will be stored in one of two 1,250,000 gallon lagoons.
e. How will the final product be distributed?
The residuals will be delivered to local farmers via 6500 gallon tanker loads. Each load will be
off-loaded to a high flotation applicator for application on a receiver site (grassland or row crop.)
2. Attach a marketability statement detailing destinations and approximate amounts of the final
products to be distributed.
The residuals have limited (N,P,K) nutrient value, but they have additional micro -nutrients that can be
utilized by crops for optimal plant growth. The program will recruit local farmers to participate in the
bulk land application program. Additionally the farmers that currently receive residuals from the
Reidsville WWTP may also participate in the alum residual applications. Additionally, the timing of the
application can me marketed as a water source during drought conditions. Typical application rates will
be from 10-13,000 gallons per acre.
3. Provide either a label that shall be affixed to the bagged process or an information sheet that shall be
provided to the contact person who receives the processed residuals. The label or information sheet
shall contain, at a minimum, the following information.
Note: Residuals will be distributed through bulk land application of liquid managed by the contracted
land application firm. See attached information sheet. (Attachment Order 1-d: Information Sheets)

3) RSC Form

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: City of Reidsville WTP
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current n
Proposed
R
City of Reidsville
Reidsville WTP
Rockingham
WQ0032723
1000
1000
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
'The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: City of Reidsville WTP
2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private.
Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: Scott Jewell — Plant Superintendent
Complete mailing address: 1100 Vance Street
City: Reidsville State: NC Zip: 27320-
Telephone number: [phone] E-mail address: siewell&ci.reidsville.nc.us
4. Facility physical address: 278 Reid Lake Rd
City: Reidsville State: NC Zip: 27320-
Coordinates: Latitude: 36' 17' 02" Longitude: 79. 39' 36"
Datum: NAD83 Level of accuracy: nearest second
Method of measurement: GPS
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
® treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: __E % industrial and % domestic)
❑ other (explain:: ).
6. Does the facility have an approved pretreatment program: ❑ Yes No
7. Facility permitted/design flow: 9 MGD and facility average daily flow: 4_5 MGD
8. Average amount of residuals being generated at this facility 200 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: n/a
Type and volume of residuals storage (i.e., outside of residuals treatment units): Two — 1.25 MG storage lagoons
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
❑ 40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
❑ Biological ® Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical and Date of analysis: 08/04/2020
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes W no. Flashpoint: >170 OF (> 140°F)
Passed reactivity test: W yes Ono. HCN: <0.25 mg/kg (<250) & H2S: <25 mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
0.174
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1,1-Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 08/24/2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
10.6
Cadmium
85
39
<0.455
Copper
4,300
11500
186
Lead
840
300
20.6
Mercury
57
17
0.108
Molybdenum
75
n/a
<3.07
Nickel
420
420
20.9
Selenium
100
100
<7.27
Zinc
7,500
2,800
52
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 4.4 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical and Date of analysis: 08/24/2020
Parameter
Result
(mg/kg)
Aluminum
132000
Ammonia -Nitrogen
3410
Calcium
955
Magnesium
1390
Nitrate -Nitrite Nitrogen
975
pH (Standard Unit)
6.8
Phosphorus
1480
Potassium
1350
Sodium
407
Total Kjeldahl Nitrogen
6070
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.41
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 10 %. This rate
is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
2,946
3,106
Injection/Incorporation
4.651
4,811
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:

❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T. 1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, ❑ heat drying, ?!? heat treatment,
thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
❑ Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.

3a) Vicinity Map

3b) Process Flow Diagram & Process Summary

77
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it 11W
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1 � '
rerr � c
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-- - -- -_-- - I' no' PIPING. PLAN RDV9Z;
---- -- - -�— FiNKBEINER, PETTIS d STROUT, INC..
CONSULTING ENGINEERS . WATER TREATMENT A
---_ -_-- -- -- I CENTERVIEW DRIVE a. PLANT IMPROVEMENTS
GREENSBORO, NC 27407
J.LLw.K t. -
REIDSVILLE, N.C. 4- »`
.S. S.
o .
sBYO rtR

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NONE
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I CENTERVIEW DRIVE
GREENSBORO, NC 27407
.... . . . ...
P 12
111011-E
ROVE XZOLA
PROCESS SCHEMATIC _RDV9902B
WATER TREATMENT AS
PLANT IMPROVEMENTS
REIDSVILLE, NC -2

PROCESS SUMMARY FOR THE
TOWN OF REIDSVILLE WTP
PWS ID# 0279020
The Town of Reidsville WTP is a 9.0 MGD facility located in Rockingham County. It draws its source
from Lake Reidsville. The plant is a conventional plant that uses aluminum sulfate as its coagulant.
They use sodium hydroxide as a pH control. The plant uses potassium permanganate as a measure to
control taste and odor associated with iron and manganese. The plant discharges its wastewater into
two settling ponds. These ponds are periodically emptied using polymer as a dewatering agent. The
ponds only contain aluminum sulfate, sodium hydroxide, potassium permanganate, iron, manganese,
and polymer that has filtered back into the ponds from the sand drying beds.

3c) Quantitative Justification

Quantitative Justification for Residuals Production Rate
Facility:
Reidsville WTP
Requested Permitted Rate:
1,000 dry tons/year
Justification:
Reidsville Water currently produces roughly 250 dry tons of biosolids a year, based on
the calculations below. The below numbers are based on the most recent analysis. The
solids can fluctuate from 4-10%. There are some years that both lagoons may be hauled
and/or cleaned out fully. They are currently permitted for 1000 dry tons a year. We
would like to keep that number in the case of the above.
Calculations:
We are estimating a hauling event once every year totaling 1,250,000 gallons.
(1,250,000 gal) x (4.5% solids) x (8.34 Ibs/gal) = 235 dt/yr
(2,000 Ibs/ton )

3d) Sampling Plan

Sampling Plan
Prior to the first liquid land application event of a calendar year, a representative composite sample
from the two lagoons will be collected. A composite sample from this sampling event will be submitted
to a certified lab for the annual TCLP analysis. (Pace Analytical) A second composite sample from this
sampling event will be submitted to a certified lab for nutrient and metals analysis. (Waypoint
Analytical)
Land application operations will not begin until all analyses have been reported and compliance
documented with all applicable permits and regulations.
The second land application event of the calendar year (if applicable) will duplicate the sampling
procedure explained above minus the TCLP analysis.

