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WQ0001346_Residual Annual Report 2020_20210228
I -q;p-Pd alr , nv-p-, t'Monroe North Carolina RESIDUALS LAND APPLICATION PROGRAM CITY OF MONROE ANNUAL REPORT 2020 PERMIT NUMBER WQ0001346 RPrP:lVPF) FEES 2 8 2021 jr Monroe North Carolina City of Monroe Water & Wastewater Residuals Land Application Program 2020 Annual Report Table of Contents 1. Certification Form & Annual Operations Summary 2. Annual Residual Sampling Summary Forms & Biosolids Analysis 3. TCLP Analysis 4. Field Summary Forms 5. Pathogen Reduction & Vector Attraction Reduction 6. Soil Analysis ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0001346 County: Union Year: 2020 Facility Name (as shown on permit): City of Monroe Land Application Operator: Ken Morris, Land Residual Coordinator Phone: 704-282-4679 Land application of residuals as allowed by the permit occurred during the past calendar year? �J Yes LJ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Total number of application fields in the permit: 35 Total number of fields utilized for land application during the year: 10 Total amount of dry tons applied during the year for all application sites: 619 Total number of acres utilizes for land application during the year: 135.3 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. RJ Yes El No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. ' Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." // �-- Russell Colbath, P.E., Water Res. Director C:7 " �J Permittee Name and Title (type or print) Signature of Permittee Date Sign ture of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1 102 (26) DENR FORM ACF (12/2006) OPERATION SUMMARY Permit # WQ0001346 FIELDS USED IN 2020 �� •, � n� n rrr.,. rr-' inn• n � _jm � �ii-iYii•IiYi---�- • • 5 •\ • � \ C I © 1 ' ��---mil®-�® -- ---------- ---------- ---------- ---------- ---------- ---------- ---------- ---------- ---------- ---------- Totals 135.3 �00 1,584 1,470 275.54 343.69 Total Gallons 0 Total Yards 3,054 Total Dry Tons 619.23 WWTP- Metric Tons 249.92 WTP- Metric Tons 311.72 Total Metric Tons 561.64 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0001346 Facility Name: Residual Source WQ # or NPDES #: WWTP Name: Residual Analysis Data City of Monroe NCO024333 Monroe WWTP (cake) Laboratory: 1) 2) 3) 4) 5) Contract Labs Parameter (mg/kg) Cone. Limit (mg/kga Sample or Composite Date 1-6-20 4-1-20 4-16-20 5-18-20 7-1-20 7-22-20 8-12-20 10-5-20 Percent Solids (%) NA 15.7 13.7 13.8 15.5 17.7 19.3 23.9 20.5 Arsenic 75 11.6 8.32 8.7 16.3 10.1 8.03 14.5 11 Cadmium 85 0.949 <0.730 1.05 1.95 0.915 1.01 0.828 1.28 Copper 4,300 371 304 319 394 306 298 473 355 Chromium NA 79.6 55.5 62.5 158 72.9 67.9 106 86.3 Lead 840 23.9 17.2 19.7 13.6 19.8 18.4 20 21.4 Mercury 57 0.847 0.48 0.498 0.17 0.43 0.544 0.448 0.309 Molybdenum 75 17.3 15.5 15.7 31.2 14.2 14.7 17.7 18.2 Nickel 420 104 73.7 75.4 52.6 63.3 64.8 70.3 70.7 Selenium 100 6.62 4.96 4.83 3.5 4.73 4.17 <2.09 <2.44 Zinc 7,500 1110 964 1010 505 847 803 795 1010 Total Phosphorus NA 25500 19000 20700 11700 18200 18200 16700 25200 TKN NA 56900 68900 62700 36100 49400 42500 33800 52200 Ammonia -Nitrogen NA 2320 9640 8550 P4740 3210 4120 2120 1870 Nitrate and Nitrite NA 65 81.8 65.269 124 164 91.6 178 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0001346 Laboratory: 1) Facility Name: City of Monroe 2) Residual Source NCO024333 3) NPDES # or WQ#: 4) WWTP Name: Monroe WWTP (cake) 5) Residual Analysis Data Contract Labs Parameter (mg/kg) Sample or Composite Date 1-6-20 4-1-20 4-16-20 5-18-20 7-1-20 7-22-20 8-12-20 10-5-20 Potassium 1690 1660 1880 1560 1790 2080 1820 2560 Sulfur 11500 11500 12500 6120 9040 9330 7950 9510 Calcium 18900 16500 17700 9030 14500 14900 12100 15500 Magnesium 2500 2160 2340 1520 2150 2200 1810 2240 Sodium 510 737 855 716 633 741 628 732 Iron 54100 33900 38700 205000 59300 56500 78200 71700 Aluminum 13100 9710 11000 11300 12900 11700 12100 16500 Manganese 2020 1610 1800 974 1590 1490 1440 1720 Organic N 54600 59300 54100 31400 46200 38400 31700 50200 pH ( standard units) 6.9 7.7 7.9 6 7 7.4 6.7 6.2 Volitile Solids % 62.1 65 64.6 45.8 58.8 59.2 54.7 56.4 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." )/,P�/tea}, Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0001346 Laboratory: 1) Facility Name: City of Monroe 2) Residual Source WQ # or NCO024333 3) NPDES #: 4) WWTP Name: Monroe WTP (cake) 5) Residual Analysis Data A & L Eastern Lab. Inc. Parameter Conc. Limit k a11-6-270 Sample or Composite Date 4-1-20(mg/kg)m 7-1-20 10-5-20 Percent Solids (%) NA 28.5 20.5 31.5 33.4 Arsenic 75 24.5 24.4 32.1 17.2 Cadmium 85 5.96 <2.44 2.21 5.48 Copper 4,300 335 461 394 395 Chromium NA 193 269 228 219 Lead 840 6.21 8 <4.76 <0.898 Mercury 57 < 0.0547 <0.0741 <0.0485 <0.0476 Molybdenum 75 41.8 55.6 42.9 46.7 Nickel 420 24.7 45.3 37.8 35.9 Selenium 100 < 8.77 < 12.2 <15.9 <7.49 Zinc 7,500 178 56.6 168 140 Total Phosphorus NA 1940 2990 3330 2530 TKN NA 19300 17200 12500 18800 Ammonia -Nitrogen NA 695 1410 317 431 Nitrate and Nitrite NA < 16.6 < 22:5 28.4 <14.5 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer dl?Vl ao>) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0001346 Facility Name: Residual Source NPDES # or WQ#: WWTP Name: Residual Analysis Data City of Monroe NCO024333 Monroe WTP (cake) Laboratory: 1) 2) 3) 4) 5) Contract Labs Parameter (mg/kg) Sample or Composite Date 1-6-20 4-1-20 7-1-20 10-5-20 Potassium 509 299 208 238 Sulfur 2560 2440 2190 2270 Calcium 2640 1900 2010 1950 Magnesium 663 433 352 404 Sodium 198 < 610 <397 <374 Iron 315000 376000 310000 311000 Aluminum 5090 9070 5300 4790 Manganese 884 417 470 829 Organic N 18600 15800 12200 18400 pH ( standard units) 6 5.5 5.7 5.9 Volitile Solids % 35 34 34.6 36.5 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." I� J�— ,4120a1 Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) City of Monroe Reports of Lab Analysis 1 St Quarter (2) WayPAo i nt . NALYTICAL 46205 City of Monroe Steve Holden Project RAS 775 Treeway Dr Information Monroe , NC 28110 Report Number : 20-007-0015 REPORTOFA Lab No : 70096 Sample ID : RAS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Date : 01/13/2020 Received : 01/07/2020 Pam« IV G � VALY.4I5 Pauric McGroary Agronomist Matrix: Solids Sampled: 1/6/2020 8:09 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Moisture 58.7 % 0.010 1 01/08/20 17:28 ADM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 41.3 % 0.010 1 01/08/20 17:28 ADM SM-2540G Total Volatile Solids 62.3 % 0.010 1 01/08/20 17:28 ADM SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 3 of 5 SAMPLE TRANSM A&L F, 7621 Whitemne R 1111CIN �11111 Hill 11111111 1Hill] o � zA QS RAS 1J1819 Office Information uuscomer imormauon Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 shol-drrnu ntnnrocne.11r`, Lab Nurnber (Lab Use Only) Sample ID Container Type Sampled Date: — — Date Recd: RA Glass (`Fes or No) Sampled Time: ;�q Time Recd: Plastic (Yes or" Sampled By: jg- ,) *A_) Recd By: elinquished Signature) Date Time Received By: (Signature) Date Time Please Place a "X" by Desired Tests Internal Lab Code: Solids % TKN P K S Ca Mg Na Fe At Mn Cu Zn NH4-N NO3-N X Cd Cr Ni Pb As Hq Se pH CaCO3 E . % Volatile Solids % Org-N Mo CI B Ba X SO4 Ag Sb Co Sn Ti V Be ALK SS Avail P Sol K Cond WIN SOL B SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH Ca0 CaCO3 M CO3 MgO C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page 5 of 5 0 WayPoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Steve Holden Project WWTP Cake Report Date : 01/15/2020 775 Treeway Dr Information : Received : 01/07/2020 Monroe, NC 28110 Pauric McGroary Report Number: 20-007-0013 REPORTOFANALYSIS Agronomist Lab No : 70094 Matrix: Solids Sample ID : WWTP Cake Sampled: 1/6/2020 8:20 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 84.3 % 0.010 1 01/09/20 18:31 ADM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 2320 mg/Kg - dry 637 1 01/14/20 14:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N 65.0 mg/Kg - dry 29.9 1 01/13/20 14:50 ZBD 4500NO3F-2011 Organic N 54600 mg/Kg - dry 1590 1 01/14/20 09:00 CALCULATION pH 6.9 S.U. 1 01/13/20 06:41 JSL 9045D Total Solids 15.7 % 0.010 1 01/09/20 18:31 ADM SM-2540G Total Volatile Solids 62.1 % 0.010 1 01/09/20 18:31 ADM SM-2540G Total Kjeldahl Nitrogen 56900 mg/Kg - dry 1590 1 01/14/20 09:00 JPJ ')M-4500-NH3C-TKP Phosphorus 25500 mg/Kg - dry 31.8 1 01/09/20 21:55 BKN 6010D Aluminum 13100 mg/Kg - dry 31.8 1 01/09/20 21:55 BKN 6010D Arsenic 11.6 mg/Kg - dry 3.18 1 01/09/20 21:55 BKN 6010D Calcium 18900 mg/Kg - dry 159 1 01/09/20 21:55 BKN 6010D Cadmium 0.949 mg/Kg - dry 0.637 1 01/09/20 21:55 BKN 6010D Chromium 79.6 mg/Kg - dry 1.59 1 01/09/20 21:55 BKN 6010D Copper 371 mg/Kg - dry 1.59 1 01/09/20 21:55 BKN 6010D Iron 54100 mg/Kg - dry 159 5 01/10/20 17:26 KKM 6010D Lead 23.9 mg/Kg - dry 1.91 1 01/09/20 21:55 BKN 6010D Magnesium 2500 mg/Kg - dry 31.8 1 01/09/20 21:55 BKN 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 7 Waypoint..(2) NALYTICAL 46205 City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Report Number : 20-007-0013 Lab No : 70094 Sample ID: WWTP Cake 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project WWTP Cake Information : REPORT OFANALYSIS Report Date : 01/15/2020 Received : 01/07/2020 Pauric McGroary Agronomist Matrix: Solids Sampled: 1/6/2020 8:20 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Manganese 2020 mg/Kg - dry 3.18 1 01/09/20 21:55 BKN 6010D Mercury 0.847 mg/Kg - dry 0.0929 1 01/09/20 16:26 TJS SW-74716 Molybdenum 17.3 mg/Kg - dry 1.59 1 01/09/20 21:55 BKN 6010D Nickel 104 mg/Kg - dry 1.59 1 01/09/20 21:55 BKN 6010D Potassium 1690 mg/Kg - dry 31.8 1 01/13/20 22:33 BKN 6010D Selenium 6.62 mg/Kg - dry 3.18 1 01/09/20 21:55 BKN 6010D Sodium 510 mg/Kg - dry 159 1 01/09/20 21:55 BKN 6010D Zinc 1110 mg/Kg - dry 7.96 1 01/09/20 21:55 BKN 6010D Sulfur 11500 mg/Kg - dry 31.8 1 01/09/20 21:55 BKN 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 SA M 1-11:FIAA�A((,Njj�� IIIIIIItllll�llN I I �'�t3 W liCLla [ fvnlwwsnrnllll�IINIIIIIIIIIII)�II���I�I�I�01-0i-2020 i 143427 7021 Whit:Innc JWVTPCake Office Information Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholdcn Mi )nroenc.on., Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: —� - Date Recd: t �t `t W W I P C �tke Glass (Yes or No) Sampled Time: • Z D Time Recd: Plastic (Yes or No) Sampled By: f l,, ecd By: R lin wished By: (Signature) Date Time Received By: (Signature) Date Time Please Place a "X" by Desired Tests Internal Lab Code: SLMONR Solids % -TKN P K �'S Ca Mg Na Fe Al Mn Cu Zn NH4•N NO3-N x x x x x x x x x x x x x x x Cd Cr Ni Pb As Hg Se pH CaCO3 E . % Volatile Solids % Or" Mo Cl 13 Ba x x x x x x x x x x x '504 Ag Sb `Co Sn' 'TI V'" Be ALK' ' SS Avail P`` Sol K - Cond WIN T SOL B SOL NA, 08G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH CaO CaCO3 M CO3 ,MgO C/N TOG, Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN•W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR _ State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page 7 of 7 (2) WayPAoint. NALYTICAL 46205 City of Monroe Steve Holden 775 Treeway Dr Monroe , NC 28110 Report Number : 20-007-0014 Lab No : 70095 Sample ID : WTP Feric 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Project WTP Feric Information : REPORT OPANALYSIS Report Date : 01/15/2020 Received : 01/07/,2j020 gwfi' Inc (faw20 Pauric McGroary Agronomist Matrix: Solids Sampled: 1/6/2020 8:52 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 71.5 % 0.010 1 01/09/20 18:31 ADM SM-2540G I Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 695 mg/Kg - dry 351 1 01/14/20 14:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N <16.6 mg/Kg - dry 16.6 1 01/13/20 14:51 ZBD 4500NO3F-2011 Organic N 18600 mg/Kg - dry 877 1 01/14/20 09:00 CALCULATION pH 6.0 S.U. 1 01/13/20 06:41 JSL 9045D Total Solids 28.5 % 0.010 1 01/09/20 18:31 ADM SM-2540G Total Volatile Solids 35.0 % 0.010 1 01/09/20 18:31 ADM SM-254OG Total Kjeldahl Nitrogen 19300 mg/Kg - dry 877 1 01/14/20 09:00 JPJ ;M-4500-NH3C-TKP Phosphorus 1940 mg/Kg - dry 17.5 1 01/09/20 22:00 BKN 6010D Aluminum 5090 mg/Kg - dry 17.5 1 01/09/20 22:00 BKN 6010D Arsenic 24.5 mg/Kg - dry 1.75 1 01/09/20 22:00 BKN 6010D Calcium 2640 mg/Kg - dry 87.7 1 01/09/20 22:00 BKN 6010D Cadmium 5.96 mg/Kg - dry 0.351 1 01/09/20 22:00 BKN 6010D Chromium 193 mg/Kg - dry 0.877 1 01/09/20 22:00 BKN 6010D Copper 335 mg/Kg - dry 0.877 1 01/09/20 22:00 BKN 6010D Iron 315000 mg/Kg - dry 1750 100 01/10/20 17:37 KKM 6010D Lead 6.21 mg/Kg - dry 1.05 1 01/09/20 22:00 BKN 6010D Magnesium 663 mg/Kg - dry 17.5 1 01/09/20 22:00 BKN 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 7 Waypoint,(2). ANALYTICAL 46205 City of Monroe Steve Holden 775 Treeway Dr Monroe , NC 28110 Report Number : 20-007-0014 Lab No : 70095 Sample ID: WTP Feric 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Project WTP Feric Information : REPORT OFANAL YSIS Report Date : 01/15/2020 Received : 01/07/2020 Pauric McGroary Agronomist Matrix: Solids Sampled: 1/6/2020 8:52 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Manganese 884 mg/Kg - dry 1.75 1 01/09/20 22:00 BKN 6010D Mercury <0.0547 mg/Kg - dry 0.0547 1 01/09/20 16:28 T]S SW-7471B Molybdenum 41.8 mg/Kg - dry 0.877 1 01/09/20 22:00 BKN 6010D Nickel 24.7 mg/Kg - dry 0.877 1 01/09/20 22:00 BKN 6010D Potassium 509 mg/Kg - dry 17.5 1 01/13/20 22:38 BKN 6010D Selenium <8.77 mg/Kg - dry 8.77 5 01/10/20 17:31 KKM 6010D Sodium 198 mg/Kg - dry 87.7 1 01/09/20 22:00 BKN 6010D Zinc 178 mg/Kg - dry 4.39 1 01/09/20 22:00 BKN 6010D Sulfur 2560 mg/Kg - dry 17.5 1 01/09/20 22:00 BKN 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 M so SAMPC,1..