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HomeMy WebLinkAboutNCG030234_MRO Copy MONITORING REPORT_20210526A TransTmh Company May 24, 2021 NCDEQ Division of Land Resources 610 East Center Avenue, Suite 300 Moorseville, NC 28115 Subject: Monthly Discharge Monitoring Report Submittal Bendel Tank & Heat Exchanger, LLC 4823 N. Graham Street, Charlotte, Mecklenburg County Stormwater Permit COC Number NCG030234 Dear Division of Land Resources: 704.596.5112 office 866.596.5112 toll -free 704.597.5069 fax irozsa bendelcorp.com 4823 North Graham Street Charlotte, NC 28269 RECEIVED HAY 2 fit 2021 DENR-DEMLR Land Quality Section viooresville Regional Office As required by the referenced Stormwater Permit Certificate of Coverage, please find enclosed an original and one copy of the monthly Discharge Monitoring Report (DMR) for the referenced facility. This DMR is being submitted as designated in the Tier III section of the permit. Bendel continues to work toward returning to below benchmarks for zinc. Copper and TSS are both below the benchmark for this month. Since TSS was in Tier I status, it is no longer in a Tier I status. Copper is currently in Tier III status and this is considered one month under the benchmark. Please call me at (704) 596-5112 if you have any questions or if you require any additional information. Sine rely ���✓ Jim Rozsa O Vice President, Operations N 3 rmy M to A w , O- v � (D N 3 O0 S O fD C ny r+ (D (D o - cn o� � rD � + G) n• O � cu C: n x ( — -c m (D n M CD N (D (D O a) CrQ (D ❑l rD -0 (D rt �• Oo N (D O n' Q O LnO Q Ln (D r+ v v S N ---h rD 0- -rt \ No 0- Lit � C CD C (D o �' w 0 n Q 0- rD CL (D O y, In m v ram+ M n O a n- y; n S cuO 0 v O 3 (D 0- o v UQ rD m rni• �� ��r+�v A O rr v O T (D DA � I r+ C ((DD 0- T (D n a) �. 0 p Q v' rr Oil M N 0, C r+0 (D G 0- O o WN rD O � 3 rD -�h 0 M � v v r+ n < (D — o O a 0 0 o (n ° m Ln c r+ (D cn 00 Ln(D (D rD — C Q rt K n r) CFQ • N 1 0 in' O r2 Q Ln N v N rr rr 1 O r+ D I3 3. v 3 � h (D (D 0- v n (D Q r+ (D, _r, ram-+• Q L' o rD m s rD O (n N ro+ rD =r 00 M S (D -+, o (D (n D rD CL -0 rD 3 0 Q (D 0 m rD v v O r+ m s 0 r+ m f+ 0 o U. 0 O 0 O . n (DD M. 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[ 0 m — 7m> zm > _ Pnm = H c 0§m m § k s M® 2 \ 0 � e m m \ m 0 § \ j \ ❑/\> m % 3 > @ > @ a > j \ / _ z \ \ Co me > § z m * z 0 ) m e 0 m \7 2 2 / g � 2 L § �m c / El z _ > \ \ [Fnvironmentaf . o Quality d, o Stormwater Discharge Outfall (SDO) 01 �� A Qualitative Monitoring Report o 095 For guidance on filling out this form, please visit https:Hdeq.ne.gov/about/divisions/energy-mineral-land-r4urces/ npdes-stormwater-gps Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 0/3 /0 / 2 /3 /4 / Facility Name: Bendel Tank and Heat Exchanger County: Inspector: Date of Inspection: Time of Inspection: A?,1/Q AW Phone No. 704-596-5112 Total Event Precipitation (inches): 112 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Offi.. ........._......._. By this signatu SS l certify that this report is accurate and complete to the best of my knowledge: of Pkrmittee or Designee) 1. Outfall Description: Outfall No. 001 Structure (pipe, ditch, etc.): Ditch/Pipe Receiving Stream: Unnamed tributary of Irwin Creek Describe the industrial activities that occur within the outfall drainage area: Sandblasting, Painting, final product storage, loading/unloading Page 1 of 2 SWU-242, Last modified 06/01/2018 �a4i� ,4�., .: � �4,; _.q.,,. ,., . ��.] \ {�. �, . '.a � .� � 2. Color: Describe the color of the disch�ge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 10 3. Odor: Describe any distinct odgr that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 02 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 01 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 01 2 3 4 5 7. Is there any foam in the stormwater discharge? 