NCG030325_MRO Copy MONITORING REPORT_20210324

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR'Regional Office.
Certificate of Coverage No. N
Person Collecting Samples: Chris Wolf
Facility Name: Division 5, LLC (DBA Hickory Steel) Laboratory Name: Con -Test
Facility County: Catawba Laboratory Cert. No.: 652
Discharge during this period: ❑■ Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes ❑■ No
If so, which Tier (1, 11, or III)?
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Code
Parameter
Outfall 1
Outfall 2
Outfall
Outfall
Outfall
N/A
Receiving Stream Class
C
c
N/A
Date Sample Collected MM/DD/YYYY
02/11/2021
02/11/2021
46529
24-Hour Rainfall in inches
1
1
00552
Non -Polar Oil & Grease in mg/L (15)
<0.33
<.33
C0530
TSS in mg/L (100 or 50*)
2.4
9.0
00400
pH in standard units (6.0 — 9.0)
6.1
6.7
NCOIL
New Motor/Hydraulic Oil Usage in
N/A
N/A
gal/month
01119
Copper, total recoverable in mg/L
<0.0022
0.0015
(0.010 FW, 0.005 SW)
01051
Lead, total recoverable in mg/ L
0.00068
0.0013
(0.075 FW, 0.220 SW)
01094
Zinc, total recoverable in mg/ L (0.126
0.085
0.057
FW, 0.095 SW)
78141
Total Toxic Organics (TTO) in mg/L(1)
N/A
N/A
* Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L.
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Signature of Permittee or Delegated AuWrized Individual
3 /
Date

con -test"
A Pace AnaocalO Laboratory
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 1, 2021
Paul Spangenberg
Mid -Atlantic Associates, Inc. - Raleigh, NC
409 Rogers View Court
Raleigh, NC 27610
Project Location: Hickory, NC
Client Job Number:
Project Number: R2951.10
Laboratory Work Order Number: 21 B0641
Enclosed are results of analyses for samples received by the laboratory on February 15, 2021. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 16

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
21BO641-01
21BO641-02
Sample Preparation Inforination
QC Data
Metals Analyses (Total)
B276907
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
B276656
B276703
B276723
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
7
9
10
10
10
11
11
11
11
12
13
14
Page 2 of 16

Table of Contents
�I con -test®
I I A Pace Analyticels Laboratory
39 Spruce Street' East Longmeadow, MA 01028' FAX [phone] * TEL. [phone]
Mid -Atlantic Associates, Inc. - Raleigh, NC
409 Rogers View Court REPORT DATE: 3/1/2021
Raleigh, NC 27610 PURCHASE ORDER NUMBER:
ATTN: Paul Spangenberg
PROJECT NUMBER: R2951.10
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 21B0641
The results of analyses performed on the following samples submitted to CON -TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION: Hickory, NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
1 21B0641-01 Storm Watcr EPA 1664B
SM21-22 2540D
SM21-22 4500 H B
SW-846 6020B
2 21B0641-02 Storm Water EPA 1664B
SM21-22 2540D
SM21-22 4500 H B
SW-846 6020B
Page 3 of 16

con -test°
A Pace Anatyticat' Laboratory
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 " FAX [phone] ` TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
Qualifications:
H-09
SM21-22 2540D
Sample received by laboratory with insufficient time remaining to perform analysis within the recommended holding time.
Analyte & Samples(s) Qualified:
Total Suspended Solids
21B0641-01[l], 21B0641-02[2]
SM21-22 4500 H B
Qualifications:
H-05
Holding time was exceeded. pH analysis should be performed immediately at time of sampling. Nominal 15 minute holding time was
exceeded.
Analyte & Samples(s) Qualified:
pH
-IB0641-01[l],21B0641-02[2]
The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
W
vww"4�
Lisa A. Worthington
Technical Representative
Page 4 of 16