`" R.ANS ry A & 1 I ����� ���� �� III 111 IN IIII ��I 11011111146205 20 04 7621 Whilrnt City of Mona>.' to 3i 15 A f'L Office Information uvIPr-ofl: Submitted By Charge To Copy To Project Steve Hoiden Cit of Monroe Rept# Acct # POB 69 Email 46205 Lab Number (Lab Use Only)ESample Monroe NC 28111 ID Container Type Sampled Date: 5h_ol-3cnrir?r_nqnrpcnc•rire }— - ZCD Date Recd: Time Recd: ✓� ecd B S _, Glass (Yes or No) Sampled Time: Plastic (Yes or No) Sampled By: He uished B : Si nature Date Time Received By: (Signature) Date Time Please Place a "Xii by Desired Tests Solids % TKN P K ' S :Ca ' Mg Na ` Fe At Mn Internal Lab Code: Cu Zn SLMONR NH4-N NO3-N x x x x x X x x x x x x x x Mo x Cd Cr Ni Pb." A 'Hg Se H CaCO3 i= . % Volatile Solids % Or -N CI B Ba x x x x x x x x x x x SO4 . A Sb ;Co' o-Sn Ti V Be ALK- SS Avail P Sol'K Cond ` " WIN_ SOL B SQL NA TOTAL P205 O&G TOTAL K20 SP.GR. TN TSS TKNW sieve#2o NH4W 'slevo#60 NO3W Sieve#too ORGN-W ASH PA CERT CaO AZ CERT .CaCO3 BTU M CO3 PCBS M Oz , R A T CtJ C!N FECAL TOC TCLP Env 1CR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments 71 Page 7 of 7 City of Monroe Reports of Lab Analysis 2nI Quarter F] (D WayPAoint. NALYTICAL 46205 City of Monroe Steve Holden Project RAS 775 Treeway Dr Information Monroe , NC 28110 Report Number : 20-093-0007 REPORTOFA Lab No : 70945 Sample ID : RAS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Date : 04/07/2020 Received : 04/02/2020 ewf« mC 64wr VALYSIS Pauric McGroary Agronomist Matrix: Solids Sampled: 4/1/2020 7:45 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Moisture 98.9 % 0.010 1 04/03/20 17:23 ADM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 1.11 % 0.010 1 04/03/20 17:23 ADM SM-254OG Total Volatile Solids 69.6 % 0.010 1 04/03/20 17:23 ADM SM-2540G Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 5 M SAMPLE-1 76 llllll lllll llll lllll ill l�� lli �lll loll ill ail llll 04_ 0 A �L Office Information .... _. RAS Submitted B, >py To Project Rept# Steve Hoiden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 il(lldln�l]!nlltilfl�l'nC.��r�, Lab Number (Lab Use Only) Sample ID Container Tye Sampled Date: —/ - Date Recd: Cl W� IZA� Glass (Yes or No) Sampled Time: Time Recd: Plastic (Yes or No) Sampled By: dz rJ i Recd B Re!' quished ignature) Date Time Received B (Signature) Date Time Please Place a "X" by Desired Tests Internal Lab Code: Solids % TKN P K Is Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N x Cd Cr Ni Pb As Hg Se pH CaCO3 E . % Volatile Solids % Or -N Mo CI B Ba X SO4 Ag Sb Co Sn Ti V Be ALK SS Avail P Sol K Cond WIN SOL B SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH Ca0 CaCO3 M CO3 MgO, C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page 5 of 5 (!DW• ayPoi nt . 7621 ain 80 -7 Road, Richmond, 27 -6446 Main 804-743-9401 0Fax $04-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Steve Holden Project WWTP Cake Report Date : 04/10/2020 775 Treeway Dr Information : Received : 04/02/2020 Monroe , NC 28110 Report Number : 20-093-0005 REPORT OFANAL YSIS Pauric McGroary Agronomist Lab No : 70943 Matrix: Solids Sample ID: WWTP Cake Sampled: 4/1/2020 9:15 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 86.3 % 0.010 1 04/03/20 17:23 ADM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 9640 mg/Kg - dry 730 1 04/09/20 14:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N 81.8 mg/Kg - dry 36.5 1 04/07/20 13:16 ZBD 4500NO3F-2011 Organic N 59300 mg/Kg - dry 1820 1 04/09/20 10:00 CALCULATION pH 7.7 S.U. 1 04/07/20 06:25 JSL 9045D Total Solids 13.7 % 0.010 1 04/03/20 17:23 ADM SM-2540G Total Volatile Solids 65.0 % 0.010 1 04/03/20 17:23 ADM SM-254OG Total Kjeldahl Nitrogen 68900 mg/Kg - dry 1820 1 04/09/20 10:00 JPJ >M-4500-NH3C-TKP Phosphorus 19000 mg/Kg - dry 36.5 1 04/07/20 18:51 KKM 6010D Aluminum 9710 mg/Kg - dry 36.5 1 04/07/20 18:51 TJS 6010D Arsenic 8.32 mg/Kg - dry 3.65 1 04/07/20 18:51 KKM 6010D Calcium 16500 mg/Kg - dry 182 1 04/07/20 18:51 KKM 6010D Cadmium <0.730 mg/Kg - dry 0.730 1 04/07/20 18:51 KKM 6010D Chromium 55.5 mg/Kg - dry 1.82 1 04/07/20 18:51 KKM 6010D Copper 304 mg/Kg - dry 1.82 1 04/07/20 18:51 KKM 6010D Iron 33900 mg/Kg - dry 36.5 1 04/07/20 18:51 TJS 6010D Lead 17.2 mg/Kg - dry 2.19 1 04/07/20 18:51 KKM 6010D Magnesium 2160 mg/Kg - dry 36.5 1 04/07/20 18:51 KKM 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 6 (2) WayPAoint.. NALYTICAL 46205 City of Monroe Steve Holden 775 Treeway Dr Monroe , NC 28110 Report Number : 20-093-0005 Lab No : 70943 Sample ID : WWTP Cake 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project WWTP Cake Information : REPORT OFANAL YSIS Report Date : 04/10/2020 Received : 04/02/2020 ?44w« mF 61wr Pauric McGroary Agronomist Matrix: Solids Sampled: 4/1/2020 9:15 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Manganese 1610 mg/Kg - dry 3.65 1 04/07/20 18:51 TJS 6010D Mercury 0.480 mg/Kg - dry 0.115 1 04/06/20 11:54 TJS SW-7471B Molybdenum 15.5 mg/Kg - dry 1.82 1 04/07/20 18:51 KKM 6010D Nickel 73.7 mg/Kg - dry 1.82 1 04/07/20 18:51 KKM 6010D Potassium 1660 mg/Kg - dry 36.5 1 04/07/20 18:51 TJS 6010D Selenium 4.96 mg/Kg - dry 3.65 1 04/07/20 18:51 KKM 6010D Sodium 737 mg/Kg - dry 182 1 04/07/20 18:51 KKM 6010D Zinc 964 mg/Kg - dry 9.12 1 04/07/20 18:51 KKM 6010D Sulfur 11500 mg/Kg - dry 36.5 1 04/07/20 18:51 KKM 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 6 54�3SANIPJ ',TRAN III11011INIIIIII111111IIII�III1ll11111l020IUY CM o6r A& WVVTPCakv AT Office Information Customer Information Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 shulden(timonroenc.orb --- -- _ _ _ Lab Number (Lab Use Only) Sample ID lContainer. Type Sampled Date: _ _ 0 2 Date Recd: W WTI' I cikc Glass (Yes or No) Sam led Time: / Time Recd: Plastic (Yes or We) Sampled B , Hv .-) Recd BY: 5ajinquish9,d,Ejy: (Signature) Date Time Received B (Signature) Date Time �zv2-J Please Place "X" by Desired Tests Internal Lab Code: SLMONR S15111ds % • TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4•N NO3-N x x x x x x x x x x x x x x .Cd Cr Ni Pb As H Se H CaCO3 E . % Volatile Solids % Or -N Mo Cl B Ba tx x x x x x x x x x x x SO4 A Sb Co Sn TI V Be ALK`° - SS- Avail P'' Sol K Cond WIN SOL B L NA O&G SP:GR. TSS Sieve#20 Steve#60 Steve#100 ASH CaO CaCO3 M CO3: M 0 C!N TOC Env TiPTAL 205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page 6 of 6 (2)W• ayPnt 7621 -7 Road, Richmond, V7 ain 80 Main $04-743-9401 0Fax 804-271-6446 -6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Steve Holden Project WTP Feric Report Date : 04/14/2020 775 Treeway Dr Information : Received : 04/02/2020 Monroe, NC 28110 I AW�c Pauric McGroary Report Number: 20-093-0006 REPORT OFANAL YSIS Agronomist Lab No : 70944 Matrix: Solids Sample ID : WTP Feric Sampled: 4/1/2020 8:06 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 79.5 % 0.010 1 04/03/20 17:23 ADM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 1410 mg/Kg - dry 488 1 04/09/20 14:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N <22.5 mg/Kg - dry 22.5 1 04/07/20 13:17 ZBD 4500NO3F-2011 Organic N 15800 mg/Kg - dry 1220 1 04/09/20 10:00 CALCULATION pH 5.5 S.U. 1 04/07/20 06:25 JSL 9045D Total Solids 20.5 % 0.010 1 04/03/20 17:23 ADM SM-2540G Total Volatile Solids 34.0 % 0.010 1 04/03/20 17:23 ADM SM-2540G Total Kjeldahl Nitrogen 17200 mg/Kg - dry 1220 1 04/09/20 10:00 JPJ >M-4500-NH3C-TKP ' Phosphorus 2990 mg/Kg -dry 122 5 04/08/20 12:48 TJS 6010D Aluminum 9070 mg/Kg - dry 122 5 04/08/20 12:48 TJS 6010D Arsenic 24.4 mg/Kg - dry 12.2 5 04/08/20 12:48 TJS 6010D Calcium 1900 mg/Kg - dry 610 5 04/08/20 12:48 TJS 6010D Cadmium <2.44 mg/Kg - dry 2.44 5 04/08/20 12:48 TJS 6010D Chromium 269 mg/Kg - dry 6.10 5 04/08/20 12:48 TJS 6010D Copper 461 mg/Kg - dry 6.10 5 04/08/20 12:48 TJS 6010D Iron 376000 mg/Kg - dry 2440 100 04/08/20 12:54 TJS 6010D Lead 8.00 mg/Kg - dry 7.32 5 04/08/20 12:48 TJS 6010D Magnesium 433 mg/Kg - dry 122 5 04/08/20 12:48 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 7 WayPAoint.. NALYTICAL 46205 City of Monroe Steve Holden 775 Treeway Dr Monroe , NC 28110 Report Number : 20-093-0006 Lab No : 70944 Sample ID: WTP Feric 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project WTP Feric Information : REPORT OFANAL YSIS Report Date : 04/14/2020 Received : 04/02/2020 Pauric McGroary Agronomist Matrix: Solids Sampled: 4/1/2020 8:06 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Manganese 417 mg/Kg - dry 12.2 5 04/08/20 12:48 TJS 6010D Mercury <0.0741 mg/Kg - dry 0.0741 1 04/06/20 11:55 TJS SW-7471B Molybdenum 55.6 mg/Kg - dry 6.10 5 04/08/20 12:48 TJS 6010D Nickel 45.3 mg/Kg - dry 6.10 5 04/08/20 12:48 TJS 6010D Potassium 299 mg/Kg - dry 122 5 04/08/20 12:48 TJS 6010D Selenium <12.2 mg/Kg - dry 12.2 5 04/08/20 12:48 TJS 6010D Sodium <610 mg/Kg - dry 610 5 04/08/20 12:48 TJS 6010D Zinc 56.6 mg/Kg - dry 30.5 5 04/08/20 12:48 TJS 6010D Sulfur 2440 mg/Kg - dry 122 5 04/08/20 12:48 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 sANji-,,.(�1�� MtLA It III IIII11111111111111111111.1111 3� � Orvof Wnt,- 54-0_-�0_•J WTP rent: 13 14 1 i 70� Office Information Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe POB 69 - — Email Monroe NC 28111 slit) ldcn«:numrocncc Sample ID Container Type Sam led Date: - -,vZp Date Recd: Acct # 46205 Number (Lab Use Only) `1� W�1T' I�eric Glass (*@s or No) Sampled Time: Time Recd: Plastic; (Yes or++M Sampled BY: ecd By: F-Lab Relipguished B : Si nature) Date y- - zo zv Time Received By: (Signature) Date Time Solids % TKN Please P Place K a S "X" by Ca Desired Mg Tests Na Fe Al Mn Internal Cu Lab Code: Zn x Cl SLMONR NH4-N x B NO3-N x Ba x x x x x x. x x x x x x "Cd Cr NI Pb As H Se H CaCO3 E . % Volatile Solids % Ot -N Mo x x x x x x x x x x x SO4` Ag Sib Co Sn Ti V' Be ALK SS Avail P Sol K Cond WIN SOL B S •,L NA T T AL Z 5 O&G, TOTAL K20 SP.GR. TN TSS TKNW Steve#2o NH4W 'Sieve#80 NO3W Sieve#100 ORGN-W ASH PA CERT CaO AZ CERT CaCO3 BTU M CO3 PCBS M 0 ' REACT CN CIN TOC Env FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page 7 of 7 (2) WayPAoi nt . NALYTICAL 46205 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com City of Monroe Steve Holden Steve Holden Project RAS Report Date : 04/24/2020 775 Treeway Dr Information : Received : 04/20/2020 Monroe, NC 28110 I dWcc Submitted By : Steve Holden Pauric McGroary Report Number : 20-111-0004 REPORT OFANAL YSIS Agronomist Lab No : 71088 Matrix: Solids Sample ID: RAS Sampled: 4/16/2020 9:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 98.5 % 0.010 Test Results Units MQL Total Solids 1.50 % 0.010 Total Volatile Solids 71.1 % 0.010 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit 1 04/22/20 11:00 CIR SM-2540G DF Date / Time By Analytical Analyzed Method 1 04/22/20 11:00 CJR SM-2540G 1 04/22/20 11:00 C]R SM-254OG L Limit Exceeded Page 3 of 5 Sf' IMPLE T" itl�illll►l�IlillVl�lllhllll!111111111NIIINII�lihhllli '0 o� 762 Cfv d 4.hnll ur )STODY Office Information RAS 'n Submitted By %,, urge I o Copy To Project Steve Holden Cityof Monroe Rept# Acct # 46205 Lab Number (Lab Use Only) POB 69 Monroe NC 28111 Sample ID Container Type Sampled Date: Email shaide_n'u n_ti_mroctic.orb - G - Date Recd: j l© RAS Glass W-es or No} Sampled Time: ,,pp Time Recd: Plastic (Yes orb Sampled B : d Recd By: linquis ed : (Signature) Date Time Received By: (Signature) Date Time Please Place a "X" by Desired Tests Internal Lab Code: Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N X Cd Cr Ni Pb I As Hg Se pH CaCO3 E . % Volatile Solids % Org-N Mo Cl a Ba X SO4 Ag Sb Co Sn Ti V Be ALK SS Avail P Sol K Cond WIN SOL B SOL NA 08G SP.GR. TSS Sleve#20 Sleve#6o Sleve#100 ASH CaO CaCO3 M CO3 M O C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA J2 Special Instructions or Remarks Comments Waypoint ANALYTICAL 46205 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-7.71-6446 www.waypointanalytical.com City of Monroe Steve Holden Steve Holden Project WWTP Cake Report Date : 04/28/2020 775 Treeway Dr Information : Received : 04/20/2020 Monroe , NC 28110 m�� PdWcce G Submitted By : Steve Holden Report Number: 20-111-0003 REPORT OPANALYSIS Pauric McGroary Agronomist Lab No : 71087 Matrix: Solids Sample ID : WWTP Cake Sampled: 4/16/2020 8:50 Test Results Units MOIL DF Date / Time By Analytical Analyzed Method Moisture 86.2 0/0 0.010 1 04/22/20 11:00 OR SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 8550 mg/Kg - dry 725 1 04/27/20 14:00 JPJ SM-4500-NH3C Nitrate+ N itrite-N 65.2 mg/Kg - dry 34.5 1 04/23/20 13:40 ZBD 4500NO3F-2011 Organic N 54100 mg/Kg - dry 1810 1 04/27/20 11:00 CALCULATION pH 7.9 S.U. 1 04/27/20 05:50 JSL 9045D Total Solids 13.8 % 0.010 1 04/22/20 11:00 OR SM-254OG Total Volatile Solids 64.6 % 0.010 1 04/22/20 11:00 OR SM-254OG Total Kjeldahl Nitrogen 62700 mg/Kg - dry 1810 1 