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HomeMy WebLinkAboutNC0004685_Fact Sheet_20210525Page 1 of 12    Fact Sheet NPDES Permit No. NC0004685 Permit Writer/Email Contact Julia Byrd, julia.byrd@ncdenr.gov: Date: April 6, 2021 Division/Branch: NC Division of Water Resources/NPDES Complex Permitting Permitting Action: ☒ Renewal ☐ Renewal with Expansion ☐ New Discharge ☐ Modification (Fact Sheet should be tailored to mod request) 1. Basic Facility Information Facility Information Applicant/Facility Name: Electric Glass Fiber America, LLC Applicant Address: 940 Washburn Switch Rd, Shelby, NC 28150 Facility Address: NCSR 1313, West of Shelby, Cleveland County Permitted Flow: 1.3 MGD Facility Type/Waste: 95 % Industrial, 5% Domestic Facility Class: Class III Biological WPCS, PC2 Treatment Units: Bar screen, grinder, flow equalization tank with pH adjustment (CaOH2), coagulation, flocculation, clarification, activated sludge/ aeration basins, secondary clarifiers, and tertiary sand filters. Sludge gravity thickener, belt filter press, and disposal of biosolids to landfill Pretreatment Program (Y/N) N County: Cleveland Region Mooresville Briefly describe the proposed permitting action and facility background: Process Description Electric Glass Fiber America, formerly PPG, a fiberglass fiber manufacturing facility in Shelby, NC.The facility is subject to NPDES permit NC0004685, to discharge 1.3 MGD of 95% industrial and 5% domestic treated wastewater to Brushy Creek (001) and Overflow Branch (002) classified as Class C waters of the Broad River Basin. The processing plant concentrates the bulk of its fiberglass manufacturing on the reinforced plastics market. Manufacturing beings with glass raw material including limestone, silica, boron, clay, and fluorspar which are blended into powder form and melted in furnaces. The batch melt furnaces operate at 2800ºF to transform the batch into molten glass which is drawn from other furnaces through electrically heated Page 2 of 12    platinum bushings into continuous fibers. The fibers are then gathered into strands and either spooled or cut in specific length. Cooling water is sprayed on the glass and keep strands contact point clean during the winding process. A water based “binder” is applied to individual fibers as they are drawn from the furnaces before being gathered into strands. The binder is a proprietary mixture of resins, film formers, lubricants, surfactants and coupling agents emulsified in a water solution. The majority of wastewater treated at the facility is spray water, lost binder, and cleaning water. The EGFA facility has two outfalls, Outfall 001 is the effluent from the wastewater treatment plant which receives wastewater from sanitary, research, boiler blowdown, forming, fabrication, coating, process wastewater, storm drains/garage pads. Outfall 002 is a non-contact cooling water outfall and currently permitted in accordance with the general permit. Wastewater is also receiving from Hanwha, a EGFA joint venture with GE, which produces a fiberglass reinforced polypropylene sheet material that is sold to molders. Permit History This permit was first issued on May 31, 1978. The permit was summarily adjudicated. It is not entirely evident why the permit was adjudicated; however, a review of historical files seems to indicate that the adjudication was filed because of a disagreement with limit development. At issuance, final effluent limitations were based on 40 CFR 410.32, Subpart C: Textile Dry Processing). While the permit was being adjudicated, interim limits were established based on the results of a field calibrated water quality model. Upon resolution of the adjudication (it was determined that textile guidelines did not apply to EGFA’s discharge), the permit was reissued in August of 1979 with water-quality limitations based on the results of the model. This original series of waste load allocations were based on a discharge flow of 0.875 MGD. The permit was renewed in 1985 with a change in allocation, however the reason for the change is not evidenced in the files. In 1988, the Division, completed a waste load allocation for this facility at an expanded flow of 1.3 MGD. The increase in flow was based on process modifications in the manufacturing facility. The Division evaluated EGFA’s discharge and developed appropriate water quality-based limitations. The current effluent limitations for BOD5 and NH3-N are based on the level B model run in 1988. The current TSS and oil and grease limits are BPJ, apparently based on the BOD5 limits developed as resolution to the 1978/79 adjudication. According to the 1998 permit renewal Fact Sheet, extensive research was conducted to determine if any federal guidelines exist for such a manufacturing operation. EGFA was contacted for a detailed description of the manufacturing process and associated end products. After conversations with EPA, regarding the applicability of textile and glass guidelines, it was determined that neither set of guidelines applied to EGFA’s process. Hanwha’s operation falls under the authority of 40 CFR 463; however, manufacturing at Hanwha is a dry process and wastewater transferred to EGFA is largely cooling water, cleaning water and domestic wastewater. Therefore, guidelines do not apply to this aspect of EGFA’s effluent either. Current Application EGFA’s permit renewal application was received on March 18, 2018 which included a request for the following modifications to the current permit requirements: 1. Removing fluoride monitoring since the facility no longer utilizes fluoride in current processes 2. Reducing oil and grease sampling to once per month 3. Sampling for ammonia only in winter months (October to March) 4. Reducing total copper, lead, and zinc sampling to semi-annually 5. Removing the PC2 facility classification Permit Action After review of the application materials and requests, the Division determined to re-issue the permit with the following modifications: 1. Total copper, zinc, and lead monitoring requirements were removed based on the RPA. 2. Season ammonia nitrogen limits were added with more stringent limits April – October. 3. Oil and Grease monitoring was reduced from weekly to monthly. 4. Quarterly upstream and effluent hardness monitoring was added. Page 3 of 12    2. Receiving Waterbody Information: Receiving Waterbody Information Outfalls/Receiving Stream(s): Outfall 001 – Brushy Creek Outfall 002 – Overflow Branch Stream Segment: 9-50-29 9-50-32-1 Stream Classification: C Drainage Area (mi2): 15.1 Summer 7Q10 (cfs) 4.0 Winter 7Q10 (cfs): 7.6 30Q2 (cfs): - Average Flow (cfs): 21.0 IWC (% effluent): 33% 303(d) listed/parameter: No Subject to TMDL/parameter: Yes- Statewide Mercury TMDL implementation Basin/Sub-basin/HUC: Broad River/ 03-08-04 USGS Topo Quad: F12SE Page 4 of 12    3.Effluent Data Summary Effluent data for Outfall 001 is summarized below for the period of January 2016 through August 2020 Parameter Units Average Max Min Permit Limit Flow MGD 0.54 0.8 0.01 MA 1.3 BOD, 5-day, 20ºC (mass) lbs/day 11.56 43.6 <0.1 DM 325.5 MA 217.0 BOD, 5-day, 20ºC (conc.) mg/l 2.53 11.1 <2 DM 30.0 MA 20.0 Total Suspended Solids mg/l 2.92 25 <2.5 DM 146.0 MA 20.0 NH3N (mass) lbs/day 0.46 2.03 <0.1 DM 97.5 MA 65.0 NH3N (conc.) mg/l 0.11 0.48 <0.1 DM 9.0 MA 6.0 pH SU - 7.7 6.2 6.0 ≥ pH ≤ 9.0 Fecal coliform #/100 ml 2.40 38 1 Monitor weekly DO mg/l 8.10 12.8 5.2 DA ≥5.0 TRC µg/l 11.37 21 2 DM 17 Temperature °C 21.50 29 11 Monitor daily Total Nitrogen mg/l 10.4 17.4 3.6 Monitor quarterly Total Phosphorous mg/l 11.55 4.6 <0.05 Monitor quarterly Oil and Grease mg/l 4.96 10 <0.6 Monitor weekly Fluoride mg/L 0.59 2.4 0.1 Monitor quarterly Total Lead mg/l <0.005 <0.005 <0.005 Monitor quarterly Total Copper mg/l <0.005 <0.005 <0.005 Monitor quarterly Total Zinc mg/l 0.009 0.025 <0.001 Monitor quarterly Chronic Toxicity P/F Pass Monitor quarterly MA-Monthly Average, DM-Daily Maximum, DA=Daily Average Effluent data for Outfall 002 is summarized below for the period of January 2016 through August 2020 Parameter Units Average Max Min Permit Limit Flow MGD 0.20 0.55 0.01 Estimate and report TRC µg/l 11.67 21 <2 DM 28.0 Temperature1 °C 15.67 19 11 See note 1 pH SU - 7.3 6.7 6.0 ≥ pH ≤ 9.0 1The temperature of effluent shall not cause an increase in the temperature of the receiving stream more than 2.8°C and in no case cause the ambient water temperature to exceed 29°C Page 5 of 12    4. Instream Data Summary Instream monitoring may be required in certain situations, for example: 1) to verify model predictions when model results for instream DO are within 1 mg/l of instream standard at full permitted flow; 2) to verify model predictions for outfall diffuser; 3) to provide data for future TMDL; 4) based on other instream concerns. Instream monitoring may be conducted by the Permittee, and there are also Monitoring Coalitions established in several basins that conduct instream sampling for the Permittee (in which case instream monitoring is waived in the permit as long as coalition membership is maintained). If applicable, summarize any instream data and what instream monitoring will be proposed for this permit action: The current permit requires instream monitoring for dissolved oxygen, temperature, and conductivity upstream and downstream three times per week in June, July, August, and September; and once per week the remainder of the year. Students t-tests were run at a 95% confidence interval to analyze relationships between instream data recorded in DMRs from January 1, 2016 through August 31, 2020. A statistically significant difference is determined when the t-test p-value result is < 0.05. Review of instream data for the past three years indicates that the dissolved oxygen standard of 5 mg/l was maintained. The downstream temperature did not exceed 29 degrees Celsius, and the differential temperature did not exceed 2.8 degrees Celsius [per 15A NCAC 02B .0211] during the period reviewed. It was concluded that there were no statistically significant differences between upstream and downstream dissolved oxygen, temperature, and conductivity. No changes for monitoring requirements are proposed. Is this facility a member of a Monitoring Coalition with waived instream monitoring (Y/N): No Name of Monitoring Coalition: NA 5. Compliance Summary Summarize the compliance record with permit effluent limits (past 5 years): The facility has not had any violations of permitted effluent limits in the last five years. Summarize the compliance record with aquatic toxicity test limits and any second species test results (past 5 years): The facility passed 19 of 19 quarterly chronic toxicity tests. Summarize the results from the most recent compliance inspection: The last facility inspection conducted January 9, 2019 and reported that the facility appeared to be operating properly and well-maintained. Compliance samples were collected by RO staff for Oil and Grease, TSS, zinc, copper, and lead. Results showed all analytes were present at the respective minimum reporting levels. 6. Water Quality-Based Effluent Limitations (WQBELs) Dilution and Mixing Zones In accordance with 15A NCAC 2B.0206, the following streamflows are used for dilution considerations for development of WQBELs: 1Q10 streamflow (acute Aquatic Life); 7Q10 streamflow (chronic Aquatic Life; non-carcinogen HH); 30Q2 streamflow (aesthetics); annual average flow (carcinogen, HH). If applicable, describe any other dilution factors considered (e.g., based on CORMIX model results): NA If applicable, describe any mixing zones established in accordance with 15A NCAC 2B.0204(b): NA Page 6 of 12    Oxygen-Consuming Waste Limitations Limitations for oxygen-consuming waste (e.g., BOD) are generally based on water quality modeling to ensure protection of the instream dissolved oxygen (DO) water quality standard. Secondary TBEL limits (e.g., BOD= 30 mg/l for Municipals) may be appropriate if deemed more stringent based on dilution and model results. If permit limits are more stringent than TBELs, describe how limits were developed: Limitations for BOD5 and NH3- N are based on a level B model conducted in 1988 for protection of instream dissolved oxygen. Oil and grease limits (10.0 mg/L MA, 15.0 mg/L) are based on BPJ. Ammonia and Total Residual Chlorine Limitations Limitations for ammonia are based on protection of aquatic life utilizing an ammonia chronic criterion of 1.0 mg/l (summer) and 1.8 mg/l (winter). Acute ammonia limits are derived from chronic criteria, utilizing a multiplication factor of 3 for Municipals and a multiplication factor of 5 for Non-Municipals. Limitations for Total Residual Chlorine (TRC) are based on the NC water quality standard for protection of aquatic life (17 ug/l) and capped at 28 ug/l (acute impacts). Due to analytical issues, all TRC values reported below 50 ug/l are considered compliant with their permit limit. Describe any proposed changes to ammonia and/or TRC limits for this permit renewal: TRC limits in the current permit apply to outfall 001 (17 µg/L DM) and outfall 002 (28 µg/L DM) are based on NC water quality standards (15A NCAC 2B .0200). There are no proposed changes. The current permit requires weekly sampling for NH3-N with limits for mass (65.0 lbs/day MA, 97.5 lbs/day DM) and concentration (6.0 mg/L MA, 9.0 mg/L DM) based on the level B model conducted in the 1988 permit renewal. Ammonia limits in the current permit apply to outfall 001 and are based on the level B model conducted in 1988. Based on the 2016 NPDES permitting guidance for implementation of ammonia criteria and results from the NH3/TRC Wasteload Allocation tool (attached), the maximum allowable concentrations for summer and winter are 2.5 mg/L and 7.8 mg/L, respectively. The winter and summer daily maximum allowable concentrations based on the WLA would be less stringent than the current permit requirements, which are based on the protection of dissolved oxygen in the receiving stream. The reissued permit will maintain the current effluent limits for winter monthly average, summer, and winter daily maximum; and summer monthly average limits will be added to the reissued permit based on protection of aquatic life. Based on the maximum and average ammonia concentrations reported in DMRs over the last 4.5 years, 0.48 mg/L and 0.11 mg/L respectively, and therefore it is anticipated that the facility currently has capacity to meet the new seasonal effluent limits. Reasonable Potential Analysis (RPA) for Toxicants If applicable, conduct RPA analysis and complete information below. The need for toxicant limits is based upon a demonstration of reasonable potential to exceed water quality standards, a statistical evaluation that is conducted during every permit renewal utilizing the most recent effluent data for each outfall. The RPA is conducted in accordance with 40 CFR 122.44 (d) (i). The NC RPA procedure utilizes the following: 1) 95% Confidence Level/95% Probability; 2) assumption of zero background; 3) use of ½ detection limit for “less than” values; and 4) streamflows used for dilution consideration based on 15A NCAC 2B.0206. Effective April 6, 2016, NC began implementation of dissolved metals criteria in the RPA process in accordance with guidance titled NPDES Implementation of Instream Dissolved Metals Standards, dated June 10, 2016. Page 7 of 12    A reasonable potential analysis was conducted on effluent toxicant data collected between January 2016 and August 2020. Pollutants of concern included toxicants with positive detections and associated water quality standards/criteria. Based on this analysis, the following permitting actions are proposed for this permit:  Effluent Limit with Monitoring. The following parameters will receive a water quality-based effluent limit (WQBEL) since they demonstrated a reasonable potential to exceed applicable water quality standards/criteria: None  Monitoring Only. The following parameters will receive a monitor-only requirement since they did not demonstrate reasonable potential to exceed applicable water quality standards/criteria, but the maximum predicted concentration was >50% of the allowable concentration: Fluoride  No Limit or Monitoring: The following parameters will not receive a limit or monitoring, since they did not demonstrate reasonable potential to exceed applicable water quality standards/criteria and the maximum predicted concentration was <50% of the allowable concentration: Total lead, copper, and zinc. Based on the RPA showing no reasonable potential to violate NC WQS and demonstrating a maximum predicated concentration of less than 50% of the allowable CW, the monitoring requirements for total lead, copper, and zinc will be removed from the reissued permit. The RPA results for fluoride demonstrated a maximum predicted concentration greater than 50% of the allowable concentration, and therefore the quarterly monitoring requirements for fluoride in the current permit will continue. Toxicity Testing Limitations Permit limits and monitoring requirements for Whole Effluent Toxicity (WET) have been established in accordance with Division guidance (per WET Memo, 8/2/1999). Per WET guidance, all NPDES permits issued to Major facilities or any facility discharging “complex” wastewater (contains anything other than domestic waste) will contain appropriate WET limits and monitoring requirements, with several exceptions. The State has received prior EPA approval to use an Alternative WET Test Procedure in NPDES permits, using single concentration screening tests, with multiple dilution follow-up upon a test failure. Describe proposed toxicity test requirement: The current permit requires chronic toxicity testing at outfall 001 @ 33% effluent concentration. No changes are proposed. Mercury Statewide TMDL Evaluation There is a statewide TMDL for mercury approved by EPA in 2012. The TMDL target was to comply with EPA’s mercury fish tissue criteria (0.3 mg/kg) for human health protection. The TMDL established a wasteload allocation for point sources of 37 kg/year (81 lb/year) and is applicable to municipals and industrial facilities with known mercury discharges. Given the small contribution of mercury from point sources (~2% of total load), the TMDL emphasizes mercury minimization plans (MMPs) for point source control. Municipal facilities > 2 MGD and discharging quantifiable levels of mercury (>1 ng/l) will receive an MMP requirement. Industrials are evaluated on a case-by-case basis, depending if mercury is a pollutant of concern. Effluent limits may also be added if annual average effluent concentrations exceed the WQBEL value (based on the NC WQS of 12 ng/l) and/or if any individual value exceeds a TBEL value of 47 ng/l Other TMDL/Nutrient Management Strategy Considerations If applicable, describe any other TMDLs/Nutrient Management Strategies and their implementation within this permit: NA Other WQBEL Considerations If applicable, describe any other parameters of concern evaluated for WQBELs: NA Page 8 of 12    If applicable, describe any special actions (HQW or ORW) this receiving stream and classification shall comply with in order to protect the designated waterbody: NA If applicable, describe any compliance schedules proposed for this permit renewal in accordance with 15A NCAC 2H.0107( c)(2)(B), 40CFR 122.47, and EPA May 2007 Memo: Based on the determination to reissue the permit with more stringent effluent limits for summer monthly average NH3-N, a schedule of compliance may be needed for the facility to meet the proposed limits. If applicable, describe any water quality standards variances proposed in accordance with NCGS 143- 215.3(e) and 15A NCAC 2B.0226 for this permit renewal: NA 7. Technology-Based Effluent Limitations (TBELs) Describe what this facility produces: fiberglass, fiberglass reinforced polypropylene List the federal effluent limitations guideline (ELG) for this facility: As discussed in Section 1, there are no federal effluent guidelines which are applicable to EGFA’s process; and Hanwha’s operation falls under the authority of 40 CFR 463, Plastics Laminating, but the wastewater received at EGFA’s facility is largely cooling water, cleaning water and domestic wastewater. It was established that EPA-promulgated effluent guidelines are not applicable to EGFA’s industrial discharge. For ELG limits, document the calculations used to develop TBEL limits: NA If any limits are based on best professional judgement (BPJ), describe development: When the permit was initially issued it was determined that no federal effluent guidelines are applicable to the effluent; and requirements for TSS and O&G were based on BPJ. Document any TBELs that are more stringent than WQBELs: NA Document any TBELs that are less stringent than previous permit: NA 8. Antidegradation Review (New/Expanding Discharge): The objective of an antidegradation review is to ensure that a new or increased pollutant loading will not degrade water quality. Permitting actions for new or expanding discharges require an antidegradation review in accordance with 15A NCAC 2B.0201. Each applicant for a new/expanding NPDES permit must document an effort to consider non-discharge alternatives per 15A NCAC 2H.0105(c)(2). In all cases, existing instream water uses and the level of water quality necessary to protect the existing use is maintained and protected. If applicable, describe the results of the antidegradation review, including the Engineering Alternatives Analysis (EAA) and any water quality modeling results: NA 9. Antibacksliding Review: Sections 402(o)(2) and 303(d)(4) of the CWA and federal regulations at 40 CFR 122.44(l) prohibit backsliding of effluent limitations in NPDES permits. These provisions require effluent limitations in a reissued permit to be as stringent as those in the previous permit, with some exceptions where limitations may be relaxed (e.g., based on new information, increases in production may warrant less stringent TBEL limits, or WQBELs may be less stringent based on updated RPA or dilution). Are any effluent limitations less stringent than previous permit (YES/NO): No If YES, confirm that antibacksliding provisions are not violated: Page 9 of 12    10. Monitoring Requirements Monitoring frequencies for NPDES permitting are established in accordance with the following regulations and guidance: 1) State Regulation for Surface Water Monitoring, 15A NCAC 2B.0500; 2) NPDES Guidance, Monitoring Frequency for Toxic Substances (7/15/2010 Memo); 3) NPDES Guidance, Reduced Monitoring Frequencies for Facilities with Superior Compliance (10/22/2012 Memo); 4) Best Professional Judgement (BPJ). Per US EPA (Interim Guidance, 1996), monitoring requirements are not considered effluent limitations under Section 402(o) of the Clean Water Act, and therefore anti-backsliding prohibitions would not be triggered by reductions in monitoring frequencies. Based on the RPA conducted with this permit renewal, the maximum predicted concentrations for total copper, lead, and zinc are less than 50% of the allowable concentrations. As noted previously, based on the RPA results which demonstrated no reasonable potential to violate state WQS, it is recommended to remove monitoring requirements for total copper, lead, and zinc from the reissued permit. The renewal application included a request to reduce O&G monitoring from once per week to once per month. Based on DMR data from the last 4.5 years oil and grease has been detected above 5 mg/L on three occasions; and the maximum detected was 10 mg/L on one occasion. In accordance with the state and federal regulations referenced above, as there are no changes in production or dilution that warrant exception of these requirements, the current effluent limits for O&G will remain in the reissued permit, with monitoring reduced from weekly to monthly. 