0 Yes 0 No. 8. Is there an oil sheen in the stormwater discharge? OYes 0 No. 9. Is there evidence of erosion or deposition at the outfall? 0 Yes Q No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 430 14 )z 1; % rnvironmentat C7mdity , 0o r �j CD f� For guidance on filling out this form, please visit littps://deq.iie.gov/about/divisions/energy-mineral-land-resour npdes-stormwater-gps o� Permit No.: N/C/ / / / / / or Certificate of Coverage No.: N/C/G/ 0/3 /0 / 2 /3 /4 / Facility Name: Bendel Tank and Heat Exchanger County: Inspector: Date of Inspection: 746%/ Time of Inspection: 12, V AV Total Event Precipitation (inches): 112 No. 704-596-5112 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature.e,,I certify that this report is accurate and complete to the best of my knowledge: of P,6rmittee or Designee) 1. Outfall Description: Outfall No. 001 Structure (pipe, ditch, etc.): Ditch/Pipe Receiving Stream: Unnamed tributary of Irwin Creels Describe the industrial activities that occur within the outfall drainage area: Sandblasting, Painting, final product storage, loading/unloading Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 110 3. Odor: Describe any distinct chlorine odor, etc.): � that the discharge may have (i.e., smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 O2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: (1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? o Yes r No. 8. Is there an oil sheen in the stormwater discharge? oYes • No. 9. Is there evidence of erosion or deposition at the outfall? • Yes o No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 aceAnalytical www.pacelabs.com May 05, 2021 Mr. Jim Rozsa Bendel Corp. 4823 North Graham St. Charlotte, NC 28269 RE: Project: BENDEL Pace Project No.: 92535253 Dear Mr. Rozsa: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on April 27, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Coleman Marchin, AECOM Jennifer Wheat, AECOM �e pCCRF�� !'9epRpSOQ`/ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 ,�aneAnalj4ical www.pacelabs.com Project: BENDEL Pace Project No.: 92535253 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 aceAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: BENDEL 92535253 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92535253001 SW-1 EPA 1664B CJM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 2540D-2011 RED 1 PASI-A PASI-A = Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 aceAnalytical www,pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BENDEL Pace Project No.: 92535253 Sample: SW-1 Lab ID: 92535253001 Collected: 04/24/21 12:10 Received: 04/27/21 11:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 05/04/21 15:14 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper ND ug/L 5.0 1 04/30/21 01:55 04/30/2118:16 7440-50-8 Lead ND ug/L 5.0 1 04/30/21 01:55 04/30/2118:16 7439-92-1 Zinc 137 ug/L 10.0 1 04/30/21 01:55 04/30/21 18:16 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services -Asheville Total Suspended Solids 8.3 mg/L 3.6 1 04/30/21 18:15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 12 aceAnalj cal www,pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BENDEL Pace Project No.: 92535253 QC Batch: 618058 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92535253001 METHOD BLANK: 3251829 Matrix: Water Associated Lab Samples: 92535253001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 05/04/21 15:14 LABORATORY CONTROL SAMPLE: 3251830 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 17.6 88 64-132 MATRIX SPIKE SAMPLE: 3251831 92535647002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 8.3 35 64-132 M1 SAMPLE DUPLICATE: 3251832 92535647001 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 aceAnalytical