4) Residuals Quality Information

4a) Laboratory Analytical Reports

Waypointo
ANALYTICAL
9/8/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-238-0033
Client Project Description: Reidsville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 8/25/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Ijp,
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2021
Arkansas
State Program
88-0650
02/07/2021
California
State Program
2904
05/10/2020
Florida
State Program
- NELAP
E871157
06/30/2021
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program
- NELAP
200078
10/10/2020
Kentucky
State Program
80215
06/30/2021
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program
- NELAP
LA037
12/31/2020
Louisiana
State Program
- NELAP
04015
06/30/2021
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
08/31/2021
Pennsylvania
State Program
- NELAP
68-03195
05/31/2021
South Carolina
State Program
84002
06/30/2021
South Carolina
State Program
84002
06/30/2021
Tennessee
State Program
02027
02/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
09/30/2020
Virginia
State Program
00106
06/30/2021
Virginia
State Program
- NELAP
460181
09/14/2020
Page 1 of 1 00001/20-238-0033
Page 2 of 8

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 20-238-0033
Client Project Description: Reidsville, NC
Lab No Client Sample ID Matrix Date Collected Date Received
87283 Reidsville WTP Solids 08/24/2020 08:45 08/25/2020
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Reidsville, NC
Lab Report Number: 20-238-0033
Date: 9/8/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 87283 (Reidsville WTP)
Analyte: Zinc
QC Batch No: 1-509850/1-509329
Target analyte(s) was identified in the method blank associated with this project, below the Method Quantitation
Limit. The result for the method blank and sample are flagged with the data qualifier J, Estimated Concentration.
Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected in the
method blank.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 88595
Analyte: Mercury
QC Batch No: L509028
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Project Reidsville, NC
Mr. Brent Collins
755 Yadkinville Road
Information
Mocksville , NC 27028
Report Number : 20-238-0033
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 09/08/2020
Received : 08/25/2020
Danyale Love
Project Manager
Lab No : 87283
Matrix: Solids
Sample ID : Reidsville WTP
Sampled:
8/24/2020
8:45
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
95.6
%
0.010
1
08/31/20 17:08
FMM
SW-DRYWT
Ammonia Nitrogen
3410
mg/Kg -
dry
568
568
1
09/02/20 15:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
975
mg/Kg -
dry
112
112
1
08/26/20 14:45
ZBD
4500NO3F-2011
Organic N
<2818
mg/Kg -
dry
2818
5682
1
08/31/20 17:10
CALCULATION
pH
6.8
S.U.
1
08/26/2013:05
ADM
9045D
Total Solids
4.40
%
0.010
0.010
1
08/31/20 17:08
FMM
2540G-2011
Total Volatile Solids
34.4
%
0.010
0.010
1
08/31/20 17:08
FMM
2540G-2011
Total Kjeldahl Nitrogen
6070
mg/Kg -
dry
5680
5
08/31/20 17:10
CLP 4500NORGD-2011
Phosphorus
1480
mg/Kg -
dry
62.7
114
1
09/03/20 05:41
DADS
6010D
Aluminum
132000
mg/Kg -
dry
105
114
1
09/03/20 05:41
DADS
6010D
Arsenic
10.63
mg/Kg -
dry
5.45
11.4
1
09/03/20 05:41
DADS
6010D
Cadmium
<0.455
mg/Kg -
dry
0.455
2.27
1
09/03/20 05:41
DADS
6010D
Calcium
9553
mg/Kg -
dry
880
1140
1
09/03/20 05:41
DADS
6010D
Chromium
47.5
mg/Kg -
dry
5.36
5.68
1
09/03/20 05:41
DADS
6010D
Copper
186
mg/Kg -
dry
7.05
11.4
1
09/03/20 05:41
DADS
6010D
Iron
42700
mg/Kg -
dry
194
227
1
09/03/20 05:41
DADS
6010D
Lead
20.6
mg/Kg -
dry
4.09
6.82
1
09/03/20 05:41
DADS
6010D
Magnesium
1390
mg/Kg -
dry
58.6
114
1
09/03/20 05:41
DADS
6010D
Manganese
5980
mg/Kg -
dry
7.39
11.4
1
09/03/20 05:41
DADS
6010D
Mercury
0.1083
mg/Kg -
dry
0.0755
0.341
1
08/31/20 11:57
DDB
7471A
Molybdenum
<3.07
mg/Kg -
dry
3.07
5.68
1
09/03/20 05:41
DADS
6010D
Nickel
20.9
mg/Kg -
dry
2.73
5.68
1
09/03/20 05:41
DADS
6010D
Potassium
1350
mg/Kg -
dry
140
227
1
09/03/20 05:41
DADS
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
L
Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 8

•
Waypoint
27090 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL
www.waypointanalyiical.com
46245
EMA Resources Inc
Project
Reidsville,
NC
Mr. Brent Collins
Report Date : 09/08/2020
755 Yadkinville Road
Information :
Received : 08/25/2020
Mocksville , NC 27028
Danyale Love
Report Number : 20-238-0033
REPORT OFANALYSIS
Project Manager
Lab No : 87283
Matrix: Solids
Sample ID : Reidsville WTP
Sampled: 8/24/2020 8:45
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<7.27
mg/Kg - dry
7.27
11.4 1 09/03/20 05:41 3ADS 6010D
Sodium
4073
mg/Kg - dry
295
568 1 09/03/20 05:41 3ADS 6010D
Zinc
52.0 B
mg/Kg - dry
18.4
28.4 1 09/03/20 17:08 3TR 6010D
Sulfur
3230
mg/Kg - dry
118
227 1 09/03/20 05:41 3ADS 6010D
Sodium Absorption Ratio
0.413
Ratio
0.01
0.01 1 09/03/20 05:41 CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-238-0033
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#100
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ory Phillips Date & Time: 08/25/2020 09:41:08
Page 7 of 8