11. Electronic Reporting Requirements The US EPA NPDES Electronic Reporting Rule was finalized on December 21, 2015. Effective December 21, 2016, NPDES regulated facilities are required to submit Discharge Monitoring Reports (DMRs) electronically. While NPDES regulated facilities would initially be required to submit additional NPDES reports electronically effective December 21, 2020, EPA extended this deadline from December 21, 2020, to December 21, 2025. The current compliance date, effective January 4, 2021, was extended as a final regulation change published in the November 2, 2020 Federal Register This permit contains the requirements for electronic reporting, consistent with Federal requirements. Page 10 of 12    12.Summary of Proposed Permitting Actions: A. Current Permit Conditions and Proposed Changes Outfall 001 1.3 MGD Parameter Current Permit Proposed Change Basis for Condition/Change Flow MA 1.3 MGD No change 15A NCAC 2B .0505 BOD5 20ºC (mass) MA 217.0 lbs/day DM 325.5 lbs/day No change WQBEL. Based on protection of DO standard. 15A NCAC 2B.0200 BOD5 20ºC (conc) MA 22.0 mg/L DM 30.0 mg/L No change WQBEL. Based on protection of DO standard. 15A NCAC 2B.0200 Total Suspended Solids MA 20.0 mg/L DM 146.0 mg/L No change BPJ NH3-N (mass) MA 65.0 lbs/day DM 97.5 lbs/day Summer: MA 27.1 lbs/day DM 97.5 lbs/day Winter: MA 65.0 lbs/day DM 97.5 lbs/day WQBEL. Based on 2016 NPDES Implementation of Ammonia Criteria and protection of DO standard. 15A NCAC 2B.0200 NH3-N (conc) MA 6.0 mg/L DM 9.0 mg/L Summer: MA 2.5 mg/L DM 9.0 mg/L Winter: MA 6.0 mg/L DM 9.0 mg/L WQBEL. Based on 2016 NPDES Implementation of Ammonia Criteria and protection of DO standard. 15A NCAC 2B.0200 Dissolved Oxygen DA ≥ 5.0 mg/L No change WQBEL. State WQ standard, 15A NCAC 2B .0200 Dissolved Oxygen (Instream) Monitor & report No change WQBEL. State WQ standard, 15A NCAC 2B .0200 pH 6 – 9 SU No change WQBEL. State WQ standard, 15A NCAC 2B .0200 Temperature, ºC Monitor daily No change Surface Water Monitoring, 15A NCAC 2B .0508 Temperature, ºC (Instream) Monitor & report No change Surface Water Monitoring, 15A NCAC 2B .0508 Fecal Coliform Monitor weekly No change WQBEL. State WQ standard, 15A NCAC 2B .0200 Total Nitrogen Monitor quarterly No change Surface Water Monitoring, 15A NCAC 2B .0508 Total Phosphorous Monitor quarterly No change Surface Water Monitoring, 15A NCAC 2B .0508 Conductivity (Instream) Monitor & report No change Surface Water Monitoring, 15A NCAC 2B .0508 Oil and Grease MA 10.0 mg/L DM 15.0 mg/L Monitor weekly MA 10.0 mg/L DM 15.0 mg/L Monitor monthly BPJ Total Hardness No requirement Monitor effluent and upstream quarterly Hardness-dependent dissolved metals WQS, 2016 Page 11 of 12    Total Lead Monitor quarterly No requirement Based on results of RPA; No RP, predicted max ≤ 50% of allowable concentration. WQS 15A NCAC 2B Fluoride Monitor quarterly No requirement Based on results of RPA; No RP but predicted max ≥ 50% of allowable concentration. WQS 15A NCAC 2B Total Zinc Monitor quarterly No requirement Based on results of RPA; No RP, predicted max ≤ 50% of allowable concentration. WQS 15A NCAC 2B Total Copper Monitor quarterly No requirement Based on results of RPA; No RP, predicted max ≤ 50% of allowable concentration. WQS 15A NCAC 2B Total Residual Chlorine 17 µg/L No change WQBEL. State WQ standard, 15A NCAC 2B .0200 Chronic Toxicity @ 33% (quarterly) No change No toxics in toxic amounts MGD – Million gallons per day, MA - Monthly Average, DM – Daily Max, DA – Daily Average B. Table. Current Permit Conditions and Proposed Changes Outfall 002 Parameter Current Permit Proposed Change Basis for Condition/Change Flow Monitor semi-annually No change 15A NCAC 2B .0505 Temperature, ºC Monitor & report No change Surface Water Monitoring, 15A NCAC 2B .0508 Total Residual Chlorine 28 µg/L No change WQBEL. State WQ standard, 15A NCAC 2B .0200 pH 6 – 9 SU No change WQBEL. State WQ standard, 15A NCAC 2B .0200 MGD – Million gallons per day, MA - Monthly Average, DM – Daily Max Page 12 of 12  13. Public Notice Schedule: Permit to Public Notice: 04/20/2021 Per 15A NCAC 2H .0109 & .0111, The Division will receive comments for a period of 30 days following the publication date of the public notice. Any request for a public hearing shall be submitted to the Director within the 30 days comment period indicating the interest of the party filing such request and the reasons why a hearing is warranted. 14. Fact Sheet Addendum (if applicable): The permittee, Electric Glass Fiber America, LLC, submitted comments on May 19, 2021 regarding revisions to the wastewater treatment plant components, requesting removal of the fluoride monitoring requirement, a typographical error by omission for TRC monitoring, and requesting removal of the PC II classification in the renewed permit. The letter from the permittee and responses from the Division are provided as attachments to this Fact Sheet. A copy of the draft permit was also submitted to US EPA Region 4, the Mooresville Regional Office, the DWR Operator Certification Program, the DWR Ecosystems Branch, and the DWR Aquatic Toxicology Branch. The DWR Operator Certification Program submitted comments via email on April 20, 2021 noting the permit should be dual classified as WW-III and PC II per 15A NCAC 08G .0306. The Mooresville Regional Office responded on May 21, 2021 in agreement that the designation as a PC -II facility should remain. See the attached email correspondences. No other comments were received by these groups. Were there any changes made since the Draft Permit was public noticed (Yes/No): Yes If Yes, list changes and their basis below: 1.1.3 MGD wwtp component list was updated based on information provided by the permittee; 2.Correction made on the Fact Sheet, Section 6, Toxicity Testing required at outfall 001 only; 3.Typographical error corrected on permit Part I A. (1) a., footnote 3 regarding TRC monitoring; 4.Dual designation of Biological WPCS III, PC2 will remain in the permit. Permittee will request this change in coordination with the MRO; 15.Fact Sheet Attachments: •Monitoring Violations Summary •RPA Spreadsheet Summary •Wasteload Allocation Summary •2016 NPDES Implementation of Ammonia Criteria-Update •Dissolved Metals Implementation Freshwater •Permit Renewal Application •Affidavit of Public Notice - The Star •Draft Permit Comments from EFGA •Draft Permit responses from the Division PERMIT FACILITY COUNTY REGION MONITOR REPORT MOMONITOR REPORT YEOUTFALL/PPI/FIELD/WNC0004685 Electric Glass Fiber AmCleveland Mooresville 2 2020 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 2 2019 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 2 2015 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 4 2020 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 4 2019 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 6 2020 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 6 2019 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 8 2020 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 8 2019 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 10 2019 002NC0004685 Electric Glass Fiber AmCleveland Mooresville 12 2019 002 LOCATION TYPE WELL ID LOCATION PARAMETER VIOLATIONDATE FREQUENCY UNIT OF MEASUREOutfall 03/31/2020Outfall 03/31/2019Outfall EffluentpH 02/28/2015 Semi-annuallysuOutfall 05/31/2020Outfall 05/31/2019Outfall 07/31/2020Outfall 07/31/2019Outfall 10/01/2020Outfall 10/01/2019Outfall 12/01/2019Outfall 01/31/2020 LIMIT CALCULATED VALUE % OVER VIOLATION TYPE VIOLATION ACTION VIOLATION COMMENTLAST UPDATED BY IDOutfall MissingNone bimsprod.cronOutfall MissingNo Action, BIMS Calculonly require semi annuaori.tuviaSampling Location MissNo Action, BIMS CalculSampling done ad repo ori.tuviaOutfall MissingNone bimsprod.cronOutfall MissingNo Action, BIMS Calculonly require semi annuaori.tuviaOutfall MissingNone bimsprod.cronOutfall MissingNo Action, BIMS Calculonly require semi annuaori.tuviaOutfall MissingNone bimsprod.cronOutfall MissingNo Action, BIMS Calculonly require semi annuaori.tuviaOutfall MissingNo Action, BIMS CalculSemi Annual samplingori.tuviaOutfall MissingNo Action, BIMS CalculSemi Annual sampling -ori.tuvia TIMESTAMP4/20/2020 1:14:41 AM##################3/27/2017 2:23:31 PM6/20/2020 1:51:02 AM##################8/20/2020 1:27:36 AM######################################################2/24/2020 8:45:36 AM2/24/2020 8:46:00 AM REQUIRED DATA ENTRYNameWQSTypeChronicModifierAcute PQL UnitsFacility NameElectric Glass Fiber America, LLCPar01ArsenicAquactic LifeC 150 FW 340 ug/LWWTP/WTP ClassIIIPar02ArsenicHuman Health Water SupplyC 10 HH/WS N/A ug/LNPDES PermitNC0004685Par03BerylliumAquatic LifeNC 6.5 FW 65 ug/LOutfall001Par04CadmiumAquatic LifeNC 1.7742 FW 12.5008 ug/LFlow, Qw (MGD)1.300Par05ChloridesAquatic LifeNC 230 FWmg/LReceiving StreamBrushy CreekPar06 Chlorinated Phenolic CompoundsWater SupplyNC 1 A ug/LHUC NumberPar07Total Phenolic CompoundsAquatic LifeNC 300 A ug/LStream ClassPar08Chromium IIIAquatic LifeNC 388.6840 FW 3217.5917 ug/LPar09Chromium VIAquatic LifeNC 11 FW 16 µg/L7Q10s (cfs)4.00Par10Chromium, TotalAquatic LifeNC N/A FW N/A µg/L7Q10w (cfs)7.60Par11CopperAquatic LifeNC 27.3996 FW 45.0541 ug/L30Q2 (cfs)Par12CyanideAquatic LifeNC 5 FW 22 10 ug/LQA (cfs)21.00Par13FluorideAquatic LifeNC 1,800 FW ug/L1Q10s (cfs)3.34Par14LeadAquatic LifeNC 14.7996 FW 418.8957 ug/LEffluent Hardness271.17 mg/L (Avg)Par15MercuryAquatic LifeNC 12 FW 0.5ng/LUpstream Hardness25 mg/L (Avg)Par16MolybdenumHuman HealthNC 2000 HH ug/LCombined Hardness Chronic107.47 mg/LPar17NickelAquatic LifeNC 127.8524 FW 1242.5619 µg/LCombined Hardness Acute117.63 mg/LPar18NickelWater SupplyNC 25.0000 WS N/A µg/LData Source(s)Par19SeleniumAquatic LifeNC 5 FW 56 ug/LPar20SilverAquatic LifeNC 0.06 FW 4.2532 ug/LPar21ZincAquatic LifeNC 436.0284 FW 466.9070 ug/LPar22Par23Par24Fll di ti f dt t ITo appy a Model IWC %: Once the Table 1. Project Information Table 2. Parameters of ConcernFreshwater RPA - 95% Probability/95% Confidence Using Metal TranslatorsMAXIMUM DATA POINTS = 58CCHECK IF HQW OR ORW WQSCHECK TO APPLY MODELApply WS Hardness WQC04685 RPA, input12/22/2020 Electric Glass Fiber America, LLC ≥Outfall 001 NC0004685 Freshwater RPA - 95% Probability/95% Confidence Using Metal Translators Qw = 1.3 MGD MAXIMUM DATA POINTS = 58 Qw (MGD) = 1.3000 WWTP/WTP Class:III COMBINED HARDNESS (mg/L) 1Q10S (cfs) = 3.34 IWC% @ 1Q10S = 37.62838469 Acute = 117.63 mg/L 7Q10S (cfs) = 4.00 IWC% @ 7Q10S = 33.49958437 Chronic = 107.47 mg/L 7Q10W (cfs) = 7.60 IWC% @ 7Q10W = 20.95683827 30Q2 (cfs) = NO 30Q2 DATA IWC% @ 30Q2 = N/A Avg. Stream Flow, QA (cfs) = 21.00 IW%C @ QA = 8.755159678 Receiving Stream:Stream Class:C PARAMETER RECOMMENDED ACTION Chronic Applied Standard Acute n # Det. Max Pred Cw Acute (FW): 903.6 Arsenic C 150 FW(7Q10s) 340 ug/L 1 0 0.3 Chronic (FW): 447.8 C.V. (default)Max MDL = 0.1 Arsenic C 10 HH/WS(Qavg) ug/L Note: n ≤ 9 NO DETECTS Chronic (HH): 114.2 Limited data set Max MDL = 0.1 Acute: 172.74 Beryllium NC 6.5 FW(7Q10s) 65 ug/L 0 0 N/A Chronic: 19.40 Acute: 33.222 Cadmium NC 1.7742 FW(7Q10s) 12.5008 ug/L 0 0 N/A Chronic: 5.296 Acute: NO WQS Chlorides NC 230 FW(7Q10s) mg/L 0 0 N/A Chronic: 686.6 Acute: NO WQS Chlorinated Phenolic Compounds NC 1 A(30Q2) ug/L 0 0 N/A Chronic:IWC? Acute: NO WQS Total Phenolic Compounds NC 300 A(30Q2) ug/L 0 0 N/A Chronic:IWC? Acute: 8,551.0 Chromium III NC 388.6840 FW(7Q10s) 3217.5917 µg/L 0 0 N/A Chronic: 1,160.3 Acute: 42.5 Chromium VI NC 11 FW(7Q10s) 16 µg/L 0 0 N/A Chronic: 32.8 Chromium, Total NC µg/L 1 0 0.3 Note: n ≤ 9 C.V. (default) Limited data set NO DETECTS Max MDL = 0.1 Acute: 119.73 Copper NC 27.3996 FW(7Q10s) 45.0541 ug/L 19 0 0.05 Chronic: 81.79 NO DETECTS Max MDL = 0.1 Acute: 58.5 Cyanide NC 5 FW(7Q10s) 22 10 ug/L 0 0 N/A Chronic: 14.9 Acute: NO WQS Fluoride NC 1800 FW(7Q10s) ug/L 19 11 4,344.0 Chronic: 5,373.2 No value > Allowable Cw Acute: 1,113.244 Lead NC 14.7996 FW(7Q10s) 418.8957 ug/L 19 0 0.050 Chronic: 44.178 NO DETECTS Max MDL = 0.1 Acute: NO WQS Mercury NC 12 FW(7Q10s) 0.5 ng/L 0 0 N/A Chronic: 35.8 Acute: NO WQS Molybdenum NC 2000 HH(7Q10s) ug/L 0 0 N/A Chronic: 5,970.2 Acute (FW): 3,302.2 Nickel NC 127.8524 FW(7Q10s) 1242.5619 µg/L 0 0 N/A Chronic (FW): 381.7 Nickel NC 25.0000 WS(7Q10s) µg/L Chronic (WS): 74.6 Acute: 148.8 Selenium NC 5 FW(7Q10s) 56 ug/L 0 0 N/A Chronic: 14.9 Acute: 11.303 Silver NC 0.06 FW(7Q10s) 4.2532 ug/L 1 0 0.310 Note: n ≤ 9 C.V. (default)Chronic: 0.179 Limited data set NO DETECTS Max MDL = 0.1 Acute: 1,240.8 Zinc NC 436.0284 FW(7Q10s) 466.9070 ug/L 19 0 0.1 Chronic: 1,301.6 NO DETECTS Max MDL = 0.1 Acute: 00 N/A Chronic: Acute: 00 N/A Chronic: Acute: 00 N/A Chronic: Acute: 00 N/A Chronic:PQLUNITSTYPE Allowable Cw REASONABLE POTENTIAL RESULTSNC STANDARDS OR EPA CRITERIA Brushy Creek No detects No detects No detects No RP , Predicted Max ≥ 50% of Allowable Cw - apply Quarterly Monitoring No detects No detects No detects No detects No detects Max reported value = 0.05 No detects a: No monitoring required if all Total Chromium samples are < 5 µg/L or Pred. max for Total Cr is < allowable Cw for Cr VI. Page 1 of 1 04685 RPA, rpa 12/22/2020 NH3/TRC WLA Calculations Facility: Electric Glass Fiber America, LLC PermitNo. NC0004685 Prepared By: Julia Byrd Enter Design Flow (MGD):1.3 Enter s7Q10 (cfs):4 Enter w7Q10 (cfs):7.6 Total Residual Chlorine (TRC) Ammonia (Summer) Daily Maximum Limit (ug/l) Monthly Average Limit (mg NH3-N/l) s7Q10 (CFS) 4 s7Q10 (CFS) 4 DESIGN FLOW (MGD) 1.3 DESIGN FLOW (MGD) 1.3 DESIGN FLOW (CFS) 2.015 DESIGN FLOW (CFS) 2.015 STREAM STD (UG/L) 17.0 STREAM STD (MG/L) 1.0 Upstream Bkgd (ug/l) 0 Upstream Bkgd (mg/l) 0.22 IWC (%) 33.50 IWC (%) 33.50 Allowable Conc. (ug/l) 51 Allowable Conc. (mg/l) 2.5 Ammonia (Winter) Monthly Average Limit (mg NH3-N/l) Fecal Coliform w7Q10 (CFS) 7.6 Monthly Average Limit:200/100ml DESIGN FLOW (MGD) 1.3 (If DF >331; Monitor) DESIGN FLOW (CFS) 2.015 (If DF<331; Limit) STREAM STD (MG/L) 1.8 Dilution Factor (DF) 2.99 Upstream Bkgd (mg/l) 0.22 IWC (%) 20.96 Allowable Conc. (mg/l) 7.8 Total Residual Chlorine 1. Cap Daily Max limit at 28 ug/l to protect for acute toxicity Ammonia (as NH3-N) 1. If Allowable Conc > 35 mg/l, Monitor Only 2. Monthly Avg limit x 3 = Weekly Avg limit (Municipals) 3. Monthly Avg limit x 5 = Daily Max limit (Non-Munis) If the allowable ammonia concentration is > 35 mg/L, no limit shall be imposed Fecal Coliform 1. Monthly Avg limit x 2 = 400/100 ml = Weekly Avg limit (Municipals) = Daily Max limit (Non-Muni) Water Resources ENVIRONMENTAL DUALITY Memorandum .r To: NPDES Complex Unit From: Toni Belnick Date: July 20, 2016 Subject: NPDES Permitting Guidance NPDES Implementation of Ammonia Criteria- Update NC has still not adopted an ammonia standard, though it is on our WQS Triennial List for next round. NC did establish ammonia chronic criteria for use in NPDES permitting back in 1989/90, which was based on EPA's 1986 criteria development document that factored in pH/Temp across three regions of the State (see attached). This evaluation resulted in ammonia chronic criteria of 1.0 mg/1 NH3-N (summer) and 1.8 mg/1 NH3-N (winter) for use in permitting purposes. NC implements these chronic criteria as Monthly Averages limits utilizing instream dilution. In 2002, NC developed procedures for complimentary acute permit limits (discussed below). PAT MCCRORY Governor DONALD R. VAN DER VAART Sec mny S. JAY ZIMMERMAN 61-14 DlrcYor The current ammonia permitting procedures should be.as follows: • The NH3/TRC Wasteload Allocation (WLA) spreadsheet automatically calculates appropriate ammonia Monthly Average limits for summer and winter. The spreadsheet assumes a background ammonia concentration of 0.22 mg/1. • For any permit (new/renewal), always run the NH3/TRC WLA spreadsheet to verify appropriate Monthly Average Ammonia Limits for protection of aquatic life. • If the allowable ammonia concentration is greater than 35 mg/l, no limit should be imposed. • • If the allowable concentration is less than 35 mg/1, then the allowable limit is needed and the spreadsheet will automatically calculate it. • For Municipal facilities, the acute limit will be expressed as a Weekly Average, and is based on multiplying the Monthly Average limit by a factor of 3. • For non -Municipal facilities, the acute limit will be expressed as a Daily Maximum, and is based on multiplying the Monthly Average limit by a factor of 5. • If a new more stringent ammonia limit is required, discuss the need for a Compliance Schedule with senior staff and then with the Permittee. • There is no RPA procedure used for ammonia; it is implemented strictly based on WLA spreadsheet results (similar to TRC). State of North Carolina Environmental Quality Water Resources 1617 Map Service Center j Raleigh, North Carolina 27699-1617 919 707 9000 Page 12 • A sample NH3/TRC WLA is attached. In this example, the spreadsheet indicates that Monthly Average ammonia limits of 3.2 mg/1 and 12.7 mg/1 should be imposed for summer and winter, respectively, in order to protect for NC's chronic ammonia criteria. Some additional considerations: • This guidance will need to be revisited after NC formally adopts an ammonia standard for both chronic and acute aquatic life protection. • In the past, some ammonia limits were based strictly on protection of our DO standard rather than ammonia toxicity, and that is why the permit writer should always verify the correct ammonia limit with any permit renewal using the WLA spreadsheet. • In the past, some practices allowed for maintaining a less stringent ammonia limit if the facility was consistently passing the WET test (i.e., biology trumps chemistry). This is no longer a valid approach and EPA would object. In April 2016 EPA expressly stated that NC cannot use biology to override chemical results. EPA also disallowed the use of Action Levels in permitting, in which toxicity test results (if passing) were used to override the need for permit limits for copper/zinc/silver/iron/chloride.   Permit No. NC0004685  Page 1 of 4    NPDES Implementation of Instream Dissolved Metals Standards – Freshwater Standards The NC 2007-2015 Water Quality Standard (WQS) Triennial Review was approved by the NC Environmental Management Commission (EMC) on November 13, 2014. The US EPA subsequently approved the WQS revisions on April 6, 2016, with some exceptions. Therefore, metal limits in draft permits out to public notice after April 6, 2016 must be calculated to protect the new standards as approved. Table 1. NC Dissolved Metals Water Quality Standards/Aquatic Life Protection Parameter Acute FW, µg/l (Dissolved) Chronic FW, µg/l (Dissolved) Acute SW, µg/l (Dissolved) Chronic SW, µg/l (Dissolved) Arsenic 340 150 69 36 Beryllium 65 6.5 --- --- Cadmium Calculation Calculation 40 8.8 Chromium III Calculation Calculation --- --- Chromium VI 16 11 1100 50 Copper Calculation Calculation 4.8 3.1 Lead Calculation Calculation 210 8.1 Nickel Calculation Calculation 74 8.2 Silver Calculation 0.06 1.9 0.1 Zinc Calculation Calculation 90 81 Table 1 Notes: 1. FW= Freshwater, SW= Saltwater 2. Calculation = Hardness dependent standard 3. Only the aquatic life standards listed above are expressed in dissolved form. Aquatic life standards for Mercury and selenium are still expressed as Total Recoverable Metals due to bioaccumulative concerns (as are all human health standards for all metals). It is still necessary to evaluate total recoverable aquatic life and human health standards listed in 15A NCAC 2B.0200 (e.g., arsenic at 10 µg/l for human health protection; cyanide at 5 µg/L and fluoride at 1.8 mg/L for aquatic life protection). Table 2. Dissolved Freshwater Standards for Hardness-Dependent Metals The Water Effects Ratio (WER) is equal to one unless determined otherwise under 15A NCAC 02B .0211 Subparagraph (11)(d) Metal  NC Dissolved Standard, µg/l  Cadmium, Acute WER*{1.136672-[ln hardness](0.041838)} ꞏ e^{0.9151 [ln hardness]-3.1485} Cadmium, Acute Trout waters WER*{1.136672-[ln hardness](0.041838)} ꞏ e^{0.9151[ln hardness]-3.6236} Cadmium, Chronic WER*{1.101672-[ln hardness](0.041838)} ꞏ e^{0.7998[ln hardness]-4.4451} Chromium III, Acute WER*0.316 ꞏ e^{0.8190[ln hardness]+3.7256} Chromium III, Chronic WER*0.860 ∙ e^{0.8190[ln hardness]+0.6848} Copper, Acute WER*0.960 ∙ e^{0.9422[ln hardness]-1.700} Copper, Chronic WER*0.960 ∙ e^{0.8545[ln hardness]-1.702} Lead, Acute WER*{1.46203-[ln hardness](0.145712)} ∙ e^{1.273[ln hardness]-1.460} Lead, Chronic WER*{1.46203-[ln hardness](0.145712)} ∙ e^{1.273[ln hardness]-4.705} Nickel, Acute WER*0.998 ∙ e^{0.8460[ln hardness]+2.255} Nickel, Chronic WER*0.997 ∙ e^{0.8460[ln hardness]+0.0584} Silver, Acute WER*0.85 ∙ e^{1.72[ln hardness]-6.59} Silver, Chronic Not applicable Zinc, Acute WER*0.978 ∙ e^{0.8473[ln hardness]+0.884} Zinc, Chronic WER*0.986 ∙ e^{0.8473[ln hardness]+0.884}   Permit No. NC0004685  Page 2 of 4    General Information on the Reasonable Potential Analysis (RPA) The RPA process itself did not change as the result of the new metals standards. However, application of the dissolved and hardness-dependent standards requires additional consideration in order to establish the numeric standard for each metal of concern of each individual discharge. The hardness-based standards require some knowledge of the effluent and instream (upstream) hardness and so must be calculated case-by-case for each discharge. Metals limits must be expressed as ‘total recoverable’ metals in accordance with 40 CFR 122.45(c). The discharge-specific standards must be converted to the equivalent total values for use in the RPA calculations. We will generally rely on default translator values developed for each metal (more on that below), but it is also possible to consider case-specific translators developed in accordance with established methodology. RPA Permitting Guidance/WQBELs for Hardness-Dependent Metals - Freshwater The RPA is designed to predict the maximum likely effluent concentrations for each metal of concern, based on recent effluent data, and calculate the allowable effluent concentrations, based on applicable standards and the critical low-flow values for the receiving stream. If the maximum predicted value is greater than the maximum allowed value (chronic or acute), the discharge has reasonable potential to exceed the standard, which warrants a permit limit in most cases. If monitoring for a particular pollutant indicates that the pollutant is not present (i.e. consistently below detection level), then the Division may remove the monitoring requirement in the reissued permit. 