04/27/20 11:00 JPJ ;M-4500-1\1113C-TO Phosphorus 20700 mg/Kg - dry 36.2 1 04/23/20 20:33 TJS 6010D Aluminum 11000 mg/Kg - dry 36.2 1 04/23/20 20:33 TJS 6010D Arsenic 8.70 mg/Kg - dry 3.62 1 04/23/20 20:33 TJS 6010D Calcium 17700 mg/Kg - dry 362 1 04/23/20 20:33 TJS 6010D Cadmium 1.05 mg/Kg - dry 0.725 1 04/23/20 20:33 TJS 6010D Chromium 62.5 mg/Kg - dry 1.81 1 04/23/20 20:33 TJS 6010D Copper 319 mg/Kg - dry 3.62 1 04/23/20 20:33 TJS 6010D Iron 38700 mg/Kg - dry 72.5 1 04/23/20 20:33 TJS 6010D Lead 19.7 mg/Kg -dry 2.17 1 04/23/20 20:33 TJS 6010D Magnesium 2340 mg/Kg - dry 36.2 1 04/23/20 20:33 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 6 Waypoint.,(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com 46205 City of Monroe Steve Holden Steve Holden Project WWTP Cake Report Date : 04/28/2020 775 Treeway Dr Information : Received : 04/20/2020 Monroe , NC 28110 to 64wr Submitted By : Steve Holden Pauric McGroary Report Number : 20-111-0003 REPORTOFANALYSIS Agronomist Lab No : 71087 Matrix: Solids Sample ID: WWTP Cake Sampled: 4/16/2020 8:50 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Manganese 1800 mg/Kg - dry 3.62 1 04/23/20 20:33 TJS 6010D Mercury 0.498 mg/Kg - dry 0.107 1 04/23/20 11:59 DDB SW-7471B Molybdenum 15.7 mg/Kg - dry 1.81 1 04/23/20 20:33 TJS 6010D Nickel 75.4 mg/Kg - dry 1.81 1 04/23/20 20:33 TJS 6010D Potassium 1880 mg/Kg - dry 72.5 1 04/23/20 20:33 TJS 6010D Selenium 4.83 mg/Kg - dry 3.62 1 04/23/20 20:33 TJS 6010D Sodium 855 mg/Kg - dry 181 1 04/23/20 20:33 TJS 6010D Zinc 1010 mg/Kg - dry 9.06 1 04/23/20 20:33 TJS 6010D Sulfur 12500 mg/Kg - dry 72.5 1 04/23/20 20:33 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 6 SAIMPLI 'FRANSNI11 AM, 1-ilS ,621 Whitcpinc Roa 1l11►11hIII lilt 11E,II1111.II';I�IIIh+III(I�ililll Office Information Submitted By Charge To Copy To Project Rept# Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden(a nxmr enc.orb Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: — v 20 Date Reed: WW'I P Cake Glass (Y s or No) Sampled Time: 51;.5 -> Time Reed: Plastic (Yes or-W&) Sampled By: £ f Reed By: F3plinquish5d : (Signature) Date Time Received By: (Signature) Date Time c� Please Place a "X" by Desired Tests Internal Lab Code: SLMONR Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N x x X x x X x x x x x x x x x 3:Cd Cr Ni Pb 'As Hg Se pH CaCO3 E . % Volatile Solids % Or -N Mo Cl B Ba x x x x x x x x x x x ;SO4 Ag Sb Co Sn Ti V: Be ALK SS Avail P' Sol K Cond WIN SOL B S.OL NA O&G SP:GR. TSS Sieve#20 Steve#60 Steve#100 ASH CaO CaCO3 M CO3 M O CM TOC Env TOTAL t?205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments 0 a� ro a a Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271.6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Steve Holden Project RAS Report Date : 05/22/2020 775 Treeway Dr Information : Received : 05/19/2020 Monroe , NC 28110 Pam« me Gov Pauric McGroary Report Number :20-140-0010 REPORT OFAIVALYSIS Agronomist Lab No : 71405 Matrix: Solids Sample ID: RAS Sampled: 5/18/2020 8:55 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 99.0 % 0.010 1 05/21/20 17:05 FMM SM-254OG Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 1.01 % 0.010 1 05/21/20 17:05 FMM SM-254OG Total Volatile Solids 71.3 % 0.010 1 05/21/20 17:05 FMM SM-254OG Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 5 SAMPLE TRANSMIT,I. A&L Eash ?{,71 t\'hitrninr IZ..o,l 1 llll!dill!II1iIIIN1l!11!�III lit 111illlNlli►llj1v Office Information '""_ `� Rept# Submitted By Charge To Steve Holden City of Monroe Copy To Project Acct # POB 69 Monroe NC 28111 Email 46205 sholdcn_ _" i`ji(jinrc�tne.urs, Lab Number (Lab Use Only) �i✓��� U Sample ID RAS Container Type Glass (Vgowr No) Sampled Date: Sampled Time: -/ -Ze_3' Date Recd: Time Reed: Plastic (Yes orWoe a Sampled By: z Recd By: rnquis d B : (Signature) Date Time Received By: (Signature) Date Time -I -w q,r] u � � Please Place a "X" by Desired Tests Internal Lab Code: Solids io TKN P K S Ca Mg Na Fe AI Mn Cu Zn NH4-N NO3-N x Cd Cr NI Pb As Hg Se pH CaCO3 -Eq. % Volatile Solids % Org-N Mo Cl B Ba x SO4 Ag Sb Co Sn Ti V Be ALK SS Avail P Sol K Cond WIN SOL B SOL NA O&G SP.GR. TSS Sieve#20 Sleve#60 Sieve#100 ASH CaO CaCO3 MgCO3 MgO I C/N TOC Env TOTAL P205 , TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments 0 Waypoint, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271.6446 46205 ANALYTICAL www.waypointanalytical.com City of Monroe Steve Holden Steve Holden Project WWTP Cake Report Date : 05/28/2020 775 Treeway Dr Information : Received : 05/19/2020 Monroe , NC 28110 Submitted By : Steve Holden Report Number: 20-140-0009 REPOR T OF A NA L YSIS Pauric McGroary Agronomist Lab No : 71404 Matrix: Solids Sample ID: WWTP Cake Sampled: 5/18/2020 8:45 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 84.5 % 0.010 1 05/21/2017:05 FMM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 4740 mg/Kg - dry 161 1 05/27/20 14:30 JPJ SM-4500-NH3C Nitrate+Nitrite-N 69.0 mg/Kg - dry 30.9 1 05/26/20 15:35 ZBD 4500NO3F-2011 Organic N 31400 mg/Kg - dry 1610 1 05/27/20 11:30 CALCULATION pH 6.0 S.U. 1 05/27/20 06:41 JSL 9045D Total Solids 15.5 0.010 1 05/21/2017:05 FMM SM-2540G Total Volatile Solids 45.8 % 0.010 1 05/21/20 17:05 FMM SM-254OG Total Kjeldahl Nitrogen 36100 mg/Kg - dry 1610 1 05/27/20 11:30 JPJ >M-4500-NH3C TKt Phosphorus 11700 mg/Kg - dry 32.3 1 05/22/20 18:44 TJS 6010D Aluminum 11300 mg/Kg - dry 32.3 1 05/22/20 18:44 TJS 6010D Arsenic 16.3 mg/Kg - dry 3.23 1 05/22/20 18:44 TJS 6010D Calcium 9030 mg/Kg - dry 323 1 05/22/20 18:44 TJS 6010D Cadmium 1.95 mg/Kg - dry 0.645 1 05/22/20 18:44 TJS 6010D Chromium 158 mg/Kg - dry 1.61 1 05/22/20 18:44 TJS 6010D Copper 394 mg/Kg - dry 3.23 1 05/26/20 14:16 KKM 6010D Iron 205000 mg/Kg - dry 323 5 05/26/20 14:21 KKM 6010D Lead 13.6 mg/Kg - dry 1.94 1 05/22/20 18:44 TJS 6010D Magnesium 1520 mg/Kg - dry 32.3 1 05/22/20 18:44 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 6 0 Waypoint 7621 Whitepine Road, Richmond, VA 23237 Maln 804-743-9401 " Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Steve Holden Steve Holden Project WWTP Cake Report Date : 05/28/2020 775 Treeway Dr Information : Received : 05/19/2020 Monroe, NC 28110 Pw« IV owr Submitted By : Steve Holden Report Number: 20-140-0009 REPORrOFANALYSIS Pauric McGroary Agronomist Lab No : 71404 Matrix: Solids Sample ID : WV11TP Cake Sampled: 5/18/2020 8:45 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Manganese 974 mg/Kg - dry 3.23 1 05/22/20 18:44 TJS 6010D Mercury 0.170 mg/Kg - dry 0.0993 1 05/27/20 11:22 DDB SW-7471B Molybdenum 31.2 mg/Kg - dry 1.61 1 05/22/20 18:44 TJS 6010D Nickel 52.6 mg/Kg - dry 1.61 1 05/22/20 18:44 TJS 6010D Potassium 1560 mg/Kg - dry 64.5 1 05/22/20 18:44 KKM 6010D Selenium 3.50 mg/Kg - dry 3.23 1 05/22/20 18:44 TJS 6010D Sodium 716 mg/Kg - dry 161 1 05/22/20 18:44 TJS 6010D Zinc 505 mg/Kg - dry 8.06 1 05/22/20 18:44 TJS 6010D Sulfur 6120 mg/Kg - dry 64.5 1 05/22/20 18:44 TJS 6010D I Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 4 of 6 SANIPLi TRANSNII-I TAI_ A&L l-�-'asteru 7021 1%!1111t•1,ire• kwltI I?II!! � 18fiI I III till IIIN I1lil NI(I I NIIII IIII INIIIII1 ill "M9 C;t-� :,t 0.dcrrrne ; C i 31 `A"AlTP CAI,P Vwww AA)l Office Information i�usiomer tnrormation Rept# Submitted By Charge To Steve Hoiden Cityof Monroe Copy To Project Acct t{ POB 69 Monroe NC 28111 Sample ID Container Type Sampled Date: Em?il 05 Lab Number (Lab Use Only) - &' D Date Recd: slu>idcn!u moniY�ctic.grt; Lfh� jv �'d�� I I Cake Glass (`�.rr No) Sampled Time: ; y S Time Recd: Plastic (Yes or4iep# Sampled By: ,� F Recd B Y: R,ej£ inquis .By: (Signature) Date Time Received By: (Signature) Date Time V n�� Please Place a 'X" by Desired Tests Internal Lab Code: SLMONR St5lids%j TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N x x x x x x x x x x x x x x x { 1 Cd Cr Ni Pb As I Hg Se H CaCO3 E . % Volatile Solids % Or -N Mo Cl B Ba x ,SO4, x . Ag x - Sb x Co x Sn x Ti x V x Be ALK ` X SS x Avail P x Sol K Cond WIN SOL 8 SAL NA TOTAL P205 O&G TOTAL K20 _SP.GR. TN I TSS TKNW Steve#2o NH4W Sieve#60 NO3W Steve#100 ORGN-W ASH PA CERT CaO AZ CERT CaCO3 BTU MQC03 PCBS M O REACT CN C/N FECAL TOC Env TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks777 Comments -- _._.._, T City of Monroe Reports of Lab Analysis 3 rd Quarter LI (2) • WayPo i nt 7621 Whitepine Road, Richmond, VA 23237 . Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project RAS Steve Holden Report Date : 07/10/2020 775 Treeway Dr Information : Received : 07/06/2020 Monroe , NC 28110 Pew,;, me 64w Pauric McGroary Report Number: 20-188-0005 REPORT OFANAL YSIS Agronomist Lab No : 72813 Matrix: Solids Sample ID : RAS Sampled: 7/1/2020 9:45 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Moisture 99.2 % 0.010 1 07/07/20 16:30 FMM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 0.800 % 0.010 1 07/07/20 16:30 FMM SM-254OG Total Volatile Solids 67.4 % 0.010 1 07/07/20 16:30 FMM SM-254OG Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 5 SAMPLE TRANSMIT] I ��I�I� ���� I�� ����N �I��� ����� ���I ������ ����I I���� ��� ��� �� 46=0 a'os Ciiv of M<mro: t3 75 Last'RAS 25A&L AT 621 Whitepine Road n Customer Information Submitted By Charge To 9 Copy To Project e✓� Mo✓ris City of Monroe POB 69 ffbe Monroe NC 28111 Email nl Y) Sample ID Container Tye Sampled Date: '1 °rr�za�-nc. bra Date Recd: .0 RASGlass ( No Sam led Time: q ;'� �' Time Recd: Plastices rye) Sampled By: or ;S Relinquished B : (Signature Date Recd By: Time Received By: (Signature) Date Time .? i p 57 Please Place a "X" by Desired Tests Solids % TKN P K S Ca Mg Na Internal Lab Code: 44 Fe Al Mn Cu Zn NH4-N NO3-N X w 0 C2CO3 Volatile Cd Cr Ni Pb As H g Se pH Eq. /° Solids 10 Org-N Mo Lin ° Cl B Ba a X Ag Sb Co Sn Ti v Be ALK SS Avail P Sol K ind WIN SOL B SOL NA 08G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH Ca0 CaCO3 M CO3 M O C/N TOC Env TOTAL TOTAL P205 K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS R CNCT FECAL TCLP ICR State Certification Needed: NORTH CAR©LINA Special Instructions or Remarks Comments o'Yt 1 C -e- (2) WayP oint 7621 Whitepine Road, Richmond, VA 23237 . Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WWTP Cake Steve Holden Report Date : 07/14/2020 775 Treeway Dr Information : Received : 07/06/2020 Monroe , NC 28110 Pauric McGroary Report Number : 20-188-0006 REPORT OFANAL YSIS Agronomist Lab No : 72814 Matrix: Solids Sample ID: WWTP Cake Sampled: 7/1/2020 10:25 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 82.3 0.010 1 07/08/20 16:31 FMM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 3210 mg/Kg - dry 141 1 07/12/20 15:30 JPJ SM-4500-NH3C Nitrate+Nitrite-N 124 mg/Kg - dry 27.9 1 07/13/20 15:30 ZBD 4500NO3F-2011 Organic N 46200 mg/Kg - dry 1410 1 07/12/20 14:00 CALCULATION pH 7.0 S.U. 1 07/13/20 05:32 JSL 9045D Total Solids 17.7 % 0.010 1 07/08/20 16:31 FMM SM-254OG Total Volatile Solids 58.8 % 0.010 1 07/08/20 16:31 FMM SM-2540G Total Kjeldahl Nitrogen 49400 mg/Kg - dry 1410 1 07/12/20 14:00 JPJ ')M-4500-NH3C-TKP Phosphorus 18200 mg/Kg - dry 28.2 1 07/09/20 03:17 JTR 6010D Aluminum 12900 mg/Kg - dry 28.2 1 07/09/20 23:46 JTR 6010D Arsenic 10.1 mg/Kg - dry 2.82 1 07/09/20 23:46 JTR 6010D Calcium 14500 mg/Kg - dry 282 1 07/09/20 03:17 JTR 6010D Cadmium 0.915 mg/Kg - dry 0.565 1 07/09/20 03:17 JTR 6010D Chromium 72.9 mg/Kg - dry 1.41 1 07/09/20 03:17 JTR 6010D Copper 306 mg/Kg - dry 2.82 1 07/09/20 03:17 JTR 6010D Iron 59300 mg/Kg - dry 282 5 07/10/20 00:21 JTR 6010D ' Lead 19.8 mg/Kg - dry 1.69 1 07/09/20 03:17 -TR 6010D Magnesium 2150 mg/Kg - dry 28.2 1 07/09/20 03:17 JTR 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 8 (2) WayPoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WWTP Cake Steve Holden Report Date : 07/14/2020 775 Treeway Dr Information : Received : 07/06/2020 Monroe , NC 28110 Report Number : 20-188-0006 REPORT OFANAL YSIS Pauric McGroary Agronomist Lab No : 72814 Matrix: Solids Sample ID: WWTP Cake Sampled: 7/1/2020 10:25 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Manganese 1590 mg/Kg - dry 2.82 1 07/09/20 03:17 JTR 6010D Mercury 0.430 mg/Kg - dry 0.0875 1 07/09/20 11:59 DDB SW-7471B Molybdenum 14.2 mg/Kg - dry 1.41 1 07/09/20 03:17 JTR 6010D Nickel 63.3 mg/Kg - dry 1.41 1 07/09/20 03:17 JTR 6010D Potassium 1790 mg/Kg - dry 56.5 1 07/09/20 23:46 JTR 6010D Selenium 4.73 mg/Kg - dry 2.82 1 07/09/20 23:46 JTR 6010D Sodium 633 mg/Kg - dry 141 1 07/09/20 03:17 JTR 6010D Zinc 847 mg/Kg - dry 7.06 1 07/09/20 03:17 JTR 6010D Sulfur 9040 mg/Kg - dry 56.5 1 07/09/20 03:17 JTR 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 4 of 8 .'0-188-0006 SAMPLE TRANSMITTAL 1701 �I I IIIII�IIIIIIIIII�IW�I�INII(IlNllflllll�IIIIIIINa6�,�:0 city of Mnrir,,e WWTPCakr• 131701 A&L Eastern Lab 7621 Whilcimic Road Rich -nand Vn Office Information Customer Information Rept# Submitted By Charge To ,.r-1 s Ci of Monroe Copy To Project Email Acct # POB 69 46205 Monroe NC 28111 I(Imorr.s@MovltoQ nc •or Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: 7 t 1.2 O Date Recd: L� W WTP Cake Glass ( or No) Sampled Time: 10- 2 - Time Recd: Plastic Yes or ND) Sampled B e,1 o ✓,4 s Recd By: Relinquished By: (Signature) Date Time Received By: (Signature) Date Time vwa Please Place a 'rX 1 by