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HomeMy WebLinkAboutNCG080991_MRO Copy MONITORING REPORT_20201230A;S11,SEFA December 22, 2020 Certified Letter DEQ Mooresville Regional Office Attn: DEMLR Stormwater Program 610 East Center Avenue Suite 301 Mooresville, NC 28115 Subject: SEFA Transportation DMR Form NCG080991 To Whom it may concern: Enclosed is the the hard copy of the DMR and supporting analytical for the SEFA Transporatation facility, COC NCG080991, located in Lincoln county. If there are any questions concerning the report, please contact me at (803) 520-9016. Sincerely, Todd Wilson Director of Environmental Services cc: Jake Stetler, SEFA Transportation Facility Manager �. (803) 520-9000 ® www.sefogroup.com Q 217 Cedar Road I Lexington, SC 29073 NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG080000 Transit and Transportation Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. N0008E Facility Name: SEFA Transportation Inc. Person Collecting Samples: Todd Wilson Laboratory Name: Pace Analytical Facility County: Lincoln I Laboratory Cert. No.: 40/12 Discharge during this period: ❑■ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes ■❑ No If so, which Tier (I, II, or III)? Part A: Vehicle & Equipment Maintenance Areas — Benchmarks in (Red) Parameter Code Parameter Outfall 1 Outfall 2 Outfall Outfall Outfall N/A Receiving Stream Class C C N/A Date Sample Collected MM/DD/YYYY 11/11/2020 11/11/2020 46529 24-Hour Rainfall in inches 1.45 1.45 00552 Non -Polar Oil & Grease in mg/L (15) < 5.0 < 5.0 C0530 TSS in mg/L (100 or 50*) 17.2 4.5 00400 pH in standard units (6.0-9.0) 7.0 6.9 NCOIL New Motor/Hydraulic Oil Usage in gal/month 215 215 Part B: Oil/Water Separators & Secondary Containment Areas at Bulk Stations & Terminals — Benchmarks in (Red) Parameter Code Parameter Outfall Outfall Outfall Outfall Outfall N/A Receiving Stream Class N/A Date Sample Collected MM/DD/YYYY 46529 24-Hour Rainfall in inches 00552 Non -Polar Oil & Grease in mg/L (15) C0530 TSS in mg/L (100 or 50*) 00400 pH in standard units (6.0-9.0) * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/l.. All other water classifications have a benchmark of 1.00 mg/l_ Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing v�iofations._" re of Permittee or Delegated Authorized Individual 12/03/2020 Date 12/22/2020 Submission Completed Stormwater NPDES Permit Data Monitoring Report NORTH CAROLINA (DMR) Upload Snvlronmenfot Quoltfy Permit and Facility Information: Please enter the permit number and other details for this upload. ..................................................................................................................................................................................... IMPORTANT. Until the eDMR system is implemented for DEMLR Stormwater Program permits, an original signed hardcopy of the DMR MUST be mailed to the address in your permit, in addition to this electronic upload. Fields marked with a red asterisk* are required. Permit Number* Enter COC or Individual Permit Number NCG080991 Must begin with NCS or NCG Facility Name: * SEFA Transportation Inc. County: * Lincoln After uploading here, the original signed hardcopy must be mailed to: DEQ Mooresville Regional Office Attn: DEMLR Stormwater Program 610 East Center Avenue Suite 301 Mooresville, NC 28115 Further contact details at https:Hdeq.nc.gov/contact/regional-offices/mooresville Monitoring Period Information: .............................................................................................................................................................................................................................................................................................................. Monitoring Period What is the YEAR of the sample date(s)? Year:* 2020 Multiple DMRs from sampling periods within the same year can be uploaded together, but please upload different years with a new submittal form. https://edocs.deq.nc.gov/Forms/Form/Submit 1/2 12/22/2020 Submission Completed DMR Upload* Click the upload button or drag and drop files here to attach document. SEFA Transportation DMR NCG080991®201203.... 