Client Name/Address
Client Project Manager/Contact
Billing Information
For laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinvilie Rd
Mocksville, NC 27028
Project Description
Project/Site Location (City/State)
RUSE! - Additional charges apply
Method of Shipment
Matrix Key
Special Detection Limit(sl
Z Fed Ex ❑Lips [3uSPs
WW -Wastewater GW - Groundwater
Date Results Needed
Courier ❑Client Drop Off
DW -Drinking Water S -Soil /Solid ❑ - Dil
4. 4$10-y{ C U-Tp
{f q L
1tieaUi•f A I � Cr �
Other
P - Product M - Misc
Project Number
Project Manager Phone 4
Project Manager Email
Purchase order Number
Site/Facility 10 4
336-399-3646
brent. collins@emaresources-cam
J2e;dsv;11c WTP
Gv
-❑
A Cool t 10C Na25203 (Micro only)
B Cool c= 6C
Waypoln}
c
C HZS0None
#r/iI ■ ■ r
ANALYTICAL
m
c
Y
M
E
p
0
E
❑
W
, I'
eq it
❑ None Required
a NaOH pH�10
2790 Whitten Road
Unless noted, all containers
V
°
w
m
(SS
Q
1
C J
W
U
F HNC13 pHf2
G HCLpH�2
Memphis, 1lY 38333
o�
o
Z
[phone]
per Table II of 40 CFR Part
a
E
x
a
T
Y
H
2
❑
rr ,,
H HVC14 pH<2
Cool <= GC NA25203
136.
3
�
Date
-rime
sample Identification
Required
Analysis / Preservative
Comments/Notes
WTP
C
v-
Meta Is:X,As, Ca, Cd,Cr,Cu,Fe, Pb
M n , Mg, Mo, H g . N i, 5e, N a, R 5, K, Zn
0
IN 1Bi111111II111111111111111111111111111I11NYI111111168� 3
EMA Re-.rrurces Inc 09 40:50
Reidsv+iie NC
For Laboratory Use Only
Sampled by (Name - Print)
rat �s
Client Remarks/Comments
Sludge Samples - Report Dry Weight
1Ce
Custody
Lab Comments
6/ N
'shed
ff 11 ,,
Relinq
by; (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
Elan CoolerTeemyp
Relinquished by: (SIGNATURE)
Date Time
Receiv by: IGNATURE)
Date Time
Relinquished hy: (SIGNATURE)
Date Time
Rec ved y: MATURE)
Da a Ti' e0S
1 ,
25 ze C)

aceAnalytical
National Center for Testing & Innovation
AW
ANALYTICAL REPORT
September 03, 2020
EMA Resources
Sample Delivery Group: L1254291
Samples Received: 08/25/2020
Project Number:
Description: Sludge
Site: REIDSVILLE WTP
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
JJwkC4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 1 of 21

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
REIDSVILLE WTP L1254291-01
5
Fn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
FC
Wet Chemistry by Method D93/1010A
10
F
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
[Al
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
RC
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
EMA Resources L1254291
09/03/2015:49 2 of 21

REIDSVILLE WTP L1254291-01 Waste
SAMPLE
SUMMARY
Collected by
Brent Collins
Collected date/time
08/24/2008:45
ONE LAB. NATIONWIDE.
Received date/time
08/25/2009:30
FP
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
F
Preparation by Method 1311
WG1533291
1 08/27/20 09:26
08/27/20 09:26
JGB
Mt. Juliet, TN
Preparation by Method 1311
WG1534773
1 08/29/2018:10
08/29/2018:10
JGB
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1533669
1 08/27/20 20:19
08/28/201105
JER
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1533680
1 08/28/20 00:00
08/28/20 00:00
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1535662
1 09/01/2014:00
09/01/2017:15
DRD
Mt. Juliet, TN
Fn
Wet Chemistry by Method D93/1010A
WG1532512
1 08/27/20 03:00
08/27/20 03:00
CAT
Mt. Juliet, TN
Mercury by Method 7470A
WG1535259
1 08/31/20 06:55
08/31/2012:37
ABL
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1535340
1 08/31/20 08:48
08/31/2010:46
CCE
Mt. Juliet, TN
Fr
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1534071
1 08/28/2013:46
08/28/2013:46
ACG
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1535717
1 09/02/20 07:05
09/02/2014:25
MT-1
Mt. Juliet, TN
FC
Pesticides (GC) by Method 8081B
WG1535604
1 09/01/201156
09/01/2019:50
MT-1
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1535602
1 09/01/20 06:59
09/01/2017:37
AO
Mt. Juliet, TN
GI
SAI
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1254291
09/03/20 15:49
3 of 21

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 4 of 21

REIDSVILLE WTP
Collected date/time: 08/24/20 08:45
Preparation by Method 1311
SAMPLE RESULTS - 01
L1254291
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
8/29/2020 6:10:10 PM
WG1534773
TCLP ZHE Extraction -
8/27/2020 9:26:19 AM
WG1533291
Fluid 1
8/29/2020 6:10:10 PM
WG1534773
Initial pH 6.58
8/29/2020 6:10:10 PM
WG1534773
Final pH 5.00
8/29/2020 6:10:10 PM
WG1534773
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
08/28/20201105 WG1533669
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 08/28/2020 00:00 WG1533680
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 6.74 T8 1 09/01/202017:15 WG1535662
Sample Narrative:
L1254291-01 WG1535662: 6.74 at 23.4C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7470A
Qualifier Dilution Analysis Batch
date / time
1 08/27/2020 03:00 WG1532512
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
0.174
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
EMA Resources
Dilution Analysis Batch
date / time
1 08/31/202012:37 WG1535259
Dilution Analysis
Batch
date / time
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 08/28/202013:46
WG1534071
1 08/28/202013:46
WG1534071
1 08/28/202013:46
WG1534071
1 08/28/202013:46
WG1534071
SDG:
DATE/TIME: PAGE:
L1254291
09/03/20 15:49 5 of 21