1. To perform a RPA on the Freshwater hardness-dependent metals the Permit Writer compiles the following information:  Critical low flow of the receiving stream, 7Q10 (the spreadsheet automatically calculates the 1Q10 using the formula 1Q10 = 0.843 (s7Q10, cfs) 0.993  Effluent hardness and upstream hardness, site-specific data is preferred  Permitted flow  Receiving stream classification 2. In order to establish the numeric standard for each hardness-dependent metal of concern and for each individual discharge, the Permit Writer must first determine what effluent and instream (upstream) hardness values to use in the equations. The permit writer reviews DMR’s, Effluent Pollutant Scans, and Toxicity Test results for any hardness data and contacts the Permittee to see if any additional data is available for instream hardness values, upstream of the discharge. If no hardness data is available, the permit writer may choose to do an initial evaluation using a default hardness of 25 mg/L (CaCO3 or (Ca + Mg)). Minimum and maximum limits on the hardness value used for water quality calculations are 25 mg/L and 400 mg/L, respectively. If the use of a default hardness value results in a hardness-dependent metal showing reasonable potential, the permit writer contacts the Permittee and requests 5 site-specific effluent and upstream hardness samples over a period of one week. The RPA is rerun using the new data. The overall hardness value used in the water quality calculations is calculated as follows: Combined Hardness (chronic) = (Permitted Flow, cfs *Avg. Effluent Hardness, mg/L) + (s7Q10, cfs *Avg. Upstream Hardness, mg/L) (Permitted Flow, cfs + s7Q10, cfs) The Combined Hardness for acute is the same but the calculation uses the 1Q10 flow.   Permit No. NC0004685  Page 3 of 4    3. The permit writer converts the numeric standard for each metal of concern to a total recoverable metal, using the EPA Default Partition Coefficients (DPCs) or site-specific translators, if any have been developed using federally approved methodology. 4. The numeric standard for each metal of concern is divided by the default partition coefficient (or site-specific translator) to obtain a Total Recoverable Metal at ambient conditions. In some cases, where an EPA default partition coefficient translator does not exist (ie. silver), the dissolved numeric standard for each metal of concern is divided by the EPA conversion factor to obtain a Total Recoverable Metal at ambient conditions. This method presumes that the metal is dissolved to the same extent as it was during EPA’s criteria development for metals. For more information on conversion factors see the June, 1996 EPA Translator Guidance Document. 5. The RPA spreadsheet uses a mass balance equation to determine the total allowable concentration (permit limits) for each pollutant using the following equation: Ca = (s7Q10 + Qw) (Cwqs) – (s7Q10) (Cb) Qw Where: Ca = allowable effluent concentration (µg/L or mg/L)   Cwqs = NC Water Quality Standard or federal criteria (µg/L or mg/L)   Cb = background concentration: assume zero for all toxicants except NH3* (µg/L or mg/L)  Qw = permitted effluent flow (cfs, match s7Q10)   s7Q10 = summer low flow used to protect aquatic life from chronic toxicity and human health through the consumption of water, fish, and shellfish from noncarcinogens (cfs)  * Discussions are on-going with EPA on how best to address background concentrations    Flows other than s7Q10 may be incorporated as applicable:   1Q10 = used in the equation to protect aquatic life from acute toxicity   QA = used in the equation to protect human health through the consumption of water, fish, and shellfish from carcinogens   30Q2 = used in the equation to protect aesthetic quality   6. The permit writer enters the most recent 2-3 years of effluent data for each pollutant of concern. Data entered must have been taken within four and one-half years prior to the date of the permit application (40 CFR 122.21). The RPA spreadsheet estimates the 95th percentile upper EPA default partition coefficients or the “Fraction Dissolved” converts the value for dissolved metal at laboratory conditions to total recoverable metal at in-stream ambient conditions. This factor is calculated using the linear partition coefficients found in The Metals Translator: Guidance for Calculating a Total Recoverable Permit Limit from a Dissolved Criterion (EPA 823-B-96-007, June 1996) and the equation: _Cdiss__ = _______1_______________ Ctotal 1 + { [Kpo] [ss(1+a)] [10-6] } Where: ss = in-stream suspended solids concentration [mg/l], minimum of 10 mg/L used, and Kpo and a = constants that express the equilibrium relationship between dissolved and adsorbed forms of metals. A list of constants used for each hardness-dependent metal can also be found in the RPA program under a sheet labeled DPCs.  Permit No. NC0004685  Page 4 of 4  concentration of each pollutant. The Predicted Max concentrations are compared to the Total allowable concentrations to determine if a permit limit is necessary. If the predicted max exceeds the acute or chronic Total allowable concentrations, the discharge is considered to show reasonable potential to violate the water quality standard, and a permit limit (Total allowable concentration) is included in the permit in accordance with the U.S. EPA Technical Support Document for Water Quality-Based Toxics Control published in 1991. 7.When appropriate, permit writers develop facility specific compliance schedules in accordance with the EPA Headquarters Memo dated May 10, 2007 from James Hanlon to Alexis Strauss on 40 CFR 122.47 Compliance Schedule Requirements. 8.The Total Chromium NC WQS was removed and replaced with trivalent chromium and hexavalent chromium Water Quality Standards. As a cost savings measure, total chromium data results may be used as a conservative surrogate in cases where there are no analytical results based on chromium III or VI. In these cases, the projected maximum concentration (95th %) for total chromium will be compared against water quality standards for chromium III and chromium VI. 9.Effluent hardness sampling and instream hardness sampling, upstream of the discharge, are inserted into all permits with facilities monitoring for hardness-dependent metals to ensure the accuracy of the permit limits and to build a more robust hardness dataset. 10.Hardness and flow values used in the Reasonable Potential Analysis for this permit included: Parameter Value Comments (Data Source) Average Effluent Hardness (mg/L) [Total as, CaCO3 or (Ca+Mg)] 271.1 mg/L NPDES DMR files Average Upstream Hardness (mg/L) [Total as, CaCO3 or (Ca+Mg)] 25.00 Default value, no hardness data available 7Q10 summer (cfs) 4.0 NPDES Files 1Q10 (cfs) 3.34 Calculated in RPA Permitted Flow (MGD) 1.3 NPDES Files Date: ____12/16/20______________________ Permit Writer: ______Julia Byrd________________  liC ROY COOPER Governor MICHAEL S.REGAN Secretary Water Resources LLNDA CULPEPPER I:NVfP0NMEi TAL QUALITY Intejjj D1FEclor March 03, 2018 Todd Douthit, Manager Manufacturing Electric Glass Fiber America LLC 940 Washburn Switch Rd Shelby, NC 28150 Subject: Permit Renewal Application No. NC0004685 Electric Glass Fiber America LLC Cleveland County Dear Applicant: The Water Quality Permitting Section acknowledges the March 2, 2018 receipt of your permit renewal application and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting branch. Per G.S. 1506-3 your current permit does not expire until permit decision on the application is made. Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a timely manner to requests for additional information necessary to allow a complete review of the application and renewal of the permit. Information regarding the status of your renewal application can be found online using the Department of Environmental Quality's Environmental Application Tracker at: https://deq.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker If you have any additional questions about the permit, please contact the primary reviewer of the application using the links available within the Application Tracker. Sincerely, rr6../ 6).,tv-kil Wren Thedford Administrative Assistant Water Quality Permitting Section ec: WQPS Laserfiche File w/application State of North Carolina I Environmental Quality I Water Resources 1617 Mail Service Center I Raleigh,North Carolina 27699-1617 919-807-6300 GLASS FOR FUTURE rh Nippon Electric Glass Renewal of NPDES Permit NCOOO4685 Electric Glass Fiber America, LLC, Shelby, N.C. Facility February 28, 2018 GLASS FOR FUTUPE GNippon Electric Glass Via Certified Mail Return Receipt Requested February 28, 2018 Wren Thedford NC DEQ Division of Water Resources WQ Permitting Section — NPDES 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Ms. Thedford: RECEIVEDIDENRIDWR MAR 0 7 2018 Water Resources Permitting 940 Washburn Switch Rd Shelby, North Carolina 28160 USA T: 7044134-2261 )024 E: douthit@ppg.com Todd Douthit Plant Manager Electnc Glass Fibers America Nippon Electric Glass Subject: Renewal of NPDES Permit NC0004685 Electric Glass Fiber America, LLC, Shelby, N.C. Facility CEC Project 122-243.0017 MAR 0 2 2018 We are pleased to enclose an original, signed NPDES Permit Renewal Application package along with the two required photocopies. This is for Electric Glass Fiber America, LLC. (EFGA) facility in Shelby, NC. We are requesting the reissuance of NPDES Permit No. NC0004685. The primary SIC Code for facility operations is 3229 -Pressed and Blown Glass- not elsewhere classified. Approximately one percent of the waste load is from the Hanwha sheet laminate facility (SIC3083). The wastewater outfall, Outfall 001, is located at latitude 35 degrees, 20 minutes, 26 seconds, by longitude 81 degrees, 37 minutes, 0 seconds with the receiving water being BrushyCreek. There have not been any changes to the facility since the previous permit renewal. We request that all NPDES permit issues be directed to Mr. Richard Young, Focus Factory Manager. The facility Manufacturing Manager, Maintenance Manager, and Enterprise Excellence Manager are authorized to sign all reports required by the permit. As part of this permit renewal package, we have included: 1. Cover letter; 2. Introduction; 3. EPA Form 1; 4. EPA Form 2C; 5. Narrative description of the sludge management plan; and 6. Analytical data. 2 The data presented in Form 2C Section V is based on plant operating data for the period December 1, 2016 to November 2017 and special analysis conducted by Pace Analytical Services Inc. Copies of the Pace reports on the special analysis have been provided in the package (Tab G). The plant operating data is from monthly DMR submittals. We are respectfully requesting NCDEQ consider the following changes to our NPDES permit: 1. Eliminate the fluoride monitoring only requirement: The fluoride utilizing processes have been eliminated from operations at EGFA and formerly, PPG Industries Fiber Glass Products, Inc. This past year three samples were below 0.5 mg/1, with one sample at 2.2 mg/l. 2. Reduce the oil and grease testing to once per month. Oil and grease has not been detected above detection levels over the last 52 weekly samples. 3. Test for ammonia October through March only: Ammonia has only been detected during winter operations because of possible nitrification inhibition during low basin temperatures. To monitor for this possibility, we request reducing ammonia monitoring during the winter months only, specifically during October through March. 4. The current permit requires quarterly sampling for copper, lead and zinc. None of these metals has been detected over the last several years. For this reason, we respectfully request reducing the metals testing to semi-annually. 5. The EGFA wastewater treatment plant is a biological treatment plant with chemical addition as shown in the attached application. Chemical addition is commonly ancillary to biological wastewater treatment, including addition of coagulants, flocculants and pH adjustment comparable to the activities conducted at this treatment plant. For this reason, we request a change in the clarification of the treatment plant to biological 3 only, eliminating the additional PC2 classification. Please note that NCDENR rescinded the PC2 classification in 2015 for the PPG Industries Fiber Glass Products, Inc., Lexington, NC wastewater treatment plant, which is comparable to this plant. Please feel free to contact me if you need any additional information or if you have any questions regarding this submittal. Sincerely, Todd Douthit Plant Manager Electric Glass Fiber America, LLC. Attachment cc: Richard Young File Electric Glass Fiber America, LLC Shelby, North Carolina NPDES Wastewater Permit Renewal Application for Permit Number NC0004685 TABLE OF CONTENTS Introduction.......................................................... Sludge Management Plan EPAForm 1 ............................................ EPA Form 2C — pages 14 Attachments to Form 2C Sections IIA and IIB EPA Form 2C — Intake and Effluent Characteristics — Outfall 001 EPA Form 2C — Intake and Effluent Characteristics — Outfall 002 Figures TopographicalMaps................................................................ Laboratory Reports PaceAnalytical........................................................................ I Tab A Tab B Tab C Tab D Tab E Tab F Tab G INTRODUCTION Electric Glass Fiber America, LLC (EGFA) operates a Fiber Glass manufacturing facility in Shelby, North Carolina. This facility operates under the existing NPDES Wastewater Permit Number NC0004685 which expires on August 31, 2018. This permit allows the facility to discharge treated wastewater at 1.3 million gallons/day to outfall 001 and to discharge non - contact cooling water to outfall 002. In addition to EGFA's Fiber Glass Manufacturing operation, a Hanwha sheet laminate manufacturing facility is located adjacent to the EGFA site and discharges approximately 10,000 gallons per day to the EGFA Wastewater treatment plant for treatment. Wastewater from EGFA and Hanwha operations are sent to EFGA's wastewater plant for treatment and both operations are covered under the existing permit. Additional details and clarification for several items relevant to this permit application are highlighted below. 1. SIC Codes and Outfall 001 Testing The SIC code for the Hanwha (sheet laminate facility) is 3083. The Hanwha site discharges 10,000 gallons wastewater per day to the EGFA wastewater treatment plant for treatment. This discharge makes up approximately 1/I00t' of EFGA's wastewater flow. Therefore, as required for the 3083 SIC code, EGFA performed volatile compound testing on Outfall 001. Results from this testing are incorporated into Form 2C of this application. 2. Outfall (002) Testing Outfall 002, the primary stotmwater outfall, is currently permitted for the discharge of non -contact cooling water. Therefore, EGFA conducted the testing as set forth in Form 2C. This testing also included the required volatile compounds for SIC codes 3083. 3. Wet Weather Only Outfalls Outfalls 003, 004, 005, 006, 007 and 008 are covered under the General Stormwater Permit #NCG070000, Certificate of Coverage #NCG070015. These outfalls are wet weather outfalls only and would contain little, if any, drainage from industrial areas. For this renewal, testing was not conducted on these wet -weather outfalls. 4. Sample Reporting and Averaging Sample reporting and averaging was provided in Form 2C as per NCDEQ DWQ's Directions for Completing Monthly Monitoring Reports " dated March, 2014. These instructions provide guidelines with respect to rules for reporting and averaging less than detectable "<" values. (i.g., a sample result with a value of less than the detectable limit is considered to equal "zero" when calculating monthly and long-term arithmetic averages). Also per NC DEQ DMR reporting guidelines, fecal coliform monthly and long -tern averages were calculated using a geometric mean. 5. Signature Authority There will be no change requested in signature authority for monthly monitoring report requirements. Signature authority for monthly reports as a "Duly Authorized Representative" per 15A NCAC 2B.0506(b)(2)(D), will remain unchanged and is delegated to the people holding the titles of Manufacturing Manager, Maintenance Manager and Enterprise Excellence Manager. SLUDGE MANAGEMENT PLAN The wastewater treatment plant (W WTP) sludge generated by the Shelby facility is a mixture of both primary and secondary sludges. The primary sludge is the result of clarification using lime, aluminum chloride, polymers and coagulants to achieve floc formation and settling. The secondary sludge is waste activated sludge from the biological treatment system. The secondary sludge also contains bentonite clay and a small amount of ferric chloride. Both sludges are combined in a sludge thickener/storage tank prior to dewatering. Polymer addition and mechanical mixing, along with dilution water, are required to prepare the sludge for the belt press. The sludge is then pumped to the belt press for dewatering. The belt press has both a gravity drain section and a pressure section where the water is removed. Typically, the solids are increased from 4-5% as it leaves the storage tank, to 25-30% solids as discharged from the belt press. The dewatered sludge is transported via screw conveyors to a roll -off box. The water is routed back to the head of the W WTP. Before the roll -off box is picked up for disposal, a paint filter test is conducted on the sludge to ensure that free liquids are not present. The dewatered sludge is then taken to a permitted, lined landfill for disposal. TAB A EPA FORM 1 Please print or type in the unshaded areas L11 -in areas ares aced for ei8e type i. e_ FORM N=EPA GENERAL LABEL ITEMS I. EPA I.D. NUMBER III. FACILITY NAME acteynch). For Approved. OMB No. 2040-0086. Approval expires 5-31-92 U.S. ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER GENERAL INFORMATION F 110000349070 T)" o Consolidated Permits Program ad the "General Instructions" before starting.) I ' 1 2 13 1+4 15 V. FACILITY PLEASE PLACE LABEL IN THIS SPACE MAILING LIST VI. FACILITY LOCATION questions, you must submit this form and the supplemental from listed in the the supplemental form is attached. If you answer "no" to each question, you excluded from Dermit reouirements: see Section C of the instructions. See at produced water other quos which arc bmugn[ ro the surface in connection wnh conventional oil ornatural MARK "X" SPECIFIC QUESTIONS res No FORMATTACHED A. Is Nis facility a publicly owned treatment works which results in a discharge to waters of the U.S.? (FORM 2A) fluids for storage of liquid hydrocereons? ATTACHED Does or wi Iia aciity (either axis ng or 16 17 18 C. Is this facility which currently results in discharges to water of the U.S. other than those described in A or B above FORM 2C 22 23 24 E. Does or will this facility treat, store, or dispose of the instmctions and which will potentially emittootons hazardous wastes? (FORM 3) produced water other quos which arc bmugn[ ro the surface in connection wnh conventional oil ornatural MARK "X" gas production, inject fluids used for containing, within one quarter mile of the well enhanced recovery of oil or natural gas, or inject YES fluids for storage of liquid hydrocereons? ATTACHED Does or wi Iia aciity (either axis ng or FORM4 31 1 32 1 sthis faci iy a proposed ataUonary sourcewhich L35 is one of the 28 indusmal categories listedin feeding operation or aquatic animal special processes such as mining of suiler by the the instmctions and which will potentially emittootons production facility which results in a discharge per year of any air pollutant regulated M under the Clean Air Act and may affect or belocated t9 20 in an attainmentrea? FORM5 s this propose aci iy (of er man those descnbed NAME OF FACILITY SKIP I Electric Glass Fiber America, LLC. Young, Richard, Focus Factory Manager the I anyareathe nlhesis following the question. Mark "X" in the box in the third column if I not submit any of these forms. You may answer 'no" if your activity is action D of the instructions for definitions of bold-faced terms. uo you or will you inject at this maiay'no usmal or municipal effluent below the lowermost stratum MARK "X" SPECIFIC QUESTIONS containing, within one quarter mile of the well FORMYESINOIATTACHED Does or wi Iia aciity (either axis ng or FORM 4) 31 1 32 1 proposed) include a concentrated animal feeding operation or aquatic animal special processes such as mining of suiler by the production facility which results in a discharge Frasch process, solution mining of minerals, in M to waters of the U.S.? (FORM 2B) t9 20 2t s this propose aci iy (of er man those descnbed in A or B above) which will result in a discharge 37 38 uo you or will you inject at this maiay'no usmal or municipal effluent below the lowermost stratum containing, within one quarter mile of the well bore, underground sources of drinking water.) FORM 4) 31 1 32 1 33 Do you or will you inject at this facility fluids for special processes such as mining of suiler by the Frasch process, solution mining of minerals, in M situ combustion of fossil fuel, or recovery of geothermal energy? (FORM 4) 37 38 39 Is this facility a proposed stationary source which is NOT one of the 28 industrial categories Mlistedintheinstructionsandwhichwillpotentially emit 250 tons per year of any air pollutant reoulated under the Clean Air Act and may affect 1940 Washburn Switch Road I Shelby 940 Washburn Cleveland 6`[a] l!I-I i9 C. CITY OR TOWN D. STATE E. ZIP CODE F. COUNTY CODE Shelbv NC 28150 EPA FORM 3510.1 (&90) CONTINUED ON REVERSE CONTINUED FROM THE FRONT VII BIOLOGICAL TOXICITY TESTING DATA v,,,.,e.a,.. ti -nam to behave that env biolooical test for scute or chronic twdedy has been made on any of your discharges or on a receiving water in relation to your discharge within dM last 3 years? V111) YES (Idrnnfr rAr tnK+) onihir.mbr d.1,l r7vxa Arlon) NO (go ro .14,11. Chronic toxicity testing (Ceriodaphnia) is conducted quarterly per NPOES permit requirements. VIII. CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Rem V pedormed by a contract laboratory or consulting fmn7 YES (list the name. add.. anal "deplane rasher of an i f-11"mnts araly_ed hy. NO (ko ra Sailon Al rack such lahoraory orfin a helox) C. D. POLLUTANTSANALYZED A. NAME B. ADDRESS area code hno.) i Pace Analytical Services, Inc. 9800 Xineey Avenue, Suite 100 704) 875-9092 All except PB, EPA Lab Code: NC00014) WW Cert. Huntersville, NC 28078 temperature,lov level chlorine, conductivity, WET No. 12 and (MBAs a CTAS) BNCO Laboratories, Inc. WW Cert. 102 Woodwinds Industrial Ct. Ste. A 919) 467-3090 No. 591 Cary, NC 27511 Research and Analytical 106 Start St. 336) 996-2841 Toxicity, Surfactants (NEW Laboratories, Inc. WE Cert. No. PO Box 473 a CTAS) 34, Biological Cart. No. 14 Kernaraville, NC 27284 IX. CERTIFICATION 1 cathfl, under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the infonnedon submitted Based on my inquiry of the person or persons who manage the system or those persons directy, responsible for gathering the information. da information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there ere significant penalties ler sub"Ifing Wise information, including the possibility of fine and imprisonment forknowing violabona. A. NAME 6 OFFICIAL TITLE (01. or praQ B. PHONE NO. ro d, @ no.) 7 C.A ou A.T lanr an. er- arca 7o (- 4.34-2.? C. SIGNATURE D. DATE SIGNED EPA Form 3570-2C (8-00) PAGE 4 of 4 TAB B EPA FORM 2C PAGES 1-4 EPA I.D. NUMBER (cap,)m. /rem l rjFann 1) Form Approved. 