Desired Tests Internal Lab Code: SLMONR Solids % -TKN P7 K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N X X X X X X X x X X X X X X x j -Cd . Cr Ni Pb As Hg Se pH CaCO3 Eq. % Volatile Solids % Or -N Mo CI B Ba X x X X x x x x x x X ,SO4 A Sb -Co Sn. TI. V Be ALK SS Avail P'' Sol K Cond WIN .SOL B SAL NA 08G, ,SP.GR. TSS Sleve#20 Sleve#60 Sleve#100 ASH Ca0 CaCO3 M CO3 M 0 C/N TOC Env - TOTAL 205 TOTAL . K20 I TN TKNW ' NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR I- I I I I., I State Certification Needed: NORTH CAROLINA - --F Special Instructions or Remarks Comments UPS 0n ice co w 0 co v rn 04 w (D WayPAoint. NALYTICAL 46205 City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Report Number : 20-188-0007 Lab No : 72815 Sample ID : WTP Ferric Cake 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project WTP Ferric Cake Information : REPORT OFANAL YSIS Report Date : 07/14/2020 Received : 07/06/2020 Pauric McGroary Agronomist Matrix: Solids Sampled: 7/1/2020 10:30 Test Results Units MOIL DF Date / Time By Analytical Analyzed Method Moisture 68.5 % 0.010 1 07/08/20 16:31 FMM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 317 mg/Kg - dry 79.4 1 07/12/20 15:30 JPJ SM-4500-NH3C Nitrate+Nitrite-N 28.4 mg/Kg - dry 15.9 1 07/13/20 15:31 ZBD 4500NO3F-2011 Organic N 12200 mg/Kg - dry 794 1 07/12/20 14:00 CALCULATION pH 5.7 S.U. 1 07/13/20 05:32 JSL 9045D Total Solids 31.5 % 0.010 1 07/08/20 16:31 FMM SM-2540G Total Volatile Solids 34.6 % 0.010 1 07/08/20 16:31 FMM SM-2540G Total Kjeldahl Nitrogen 12500 mg/Kg - dry 794 1 07/12/20 14:00 JPJ ")M-4500-NH3C-TKP Phosphorus 3330 mg/Kg - dry 79.4 5 07/10/20 16:57 TJS 6010D Aluminum 5300 mg/Kg - dry 79.4 5 07/10/20 16:57 TJS 6010D Arsenic 32.1 mg/Kg - dry 7.94 5 07/10/20 16:57 TJS 6010D Calcium 2010 mg/Kg - dry 794 5 07/10/20 16:57 TJS 6010D Cadmium 2.21 mg/Kg - dry 1.59 5 07/10/20 16:57 TJS 6010D Chromium 228 mg/Kg - dry 3.97 5 07/10/20 16:57 TJS 6010D Copper 394 mg/Kg - dry 7.94 5 07/10/20 16:57 TJS 6010D Iron 310000 mg/Kg - dry 317 10 07/10/20 17:02 TJS 6010D Lead <4.76 mg/Kg - dry 4.76 5 07/10/20 16:57 TJS 6010D Magnesium 352 mg/Kg - dry 79.4 5 07/10/20 16:57 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 7 (2) Waypoint, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WTP Ferric Cake Steve Holden Report Date : 07/14/2020 775 Treeway Dr Information : Received : 07/06/2020 Monroe, NC 28110 Report Number : 20-188-0007 REPORT OPANALYSIS Pauric McGroary Agronomist Lab No : 72815 Matrix: Solids Sample ID : WTP Ferric Cake Sampled: 7/1/2020 10:30 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Manganese 470 mg/Kg - dry 7.94 5 07/10/20 16:57 TJS 6010D Mercury <0.0485 mg/Kg - dry 0.0485 1 07/09/20 12:01 DDB SW-7471B Molybdenum 42.9 mg/Kg - dry 3.97 5 07/10/20 16:57 TJS 6010D Nickel 37.8 mg/Kg - dry 3.97 5 07/10/20 16:57 TJS 6010D Potassium 208 mg/Kg - dry 159 5 07/10/20 16:57 TJS 6010D Selenium <15.9 mg/Kg - dry 15.9 10 07/10/20 17:02 TJS 6010D Sodium <397 mg/Kg - dry 397 5 07/10/20 16:57 TJS 6010D Zinc 168 mg/Kg - dry 19.8 5 07/10/20 16:57 TJS 6010D Sulfur 2190 mg/Kg - dry 159 5 07/10/20 16:57 TJS 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 4 of 7 SAMPLE T'RANsmirrAL t A&L Eastern I 7621 Whitcnme Rmd Riclm,nt 11111111111111lillillliiiiI llllillllllllMIIMIIIIIIIM a6 �8�7 c ry o, Monroe oe <o�o WTP FF'fflc Cake 13 19 31 FIiL Office Information Rept# Customer Information Charge To Copy To Project mCityof Monroe POB 69 Email Submittedqlas� Monroe NC 28111 Krnornti@ rm-orwoe. c, 0 Sam le ID ye Sampled Date: p Date RMT Acc# # 46205 Lab Number Lab Use Only) f Y)[WTP LS j.`tT1C Le or No) s or ) Relinquished By: (Signature) Date Time Sam led Time: /p:ao Time Recd: Sampled By: o,rr ��. Received B Signature Recd By: Date Time ? 0 TKN Please P Place A" K ' , a S "X" b Ca Y Desired Mg Tests , Na Fe Ale Mn intemai Cu Lab Code: Zn %� SLMONR NH4-N x NO3-N �( ES04,� x x x x x x x x x x x Cr-,. x NL�; x Pb x As x .H x Ss x H x Cam. E.% volatile' Solids% x Or -N-' x Mo x CI, BBa SOL NA TQTAL P205 Ag ` ;` O&Gr-- . T4 At, 'rr; K20 .Sb._ -'SP.GR. x `: r ,'.. TN fi Co: -TSS- Y'-• _T1CAj =Sh Steve#20 tom..-eaisj. a, NHgWAd TL =steve#so :.. No3W µ.y$_" s1eve#100 �, ORGN-W : , .136 : 4 ASH 4 .: PA CERT ' ' ALK; ? XCaO z nA : -» AZVERT . -SS �CaCO3 BTU. JAvail,P: ol`K Y Cond.. IN :. ;' SOL B M CO3 .... PC, BS M 9 03:: FACT - `CN C/N _ ; FECAL TOC ` TCLP Env ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments 44 0 w rn ro a WaypointNALYTICAL 46205 Ken Morris City of Monroe Project RAS Ken Morris 775 Treeway Dr Information Monroe , NC 28110 Submitted By : Ken Morris Report Number : 20-209-0002 Lab No : 73169 Sample ID: RAS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Date : 07/30/2020 Received : 07/27/2020 Pauric McGroary REPORT OFANAL YSIS Agronomist Matrix: Solids Sampled: 7/22/2020 9:00 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Moisture 99.3 % 0.010 1 07/28/20 17:10 FMM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 0.690 % 0.010 1 07/28/20 17:10 FMM SM-2540G Total Volatile Solids 68.3 % 0.010 1 07/28/20 17:10 FMM SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 3 of 5 M SAMPLE TRANSMITI A&L :Cast( 7671 Whitenine Rnmri k.. 11111Ilbi 1111111111IN111111H1111111uIII111111111 *C,, RAs 100t 44 nformation Customer Information Rept# Submitted By Charge To Copy To Project o,r r• S Cityof Monroe POB 69 Email Acct # _ 6205 r (Lab Use Only) FN Monroe NC 28111 Sample ID Container Type Sampled Date: .?�-,2 o Date Recd: rl i ���'%SPlastic Glass (error Sam led Time: ,' oo Time Recd: r Chi) Sampled By: 4 r r� s Recd By: uished B : (Signature) Date Time Received By: Signature Date Time LA 2 Please Place a " ' by Desired Tests Internal Lab Code: Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N X Cd Cr Ni Pb As Hg Se pH CaCO3 Eq. % Volatile Solids % Org-N Mo Cl B Ba X SO4 Ag Sb Co Sn Ti V Be ALK SS Avail P Sol K Cond WIN S0L B SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH CaO CaCO3 M CO3 MgO C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU' PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments I) r 0 Ln rn rt a (2) WayPoint . 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WWTP Cake Original Report Date : 08/04/2020 Ken Morris Revised Report Date: 08/18/2020 775 Treeway Dr Information : Received : 07/27/2020 Monroe , NC 28110 Report Number : 20-209-0003 Lab No : 73170 Sample ID: WWTP Cake REPORT OPANALYSIS Matrix: Solids Sampled: 7/22/2020 7:25 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 80.7 % 0.010 1 07/28/20 17:10 FMM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 4120 mg/Kg - dry 130 1 08/03/20 09:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N 164 mg/Kg - dry 24.9 1 08/03/20 14:51 ZBD 4500NO3F-2011 Organic N 38400 mg/Kg - dry 1300 1 08/03/20 07:00 CALCULATION pH 7.4 S.U. 1 08/03/2017:12 ADM 9045D Total Solids 19.3 % 0.010 1 07/28/20 17:10 FMM SM-2540G Total Volatile Solids 59.2 % 0.010 1 07/28/20 17:10 FMM SM-254OG Total Kjeldahl Nitrogen 42500 mg/Kg - dry 1300 1 08/03/20 07:00 JPJ ')M-4500-NH3C-TKP Phosphorus 18200 mg/Kg - dry 25.9 1 07/30/20 00:37 JTR 6010D Aluminum 11700 mg/Kg - dry 25.9 1 07/30/20 00:37 KKM 6010D Arsenic 8.03 mg/Kg - dry 2.59 1 07/30/20 00:37 JTR 6010D Calcium 14900 mg/Kg - dry 259 1 08/01/20 11:38 KKM 6010D Cadmium 1.01 mg/Kg - dry 0.518 1 07/30/20 00:37 JTR 6010D Chromium 67.9 mg/Kg - dry 1.30 1 07/30/20 00:37 JTR 6010D Copper 298 mg/Kg - dry 2.59 1 07/30/20 00:37 JTR 6010D Iron 56500 mg/Kg - dry 518 10 07/30/20 19:11 KKM 6010D Lead 18.4 mg/Kg - dry 1.55 1 07/30/20 00:37 JTR 6010D Magnesium 2200 mg/Kg - dry 25.9 1 07/30/20 00:37 JTR 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 6 (D WayPoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WWTP Cake Original Report Date : 08/04/2020 Ken Morris Revised Report Date: 08/18/2020 775 Treeway Dr Information : Received : 07/27/2020 Monroe , NC 28110 Report Number : 20-209-0003 REPORT Of ANALYSIS Lab No : 73170 Sample ID: WWTP Cake Matrix: Solids Sampled: 7/22/2020 7:25 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Manganese 1490 mg/Kg - dry 2.59 1 07/30/20 00:37 JTR 6010D Mercury 0.544 mg/Kg - dry 0.0818 1 07/30/20 11:16 DDB SW-7471B Molybdenum 14.7 mg/Kg - dry 1.30 1 07/30/20 00:37 JTR 6010D Nickel 64.8 mg/Kg - dry 1.30 1 07/30/20 00:37 JTR 6010D Potassium 2080 mg/Kg - dry 51.8 1 07/30/20 00:37 JTR 6010D Selenium 4.17 mg/Kg - dry 2.59 1 07/30/20 00:37 JTR 6010D Sodium 741 mg/Kg - dry 130 1 07/30/20 00:37 JTR 6010D Zinc 803 mg/Kg - dry 6.48 1 07/30/20 00:37 JTR 6010D Sulfur 9330 mg/Kg - dry 51.8 1 07/30/20 00:37 JTR 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 4 of 6 III��IIIIIIIuiNIN11111IN� 111IF11iNfIlllh� � �3 SAMPLETRANSMIT`;�w„rrn°°„", Ww7 P c:,k, 100336 A&L Easterr 7621 Whitenine llwad Richmond VA 23237 Tel: K0.1-7•143-9401 Office Information Customer Information Rept# Submitted By Charge To Copy To Project 9*% or City of Monroe Acct # _%< POB 69 Email 46205 Monroe NC 28111 KMor r ; S6; rAArYoe nc -or Lab Number (Lab Use Only) Samplo ID Container Type Sampled Date: '7-.2 a --02,0 Date Recd: 22 1-�,1 J t i v wM Cake Glass (`�sor Sampled Time: ?:,A5 Time Recd: Plastic es W) Sampled By: e*-., M o-e r 4S Recd By: Relinquished By: (Signature) Date Time Received By: (Signature) Date Time Please Place a 'X" by Desired'tests Intemal Lab Code: SLMONR S40lids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N N033-N x x x x x x x x x x x x x x x ` .Cd Cr Ni Pb As Hg Se- - - -. H . _ CaCO3 -E . % Volatile Solids % Or -N -Mo :. Cl B- Ba x x x x x ; x x x x x x ,SO4- 'Ag : 'Sb Co Sn` Ti' V Be ALK SS AVai1 P' =501 K Corid WIN SOL E SAL NA O&G SP GR. TSS Sleve#20 Steve#60 Sieve#100 ASH CaO' : CaCO3 MgCO3: M O C/N TOC Env TOTAL. 205 TOTAL K20 - TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTIU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments 44 0 v rn w (2) WayPAoint NALYTICAL 46205 City of Monroe Project RAS Ken Morris 775 Treeway Dr Information Monroe , NC 28110 Report Number : 20-226-0010 REPORTOPA Lab No : 73365 Sample ID : RAS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Report Date : 08/19/2020 Received : 08/13/2020 IGt��G 111 � CdQpW L YSIS Pauric Mc Groary Ph.D., CPA NA Agronomist Matrix: Solids Sampled: 8/12/2020 8:49 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Moisture 99.0 % 0.010 1 08/16/20 13:00 FMM SM-254OG Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 0.990 % 0.010 1 08/16/20 13:00 FMM SM-2540G Total Volatile Solids 71.3 % 0.010 1 08/16/20 13:00 FMM SM-254OG Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 3 of S SAMPLE; TRAi 20 AM I111111146205 7621 l hli G'+ra':4mrro 123235 Office Information KHJ � Submitted By .,y Copy To Project o r r . s _ Cityof Monroe POB 69 Email Monroe NC 28111 r+tior,.;s@mov�rJ� roc o Sample ID Container T pe Sampled Date: —126- 20 Date Recd: Rept4 Acct # 46205 Lab Number (Lab Use Only) RA S Glass (lW or o Sampled Time: Time Recd: Plastic, Ces r I") Sampled By: vi'o ,,3 Recd By: Relinquished By. (Signature) Date Time Received By:. (Signature) Date Time 8- o Please Place'a ' X" by Desired Tests Internal Lab Code: Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N X Cd Cr Ni Pb I As Hg Se pH CaCO3 Eq. % Volatile Solids % Org-N Mo Cl B Ba X SO4 Ag Sb Co Sn Ti V Be I ALK SS Avail P Sol K Cond WIN SOL B SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Steve#100 ASH CaO CaCO3 MgCO3 Mg0 C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA S cial Instructions or Remarks Comments F7 - I I (2) Waypo int 7621 Whitepine Road, Richmond, VA 23237 . Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WWTP Cake Ken Morris Report Date : 08/25/2020 775 Treeway Dr Information : Received : 08/13/2020 Monroe , NC 28110 m Pam, L I" �QO W Report Number: 20-226-0011 REPORT OFANAL YSIS Pauric Mc Groary Ph.D., CPAAgronomist Lab No : 73366 Matrix: Solids Sample ID: WWTP Cake Sampled: 8/12/2020 8:04 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 76.1 % 0.010 1 08/17/20 16:16 FMM SM-254OG Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 2120 mg/Kg - dry 105 1 08/20/20 15:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N 91.6 mg/Kg - dry 20.6 1 08/18/20 15:47 ZBD 4500NO3F-2011 Organic N 31700 mg/Kg - dry 1050 1 08/20/20 10:00 CALCULATION pH 6.7 S.U. 1 08/18/2015:20 ADM 9045D Total Solids 23.9 % 0.010 1 08/17/20 16:16 FMM SM-2540G Total Volatile Solids 54.7 % 0.010 1 08/17/20 16:16 FMM SM-2540G Total Kjeldahl Nitrogen 33800 mg/Kg - dry 1050 1 08/20/20 10:00 JPJ 'PM-4500-NH3C-TKP Phosphorus 16700 mg/Kg - dry 20.9 1 08/18/20 20:46 TJS 6010D Aluminum 12100 mg/Kg - dry 20.9 1 08/18/20 20:46 TJS 6010D Arsenic 14.5 mg/Kg - dry 2.09 1 08/25/20 04:38 JADS 6010D Calcium 12100 mg/Kg - dry 209 1 08/18/20 20:46 TJS 6010D Cadmium 0.828 mg/Kg - dry 0.418 1 08/18/20 20:46 TJS 6010D Chromium 106 mg/Kg - dry 1.05 1 08/25/20 04:38 JADS 6010D Copper 473 mg/Kg - dry 2.09 1 08/25/20 04:38 DADS 6010D Iron 78200 mg/Kg - dry 209 5 08/19/20 17:15 TJS 6010D Lead 20.0 mg/Kg - dry 1.26 1 08/25/20 04:38 ]ADS 6010D Magnesium 1810 mg/Kg - dry 20.9 1 08/18/20 20:46 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 6 (2)WayPoi nt 7621 -7 Road, Richmond, V7 . Main 804-743-9401 "Pax ain 80 -6446 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WWTP Cake Ken Morris Report Date : 08/25/2020 775 Treeway Dr Information : Received : 08/13/2020 Monroe , NC 28110 mm � PGtiW'G irl kOW Report Number : 20-226-0011 REPORTOFANALYSIS Pauric Mc Groary Ph.D., CPAAgronomist Lab No : 73366 Matrix: Solids Sample ID: WWTP Cake Sampled: 8/12/2020 8:04 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Manganese 1440 mg/Kg - dry 2.09 1 08/25/20 04:38 ]ADS 6010D Mercury 0.448 mg/Kg - dry 0.0589 1 08/19/20 11:41 DDB SW-7471B Molybdenum 17.7 mg/Kg - dry 1.05 1 08/18/20 20:46 TJS 6010D Nickel 70.3 mg/Kg - dry 1.05 1 08/25/20 04:38 JADS 6010D Potassium 1820 mg/Kg - dry 41.8 1 08/25/20 04:38 JADS 6010D Selenium <2.09 mg/Kg - dry 2.09 1 08/25/20 04:38 DADS 6010D Sodium 628 mg/Kg - dry 105 1 08/18/20 20:46 TJS 6010D Zinc 795 mg/Kg - dry 5.23 1 08/25/20 04:38 JADS 6010D Sulfur 7950 mg/Kg - dry 41.8 1 08/18/20 20:46 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 6 Sf1NIP1,F�26 'USTODY 11111111 111I 11D 11 IN 11111111111 0a 113 -0 Cdv of WMmtoe 1� 33 59 W W T P C,4, I A Office Information _ _ . � Submitted By Charge To Copy To Project V ; s C4 of Monroe POB 69 Email Rept# Acct # 46205 Monroe NC 28111 K ar ,Q„ Lab Number (Lab Use Only) Sample ID ContainerType Sampled Date: ^• _ ao Date Recd: WWTP Cake ,Glass Y4% or o Sam led Time: Time Recd: Plastic es or Imo) Sampled By: ,�,.;s Recd By: FRelinquished y: (Signature) Date lime Received By: (Signature) Date Time -4— M,-04j��x . . 