REIDSVILLE WTP SAMPLE RESULTS
Collected date/time: 08/24/20 08:45 L1254291
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
08/28/202013:46
WG1534071
1,1-Dichloroethene
ND
0.0500 0.70 1
08/28/202013:46
WG1534071
2-Butanone (MEK)
ND
J0 0.500 200 1
08/28/202013:46
WG1534071
Tetrachloroethene
ND
0.0500 0.70 1
08/28/202013:46
WG1534071
Trichloroethene
ND
0.0500 0.50 1
08/28/202013:46
WG1534071
Vinyl chloride
ND
0.0500 0.20 1
08/28/202013:46
WG1534071
(S) Toluene-dH
112
80.0-120
0812812020 13.46
WG1534071
(S) 4-Bromofluorobenzene
103
77.0-126
0812812020 13.46
WG1534071
(S) 1,2-Dichloroethane-d4
91.4
70.0-130
081281202013.46
WG1534071
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) Z4-Dichlorophenyl Acetic Acid 64.8
Pesticides (GC) by Method 8081B
Result
Analyte
mg/I
Chlordane
ND
Endrin
ND
Heptachlor
ND
Lindane
ND
Methoxychlor
ND
Toxaphene
ND
(S) Decochlorobiphenyl
87.0
(S) Tetrochloro-m-xylene
72.9
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 09/02/202014:25
WG1535717
0.00200
10
1 09/02/202014:25
WG1535717
14.0-158
091021202014.25
WG1535717
Qualifier RDL Limit Dilution Analysis Batch
mg/I mg/I date / time
0.00500
0.03 1
09/01/202019:50
WG1535604
0.00500
0.02 1
09/01/202019:50
WG1535604
0.00500
0.0080 1
09/01/202019:50
WG1535604
0.00500
0.40 1
09/01/202019:50
WG1535604
0.00500
10 1
09/01/202019:50
WG1535604
0.0100
0.50 1
09/01/202019:50
WG1535604
10.0-128
091011202019.50
WG1535604
10.0-127
091011202019.50
WG1535604
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-Fluorobiphenyl
(S) Z4, 6-Tribromophenol
(S) p-Terphenyl-d14
ACCOUNT:
EMA Resources
ONE LAB. NATIONWIDE. *
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
mg/I
date/time
ND
0.100
7.50
1 09/01/202017:37
WG1535602
ND
0.100
0.13
1 09/01/202017:37
WG1535602
ND
0.100
0.13
1 09/01/202017:37
WG1535602
ND
0.100
0.50
1 09/01/202017:37
WG1535602
ND
0.100
3
1 09/01/202017:37
WG1535602
ND
0.100
2
1 09/01/202017:37
WG1535602
ND
0.100
5
1 09/01/202017:37
WG1535602
ND
0.100
400
1 09/01/202017:37
WG1535602
ND
0.100
200
1 09/01/202017:37
WG1535602
ND
0.100
100
1 09/01/202017:37
WG1535602
ND
0.100
400
1 09/01/202017:37
WG1535602
ND
0.100
2
1 09/01/202017:37
WG1535602
32.2
10.0-120
091011202017.37
WG1535602
19.1
10.0-120
091011202017.37
WG1535602
52.5
10.0-127
091011202017.37
WG1535602
67.9
10.0-130
091011202017.37
WG1535602
67.0
10.0-155
091011202017.37
WG1535602
77.1
10.0-128
091011202017.37
WG1535602
PROJECT:
SDG:
DATE/TIME: PAGE:
L1254291
09/03/20 15:49 6 of 21
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc

WG1533669 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1254291-01
Method Blank (MB)
(MB) R3564830-1 03/23/201101
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1254422-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1254422-01 03/23/2011:03 • (DUP) R3564330-3 03/23/201109
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide ND ND 1 0.000 20
L1254422-09 Original Sample (OS) • Duplicate (DUP)
(OS) L1254422-09 03/23/2011:26 • (DUP) R3564330-8 03/23/201127
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3564830-2 08/28/201102
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.38 95.1
Rec. Limits LCS Qualifier
85.0-115
L1254422-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1254422-03 03/23/20 11:13 • (MS) R3564330-4 03/23/20 11:14 • (MSD) R3564330-5 03/23/20 1115
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.36 1.14 81.5 68.7 1 75.0-125 J6 17.1 20
L1254422-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1254422-07 03/23/20 11:19 • (MS) R3564330-6 03/23/20 11:20 • (MSD) R3564330-7 03/23/20 1122
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.28 1.20 77.0 72.2 1 75.0-125 J6 6.42 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 7 of 21

WG1533680
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3564662-1 03/23/20 0000
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Sulfide U 7.63 25.0
L1254266-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1254291-01
(OS) L1254266-02 03/23/20 00:00 • (DUP) R3564662-3 03/23/20 00:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Sulfide ND ND 1 0.000 20
L1254936-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1254936-02 03/23/20 00:00 • (DUP) R3564662-6 03/23/20 00:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3564662-2 08/28/20 00:00
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Sulfide 100 84.1 84.1
Rec. Limits LCS Qualifier
70.0-130
L1254934-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1254934-01 03/23/20 00:00 • (MS) R3564662-4 03/23/20 00:00 • (MSD) R3564662-5 03/23/20 00:00
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Sulfide 100 ND 86.9 88.0 86.9 88.0 1 70.0-130 1.33 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 3 of 21

WG1535662 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1254291-01
Laboratory Control Sample (LCS)
(LCS) R3566233-1 09/01/201715
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 10.0 100 99.0-101
Sample Narrative:
LCS:10.04 at 22.8C
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 9 of 21