Table of Contents
con -test°
A Pace AnalytkaPe Laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
reject Location: Hickory, NC Sample Description: Work Ordcr. 21 B0641
Date Received: 2/15/2021
Field Sample #: 1 Sampled: 2/11/2021 11:30
Sample ID: 21B0641-01
Samole Matrix: Storm Water
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Copper
0.0022
0.0010
0.00087
mg/L I
SW-846 6020B
2/23/21
2/25/21 13:22
TBC
Lead
0.00068
0.00050
0.000085
mg/L 1
SW-846 6020B
2/23/21
2/25/21 13:22
TBC
Zinc
0.085
0.010
0.0023
mg/L I
SW-846 6020B
2/23/21
2/25/21 13:22
TBC
Page 5 of 16

40 con -test"
A Pace Analy6calO Laboratory
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 ' FAX [phone] ` TEL. [phone]
'roject Location: Hickory, NC Sample Description: Work Order: 21 B0641
Date Received: 2/15/2021
Field Sample #: 1 Sampled: 2/11/2021 11:30
Sample ID: 21B0641-01
Sample Matrix: Storm Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date
Date/Time
Analyte
Results RL DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
pH @20.7°C
6.1
pH Units 1 H-05
SM21-22 4500 H B
2/18/21
2/18/21 16:10
RAV
Total Suspended Solids
2.4 1.0 0.32
mg/L 1 H-09
SM21-22 2540D
2/18/21
2/18/21 12:00
LL
Oil & Grease (HEM)
ND 1.4 0.33
mg/L 1
EPA 1664B
2/19/21
2/19/21 13:00
LL
Page 6 of 16

Table of Contents
con -test°
A Pace AnalyticalO Laboratory
39 Spruce Street " East Longmeadow, MA 01028 ' FAX [phone] ` TEL. [phone]
reject Location: Hickory, NC
Sample Description:
Work Order:
21 B0641
Date Received: 2/15/2021
Field Sample #: 2
Sampled: 2/11/2021 11:30
Sample ID: 21B0641-02
Sample Matrix: Storm Water
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
Copper
0.0015
0.0010 0.00087 mg/L I
SW-846 6020B
2/23/21
2/25/21 13:31
TBC
Lead
0.0013
0.00050 0.000085 mg/L 1
SW-846 6020B
2/23/21
2/25/21 13:31
TBC
Zinc
0.057
0.010 0.0023 mg/L I
SW-846 6020B
2/23/21
2/25/21 13:31
TBC
Page 7 of 16

con-kst°
A Pace Analytical" Laboratory
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
roject Location: Hickory, NC Sample Description: Work Order: 21B0641
Date Received: 2/15/2021
Field Sample #: 2 Sampled: 2/11/2021 11:30
Sample ID: 21B0641-02
Sample Matrix: Storm Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date
Date/Time
Analyse
Results RL DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
pH @20.1*C
6.7
pH Units I H-05
SM21-22 450011 B
2118/21
2/I8/21 16:10
RAV
Total Suspended Solids
9.0 1.0 0.32
mg/L I H-09
SM21-22 2540D
2/18/21
2/18/21 12:00
LL
Oil & Grease (HEM)
ND 1.4 0.33
mg/L I
EPA 1664B
2/19/21
2/19/21 13:00
LL
Page 8 of 16

0 eon -tat°
A Pace AnalyficaP Laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
EPA 1664B
Lab Number [Field ID] Batch Initial [mLJ Date
21BO641-01[1] B276723 1000 02/19/21
21BO641-02[2] B276723 1000 02/19/21
Table of Contents
SM21-22 2540D
Lab Number [Field ID]
Batch
Initial [mLJ
Date
21BO641-01[1]
B276656
500
02/18/21
21BO641-02[2]
B276656
500
02/18/21
SM21-22 4500 H B
Lab Number [Field ID]
Batch
Initial [mLJ
Date
21BO641-01 [1]
B276703
50.0
02/18/21
21BO641-02 [2]
B276703
50.0
02/18/21
Prep Method: SW-846 3005A
Analytical Method: SW-846 6020B
Lab Number [Field ID]
Batch
Initial [mLJ Final [mLJ
Date
10641-01 [1] B276907 50.0 50.0 02/23/21
: t]30641-02 [2] B276907 50.0 50.0 02/23/21
Page 9 of 16