110000349070 OMB No. 2040-0086. Please Drint or Noe in the unshaded areas only. I Approval expires 3-31-98. FORM 2C NPDES U.S. ENVIRONMENTAL PROTECTION AGENCY APPLICATION FOR PERMIT TO DISCHARGE WASTEWATEREPAEXISTINGMANUFACTURING, COMMERCIAL, MINING AND SILVICULTURE OPERATIONS Consokdeted Pearl Program I. OUTFALL LOCATION For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. A. OUTFALL NUMBER B. LATITUDE C. LONGITUDE fur) 1. DEG. 2. MIN. 3. SEC. 1. DEG, 2. MIN. 3. SEC. D. RECEIVING WATER (name) 001 35 20 26 81 37 0 Brushy Creek 002 35 19 23 81 38 12 Unnamed Tributary to Beaverdam Creek 003 35 19 36 81 38 7 Unnamed Tributary to Beaverdam Creek 004 35 19 48 81 37 44 Unnamed Tributary to Beaverdam Creek 005 35 19 42 81 37 38 Unnamed Tributary to Beaverdam Creek IL FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations, treatment units. and outfalls. If a water balance cannot be determined (e. g., for certain mining activities), provide a pictonal description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water mrlotf; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if necessary. 1. OUT- 2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT FALLNO. (h I) b. AVERAGE FLOW b. UST CODES FROM a. OPERATION (list) (include units) a. DESCRIPTION TABLE 2C-1 001 see Attachment 2CII.e. Outfall 001 002 Non -contact Cooling eater 115.000 GPD None underground spring eater 35,000 GPO None Stormiater - Peak Plov. i-1hr 74.9 CFS None 003 Stormvater - Peak Plow i -/hr 13.9 CPS None 004 stormvater - Peak Ploy 1'/hr 2.3 CFS Ponx 005 9toonwater - Peak Flow 1"/ht 1.3 CPS Continued on Nexc Page... OFFICIAL USE ONLY (e/flnenl ¢uuideGnes slrheoregoner) EPA Form 3510.2C (8.90) PAGE 1 of 4 CONTINUE ON REVERSE EPA I.D. NUMBER (copyfrom lnnr l JPan„ 1) Form Approved. 110000349070 OMB No. 2040-0086. Please print or type in the unshaded areas only. I I Approval expires 3-31-98. FORM 2C NPDES U.S. ENVIRONMENTAL PROTECTION AGENCY APPLIFOR PERMIT TO DISCHARGE WASTEWATER CEPA EXISTING MANUF CTURING,4COMMERCIAL, MINING AND SILVICULTURE OPERATIONS Consolidated Permits Program I. OUTFALL LOCATION For each outfall, list the latitude and longitude of Its locaflon to the nearest 15 seconds and the name of the receiving water. A. OUTFALL NUMBER B. LATITUDE C. LONGITUDE l-) 1. DEG. 2. MIN. 3. SEC. 1. DEG. 2. MIN. 3. SEC. I D. RECEIVING WATER (.a,,) 006 35 19 23 81 37 18 Unnamed Tributary to Beaverdam Creek 007 35 19 25 81 37 29 Unnamed Tributary to Beaverdam Creek 008 35 19 24 81 37 48 Unnamed Tributary to Beaverdam Creek II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water. operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more debuted descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations, treatment units, and oudalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of. (1) All operations contributing wastewater to the effluent, including process wastewater. sanitary wastewater, cooling water, and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets K necessary. 1. OUT- 2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT FALLNO. (Gori) b. AVERAGE FLOW b. LIST CODES FROM a. OPERATION (list) (melude umrs) a. DESCRIPTION TABLE 2C-1 006 stoxmwacer - Peak Plow 1" Er 2,a CFS Nene 007 stormvater - Peak Plov 1^/Er 12.2 CPS None OOB 9torewater - Peak Flow 1^/hr 12.9 CFS None OFFICIAL USE ONLY (e{puen, gurd h.,,r sub-cmrgones) EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE CONTINUED FROM THE FRONT C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal? YES (¢ampler, rhe /ollowmg table) m NO (go w Semon lll) 3. FREQUENCY 4. FLOW a. DAYS PERWEEK Irwfeawmgr) b. MONTHS PER YEAR1. avr''h"r"ergr) a. FLOW RATE (,n mgd) B. TOTAL VOLUME Ir( -A 1. 11h note) 1. OUTFALLNUMBER (141) 2. OPERATION(s) CONTRIBUTING FLOW ImJ LONG TERMAVERAGE 2. MAXIMUMDAILY 1. LONG TERMAVERAGE 2. MAXIMUMDAILY G DURATION in Jmx) III. PRODUCTION A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility? YES (comp/ere Ire. 111-13) ® NO W, m Sorunn AV) B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure ofoperaXon)? YES (complete ire. 1110 ® NO (lw m Srauon 11) C. If you answered 'yes' to Item III -B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the applicable effluent guideline, and indicate the affected outfalls. 1. AVERAGE DAILY PRODUCTION 2. AFFECTED OUTFALLS G.rr anyali rmmberr) a. QUANTITY PER DAY b. UNITS OF MEASURE e. OPERATION, PRODUCT, MATERIAL. ETC. AP -h') IV. IMPROVEMENTS A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater treatment equipment or practices or any other environmental programs which may effect the discharges described in this application? This includes, but is not limited to, permit conditions. administrative or enforcement orders, enforcement compliance schedule letters, stipulations. court orders, and grant or loan conditions. YES (complete the (ollowmg roble) NO (go ro Gem 11'-B) 1. IDENTIFICATION OF CONDITION, AGREEMENT, ETC. 2. AFFECTED OUTFALLS 3. BRIEF DESCRIPTION OF PROJECT 4. FINAL COMPLIANCE DATE a NO. D. SOURCE OF DISCHARGE a REQUIRED b. PROJECTED B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for construction. MARK W IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED EPA Form 3510-2C (8.90) PAGE 2 of 4 CONTINUE ON PAGE 3 EPA Fofm 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE CONTINUED FROM THE FRONT VII. BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reeaon to believe that any biological Lest for acute or chronic toxloity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? YES (,dery Jwhe rare) ore/ drsmbe rhea purpurer hrlow) NO (Su lir S'ern. Vlll) Chronic toxicity testing (Ceriodaphnia) is conducted quarterly per NPDES permit requirements. VIII. CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? YES(her the name. ddm.. anal Weplrone.,.ber o%am/palhaanh onoly-edhy. NO (g. to S'ation/d) each ,h lahumrury orinn hdl ) C. TELEPHONE D. POLLUTANTS ANALYZED A. NAME ADDRESS ore. axle Ann.) fist) Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 704) 1175-9092 All except pH, temlerature.low levelSPALabCode: NC00014) ww Cert. Hunteraville, NC 28078 chlorine, conductivity, war No. 12 and (tABAB a CTAS) ENCO Laboratories, Inc. wN Cert. 102 woodwinds Industrial Ct. Ste. A 919) 467-3090 No. 591 Cary, NC 27511 Research and Analytical 106 Short St. 1336) 996-2841 Toxicity, Surfactants IFAS Laboratories, Inc. ww Cert. No. PO Box 473 a CTAS) 34, Biological Cert. No. 19 rnezaville, NC 27284 IX. CERTIFICATION 1 cedify under penally of low that this document and all attachments vers prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the inhumation submitted. Based on my inquiry of the person or persons who manage Me system or Mose persons directly responsible for gathering the information, the Information subrra(fed is, to the best of my knowledge and belief, We, accurate, and complete. I am aware that them are significant penalties for submitting false information. inducting the possibility of fine and imprisonment Mr knowing violations. A. NAME a OFFICIAL TITLE (npe uryrrer) B. PHONE NO. (ams cods Ano) odd J'.4.1 Plant /'law. er" Ios4 t 34F-z2G C. SIGNATURE C1AT UR1/+/^/'Illi, - [ D. DATE SIGNED z - ZS- ( 8 EPA Forth 351 D -2C (8-90) PAGE 4 of 4 TAB C ATTACHMENTS TO FORM 2C SECTIONS IIA AND IIB EPA FORM 2C SECTION ILA OUTFALL 001 SCHEMATIC Electric Glass Fiber America, I.I.C. City Water Supply 1,500,000 gpd Research Misc. Sanitary Boiler Misc Process Filtration Forming 1,000 gpd 3,000 60,000 43,000 Water 15,000 850,000 Bpd Bpd gpd 75.000 gpd gpd gpd poration Stormwater Garage/ PadsL—C33 185,000 gpd) W WTP 000BPd 1" rainfall See W WTP Schematic) Product 1,300 gpd HANWA SIC CODE 83083 10,000 gpd Sludge OUTFALL DewateringP MGD 33,250 gpd up [0 1.3 MGD EPA FORM 2C SECTION ILA OUTFALL 002 SCHEMATIC Electric Glass Fiber America, LLC. City Water Supply Stormwater 98.6 acres Non -Contact peak flow = Cooling up to 74.9 cfs 115,000 gpd Underground Spring est. 35,000 gpd Outfall 002 Up to 150,000 gpd stormwater Notes: Outfall #002 is the primary stormwater outfall for the Industrial portions of the property. Cooling water discharges from the outfall are permitted under #NC0004685. Stormwater Discharges are covered under the General Stormwater Discharge Permit #NC070000, COC #NCG070015 Stormwater Peak Flows were calculated using the Rational Method (Q = CIA) where: Q = peak flow (cfs) C = Runoff Coefficient (where: 0.9 = Impermeable, 0.8 = Graveled, 0.3 = Grassed, 0.1 = Wooded) I = Intensity A = Area (acres) Note: The above peak flow for stormwater was calculated using an intensity of 1"/hr. The runoff coefficient (C) used was 0.76 based on the following estimate: 80% Industrial, (0.9). 10% wooded (0.1) EPA FORM 2C SECTION ILA OUTFALL 003, 004, 005, 006, 007 & 008 SCHEMATIC Electric Glass Fiber America, LLC. Stormwater Stormwater Stormwater Stormwater Stormwater Stormwater 30.8 acres 3.1 acres 2.7 acres 9.0 acres 33.8 acres 2.6 acres Outfall Outfall Outfall Outfall Outfall Outfall 003 #004 #005 #006 #007 #008 Peak Flow Peak Flow Peak Flow Peak Flow Peak Flow Peak Flow 12.9 cfs 2.3 cfs 1.3 cfs 2.8 cfs 12.2 cfs 0.9 cfs Discharges from Outfalls #003, #004, #005, #006, #007 & #008 are covered under the General Stormwater Discharge Permit #NC070000, COC #: NCG070015. These areas contain limited drainage from industrial areas of the property. Outfall 002 is the primary stormwater discharge point of the Industrial portions of the property. Peak Flows were calculated using the Rational Method (Q = CIA) where: Q = peak flow (cfs) C = Runoff Coefficient (where: 0.9 = Impermeable, 0.8 = Graveled, 0.3 = Grassed, 0.1= Wooded) I = Intensity A = Area (acres) Note: The above peak flows were calculated using an intensity of 1"/hr. See below for runoff coefficient calculations. RUNOFF COEFFICIENT CALCULATIONS OUTFALL C 003 0.42 20% Industrial (.9), 80% grassed (.3) 004 0.75 90% paved parking lot (.9) and 10% grassed (.3) 005 0.48 30% paved parking lot (.9) and 70% grassed (.3) 006 0.31 95% lawn (.3), 2.5% wooded (.1), 2.5% graveled (.8) 007 0.36 10% Industrial (.9) and 90% grassed (.3) 008 0.36 10% Industrial (.9) and 90% grassed (.3) EPA FORM 2C SECTION 11.11 W WTP Treatment / OUTFALL 001 SCHEMATIC Electric Glass Fiber America, I.I.C. NPDES Permit NCOOD4685 Renewal Application Process Water — (0.8 MGD) Eary—(0.06 MGD) Screenater—(0.12 MGD) IT HANWA—(0018MGD) OUTFALL 0001 14 1 Flocculation yA Grinding IComminutors 1-0I -T xreenin 1-U S .nrerl.non tsenlln I Recycle / I 2{ Coding water 1-0 al 3A SLUDGE PROCESS SCHEMATIC a.s Gravely Thickener 3{ Bann 5-L MWO.113-L5-Q Polymer Belt Press 5-E.1-0.5{ Dilution Water Wast.H.W Sludge. WVTPa-C .neB113-0 Grmcmg Flow toad Flash Mla Primary li equalisation Equalization Tank CliinfZ 1-O 2-D 1-0, Ili, 2l 1-U time AICI Anionic Polymer Slue to Cationic Coaeulan[ Thickener Secondary Clarifiers (3) 2-C, 1-U 1-V Anionic Polymer Sludge to Thickener Aeration Tanks(!) 2-U Lime H1P0. Defoamer RAS to Alratl0h Bentonite Clay Treatment Codes Used From Table 2C-1 14 1 Flocculation 1-L Grinding IComminutors 1-0 Mi,ine I -T xreenin 1-U S .nrerl.non tsenlln I 1-V Ane Rltneon 2{ chem'.] P,.clphat.. 1-0 ulat'on 3A Ao...d Slud e a.s 3{ BannMWO.113-L5-Q TAB D EPA FORM 2C INTAKE AND EFFLUENT CHARACTERISTICS OUTFALL 001 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. Youmry report wma or M Mtlas Yrlormaborr EPA I.D. NUMBER (r., tn. Rem 1w Farm I) n separate Mots (use fame •ama Rama" kal M Cwnpe lllp that papas. 110000349070 SEE INSTRUCTIONS. EPA Form 3510.2C (690) PAGE V-1 CONTINUE ON REVERSE ou FUL No. V. INTAKE AND EFFLUENT CHMUCTERISTICS (mMnuadlpn pope S a Fpm 2{J PART A -You mule poNde the revels of le Meet ave anaNMs W every POYand In Ws IaMe, C.4,14%. MDIs IYr each MIM, Sea W Wglon9 br 9WNbrW MM W. 8. UNITS 4. INTAKE 2. EFFLUENT r r/Dark) n rana9 to. MAXIMUM W MY VALUE c. LONG TERM AVRG. VALUE a. LONG TERM a MAXIMUM DAILY VALUE p/mrulaSle) P/mnilaelr) AVERAGE VALUE If NO. OF a. OONCEM D. NO. OF INiRAl10N1. POLLUTANT CONCE 121 MAIM CONCENTIUTON 121 W35 111 CONCEMRATCN 121 MISS ANALYSES TgATION D.MA86CpNCFNt{RAnca, 12)tM99 ANKYSEG BMFMmlcal OXYpw 7.2 31.2 2.33 9.95 1.71 7.22 52 mg/L lbs Demand (81111) to ChemlWOgym 25 0 1 h /L lbs Demand (I c Total Oman. C. 4.5 24.4 N/A N/A N/A N/A 1 mg/L lbs Dent ) TotalSoad. IDSDeoded 4.0 21.7 1.0 i 52 mg/L lbs c. Arn.la(iuM c0.1 0 52 Tg/L lbs VALUE VALUE VALUE VALUE L Fax 0.65 0.57 0.50 365 MGD 9. Temperleure VALUE VALUE VALUE VALUE p.rmw) 25 23.3 19.6 258 c In. TemPoroture VALUE VALUE VALUE VALUE rnm•v.) 28 27.5 24.1 258 C MINIMUM NUM MINIMUM MAAMUM rPH 6.2 4 258 STANDARD UNITS PARTB- MaM'X'tncobmn24MrtRhpM Youknowor Mvemesonto DMew Iapms Ma 'X'nwlumn2.EWawhpq MyoubWieve IoeaeawM.BpumaMWumn2aMranyp aMR iUMfimdedeew detwN. or inor" but exannall In an emMM MrstMms pWaYra, you mule praiw Na Marls of N bast oM anaMlsW Me Poluleni Fp other polulaMa M anaw You mark colo m 2s, you must anoM9a Uan4MM 4N p N e rytipl dlMa porlearral n alcr thicintep, CoMpeta oM MDM M Ycl1 MMa1. Gee the nstnIobons for notational Meals aM nalmaMt. 2. MARK -X' 3. EFFLUENT 4. UNITS 5. IN (, -W)) L POLLUTANT D. MAXIMUM M DAY VALUE c LONG TERM AVRG. VALUE a. LONG TERM AVERAGE AND a b a. MAXIMUM DAILY VALUE (rl m uluM1lrJ (rlmrnlnnlo) VALUE CAB NO. O. W. OF a CONCENY II) b. NO. OFffi.E ED OFU'V O 1y M IleN-4dk) PRESENT AHSEM C XT'aonI (21.6 COrICENTRATON 121MV9 CONCEN ,,A 121M0.49 ANALYSES TRATION b.MAIS CpNCEMMiIIXi IIIMA59 AIULYBEB a womdo2495"7-9) x E. ClAonne Toad xRandUN Calor X d.F«N Caklmm 20.0 3.38 1.96 52 M/100 mlX 04994tH) 2.2 11.9 2.2 10.5 0.85 3.5 4 mg/L lbs L NtrnwNmM X 17.4 94.3 17.4 82.7 14.63 61.0 4 mg/L I lbsP• M EPA Form 3510.2C (690) PAGE V-1 CONTINUE ON REVERSE ITEM V -B CONTINUED FROM FRONT EPA Fa m 0515W (690) PAGE V-2 CONTINUE ON PAGE V-3 2, MARK W 3. EFFLUENT 4, UNITS 5. INTAKE ( mall 1. POLLUTANT b. MAXIMUM 50OAY VALUE c. LONG TERM AVRG. VALUE E. LONG TERM AND b a. MAXIMUM DAILY VALUE 4f—fik/r) ilmwluAlol AVERAGE VALUE CAS NO, BEUEVED BEUEVEO III 4. NO. OF E. CONCE III b. NO. OF GI III l/mnilunl•1 VRESENL 4BSEN! CONCENTPAI RIk4bB CONC ,AnON 121 MARS CONUNTRAIIDN 121 MAW AWILYSES TR E. MASE CATIONENTWITION (21MA99 ANALYSES WTOW 0,'.0,'.(u. 1) b'apa"n 5 52 mg/L lbso.Z.X L P"o.pnome Ma Pl, T./X\ 3.6 19.5 3.6 7.1 1.32 5.5 4 mg/L lbs 222}1401 1. Radosc 1)PWM1a. To1W X 2) Beta. Telal X Ta1N HI Ra4wm )2S. TOW SU MY u•.ar 32.1 174.0 1 mg/L lb. 1H06TSd1SJAE v m 1) n. SUIMa v 1AMsiSJ) I. . Sunaclanb X u0.4 O 1 mg/L lbs a. AN— TOW X X0.1 0 1 mg/L b. 0A2&965) p. Baum0 . T"W2N -2i2) X 7 24) X 0.36' 1.9 1 mg/L lbs r. C.w Tei 7""") x X 05 o 1 mg/L lb. 43"M) I. M.'.0 . Tow X 2.]B 12.9 1 mg/L The 74310,9") u. Mo114Meum, Total X74WW7) v Manpan — T..l X743T. Taal V«aysl x/ TiUm.. TOW XH324) EPA Fa m 0515W (690) PAGE V-2 CONTINUE ON PAGE V-3 EPA FOm 351620 (600) PAGE V-3 CONTINUE ON REVERSE EPA I.D. NUMBERI 1— Ixw 1,0— — I) OUTFALL NUMBER 130000349070 001 CONTINUED FROM PAGE 3 OF FORM 2-C PART C - B you aro • primary eMumM 0M Ws ou11Y caMYM promas ymmtvM ar. most to Table 202 in nM Immruch na to Memnle which of Me GCIMS harlcns you Mum Ier for Me* X- In column 2+ for Y such GCrWS f... Inal apply to your neumry ant for A.l logo me1W. ayame.s. W halal pMnob. B your are rid I Wre4 to mark column 2-a (aemWvy whir mrs nWpowss wuMw Vat oullYk. a+0 mnapuia0 GUMS a lou). me* 'X' in column 240 for each ptlla6tl you know or Im. ruwn t0 bIIMW Is owes nl. Mah'X' In COWmn 24 for /NN pollution you ONls" Is abs/n1. M you Want column 2a M " pdYXam, you mug prouf4alhe mMs Of at Mug A. m IFw m that poWlala. B you mark column Tb for any polulamyou must prou4e the mWhs of at ben one analysis for that po1Mn0 M you kn.w or haw rump to N"n 0 MI M discharged In co sommea lam of 10 ppb or pnatx. B you mi Column 21, for aGoMn. acryon tri La binllrophand, or 2-mMh*4. B Mnt rophanol, you mum prowft the stab of M Mar OM mMy ns for each of them pokilem. WhKh you halon a hew me. 1. Nam. MM you OiaCMrya M CpKemm.ne.1100 opo or greater. 01Mm10e, W polN/ma for Which you mark column 2b, you mum either submit r Mar an Nei or brieRy, 0eacme this MOWS the poeueu is ingsi 10 W 4iWhargeo, We Met Mime ant 2 pees to Ibis pm. plea4 1aMaW each camugy, CompMa .m takes (as ) Fear) M each ouCY, Sea iMMC1Mm for a40MoM MOM and mememenb. 2 YARN'X' 3. EFFLUENT 4, UNITS 5. INTAKE (aryi Ml 1. POLLUTPNT p. MAVMl1N b DAY VALUE c. LONG TERM AVRG. a. LONG TERM ANO n. a a. MAXIMUM DNLY VMUE p/mru,Ae) VALUE(a—d.AW) AVERAGE VALUE CASNNMBER TESnNG BFIIEVEO BEpE'E. IL NO. OF aLONCEN- arlyIllIp11 Of—for") gEOVIRED Pg. T ABSENT LONLENIIUnW 121 MP64 CONCENTMTON 12I AUS$ CONLENigAl10N I$I MP 33 ANALYSES TRATION b. MASS LgyLENTRAWN 121NP33 NIOLYSF YSE METALS, CYANIDE, AND TOTAL PHENOLS I M. MMnmy, Tobi x(]eW26U) 2WAr•arm, Tpbl X c0.01 0 1 mg/L lb. pee0.J62) 3M. BwyWm, TWA x(]4641-T) 4M_Ca mu JoW xIT191 SWImT440-42-3 X c.05 0 l mg/L lbs 0 IM.Cappw, TOW x c0. 005 0 4 mg/L lbs 74654a) X <0.005 0 4 mg/L lbsQM4C9-931) 1 BM. M.—q TOW XOU497-g 9M. Nickel, TOW Xn4WA2n1 I OM. Smamum, XTOWIn32O3-2) IM, ShI1ect.22 X c0.005 0 1 mg/L lbse) )TOM 12M. Thallom. TWA (7440-2M) X 13M, Zinc. Tonal Tee6 ) X 14M, CyaWOe, TOM (57.12-5) X TarDIOXIN 2.)754.m-/ DESCRIBE RESULTS chbmWMn xOenn11940(t -01 EPA FOm 351620 (600) PAGE V-3 CONTINUE ON REVERSE EPA Form 061&2C (&so) PAGE VJ CONTINUE ON PAGE V-5 L MARN'N' S. EFFLUENT UNITS 6. WTARE (,,-A 1. POLLUT,WT p. YNOYUY 50 WY VALUE c. LONG TERM AVRG, a LONG TERM AND e. c p. YAEIMUM DAILY VALUE r/mrulr2lel VALUE 41m .....b q AVENGE VALUE GAS NUMBER tEaiING 19FilEVED I)EUEVEO p. NO. OF aCONCEW Itl NO OF Itl Itl Itl R/nTr/rnrnlW(r) PEOUMED PPESENi IBSEM CONCENiMnm III. cO 121. CONCENTRATION 121 MRaa ANALY$EB TRATION p.MA55 CCNCEMMiNIN 121 MA55 YSE GC MS FRACTION- VOLATILE COMPOUNDS IV.xm X 005 0 1 1Pg/L lbs 01L221 ZV. M1e X 0 11g/L lbs pox --11p') 05 71412) e X 0 1 mg/L lbs002 lnilow- V M& X U2M 1) N2d&II SV. &omobm X c.002 0 1 mg/L lbs7}2&2) eV. CemwTerveUlro00e X x.002 0 1 mg/L lb. eruenexc.002 0 1 mg/L lbs W(7M 3); ene X002 0 1 m3/L lbs enww xc,002 0 1 mg/L lbs w. 2CNwunyNinylEner X 005 0 1 Pg/L lbs M") IVC( .r / x 002 0 1 mg/L lbs6xd&]) tN. O"<Nwa p,omemen.ne X c. 002 0 1 mg/L lbs 7&Ix l I IV.OvlAero- tiluwomeuene X 002 0 1 Irg/L lbs Ix&2t-0 14v. 1. X 002 0 1 11g/L lbs 117=3) Isv. 1.2-O ,N X c.002 0 1 mg/L lbs em.o (0)-06-x1 Iw.tYOCNoro- X c.002 0 1 11g/L lbs enslwN OS]Se) IN. LDI?eNwo- x c.002 0 1 I1g/L lbs FreP.napuxal IeV., }ptlYoro- prp ne X c.002 0 1 mg/L lbs Isea>sil Iw. Enseeniem Vx c, 002 0 1 mg/L The tl00M1-el 2w. MenM X 002 0 1 mg/L lba 9romlEe (4(191 xtV. M. 002 0 1 mg/L 169 CRMee (7"7.3) EPA Form 061&2C (&so) PAGE VJ CONTINUE ON PAGE V-5 EPA Fwm 35162C (690) PAGE V-5 CONTINUE ON REVERSE 2 MARK'%' 3. EFFLUENT A. UNITS 5. INTAKE ( 1wn,0 1. POLLUTANT N W IDAp. MAXIMUM b MY VALUE p. LONG TERN AVRG. Anse) A LONG TEPM AND p c MAXIMUM DAILY VALUE O VALUE TERM AVENGE VALUE GAS NUMBED iEstlnG BELIEVED O. NO. OF e. CONGER III p. NO.OfBELIEVEDP) III DI r/rnvrlurtle) REWMED MEWND rBSEM CCNCEMMIIOx 13)NI CONCENTMTICN 121M.9S C.4')RA11ON AS ANALYSES TPATION p. MASS CONCENTRATRIR 131MA55 YSE GCNS FRACTION- VOLATILE COMPOUNDS Kwmw,..p 2N. M."In./ x 002 0 mg/L lbs Cw.(75aa2) 3]V. 1.1.3 L T.tr.vNo wm.n. X 002 0 1 mg/L lbs 0.34524V. T.p.dA.. c.002 0 1 mg/L lbs Mllene(t2i-1H) 25V. TuA—/ x 002 0 1 mg/L lbs 000.90.3) 28V. laTrem- umMrwmA.ne X 002 0 1 ng/L lbs 156da52N, IJ 1 -TA X 002 0 1 mg/L lbs mem (7tasal 2ev.t ,3-Trwewo V 002 0 1 mg/L lbs 39v inWwo- c.002 0 1 mg/L lbs empme psora) pv. Tnrlba W— .m.n.X 002 0 1 mg/L lbs S" nV'wnA CNI V 002 0 1 mg/L lb. 75010 3CIM5 FRACTION -ACID COMPOUNDS IA. 2LMmopMnd x( 9S53a) IA1.6pWwo- xppwwl (1200.0.21 e9ry4 X0- ppenN O05-07-9) 000 sA. souvveo- xCre.a lsNa2-t) 5A2.-pMb xOw51.10.5) 9A 2—W," W7] 5) A 4Npop . 1100-92- ) SA. Pcnlwow xC'..,, (511-W) 9A. P.nla XMen.l (eland) pAPn M tloa9sx) 11A 2. aTrh:JN o- xAh.d(eapen) EPA Fwm 35162C (690) PAGE V-5 CONTINUE ON REVERSE EPA F01m 351120 (6%) PAGE VE CONTINUE ON PAGE V4 2. MARK'%' I 3. EFFLUENT t UNRS 5. INTAKE (, ,—A 1. POLLUTANT b. MAXIMUM M DAY VALUE c. LONG TERM AVRG. LONG TERM XND e r a. MAXIMUM DAILY VALUE (m.uLA,I.) VALUE yLnvJWrle) AVERAGE VALUE CAS NUMBER TEsnNO BFilEvBG BEUEYEO O.NO.OF aCONCEK O. NO. OF III tlI 1D I+1 REOUIREO PRESENT A85EM CONLEMMTION 12)MAM CONCENTIUTC I21MA55 CONCE("MMN 12)N>99 ANALYSES T TION E.M s CCNCENTFATION 121 NA95 YSE GCMS FRACTION- BASEMEUTRAL COMPOUNDS 1B. A..., .n xjo:LM4) 28.hmyNeNM Ro6M-01 x 38. MNr.wn. 12112-7) x B.e«Imn. 92-02.5) x 5& e.rix•(•) AMN•c•n. vx5655]1 88.Bmxo lul xPyram (.2132-7) 28. 3.-0•nxo- Marne,m• X 205843) ee. e•nm LN,p xPNyNm (191342) 9B. Bmza (i) Flum•nNme x1202L69) 11;11; v Bl) 9b-1) 118. BY Q, N,,— E V 111 ) B.BNG20, M.,m( t024p] X0@-0PI 3& ltlM. 8.81.1: 17 005 0 1 mg/L lb. 1-71112x14148. A N.nf1 E6 rEB,er xool-P. 101-56]1 158. BNM B.N]31 VxPBMM•N 185594) 168.zLNao- x p+-5aqne.acnolP Bbn,M 2-3ENw x IM C" x218-01-9) ne. Dea,:.1x(11 52-79 x 5NP0208.1.2-PtlWro- Xb.rmm• 1BSso-+I 2+8. 1.]LMIbu b.ru•n. I5.u511 x EPA F01m 351120 (6%) PAGE VE CONTINUE ON PAGE V4 CONTINUED FROM PAGE VA EPAFa 661M1X(690) PAGE V-7 CONTINUE ON REVERSE MARR'1C 8. EFFLUENT UNRS 5. WARE( imwQ 1. POLLUTANT b. MAMMOM W DAY VALUE c. LONG TERM AVRG. LONG TERM AND p MA%MUM DNLY VALUE (I m.ulw lel VALUE 1 AVERAGE VALUE CAB NUMBER TESIINO BELEVEO tl. NO. OF. b. NO. OFBELIEVEDtli111111111 mutlulAel REOUREO PRESENT A W coNCENTPAT1di 121MA55 CCNCENiMi1CN 121M65 CONCENTRAT1oN 121M0.55 ANALYSES TRATION b. MASS CIX FNTMTK 121MAss YSE GC/MS FRACTION –B NEUTRAL COMPOUNDS (—,-0 228.tFpmiors x 22B. 3,1A — 91-W ) xb.... NB. D .N Nb m.4(.#2) 258. N .Mo PM1N9M. 131-11-3)x MB_p WW 005 0 mg/i :bsPh,M.t. (S 7] 21 219.2,.-09.bo- WIN. (121-1.-31 x 2e8.36-0.Ao- 1pwme ISoe-2a31 298. DN2-0uM x 2OB. 11-Dp hyd,.. (.v Am- Lenzene 1122E 4) 11 B. M—nN.n. v 20f ) 12B. FW—n. v 0o-727 228.....Wpro- b.m.n.0W4-11 x NB. N...Worn x..0on.lmaa» 558. N.uWoro- 77474) 17 1) MBINO.Waa mM. l(67-72-1)xz-t) 37B. lmm. 11.22WPn.n. Ii W5) me l.apliwm. x7SWl) 29B. N.PIM.In. ISI -2021 08. NM.bmmm 969}2) x IB. N YpuZ,l.m1n. 162-7s9) 420. KNromo& NAapyMMn. X031# EPAFa 661M1X(690) PAGE V-7 CONTINUE ON REVERSE CONTINUED EPA Form 351aX (690) PAGE Vd CONTINUE ON PAGE V-9 3. MARK X' 3. EFFLUENT A. UNRS 5. INTAKE (......p 1. POLLUTANT 0. MAXIMUM 30 MY VALUE a LONG TERM AVRG. LONG TERM AND 9. MAXIMUM ONLY VALUE 0/mndAle) VALUE phm.n4Al.1 AVERAGE VALUE CAS NUMBER TE6TNG BHIEVFD BELIEVED E. NO. OF •CONGER III E. NO.OFpllyIII lmvllu5l<) REOLWED %iESEHT ABSEM CONCENTRRTION 1$I MA$$ CONLENTRATIpI DI MA55 CONCENTRATION 131 MA55 AILALVSES TMTION U. MASS CONCENTRATION I$I MA55 LYSE GEMS FRACTION-BASEMEUTRAL COMPOUNDS 1-1--)) RtMb4338. 9w6.ewme,. l(8&3M)X u5. PnmMlwe•• g5-0I.el x/ 458. P5,«I• D$?9a9) X b8. I $.4TM1 X021140.6b4qOCMSFRACTION - PESTICIDES 1p.N \/ 13699o-$) x 2P—AHC / xOtswd) JP. / 3t"&7) x AP. AHC56da9) X OF n.B11C94661 X IP. CM * / 57-749) x P. A•'.DOT X156$631 9P. 4.4 -DDE p3-5Sq X 9P.•A''ODD3SHr X maszp IIP..-E e.JM1n / n1636n x 11P. 9 -End• w nlb 9n X IJP. Eb.&AOP XIIOJI-074103, 14P. Entrin p$-$691 X 15P. EnJnN6e6Y6 XH31 -9]J) 16P. Hepd< X76N6) EPA Form 351aX (690) PAGE Vd CONTINUE ON PAGE V-9 EPA I.D. NUMBER (.,y/ Ire.l w— ii OUTFALL NUMBER CONTINUED FROM PAGE V4 110000349070 001 PA PAM 351030 (6 W) PAGE V -B 3 EFFLUENT 4, UNRB mmm 5. INTAKE 1. PoLLUTANi 0. MAXIMUM 50 DAY VALUE LONG TERM AVAG. A. LONG TERM AND p MA%IMUM DAILY VALUE p/aalollr) VALUE yl.nrmhlr) AVERAGE VALUE CAG NUMBER TE NO BELIEVED BEUEYEO O. NO. OF 6. CONGER- O, NO. OFIIInlPI111 11.1 O REWIRED PREMW ABSENT DNCENTRATION 131 M466 GONCEN1MTdi 131 M455 CCNCENTNAPON 1]I MFSG ANALYSEG RATION E. M/SG CCNLENTM1. 