WG1532512 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1254291-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
ONE LAB. NATIONWIDE. *
(LCS) R3564212-1 08/27/20 03:00 • (LCSD) R3564212-2 08/27/20 03:00
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg.F Deg.F Deg.F
Ignitability 126 131 125 104 98.9 95.6-104 4.70 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 10 of 21

WG1535259
Mercury by Method 7470A
Method Blank (MB)
(MB) R3565661-1 03/31/201233
MB Result MB Qualifier MB MDL
Analyte mg/I mg/I
Mercury U 0.00330
Laboratory Control Sample (LCS)
(LCS) R3565661-2 08/31/20 12:35
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Mercury 0.0300 0.0314 105
QUALITY CONTROL SUMMARY
L1254291-01
MB RDL
mg/I
0.0100
Rec. Limits LCS Qualifier
80.0-120
L1254291-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1254291-01 03/31/20 12:37 • (MS) R3565661-3 03/31/20 12:39 • (MSD) R3565661-4 03/31/20 12:41
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0293
0.0311 97.5 104 1 75.0-125 6.01 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 11 of 21

WG1535340
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1254291-01
(MB) R3565632-1 03/31/201030
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic 0.0581
J
0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS)
(LCS) R3565632-2 03/31/201033
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte mg/I
mg/I
Arsenic 10.0
9.72
97.2
80.0-120
Barium 10.0
9.91
99.1
80.0-120
Cadmium 10.0
9.71
97.1
80.0-120
Chromium 10.0
9.50
95.0
80.0-120
Lead 10.0
9.77
97.7
80.0-120
Selenium 10.0
10.1
101
80.0-120
Silver 2.00
1.88
93.9
80.0-120
LCS Qualifier
L1254947-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1254947-01 03/31/20 10:36 • (MS) R3565632-4 03/31/20 10:41 • (MSD) R3565632-5 03/31/20 10:43
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.89
9.91
98.9
99.1
1 75.0-125
Barium
10.0
ND
9.89
9.92
98.1
98.4
1 75.0-125
Cadmium
10.0
ND
9.72
9.77
97.2
97.7
1 75.0-125
Chromium
10.0
ND
9.49
9.62
94.2
95.5
1 75.0-125
Lead
10.0
0.325
10.1
10.1
97.9
97.9
1 75.0-125
Selenium
10.0
ND
10.2
10.2
102
101
1 75.0-125
Silver
2.00
ND
1.88
1.90
94.1
94.9
1 75.0-125
MS Qualifier MSD Qualifier RPD
0.159
0.308
0.541
1.33
0.0514
0.266
0.819
ONE LAB. NATIONWIDE. *
RPD Limits
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 12 of 21

WG1534071 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1254291-01
ONE LAB. NATIONWIDE. *
Method Blank (MB)
(MB) R3564853-3 03/23/201043
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0167
0.0500
Carbon tetrachloride
U
0.0167
0.0500
Chlorobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroethene
U
0.0167
0.0500
2-Butanone (MEK)
U
0.167
0.500
Tetrachloroethene
U
0.0167
0.0500
Trichloroethene
U
0.0167
0.0500
Vinyl chloride
U
0.0167
0.0500
(S) Toluene-dH
110
80.0-120
(S) 4-Bromofluorobenzene
102
77.0-126
(S) 1,2-Dichloroethane-d4
91.4
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3564853-1 08/28/20 08:05 • (LCSD) R3564853-2 08/28/20 09:38
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
0.219
0.230
87.6
92.0
70.0-123
Carbon tetrachloride
0.250
0.243
0.214
97.2
85.6
68.0-126
Chlorobenzene
0.250
0.248
0.255
99.2
102
80.0-121
Chloroform
0.250
0.217
0.227
86.8
90.8
73.0-120
1,2-Dichloroethane
0.250
0.220
0.222
88.0
88.8
70.0-128
1,1-Dichloroethene
0.250
0.237
0.222
94.8
88.8
71.0-124
2-Butanone (MEK)
1.25
1.02
0.999
81.6
79.9
44.0-160
Tetrachloroethene
0.250
0.250
0.240
100
96.0
72.0-132
Trichloroethene
0.250
0.237
0.247
94.8
98.8
78.0-124
Vinyl chloride
0.250
0.215
0.213
86.0
85.2
67.0-131
(S) Toluene-dH
108
109
80.0-120
(S) 4-Bromofluorobenzene
101
101
77.0-126
(S) 1,2-Dichloroethane-d4
96.9
95.6
70.0-130
LCS Qualifier
LCSD Qualifier RPD
4.90
12.7
2.78
4.50
0.905
6.54
2.08
4.08
4.13
0.935
RPD Limits
20
20
20
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 13 of 21