Table of Contents
con-tEst"
A Pace Ana/yUci;P laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B276907 - SNV-846 3005A
Blank (B276907-BLKI)
Prepared: 02/23/21 Analyzed: 02/26/21
Copper
ND
0.0010
mg/L
Lead
ND
0.00050
mg/L
Zinc
ND
0.010
mg/L
LCS (B276907-BS1)
Prepared: 02/23/21 Analyzed: 02/25/21
Copper
0.925
0.010
mg/L
1.00 92.5
80-120
Lead
0.475
0.0050
mg/L
0.500 95.0
80-120
Zinc
0.940
0.10
mg/L
1.00 94.0
80-120
LCS Dup (B276907-BSDI)
Prepared: 02/23/21 Analyzed: 02/25/21
Copper
0.890
0.010
mg/L
1.00 89.0
80-120 3.84 20
Lead
0.465
0.0050
mg/L
0.500 93.0
80-120 2.14 20
Zinc
0.906
0.10
mg/L
1.00 90.6
80-120 3.69 20
Page 10 of 16

con -test®
A Pace AnalyticW Laboratory
39 Spruce Street ' East Longmeadow, MA 01028 " FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Com,entional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
Table of Contents
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B276656 - SM21-22 2540D
Blank (B276656-BLKI)
Prepared & Analyzed: 02/18/21
Total Suspended Solids
LCS (B276656-BSI)
ND
2.5 mg/L
Prepared & Analyzed: 02/18/21
Total Suspended Solids
Batch B276703 - SM21-22 4500 H B
120
10 mg/L
200 60.0 57.4.123
LCS (B276703-BS1)
Prepared & Analyzed: 02/18/21
pH
Batch B276723 - EPA 1664B
6.00
pH Units
6.00 100 90-110
Blank (B276723-BLKI)
Prepared & Analyzed: 02/19/21
Oil & Grease (HEM)
LCS (B276723-BS1)
ND
1.4 mg/L
Prepared & Analyzed: 02/19/21
Oil & Grease (HEM)
Matrix Spike (B276723-MS1)
20
Source:
mg/L
21BO641-02
20.0 101 78-114
Prepared & Analyzed: 02/19/21
Oil & Grease (HEM)
170
14 mg/L
200 ND 86.5 78-114
Page 11 of 16

Table of Contents
con -test®
A Pace Ana/yticalO Laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
t
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
ND
Not Detected
RL
Reporting Limit is at the level of quantitation (LOQ)
DL
Detection Limit is the lower limit of detection determined by the MDL study
MCL
Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
H-05 Holding time was exceeded, pH analysis should be performed immediately at time of sampling. Nominal 15
minute holding time was exceeded.
H-09 Sample received by laboratory with insufficient time remaining to perform analysis within the recommended
holding time.
Page 12 of 16

Table of Contents
con -test"
A Pace Analytical® Laboratory
39 Spruce Street' East Longmeadow, MA 01028' FAX [phone]' TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
EPA 1664B in Water
Oil & Grease (HEM)
CT,MA,NH,NYRI,NC,ME,VA
SM21-22 2540D in Water
Total Suspended Solids
CT,MA,NH,NY,RI,NC,ME,VA
SM21-22 4500 HB in Water
pH
CT,MA,RI
SW-846 6020B in Water
Copper
CT,NH,NY,ME,VA,NC
Lead
CT,NH,NY,ME,VA,NC
Zinc
CT,NH,NY,ME,VA,NC
Con -Test, a Pace Environmental Laboratory,
operates under the following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2017
100033
03/l/2022
MA
Massachusetts DEP
M-MA100
06/30/2021
CT
Connecticut Department of Publilc Health
PH-0165
12/31/2022
NY
New York State Department of Health
10899 NELAP
04/1/2021
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2022
RI
Rhode Island Department of Health
LA000112
12/30/2021
NC
North Carolina Div. of Water Quality
652
12/31/2021
NJ
New Jersey DEP
MA007 NELAP
06/30/2021
FL
Florida Department of Health
E871027 NELAP
06/30/2021
VT
Vermont Department of Health Lead Laboratory
LL720741
07/30/2021
ME
State of Maine
MA00100
06/9/2021
VA
Commonwealth of Virginia
460217
12/14/2021
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2021
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2021
NC-DW
North Carolina Department of Health
25703
07/31/2021
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2021
MI
Dept. of Env, Great Lakes, and Energy
9100
09/6/2021
Page 13 of 16