www,pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BENDEL Pace Project No.: 92535253 QC Batch: 617275 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92535253001 METHOD BLANK: 3248010 Matrix: Water Associated Lab Samples: 92535253001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 04/30/2117:21 Lead ug/L ND 5.0 04/30/2117:21 Zinc ug/L ND 10.0 04/30/2117:21 LABORATORY CONTROL SAMPLE: 3248011 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 507 101 85-115 Lead ug/L 500 477 95 85-115 Zinc ug/L 500 458 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3248012 3248013 MS MSD 92535561001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 133 500 500 684 687 110 111 70-130 0 Lead ug/L ND 500 500 430 430 86 86 70-130 0 Zinc ug/L 324 500 500 784 789 92 93 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3248014 3248015 MS MSD 92535476001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 516 515 103 102 70-130 0 Lead ug/L ND 500 500 474 472 95 94 70-130 0 Zinc ug/L ND 500 500 467 468 92 92 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 ,A�ace Analytical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BENDEL Pace Project No.: 92535253 QC Batch: 617510 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92535253001 METHOD BLANK: 3249152 Matrix: Water Associated Lab Samples: 92535253001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/30/21 18:09 LABORATORY CONTROL SAMPLE: 3249153 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 251 240 96 90-110 SAMPLE DUPLICATE: 3249265 92535309001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 8870 8600 3 SAMPLE DUPLICATE: 3249266 92535717001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 323 355 9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 ,axAnaljdical www.pacelabs.com QUALIFIERS Project: BENDEL Pace Project No.: 92535253 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 aceAnalXical o www.pacelabs,com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BENDEL Pace Project No.: 92535253 Lab ID Sample ID QC Batch Method QC Batch 92535253001 SWA EPA1664B 618058 92535253001 SW-1 EPA 200.7 Rev 4.4 1994 617275 92535253001 SW-1 SM 2540D-2011 617510 Date: 05/05/2021 05:07 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Analytical Method Batch EPA 200.7 Rev 4.4 1994 617309 Page 9 of 12 Document Name: Document Revised: October 28, 2020 �IaceAnalytical Sample Condition Upon Rece(pt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office Laboratory receiving samples; Asheville ❑ Eden[] Greenwood ❑ Huntersville W Raleigh❑ Mec'h•'anicsville❑ Atlanta❑ ❑ Kernersville Client Name: WO# : 92535253 r,� t Project H: COMM,e xEJUPS njosps Do ❑ Commercial [�Pace ❑Other: Custody Seal Present? ❑Yes 'r❑, No Seals Intact? ❑Yes [EINo Date/Initials Person Examining Contents.i-i P I I r, ` ; ` Q Packing Material: ❑Bubble Wrap InBubble Bags ❑None ❑ Other Biological Tissue Frozen? ❑Yes ❑No EfN/A ThermomSIRGun ID: Type of Ice: (]Wet []Blue ❑None j ( Correction Factor: Cooler Temp: �' Add/Subtract (°C) 0.0°C Temp should be above freezing to VC ❑Samples out of temp criteria. Samples on Ice, cooling process Cooler Temp Corrected (°C):` ,' has begun USDA Regulated Soil ( Q'N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally, nyas MNn inrludino Hawaii and Puertn Ricol? nYes FINo Comments/Discrepancy: Chain of Custody Present? MYes ❑No, ❑N/A 1. Samples Arrived within Hold Time? dyes [:]No ❑N/A 2. Short Hold Time Analysis (02 hr.)? ❑Yes dNo QWA 3, Rush Turn Around Time Requested? ❑Yes dNo [I N/A 4. Sufficient Volume? 10Yes [:]No ❑N/A 5. Correct Containers Used? Pace Containers Used? NYes (Yes [-]No ❑No ❑N/A ❑N/A 6. Containers Intact? 