1 0 If 44,2 2� Please Place a "X" by Desired Tests Intemal Lab Code: SLMONR Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N X X X X X X X X X X X.X X X X *: Cd Cr Ni Pb As Hg Se pH CaCO3 E . % Volatile Solids % Or -N Mo CI B Ba X X X X X X X x X X X ,SO4 Ag Sb Co Sn TI V Be ALK' ° SS Avail P Sol K Cond WIN SOL B STL NA O&G _SP:GR. TSS Sleve#20 Sleve#60 SievelFloo ASH CaO CaCO3 M CO3 M O C/N TOC Env WTAL -,, P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments City of Monroe Reports of Lab Analysis 4" Quarter Waypoint..NALYT(2) ICAL 46205 City of Monroe Project RAS Ken Morris 775 Treeway Dr Information Monroe , NC 28110 Report Number: 20-280-0004 Lab No : 73890 Sample ID : RAS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OPANAL Y.4I5 Report Date : 10/12/2020 Received : 10/06/2020 ku W Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 10/5/2020 9:10 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Moisture 98.4 % 0.010 Test Results Units MOL Total Solids 1.61 % 0.010 Total Volatile Solids 72.0 % 0.010 1 10/08/2016:06 FMM SM-2540G DF Date / Time By Analytical Analyzed Method 1 10/08/2016:06 FMM SM-2540G 1 10/08/2016:06 FMM SM-254OG Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 5 SANIPLE, `I RJ A, 7h71 V II�II IfII) IMI BI�II II�� I�I� �l ���I �II �II'II �� 0 4620, 20 CIN of Monroe 14 17 Ken Moths FODY Office Information F Customer Information Rept;;' Submitted By Charge To Copy To Project 5 City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: t ? o Date Recd: l tl [Z:iS Glass ( or Sampled Time: ; t o Time Recd: Plastic es r Sampled B p y: �,r. s Recd By: Relinquished B Signature Date Time Received By: (Signature) Date Time D- 1 '" i Please Place a "X" by Desired Tests Internal Lab Code: Solids % TKN P K S Ca Mg Na Fe At Mn Cu Zn NH4-N NO3-N Cd Cr Ni Pb As Hg Se pH CaCO3 Eq. % Volatile Solids % Org-N Mo Cl B Ba X SO4 Ag Sb Co Sn Ti V Be ALK SS Avail P Sol K Cond WIN SOL B SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH CaO CaCO3 M CO3 MgO, C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments n AN w 0 in v rn rt w (2) Waypo int. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WWTP Cake Ken Morris Report Date : 10/15/2020 775 Treeway Dr Information : Received : 10/06/2020 Monroe , NC 28110 D IG��G mm f�l C'/QOW Pauric Mc Groary Ph.D., CPAAgronomist Report Number : 20-280-0006 REPORT OFANALYSIS Lab No : 73892 Matrix: Solids Sample ID: WWTP Cake Sampled: 10/5/2020 8:25 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 79.5 % 0.010 1 10/08/20 16:06 FMM SM-254OG Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 1870 mg/Kg - dry 122 1 10/13/20 14:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N 178 mg/Kg - dry 23.2 1 10/13/20 13:54 ZBD 4500NO3F-2011 Organic N 50200 mg/Kg - dry 1220 1 10/13/20 10:00 CALCULATION pH 6.2 s.u. 1 10/12/2016:30 ADM 9045D Total Solids 20.5 % 0.010 1 10/08/20 16:06 FMM SM-2540G Total Volatile Solids 56.4 % 0.010 1 10/08/20 16:06 FMM SM-2540G Total Kjeldahl Nitrogen 52200 mg/Kg - dry 1220 1 10/13/20 10:00 JPJ ')M-4500-NH3C-TKP Phosphorus 25200 mg/Kg - dry 24.4 1 10/12/20 19:46 TJS 6010D Aluminum 16500 mg/Kg - dry 24.4 1 10/12/20 19:46 TJS 6010D - Arsenic 11.0 mg/Kg - dry 2.44 1 10/12/20 19:46 TJS 6010D Calcium 15500 mg/Kg - dry 244 1 10/13/20 17:59 TJS 6010D Cadmium 1.28 mg/Kg - dry 0.488 1 10/12/20 19:46 T]S 6010D Chromium 86.3 mg/Kg - dry 1.22 1 10/12/20 19:46 TJS 6010D Copper 355 mg/Kg - dry 2.44 1 10/12/20 19:46 TJS 6010D Iron 71700 mg/Kg - dry 244 5 10/13/20 18:04 TJS 6010D Lead 21.4 mg/Kg - dry 1.46 1 10/12/20 19:46 TJS 6010D Magnesium 2240 mg/Kg - dry 24.4 1 10/12/20 19:46 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 7 (2) WayPoint 7621 Whitepine Road, Richmond, VA 23237 , Main 804-743-9401 ° Fax 804-271-6446 A N A LYTI CAL www.waypointanalytical.com 46205 City of Monroe Project WWTP Cake Ken Morris Report Date : 10/15/2020 775 Treeway Dr Information : Received : 10/06/2020 Monroe , NC 28110 � Report Number: 20-280-0006 REPORT Of ANALYSIS Pauric Mc Groary Ph.D., CPAAgronomist Lab No : 73892 Matrix: Solids Sample ID: WWTP Cake Sampled: 10/5/2020 8:25 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Manganese 1720 mg/Kg - dry 2.44 1 10/12/20 19:46 ]ADS 6010D Mercury 0.309 mg/Kg - dry 0.0736 1 10/13/20 13:25 DDB SW-7471B Molybdenum 18.2 mg/Kg - dry 1.22 1 10/12/20 19:46 TJS 6010D Nickel 70.7 mg/Kg - dry 1.22 1 10/12/20 19:46 TJS 6010D Potassium 2560 mg/Kg - dry 48.8 1 10/12/20 19:46 TJS 6010D Selenium <2.44 mg/Kg - dry 2.44 1 10/12/20 19:46 TJS 6010D Sodium 732 mg/Kg - dry 122 1 10/13/20 17:59 TJS 6010D Zinc 1010 mg/Kg - dry 6.10 1 10/12/20 19:46 TJS 6010D Sulfur 9510 mg/Kg - dry 48.8 1 10/13/20 17:59 TJS 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 4 of 7 S11MPL T City , I N&)nioe WW iP Cake II�II III I I II I IlIM INII �I lIIII III NI I IIII I� 6-�': "hO}' 14 27 46 Office Information vustomer intormation Rept# Submitted By Charge To Copy To Project o►ryi`s Cityof Monroe Acct # POB 69 Email 46205 Monroe NC 213111 :s@ o Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: _ _ ,1 o Date Recd: L W WTP Cake Glass (Ys or o Sampled Time: ; a� Time Recd: Plastic e ram) Sampled By: ►Aov-ynL Recd By: Relinquished By: (Signature) Date Time Received By: (Signature) Date Time Please Place a " X" by Desired Tests Internal Lab Code: SLMONR Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N x x x x x x x x x x x x x x x Cd Cr Ni Pb As Hg Se pH CaCO3 Eq. % Volatile Solids % Or -N Mo Cl B Ba x x x x x x x x x x x iSO4 Ag Sb Co Sn Tf V Be ALK S5' AvailP' Sol K Cond WIN SOL B StAL NA O&G• -SR.3R. TSS Steve#20 Sieve#80 Steve#100 ASH Ca0 1 CaCO3 M CO3 MgO C/N TOC Env TOTAL 205 TOTAL K20 TN TKNW NH4W NO3W I ORGN•W PA CERT AZ CERT BTU PCBS R CT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA 5 octal Instructions or Remarks Comments (2) Waypo int. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WTP Ferric Cake Ken Morris Report Date : 10/15/2020 775 Treeway Dr Information : Received : 10/06/2020 Monroe , NC 28110 D I Aw�G mm f�l �Qp W 4 Pauric Mc Groary Ph.D., CPAAgronomist Report Number : 20-280-0005 REPORTOPANALYSIS Lab No : 73891 Sample ID : WTP Ferric Cake Matrix: Sampled: Solids 10/5/2020 10:28 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 66.6 % 0.010 1 10/08/20 16:06 FMM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 431 mg/Kg - dry 74.9 1 10/13/20 14:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N <14.5 mg/Kg - dry 14.5 1 10/13/20 13:53 ZBD 4500NO3F-2011 Organic N 18400 mg/Kg - dry 749 1 10/13/20 10:00 CALCULATION pH 5.9 S.U. 1 10/12/2016:30 ADM 9045D Total Solids 33.4 % 0.010 1 10/08/20 16:06 FMM SM-254OG Total Volatile Solids 36.5 % 0.010 1 10/08/20 16:06 FMM SM-2540G Total Kjeldahl Nitrogen 18800 mg/Kg - dry 749 1 10/13/20 10:00 JPJ >M-4500-NH3C-TKP Phosphorus 2530 mg/Kg - dry 15.0 1 10/12/20 19:41 TJS 6010D Aluminum 4790 mg/Kg - dry 15.0 1 10/12/20 19:41 TJS 6010D Arsenic 17.2 mg/Kg - dry 1.50 1 10/12/20 19:41 TJS 6010D Calcium 1950 mg/Kg - dry 749 5 10/13/20 17:49 TJS 6010D Cadmium 5.48 mg/Kg - dry 0.299 1 10/12/20 19:41 TJS 6010D Chromium 219 mg/Kg - dry 0.748 1 10/12/20 19:41 TJS 6010D Copper 395 mg/Kg - dry 1.50 1 10/12/20 19:41 TJS 6010D Iron 311000 mg/Kg - dry 599 20 10/13/20 17:54 TJS 6010D Lead <0.898 mg/Kg - dry 0.898 1 10/12/20 19:41 TJS 6010D Magnesium 404 mg/Kg - dry 15.0 1 10/12/20 19:41 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 7 (2) • O' Way �� 7621 Whitepine Road, Richmond, VA 23237 P , Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Project WTP Ferric Cake Ken Morris Report Date : 10/15/2020 775 Treeway Dr Information : Received : 10/06/2020 Monroe , NC 28110 Report Number :20-280-0005 REPORT OFANAL YSIS Pauric Mc Groary Ph.D., CPA Agronomist Lab No : 73891 Sample ID: WTP Ferric Cake Matrix: Solids Sampled: 10/5/2020 10:28 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Manganese 829 mg/Kg - dry 1.50 1 10/12/20 19:41 ]ADS 6010D Mercury <0.0476 mg/Kg - dry 0.0476 1 10/13/20 13:22 DDB SW-7471B Molybdenum 46.7 mg/Kg - dry 0.748 1 10/12/20 19:41 TJS 6010D Nickel 35.9 mg/Kg - dry 0.748 1 10/12/20 19:41 TJS 601 OD Potassium 238 mg/Kg - dry 29.9 1 10/12/20 19:41 TJS 6010D Selenium <7.49 mg/Kg - dry 7.49 5 10/13/20 17:49 TJS 6010D Sodium <374 mg/Kg - dry 374 5 10/13/20 17:49 TJS 6010D Zinc 140 mg/Kg - dry 3.74 1 10/12/20 19:41 TJS 6010D Sulfur 2270 mg/Kg - dry 150 5 10/13/20 17:49 TJS 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 4 of 7 SAMPLE !III!INIIINIIIIIIIIIMIIIINIIIIIIIII IIINII11111002020 City of Monroe 14 2. 35 W 1 P Fvrnc Cake CUSTODY Office Information Customer Information Rept# FAcct Submitted By Charge To Copy To Project 1Ko r r City of Monroe # PC sg Email 46205 Monroe NC 28111 kY'UreZ n - Or Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: t� -5 _ o Date Reed: - -` ��' TP Ferris t;:,1i e Glass (fie o o Sampled Time: >' a i Time Recd: Plastic es or W) Sampled B : ;S Recd By: Relinquished By: (Signature) Date Time Received B Signature) Date Time Please Place a "X" by Desired Tests Internal Lab Code: SLMONR Solids % TKN • P _ K' . S x :Ca '' mg Na< < Fe All: Mn Cu Zn NH4-N NO3-N X. ,. Cd X Cri x Nla x X X H' X -.Se x H x CaCO3., E�.:Y• x Volatile' X r-N X Mo X CI X B x Ba X r SO4„ X A - X -Sbs X ' Co; . X `Sn -:' X T1 X : V.'-` X = .Be ALK:- ` X �Ss t X .Avail,P; X :.Sol K Cond WIN SOL B SOL NA 0&G ' = SP.GR. TSS, 61eve#20 ySlev_ej€80 Sieve#100 4 SASH 4 r Ca0 CaCO3 M CO3 M O» :: C/N TOC Env TQTAL P205$ TQ. AI,.v 11<20 rt'• TN KNW_ JNHW4.NOW ORGN-W PA CER7 AZ CERT -;,BTU': PCBS `CN FECAL TCLP ICR f State Certification Needed: NORTH CAROLINA pecial Instructions or Remarks Comments I ^I rn a E (--- aceAnalytical Report of Analysis City of Monroe PO Box 69 Monroe, NC 28111 Attention: Ken Morris Project Name: Land Application Lot Number:VJ08015 Date Completed:10/25/2020 10/26/2020 10:41 AM Approved and released by: Project Manager I: Hannah K. Lucas rpCAAB 1 ANSI NallonalAcna0 ACCREDI1 T TE EDD TESTING LA001UTORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 18 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative City of Monroe Lot Number: VJ08015 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. Inorganic non-metals The pH analysis associated with the samples in this report were performed after the method recommended 15 minute holding time. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of 18 a PACE ANALYTICAL SERVICES, LLC Sample Summary City of Monroe Lot Number: VJ08015 Sample Number Sample ID Matrix Date Sampled Date Received 001 WWTP CAKE Solid 10/05/2020 0842 10/07/2020 002 WTP CAKE Solid 10/05/2020 1030 10/07/2020 (2 samples) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 18 Inorganic non-metals Client:City of Monroe Laboratory ID: VJ08015-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/05/2020 0842 % Solids: 20.0 10/09/2020 0009 Date Received:10/07/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ignitability) 1010A 1 10/14/2020 1250 KMC 69894 1 (Reactive Cya) 7.3.3 1 10/20/2020 0000 MSG 10/17/2020 1622 1 (Reactive Sul) 7.3.4 1 10/20/2020 2207 SRB 10/17/2020 1622 1 (Soil pH meas) 9045D 1 10/16/2020 1747 AAB 70227 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 o F 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 ND 50 mg/kg 1 Soil pH measured in water @ 20.8 ° C 9045D 6.2 su 1 a LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 18 TCLP Volatiles Client: City of Monroe Laboratory ID: VJ08015-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/05/2020 0842 % Solids: 20.0 10/09/2020 0009 Date Received:10/0712020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/5030B 8260D 10 10/15/2020 1514 TML 70049 10/13/2020 2311 CAS Analytical Parameter Number Method Result Q LOQ Units Run Benzene 71-43-2 8260D ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260D ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 8260D ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260D ND 0.050 mg/L 1 Chloroform 67-66-3 8260D ND 0.050 mg/L 1 1,2-Dichloroethane 107-06-2 8260D ND 0.050 mg/L 1 1,1-Dichloroethene Tetra chloroethene 75-35-4 127-18-4 8260D 8260D ND ND 0.050 0.050 mg/L mg/L 1 1 Trichloroethene 79-01-6 8260D ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260D ND 0.010 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 96 70-130 1,2-Dichloroethane-d4 92 70-130 Toluene-d8 96 70-130 LOO = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 18 TCLP Semivolatiles Client: City of Monroe Laboratory ID: VJ08015-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/05/2020 0842 % Solids: 20.0 10/09/2020 0009 Date Received:10107/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 10/23/2020 1206 SCD 10/21/2020 1830 70692 10/13/2020 2311 Parameter CAS Number Analytical Method 1,4-Dichlorobenzene 106-46-7 8270E 2,4-Dinitrotoluene 121-14-2 8270E Hexachlorobenzene 118-74-1 8270E Hexachlorobutadiene 87-68-3 8270E Hexachloroethane 67-72-1 8270E 2-Methylphenol 95-48-7 8270E 3+4-Methylphenol Nitrobenzene 106-44-5 98-95-3 8270E 8270E Pentachlorophenol 87-86-5 8270E Pyridine 110-86-1 8270E 2,4,5-Trichlorophenol 95-95-4 8270E 2,4,6-Trichlorophenol 88-06-2 8270E Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl H 84 37-129 2-Fluorophenol H 44 24-127 Nitrobenzene-d5 H 83 38-127 Phenol-d5 H 68 28-128 Terphenyl-d14 H 96 10-148 2,4,6-Tribromophenol H 84 41-144 Result Q LOQ Units Run ND H 0.040 mg/L 1 ND H 0.080 mg/L 1 ND H 0.040 mg/L 1 ND H 0.040 mg/L 1 ND H 0.040 mg/L 1 ND H 0.040 mg/L 1 ND H 0.040 mg/L 1 ND H 0.040 mg/L 1 ND H 0.20 mg/L 1 ND H 0.040 mg/L 1 ND H 0.040 mg/L 1 ND H 0.040 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 18 TCLP Herbicides I Client: City of Monroe Laboratory ID: VJ08015-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/05/2020 0842 % Solids: 20.0 10/09/2020 0009 Date Received: 10107/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 10/23/20201531 JJG 10/21/20201959 70687 10/13/20202311 CAS Analytical Parameter Number Method Result Q LOQ Units Run 2,4-D 94-75-7 8151A ND H 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND H 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA H 78 50-112 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitalion of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 18 TCLP Pesticides Client: City of Monroe Laboratory ID: VJ08015-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/05/2020 0842 % Solids: 20.0 10/09/2020 0009 Date Received: 10107/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311 /3520C 8081 B 1 10/22/2020 1640 DAL1 10/21 /2020 1245 70636 10/13/2020 2311 CAS Analytical Parameter Number Method Result Q LOQ Units Run gamma-BHC (Lindane) 58-89-9 8081B ND H 0.00040 mg/L 1 Chlordane 57-74-9 8081B ND H 0.0040 mg/L 1 Endrin 72-20-8 8081B ND H 0.00040 mg/L 1 Heptachlor 76-44-8 8081B ND H 0.00040 mg/L 1 Heptachlor epoxide 1024-57-3 8081 B ND H 0.00040 mg/L 1 Methoxychlor 72-43-5 8081 B ND H 0.0016 mg/L 1 Toxaphene 8001-35-2 8081B ND H 0.0080 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl H 78 20-131 Tetrachloro-m-xylene H 79 26-132 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 8 of 18 TCLP Metals Client: City of Monroe Laboratory ID: VJ08015-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/05/2020 0842 % Solids: 20.0 10/09/2020 0009 Date Received:10/0712020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3010A 601OD 1 10/15/2020 1930 KSH2 10/15/2020 0910 69970 10/13/2020 2311 1 1311/7470A 7470A 1 10/15/2020 1401 JAB2 10/15/2020 0805 69958 10/13/2020 2311 CAS Analytical Parameter Number Method Result Q LOQ Units Run Arsenic 7440-38-2 601OD ND 0.15 mg/L 1 Barium 7440-39-3 601OD ND 0.25 mg/L 1 Cadmium 7440-43-9 601OD ND 0.050 mg/L 1 Chromium 7440-47-3 601OD ND 0.10 mg/L 1 Lead 7439-92-1 601OD ND 0.10 mg/L 1 Mercury Selenium 7439-97-6 7782-49-2 7470A 601OD ND ND 0.0020 0.20 mg/L mg/L 1 1 Silver 7440-22-4 6010D ND 0.10 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 9 of 18 Inorganic non-metals Client: City of Monroe Laboratory ID: VJ08015-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/05/2020 1030 % Solids: 50.3 10/09/2020 0009 Date Received:10/07/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ignitability) 1010A 1 10/14/2020 1441 KMC 69894 1 (Reactive Cya) 7.3.3 1 10/20/2020 0000 MSG 10/17/2020 1622 1 (Reactive Sul) 7.3.4 1 10/20/2020 2207 SRB 10/17/2020 1622 1 (Soil pH meas) 9045D 1 10/16/2020 1750 AAB 70227 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 ° F 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 ND 50 mg/kg 1 Soil pH measured in water @ 21 ° C 9045D 5.3 su 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 10 of 18 TCLP Volatiles Client: City of Monroe Laboratory ID: VJ08015-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/05/2020 1030 % Solids: 50.3 10/09/2020 0009 Date Received:10/07/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/5030B 8260D 10 10/15/2020 1537 TML 70049 10/13/2020 2311 CAS Analytical Parameter Number Method Result Q LOQ Units Run Benzene 71-43-2 8260D ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260D ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 8260D ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260D ND 0.050 mg/L 1 Chloroform 67-66-3 8260D ND 0.050 mg/L 1 1,2-Dichloroethane 107-06-2 8260D ND 0.050 ni 1 1,1-Dichloroethene Tetra chloroethene 75-35-4 127-18-4 8260D 8260D ND ND 0.050 0.050 mg/L mg/L 1 1 Trichloroethene 79-01-6 8260D ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260D ND 0.010 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 93 70-130 1,2-Dichloroethane-d4 94 70-130 Toluene-d8 93 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quanlitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % 11 = Out of holding time 'A = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 11 of 18 TCLP Semivolatiles Client:City of Monroe Laboratory ID: VJ08015-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/05/2020 1030 % Solids: 50.3 10/09/2020 0009 Date Received:10/07/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 10/23/2020 1601 SCD 10/21/2020 1830 70692 10/13/2020 2311 CAS Analytical Parameter Number Method Result Q LOQ Units Run 1,4-Dichlorobenzene 106-46-7 8270E ND H 0.040 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270E ND H 0.080 mg/L 1 Hexachlorobenzene 118-74-1 8270E ND H 0.040 mg/L 1 Hexachlorobutadiene 87-68-3 8270E ND H 0.040 mg/L 1 Hexachloroethane 67-72-1 8270E ND H 0.040 mg/L 1 2-Methylphenol 95-48-7 8270E ND H 0.040 mg/L 1 3+4-Methylphenol 106-44-5 8270E ND H 0.040 mg/L 1 Nitrobenzene 98-95-3 8270E ND H 0.040 mg/L 1 Pentachlorophenol 87-86-5 8270E ND H 0.20 mg/L 1 Pyridine 110-86-1 8270E ND H 0.040 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270E ND H 0.040 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270E ND H 0.040 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl H 89 37-129 2-Fluorophenol H 60 24-127 Nitrobenzene-d5 H 94 38-127 Phenol-d5 H 76 28-128 Terphenyl-d14 H 102 10-148 2,4,6-Tribromophenol H 82 41-144 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 12 of 18 TCLP Herbicides � I Client: City of Monroe Laboratory ID: VJ08015-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/05/2020 1030 % Solids: 50.3 10/09/2020 0009 Date Received:10107/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 10/23/20201555 JJG 10/21/20201959 70687 10/13/20202311 CAS Analytical Parameter Number Method Result Q LOQ Units Run 2,4-D 94-75-7 8151A ND H 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND H 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA H 81 50-112 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 13 of 18 TCLP Pesticides Client: City of Monroe Laboratory ID: VJ08015-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/05/2020 1030 % Solids: 50.3 10/09/2020 0009 Date Received:10/07/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 10/22/20201656 DAL1 10/21/20201245 70636 10/13/20202311 CAS Analytical Parameter Number Method Result Q LCQ Units Run gamma-BHC (Lindane) 58-89-9 8081B ND H 0.00040 mg/L 1 Chlordane 57-74-9 8081B ND H 0.0040 mg/L 1 Endrin 72-20-8 8081B ND H 0.00040 mg/L 1 Heptachlor 76-44-8 8081 B ND H 0.00040 mg/L 1 Heptachlor epoxide 1024-57-3 8081B ND H 0.00040 mg/L 1 Methoxychlor 72-43-5 8081B ND H 0.0016 mg/L 1 Toxaphene 8001-35-2 8081B ND H 0.0080 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl H 82 20-131 Tetrachloro-m-xylene H 74 26-132 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 14 of 18 TCLP Metals Client: City of Monroe Laboratory ID: VJ08015-002 Description: WTP CAKE Matrix: Solid Date Sampled:110/05/2020 1030 % Solids: 50.3 10/09/2020 0009 )ate Received:10/07/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3010A 601 OD 1 10/15/2020 1933 KSH2 10/15/2020 0910 69970 10/13/2020 2311 1 1311/7470A 7470A 1 10/15/2020 1404 JAB2 10/15/2020 0805 69958 10/13/2020 2311 Parameter CAS Number Analytical Method Result Q LOQ Units Run Arsenic 7440-38-2 601OD ND 0.15 mg/L 1 Barium 7440-39-3 601OD ND 0.25 mg/L 1 Cadmium 7440-43-9 601OD ND 0.050 mg/L 1 Chromium 7440-47-3 601OD ND 0.10 mg/L 1 Lead 7439-92-1 6010D ND 0.10 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 mg/L 1 Selenium 7782-49-2 601OD ND 0.20 mg/L 1 Silver 7440-22-4 601OD ND 0.10 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 15 of 18 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 16 of 18 !r <CD � D M S 0 5� oz M N r r CD m 0 o 3 C 3 m y (� m mr J C N 0 � m o= ro y �o 2 O y '�-e�,�' Ghulr� oi`Gusti�avJ�scor� t;lle�t (� Fiepert t� 1 � o -{ r ly 1'4e .. --- Cr, i7ttcl Kw, AJdress I Telophaia No. `l OA (q Emal Ci(}' SFoir: Gip (:rxie Prx�cr oiM'fl� N4C_ d FF 1 1 l i.tln ,r3 Project)) � � 2.Nao>I harlw L OL* 1 P.� J� 0 r �(R 3. ii �546 Project —� P.O Nunbsr HLMIJ6r 5lima'rD; t1MH1IL'111 IGo tolion (C�antl�rxrs'c�r u�rc'I;arell:iu nary be Oaie cdo`tvned to 0 ,e line}) Shcaly Environi-nenta! Services, Inc. l06 Vantage Po;n- Criv-a West Columbia, Soutt CO'DlirlR 29172 Number 57242 Telepnunc-No. eD:s-79l-9700 Fax ire. &j3-r5?1-91'I; vw',5 Siletll�lut.o7r rY� Glt•r Qt-oGe Va A ' l; (Pj-Mpd Namj) 4 Fvaid Paramew-s {j.e., pti, terip, rj � ca-1 ba re❑orted txl!nw Page - j ref r !+urrber of Lai .1e13 4-ii`Jil.9 [arlalxrTy r-P'ui aliss y' I hrn5rr'x1ht; (usnduje ur lait) v" �� 50lunTiksdtasa if ��lA __ ! Matrix rn a .� S I,I�I�/ .. f, s , +�}tr�pl/�� Cull:' tin Q, c •t'�ry }3tY Q -F'l l 5 I Time {n Ila 0 to I Intt pp RGran;s / caoifr 10 xOY-.•-_ ��''��o t 1 F ctSr 1 i'Wli;{il Stir. Tumkcune Terra Him1kad (FtiirAan aPProval Mpi: d to mpudded TAT- �iI I�1t1 ❑ Pu Pt aumpie Disposal qC Roqukramen`.s (S(r<�fy} Pass b;e Fa rd IGEnti'IcatfOri - {Pk'a:li pr,�; fj r; Fet�m CII3nY `�aOiSposai bylaC Alazad CRama•abA n'kn Iu6i ( uPd3m cl.Wnoan 1. Relirqulshad 4138 er Daly Time 1. Recsverl by Date rime. L Halil quistl=dE3• [ Da4L Tirllle �+ !F. Rernlvrrl h Date Time a r{nli3 yuiahad E/l Dale I Ime 3. RC v9d by _ - Date Time 4. Reltrq6shedl<g itl^ ...,_.CE:.._ ';.rie 4-- . UUu•al�} Re a ------ Claire — Time [Vote All samples are retained for fourtveeks from receipt unless other arrangements are luau usEC,•i�_Y -- made. Acr,iconlce([h nYar ur.c pl,vPa%k RaciiuT'E: Tamadlank u Y I ZI N i D M Z 1D m C ''0 V/ r n PACE ANALYTICAL SERVICES, LLC I� Samples Receipt Cheeldlst (5114C) (ME001ktC-15) Revised.9129/202D dG+"rUtc7y;Kd! Issuirg AuUiurity: Pace ENV - WCOL gage 1 of 1 Sau1PIe Receipt Checklist (SRC) Gliznt: CITY(J- MONROR Cooterkspecwdbyidatc: r« _! to�sr�tial Lu1,l: VJoRocs F-y- rmeceipt.- ✓ P.c Client. ✓ No I . V� ere custody sca:s pruwnt on the cnolt-O No I ✓ NA 12. If cusloclo• semis were resent; ~Verb th:j itllut [ anti ,>nbr p{ en? IH51iIlID; °__ (�r[or'ineStripIEJ: "" Tmwdby: N4 IOr' giral temperature upon receipt! Derived (Corrcctcd) tcmpe:ature tipon re.ceipL ®Solid Snap -Cup iD:- + l.J q NA / NA :Ic NA i NA e. NA f NA o�, tv4cthod: [�l'c ttperat� DlarJc gainsr Btltr:ra [RGttn ID: ' IR Gun Correction Factor: 0 "C ✓ ?viethol cA coolant: Wt:t h= ❑ Ice Packs ❑ Dn-- Ice None Vcs No 0NA 3. Iftempera'urc of any c;loler cxceedeLiCYC, wes P:UjectNfRnagmr VotftieO PM wus Notified br^. phcine ! email ? fur erica -face (circle one). U res Na J N.4 4. Is rli<; Cora-rel•cial courier's packing slap attached to this ibna7 21 Y'es, NO S. V,'ct e p riper clrstoi} procetlul�s ;rclingoished, tlei awed} followed? ✓ Y•t:s Lj 1.rn G. LVer•e sivavly IDs listed on 11ir C04'-. J Yes ❑ ho 7. Were sample 1ps listed on ail silmplc containers? ✓ Yes -Nol S. Was collection mate & firm- listed on tfie COC" ✓ Yes 1tiu 9. �A'ns collectiurl duw ttn>g lks'ed t)n all .saluple conlaincrs7 Yes ❑Nu 10, Vid all container )Abe" i tfu.-mation (ID, dEte, time) rr cc with tiro CpC'1 J Yes 'dO L : 1. Were es's to by pctformei listed on the CUC? ,. �No 12_ Did 0 €am-ple5 arrive in ills prapar contaircm for each test aji,&ai it: goad condition (,unbroken, Ikh- Un, etc.)