877.99KB Only PDFs are accepted. Comments: * By checking the box and signing box below, I certify that: o I have given true, accurate, and complete information on this form; o I agree that submission of this Data Monitoring Report (DMR) upload form is a "transaction" subject to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act'); o I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act'); o I understand that an electronic signature on this upload form has the same legal effect and can be enforced in the same way as a written signature; AND • I intend to electronically sign and submit this DMR upload form. Full Name:* Todd Wilson Name of person submitting this form Email Address:* twilson@sefagroup.com Phone Number:* 8035209000 Signature: Date: * 12/22/2020 https://edocs.deq.nc.gov/Forms/Form/Submit 2/2 IeAnalyticalo www.pecolobs.com November 19, 2020 Todd Wilson Sefa Group 855 Dukeville Rd. Salisbury, NC 28146 RE: Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 Dear Todd Wilson: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 11, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, A �h --- D Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Jason Steele, Sefa Group REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 aceAnalytical www.pecolobs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 aceAnalytical www,pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 Lab ID Sample ID Matrix Date Collected Date Received 92505313001 92505313002 D-SW-1 D-SW-2 Water Water 11/11/20 08:42 11/11/20 08:52 11/11/20 12:29 11/11/20 12:29 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 aceAnalytical www,pamlabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Storm Water SEFA Denver, NC 92505313 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92505313001 D-SWA EPA 1664E HH 1 PASI-C SM 2540D-2011 RED 1 PASI-A EPA9040C SMK 1 PASI-A 92605313002 D-SW-2 EPA 1664B HH 1 PASI-C SM 2540D-2011 RED 1 PASI-A EPA 9040C SMK 1 PASI-A PASI-A= Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 14 (�Ia'ceAnalyticalv www.pacelobs.com ANALYTICAL RESULTS Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: D-SW-1 Parameters Lab ID: 92505313001 Collected: Report Results Units Limit 11/11/20 08:42 MDL DF Received: 11/11/20 12:29 Matrix: Water Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 5.0 1 11/19/20 09:45 2640D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services -Asheville Total Suspended Solids 17.2 mg/L 4.2 4.2 1 11/13/20 18:26 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 7.0 Std. Units 0.10 0.10 1 11/15/20 19:57 D6,H3 Date: 11/19/2020 04:39 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 14 ,�aceAnalytical" www.paceiobs.com ANALYTICAL RESULTS Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: D-SW-2 Parameters Lab ID: 92605313002 Collected: Report Results Units Limit 11/11/20 08:52 MDL DF Received: 11/11/20 12:29 Matrix: Water Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 5.0 1 11/19/20 09:46 2640D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services -Asheville Total Suspended Solids 4.5 mg/L 2.8 2.8 1 11/13/20 18:27 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 6.9 Std. Units 0.10 0.10 1 11/15/20 20:08 H3 Date: 11/19/2020 04:39 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 14 �-aoeAnalyfical www.pacelobs.com QUALITY CONTROL DATA Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 QC Batch: 581465 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92505313001, 92505313002 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 3075444 Matrix: Water Associated Lab Samples: 92505313001, 92505313002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 5.0 11/19/20 09:39 LABORATORY CONTROL SAMPLE: 3075445 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 18.5 92 64-132 MATRIX SPIKE SAMPLE: 3075446 92504562002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 6.6 20 12.7 30 64-132 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2020 04:39 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aceAnalytical www.pocofabs.com QUALITY CONTROL DATA Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 QC Batch: 580302 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92505313001, 92505313002 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 3069865 Matrix: Water Associated Lab Samples: 92505313001, 92505313002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 2.5 11/13/20 18:16 LABORATORY CONTROL SAMPLE & LCSD: 3069866 3070106 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Suspended Solids mg/L 250 244 244 97 97 90-110 0 25 SAMPLE DUPLICATE: 3070107 92505875001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 174 236 30 25 D6 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/19/2020 04:39 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 aceAnalytical www.pecolobs.com QUALITY CONTROL DATA Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 QC Batch: 580431 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92505313001, 92505313002 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE DUPLICATE: 3070425 92504392002 Dup Max Parameter Units Result Result RPD RPD Qualifiers pH at 25 Degrees C Std. Units 6.6 6.1 8 9 D6,H3 SAMPLE DUPLICATE: 3070426 92505313001 Dup Max Parameter Units Result Result RPD RPD Qualifiers pH at 25 Degrees C Std. Units 7.0 6.7 5 9 