6Yes ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ❑No f! N/A 8. Sample Labels Match COO -includes Date/Time/ID/Analysis Matrix: ❑Yes QNo ❑N/A 9<1`�'z1,01��'tcN- Headspace in VOA Vials (>5.6mm)? ❑Yes [—]No IdN A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑No []No '�' N/A , N/A 11, COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Lot ID of split containers: Date: Date: Field Data Required? ❑Yes ONO Page 10 of 12 Document Name: Document Revised: October 28, 2020 Sample Condition Upon Receipt(SCUR) Page 2 of 2 ?cekmoical' Document No.: Issuing Authority: , F-CAR-05.033-Itev.07 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/801S (water) DOC, LLHg **Bottom half of box is to list number of bottles Project 11 colo o 3 PM: NMG Due Date: 05/06/21 CLIENT: 92—AECOM CHA D \ Z ¢ z ¢ ¢ U x O z Z pV W Z N"V N 6 2 N Ir Z M •> 2 Z y 2 v d 2 S a 2 a .°�, ro T a m G Z N Z V o. a Z 2 Q Z z O ai a > O O " ¢ x0 W v a a O .o ? z z m S u N a > > a c N S Z `0 v v = N z C vNi O j ro Z j o c a w a a VV N �'N m a m a 'N a o CJ n E Ul n E E ¢LonO Ul E .D E ¢ E N O O O a a n a ¢ u E E E C-La a v o M E E E 20 :' E E E E E nLn N © N L vEi n vEi of rn Q Q 1 E O !D " N tn tn QE O O Ov E E a M N ri N v Z M N v rN-1 lJ Q W ur rti T M VI rl IA M a M a: QI N t7 61 1 Ol SL a y x lJ r'1 N N ffJ1 M C t7 rJ 0 a m a m a ® rl m a m a m a co a m 3 l7 a c9 ¢ l� a O a 0 a U a l7 > l7 > t9 o O > > a N a � a fn QJ a > o 1 2 3 4 S 7 8 \J\Nl 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative lot 4 adjusted added Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 11 of 12 N o In oo ti w I-] 4- w N ITEM # _. m o I , °o b O o a i o o m n F S o� 0 m o 0 9 c Z PF 66 g O D> aN � � N ro 0 4 3 o n T (t o N F � � c a m nz n n M 3 0 3 n x ® a In c 0 �oPfor�a�fo� n Y a»K (7 n A w fG o� r o,° vo`�o A N i -4 C' c to (- \ ��, p m u� ,� 1, P ry o a e CODE (sea valid codes to loll) ZMATRIX i m SAId PLE TYPE (G=GRAB C=COId P) 1 \ N m _ p1 o m -• o D 3 1I J o t D -zi '0 , Z m 0 T� -i Z Z M (� Q m 0 0 0 m n m m Z (V` > 0 . In 3 r•0- z . � D r7i m m SAMPLETEMPAT COLLECTION In M y i - �i-` C v a a v v a D 0 a o D� w < f+ �� # OF CONTAINERS fa -0 v v o N 0 0 • H2SO4 m n gp 3 m w a HNO3 � o ' 4 HCI Q N l NaOF1 w K c ` \\ ; Methanol j Other 0 C Analyses Test YIN t i s-• (\ Q \ v C Dj D D < TPH SGT•11011664 �( 200.7 (Cu, Ple, 7_n) z m t u \+ 1'SS 2540D c o 3 0 _ a `" a a a a a ro v w �'""" TCMP in C (-. m - - - ----_ Residual Chlorine (YIN) _ 0 0 o c a 0 Received on —_ �.,` 5 Ice (Y/N) ✓-n z ; Vt usto y Scaled o O Cooler (YIN) !..' o z ti ,11I / tjj (Samples (Y!N) (D 0 >7 _ m z o � c 0 C �C N N N m{ D O 0 � 91 Z �0 ID <D N K CD 7 .� Q CD a (� c �— O Iz 0 (o r O CD rD a c w m Page 12 of 12 Pace Analytical Services, LLC ,�aceAnaljdical © 9800 KinteyAve. SuiteNC 100 078 www.pacelabs.com (704)875-9092 May 05, 2021 Mr. Jim Rozsa Bendel Corp. 4823 North Graham St. hd;°eo Charlotte, NC 28269 ° RE: Project: BENDEL Pace Project No.: 92535253 Dear Mr. Rozsa Enclosed are the analytical results for sample(s) received by the laboratory on April 27, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me Sincerely, iV 1 Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Coleman Marchin, AECOM Jennifer Wheat, AECOM �e p,CCRF� y 9e0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 ��, l ,,FaceAnalydcal mm.pacelabs.com Project: BENDEL Pace Project No.: 92535253 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 accAnalyfical www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: BENDEL 92535253 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92535253001 SW-1 EPA 1664E CJM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 2540D-2011 RED 1 PASI-A PASI-A = Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BENDEL Pace Project No.: 92535253 Sample: SW-1 Lab ID: 92535253001 Collected: 04/24/21 12:10 Received: 04/27/21 11:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 05/04/21 15:14 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper ND ug/L 