131... ZNALYGES OCMG FRACT)ON- PEGTICIOES (rw11n1 r10 ITP. R.pr x1102"1-3) I fiP. PCB.1343 x IBP.PCB-1154 I IOW -0&11 201. PCB -1331 x S P. PCB.12u v 1") 11141-1")x 33P. PC6t20 v p3mz-za61 x 3IP. KS -1360 v ItID%6351 uv. vcB•tm6 836]411-31 Z1-]S3)T1=11 1 v 600 PA PAM 351030 (6 W) PAGE V -B TAB E EPA FORM 2C INTAKE AND EFFLUENT CHARACTERISTICS OUTFALL 002 PLEASE PRINT OR TYPE IN THE UNSHADED MEAS ONLY. Youmay rpon some mal of eEarllub0n EPA ID. NUMBER (nryn Ir free I of r,mn 1) on•enere.afraid, lac. herr same kA+nM.Yeas d comple" these pepea 110000349070 SEE INSTRUCTIONS. W fAI NO. V. INTAKE AND EFFLUENT CHARACTERISTICS (CmlNurEAOTn pq ] of "i" 2 -C7 PART A-Ydu mol mom.In. ..I. d d Med mN anayeu for. very poYnFll in mill able. Complete oner vi W sell aullsl. Sas huwcuone Mr e5E5bnal ddaM. 3, UNITS 4. INTAKE 2. EFFLUENT b M-Jelmkl e hmv0 b. MA%IMUNI 30 MY VALUE c. LONG TERM AVRG. VALUE a. LONG TERM if. MAXIMUM DAILY VALUE r2mnlMN) rymmlNAlr) AVERAGE VALUE J. NO. OF e. CONCEAL b. NO. Of I. POLLUTANT CONCENRUTON Or MASS CONCENTRATION 121 MASS IIICCNCENRATION 2). ANALYSES TRATION b. MAGS CONCENTRATON 121 MA53 ANALYSES e. B1.Mmael O'Non 0.02 0 1 mg/L lbs Demand (6110) b. Chemical OMen 25 0 1 mg/L lbs Demand (IOP) c. Total Organa Carom 2.1 0.53 1 mg/L lbs Irn1) of TOW Suspended Sold. (MI Q 5 0 1 mg/L lbs e. AmmmM lm£) 0.27 0.07 1 mg/L lbs VALUE VALUE VALUE I. Floe, 0303 01 02 2 MGD p. Twgrah a VALUE VALUE VALUE C VALUE mire) 14 1 h. Temperature VALUE VALUE VALUE C VALUE mmmrr) 19 1 MINIMUM MAXIMUM MINIMUM MAAMUM i, PH 6.7 7.1 2 STANDARD UNITS PARTS- Md 'X' in c.unn 2i for Oa pc M You k m un nasm to M w m pawn. Mark 'X' in column 2-b for each pdgnant You believe to be abl a at 6 ed. redk column 2. M Mly palulxp rhiclr is MNMO eller dindly, m melent DN epreMlyin an eIMMM Inei atims pui.M.. you mull moved Ins neaps of At bast on. emesis lar that popuUmt. For What Miriam. lar which you mark cold. L. you must pri yuaMpative Ens Dr en a .neigh ollMir 00011 n W CiMNr Complete one table for each oWal. See the lnslrudions ler addtional details and requirements. 2. MaRK'X].EFFLUENT 4. UNITS S. INTNtEI nn+o0 t. POLLUTANT b, MAXIMUM 00 MY VALUE c. LONG TERM AVRG. VALUE a. LONG TERM AVERAGE AND e •. MAXIMIMI DAILY VALUE lr VALUE CAS NO. d. NO. OF a. CONCETL b. NO. OFEEUEVOBFUEYEDtllIliIp111 b/rnJnblr) PRESENT ABSENT CONCENTigN 121MA95 CCNCEN.. RI MASS CONCENTRATION 121 MASSM ANALYSES TRATION b.MASS CONOENBATON L1 M435 ANALYSES BeMd2495& x52-91 I b.CNanne. TOW 1910 0098 19.0 10.5 .0018 2 ug/L lbs Ruud M 0098 c C.I. X d. Feed CoM m X e. roan. a$ ") x I. Nbde-Nell• XbeM EPA Form 35100.2C (8-90) PAGE V-1 CONTINUE ON REVERSE ITEM V -S CONTINUED FROM FRONT EPA FOml351PX (&W) PAGE V-2 CONTINUE ON PAGE V-3 2. MARK X' 3. EFFLUENT 4. UNRS 5. INTAKE tr w.rOO L POILIRANT 9. M MkAM M DAY VALUE O. LONG TERM AVRG. VALUE B. LONG TERM AND n n. MAXIMUM DAILY VALUE 4/mrulullrl 4/.n.ulWlcl AVERAGE VALUE CAS NO. BEIIEVEG BEIIEVEO Itl 6. NO. OF LCONCEK U'NO'OF 111 Itl r/•nrrrlWle) PFESEM R05EM COrM:ENTRATIW I]ILWS COruCENTRATKJN I11 W95 Cd+[ENinAnON 2)MASS ANALYSES RATION O.MA55 CONCEMRATON IIIMa95W ANALYSES TOWIXenpxxo lO, x1) 09On4Ga" x 7T23 1w) 1. R6ON4ptlMN 1)Abnp. tOW X 2)6ea, TmM X 3) R6vlum, xTa R14) Retlum 226, v k. SW ea V ulO6-T9d1 S 9MIa•A x n. SUMb X14MSw1 s mm n X o. AMmnum, T. c0.1 0 1 Tg/L lbs 7429-965) p. Bknum, TeW v 74 3P3) Boron. T"/ 7""241 33.7 8.4 1 mg/L lbs r. C" TOW puwal x P,I— T6W X 1.37 0.34 1 mg/L lba IT i) TOaI X 6.68 1.67 1 mg/L lbs 4,3' u. Md ... Toal xT4]9-96)1 v. Manpeneu, W Xpuo-vo-sl a.T., TOW440.]13) x v. TNnlum, Ta XR44"I$) EPA FOml351PX (&W) PAGE V-2 CONTINUE ON PAGE V-3 EPA LD. NUMBER µsyn aim /um l o/Hem 11 OUTFALL NUMBER CONTINUED FROM PAGE 3 OF FORM 2-C 1100003490J0 002 PART C - HIP rte • ppmcry mdugry and lags ousbl mmcmt peoceu wagawefar, nbr m Tebb 2u2In ms 1nglugbne to dgnmina wNO of the GCRAS iragbn. you mug nM for. Made Win column 2a lar N heck GCWS hN1wrLL test apply to roar molugry eM for ALL bob therms Wedges. and nW Pllenok. If you sm MI didar e l to sees cdomn 2-e (Paoamd y lndognea nOnp9cism eggs. oWNk, clod mrvpueN Gcows eegbn d meM -X' in column 2-b M mch pobmm you lama ce esn neon to bNbm is prompt. Me* 'X' In column 2-c for each pollultnt Wu Mason is absent. If you meM column 29 for airy poludid! you mug mV the pea} a al beg om andabas M Mug poW Xg..passed, 2b bus goy pWYMfII, yW mug pnwUe 1M pasateoIst Mm10us market{ or test polaMmnYW sees G NN fisher, ba}N awi be dlKMfpol In <oMsmnlbns 0110 ppb or yngef. If di mark Column 2b lar }rvb}, ecr i nus , 2.4 dlnNophenN, of 2 -methyl-<, 6 dInIINpNnol, you mug pfoNde IM neule of g beg one an.yxe lar each .1 than pddaane which rou Mcw or Nag neem 10 stages beet you gedu ri n heedpnbgbne M too ppb w pnalef, gnerene, for popNSMe far whbh YW mete column 2b. YW mug mow euMns Is beg one order of prefer mecnbe me reasons IM Pi M le e " to be g shad ed, Not that Nen to ) Payee to Nb pees. Flame reabw eah carefully, Complete one table mol 2 pcptg for each ruses. See Inclmdmne for tddabMl dMa} ark maps2. MAFtEX 3, EFFLUENT t. UNDS 5, p TAXE Lnwma0 1. POLLI/TN9T b. MAXIMUM 00 DAY VALUE c, LONG TERM AVRG. a. LONG TERM AND p a. MAXBAUM DAILY VALUE plmrnlmlr2 VALUE pluwnl dlrl AVERAGE VALUE CAB NUMBER TES,NO BELIEVED gELIEVEO d. NO. OF a, CONCEAL b. NO.OFIOp1III RASION III l—inter) REOIIIREO PRESENT ABSENr C.,C 121 W65 CCNCEx(') TION 121 MA65 CONCENIRATON 121 eM65 ANALYSER TRAT ON s. MA55 CONCENTRATION i21MA56 YBE METALS, CYANIDE, AND TOTAL PHENOLS I M. Ammon, Total x74418L1 2M,Ari Tool X <0.01 0 1 Ing/L lbs0440.30.3) 38-2) 3M. Beryllium, Tot x044011-01 SM. Cummum, Tot x(7a 3-91 SM. Chu mium, 05 0 1 mg/L lbs ret(Taa0AT31 SM. Copper. Tot x]NO-50d) M. Lead, Tet x(7439-2-1) We. Mew, Tot x(7439 974S) 9M. Will, Total 7440-02-0) ISM. Selenium, Tot (T28N9-2) 440Toral22-4) X <0.005 0 1 mg/L lbs 12M, Thabum, Tot (7440.28-0) 13M. 21no Tolg v 7440383) 1'M. Cysn", v TMA (57-123) 15M. Phenols. Tom DIOXIN 1371 -TSA DEBCRIBE RESULTS deem (176 18) EPA Form 3516X 18-01 PAGE V-3 CONTINUE ON REVERSE THE FROM2. MAR77 0. EFFLUENT UNITS S. INTAKE ( umuQ 1. POLLMANT p. MA%IMUM JO MY VALUE c. LONG TERM AVRG. s. LONG TERM AND N RIEIIIRIPRESENT a. MA%IMUM DAILY VA UE pfM1!! e) VALUE Q/mvJoDle AVERAGE VALUE CAS NUMBER 9FLEVED BELIEVED 6NO.OF aCONCEK IE D. NO.OF III 0, IT il nv IMle) ABSENT COm.- r- ON RI Me88 CONCENIMTION 121M5s6 CONLENTRATON 121MFSa AHALYaES TRATION p. MA63 CCNCENIRATION RI MA55 LYSE GCIMS FRACTION-VOI TILE COMPOUNDS 1V. in V c 005 0 1 mg/L lbs 42'4) N. AvAe x 05 0 1 Ilg/L lbsIDT -1y1) 9V. 314UnB e x 002 0 1 ng /L lbs2) AV. Bb (01— 4 Eft 1L 0 1 mg/L lbs 24 1) SV. Brame . x 002 0 1 mg/L lbsS2"2) w.cenTroaNbIN c.002 0 1 Ilg/L lbs @62151N. CNm°pemru x 002 0 3 mg/L lbs17) ev. cw.m N°m°mMMN X 002 0 1 t3/L lbs 12H41 X<. 002 0 1 mg/L lbs S JI w.1LNwsIIM754d'r X 005 0 1 Ilg/L lbs 110.]5-0) IIV.CNoff X 002 0 1 lbs 874 31IMm9/L DOW. I:Io..nie0.. 002 0 1 Ig/L lbs 7"27013V. PUaMwemeuene 002 0 1 mg/L lbs 714) 14V.IuV. U75 X/ 002 0 I ag/L lbsU -m- O5->.-21 15V. 1,2-DCMmo x 002 0 1 mg/L lbs107-06-2) 1 X 002 0 1 mg/L lbsty-0'y2, ylO" e 17V. 1.2-0iwpo- x 002 0 1 L lbs propene(S-0T4) 1 1 Iw. LlUtllbo- proppene X 002 0 1 rtg/L lbe 5/2-75b) Iev. ENMeIRxN V 002 0 1 mg/L lbs 002 0 1 IIg/L lba B—IM pHiy) 21V. LM" 002 0 1 Dg/L iba cxwnae (uT4) EPA Fpm 3510.20 (690) PAGE V4 CONTINUE ON PAGE V-5 CONTINUED FROM PAGE VJ EPA Fpm 551&2C (&90) PAGE V.6 CONTINUE ON REVERSE 3. MARR-A- 0. EFFLUENT UNITS 5. WTME 1, POLLUTANT b. MA M, JO WY VALUE e. LONG TERM AVRG. LONG TERM AND brEWFE] MAA IUM OAILY VALUE 4/aml,.uel VALUE (4 a+nlaele) AVERAGE VALUE CAS NUMBER NSEUEYED E. NO. OF CONCEP& b. NO.OFBELIEVED111IqItltll lr/wurlydla) PRESENT ABSENt CONCEMMTON 134 CONCENT TION 131 MA66 CONCENTRAl10N 131 MP66 ANALYSES TRATION b. MASS LONLENTMTBN 2)MASS YBE GC/MS FRACTION– VOLATILE COMPOUNDS (•.wrnued) 2V, M."./ x 002 0 mg/L IDSCMn& (7"0.2) 23V. 1112. T... . X 002 0 1 mg/L lbs VW0.x&524V. Teb.a9«o- V( 127-1 002 0 1 mg/L lba 25V.Tau.rn25V. TE x 002 0 1 mg/L lbs Z6V.1]-Trem- DicSN.eemylene X 002 0 1 mg/L lb. 1564032N. 11.1-Tn X 002 0 1 mg/L lb. emw. 171-5541 28P¢ neL1I- Trbi1]" 651wo- 002 0 1 mg/L lb. eme 26v TRm«o- X 002 0 1 my/L Ins Mllene p0.0181 xM. TriaAuemmemme X 002 0 1 mg/L lbs 540. nv.wnP cm«le. x 002 0 1 mg/L lbsw1;1 3CWS FRACTION—AC IO COMPOUNDS 1A2CNwwmnm x(9&5]-8) 3A.2 FQC x0b.na U2Me ) 2A 26-0im * xphend(105-0]-9) U.6-0mNo O- Creea (53444) wz4 . x0..1(51-2") 60.2.NbW-a x(e&]&5) 7A.84.bapberM xI0 -02a) BA. PCNwPK xCr..a 150-50.7) 9A PenMaiwa- Vxh.na(8]-8&5) 1oA Pb.na x/ 11A.z10-Trw,we. ph.n, (ewsxl x EPA Fpm 551&2C (&90) PAGE V.6 CONTINUE ON REVERSE EPA F Wm 351M36 (&90) PAGE V5 CONTINUE ON PAGE V-7 3. MARK'X' J. EFFLUENT 6. UNRB 5. INTAKE (npumop 1. PoLLUTANT p, MAXIMUM BO DAY VALUE c LONG TERM AVRG. a. LONG TERM AND a b c a. MAXIMUM DAILY VALUE (Im.wLdlq VALUE pLe+u W/z) AVERAGE VP1UE CAS NUMBER 1E911NG BEIJEVED eEUEVED O. No. OF t CONCEK b. NO, OF III DI. III 111 Mle) PEST D PgESENT ABSENT CONCEN"' nON 131 MASS CONCE MAATION 131 MASS CONCE")FATON 131 MA55 ANPLYSES TRNTION b. MA CONCENigA"LN I31 MA55 YSE GCIMS FRACTION— BASE/NEUTRAL COMPOUNDS 1B.Acenaphth— xB1-33-9) 3B.Acen,hWne x3069641 38.M raun 130.1241 x e8. B .-. 9347-5) se. Benzo (u) Annnc.n. X wss4) BB. Beniu(o) xP„.n. (5LLJ34, 7B. ].48enxu r en. 205A9-3) ee. e.n:. peJ xPeplene1191-N3) 9B.Benz w F0142. 2ene X hM,.eo. M n) XM11191-1)-') 110. ImNInOEther x 2B. IB. XEther (unpm0{103--1) 80 138, & 117-014) NmylfAfl,IPnmM mel Em' x101-sSJ) 1 SB. wtM Ben4 xPMlliele(85 &7) 668. 3-Chloro- pl .N " 91-567) 178, 4CM 0-0 Phenyl M. Vx797za7 1318-01-9) 198.04enm (nh) MPrew a x5Y76JI 308.11-oicAbro- Xbenzene (9650.1) r B.I to -NW. bmleene(5a1-7J1) x EPA F Wm 351M36 (&90) PAGE V5 CONTINUE ON PAGE V-7 EPA Form 3510.20 (8-90) PAGE V-7 CONTINUE ON REVERSE x. MAR 3. EFFLUENT UNITS S. INTAKE (n f—ul 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c LONG TERM AVRG. a. LONG TERM AND e. r c a. MAXIMUM DAILY VALUE IrlmnJnel.) VALUE y/mm4d/.) AVERAGE VALUE LAS NUMBER STING eEuBVED 6EUEVE a. NO. OF a. CONCExt Ib.NO. OF D1 01 111 OI11RE0 PRESENT PBSEM CONCENTRATION O)MASS CONCENTRATION ($1 MASS CONCENTRATION IxI MA55 ANALYSES TRATION b. MASS CONCENTRATION I$I MASS ANALYSES GOATS FRACTION-BAS EUTRAL COMPOUNDS 1.•rmm,...0 22B.l/-D61om- XbemMe (101,x6'7) 235.3 HA~' M—d.na(91.941) 24B.0 MO v Nifialte(U,ML2) 25B.0meNyl MNe11- 131-11-3) m. DI-N-Bum P.M. 1x47421 27B.24-Dn. taMenx (121-142) 28B. 26U xtduens(606-30.x) 29B. CFN-0 M PMheMP (I 17246) enyt311,. etl1,$- Dghnehybrlee Azm Xbenzene111x228- EYrorannnna 21M 4o1xOw X 128. FMwem xMMT) 338. Hesadloro- benzene (1161411 B. Heee.W.— bubbene (87243) 35B. Hev.Mwo- rydo7en71474)(71474)) 6B NeaaWw xM.ne (67-72-1) 311,.111.13M1 PyremPI 193-39-51 39B. leophomne nds9 p 31 B. NephNYene 91-20.3) eOB. Ntrabenzsie 19695]) I X B. liNltro- itoB metrrylemim X 62459) x2B. &Nitrosob- N-%aONamine X16x121-71 EPA Form 3510.20 (8-90) PAGE V-7 CONTINUE ON REVERSE ft1MIN11Ff1 3. MARX'X' 3. EFFLUENT l UNITS 5. INTAKE (rr"_ILPOLLUTMITp. MAXIMUM 30 DAY VALUE c. LONG TERM AWG. A. LONG TERM AND p, c e. MAXIMUM DAILY VALUE I/nrndnala) VALUE [/wntlrAlo) AVERAGE VALUE CAB NUMBER iEsilNa BELIEVED BELIEVED d NO. OF L CONCEN- E. NO. OF p III p( III rlwvJrrAle) REOVIRED PRESENT ABSEM CM'C ENTRRTION 121MA55 CONCENTMTIDN NIMASS CONCENTRATIDN 131M496 ANALYSES TMTION p.MASS CONLEMRRTI IN 121 MF5E YSE GCMS FRACTION– BASEMEUTRAL COMPOUNDS (n 1-1) 438 NN.o alvOenyM1mma x B 3M) B. PnenurMana am") x 458. Pyrene v 130.00A) 468. 1.24Try 120-02-1) GCMS FRACTION – PESTICIDES IP.NJinN04Oo21 2P. , BHC / x319-844) MC v 4) PFP HC9) HC / x1141641 53-048) IP. 4A' -DOT 5b2?3) SP.4 f -DDE 72 -SSB) 9P.4/' -DDD \/ 12-wx IOP. peMrn v W5]-1) 11 P. u-EnamXm \/ 115-24n x IIP. hEnauMen 1115.24(1 / x I3P. EnaoWM1n WIN, 1031-012) 14P. En.n 72-2") uv.E e,m M&h, e 7421-9 1 16P.Hropc W 7642) EPA Fo m 3510.2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 SPA Form 35132C (390) PAGE V-9 EPA G. NUMBER(,, from Lam lu//u.m l)OU NUMBER 110000349070 002TFALL CONTINUED FROM PAGE V-0 MARK 'X EFFLUENT 4, UNITS S. INTAKE ppumnQ 1. POLLUTANT 0. MAXIMUM ]0 DAY VALUE c. LONG TERM AVRG, a. LONG TERM AND nE e. a e. MAXIMUM DAILY VALUE p/mmbM1le) VALUE 01mmlMle) AVERAGE VALUE CAS NUMBER 6EUEVE0 0. NO. OF 6. CONCEN- 0_NO.OFSEUEVEUtOlrnIII I!Im IWe) PRESEM ABSEM OgyCFMMnON 1$I MA55 GONCFNTRTTION 121 MA56 CONCENTRAPON 121 MA56 ANPLYSES RATION O. MA55 CONCENTgpTION 121 MA55 YSE DONS FRACTION- PESTICIDES (r. ... . .Q 17P. HepncM1lw 1 e X102to245]-]) 16P. PCB -1242 5]464219) 19P. PCS -1291 x(1108]631) 29P. PC0-1221 / 11104-2631 x 21P.PC0-1232 / 11141-163) x 22P. PCB -1248 v 126]2-246) 23P.P061260 v 1109F616) 24P. PCB -1016($62411'2) 15P. T...h.- \ 6001-052) SPA Form 35132C (390) PAGE V-9 TAB F TOPOGRAPHIC MAP FORM 1 SECTION XI Kingston ) 9821 1, OUTFALL 001 TO BRUSHY CREEK LATITUDE: 35'20'25" l J-/ I LONGITUDE: 81'36' 58deWwjI b o 77 Wiliam 3• - ' f ' P su6riNtyn hil. i• - 'f'Ill:\ YY L •' sae OUTFALL 002 TO OVERFLOW o r LATITUDE: 3519'27" LONGITUDE: 81'37'50" + 1 1 REFERENCE SCALE IN FEET y 1. U.S.G.S. 7.5' TOPOGRAPHIC MAP, BOILING SPRINGS NORTH NEEMMEEM AND SHELBY QUADRANGLE, NORTH CAROLINA DATED: 2002. 0 2000 4000 ELE940 W S BTRIC S RN SWITCH ROAD S FIBER AMERICA, LLC Civil & Environmental Consultants, Inc. SHELBY, NORTH CAROLINA R 1900 Center Park Drive - Sufte A - Charlotte, NC 28217 Ph: 980.237.0373 - Fall: 980.237.0372 SITE LOCATION MAP w .cecinc.com ZDRAWN BY: JK$ I CHECKED BY: GPT APPROVED BY: - FIGURE NO.: DATE: JANUARY 2018 DWG SCALE: V = 2000'1 PROJECT NO: 122-243.015 TAB G LABORATORY REPORTS zacAna4 al' pamws.mn November 14, 2017 Mr. Guy O'Connor Electric Glass Fibers of America, LLC 940 Washburn Switch Road Shelby, NC 28150 RE: Project: Permit Renewal 001 Pace Project No.: 92361385 Dear Mr. O'Connor: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Muntersville, NC 28078 704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 01, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNUNELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Sarah Graham for Angela Baioni angela.baioni@pacelabs.com 704)875-9092 Project Manager Enclosures cc: John Littlejohn, Electric Glass Fibers of America, LLC Mr. Richard Young, Electric Glass Fibers of America, LLC Ab, REPORT OF LABORATORY ANALYSIS This report shall not be %produced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 23 Pace Analytical" ww.pxe w o= Project: Permit Renewal 001 Pace Project No.: 92361385 Pace Analytical Services, LLC 9900 Kincey Ave. Suite 100 Huntersville. NC 28079 704)075-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not 6e reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 23 PaceAnalytical" xuwpxebba.ovn SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Sufte 100 Huntersville, NC 28078 704)875-9092 Project. Pace Project No Permit Renewal 001 92361385 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92361385001 001 EPA200.7 DS, SH1 7 PASI-A EPA 625 Bpi 5 PASI-C EPA 624 GAW 35 PASI-C EPA 300.0 CDC 1 PASI-A SM 5220D SLB 1 PASI-A SM 53108 KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the wrl0en consent of Pace Analytical Services, LLC. Page 3 of 23 162ceAnaocal' ANALYTICAL RESULTS Pau Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)8759092 Project: Permit Renewal 001 Pace Project No.: 92361385 Sample: 001 Lab ID: 92361385001 Collected: 11/01/1708:00 Received: 11/01/1709:00 Matrix:Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Aluminum NO ug/L 100 1 11/07/17 01:15 11/13/17 14:49 7429-90-5 Arsenic NO ug/L 10.0 1 11/07/1701:15 11/14/1701:26 7440-38-2 Boron 367 ug/L 50.0 1 11/07/1701:15 11/13/1714:49 7440-42-8 Chromium NO ug/L 5.0 1 11/07/1701:15 11/13/1714:49 744047-3 P8 Iron NO ug/L 50.0 1 11/07/1701:15 11/13/1714:49 7439-89-6 PB Magnesium 2380 ug/L 100 1 11/07/17 01:15 11/13/17 14:49 7439-95-4 Silver ND ug/L 5.0 1 11/07/1701:15 11/13/1714:49 7440-22-4 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Di-n-butylphthalate NO ug/L 5.0 1 11/0711710:06 11/08/1723:43 84-74-2 bis(2-Ethylhexyl)phthalate NO ug/L 5.0 1 11/07/1710:06 11/08/1723:43 117-81-7 Surrogates Nitrobenzene-d5(S) 53 q 10-120 1 11/07/1710:06 11/08/1723:43 4165-60-0 2-Fluorobiphenyl(S) 49 15-120 1 11/07/17 10:06 11/08/17 23:43 321-60-8 Terphenyl-014 (S) 58 11-131 1 11/07/17 10:06 11/08/17 23:43 1718-51-0 624 Volatile Organics Analytical Method: EPA 624 crolein NO ug/L 5.0 1 11/03/1702:27 107-02-8 lcrylonilrile NO uglL 50.0 1 11/03/1702:27 107-13-1 3enzene NO uglL 2.0 1 11/03/1702:27 7143-2 Bromodichloromethane NO uglL 2.0 1 11/03/17 02:27 75-274 Bromoform NO uglL 2.0 1 11/03/17 02:27 75-25-2 Bromomethane NO ug/L 2.0 1 11/03/1702:27 74-83-9 Carbon tetrachloride NO uglL 2.0 1 11/03/17 02:27 56-23-5 Chlorobenzene NO ug/L 2.0 1 11/03/17 02:27 108-90-7 Chloroethane NO ug/L 2.0 1 11103/1702:27 75-00-3 2-Chlorcelhylvinyl ether NO ug/L 5.0 1 11/03/1702:27 110-75-8 c2 Chloroform NO ug/L 2.0 1 11/03/1702:27 67-66-3 Chloromethane NO ug/L 2.0 1 11/03/1702:27 74-87-3 Dibromochloromelhane NO ug/L 2.0 1 11/03/1702:27 12448-1 Dichlorodifluoromethane NO ug/L 2.0 1 11/03/1702:27 75-71-8 1,1-Dichloroethane NO ug/L 2.0 1 11/03/17 02:27 75-34-3 1,2-Dichloroethane NO ug/L 2.0 1 11/03/17 02:27 107-06-2 1,1-Dichloroethene NO ug/L 2.0 1 11/03/17 02:27 75-35-4 cis-1,2-Dichloroethene NO ug/L 2.0 1 11/03/17 02:27 156-59-2 trans-1,2-Dichloroethene NO ug/L 2.0 1 11/03/17 02:27 156-60-5 1,2-Dichloropropane NO uglL 2.0 1 11/03/17 02:27 78-87-5 cis-1,3-Dichloropropene NO uglL 2.0 1 11/03/1702:27 10061-01-5 trans-1,3-Dichloropropene ND ug/L 2.0 1 11/03/1702:27 10061-02-6 Ethylbenzene NO ug/L 2.0 1 11/03/1702:27 10041-4 Methylene Chloride ND ug/L 2.0 1 11/03/1702:27 75-09-2 1,1,2,2 -Tetrachloroethane ND ug/L 2.0 1 11/03/1702:27 79-34-5 Tetrachloroethane ND ug/L 2.0 1 11/03/17 02:27 127-18-4 Toluene ND ug/L 2.0 1 11/03/1702:27 108-88-3 1,1,1 -Trichloroethane ND ug/L 2.0 1 11/03/1702:27 71-55-6 1,1,2 -Trichloroethane ND ug/L 2.0 1 11/03/17 02:27 79-00-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 23 Pats Analytical Services, LLC aceAmlytical 9500 ncey Ave. Sude Huntersville, NC 28078078 areslsbs.owi (704)875-9092 ANALYTICAL RESULTS Project: Permit Renewal 001 Pace Project No.: 92361385 Sample: 001 Lab ID: 92361385001 Collected: 11/01/1708:00 Received: 11/01/1709:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 624 Volatile Organics Analytical Method: EPA 624 Trichloroethene ND ug/L 2.0 1 11/03/17 02:27 79-01-6 Trichlorofluoromethane ND ug/L 2.0 1 11/03/1702:27 75-69-4 Vinyl chloride ND ug/L 2.0 1 11/03/1702:27 75-01-4 Surrogates 4-Bromofluorobenzene(S) 98 % 70-130 1 11/03/1702:27 460-00-4 Toluene-d8(S) 104 % 70-130 1 11/03/1702:27 2037-26-5 1,2-Dichloroethane-d4(S) 103 % 70-130 1 11/03/1702:27 17060-07-0 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 32.1 mg/L 1.0 1 11/06/1717:48 14808-79-8 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND mg/L 25.0 1 11/13/17 19:02 L2 53108 TOC Analytical Method: SM 53108 Total Organic Carbon 4.5 mg/L 1.0 1 11/02/1719:15 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 23 2C6Ana0cal e weeyzelsbe.txvn QUALITY CONTROL DATA Project: Permit Renewal 001 Pace Project No.: 92361385 OC Batch: 385479 QC Batch Method: EPA 200.7 Associated Lab Samples: 92361385001 MSD Spike Conc. Analysis Method: Analysis Description: EPA 200.7 200.7 MET METHOD BLANK: 2137810 Rec Matrix: Water Units Conc. Associated Lab Samples: 92361385001 Rec Limits Qualifiers Aluminum ug/L 5000 4640 Blank Reporting 85-115 Parameter Units Result Limit 467 Analyzed Aluminum ug/L ND 100 11/13/1716:30 Arsenic ug/L ND 10.0 11/14/17 01:20 Boron ug/L NO 50.0 11/13/1716:30 Chromium ug/L 200 5.0 11/13/1714:34 Iron ug/L 188 50.0 11/13/1714:34 Magnesium ug/L ND 100 11/13/1716:30 Silver ug/L ND 5.0 11/13/1716:30 LABORATORY CONTROL SAMPLE: 2137811 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)875.9092 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2137812 MS 92361368001 Spike Parameter Units Result Conic. MSD Spike Conc. Spike LCS LCS Rec Parameter Units Conc. Result Rec Limits Qualifiers Aluminum ug/L 5000 4640 93 85-115 Arsenic ug/L 500 467 93 85-115 Boron ug/L 500 456 91 85-115 Chromium ug/L 500 446 89 85-115 Iron ug/L 5000 4460 89 85-115 Magnesium ug/L 5000 4470 89 85-115 Silver ug/L 250 229 91 85-115 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2137812 MS 92361368001 Spike Parameter Units Result Conic. MSD Spike Conc. 2137813 MS Result MSD Result MS Rec MSD Rec Ret Limits RPD Qual Aluminum ug/L ND 5000 5000 4760 4750 94 94 70-130 0 Arsenic ug/L NO 500 500 478 478 96 96 70-130 0 Boron ug/L 0.090 500 500 557 560 93 94 70-130 1 mg/L Chromium ug/L NO 500 500 444 442 88 88 70-130 1 Iron ug/L 0.23 5000 5000 3450 3450 64 64 70-130 0 M1 ri Magnesium ug/L 1.6 5000 5000 6070 6090 90 90 70-130 0 mg/L Silver ug/L NO 250 250 232 232 93 93 70-130 0 Results presented on this page ere In the units indicated by the'Unbs' column except where an alternate unit Is presentee to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 23 CeAnaytical e eawrpaaltle.00+n QUALITY CONTROL DATA Project: Permit Renewal 001 Pace Project No.: 92361385 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Nuntersville. NC 28078 704)075-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137814 2137815 MS MSD 92361488001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conic. Result Result % Rec Roo Limits RPD Qual Aluminum ug/L 4650 4660 0 Arsenic ug/L 468 469 0 Boron ug/L 485 483 0 Chromium ug/L 626 625 0 Iron ug/L 4430 4490 1 Magnesium ug/L 4710 4750 1 Silver ug/L 229 229 0 Results presented on this page are in the units indicated by the 'UmW column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 23 i PaceAnaVical" wewpacwaoacnm QUALITY CONTROL DATA Project: Permit Renewal 001 Pace Project No.: 92361385 QC Batch: 385093 Analysis Method: EPA 624 QC Batch Method: EPA 624 Analysis Description: 624 MSV Associated Lab Samples: 92361385001 METHOD BLANK: 2134818 Matrix: Water Associated Lab Samples: 92361385001 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1 -Trichloroethane ug/L ND 2.0 11/02/1717:58 1,1,2,2 -Tetrachloroethane ug/L ND 2.0 11/02/17 17:58 1,1,2 -Trichloroethane ug/L NO 2.0 11/02/17 17:58 1,1-Dichloroethane ug/L ND 2.0 11/02/1717:58 11-Dichloroethene ug/L NO 2.0 11/02/17 17:58 1,2-Dichloroethane ug/L NO 2.0 11/02/17 17:58 1,2-Dichloropropane ug/L NO 2.0 11/02/17 17:58 2-Chloroethylvinyl ether ug/L NO 5.0 11/02/17 17:58 Acrolein ug/L NO 5.0 11/02/1717:58 Acrylonitrile ug/L NO 50.0 11/02/1717:58 Benzene ug/L NO 2.0 11/02/1717:58 Bromodichloromethane ug/L NO 2.0 11/02/1717:58 Bromofonn ug/L NO 2.0 11/02/1717:58 Bromomethane ug/L NO 2.0 11/02/1717:58 Carbon tetrachloride ug/L NO 2.0 11/02/17 17:58 Chlorobenzene ug/L NO 2.0 11/02/17 17:58 Chloroethane ug/L ND 2.0 11/02/1717:58 Chloroform ug/L NO 2.0 11/02/1717:58 Chloromethane ug/L NO 2.0 11/02/1717:58 cis-1,2-Dichlcroethene ug/L ND 2.0 11/02/1717:58 cis- 1, 3-Dichloropropene ug/L ND 2.0 11/02/1717:58 Dibromochloromethane ug/L NO 2.0 11/02/1717:58 Dichlorodifluoromethane ug/L NO 2.0 11/02/1717:58 Ethylbenzene ug/L ND 2.0 11/02/1717:58 Methylene Chloride ug/L NO 2.0 11/02/1717:58 Tetrachloroethene ug/L NO 2.0 11/02/1717:58 Toluene ug/L NO 2.0 11/02/17 17:58 trans-1,2-Dichloroethene ug/L NO 2.0 11/02/1717:58 trans-1,3-Dichloropropene ug/L NO 2.0 11/02/17 17:58 Trichloroethene ug/L NO 2.0 11/02/17 17:58 Trichlorofluoromethane ug/L NO 2.0 11/02/1717:58 Vinyl chloride ug/L NO 2.0 11/02/1717:58 1,2-Dichloroethane-d4 (S) 97 70-130 11/02/17 17:58 4-Bromofluorobenzene (S) 100 70-130 11/02/1717:58 Toluene -d8 (S) 104 70-130 11/02/1717:58 LABORATORY CONTROL SAMPLE: 2134819 Qualifiers Pap Analytical Semloee, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 704)875-9092 Spike LCS LCS %Res Parameter Units Conc. Result %Rec Limits Qualifiers 1,1,1 -Trichloroethane ug/L 20 18.2 91 52-162 fthh b presented on this page are in the unit. Indicated by the "Unit." column e ... pt where en Nterri unit la peMnted to tM right of ate neua. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Anal0t;al Services, LLC. Page 8 of 23 PaceAna/ytical e awwpxNebawm QUALITY CONTROL DATA Project: Permit Renewal 001 Pace Project No.: 92361385 Pace Analytical Services, LLC 9800 Kincey Ave. Sufte 100 Huntersville, NC 28078 704)8759092 LABORATORY CONTROL SAMPLE: 2134819 Spike LCS LCS Rec Parameter Units Cone. Result Rec Limits Qualifiers 1,1,2,2 -Tetrachloroethane ug/L 20 17.1 86 46.157 1,12 -Trichloroethane ug/L 20 18.6 93 52-150 1,1-Dichloroethane ug/L 20 17.5 87 59-155 1,1-Dichloroethene ug/L 20 19.2 96 1-234 1,2-Dichloroethane ug/L 20 18.2 91 49-155 1,2-Dichloropropane ug/L 20 19.3 97 1-210 2-Chloroethylvinyl ether ug/L 40 29.8 75 1-305 Acrolein ug/L 100 130 130 15-152 Acrylonitrile ug/L 100 89.0 89 75-132 Benzene ug/L 20 18.5 93 37-151 Bromodichloromethane ug/L 20 18.4 92 35-155 Bromoform ug/L 20 16.3 81 45-169 Bromomethane ug/L 20 20.1 100 1-242 Carbon tetrachloride ug/L 20 18.5 93 70-140 Chlorobenzene ug/L 20 18.1 91 37-160 Chloroethane ug/L 20 18.9 94 14-230 Chloroform ug/L 20 17.8 89 51-138 Chloromethane ug/L 20 17.3 87 1-273 cis-1,2-Dichloroethene ug/L 20 18.4 92 68-146 cis-1,3-Dichloropropene ug/L 20 19.2 96 1-227 Dibromochloromethane ug/L 20 16.8 84 53-149 Dichlorodifluoromethane ug/L 20 16.2 81 70.130 Ethylbenzene ug/L 20 17.5 88 37-162 Methylene Chloride ug/L 20 21.6 108 1-221 Tetrachloroethene ug/L 20 18.8 94 64148 Toluene ug/L 20 18.5 92 47-150 trans-1,2-Dichloroethene ug/L 20 18.3 92 54156 trans-l,3-Dichloropropene ug/L 20 18.9 94 17-183 Trichloroethene ug/L 20 19.6 98 71-157 Trichlorofluoromethane ug/L 20 17.9 90 17-181 Vinyl chloride ug/L 20 18.2 91 1-251 1,2-Dichlorcethane-d4 (S) 103 70-130 4-Bromofluorobenzene (S) 96 70-130 Toluene -08(5) 104 70-130 MATRIX SPIKE SAMPLE: 2134821 92361205001 Spike MS MS Rec Parameter Units Result Cone. Result Roe Limits 1,1,1 -Trichloroethane ug/L NO 20 20.9 105 46-171 1,1,2,2 -Tetrachloroethane ug/L ND 20 18.2 91 73-159 1,1,2 -Trichloroethane ug/L NO 20 20.0 100 64152 1,1-Dichlormthane ug/L NO 20 20.1 100 43-172 1,1-Dichloroethene ug/L NO 20 22.1 111 48-189 1,2-Dichlormthane ug/L NO 20 20.4 102 42-171 1,2-Dichloropropane ug/L NO 20 21.6 108 55157 Results presented on this page are in the units indicated by Me -Unlu- column except where an alternate unit is presented to the night of the result. REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 23 162ceft ytical e wlrwystwkGe.mm QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Sufte 100 Huntersville, NC 28078 704)875-9092 Project: Permit Renewal 001 ug/L ND ND 1,1,2,2 -Tetrachloroethane ug/L ND Pace Project No.: 92361385 1,1,2 -Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L MATRIX SPIKE SAMPLE: 2134821 ND 1,1-Dichloroethene ug/L ND ND 1,2-Dichloroethane ug/L 92361205001 Spike MS Ms Red Parameter Units Result Conc. Result Rec Limits Qualifiers 2-Chloroethylvinyl ether ug/L ND 40 ND 0 70-130 M1,c2 Acrolein ug/L ND 100 138 138 70-130 M1 Acrylonitrile ug/L ND 100 101 101 70-130 Benzene ug/L ND 20 20.3 101 54-163 Bromodichloromethane ug/L ND 20 19.8 99 56-152 Bromoform ug/L ND 20 17.1 85 53-151 Bromomethane ug/L ND 20 16.8 84 10-200 Carbon tetrachloride ug/L ND 20 20.1 101 41-175 Chlorobenzene ug/L ND 20 20.7 103 67-152 Chloroethane ugll- ND 20 22.8 114 23-200 Chloroform uglL ND 20 18.4 92 51-166 Chloromethane uglL ND 20 17.0 85 40-175 cis-1,2-Dichloroethene ug/L ND 20 21.2 106 45-174 cis-1,3-Dichloropropene ug/L ND 20 19.9 100 38-146 Dibromochloromethane ug/L ND 20 18.8 94 65-144 Dichlorodifluoromethane ug/L ND 20 18.5 92 70-130 Ethylbenzene ug/L ND 20 19.8 99 57-152 Methylene Chloride ug/L ND 20 20.0 100 40-167 Tetrachloroethene ug/L ND 20 21.0 105 59-155 Toluene ug/L ND 20 20.6 103 47-162 trans-12-Dichlorcethene ug/L ND 20 21.1 106 47-178 trans-1,3-Dichloropropene ug/L ND 20 19.4 97 39-148 Trichloroethene ug/L ND 20 21.7 109 60-153 Trichlorofluoromethane ug/L ND 20 21.3 107 42-199 Vinyl chloride ug/L ND 20 21.2 106 46-176 12-Dichlorcethane-d4 (S) 101 70-130 4-13romofluorobenzene (S) 96 70-130 7oluene-d8 (S) 96 70-130 SAMPLE DUPLICATE: 2134820 92361204001 Dup Parameter Units Result Result RPD Qualifiers 1,1,1 -Trichloroethane ug/L ND ND 1,1,2,2 -Tetrachloroethane ug/L ND ND 1,1,2 -Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L ND ND 1,1-Dichloroethene ug/L ND ND 1,2-Dichloroethane ug/L ND ND 1,2-Dichloropropane ug/L ND ND 2-Chloroethylvinyl ether ug/L ND ND Acrolein ug/L ND ND Acrylonitrile ug/L ND ND Benzene ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Results preaantetl an We pace an In the unea Inc2ote4 by the "Units" column excW where an altamab writ Is praaai b are right a/ the rnult REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 23 2ceAnaVical a QUALITY CONTROL DATA Project: Permit Renewal 001 Pace Project No.: 92361385 SAMPLE DUPLICATE: 2134820 92361204001 Dup Parameter Units Result Result Bromomethane ug/L ND ND Carbon tetrachloride ug/L NO ND Chlorobenzene ug/L ND NO Chloroethane ug/L ND NO Chloroform ug/L ND NO Chloromethane ug/L ND NO cis-1,2-Dichloroethene ug/L NO ND cis-1,3-Dichloropropene ug/L NO ND Dibromochloromethane ug/L NO ND Dichlorodifluoromethane ug/L NO ND Ethylbenzene ug/L NO ND Methylene Chloride ug/L ND ND Tetrachlorcethene ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L NO NO trans-1,3-Dichloropropene ug/L ND NO Trichloroethene ug/L NO NO Trichlorofluoromethane ug/L ND NO Vinyl chloride ug/L ND NO 1,2-Dichloroethane-d4 (S) 100 102 4-Bromofluorobenzene (S) 100 97 Toluene -d8 IS) 106 102 RPD Qualifiers 2 3 4 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Muntersville, NC 28078 704)875-9092 Resulb pnwrlW on this page an in the ones IrMlute! by the'UnW column except where an Ntemate unit Is presel to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 23 PaceAnaVical e www.pocabbs can QUALITY CONTROL DATA Project: Permit Renewal 001 Pace Project No.: 92361385 QC Batch: 385556 Analysis Method: EPA 625 QC Batch Method: EPA 625 Analysis Description: 625 MSS Associated Lab Samples: 92361385001 METHOD BLANK: 2138167 2138168 Matrix: Water Associated Lab Samples: 92361385001 Spike LCS LCS Ret Parameter Units Conc. Result % Rec Limits Qualifiers Blank Reporting 50 41.6 83 Parameter Units Result Limit Analyzed Qualifiers bis(2-Ethylhexyl)phthalate ug/L NO 5.0 11/08/17 11:48 Di-n-butylphthalate ug/L ND 5.0 11/08/17 11:48 2,4,6-Tdbromophetol(S) 88 10-137 11/08/17 11:48 2-Fluorobiphenyl(S) 73 15-120 11/08/17 11:48 2-Fluorophenol(S) 38 10-120 11/08/17 11:48 Nitrobenzene -d5 (S) 81 10-120 11/08/1711:48 Phenol -d6 (S) 25 10-120 11/08/17 11:48 Terphenyl-d14 (S) 74 11-131 11/08/17 11:48 Pace Anaytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)8759092 LABORATORY CONTROL SAMPLE: 2138168 2138170 Spike LCS LCS Ret Parameter Units Conc. Result % Rec Limits Qualifiers bis(2-Ethylhexypphthalate ug/L 50 41.6 83 8-158 Di-n-butylphthalate ug/L 50 40.9 82 1-118 2,4,6-Tribromophenol (S) 91 10-137 2-Fluorobiphenyl (S) 74 15-120 2-Fluorophenol (S) 39 10-120 Nitrobenzene -d5 (S) 78 10-120 Phenol -d6 (S) 29 10-120 Terphenyl-014 (S) 70 11-131 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2138169 2138170 MS MSD 92361660001 Spike Spike MS MSD MS MSD Rec Parameter Units Result Conc. Conc. Result Result Rec Ret Limits RPD Dust bis(2-Ethylhexyl)phthalate ug/L NO 100 100 88.1 85.2 88 85 8-158 3 Di-n-butylphthalate ug/L NO 100 100 87.7 83.4 Be 83 1-118 5 2,4,6-Tribromophenol (S) 100 98 10-137 2-Fluorobiphenyl (S) 73 77 15-120 2-Fluorophenol(S) 53 52 10-120 Nitrobenzene-d5(S) 80 81 10-120 Phenol-d6(S) 45 43 10-120 Terphenyl-d14(S) 48 39 11-131 Results presented on this page are In the units indicated by Me -Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 23 PaceAnaVical e arw-0rraleD<.mrr Project: Permit Renewal 001 Pace Project No.: 92361385 QC Batch: 385402 QC Batch Method: EPA 300.0 Associated Lab Samples: 92361385001 METHOD BLANK: 2136998 Associated Lab Samples: 92361385001 Parameter Units Sulfate mglL LABORATORY CONTROL SAMPLE: 2136999 Parameter Units Sulfate m91L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)8769092 QUALITY CONTROL DATA Analysis Method: EPA 300.0 Analysis Description: 300.0 IC Anions Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 11/06/1713:48 Spike LCS LCS % Rec Com. Result % Rec Limits Qualifiers 50 49.7 99 9x110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137000 2137001 MS MSD 92361863002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate mg/L NO 50 50 52.4 52.9 104 105 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137002 2137003 MS MSD 92361823001 Spike Spike MS MSD MS MSD e/ Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate mg/L ND 50 50 53.0 53.1 106 106 90-110 0 Result. presented on MIs page em In the units indicated Ey me "UnlW column except where an alternate unit Is presented to the night of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 23 2ceAnayicalo sarwPacablet com QUALITY CONTROL DATA Pace Analytical services, LLC 9800 Kincey Ave. Suite 100 Hunters,ndle. NC 28078 704)8759092 Project: Permit Renewal 001 Pace Project No.: 92361385 OC Batch: 386547 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92361385001 METHOD BLANK: 2143913 Associated Lab Samples: 92361385001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 2143914 Parameter Units Chemical Oxygen Demand mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 25.0 11/13/1719:02 Spike LCS LCS % Rao Conc. Result % Roo Limits Qualifiers 1120 751 67 90-110 L2 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2143915 2143916 MS MSD 92360409001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conic. Result Result Rao % Rao Limits RPD Qual Chemical Oxygen Demand mg/L 803 150 150 900 907 65 69 90-110 1 MO MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2143917 2143918 MS MSD 92361431002 Spike Spike MS MSD MS MSD % Rao Parameter Units Result Conic. Conic. Result Result Rec % Rao Limits RPD Qual Chemical Oxygen Demand mg/L 27.0 150 150 145 141 79 76 90-110 3 MO Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services. LLC. Page 14 of 23 ZeAnaVical* auw.psosltla.ayn QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kmcey Ave. SuHe 100 Huntersville, NC 28078 704)875.9092 Project: Permit Renewal 001 Pace Project No.: 92361385 QC Batch: 384971 Analysis Method: SM 53108 QC Batch Method: SM 5310B Analysis Description. 5310B TOC Associated Lab Samples: 92361385001 METHOD BLANK: 2133960 Matrix: Water Associated Lab Samples: 92361385001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 11/02/17 16:28 LABORATORY CONTROL SAMPLE: 2133961 Spike LCS LCS % Rec Parameter Units Conic. Result Rec Limits Qualifiers Total Organic Carbon mg/L 25 23.6 94 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2133962 2133963 MS MSD 92361364001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Dust Total Organic Carbon mg/L 9.5 25 25 32.4 32.3 91 91 90110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/1412017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 23 PaceAnalytical Kincey Ave. Suite 100 aceAnalytical a Huntersvllle, INC 28078 m. w.pacelabs. caro (704)0769092 QUALIFIERS Project: Permit Renewal 001 Pace Project No.: 92361385 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS L2 Analyte recovery in the laboratory control sample (LCS) was below OC limits. Results for this analyte in associated samples may be biased low. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than the blank or were below the reporting limit. c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether. REPORT OF LABORATORY ANALYSIS This repo" shall not be reproduced, except in full, Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 23 ZcAnapical e e Pecsieba.mn QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Permit Renewal 001 Pace Project No.: 92361385 Pap Analytical Services, LLC 98001(incey Ave. SuRe100 Huntersville, NC 28078 704)8759092 Date: 11/14/2017 05:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 23 Analytical Lab ID Sample ID OC Batch Method OC Batch Analytical Method Batch 92361385001 001 EPA 200.7 385479 EPA 200.7 385555 92361385001 001 EPA625 385556 EPA625 385759 92361385001 001 EPA 624 385093 92361385001 001 EPA 300.0 385402 92361385001 001 SM 5220D 386547 92361385001 001 SM 5310B 384971 Date: 11/14/2017 05:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 23 Laboratory receiving samples: Asheville Eden Greenwood Huntersville Ralelgh Mechanicsville[] lien` Name: me: ^` i G Projecta:I WN 92361385 L C TV1 U bfi Q :JILh II'III IIIII I'IIIIIIIICourier: Fed Ea UPS USPS Client Commercial [')Pace []Other:_ 92361386 t Custody Seal Present? Yes NO Seals Intact? rryX/ Packing Material: Bubble Wrap LJBubble Bags Thermomet ` IR Gun ID: tqU1 Ty7f Correction Factor: Cooler Temp Corrected PC):. Dyes Oo Date/Initial; Person Examining Contents: 1 None Other Biological Tissue Fr ran? Yes No N/A wet Blue none Temp should be above freezing to 6'C Samples out of temp criteria Samples on ice. coding process has begun USDA Regulated Still (a N/A, water samplel Did samples onglyyAte In a quarantine tone within the United States'. CA, NY, or X Icheck maps)] ny.. Title Did samples originate from a foreign source i nternationa0y, nrludine Hawaii and Puerto Riml? 17IYes I "{Na Document Name: Document Revised August 4, 7017 Simple Condition Up.Recel tiSCURI Pae 1 of 7 Document No.: Issuing Authority: t CBAnaiyUCdl es F-CAR-CS-033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville Eden Greenwood Huntersville Ralelgh Mechanicsville[] lien` Name: me: ^` i G Projecta:I WN 92361385 L C TV1 U bfi Q :JILh II'III IIIII I'IIIIIIIICourier: Fed Ea UPS USPS Client Commercial [')Pace []Other:_ 92361386 t Custody Seal Present? Yes NO Seals Intact? rryX/ Packing Material: Bubble Wrap LJBubble Bags Thermomet ` IR Gun ID: tqU1 Ty7f Correction Factor: Cooler Temp Corrected PC):. Dyes Oo Date/Initial; Person Examining Contents: 1 None Other Biological Tissue Fr ran? Yes No N/A wet Blue none Temp should be above freezing to 6'C Samples out of temp criteria Samples on ice. coding process has begun USDA Regulated Still (a N/A, water samplel Did samples onglyyAte In a quarantine tone within the United States'. CA, NY, or X Icheck maps)] ny.. Title Did samples originate from a foreign source i nternationa0y, nrludine Hawaii and Puerto Riml? 17IYes I "{Na CLIENT NOTIFICATION/RESOLUTION Person Contacted. Comments/Sample Discrepancy: Lot IO of split containers' Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? IJYes LJNO Date/Time: Date: Date: Note: Whenever there Is a discrepancy affecting North Caruana compliance samples, a copy or this form will be sent to the North Carolina OEHNR Certification Office (i e Out of hold, mcorrect preservative, out of temp, Incorrect conialnersl Page 18 of 23 Comments/Discrepancy: Chain of Custody Present? es ONO N/A 1. Samples Arrived within Hold Time?res ONO N/A 7. Short Hold Time Analysis 1<72 hr.j? Dyes N N/A 3. Rush Tum Around Time Requested? ym Na N/A 4. Sufficient Volume? Y ONO N/A 5 Correct Containers Used? Pace Containers Used? 61 Yes ONO ONO N/A ON/A 6. Containers intact? Yes NoN A 7. Dissolved analysis: Samples Field Filtered? Yes No N/A a. Sample Labels Match COC? Includes Date/Time/ID/Analysis Matrix: es ONO N/A 9. Heads ace in VOA Vials b5 6mm17 Dyes dNQ ONJA 10. Trip Blank Present? Trip Blank Custody Seals Present] Dyes yrs o No N/ n/A 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted. Comments/Sample Discrepancy: Lot IO of split containers' Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? IJYes LJNO Date/Time: Date: Date: Note: Whenever there Is a discrepancy affecting North Caruana compliance samples, a copy or this form will be sent to the North Carolina OEHNR Certification Office (i e Out of hold, mcorrect preservative, out of temp, Incorrect conialnersl Page 18 of 23 mO 0 3 r 0 0as O N 3 Cr CrO n N O 3 P O ncme a Oa 9 4U-125 mL Plastic Unpresemed (N/A) (Cl.) r i x SPZU-500 mL Plastic Unpreserved (N/A) A v2 CLCL o BP4S-12S mL Plastic H2SO4 IpH <2) (Cl e 3 n IM -250 mL plastic HNO3 (pH <2) 2e. Oovw O w Mo WGPU-Wide-mouthed Glass far Unpresened 6 10 T A H Z AG1U-1 liter Amber UAPresemed IN/A) (CI-) zzzzAGIN-] iRn Ncy n AG3U-2SO ml Amber Unptesemed (N/A) ICH L N 3 AG3S-1 liter Amber H2SO4 (pH < 2) pc AUS -250 ml Amber H2SW (pH < 21 n = o 'n vc AG3AIMMI.250 mL Amber NHACI (N/A)(Cf) e mO 0 3 r 0 0as O N 3 Cr CrO n N O P ncme 9 4U-125 mL Plastic Unpresemed (N/A) (Cl.) BP3U-2SO mL Plastic Unpresemeci (N/A) SPZU-500 mL Plastic Unpreserved (N/A) 9PIU I iter Plastic Unpreterved (N/A) BP4S-12S mL Plastic H2SO4 IpH <2) (Cl IM -250 mL plastic HNO3 (pH <2) BP4Z-125 ml. Plastic 2N Acelate & NaOH 1>91 BPeC-12S mi. Plastic NaOH (pH > 12) (0-1 WGPU-Wide-mouthed Glass far Unpresened T AG1U-1 liter Amber UAPresemed IN/A) (CI-) zzzzAGIN-] liter Amber HCI IPH < 21 AG3U-2SO ml Amber Unptesemed (N/A) ICH AG3S-1 liter Amber H2SO4 (pH < 2) AUS -250 ml Amber H2SW (pH < 21 AG3AIMMI.250 mL Amber NHACI (N/A)(Cf) DG9H40 mt VOA I ICI (N/A1 VG9T40 mL VOA Na2S2O3 (N/A) VG9U<O mL VOA Unp IN/A) OG910-a0 mL VOA 143PO4 IN/A) VOAK (9 vols per k 1)5035 kit IN/A) V/GK 13 vials per ki*VPH/W s kA (N/A) SPST-12S mL Stenle Plastic (N/A - lab) SP23.250 mL Sterne Plastic (N/A -lab) BPM -250 mL Plastic (NH2)25D4 (9.3-9 71 Cubdainer USGU-20 ml Scintillation vials (N/A) GN mO 0 3 r 0 0as O N 3 Cr CrO n N G CHAIN -OF -CUSTODY I Analytical Request Document PaeeAnalytieal TIIe Chain- CuVady Is a LEGAL DOCUMENT All relevant fieltls must be enmpleled accurately patrol. Wm Section A Section ISSedbeC pa / W / m Required Clmnl htlwr wm Required Pr,.t i.,m.enai " a pIm ace Iniwmam. Elfaai.:a.fAReport To R: t Alwi ion. n.<..a+ 9vow•,$(It,,.. St}o( RI? eopyTo a t, Compan,Nan,e Rog REGULATORY AGENCY SAC16y f -E va/f0 Tei L,'"/se Me,e, a0 NPDES GROUND WATER DRINKING WATEREmalToPurMa:u. Ot crrNo Pia Q.a. H .. o.... , UST RCRA OTHER7W•YJY-)l LI ri,Ylr wgeet a.v.e. e..,. Prrw•u IA..^r Site LOCat100RoqursledDueDaWITAT; Purred NlmWur van. anuue LSTATE: Requested Analysis Filtered VIN( srcdunD Malde Codes Ragmreecl....,err,..n.., r,w l4lt r•_ne E COLLECTED Preservatives z DnnMug Waler DW Wale, oU ZZ WT Waste Water WW M oaten. S:. rfo.<Oanl Q forSSet'SuM SL M+xnP SAMPLE ID al oL3 to WiWP lAd o-9 W I ouz C Q O IAuAR S",,"Is iDs MUST BE UNIQUE Team TS 0 oft, (: p C 6iuj 8 d L'1oT a TI-TCT,.E N J v°• aa n^ tl U (' v oA rt TIME i• Z z i y 1 O Or O Pace Project No./ Lab I.D. li,lr7 .Toe r.1,1r7 qR» r 2 06/ C nln odb 1•./$7 e..a s a a Oe/ C Asti as.d 17 are TTTso/ C e/111n ogee p, ./n aSA) I 001 C 111$7 W 1 7 0806 3 7T 001 C d/147 oUw is 1111 aged 1 e eel C 111$7 Ogea I od a7 I 9 0 11 ADDITIONAL COMMENTS RELINQUISHED By I AFFILIATION DATE TME ACCEPTED By I AFFILIATION DATE TIME P -J -el T., .LGA 61. O'Gowner SAMPLE CONDITIONS 1 h 3 Clete I I r) S r SAMPLER NAME AND SIGNATURE gU C eE: PRINT Name or SAMPLER: G.eG.www Oori i E u ajni mcr SIGNATURE or SAMPLER: /_ DATE Signed ItMMONYI: 1 • 1. 7 N1. 1 LI 4n l...... nal eli +w F-ALL-0-020rev.07• 154A y Analytical Results Pace Analytical 9800 Kincey Suite 100 Huntersville, NC 28078 Receive Date: 11/02/2017 Reported: 11/08/2017 For: 92361385 Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 171102-17-01 MBAS 001 <0.1 mg/L sMSWC-2000 11/03/2017 MD Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/ 34697 Page 1 gage 21 of 23 Condition of Receipt Sample Number 171102-17-01 Temp on Arrival: 3 Parameter Schedule: MBAS Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 Q, 22 of 23 Chain of Custody Wo. hurdor 9235'395 W rrhnrcler N,mic Pei^ut Renewal 001 Wcti ull R,apn s Lrtl By 'r1 S „ Pace Analytical• Row I toys e• To {ubeplYaCI TO _ R uNtb m A gi,1a Baur. Pace Analytical Cha0one J"{LA-4tSUIt IL_E PO 9800 'St Ave 8OIL r Munnr5v4le Nf..B07B OlS 078Soth, 100 l lh phone 170418 %59092 - 1 /' 1Emailar3eWDeroni@pacelabscom122- Z 1. r'uV -- qM [s Vi State or Sample On In NC Fel j •r••wwa C&IMM • Militia!LAS USE ONLY 1 ror tlltl20170abp BCW0, i X Z 7 4 C awr Tmalen R•lea••a Sr 0a1•TrM 81 DalelTMr1• 1 e' 2 7 Cooler Temperature on Recei t `C Custod SW r N Received on Ica V nor N Sam lea Intact V N f M 7 Al t -(: 002rev W 2aMarch2009 NO nOl N lD m N `(d 00 a n W 00NUZ d j dN N CONN O Ca 0G. 11ceAnaly & O ssw.psalebauonl November 15. 