WG1534071 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1254291-01
L1254673-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1254673-01 08/28/20 14:06 • (MS) R3564853-4 03/23/20 1427
Spike Amount
Original Result
MS Result
MS Rec.
Dilution Rec. Limits MS Qualifier
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.186
74.4
1 17.0-158
Carbon tetrachloride
0.250
ND
0.185
74.0
1 23.0-159
Chlorobenzene
0.250
ND
0.217
86.8
1 33.0-152
Chloroform
0.250
ND
ND
77.2
1 29.0-154
1,2-Dichloroethane
0.250
ND
0.205
82.0
1 29.0-151
1,1-Dichloroethene
0.250
ND
0.173
69.2
1 11.0-160
2-Butanone (MEK)
1.25
ND
0.961
76.9
1 10.0-160
Tetrachloroethene
0.250
ND
0.197
78.8
1 10.0-160
Trichloroethene
0.250
ND
0.194
77.6
1 10.0-160
Vinyl chloride
0.250
ND
0.171
68.4
1 10.0-160
(S) Toluene-dH
106
80.0-120
(S) 4-Bromofluorobenzene
98.4
77.0-126
(S) 1,2-Dichloroethane-d4
92.2
70.0-130
L1254266-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1254266-04 03/23/20 13:05 • (MS) R3564353-6 03/23/20 14:43 • (MSD) R3564353-7 03/23/2015:07
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec. Dilution
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.187
0.194
74.8
77.6 1
Carbon tetrachloride
0.250
ND
0.180
0.194
72.0
77.6 1
Chlorobenzene
0.250
ND
0.229
0.238
91.6
95.2 1
Chloroform
0.250
ND
ND
ND
79.2
83.2 1
1,2-Dichloroethane
0.250
ND
0.218
0.221
87.2
88.4 1
1,1-Dichloroethene
0.250
ND
0.168
0.186
67.2
74.4 1
2-Butanone (MEK)
1.25
ND
1.15
1.11
92.0
88.8 1
Tetrachloroethene
0.250
ND
0.193
0.207
77.2
82.8 1
Trichloroethene
0.250
ND
0.189
0.203
75.6
81.2 1
Vinyl chloride
0.250
ND
0.155
0.182
62.0
72.8 1
(S) Toluene-dH
107
109
(S) 4-Bromofluorobenzene
97.6
101
(S) 1,2-Dichloroethane-d4
93.5
95.5
Rec. Limits
17.0-158
23.0-159
33.0-152
29.0-154
29.0-151
11.0-160
10.0-160
10.0-160
10.0-160
10.0-160
80.0-120
77.0-126
70.0-130
MS Qualifier MSD Qualifier RPD RPD Limits
3.67
27
7.49
28
3.85
27
4.93
28
1.37
27
10.2
29
3.54
32
7.00
27
7.14
25
16.0
27
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 14 of 21

WG1535717
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3566697-1 09/02/201311
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S) Z4-Dichlorophenyl Acetic 61.4
Acid
QUALITY CONTROL SUMMARY
L1254291-01
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
0.000667
0.00200
0.000667
0.00200
14.0-158
Laboratory Control Sample (LCS)
(LCS) R3566697-3 09/02/20 13:40
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
2,4-D 0.0500
2,4,5-TP (Silvex) 0.0500
(S) Z4-Dichlorophenyl Acetic
Acid
0.0309 61.8 50.0-120
0.0334 66.8 50.0-125
672 14.0-158
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 15 of 21

WG1535604
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1254291-01
(MB) R3566335-1 09/01/201746
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
89.7
10.0-128
(S) Tetrochloro-m-xylene
77.6
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3566335-2 09/01/20 1758
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00908
90.8
55.0-129
Endrin
0.0100
0.00913
91.3
57.0-134
Heptachlor
0.0100
0.00840
84.0
27.0-132
Methoxychlor
0.0100
0.00923
92.3
54.0-155
(S) Decachlorobiphenyl
91.1
10.0-128
(S) Tetrochloro-m-xylene
70.5
10.0-127
L1252949-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1252949-01 09/01/20 13:11 • (MS) R3566335-3 09/01/20 13:23 • (MSD) R3566335-4 09/01/20 13 35
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.00899
0.00885
89.9
88.5
1 14.0-141
Endrin
0.0100
ND
0.00915
0.00925
91.5
92.5
1 10.0-160
Heptachlor
0.0100
ND
0.00874
0.00875
87.4
87.5
1 16.0-136
Methoxychlor
0.0100
ND
0.00938
0.00970
93.8
97.0
1 10.0-160
(S) Decachlorobiphenyl
79.3
80.4
10.0-128
(S) Tetrochloro-m-xylene
76.3
74.2
10.0-127
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
1.57 40
1.09 39
0.114 40
3.35 34
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 16 of 21

WG1535602 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1254291-01
Method Blank (MB)
(MB) R3566149-2 09/01/201156
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
65.3
10.0-127
(S) 2-Fluorobiphenyl
84.4
10.0-130
(S) p-Terphenyl-d14
84.7
10.0-128
(S) Phenol-d5
22.9
10.0-120
(S) 2-Fluorophenol
39.7
10.0-120
(S) 2,4, 6-Tribromophenol
78.5
10. 0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3566149-1 09/01/20 1135
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.413
82.6
18.0-120
2,4-Dinitrotoluene 0.500
0.489
97.8
49.0-124
Hexachlorobenzene 0.500
0.435
87.0
44.0-120
Hexachloro-1,3-butadiene 0.500
0.353
70.6
19.0-120
Hexachloroethane 0.500
0.394
78.8
15.0-120
Nitrobenzene 0.500
0.366
73.2
27.0-120
Pyridine 0.500
0.0587
11.7
10.0-120
2-Methylphenol 0.500
0.334
66.8
28.0-120
3&4-Methyl Phenol 0.500
0.327
65.4
31.0-120
Pentachlorophenol 0.500
0.488
97.6
23.0-120
2,4,5-Trichlorophenol 0.500
0.486
97.2
44.0-120
2,4,6-Trichlorophenol 0.500
0.472
94.4
42.0-120
(S) Nitrobenzene-d5
60.4
10.0-127
(S) 2-Fluorobiphenyl
84.8
10.0-130
(S) p-Terphenyl-d14
86.2
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1254291 09/03/20 15:49 17 of 21