5.0 1 04/30/2101:55 04/30/2118:16 7440-50-8 Lead ND ug/L 5.0 1 04/30/21 01:55 04/30/2118:16 7439-92-1 Zinc 137 ug/L 10.0 1 04/30/2101:55 04/30/2118:16 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services -Asheville Total Suspended Solids 8.3 mg/L 3.6 1 04/30/21 18:15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 12 ,l .1-aceAnalyfical wmv.pacelabs.com QUALITY CONTROL DATA Project: BENDEL Pace Project No.: 92535253 QC Batch: 618058 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92535253001 METHOD BLANK: 3251829 Associated Lab Samples: 92535253001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 3251830 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 05/04/2115:14 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 17.6 88 64-132 MATRIX SPIKE SAMPLE: 3251831 92535647002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 8.3 35 64-132 M1 SAMPLE DUPLICATE: 3251832 Parameter Total Petroleum Hydrocarbons 92535647001 Dup Units Result Result mg/L ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 aCeAnalykal o wvm,pacelabs.com Project: BENDEL Pace Project No.: 92535253 QC Batch: 617275 QC Batch Method: EPA 200.7 Rev 4.4 1994 Associated Lab Samples: 92535253001 METHOD BLANK: 3248010 Associated Lab Samples: 92535253001 Parameter Units Copper ug/L Lead ug/L Zinc ug/L QUALITY CONTROL DATA Analysis Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 04/30/21 17:21 ND 5.0 04/30/2117:21 ND 10.0 04/3012117:21 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 3248011 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 507 101 85-115 Lead ug/L 500 477 95 85-115 Zinc ug/L 500 458 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3248012 MS 92535561001 Spike Parameter Units Result Cone. MSD Spike Cone, 3248013 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual Copper ug/L 133 500 500 684 687 110 111 70-130 0 Lead ug/L ND 500 500 430 430 86 86 70-130 0 Zinc ug/L 324 500 500 784 789 92 93 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3248014 3248015 MS MSD 92535476001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 516 515 103 102 70-130 0 Lead ug/L ND 500 500 474 472 95 94 70-130 0 Zinc ug/L ND 500 500 467 468 92 92 70-130 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 � aceAnalylical wmv,pacelabsxam QUALITY CONTROL DATA Project: BENDEL Pace Project No.: 92535253 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 617510 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92535253001 METHOD BLANK: 3249152 Matrix: Water Associated Lab Samples: 92535253001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/30/21 18:09 LABORATORY CONTROL SAMPLE: 3249153 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 251 240 96 90-110 SAMPLE DUPLICATE: 3249265 92535309001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 8870 8600 3 SAMPLE DUPLICATE: 3249266 92535717001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 323 355 9 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 i aceAnalylical wvm.pace Iabs.com QUALIFIERS Project: BENDEL Pace Project No.: 92535253 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 ,�aceAnalj&al www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: BENDEL 92535253 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92535253001 SWA EPA1664B 618058 92535253001 SW-1 EPA 200.7 Rev 4.4 1994 617275 EPA 200.7 Rev 4.4 1994 617309 92635253001 SW-1 SM 2540D-2011 617510 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/05/2021 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 12 Document Name: Document Revised: October 28, 2020 Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: ace Ana lwical1 F•CAR•CS•033-Rev.07 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Wuntersvilie A Raleigh[] Mec'h•'anicssviille❑ ❑ Atlantan Kernersville Client Name: WO# : 92535253 