2017 Mr. Guy O'Connor Electric Glass Fibers of America, LLC 940 Washburn Switch Road Shelby, NC 28150 RE: Project: Permit Renewal 002 Pace Project No.: 92361389 Dear Mr. O'Connor: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)8759092 Enclosed are the analytical results for sample(s) received by the laboratory on November 01, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, a,qq. Angela Baioni angela.baioni@pacelabs.com 704)875-9092 Project Manager Enclosures cc: John Littlejohn, Electric Glass Fibers of America, LLC Mr. Richard Young, Electric Glass Fibers of America, LLC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 20 1 -Pace Analytical www paterabs. tom Project: Permit Renewal 002 Pace Project No.: 92361389 Pace Analytical services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 704)8769092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VrginialVELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 20 Pace Analytical Services, LLC aca mlytical 9800 ncey Ave. Suite100 Hunlersville, NC 28078 706)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No. Permit Renewal 002 92361389 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92361389001 002 EPA 200.7 SHi 7 PASI-A EPA 624 GAW 35 PASI-C SM 2540D SLB 1 PASI-A SM 52108 KMM 1 PASI-A EPA 350.1 1993 Rev 2.0 BRJ 1 PASI-A SM 5220D SLB 1 PASI-A SM 53108 KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not oe reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 20 1 !f'dceAn Vital o ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 704)875-9092 Project: Permit Renewal 002 Pace Project No.: 92361389 ND ug/L 5.0 1 11/03/17 02:45 107-02-8 Acrylonitrile Sample: 002 Lab ID: 92361389001 Collected: 11/01/1707:55 Received: 11/01/1709:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 ND ug/L Aluminum NO ug/L 100 1 11/14/1712:35 11/15/1712:26 7429-90-5 Arsenic NO ug/L 10.0 1 11/14/17 12:35 11/15/17 12:26 7440-38-2 Boron 33700 ug/L 500 10 11/14/17 12:35 11/15/17 14:10 7440-42-8 M6 Chromium NO ug/L 5.0 1 11/14/1712:35 11/15/1712:26 7440-47-3 Iron 1370 ug/L 50.0 1 11/14/17 12:35 11/15/17 12:26 7439-89-6 Magnesium 6680 ug/L 100 1 11114/1712:35 11/15/1712:26 7439-95-4 Silver NO ug/L 5.0 1 11/14/1712:35 11/15/1712:26 7440-22-4 624 Volatile Organics Analytical Method: EPA 624 Acrolein ND ug/L 5.0 1 11/03/17 02:45 107-02-8 Acrylonitrile NO ug/L 50.0 1 11/03/1702:45 107-13-1 Benzene ND ug/L 2.0 1 11/03/17 02:45 71-43-2 Bromodichloromethane ND ug/L 2.0 1 11/03/1702:45 75-27-0 Bromoform ND ug/L 2.0 1 11/03/1702:45 75-25-2 Bromomethane ND ug/L 2.0 1 11/03/1702:45 74-83-9 Carbon tetrachloride ND ug/L 2.0 1 11/03/17 02:45 56-23-5 Chlorobenzene ND ug/L 2.0 1 11/03/1702:45 108-90-7 hloroethane ND ug/L 2.0 1 11/03/1702:45 75-00-3 t-Chloroethylvinyl ether ND ug/L 5.0 1 11/03/17 02:45 110-75-8 c2 hlomform ND ug/L 2.0 1 11/03/1702:45 67-66-3 Chloromethane ND ug/L 2.0 1 11/03/1702:45 74-87-3 Dibromochloromethane ND ug/L 2.0 1 11/0311702:45 124-48-1 Dichlorodifluoromethane NO ug/L 2.0 1 11/03/17 02:45 75-71-8 1,1-Dichloroethane NO ug/L 2.0 1 11/03/1702:45 75-34-3 1,2-Dichlorcethane NO ug/L 2.0 1 11/03/1702:45 107-06-2 1,1-Dichloroethene ND ug/L 2.0 1 11/03/17 02:45 75-35-0 cis-1,2-Dichloroethene NO ug/L 2.0 1 11/03/1702:45 156-59-2 trans-1,2-Dichloroethene NO ug/L 2.0 1 11/03/17 02:45 156-60-5 1,2-Dichloropropane NO ug/L 2.0 1 11/03/17 02:45 78-87-5 cis-1,3-Dichloropropene NO ug/L 2.0 1 11/03/17 02:45 10061-01-5 trans-1,3-Dichloropropene NO ug/L 2.0 1 11/03/17 02:45 10061-02-6 Ethylbenzene NO ug/L 2.0 1 11/03/17 02:45 100-41-4 Methylene Chloride NO ug/L 2.0 1 11/03/17 02:45 75-09-2 1,1,2,2 -Tetrachloroethane ND ug/L 2.0 1 11/03/1702:45 79-34-5 Tetrachloroethene NO ug/L 2.0 1 11/03/17 02:45 127-18-4 Toluene NO ug/L 2.0 1 11/03/1702:45 108-88-3 1,1,1 -Trichloroethane ND ug/L 2.0 1 11/03/1702:45 71-55-6 1,1,2 -Trichloroethane ND ug/L 2.0 1 11/03/17 02:45 79-00-5 Trichloroethene ND ug/L 2.0 1 11/03117 02:45 7901-6 Trichlorofluoromethane NO ug/L 2.0 1 11/0311702:45 75-69-0 Vinyl chloride NO ug/L 2.0 1 11/03/1702:45 75-01-4 Surrogates 4-Bromofluorobenzene (S) 94 70-130 1 11/03/17 02:45 460-00-4 Toluene-d8(S) 101 70-130 1 11/03/1702:45 2037-26-5 1,2-Dichlorcethane-d4(S) 101 70-130 1 11/03/1702:45 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 20 162ceAnaVical e wewPW#18W cmn ANALYTICAL RESULTS Pau Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)8759092 Project: Permit Renewal 002 Pace Project No.: 92361389 Sample: 002 Lab ID: 92361389001 Collected: 11/01/1707:55 Received: 11/01/1709:00 Matrlx:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 2.5 1 11/02/17 08:29 52108 BOD, 5 day Analytical Method: SM 5210B BOD, 5day ND mg/L 2.0 1 11/02/1702:41 11/06/1721:19 B2,1_2 350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0 Nitrogen, Ammonia 0.27 mg/L 0.10 1 11/09/17 01:16 7664-41-7 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND mg/L 25.0 1 11/13117 19:02 L2 53108 TOC Analytical Method: SM 53108 Total Organic Carbon 2.1 mg/L 1.0 1 11/02/17 19:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20 1 !2ceAnaViC8l e wewpaMtlaoom QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)8759092 Project Permit Renewal 002 Pace Project No.: 92361389 QC Batch: 386674 Analysis Method: EPA200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92361389001 METHOD BLANK: 2144442 Matrix: Water Associated Lab Samples: 92361389001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Aluminum ug/L NO 100 11/15/17 12:20 Arsenic ug/L NO 10.0 11/15/1712:20 Boron ug/L NO 50.0 11/15/17 14:04 Chromium ug/L NO 5.0 11/15/1712:20 Iron ug/L NO 50.0 11/15/1712:20 Magnesium ug/L NO 100 11/15/1712:20 Silver ug/L NO 5.0 11/15/1712:20 LABORATORY CONTROL SAMPLE: 2144443 Spike LCS LCS e/ Rec Parameter Units Conc. Result Rec Limits Qualifiers Aluminum uglL 5000 4830 97 85-115 Arsenic ug/L 500 485 97 85-115 Boron ug/L 500 486 97 85115 Chromium ug/L 500 480 96 85-115 Iron ug/L 5000 4750 95 85-115 Magnesium ug/L 5000 4790 96 85-115 Silver ug/L 250 245 98 85-115 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2144444 2144445 MS MSD 92361389001 Spike Spike MS MSD MS MSD Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Aluminum ug/L NO 5000 5000 4920 4970 98 99 70-130 1 Arsenic ug/L NO 500 500 493 492 99 98 70-130 0 Boron ug/L 33700 500 500 36700 36600 608 584 70-130 0 M6 Chromium ug/L NO 500 500 490 495 98 99 70.130 1 Iron ug/L 1370 5000 5000 6240 6250 97 98 70-130 0 Magnesium ug/L 6680 5000 5000 11800 11800 103 103 70-130 0 Silver ug/L NO 250 250 247 252 99 100 70-130 2 Results presented on this page are in the unite Indicated by the'UrW column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 20 aceAnalytical awwpecial com QUALITY CONTROL DATA Project: Permit Renewal 002 Pace Project No.: 92361389 QC Batch: 385093 Analysis Method: EPA624 QC Batch Method: EPA 624 Analysis Description: 624 MSV Associated Lab Samples: 92361389001 METHOD BLANK: 2134818 Associated Lab Samples: 92361389001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1 -Trichloroethane ug/L NO 2.0 11/02/1717:58 1,1,2,2 -Tetrachloroethane ug/L NO 2.0 11/02/1717:58 1,1,2 -Trichloroethane ug/L NO 2.0 11/02/17 17:58 1,1-Dichloroethane ug/L NO 2.0 11/02/17 17:58 1,1-Dichlorcethene ug/L NO 2.0 11/02/1717:58 1,2-Dichloroethane ug/L NO 2.0 11/02/1717:58 1,2-Dichloropropane ug/L NO 2.0 11/02/1717:58 2-Chloroethylvinyl ether ug/L NO 5.0 11/02/1717:58 Acrolein ug/L NO 5.0 11/02/1717:58 Acrylonitrile ug/L NO 50.0 11/02/1717:58 Benzene ug/L NO 2.0 11/02/1717:58 Bromodichloromethane ug/L NO 2.0 11/02/1717:58 Bromoform ug/L NO 2.0 11/02/1717:58 Bromomethane ug/L NO 2.0 11/02/1717:58 Carbon tetrachloride ug/L NO 2.0 11/02/17 17:58 Chlorobenzene ug/L ND 2.0 11/02/1717:58 Chloroethane ug/L NO 2.0 11/02/17 17:58 Chloroform ug/L NO 2.0 11/02/1717:58 Chloromethane ug/L NO 2.0 11/02/1717:58 cis-1,2-Dichloroethene ug/L NO 2.0 11/02/1717:58 cis-1,3-Dichloropropene ug/L NO 2.0 11/02/1717:58 Dibromochloromethane ug/L NO 2.0 11/02/1717:58 Dichlorodifluoromethane ug/L NO 2.0 11/02/1717:58 Ethylbenzene ug/L NO 2.0 11/02/17 17:58 Methylene Chloride ug/L NO 2.0 11/02/1717:58 Tetrachloroethene ug/L NO 2.0 11/02/17 17:58 Toluene ug/L NO 2.0 11/02/17 17:58 trans-1,2-Dichloroethene ug/L NO 2.0 11/02/17 17:58 trans-1,3-Dichloropropene ug/L NO 2.0 11/02/1717:58 Trichloroethene ug/L ND 2.0 11/02/17 17:58 Trichlorofluoromethane ug/L NO 2.0 11/02/1717:58 Vinyl chloride ug/L ND 2.0 11/02/1717:58 1,2-Dichloroethane-d4 (S) 97 70-130 11/02/17 17:58 4-Bromofluorobenzene (S) 100 70-130 11/02/17 17:58 Toluene -d8 (S) 104 70-130 11/02/1717:58 Qualifiers Pace Anatyllcal Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 704)075-9092 LABORATORY CONTROL SAMPLE: 2134819 Spike LCS LCS % Rae Parameter Units Cone. Result % Rae Limits Qualifiers 11,1 -Trichloroethane ug/L 20 18.2 91 52-162 Results presentee on M4 pope an in Me units Indicated by the "Units" column except where an alternate unit is presented to the right of Me result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 20 ceAnaVical e aaa Psestabemn QUALITY CONTROL DATA Project: Permit Renewal 002 Pace Project No.: 92361389 LABORATORY CONTROL SAMPLE: Parameter 2134819 Units Spike Conc. 1 -CS Result LCS Rec Rec Limits 1,1,2,2 -Tetrachloroethane ug/L 20 17.1 86 46.157 1,1,2 -Trichloroethane ug/L 20 18.6 93 52-150 1,1-Dichloroethane ug/L 20 17.5 87 59.155 1,1-Dichloroethene ug/L 20 19.2 96 1-234 1,2-Dichloroethane ug/L 20 18.2 91 49-155 1,2-Dichloropropane ug/L 20 19.3 97 1-210 2-Chloroethylvinyl ether ug/L 40 29.8 75 1-305 Acrolein ug/L 100 130 130 15-152 Acrylonitrile ug/L 100 89.0 89 75-132 Benzene ug/L 20 18.5 93 37-151 Bromodichloromethane ug/L 20 18.4 92 35-155 Bromoform ug/L 20 16.3 81 45-169 Bromomethane ug/L 20 20.1 100 1-242 Carbon tetrachloride ug/L 20 18.5 93 70-140 Chlorobenzene ug/L 20 18.1 91 37-160 Chloroethane ug/L 20 18.9 94 14-230 Chloroform ug/L 20 17.8 89 51-138 Chloromethane ug/L 20 17.3 87 1-273 cis-12-Dichloroethene ug/L 20 18.4 92 68-146 cis-1,3-Dichloropropene ug/L 20 19.2 96 1-227 Dibromochloromethane ug/L 20 16.8 84 53-149 Dichlorodifluoromethane ug/L 20 16.2 81 70-130 Ethylbenzene ug/L 20 17.5 88 37-162 Methylene Chloride ug/L 20 21.6 108 1-221 Tetrachloroethene ug/L 20 18.8 94 64148 Toluene ug/L 20 18.5 92 47-150 trans-1,2-Dichloroethene ug/L 20 18.3 92 54-156 trans-1,3-Dichloropropene ug/L 20 18.9 94 17-183 Trichloroethene ug/L 20 19.6 98 71-157 Trichlorofluoromethane ug/L 20 17.9 90 17-181 Vinyl chloride ug/L 20 18.2 91 1-251 1,2-Dichloroethane-d4 (S) 103 70-130 4-Bromofluorobenzene (S) 96 70-130 Toluene-d8(S) 104 70-130 Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 704)875-9092 Qualifiers MATRIX SPIKE SAMPLE: Parameter 2134821 Units 92361205001 Result Spike Colic. MS Result MS Rec Rec Limits Qualifiers 1,1,1 -Trichloroethane ug/L NO 20 20.9 105 46-171 1,1,2,2 -Tetrachloroethane ug/L NO 20 18.2 91 73-159 1,1,2 -Trichloroethane ug/L NO 20 20.0 100 64152 1,1-Dichloroethane ug/L NO 20 20.1 100 43-172 1,1-Dichloroethene ug/L NO 20 22.1 111 48-189 1,2-Dichloroethane uglL NO 20 20.4 102 42-171 1,2-Dichloropropane ug/L NO 20 21.6 108 55-157 Results presented on this page are in the units indicated by the'Units' column except where an alternate unit is presented to an right of re.ua. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 20 f ZeAnalyfical* xww.Wroleba.00m QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kinsey Ave. Suge 100 Huntersville, NC 28078 704)076-9092 Project: Permit Renewal 002 Pace Project No.: 92361389 MATRIX SPIKE SAMPLE: 2134821 92361205001 Spike MS MS Ree Parameter Units Result Conc. Result Rec Limits Qualifiers 2-Chloroethylvinyl ether ug/L NO 40 NO 0 70-130 M1,c2 Acrolein ug/L NO 100 138 138 70-130 M1 Acrylonitrile ug/L NO 100 101 101 70-130 Benzene ug/L NO 20 20.3 101 54163 Bromodichloromethane ug/L NO 20 19.8 99 56-152 Bromofonn ug/L NO 20 17.1 85 53-151 Bromomethane ug/L NO 20 16.8 84 10-200 Carbon tetrachloride ug/L NO 20 20.1 101 41-175 Chlorobenzene ug/L NO 20 20.7 103 67-152 Chloroethane ug/L NO 20 22.8 114 23-200 Chloroform ug/L NO 20 18.4 92 51-166 Chloromethane ug/L NO 20 17.0 85 40-175 cis-1,2-Dichloroethene ug/L NO 20 21.2 106 45-174 cis-1,3-Dichloropropene ug/L NO 20 19.9 100 38-146 Dibromochloromethane ug/L NO 20 18.8 94 65-144 Dichlorodifluoromethane ug/L NO 20 18.5 92 70-130 Ethylbenzene ug/L NO 20 19.8 99 57-152 Methylene Chloride ug/L NO 20 20.0 100 40-167 Tetrachloroethene ug/L NO 20 21.0 105 59-155 Toluene ug/L NO 20 20.6 103 47-162 trans-1,2-Dichloroethene ug/L NO 20 21.1 106 47-178 trans-1,3-Dichloropropene ug/L NO 20 19.4 97 39-148 Trichloroethene ug/L NO 20 21.7 109 60-153 Trichlorofluoromethane ug/L NO 20 21.3 107 42-199 Vinyl chloride ug/L NO 20 21.2 106 46-176 1,2-Dichloroethaned4 (S) e/ 101 70-130 4-Bromofluorobenzene (S) a/ 96 70-130 Toluene -d8 (S) 96 70-130 SAMPLE DUPLICATE: 2134820 92361204001 Dup Parameter Units Result Result RPD Qualifiers 1,1,1 -Trichloroethane uglL NO NO 1,1,2,2 -Tetrachloroethane ug/L NO NO 1,1,2 -Trichloroethane ug/L NO NO 1,1-Dichloroethane ug/L NO NO 1,1-Dichloroethene uglL NO NO 1,2-Dichloroethane uglL NO NO 1,2-Dichloropropane ug/L NO NO 2-Chloroethylvinyl ether ug/L NO NO Acrolem ug/L NO NO Acrylonitrile ug/L NO NO Benzene ug/L NO NO Bromodichloromethane ug/L NO NO Bromoform ug/L NO NO Results Presented on this page are In Me units indicated by the'Unitc' column except when an altemate unit is presented to In. right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20 25ceAnayicale wswpecelabs.com QUALITY CONTROL DATA Project. Permit Renewal 002 Pace Project No.: 92361389 SAMPLE DUPLICATE: 2134820 Parameter Units 92361204001 Result Dup Result Bromomethane ug/L NO NO Carbon tetrachloride ug/L NO NO Chlorobenzene ug/L NO NO Chloroethane ug/L NO NO Chloroform ug/L NO NO Chloromethane ug/L NO NO cis-1,2-Dichloroethene ug/L NO NO cis-1,3-Dichloropropene ug/L NO NO Dibromochloromethane ug/L NO NO Dichlorodifluoromethane ug/L NO NO Ethylbenzene ug/L NO NO Methylene Chloride ug/L NO NO Tetrachloroethene ug/L NO NO Toluene ug/L NO NO trans-1,2-Dichloroethene ug/L NO NO trans-1,3-Dichloropropene ug/L NO NO Trichloroethene ug/L NO NO Trichlorofluoromethane ug/L ND NO Vinyl chloride ug/L NO ND 1,2-Dichloroethane-d4 (S) 100 102 4-Bromofluorobenzene (S) 100 97 Toluene -d8 (S) 106 102 RPD Qualifiers 2 3 4 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)875-9092 Results presenteci on this page are in Me unite Indicated by Me "Unita" column except where an altemate unit Is presentee to the right of Me meet. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20 2ace Analytical a saew7arelNN,. QUALITY CONTROL DATA Project: Permit Renewal 002 Pace Project No.: 92361389 QC Batch: 384949 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92361389001 METHOD BLANK 2133904 Matdx: Water Associated Lab Samples: 92361389001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 11/02/1708:25 Pace Analytical Servicas, LLC 9800 Kincey Ave. Suds,100 Huntersville, NC 28078 704)875-9092 LABORATORY CONTROL SAMPLE: 2133905 Spike LCS LCS % Rec Parameter Units Corl Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 228 91 90-110 SAMPLE DUPLICATE: 2133906 92361383001 Cup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND NO SAMPLE DUPLICATE: 2133907 92361391003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND NO Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Face Analytical Services, LLC. Page 11 of 20 PaceftVica/ a aww.panabt.com Project: Permit Renewal 002 Pace Project No.: 92361389 OC Batch: 384933 OC Batch Method: SM 52108 Associated Lab Samples: 92361389001 METHOD BLANK: 2133872 Associated Lab Samples: 92361389001 Parameter BOD, 5 day QUALITY CONTROL DATA Analysis Method: SM 52108 Analysis Description: 52108 BOD, 5 day Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mg/L ND 2.0 11/06/1720:53 Pace Analytical Services, LLC 9800 Kincey Ave. Sults 100 Hunlersville, NC 28078 704)875-9092 LABORATORY CONTROL SAMPLE: 2133873 Spike LCS LCS % Red; Parameter Units Conic. Result % Roo Limits Qualifiers BOD, 5 day mg/L 198 154 78 84.6-115.4 L2 SAMPLE DUPLICATE: 2133874 92361437001 Dup Parameter Units Result Result RPD Qualifiers HOD, 5 day mg/L ND ND D6 Results presented on this page are In the units Indicated by the 'UMW column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 20 1!2ceAnaoical a 0 N pacelabs com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 704)875-9092 Project: Permit Renewal 002 Pace Project No.: 92361389 QC Batch: 385507 Analysis Method: EPA 350.1 1993 Rev 2.0 QC Batch Method: EPA 350.1 1993 Rev 2.0 Analysis Description: 350.1 Ammonia Associated Lab Samples: 92361389001 METHOD BLANK: 2137940 Matrix: Water Associated Lab Samples: 92361389001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 11/09/17 00:36 LABORATORY CONTROL SAMPLE: 2137941 Spike LCS LCS %Rec Parameter Units Conc. Result Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137942 2137943 MS MSD 92361633002 Spike Spike MS MSD MS MSD Rec Parameter Units Result Conc. Conc. Result Result % Rec Rec Limits RPD Qual Nitrogen, Ammonia mg/L 4.8 5 5 9.6 9.6 97 97 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137944 2137945 MS MSD 92362056001 Spike Spike MS MSD MS MSD Rec Parameter Units Result Conc. Conc. Result Result % Rec Rec Limits RPD Qual Nitrogen, Ammonia mg/L NO 5 5 4.9 4.9 98 98 90-110 0 Results presented on this page are in the units indicated by the -Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, I.I.C. Page 13 of 20 21! eAnalytical a srwpacelaes.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntemville, NC 28078 704)875-9092 Project: Permit Renewal 002 Pace Project No.: 92361389 QC Batch: 386547 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Descripfiow 5220D COD Associated Lab Samples: 92361389001 METHOD BLANK: 2143913 Associated Lab Samples: 92361389001 Parameter Units Chemical Oxygen Demand mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 25.0 11/13/1719:02 LABORATORY CONTROL SAMPLE: 2143914 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 1120 751 67 90-110 L2 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2143915 2143916 MS MSD 92360409001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chemical Oxygen Demand mg/L 803 150 150 900 907 65 69 90-110 1 MO MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2143917 2143918 MS MSD 92361431002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 27.0 150 150 145 141 79 76 90-110 3 MO Results presented on this page are In the units indicated by the "Units" column except where an alternate unit la presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20 ZeAnapical' swww.penlabscom Project: Permit Renewal 002 Pace Project No.: 92361389 QC Batch: 384971 QC Batch Method: SM 53108 Associated Lab Samples: 92361389001 METHOD BLANK: 2133960 Associated Lab Samples: 92361389001 Parameter Units Total Organic Carbon mg/L QUALITY CONTROL DATA Analysis Method: SM 5310B Analysis Description: 53108 TOC Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 1.0 11/02/1716:28 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)8759092 LABORATORY CONTROL SAMPLE: 2133961 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carlon mg/L 25 23.6 94 90-110 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2133962 2133963 MS MSD 92361364001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec Rec Limits RPD Qual Total Organic Carbon mg/L 9.5 25 25 32.4 32.3 91 91 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 20 2IA- PaceAnalytical e www0acelabtoam QUALIFIERS Project: Permit Renewal 002 Pace Project No. 92361389 DEFINITIONS Pace Analytical Services, LLC 9800 Kinoey Ave. Suke 100 Huntereville, NC 28078 704)879-9092 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS 82 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated for the dilution using the most amount of sample. D6 The precision between the sample and sample duplicate exceeded laboratory control limits. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20 2cekwcalo Paoall QUALITY CONTROL DATA CROSS REFERENCE TABLE Pau Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 704)875-9092 Project: Pace Project No.: Permit Renewal 002 92361389 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92361389001 002 EPA 200.7 386674 EPA 200.7 386787 92361389001 002 EPA624 385093 92361389001 002 SM 2540D 384949 92361389001 002 SM 5210B 384933 SM 52108 384937 92361389001 002 EPA 350.1 1993 Rev 2.0 385507 92361389001 002 SM 5220D 386547 92361389001 002 SM 53108 384971 Date: 11/15/2017 07:59 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 20 Laboratory receiving samples: Asheville L] Eden Greenwood 0 Huntersville Raleigli Mechanicsville[; Courier Commercial Client Name: WO# • 92361389 L—:1for, (,,tics, %1n yF P+Y,.r Project #: III IIIIIIIIvlllllllllllL]Eod Ea UPS USPS []Client Pace Other 92381389 i L Custody Seal Present? Document Name. Document Revised August d, 7017 Nio Sample Condluon Upon Recei t(SCUR) Page 1 of 2 No Issuing Authorityc7CeAnNyftealDocument Lf Other Biological Tissue Fr all G-CARS-033-Rev.OA Pace Quality Office Laboratory receiving samples: Asheville L] Eden Greenwood 0 Huntersville Raleigli Mechanicsville[; Courier Commercial Client Name: WO# • 92361389 L—:1for, (,,tics, %1n yF P+Y,.r Project #: III IIIIIIIIvlllllllllllL]Eod Ea UPS USPS []Client Pace Other 92381389 i L Custody Seal Present? Yes []NO Seals Intact? []yes Nio Date/Initials Person Examining Contents '. I)3 ILIL Packing Material: bubble Wrap []Bubble Bags None Lf Other Biological Tissue Fr all Thermometer RGun 1O wit Type Cave Sone yes LINO N/A Short Hold Time Analysis c72 hr.7 olS1[e: 2. L9No N/A Correction Factor: Cooler Temp Corrected j'C): r/es Temp should be above freezing to 6'C N/A A. Sufficient Volume? Sampler out of remp,ter., Samples ar qe, Cooling process ONO N/A 5. has betun USDA Regulated Soils N/A, water samples ONO ONO ON/A N/A Did samples originate in a quarantine tone within the United States CA, NY, or SC (cmeck maps)? Did samples Originate from a foreign source (internationally, Yes No N/ 7. includine Hawaii and Puerto Rica Pny'es nNo CLIENT NOTIFICATION/RESOLUTION Person Contacted. Comments/Sample Discrepancy: tot iD of split containers Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? Yes No Date/Time: Date Date: is NoteWhenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form ii be sem to the North Carolina Df HNR Certification Office (i e Out of hold, incorrect preservative, out of temp, mco[rect contalners) Page 18 of 20 Commanta/Dhaepancy: 1. Chain of Custody Present/ MYeI, ONO N/A Samples Arrived within Hold Time? res O-,No N/A 2, Short Hold Time Analysis c72 hr.7 res L9No N/A 3. Rush Turn Around Time Requested? r/es No N/A A. Sufficient Volume? kL2y t ONO N/A 5. Correct Containers Used? Pace Containers Used? Y res ONO ONO ON/A N/A 6. Containers Intact?ret No N/ 7. Dissolved analysis: Samples Field Filtered? r Nn N/A a. Sample labels Match COO Includes Date/Time/10/Analysis Matrix: Yes w ON. N/A 9. Head space in VOA Vials(>5-6mmj? El yes EJNPI ON/A 10, Trip Blank Present? Trip Blank Custody Seals Present? Yes res NO ho N/ N/A 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted. Comments/Sample Discrepancy: tot iD of split containers Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? Yes No Date/Time: Date Date: is NoteWhenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form ii be sem to the North Carolina Df HNR Certification Office (i e Out of hold, incorrect preservative, out of temp, mco[rect contalners) Page 18 of 20 m 00 LZ r rO 0 e Y i Meme 0 ti w 2 eP3U-250mLPbslK UOprM"ed(N/A) 2Z Z 9P2U-SOO mL Plastic Unpresened (N/AI jw a w a V6 -12S ml Plastic I,l ION. 21 (CO Dd 0 M a 3 P42.125 mL Plastic 2N Acetate 6 NaOH (>9) w M e 0O OW -125 ml Plastic NaOH (PH a 22) ICI -I 0 O INGPU-Wide-motdbed Glass jar Unpreser d s m y Z 1L AGIN-1 bier Amber HCI (pH. 2) ton N AG341-250 ml Amber Unprese,"d INN (a) b yy ryM AGISI liter Amber H25O4 lost <2) e i AGJS-250 mL Amber HISOA (pH <2) w on69OX i AG3AIOG3A)-250 mL Amber NIMCI (N/A)(Clk) r rO 0 m1 Y Meme IPeU-125 mL PtastiC Unpmsened (N/A) (O-) eP3U-250mLPbslK UOprM"ed(N/A) 9P2U-SOO mL Plastic Unpresened (N/AI a tU-1 icier Plkstc Unprese iced (Il V6 -12S ml Plastic I,l ION. 21 (CO SP3111a-250 ml plastic HNO3 (PH c 2) P42.125 mL Plastic 2N Acetate 6 NaOH (>9) OW -125 ml Plastic NaOH (PH a 22) ICI -I INGPU-Wide-motdbed Glass jar Unpreser d AGIU-1 liter Amber Unpreferved IN/A) (CI-) AGIN-1 bier Amber HCI (pH. 2) AG341-250 ml Amber Unprese,"d INN (a) AGISI liter Amber H25O4 lost <2) AGJS-250 mL Amber HISOA (pH <2) AG3AIOG3A)-250 mL Amber NIMCI (N/A)(Clk) V_ DG9H-a0 mL VOA IICI(N/Al VGITA0 ml VOA MZS203 (N/A) VGW40 mL VOA Uro IN/AI tt `` CY DGIP-40 mL VOA 143PO4 IN/A) VOM (e trial, per kill -5035 kit (N/AI V/Ga 13 trials No Wd VPH/Gas kit IN/A) 3PST V5 mL Slarve Platt. (N/A -bb) SPIT -250 mL Sterile Pil lK (N/A -lob) N3A-750 ml Plastic INH2)2500 (9 3-9 7) zzzzzz Cubit kw VSGU 20 ml Scintillation V wls 1N/A) GN r CHAIN -OF -CUSTODY I Analytical Request Document PaeeAnalytical Tile CNalnof-Cusbdy Is a LEGAL DOCUMENT All nPevant Gents must De mmpleted accuralcly we eaLsla6L.mm Section A Section B Section C RRCyyOuhayd C111!Inlpmalion RMINrad Pm,11 In:ornu!. Inv,. Intmnal,M R,parl To pI M ` Allontw l rl.Jr{ j /OrrFI { rF ofLWF D'e.i.' CmrpA, N. YOW eA J..r.. SA..gd RG Cn9y TD REGULATORY AGENCY Ad&o,,s 51111 A•G E'itdo ToS [.ii/ej,„ PDES GROUND WATER ORINKING WATER UST RCRA OTHER 6nae To Pu¢nax-On4r No rx"owx' H1r v T:n M1getl Nunes P.r.V"w¢' SIN L.Uw STATE: Requeatod Due DMoi,TAT: tAm,d Numb. r""r"^"" Requested Analysis Filtered YIN) S Am D Matrix Cedes AT._ r_nnr S 8 COLLECTED PreservaIWS tL Per hL DUnxrr.l Wavr DW W.ncr WT zIju 4 Wase Wme WW RW,rrl V m couoop.e c`wsIILFcrAlr w O lti I SnIVSrwU SL m y ri en a SAMPLE ID at a V x ftm WP IAd. 09..a Air AR 2 F 2; 6:rnrVlt IDs MUST BE UNIDUE Tgyc IS DO., oT Cx w ww 0 EeN o ' 4 U a 2a U 30 O Oil 8wgzUUmm 2 f s Q r V IT Pete P No./ Lab I.D. DATE TIME DATE TIME n O i S 2 2 1 O O 1. G F•/./17 o7sil 13 1 1.1 1 1 1• I 2 00,, G r7 07s -.r eoi- G Td/.7 awls- I r 007 G rI/./.7 eur 1 6 007- L h7 o rr 6 oei 1./ 7 0>rr T 601 G NIrlf7 OFri f e 9 10 11 12 ADDITIONAl. COMMENTS RELINIX11511ED BY I AFFILIATION DATE TIME ACCEPTED BY I AFRLIATIOI. DATE TIME SAMPLE CoNDn"C"S 16F G, C4..e. /rPli I./Ir7 os r I' 3u q- 7/) IV 1 SAMPLER NAME AND SIGNATURE u S e E LI PRINT Name of SAMPLER. Guy' O Co SIGNATURE W SgYPLFA: /y G! DATE Si — IR Evi4/17B Y^1xarL 1 .'rnl Rn X.myes.v,'.6.yMIP.xv'. NL11p 61y P'rPrmm kYnrs Yd agex/gm Nm cR Te:d 15`: pn mmNln.H•y Nrm.wnx, )n M1r.s F -ALL -0-020r LT. 15-M2 2ceAna0ca1a awwpKaltlta0m November 22, 2017 Mr. Guy O'Connor Electric Glass Fibers of America, LLC 940 Washburn Switch Road Shelby, NC 28150 RE: Project: CTAS Resample - Permit Renewal Pace Project No.: 92362439 Dear Mr. O'Connor: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvills, NC 28078 704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 08, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, axq£Q, 4Y1- `$cuam Angela Baioni angela.baioni@pacelabs.com 704)875-9092 Project Manager Enclosures cc: John Littlejohn, Electric Glass Fibers of America, LLC Mr. Richard Young, Electric Glass Fibers of America, LLC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Seroces, LLC. Page 1 of 6 Laboratory receiving samples: Asheville Eden Greenwood Huntersville[]' Raleigh Mechanicsville Client Name: WO# : 92362439Projects ps 111111IIIIIIIICourier: fed Ex UPS USPSSPS Client Commercial e OtnerIIIIIIII 92362439 Custody Seal Present? Yes Jam° Seals intact? []Yes ..No Date/InnlaK Person Examining Contents: Packing Material: []Bubble Wrap Bubble Bags IDNdne Other Biological Tissue Frozen? Thermometer: I Yes_-qN0 []N/A lit Gun ID: I I l o I Type of lea: Wet 91ue []None Correction Factor: Cooler Temp Corrected ('Cj: Temp should be above freezing to 6Y Samples out of temp Cniena Samples on ice, cooling process hasbelun USDA Regulated Soil N/A, water sample) Did samples origin a in a quarantine zone within the United States U, NY, or SC (check mapsi7 Did samples originate from a foreign source (internationally, MYes n. mtludlne Hawaii and Puerto RICOI? ayes Died Document Name: Document Revised: August a, 2017 comments/Oisne anry: Chain of Custody Present? V Sample Condition Upon Recei t(SCUR) Pae 1 or 2 1. Document No.: Issuing Authority: Dive aCeAnalybcal 2, Short Hold Time Analysis 1<72 hr.)