WG1535602 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1254291-01
Laboratory Control Sample (LCS)
(LCS) R3566149-1 09/01/20 1135
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 23.4 10.0-120
(S) 2-Fluorophenol 39.8 10.0-120
(S) 2,4, 6-Tribromophenol 83.5 10. 0-155
L1253440-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1253440-01 09/01/2013:42 • (MS) R3566149-3 09/01/2014:03 • (MSD) R3566149-4 09/01/2014:25
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.268
0.282
53.6
56.4
1 17.0-120
5.09
2,4-Dinitrotoluene
0.500
ND
0.382
0.386
76.4
77.2
1 39.0-125
1.04
Hexachlorobenzene
0.500
ND
0.342
0.346
68.4
69.2
1 35.0-122
1.16
Hexachloro-1,3-butadiene
0.500
ND
0.253
0.254
50.6
50.8
1 12.0-120
0.394
Hexachloroethane
0.500
ND
0.253
0.272
50.6
54.4
1 10.0-120
7.24
Nitrobenzene
0.500
ND
0.255
0.271
51.0
54.2
1 12.0-120
6.08
Pyridine
0.500
ND
ND
0.113
18.5
22.6
1 10.0-120
20.1
2-Methylphenol
0.500
ND
0.247
0.257
49.4
51.4
1 10.0-120
3.97
3&4-Methyl Phenol
0.500
ND
0.244
0.264
48.8
52.8
1 10.0-120
7.87
Pentachlorophenol
0.500
ND
0.442
0.427
88.4
85.4
1 10.0-128
3.45
2,4,5-Trichlorophenol
0.500
ND
0.414
0.414
82.8
82.8
1 33.0-120
0.000
2,4,6-Trichlorophenol
0.500
ND
0.394
0.391
78.8
78.2
1 26.0-120
0.764
(S) Nitrobenzene-d5
46.0
49.6
10.0-127
(S) 2-Fluorobiphenyl
66.5
66.1
10.0-130
(S) p-Terphenyl-d14
76.3
74.3
10.0-128
(S) Phenol-d5
18.2
19.0
10.0-120
(S) 2-Fluorophenol
27.8
28.4
10.0-120
(S)2,4,6-Tribromophenol
80.5
77.0
10.0-155
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
37
30
36
37
31
31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 13 of 21

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. *
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
Fp
Fc
FS
Fn
Fr
Fc
SAI
Rc
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J0
J0: The identification ofthe analyte is acceptable, but the reported concentration is an estimate. The calibration met
method criteria.
J6
The sample matrix interfered with the abilityto make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1254291 09/03/20 15:49 19 of 21

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7C71
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
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OR
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VWY
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CA co
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W o �AZ NM O�
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ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
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AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L12 542 91 09/03/2 0 15:49 20 of 21

EMA Resources
i755 Yadkinville Road
Mocksville, NC 27028
Billing Information: l
Mr. Brent Collins Pres
755 Yadkinville Road Chk
Mocksville, NC 27028
An
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Container
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12065 Lebanon Rd 0!v
Mount Juliet, TN 37122 `
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Mr. Brent Collins
Email To: [e-mail]
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Phone [phone]
Fax: [phone]
Client Project a
Lab Project #
Collected by (print):
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Site/Facility ID a
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Packed on Ice IN Y
Rush? (Lab MUST Be Notified) Quote a
—Same Day Five Day
_ Next Day _ 5 Day (Rod Only) Date Results Needed
_ Two Day —10 Day (Rad Only) No.
—Three Day of
Sample ID
Comp/Grab
Matrix •
Depth
Date
Time
ntr5
Remarks Sample p[[ab onlYl
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55 Soil AIR - Air F- Filter
SS - -Groundwater B - FilterBioassayCOC
WW - Wastewater
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pH Temp
Flow Other
Sample t' i
CCC Seal Present/Intact: _NP r N
signed/Accuratm : � _N
Bottles arrive intact: _A _N
Correct bottles used: y,A _N
Sufficient volume sent: �l mmN
If Aanlicadle
von zero Headspace: y N
Preservation Correct/Checked: �Y N
RAD Screen <0.5 1nR/hr: XHCL�*
Samples returned via:
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Relinquished by: (Signature)
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Trip Blank Received: Yes /
TOR MeoH
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Relinquished by : (Signature)
Date:
Time
Received by: (Signature)]
c Bottles Received:
If preservation required by Login: Date/Time
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4b) Residuals Information Sheet

Residuals Information Sheet
Generator: City of Reidsville WTP
Facility:
Reidsville WTP
Address:
278 Reid Lake Rd
Reidsville, NC 27320
Phone:
336-342-4002
Contact:
Scott Jewell
Land Application Contractor: EMA Resources Inc.
755 Yadkinville Rd
Mocksville, NC 27028
Phone: [phone]
Contact: Brent Collins
Please Note: The application of these residuals is only allowed in accordance with subject permit.
(WQ0002376)
All applicable setbacks in accordance with 15A NCAC 02T .1108(b) will be adhered and is the
responsibility of the land application contractor.
Application rates shall be applied at agronomic rates for intended uses.
No residuals shall be applied to any site that is flooded, frozen, or snow covered.
Adequate procedures will be implemented to prevent surface runoff of residuals in any surface waters.
The attached residuals analysis report is a summary of major and micro -nutrients available in the
residuals.
If you have any questions concerning this information, you may contact EMA Resources Inc, at the
number listed above.

5) Operation & Maintenance Plan

Standard Operating Procedure and Operation
and Maintenance Plan for the Reidsville WTP
Land Application Program
1. Purpose
a. Ensure the requirements of the Reidsville WTP Distribution of Class A
Residuals Permit# WQ0032723 are met.
2. Personnel
a. The following is a list of personnel in order they are to be contacted when
information needs to be shared.
i. EMA Resources Inc.
1. Brandon Shaffer — Project Manager — [phone]
2. Mike Collins — Director of Operations — [phone]
3. Brent Collins — Director of Technical Services — [phone]
ii. Reidsville WTP
1. Scott Jewell — Plant Superintendent — [phone]
3. Operational Functions
a. The operational function of this project it going to involve mixing the lagoon
with a tractor powered Houle pump to achieve a well -mixed and consistent
material that is suitable for land application. It is going to be spread at
agronomic rates that are determined using the Realistic Yield Expectations
(RYE) as outlined in the permit, the amount of other nutrient sources the
landowner and operator has applied, and the residuals nutrient and metal
sample that is current for that monitoring period. It is going to be spread
with a liquid applicator that will use pressure to spread the material in such
a way as to achieve a consistent spread pattern. The material is going to be
land applied on fields that have a crop growing on them that are going to
either be grazed or cut for animal feed. Application rates will be reduced
by 25% on fields that are primarily used for grazing in accordance with