1 Project tt: III 1111111111111111111 ❑ Commercial UPace ❑Other: Custody Seal Present? ❑Yes `n No Seals intact? ❑Yes 92535253 I 3 No Date/Initials Person Examining Contents.., ontentsr/ r4 Packing Material: ❑Bubble Wrap QBubble Bags ❑None ❑ other Biological Tissue Frozen? Thermometer: ❑Yes ❑No CgN/A �IRGtin ID: C` �j�(i� { ®wet []Blue ❑None Type of Ice: Correction Factor: Cooler Temp: Add/Subtract ('C) O.O°C Temp should be above freezing to VC „tf ; ❑Samples out of temp criteria. Samples on ice, cooling process Cooler Temp Corrected ('C): = has begun USDA Regulated Soil ( ®fNIA, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (internationally, ^ I IYPS MNn inrludina Hawaii and Puerto Ricol? nYes FlNo Comments/Discrepancy: Chain of Custody Present? (5Yes ❑No, ❑N/A 1. Samples Arrived within Hold Time? 6es ❑No ❑N/A 2. Short Hold Time Analysis (02 hr.)? ❑Yes dNo [I N/A 3, Rush Turn Around Time Requested? Des dNo ❑N/A 4. Sufficient Volume? ]Yes ❑No ❑N/A S. (W t Correct Containers Used? -Pace Containers Used? NYes GdYes [:]No ❑No ❑N/A ❑N/A 6. Containers Intact? Yes ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? []Yes ❑No dN/A B. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: ❑Yes QNo ❑N/A .' 1") '�_ 1k7 1"s t`61(f,Cs Headspace in VOA Vials (>S-6mm)? ❑Yes ❑No ldN/A 1o. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑No ❑No `PN/A '9N/A 11, COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? ❑Yes ❑No Lot ID of split containers: Date/Time: Date: Date: Page 10 of 12 . aceAnalytrcal Document Name: Sample Condition Upon Recei Document No.: F-CAR-05.033-Rev,07 `Check mark top half of box if pH and/or dechiorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottles Document Revised: October 28, 2020 Page 2 of 2 Issuing Authority: Pace Carolinas Quality Office Project r-1� PH: N1`I6 Due Date: 06/06/21 CLIENT: 92-nI=COM CHA a U 4 Z a a a E Ln N �I 4 m Q Z 2 a e c N a E o In N m Q z 2 a d a E o O Ln 7 ® a m Z a c� 0. C U ° c-1 a m U z a V O N Ln N s-1 w a m a rn z = N CL G o N N Z a m i O M a ru a Q z N J Ln N �-1 N M m U a .... Q Z N J vEi N N (J aa.. v a 0 - 'o Co 4. C ° �, W � H d a `a a Q " s ri 00 4 N y S a u M Q N X W e 4 Z a a E J E o N D 0 d v a N w Q '= ,-i VI U ¢ x. a. V O N i E a. o l!1 N CA 0 ¢ U 4 i Z N o E Q E N m l7 a [[ 0 ¢ a \ 2 U x Q O J E Q C ttm�� A a z` M N N Q p J E q }- W al > Q \ Z 0. C n Q J E b Z) W 4 ,� 0 x O J E Q ct fL W ® .� m a Ln e3, � v 0. •2 � 9 V` a rL _° ' r, U ¢ Z u M N Cl. m N J E N � yr Q a u G tl. E ul � rn n a ® N ry 2 Z u J E a m •> a ttii N a c E a E o O c-I 1�7 ¢ z ti R7 > 0 O 0 V1 J E O N Lo ' Q JU n Z yaj a [' � w A 'Q J E D V CM q 1 F N \ \ N., I N\\\ 3 4 S \d\ N 6 P\— \NNN8 9 \\\N 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added lot N Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 11 of 12 A m e S m D 3 C C A oGJ to p M trl (n !. W to ITEM } .00. • ma0 O aCm n,o noo 0 3 o a N u m m a 0 o 3 o n -U O L D a N t n v O v n C ° n V p A A D n ) rP � \ T ,l g O v �o l.1ATRIX CODE (see valid codes to loft) C SAMPLETYPE (G=GRAB C=COMP) ( c m fJ D tV n G1 A U O c, n A Z Z 0 m t� 3 �n m Q m N m Lt m D o co D z Z o �r v-u > N � �V�t o d� g m SAMPLETEMPAT COLLECTION no m 1 \ `\�, `� T A•• - m ` c�Y{� ft OF CONTAINERS m m obi Q Unproserved {, 3 m v o v 0 p o` m 3 6 m m a G 0 H2SO4 # HNO3 y ro m R co m o m HCI N NaOH r�\ � m Na2S203 N o00 ���666DDD �. Methanol Other 'o _ _ Analyses Test YIN � m D � ra -- � -- � TPH SGT-HEM 1664 200.7 (Cu, Pb, Zn) A to N TSS 2540D to 3 o. o, 3 � D a M -- a z � � ' p fD .0 - _ v TEMP in C " z a to n o � L a o to - __ — Residual Chlorine (YIN) Received on Ice • �_`'� v nn D (Y/N) z l = A a uslo Y Sealed o O Cooler YIN z N � /) l/j les I I [Itt I (YIN) VI 3-10 m a: n O � C N 0 O K C7 O 'Y 0 rn ,Z ,-Zd m m (D a (p N 3 c cr 0 m a v � (o a n n c w m C Page 12 of 12