? Yes f-CAR-CS-033-Rev.04 Pace Quality Office 3. Laboratory receiving samples: Asheville Eden Greenwood Huntersville[]' Raleigh Mechanicsville Client Name: WO# : 92362439Projects ps 111111IIIIIIIICourier: fed Ex UPS USPSSPS Client Commercial e OtnerIIIIIIII 92362439 Custody Seal Present? Yes Jam° Seals intact? []Yes ..No Date/InnlaK Person Examining Contents: Packing Material: []Bubble Wrap Bubble Bags IDNdne Other Biological Tissue Frozen? Thermometer: I Yes_-qN0 []N/A lit Gun ID: I I l o I Type of lea: Wet 91ue []None Correction Factor: Cooler Temp Corrected ('Cj: Temp should be above freezing to 6Y Samples out of temp Cniena Samples on ice, cooling process hasbelun USDA Regulated Soil N/A, water sample) Did samples origin a in a quarantine zone within the United States U, NY, or SC (check mapsi7 Did samples originate from a foreign source (internationally, MYes n. mtludlne Hawaii and Puerto RICOI? ayes Died CUENT NOTIFICATION/RESOLUTION Person Contacted. Comments/Sample Discrepancy: Los 10 of split containers. Project Manager SCURF Review: Date/time: Date: Field Data Requlred? Utes UND Project Manager SRF Review: Date: Note whenever then is a discrepancy affecting North Carolina compliance Sampks, a copy of this farm will be sent to the North Carolina DEHNR Certification Office (,.e. Out of hold, riconect pn1ervattse, out or temp. mcorrect containers( Page 2 of 6 comments/Oisne anry: Chain of Custody Present? V rINO nNJA 1. Samples Arrived within Hold Time?Yes Dive N/A 2, Short Hold Time Analysis 1<72 hr.)? Yes o ON/A 3. Rush Tum Around Time Requested? res o N/A 4. Sufficient Volume? es i]Np N/A 5. Correct Containers Used? Pace Containers Used? es es NO NO N/A ON/A 6. Containers Intact?es no N A 7. Dissolved analysis: Samples Field Filtered? M A B. Sample Libels Match COC? Includes Date/Tlme/ID/Anal is Matrix: Elyes No N/A 9. Heads ace In VOA Vials (a5-6mm)? yes No lYl< 1 10. Trip Blank Present? Trip Blank Custody Seals Presents Yes r1yes rImo N/A A Il. CUENT NOTIFICATION/RESOLUTION Person Contacted. Comments/Sample Discrepancy: Los 10 of split containers. Project Manager SCURF Review: Date/time: Date: Field Data Requlred? Utes UND Project Manager SRF Review: Date: Note whenever then is a discrepancy affecting North Carolina compliance Sampks, a copy of this farm will be sent to the North Carolina DEHNR Certification Office (,.e. Out of hold, riconect pn1ervattse, out or temp. mcorrect containers( Page 2 of 6 ni W Cr0 nN L O r 0Y Y1+ NN 4J 0 V P1 O 33 11em1 0 s 1114U-125 ml Plastic Unproserved (N/A) (Cl.) w' P3U-2SO mL Plastic Unyrescrved (N/A1 w i 8 v PIU -1 Ater Plastic Unpresnraed IN/AI D 1lP4S-125 mL Plasli H2SO4 ION c 2) (Cl ) a O M P;Iil ml plasM HNO3 ION c 2) Sn 3 P42-125 mL Plash IN ACIta1e & WON 1>91 w NX2aat i w 6C Q1 es AG1U-1 blew Amber Unpresemad IN/A1 [Cl.) NA A151W) Ater Amber HCl (OH < 21 v n n AGJU-250 mt Amber Unpmsemed IN/AI ICI.) a39 o N w v AG3A(OG3A1-250 mL Amber NH4C1 (N/AIICI-) 2 nc DGSH 40 mL VOA IICI IN/A) e s Cr0 nN L O r 0Y Y1+ NN 4J 0 V P1 O 11em1 1114U-125 ml Plastic Unproserved (N/A) (Cl.) P3U-2SO mL Plastic Unyrescrved (N/A1 611`21.1400 mL PlastiC Unpreserved IN/A) PIU -1 Ater Plastic Unpresnraed IN/AI 1lP4S-125 mL Plasli H2SO4 ION c 2) (Cl ) P;Iil ml plasM HNO3 ION c 2) P42-125 mL Plash IN ACIta1e & WON 1>91 W -12S mL Plastic NaOH ION o 12) (Cl.) WGPU-Wide-mouxbes Glass lar Unprese,imd AG1U-1 blew Amber Unpresemad IN/A1 [Cl.) A151W) Ater Amber HCl (OH < 21 AGJU-250 mt Amber Unpmsemed IN/AI ICI.) AGIS-1 liter Amber H2504 (PH c 2) AGIIS450 ml Amber H2504 ION c 21 AG3A(OG3A1-250 mL Amber NH4C1 (N/AIICI-) DGSH 40 mL VOA IICI IN/A) VG9Td0 mt VOA Na2S203 IN/A) VG9UJ0 mL V0A Uny (N/A) OG9P-40 ml VOA H3PO4 (N/A1 VOAK I6 rials per kis)-5035 bl (N/A1 V/GK 13 wk ON MI-VPH/Gas kit IN/A) SPST-12S mL SWriIe Plast¢ (N/A - lab) SP2T-2SO mL Sterile Plastic (N/A -lab) A1_1 z KPM-250 ml Plastic (NH2)2504 (93.9.7) Culma irw VSGU 20 mL Scmueatipn Vlals (N/A) GN Cr0 nN L O r 0Y Y1+ NN 4J O CHAIN -OF -CUSTODY 1 Analytical Request Document m PaceAnalytical The Chun-o(.Custady is a LEGAL DOCUMENT All retevam fielus muss De competed accurawi, O a NI.Nm.roe 0 Section A Serlion 8 $eC110F1 C ra•R/rn Page: I o1 a Requkao Cbenl Inbn',Vo R"UIne Pm t lnlorm.no• InVeK.e Inloi Noo leafi:c t:4.F F•6. ,f A.e.w R°pnn ro R...2 %+t MtEminn Addluv cony Ta Cr ,pah, Name 61u o'Cis—, REGULATORY AGENCY T;tOldy /t.L .Tante. Sal+ (,iillf( A°°Oef PDES GROUNDWATER DRINKING WATER UST RCRA OTHER Emw To Pu.rsc O.d:r No M+' rarnvan nF Prada Name .r PniPaw^Vd 7q - YiiF-]2]ylf *vaav SNe LocHbn STATE: A LReaeoetooDIMDaAT: Is ojeel Nun•EEr P..,r Prmk 1 Requested Analysts FiMemd YIN) soEtlen D ram. coeds R.mrwcwrrrl rImm+..r• w11Pla cmc P 7- COLLECTED Preservatives t UrcNmg Waley DW Winer WT4t3u ZZ Wa31e WaNr WIN SIE rpMlpnE rP n'} RMhe. P 1 S1Mi ENCLI/A W Z r p5uV5oYE SL SAMPLE ID 6}J o w a fEt4^ p e twrPevP In.z o -u .I N. AR 2 Samek IDa MUST BE UNIQUE TMsue TS OINeI OT OU Z TIT,., M e toI TOATETIM i S 2 2 Oz2 Pap PrOOO NI Lab I.D. 1 3 7 M S 6 7 8 B 10 11 13 AOpl10NAl COIMIErm RELINQUISHE D BY AFFILATION DATE TMIE ACCEPTSP BY I AFFIJATKAi DATE TIME SAMPLE CONDITgNS F*, Ake r.. r e rb..er iPP& I. !r7 A> 6.k 2114 SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: SIGNATURE M SAMPLER: DATE Spnod s /r% IMMIDDIYYI' q Fenny— ynr.rrr.,y,'... •I P.., NEI n JLWIi +e rnw..0 w..+.mmin. a.'.,End 1 v..ry+.w,mvm ALL-0-030sev 07. 1 i RESEARCh & /ANAlyTICAI LAbORATORIES, INC@ For: Pace Analytical-Huntersville 9800 Kincey Avenue Suite 100 Huntersville, NC 28078 Attn: Angela Baioni Report of Analysis 11/21/2017 11111111#14,,, GAS, RikY%Tc'h,, tu;c 2 'Co NC #34 z. - NC 1137701 4 Z 0 AIA Client Sample ID: Effluent Lab Sample ID: 42542.01 Site: Pace -Huntersville Collection Date: 11/8/2017 8:00 Parameter Method Result Units Rep Limit Analyst Analysis Date/Tlme CTAS SM5540D <0.4 mg/L 0.4 DW 11/9/2017 1530 NA = not onolyzeo P.O. Boz 473 106 Short Street Kemersville, North Carolina 27264 Tel: 336.996.2841 Fax 336-996.0326 www randalabs corn Page t Page 5 of 6 C....n of Custody aceAnalyt) www.p°cebe Workorder: 92362439 Workorder Name: CTAR Re on I Invoice To a Subcontract 70 mubuns nequestlea t3y: l l/GL/ZLU9 Angela Baioni Re uested Anal sis Pace Analytical Charlotte QHLabsP.O. v egg al9800KinceyAve. Suite 100 Huntersville, NC 28078, 01 -- Phone(704)875-9092 Email: angela.baioni@pacelabs.com' State of Sample Origin: NC 3 In _ 9 q `'o dT, -1 I Preserved Containers Item sample Collect a ID DateRme Lab ID Matrix i Effluent 11181201706:00 92362439001 Water X LAB USE O 2 y 54- 7— Transfers Released By Date/Time Received By Date/Tlme Comments 1 2 3 Cooler Tem erature on Recei t C Custody S Itir N T Received on Ice Y or N Samples Intact Y or N F -FAS Tv R2ewE rn Wednesdav, November 08. 2017 1252:03 PM FMT-ALI 241VIarch2009 P,,, _ r AFFIDAVIT OF INSERTION OF ADVERTISEMENT The Star Shelby, N.C. Cleveland County The Star does certify that the advertisement for: PUBLIC NOTICE North Carolina Environmental Management Commission! NPDES Unit 1617 Mail Service Measuring 8.45 inches appeared in The Star, a newspaper published in Cleveland County, Shelby, N.C., in issue(s): 04/21/2021 Name of Account: NCOENR—DWR— Star Account Order Number: 54608511 Ad Number: 54750645 Sworn to, and subscribed before me this 21 st day of April, 2021. /71/'&7 Print Name (ClassifieRepresentative) Signature (Classified R tutfikadluit. 6 IL lQ`�I:•Ta/rh � �Stephanie B. Sisk, Notary Public Commission Expires March 23, 2025 1.1:1rrr rrr' v t' AND . : PUBLIC NOTICE • 'North Carolina Environmental Management Commission/ NPDES Unit 1617 Mall Service Center Rale&gh, NC 276943-1617 Notice of Intent to ls&ue a NPDES Wesley/Wet Per- mit NZr3d)4685 Electric Glass Fiber America. LLC. The North Carottria Environments! s) Commission proposes to Js5Ji a NPDES wastewater age permit to the persons) listed below Writ- ten Sad comments averting the pry penny it be accdays Rear the publish date of this Di Doke. The rector of the NC Division of Water Re- sources PM) may hold a pubic hearing should there be a esiniricant degree C%r pvbfit: Oiliest. mai l ail comments audio- - oration requests to DWR et the above address. Interested persons mil the DWR ar 512 N. Safibury Street Re- Fi igh. NC 27804 to review Vitae -nation on Re Add,. tonal Infodmtion on HPDES peeves arei this notice may De found on our wlgbsiler arras urcasAvate: oscines -perm Weastewater-bregr as vestemier gaalc-hotigas ,or by vatting E Fiber Arnerral LLC{9j940 Washburn Sweet' Road Sl-ietky. NC 28150] has u s1ad rt* news! of NPDES permit N00004€85 for its Shety Family Wags water Treatment Mien), located in Ceveland County. This pairniad facility dcyt ipes keeled mart:opal and industrial wastewater to Brush Creek and Oveil iw Branch. class C waters in the Broad Rrvur Resin Same of fie parameters in the perrnh ate wafer Mislay limited This discharge may affect future all:tcabons in this ssymeri of me &cad River, 4.21. 2021 54608511 l!i Nippon Electric Glass Electric Glass Fiber America, LLC 940 Washburn Switch Road, Shelby, NC 28150 Telephone Number: 704-434-2261 Via Certified Mail Return Receipt Requested May 19, 2021 Ms. Julia Byrd NC DEQ Division of Water Resources WQ Permitting Section -NPDES Industrial Permitting, Wastewater Branch 161 7 Mail Service Center Raleigh, NC 27699-1617 Subject: Dear Ms. Byrd: Draft NPDES Permit Renewal Comments Permit NC0004685 Electric Glass Fiber America, LLC, Shelby, N.C. Facility Cleveland County Electric Glass Fiber America (EGF A) received the draft NPDES permit and fact sheet on April 29, 2021 for the facility located at 940 Washburn Switch Road, near Shelby in Cleveland County. After review of the Draft Permit package, EGF A has the following questions or comments: On Page 2 of 9 of the Draft Permit, the listed wastewater treatment facility component description has a few components either missing or incorrect. There have been no component changes from the current permit, so we respectfully request Item I on Page 2 of 9 to read as follows (changes are shown in Italics): "Item I. Continue operation of a 1.3 MGD wastewater treatment facility consisting of the following components: •An overflow/storage basin [add component}; •Bar screen and grinder; •An influent wet well with lime addition [ Component name change]; •Influent pwnps;•A surge tank [add component],· Page1J3 l!i Nippon Electric Glass Electric Glass Fiber America, LLC 940 Washburn Switch Road, Shelby, NC 28150 Telephone Number: 704-434·2261 •One (1) load equalization tank with aluminum chloride addition ["and coagulant" removed}; •One (1) prima,y flash mix tank with polymer addition; •Two (2) primary clarifiers; •Two (2) aeration basins with lime, bentonite clay and defoamer addition ["hydrogen phosphate" removed, "bentonile clay" added};•One (1) Secondary Flash Mix Tank with ferric chloride and polymer addition [component added} •Three (3) secondary clarifiers ["with ferric chloride and polymer addition" removed]; •One (1) Aeration Splitter Box for Return Activated Sludge [''flow splitter for waste and return activated sludge" removed}; •One (1) sand filter {"with defoamer addition" removed}; •One ( 1) effluent holding tank ['for reuse/cooling water" removed}; •One (1) sludge thickener tank; and •One (1) sludge belt press with polymer addition." 2.EGF A respectfully requests justification for leaving the fluoride-monitoring requirement in the permit. Use of fluoride as an ingredient was discontinued at this facility circa 2003. Fluoride is still occasionally detected in the wastewater discharge, as it is present as a trace contaminant in the facility raw materials (dolomitic limestone), and in city water used in plant operations, but at a much lower level than historical records indicate, when it was a formulation component. Over the last two years (2019 -2020), fluoride in the effluent has been well below 1.0 mg/L and was typically near non-detect concentrations. As discussed on Thursday, May 6, 2021, EGF A believes there is a typographic error by omission on Part IA.(1.)a, Footnote 3 regarding Total Residual Chloride (TRC) monitoring. Page 6 on the Draft Permit Fact Sheet indicates no planned changes to the TRC limits for this permit renewal, however in the draft permit at Part IA.(! .)a Effluent Limitations and Monitoring Requirements the wording of Footnote 3 regarding TRC has been modified by omission of one sentence. EGF A respectfully requests reinstating the missing sentence into the new permit. For your convenience, this revises Footnote 3 in the above referenced table to read as follows: "The Division shall consider all effluent Total Residual Chlorine values reported below 50 ug/L to be in compliance with the permit. However, the permittee shall continue to record and submit all values reported by a North Carolina certified laboratory (including field certified), even if these values fall below 50 ug/L. Monitoring and Page213 3. l!i Nippon Electric Glass Electric Glass Fiber America, LLC 940 Washburn Switch Road, Shelby, NC 28150 Telephone Number: 704-434-2261 effluent limitation for TRC apply only if chlorine is added for disinfection." (Italics show the omitted sentence). In the NPDES permit application filed in 2017, EGF A requested deletion of the PC2 operator requirement, which was granted in the draft permit. Based on the discussions on May 6, 2021, EGF A understands that the DWQ received a comment that this determination is made by the NC DEQ Regional Office. EGF A will proceed with making this request to the Regional Office by May 19, 2021. Please note that DWQ rescinded the PC2 classification in 2015 for the EGF A, Lexington, NC wastewater treatment plant, which is comparable to this plant. EGF A respectfully requests that DWQ not issue the new NPDES permit until this matter has been addressed with the Regional Office. In the NPDES-Fact sheet there is a typographic error on Page 7 of 12. EGF A requests deletion of "and 002" describing the current toxicity testing requirement. The fact sheet indicates no changes are proposed to the current permit. The current permit requires chronic toxicity testing only at outfall 001 @ 33% effluent concentration. Please feel free to contact Terry Steinert at 704-434-2261 x22007 if you need any additional information or if you have any questions regarding this submittal. Alan Toney Manufacturing Manager Electric Glass Fiber America, LLC. Attachment cc: Richard Young, EGF A Terry Steinert, EGF A File Page3l3 May 25, 2021 Mr. Richard Young, Focus Factory Manager Electric Glass Fiber America, LLC 940 Washburn Switch Road Shelby, North Carolina 28150 Subject: Response to Permit Renewal Comments Permit NC0004685 EFGA, LLC, Shelby Facility Cleveland County Grade III Biological, PC II WPCS Dear Mr. Young: The Division received the letter from Electric Glass Fiber America (EFGA), dated May 19,2021, regarding the draft NPDES Permit NC0004685. Please see responses to the questions and comments summarized below: 1. The permitted 1.3 MGD treatment system description was updated to reflect current components operating at the facility [See the Supplement to Permit Cover Page (1.)]. 2. EGFA requested that the fluoride-monitoring requirement be removed from the permit since use of fluoride as an ingredient was discontinued at the facility in 2003. Based on results of the RPA conducted with this permit renewal, fluoride demonstrated a maximum predicted concentration greater than 50% of the allowable concentration, and therefore the quarterly monitoring requirements for fluoride in the current permit will continue. Please see the RPA sheets attached to the Fact Sheet. 3. The typographical error by omission regarding Total Residual Chlorine (TRC) monitoring in Part I A (1.) (a.), Footnote 3, was corrected [See A. (1.)]. 4. The dual classification of Grade III biological and physical/chemical grade II WPCS is maintained in the reissued permit, per 15A NCAC 08G .0306. Please see the Division responses regarding this request attached to the Fact Sheet. From:Tuvia, Ori A To:Byrd, Julia Cc:Kinney, Maureen; Basinger, Corey; Pitner, Andrew Subject:RE: [External] EGFA Comments RE: [EXT] Draft Permit for Electric Glass Fiber America LLC, NC0004685 Date:Friday, May 21, 2021 11:08:24 AM Good Morning Julia Reviewing the request I believe that the facility should remain a PC II designation, They still have active chemical treatment units and based on the flow and size of the plant It seems appropriate. Thank you, Ori From: Young, Richard [mailto:Richard.Young@neg-us.com] Sent: Wednesday, May 19, 2021 3:17 PM To: Byrd, Julia <julia.byrd@ncdenr.gov>; Tuvia, Ori A <ori.tuvia@ncdenr.gov> Cc: Toney, Alan <Alan.Toney@neg-us.com>; Hale, Kenneth <Kenneth.Hale@neg-us.com>; Steinert, Terry <terry.steinert@neg-us.com>; Littlejohn, John <John.Littlejohn@neg-us.com> Subject: [External] EGFA Comments RE: [EXT] Draft Permit for Electric Glass Fiber America LLC, NC0004685 CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Good afternoon, This email is in response to the Draft NPDES permit NC0004685 for the Electric Glass Fiber America LLC. Shelby Facility. Find in attachment two letters that are being mailed hard copy to both of you. One letter contains comments in regard to the Renewal Permit and the other letter is addressed to Mr. Tuvia requesting the facility’s PCII classification be remove while the permit is open. Please feel free to contact Terry Steinert or myself if you have questions or need additional information regarding this submittal. Kind regards, Richard Young Focus Factory Manager Fiber Prep / Waste Water / Solid Waste NEG Shelby Plant – 940 Washburn Switch Road, Shelby, NC 28150 T: +1 (704) 434-2261 | M: (704) 477-6409 Richard.Young@neg-us.com This e-mail transmission contains information that is intended to be private and confidential. It is intended only for the addressee. If you received this e- mail in error, please do not read, copy or disseminate it in any manner. Please reply to this message immediately by informing the sender that the message was misdirected and/or received in error. After replying please erase it from your computer system. From: Byrd, Julia <julia.byrd@ncdenr.gov> Sent: Monday, April 19, 2021 3:04 PM To: Young, Richard <Richard.Young@neg-us.com> Subject: [EXT] Draft Permit for Electric Glass Fiber America LLC, NC0004685 CAUTION! This is an EXTERNAL email originated from outside the organization. Do not click links or open attachments unless you recognize the sender and know the content is safe. Good afternoon, Please see the following links to review the draft permit and cover letter, and see attached to review the fact sheet for NPDES permit NC0004685 for the Electric Glass Fiber America LLC. Shelby Facility WWTP. I have also provided a link to the NPDES Standard Conditions for your reference. The 30-day public notice period to comment, ask questions, or request an extension to review this draft permit ends on 5/20/2021. The EPA comment period ends on 5/28/2021. Please contact me with any comments you might have. You can reach me via email or feel free to call 202-550-0606 Draft Cover Letter and Permit: https://edocs.deq.nc.gov/WaterResources/DocView.aspx? id=1723613&dbid=0&repo=WaterResources Renewal Application: https://edocs.deq.nc.gov/WaterResources/DocView.aspx? id=643705&dbid=0&repo=WaterResources NPDES Standard Conditions: https://bit.ly/3k5NFaL Thank you! Julia Byrd Environmental Engineer **Email preferred during this State of Emergency** NC DEQ / Division of Water Resources / Water Quality Permitting NPDES Industrial Permitting, Wastewater Branch 919 707 3707 office 919 707 9000 main office julia.byrd@ncdenr.gov Physical Address: 512 North Salisbury St.,Raleigh, NC, 27604 Mailing Address: 1617 Mail Service Center, Raleigh, NC, 27699-1617 Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties NEG-US CONFIDENTIALITY NOTICE: This email (including any attachments) is intended for the sole use of the intended recipient/s and may contain confidential information, which also may be legally privileged. Any reliance upon, access to, review, disclosure, copying, forwarding or other distribution of any or all of the contents in this message by others who are From:Kinney, Maureen To:Byrd, Julia; Thomas, Zachary T; Moore, Cindy; r4npdespermits@epa.gov Cc:Basinger, Corey; Templeton, Mike Subject:RE: Draft Permit for Electric Glass Fiber America LLC, NC0004685 Date:Tuesday, April 20, 2021 9:14:11 AM Attachments:image001.png Julia, FYI…This permit is dual classified as WW-III and PC-II. This isn’t notated in the draft letter or permit. Maureen From: Byrd, Julia <julia.byrd@ncdenr.gov> Sent: Monday, April 19, 2021 2:49 PM To: Kinney, Maureen <Maureen.Kinney@ncdenr.gov>; Thomas, Zachary T <zachary.thomas@ncdenr.gov>; Moore, Cindy <cindy.a.moore@ncdenr.gov>; r4npdespermits@epa.gov Cc: Basinger, Corey <corey.basinger@ncdenr.gov>; Templeton, Mike <mike.templeton@ncdenr.gov> Subject: Draft Permit for Electric Glass Fiber America LLC, NC0004685 Good afternoon, Please see the following links to review the draft permit and cover letter, and see attached to review the fact sheet for NPDES permit NC0004685 for the Electric Glass Fiber America LLC. Shelby Facility WWTP. I have also provided a link to the NPDES Standard Conditions for your reference. The 30-day public notice period to comment, ask questions, or request an extension to review this draft permit ends on 5/20/2021. The EPA comment period ends on 5/28/2021. Please contact me with any comments you might have. Thank you! Draft Cover Letter and Permit: https://edocs.deq.nc.gov/WaterResources/DocView.aspx? id=1723613&dbid=0&repo=WaterResources Renewal Application: https://edocs.deq.nc.gov/WaterResources/DocView.aspx? id=643705&dbid=0&repo=WaterResources NPDES Standard Conditions: https://bit.ly/3k5NFaL