USDA-NRCS 590. Grazed fields will be determined by the farmers and EMA
project managers.
4. Maintenance Schedule
a. EMA Resources Inc. will follow the maintenance schedule as recommended
by the EMA Resources Operations Manager (Mike Collins) for the
equipment necessary to complete the job.
S. Safety Measures
a. Reidsville Water and EMA Resources Inc. believe in operating in a safety
conscious manner and all employees participate in safety training that is
designed to help employees recognize safety issues and take steps to
prevent accidents from occurring. In addition, EMA Resources employees
have the authority to stop operations if they think any aspect of the
operation is going to cause environmental or personal harm.
6. Spill Response Plan
a. In the unlikely event of a spill, the following action shall be taken
immediately.
i. Management of Spill Clean-up Activities: The EMA Resources
Project Manager shall take immediate charge and initiate clean-up
activities. EMA Resources labor and equipment is to be utilized. In
the event additional labor and equipment is required, assistance may
be requested from Reidsville Water, The NC Department of
Transportation, and other private contractors as necessary.
ii. Halt the Source of the Spill: Such as a ruptured container or
damaged transport unit.
iii. Contain the Spill: Form a barrier. Sufficient quantities of straw shall
be used for such purposes. Earthen barriers may be constructed to
augment the straw bale containment area of the spill. The
Operations Manager or the person in charge on the spill site will be

advise the clean-up personnel where to get the straw, lime, and other
items necessary to complete the clean-up operation. le. local farmers,
farm supply centers, nurseries.
iv. Initial Clean -Up: Employ front-end loaders, vacuum equipment,
sludge application vehicles, and/or local septic tank service to
remove as much of the spilled material as possible. Straw and/or
sand should be scattered in the spill area to soak up the remaining
material. The straw and sand soaked material will be collected and
removed to a disposal area approved by representatives of the state
regulatory agency.
v. Final Clean-up: Employ rotary brush sweeper if needed and apply
lime to the spill area upon the approval of the clean-up efforts by the
state regulatory representative. If the event occurs on private
property, the clean-up will be completed to the satisfactory of the
property owner and state regulatory representatives. The ultimate
goal will be restore the spill area to its original condition if possible.
vi. Notification: As soon as possible after the spill occurs, the EMA
Resources Project Manager or designee will notify the Reidsville
Water and EMA Resources main offices. EMA Resources office staff
are then responsible for notifying other key EMA Resources
personnel.
vii. Reporting_ EMA Resources staff will notify the Winston Salem
regional office of the NCDENR by telephone [phone] as soon
as possible, but not more than 24 hours after, or on the next working
day following the occurrence. The EMA Project Manager shall
provide a written report with 48 hours of the spill to the EMA
Resources Director of Technical Services and Reidsville Water staff.
The report shall list all relative information and actions taken. With
the assistance of EMA Resources personnel, and Reidsville Water
personnel, a written report will be filed with the Winston Salem
regional office within 5 days of the occurrence. For after hours
reporting, the Division's emergency number shall be called to report
all incidences [phone].

7. Inspection Plan
a. Inspection for the land application of residuals will conducted on a
minimum of a weekly basis at the land application site during land
application activities. The inspection frequency is based on the time frame
that it is going to take to complete the project and the amount of dry tons
to be land applied from this facility. The inspections will consist of
inspecting a current field that is being applied as well as inspecting random
fields that have been completed. Inspections will be conducted by Brandon
Shaffer — Project Manager. These inspections will consist of the following:
i. Verifying the application rates for each field that plan on receiving
material.
ii. Checking the calculated loads to ensure the correct amount of
residuals are being land applied.
iii. Ensure that all manned equipment has a copy of the permit and the
operation and maintenance plan.
iv. Ensure that the field has been flagged properly and that all buffers
are being adhered to.
v. Ensure proper signage has been posted
vi. Verify that the proper number of samples of the residuals have been
taken and that it meets the criteria for land application.
vii. The records will be kept in the EMA Resources project files in the
main office. Copies of all analyses and records will be forwarded to
Reidsville Water and kept on file.
viii. EMA Resources and Reidsville Water staff will immediately inform the
other part if any of the following conditions are noted.
1. Any occurrence with the distribution program resulting in the
land application of significant amounts of material that is
abnormal in quantity or characteristics.
2. Any failure of the distribution system that results in the release
to surface waters.
3. Any time that self -monitoring indicates that the facility has
gone out of compliance with the permit.
4. Any process failure that results in the system not adequately
treating the residuals.

5. Any spill or discharge from a vehicle or piping system during
residuals transportation.
6. Any release that requires immediate reporting outside normal
business hours shall be called in by EMA Resources staff to
DENR at [phone]. This number is to be called in the
event of a release to surface waters or imminent failure of a
storage system when the event occurs outside of normal
business hours.
8. Sampling and Monitoring Plan
a. Sampling for this project consists of sampling the residuals prior to land
application occurring in order to ensure that the residuals are suitable for
land application.
b. The samples will be collected from the storage lagoon that holds the
residuals
c. Brandon Shaffer, Brent Collins, or other designee will be responsible for
sample collection for nutrient and metal, and TCLP.
d. Nutrient, metal and TCLP sample aliquots will be collected randomly and
consist of at least 7 individual aliquots mixed together in order to get the
composite sample for these parameters.
e. The residuals will be sampled once per permit cycle for TCLP including the
RClls.
f. Metal and nutrient parameters will be collected and analyzed based on the
requested dry ton numbers in the permit application.
9. Environmental Impacts
a. The environmental impacts for residuals may be affected by this procedure.
b. This procedure helps assure that land application is conducted in a safe and
efficient manner while ensuring compliance with the laws and regulations
and to minimize exposure, negative environmental impacts and public
relation concerns.

City of Reidsville WTP Permit Renewal -
WQ0032723
Final Audit Report 2021-05-28
Created:
2021-05-27
By:
Brent Collins ([e-mail])
Status:
Signed
Transaction ID:
CBJCHBCAABAAOyyybtclVowO46H3205cdMNlg2laPtFR
"City of Reidsville WTP Permit Renewal - WQ0032723" History
Document created by Brent Collins ([e-mail])
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Agreement completed.
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