D6,H3 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/19/2020 04:39 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 a ce Analytical www.pacelobs.com QUALIFIERS Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/19/2020 04:39 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 aceAnalytical www.pacolabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Storm Water SEFA Denver, NC Pace Project No.: 92505313 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92505313001 D-SW-1 EPA1664B 581465 92505313002 D-SW-2 EPA1664B 581465 92505313001 D-SW-1 SM 2540D-2011 580302 92605313002 D-SW-2 SM 2540D-2011 580302 92505313001 D-SW-1 EPA 9040C 580431 92505313002 D-SW-2 EPA 9040C 580431 Date: 11/19/2020 04:39 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch Page 11 of 14 Jrj' Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Pke Ana lytical Document No.: Issuing Authority: F-CAR-CS-033-Rev,07 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville 0 Raleigh[] Mechanicsville[] Atlanta❑ I(ernersvilie❑ Sample Condition Client Name: -UponProject # Ef I/Nr���gVe�'&� i0�� Courier: ❑Fed Ex []UPS v ❑USPS `[QClient ® Commercial �(XPace []Other:tiT ,,I tt Custody Seal Present? []Yes ONo Seals Intact? [Dyes ONo WO#:92505313 1111111111111111111111 92505313 Date/initials Person Examining Contents: Packing Material: ❑Bubble Wrap [Bubble Bags ❑None ❑ Other Biological Tissue Frozen? / ®Yes []No KN/A Thermom71ete: �Vv et ❑❑ Blue None R Gun ID: 92TO61 Type of Ice: Correction Factor: Cooler Temp: Add/Subtract (°C) 0.0 Temp Should be above freezing to VC ❑Samples out of temp criteria. Samples on ice, cooling process Cooler Temp Corrected (°C): Li ° has begun USDA Regulated Soil N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, mv­ nhi., inrludine Hawaii and Puerto Rico)? i1Yes FINo Comments/Discrepancy: Chain of Custody Present? Yes ONO ❑N/A 1. Samples Arrived within Hold Time? �es ❑No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes jgNo ❑N/A 3. Rush Turn Around Time Requested? ❑Yes No ❑N/A 4. Sufficient Volume? RlYes ❑No []N/A S. Correct Containers Used? -Pace Containers Used? Aes Yes []No []NO ❑N/A ❑N/A 6. Containers Intact? Yes []No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes No ❑N/A 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: Wl( 1E1Yes ❑No ❑N/A 9. Headspace in VOAVials (>5-6mm)? Dyes (:]No LAIN/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ONO ❑No ?N/A JZ N/A 11. COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes [:]No CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Lot ID Of split containers: Date: Date: Page 12 of 14 I'A'ce/lnalytical Condition Upon Recei Document No.: F-CAR-CS-033-Rev,07 Page 2 of 2 Issuing Authority: Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottles Project Y Q5313 PM: MWI3 Due Date: 11/26/20 CLIENT: 92-SefaProup z z z V ® M u �' ? 2 a z b Z M N _ N v Oa N ~ Q z N 2 N v N V = z Z :R N M } ? nJ w v a Z x o a n c9i 2 N v °' 1: x a Z ¢' z 'Zz Q Z a o Z 2 a a a a O LA p a u z H o a _ n a 0 v n ? m O Z 2 M O y u u ry N d a re > ik v j j j N = N z c 7 v x D O = C a. a0 a > '3 .2 2 o e m m ro a ra a u N ro M n. n a u c ° v a E �' E A E a E a E O a s 4 O z a O a O a O a 4 C ° a m a n E a d e v ° E J E J E J E C w J E J E a J E a �, E E r; a `a a w` E a m J E , M > E > J > > s N m vi J E n -� E -1 E J E In E a E N N 0MNj N N N N o7E �y M N N ^� � V E a M N C m C rNi It 17-1 N en .4 M M M 0~1 01 I QI Q tJ Y�9 N M ® U° M « _ a m a m ® a m a m a m a m a m 3 l7 a Q a W a 0 a 0 a O a 0 ® U > (2 > U' C ® > 37 > 0. w o. yr a. to 0 ¢ rn > a o 1 '\\N\ I NN 1. 2 3 vX 5 G I \NM 7 9 LIN 10 � 11 \N1 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot # adjusted added Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina 0EHNR Certification Office (i.e, Out of hold, incorrect preservative, out of temp, incorrect containers. Page 13 of 14 -- ; M m a o A a N a a ••� O rp Oe 'd W 0 4s W N a ITEM # c m � � n � N 3 'a a a n CL n O d 0 m W n7 > p j ( C ty it z n "+ -o o ; � QQ as ydy�1) „ C d N O C t 3 0 v o ton) Z MATRIX CODE (seo vaW codes to n 1 I'I\ C SAMPLE TYPE (G=GRAB C=COIAP) Cn N ur p m rn o 0 _ z z r D m m < \ g m m r3 m z C) c En N p tl y n v Q QV(", vn �ij 3 m v \ - \ SAMPLETEIAPATCOLLECTION M m ym < p OF CONTAINERS v �aom v 0 m o` Unpreserved P S C / H2SO4 0 o m o # m 3 ( HNO3 3 ffi HCI � M N m ro m o NaOH fl: b J Na2S2o3 < M d Methanol E ! 0 m Other a Analyses Test YIN pH a n o z A TSS 7` ;`. Oil and Grease (Non -Polar IFc w; n o 3 t � v - s m V --- TEMP in C f' N N -- — ResidualChlorne (YIN) nz S. Received on Ice D (YIN) g T r ; uslo y Sealed o �,r, Cooler o YIN z Samples Intact (YIN) s R N "D S N 7 z o 6 N �"n <C N O D � O O D � (v D 0 = d < <p aC y N pp N O � n 0 El _ 0 3 �a a m n c m (D 1 Page 14 of 14