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Table of Contents
TRACK ANOTHER SHIPMENT
921888001943
ADD NICKNAME
Delivered
Thursday, February 18, 2021 at 10:54 am
FROM
Salem Steel
Chris Wolf
1720 Vargrave St.
WINSTON SALEM, NC US 27107
828-455-1520
Shipment Facts
TRACKING NUMBER
921838001943
DIMENSIONS
25x16x16 in.
TOTAL PIECES
1
PACKAGING
Your Packaging
STANDARD TRANSIT
2/16/21 by 10:30 am 0
Travel History
DELIVERED
Signed for by: R.PIETRAS
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
SERVICE
FedEx Priority Overnight
DELIVERY ATTEMPTS
1
TO
Con -Test Analytical Laboratory
Login - Sample Receiving
39 Spruce St.
Building 1
East Longmeadow, MA US 01028
413-525-2332
TOTAL SHIPMENT WEIGHT
71.1 Ibs / 32.25 kgs
SPECIAL HANDLING SECTION
Deliver Weekday, Non Standard Packaging
ACTUAL DELIVERY
2/18/21 at 10:54 am
WEIGHT
71.1 Ibs / 32,25 kgs
DELIVERED TO
Shipping/Receiving
TERMS
Third Party
SHIP DATE
2/15/21 0
A
Page 15 of 16

Table of Contents
I Have Not Confirmed Sample Container
Numbers With Lab Staff Before Relinquishing
Over Samples
AN^L.V"0A1-. LAE3C)"A'Tt7F1Y
.. 1:::' ::: . ... 27T Rie . $ 2QtT
Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client (-A (-'\ A
Received By DateTime
How were the samples In Cooler 1 No Cooler On Ice 1 No Ice
received? Direct from Sampling
Ambient
Melted Ice
Were samples within
By Gun #
_ Actual Temp - � j
Temperature? 2-6°C T
By Blank #
Actual Temp
Was Custody Seal Intact?
;i Va _ _
Were Samples Tampered with?
�)
Was COC Relinquished ?
Does Chain Agree With Samples?_
Are there broken/leaking/loose caps on any samples? r✓
Is COG in ink/ Legible? 1
Were samples received within holding time?
f
Did COC include all Client
i
Analysis ; Sampler Name
i'
pertinent Information? Project
;
ID's T Collection Dates/Times
-;
Are Sample labels filled out and legible?
i
Are there Lab to Filters?
Who was notified?
Are there Rushes?
Who was notified?
Are there Short Holds?
;
Who was notified? t_,,
Is there enough Volume?
i
Is there Headspace where applicable?
ty /A
MS/MSD?E�
roper Media/Containers Used?
Is splitting samples required?
+�
JVere trip blanks received?
On COC? i<
Do all samples have the proper pH?
Acid -i Base
Un -
1 Liter Amb.
1 Liter Plastic
:2. 16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz Amb/Clear
Meoh-
250 mL Amb.
250 mL Plastic
4oz Amb/Clear
Bisulfate-
Flashpoint
Col./Bacteria
2oz Amb/Clear
DI-
Other Glass
Other Plastic
Encore
Thiosulfate-
SOC Kit
Plastic Ba2
Frozen:
Sulfuric-
Perchlorate
Ziplock
s x,>�r
h Y
,e,
0,;>
�-
Un -
1 Liter Amb.
1 Liter Plastic
16 oz Amb.
HCL-
600 mL Amb.
500 mL Plastic
8oz Amb/Clear
Meoh-
250 mL Amb.
250 mL Plastic
4oz Amb/Clear
Bisulfate-
Col./Bacteria
Flashpoint
2oz Amb/Clear
DI-
Other Plastic
Other Glass
Encore
Thiosulfate-
SOC Kit
Plastic Bag
Frozen:
Sulfuric-
Perchlorate
Zi lock
comments:
QN VeC)f-'A �('-\h�, C"Vw3
T5S to b� :eLe•v0\ t"Ae t b�
t,)n „d,k-v,,'.\ Wx-,