? Yes r No 13. Was adequatc sample vu[urrrc available? '— ✓ Ycs N—r 14. Were all sunlpl.s received wilhiro ii the holding timer 4 wbclt:ts, wYwhever c,,rr..cv first' o Yee _ No i5. t�'erc am sarrnlescontainers missioF}rcxccss (circle nnm)satttplesNutlisiu' In CO[? d Yes No ©NA 16. For VOA and RSK• 175 samples., were bubbles prrsent > pea-sizL" (t^o: bntin i:r diamct in auy of the VOA vials? Yes No J RA 17. Vdery Lill DROhretal�,'nurrienr samples r+xcivad at a nN of { 27 _ Yes NO! J INA I 1 S. Wien; a 1 cyanide sannpi95 recei ved al a pH 5 12 and "llfidc sarnu:e:, mc-civrd at a pH > r3" 19. 1 applicaUle NH.,- 'KIN!c}alndetpheno.625.1r60U, (- U.SmpiL) samplCa tree of ❑ ''Yea ❑ND LNAI - ❑ Yzs ❑ No L-1JNA 2r7. Wcrc client remarkv,-cyicsLi ('.c. requested dilutiar:s. ` S q5 ISD dr signation;, Vtc...) Corrrectly lr'snscribcd from the C7C into file ;.t)rnrncnt s:crion in LIMP Yes ✓ No 21. W'as llw uotc nuitther listed on the coiAuin_r Iabzi? !f es, uate r Sample Preservation (Must be ctnrlplcted far any samples) inconvu(l; preserved or with lteadspwx,) With ,were received incgrrect[p pr"Lrved and Were F.djUKLk;d accordingly .r sample L-cccivijr; wide NA nlz, of eirc c onc; H2SO4, FIN03, HU, NaOH usatg SR Y NA I'irne of g, csc: VatiDr'NA if awre thurr, one preser vitivc is tleedrd, plctisc rote in die coimnents below. Sslmp+!e(s) rr^ _were received widl bul+1--6-G nlut in dinmotcr. ISamFdes{s) �a ._ �— ,avvre received w;th "l'lt(; z 0.5 :n�j'L ([f 1i19 is; rru�i e•nd tv�ere acljlwad OCONdingl j in sample receivingC. with socimn thiosulfax (Na,S,S3_) witti Sli dy ID: N,h L•at'code labels applied hy. AHD' CoIntTlants' Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 18 of 18 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 44.6 Land Owner: Ben Myers Annual Dry Tons Applied: 150.9343 Operator: Same Crop 1 Name: Fescue (Past.) Site #: NC-LTN18 Acres Permitted: 44.6 Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 Y y G ro Q Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume A lied er PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cord. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches a E Y F. o w o- �. * 0 W �, -- N o m " co w +� * w 0 TKN mg/kg Y o � oc o mg/kg Nitrate and Nitrite mg/kg PAN Applied (]bs/acre) Name of CropType Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 20 450 20.5 1.742 WTP CAKE D 0 S 0.5 0.4 17,200 1,410 1 22.5 24.539 NA Fescue June 20 450 15.5 1.317 WWTP CAKE D 0 S 0.5 0.3 36,100 4,740 69 31.207 NA Fescue June 20 84 20.5 0.325 WTP CAKE D 0 S 0.5 0.4 17,200 1,410 22.5 4.581 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 984 0 ::::....:. As Cd Cu Cr Pb Hg Mo Ni Se Zn P 60.326 0.000 Lime Applied Annuallbs/acre 0.144 1.168 1.312 36 0.015 0.137 0.152 34 2.944 17.587 20.531 1338 1.528 16.341 17.869 X 0.069 2.079 2.148 267 0.001 0.036 0.037 15 0.312 1.029 1.341 X 0.326 2.956 3.282 374 0.060 0.242 0.302 89 1.564 52.269 53.833 2498 43.178 ::. . Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop ... .. .:: .. .. 122 50 1 ceruiy, unuer penalty of iaw, tnat tnis document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." n / *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 150.93 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Ben Myers Owner: Same Predominant Soil Series: BdB2-Badin Acres Used: 44.6 Acres Permitted: 44.6 Site #: NC-UN18 Field #: 1 Residual Analvsis Data (Heavy Metals and Total Phosphorus use mp-/kE, % Solids use Raw Percent #): . positeWIN Com- Date EMENNUME OEM 0 VIM otal �To"tal Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 21 L3]4 J L 5 L6J 7] L8J 9 10 J 11 12 DT/Ac./ App. Event 2.07 1.32 Arsenic 0.000 1 0.000 0.000 0.101 0.043 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.144 Cadmium 0.000 0.000 0.000 0.010 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015 Copper 0.000 0.000 0.000 1.906 1.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.944 lChromium 0.000 0.000 0.000 1.112 0.416 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.528 Lead 0.000 0.000 0.000 0.033 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.069 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.000 0.000 0.000 0.230 0.082 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.312 denum Nickel 0.000 0.000 0.000 0.187 0.139 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.326 Selenium 0.000 0.000 0.000 0.050 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.060 Zinc 0.000 0.000 0.000 0.234 1.330 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.564 ITotal Phos- 0.000 0.000 0.000 12.361 30.818 0.000 0.000 0.000 0.000 0.000 0.000 0.000 43.178 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) M ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Ben Myers Operator: Same Crop 1 Name: Fescue (Past.) WQ Permit #: WQ0001346 Field #: 2 Annual Dry Tons Applied: 125.3154 Site #: NC-UN18 Acres Utilized: 27.6 Acres Permitted: 27.6 Predominant Soil Series: GoB-Golston Cation Exchange Capacity (non 503): N/A Crop 1 Max. PAN: 135 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 o = Q Volume applied pP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, W # Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist) Precip. Past 24 Hrs. inches y 4 b 0 d o� * ° ° o w co * 7y w ° * w TKN mg/kg Z a E3 o El °O ° 2. mg/kg Nitrate and Nitrite mg/kg PAN Applied (]bs/acre) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 Oct 20 250 20.5 1.564 WWTP D 0 S 0.5 0.3 52,200 1,870 178 50.705 NA Fescue Oct 20 125 33.4 1.274 WTP D 0 S 0.5 0.4 18,800 431 14.5 19.307 NA Fescue Nov 20 150 20.5 0.938 WWTP D 0 S 0.5 0.3 52,200 1,870 178 30.423 NA Fescue Nov 20 75 33.4 0.764 WTP D 0 S 0.5 0.4 18,800 431 14.5 11.584 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 6001 o As Cd Cu Cr Pb Hg Mo Ni Se Zn P 112.0191 0.000 Lime Applied Annuallbs/acre 0.125 4.869 4.994 36 0.029 0.468 0.497 34 3.386 27.628 31.014 1338 1.324 19.743 21.067 1 X 0.111 5.175 5.286 267 0.002 1.441 1.443 15 0.281 3.816 4.097 X 0.500 4.966 5.466 374 0.043 2.422 2.465 89 5.625 65.755 71.380 2498 136.413:::: :::::::::::::::::::::::::: .................. .......................... Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop 135 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Permit #: WQ0001346 Operator: Ben Myers Owner: Acres Used: 27.6 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Same Predominant Soil Series: 27.6 Site #: NC-UN18 Field #: 125.30 N/A GoB-Golston 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 L2]3 j4 5 6 7 8 9 J 110111 10/5/20 J 10/5/20 12 % Solids 20.5 33.4 Arsenic 11 17.2 Cadmium 1.28 5.48 Copper 355 395 Chromium 86.3 219 Lead 21.4 0.898 Mercury 0.309 0.0476 Molyb- denum 18.2 46.7 Nickel 70.7 35.9 Selenium 2.44 7.49 Zinc 1010 140 Total I Phos- horus 25200 2530 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ITotal DT/Ac./ App. Event 1 1 1 21 L3J L4 J L5]6j L 7 8 9] 1101 2.50 11 J 2.04 12 y 0 Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 0.000 0.055 1 0.070 0.000 0.125 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.022 0.000 0.029 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.776 1.610 0.000 3.386 ^hromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.432 0.893 0.000 1.324 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.107 0.004 0.000 0.111 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.002 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.091 0.190 0.000 0.281 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.354 0.146 0.000 0.500 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.012 0.031 1 0.000 0.043 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.054 0.571 0.000 5.625 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 126.101 10.312 0.000 136.41 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier ,9a-(a-11 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 7 Acres Utilized: 5.7 Land Owner: Ben Myers Annual Dry Tons Applied: 27.1533 Site #: NC-UN18 Acres Permitted: 5.7 Operator: Same Crop 1 Name: Fescue (Past. Predominant Soil Series: CmB-Cid Crop 1 Max. PAN: 141 Cation Exchange Capacity (non 503): N/A Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: -3 Y U Q Volume applied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons /o Solids Volume A hed er PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist) Precip. Past 24 Hrs. inches y � � �° ° oa w * o w W _ co -- * N' o' = � � I 9 w * w TKN mg/kg Z a o 3 oo ° CD R. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Sept 20 28 31.5 1.303 WTP Cake D 0 S 0.5 0.4 12,500 317 28.4 13.188 NA Fescue Sept 20 98 23.9 3.461 WWTP Cake D 0 S 0.5 0.3 33,800 2120 91.6 73.749 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 1 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 126 0 ::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 86.938 1 0.000 Lime Ap plied Annuallbs/acre 0.184 0.011 4.301 1.328 0.151 0.003 0.234 0.585 0.056 5.941 124.275 .......... ....... Date lbs/ac Prior Years Cumulative lbs/ac 0.671 0.115 16.281 6.361 1.015 0.018 1.18 2.697 0.301 31.824 Current Cumulative lbs/ac 0.855 0.126 20.582 7.689 1.166 0.021 1.414 3.282 0.357 37.765 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit lst/2nd Crop 141 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." y� *Application Method: S - Surface, IN - Injection, INC - Incorporation �,Z.2-�LAG A( **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 27.15 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Ben Myers Owner: Same Predominant Soil Series: CmB-Cid Acres Used: 5.7 Acres Permitted: 5.7 Site #: NC-UN18 Field #: 7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 11 L2J3 4 5 6 7 7/1/20 8 8/12/20 % Solids 31.5 23.9 Arsenic 32.1 14.5 Cadmium 2.21 0.828 Copper 394 473 Chromium 228 106 Lead 4.76 20 Mercury 0.0485 0.448 I Molyb- denum 42.9 17.7 Nickel 37.8 70.3 Selenium 15.9 2.09 Zinc 168 795 Total I Phosn 3330 16700 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 1 1 1 2 J L3JL4J L5J L6J7 8J L9J 10 11 12 ITotal DT/Ac./ oyr App. Event 1.30 3.46 Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 1 0.084 0.100 0.000 0.000 0.000 0.000 0.184 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.006 0.000 0.000 0.000 0.000 0.011 Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.027 3.274 0.000 0.000 0.000 0.000 4.301 1-hromium 0.000 0.000 0.000 0.000 0.000 0.000 0.594 0.734 0.000 0.000 0.000 0.000 1.328 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.012 0.138 0.000 0.000 0.000 0.000 0.151 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.000 0.003 Molyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.112 0.123 0.000 0.000 0.000 0.000 0.234 denum Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.099 0.487 0.000 0.000 0.000 0.000 0.585 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.041 0.014 0.000 0.000 0.000 0.000 0.056 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.438 5.503 0.000 0.000 0.000 0.000 5.941 Tota Phosl 0.000 0.000 0.000 0.000 0.000 0.000 8.678 115.597 0.000 0.000 0.000 0.000 124.28 -'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance With a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Xo-- A4vo,+,- Signature of Land Applier ate( Date DENR FORM MFLSF (12/2006) s ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 8 Acres Utilized: 16 Land Owner: Ben Myers Annual Dry Tons Applied: 72.4606 Site #: NC-UN18 Acres Permitted: 16 Operator: Same Crop 1 Name: Fescue (Past.) Predominant Soil Series: CmB-Cid Crop 1 Max. PAN: 141 Cation Exchange Capacity (non 503): N/A Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 O Y N q Y o Q Volume applied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons /o Solids Volume A lied er PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Wasteetc) , Soil Cond. (Dry' Wet' Moist) Precip. Past 24 Hrs. inches y q b o � n * � o w * N' *� o' 0 w -, °= * N *� 0 TKN mg/kg z a q o El ao ° � � �. mg/kg Nitrate and Nitrite mg/kg PAN Applied (]bs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Sept 20 360 23.9 4.529 WWTP Cake D 0 S 0.5 0.3 33,800 2,120 91.6 96.514 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS:J 360 0 :.: As Cd Cu Cr Pb HR Mo Ni Se Zn P 96.514 0.000 Lime Applied Annuallbs/acre 0.131 0.008 4.285 0.960 0.181 0.004 0.160 0.637 0.019 7.203 151302 Date lbs/ac Prior Years Cumulative lbs/ac 0.658 0.115 13.555 3.481 0.995 0.023 1.108 0.906 0.193 27.589 Current Cumulative lbs/ac 0.789 0.123 1 17.840 4.441 1.176 0.027 1.268 1.543 0.212 34.792 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit l st/2nd Crop 141 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." / *Application Method: S - Surface, IN - Injection, INC - Incorporation . -eti. **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Permit #: WQ0001346 Operator: Ben Myers Owner: Acres Used: 16 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Same Predominant Soil Series: 16 Site #: NC-UN18 Field #: 72.48 N/A CmB-Cid 8 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 6 7 8 8/ 12/20 9 10 11 12 % Solids 23.9 Arsenic 14.5 Cadmium 0.828 Copper 473 Chromium 106 Lead 20 Mercury 0.448 Molyb- denum 17.7 Nickel 70.3 Selenium 2.09 Zinc 795 Total I Phos- horus 16700 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ITotal DT/Ac./ App. Event 1 1 1 L 2 3 4 L_j5 6 7 8 4.53 9 10 11 12 o Arsenic 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.131 0.000 0.000 0.000 0.000 0.131 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 0.000 0.000 0.000 0.000 0.008 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.285 0.000 0.000 0.000 0.000 4.285 hromiu 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.960 0.000 0.000 0.000 0.000 0.960 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.181 0.000 0.000 0.000 0.000 0.181 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.160 0.000 0.000 0.000 0.000 0.160 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.637 0.000 1 0.000 0.000 0.000 0.637 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 0.000 0.000 0.000 0.000 0.019 Zinc 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 7.203 0.000 0.000 0.000 0.000 1 7.203 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 151.302 0.000 0.000 0.000 0.000 151.30 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: William Griffin Operator: Same WQ Permit #: WQ0001346 Field #: 3 Annual Dry Tons Applied: 37.6199 Site #: NC-UN29 Predominant Soil Series: BaB-Badin Acres Utilized: 7.4 Acres Permitted: 7.4' Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 C� Volume applied PP enter one Solids/ ( ) Liquid 9 Cu. Yds Gallons u /o Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches D r° b �' o F a * ° o w w io N w p- * w 0 TKN mg/kg Z. a o °Q ° mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 Sept 20 150 23.9 4.080 WWTP Cake D 0 S 0.5 0.3 33,800 2,120 91.6 86.949 NA Fescue Sept 20 28 31.5 1.004 WTP Cake D 0 S 0.5 0.4 12,500 317 28.4 10.158 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ........ .......... TOTALS: 178 0 ::::::::... As Cd Cu Cr Pb Hg Mo Ni Se Zn I P 97.108 0.000 Lime Applied Annuallbs/acre 0.183 0.011 4.648 1.321 0.173 0.004 0.230 0.649 0.049 6.823 142.932 Date lbs/ac Prior Years Cumulative lbs/ac 0.867 0.127 23.288 9.578 1.285 0.023 1.849 3.446 0.868 37.79 Current Cumulative lbs/ac 1.050 0.138 27.936 10.899 1.458 0.027 2.079 4.095 0.917 44.613 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit Ist/2nd Crop 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation A14-1,c� v2/v2 �.oL J **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 37.59 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: William Griffin Owner: Same Predominant Soil Series: BaB-Badin Acres Used: 7.4 Acres Permitted: 7.4 Site #: NC-UN29 Field #: 3 Residual Com- posite Date % Solids Arsenic Cadmium Lead Data Metals and Total Phosphorus use 7/ 1 /20 31.5 32.1 2.21 394 228 4.76 0.0485 8/12/20 23.9 14.5 0.828 473 106 20 0.448 % Solids use Raw Percent #): denum 42.9 1 17.7 Nickel 37.8 70.3 Selenium 15.9 2.09 Zinc 168 795 Total I Phos- horus 3330 16700 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 L 2j 3 4j 5 6 7 1.00 8 4.08 9 10 11 12 o Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.064 1 0.118 0.000 0.000 0.000 0.000 0.183 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.007 0.000 0.000 0.000 0.000 0.011 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.788 3.860 0.000 0.000 0.000 0.000 4.648 :_'hromium 0.000 0.000 0.000 0.000 0.000 0.000 0.456 0.865 0.000 0.000 0.000 0.000 1.321 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.010 0.163 0.000 0.000 0.000 0.000 0.173 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.086 0.144 0.000 0.000 0.000 0.000 0.230 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.076 0.574 0.000 0.000 0.000 0.000 1 0.649 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.032 0.017 0.000 0.000 0.000 0.000 0.049 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.336 6.487 0.000 0.000 0.000 0.000 6.823 ITotal Phos- 0.000 0.000 0.000 0.000 0.000 0.000 6.660 136.272 0.000 0.000 0.000 0.000 142.932 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". -,J/\ 2.- iA � Signature of Land Applier a ai l Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: William Griffin Operator: Same WQ Permit #: WQ0001346 Field #: 4 Annual Dry Tons Applied: 19.8963 Site #: NC-UN29 Acres Utilized: 2.9 Acres Permitted: 2.9 Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 o Y QLiquid Volume applied (enter one) Solids/ Cu. Yds Gallons "�u Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. Wet Moist) Precip. Past 24 Hrs. inches a � o * N o' w w * TKN mg/kg Z Y o El as o w. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Aug 20 75 31.50 6.861 WTP Cake D 0 S 0.5 0.4 12,500 317 28.4 69.433 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0•000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ........ .......... TOTALS: 75 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 69.433 0.000 Lime Applied Annuallbs/acre 0.440 0.030 5.406 3.128 0.065 0.001 0.589 0.519 0.218 2.305 45.688 0.401 0.061 11.052 3.942 0.642 0.012 0.891 1.237 0.141 17.892 ........... 0.841 1 0.091 16.458 7.070 0.707 0.013 1.480 1.756 0.359 20.197 36 134 1338 X 267 15 X 374 89 2498 1227 50 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation eAn. Ayla sz( **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 19.89 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: William Griffin Owner: Same Predominant Soil Series: BdB2-Badin Acres Used: 2.9 Acres Permitted: 2.9 Site #: NC-UN29 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date L21J 2 3 4 5 L6J L7 7/ 1 /20 8 9 10 11 12 % Solids 31.5 Arsenic 32.1 Cadmium 2.21 Copper 394 Chromium 228 Lead 4.76 Mercury 0.0485 Molyb- denum 42.9 Nickel 37.8 Selenium 15.9 Zinc 168 Total I Phos- horus 3330 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App' Event 1 1 1 1213 4 L5J 6 7 6.86 8 9 10 11 12 o Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.440 1 0.000 0.000 1 0.000 0.000 0.000 1 0.440 Cadmium 0.000 0.000 0.000 0.000 1 0.000 0.000 0.030 0.000 0.000 0.000 0.000 0.000 0.030 Copper 0.000 0.000 0.000 0.000 0.000 0.000 5.406 0.000 0.000 0.000 0.000 0.000 5.406 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 3.128 0.000 0.000 0.000 0.000 0.000 3.128 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.065 0.000 0.000 0.000 0.000 0.000 0.065 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.589 0.000 0.000 0.000 0.000 0.000 0.589 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.519 0.000 0.000 0.000 0.000 0.000 0.519 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.218 0.000 0.000 0.000 0.000 0.000 0.218 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 2.305 0.000 0.000 0.000 0.000 0.000 2.305 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 45.688 0.000 0.000 0.000 0.000 0.000 45.688 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ;!� 0-4 ,1 Signature of Land Applier .z d-0lz i Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Tom Appenzeller Operator: William Griffin Crop 1 Name: Fescue (Past.) WQ Permit #: WQ0001346 Field #: I Annual Dry Tons Applied: 86.2175 Site #: UN-UN30 Predominant Soil Series: BdB2-Badin Crop 1 Max. PAN: 122 Acres Utilized: 13.1 Acres Permitted: 13.1 Cation Exchange Capacity (non 503): N/A Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 0 N >~ La Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches a 4 b �° o o o w p- * ° o ;� w �, ; �- N' w ., o ?- N * TKN mg/kg Z a E o 0 o � � mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 July 20 300 31.5 6.075 WTP Cake D 0 S 0.5 0.4 1 12,500 317 28.4 61.482 NA Fescue Aug 20 25 31.5 0.506 WTP Cake D 0 S 0.5 0.4 12,500 317 28.4 5.124 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0•000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 325 0 :::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 66.606 1 0.000 Lime Applied Annuallbs/acre 0.422 0.029 5.185 3.000 0.063 0.001 0.565 0.497 0.209 2.211 43.823 :: : : Date lbs/ac Prior Years Cumulative lbs/ac 0.883 0.125 18.374 6.756 1.158 0.022 1.539 2.405 0.353 35.061 Current Cumulative Ibs/ac 1.305 0.154 23.559 9.756 1.221 0.023 2.104 2.902 0.562 37.272 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 1 2498 Permit PAN Limit lst/2nd Crop 122 50 ..i certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1-/kQ L( **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date* Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant LoadinIZ Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: City of Monroe WQ0001346 Operator: Tom Appenzeller Owner: Acres Used: 13.1 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): William Griffin Predominant Soil Series: 13.1 Site #: NC-UN30 Field #: 86.20 N/A BdB2-Badin 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 11 1 21 L3J4 51 6j L7J 7/l/20 1 81 9 LOJ 11 12 % Solids 1 31.5 Arsenic 32.1 Cadmium 2.21 Copper 394 Chromium 228 Lead 4.76 Mercury 0.0485 Molyb- denum 42.9 Nickel 37.8 Selenium 15.9 Zinc 168 Total IPhos- horus 3330 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ITotal DT/Ac./ APP • Event 1 1 1 L 2j L3J4 5 6 7 6.58 8 9 10 11 12 y Arsenic 0.000 1 0.000 0.000 0.000 0.000 0.000 0.422 1 0.000 0.000 0.000 0.000 0.000 0.422 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.029 0.000 0.000 0.000 0.000 0.000 0.029 Copper 0.000 0.000 0.000 0.000 0.000 0.000 5.185 0.000 0.000 0.000 0.000 0.000 5.185 1'�lirornium 0.000 0.000 0.000 0.000 0.000 0.000 3.000 0.000 0.000 0.000 0.000 0.000 3.000 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.063 0.000 0.000 0.000 0.000 0.000 0.063 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.565 0.000 0.000 0.000 0.000 0.000 0.565 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.497 0.000 0.000 0.000 0.000 0.000 0.497 Selenium 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.209 0.000 0.000 0.000 0.000 0.000 0.209 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 2.211 0.000 0.000 0.000 0.000 0.000 2.211 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 43.823 0.000 0.000 0.000 0.000 0.000 43.823 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". /6 Q" M 0-1,� Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Tom Appenzeller Operator: Same WQ Permit #: WQ0001346 Field #: 5 Annual Dry Tons Applied: 63.1377 Site #: NC-UN30 Predominant Soil Series: BaB-Badin Acres Utilized: 10.8 Acres Permitted: 10.8 Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons /o Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist) Precip. Past 24 Hrs. inches a cn o' n * ° ° o w �, -- * N w , 9 °-= * R � TKN mg/kg Z a El o ao ° mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Aug 20 238 31.5 5.846 WTP cake D 0 S 0.5 0.4 12,500 317 28.4 59.164 NA Fescue 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 238 0 :::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 59.164 0.000 Lime Applied Annuallbs/acre 0.376 0.026 4.610 2.668 0.056 0.001 0.502 0.442 0.186 1.966 38.961 Date lbs/ac Prior Years Cumulative lbs/ac 0.344 0.074 9.417 3.483 0.72 0.015 0.797 1.239 0.132 20.332 Current Cumulative lbs/ac 1 0.720 1 0.100 14.027 6.151 0.776 0.016 1.299 1.681 0.318 22.298 Permitted C. P. L. R.**** 36 34 1 1338 1 X 267 15 X 374 89 2498 Permit PAN Limit lst/2nd Crop 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 42**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Monroe WQ0001346 Tom Appenzeller Owner: 10.8 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Same Predominant Soil Series: 10.8 Site #: NC-L N30 Field #: 63.18 N/A BaB-Badin 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 1 L 2j 1 31 L4J5 6 7 7/l/20 8 9 10 11 12 % Solids 31.5 Arsenic 32.1 Cadmium 2.21 Copper 394 Chromium 228 Lead 4.76 Mercury 0.0485 Molyb- denum 42.9 Nickel 37.8 Selenium 15.9 Zinc 168 Total I Phos- horus 3330 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2 3 4 5 6 7 5.85 8 9 10 11 12 o " Arsenic 0.000 1 0.000 0.000 0.000 0.000 0.000 0.376 0.000 0.000 0.000 1 0.000 0.000 0.376 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.026 0.000 0.000 0.000 0.000 0.000 0.026 Copper 0.000 0.000 0.000 0.000 0.000 0.000 4.610 0.000 0.000 0.000 0.000 0.000 4.610 �hromjum 0.000 0.000 0.000 0.000 0.000 0.000 2.668 0.000 0.000 0.000 0.000 0.000 2.668 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.056 0.000 0.000 0.000 0.000 0.000 0.056 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 1 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.502 0.000 0.000 0.000 0.000 0.000 0.502 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.442 0.000 0.000 0.000 0.000 0.000 1 0.442 Selenium 0.000 1 0.000 0.000 0.000 0.000 0.000 0.186 1 0.000 0.000 0.000 1 0.000 0.000 0.186 Zinc 0.000 1 0.000 0.000 0.000 1 0.000 0.000 1.966 0.000 0.000 0.000 0.000 0.000 1.966 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 38.961 0.000 0.000 0.000 0.000 0.000 38.961 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". signature of Land Applier 2 '/jo 2- i Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Henry Myers Operator: Same Crop 1 Name: Fescue (Past.) WQ Permit #: WQ0001346 Field #: 3 Annual Dry Tons Applied: 14.9856 Site #: NC-UN31 Acres Utilized: 2.5 Acres Permitted: 2.5 Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 O y o c� Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons "�o Solids Volume Applied per pP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D ( rY, Wet Moist) Precip. Past 24 Hrs. inches > � � O a ?Y * °� o * w' o EL * = TKN mg/kg Z. = Ei El o oF; w. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Sept 20 56 23.9 4.509 WWTP Cake D 0 S 0.5 0.3 33,800 2,120 91.6 96.085 NA Fescue Sept 20 14 31.5 1.486 WTP Cake D 0 S 0.5 0.4 12,500 317 28.4 15.035 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 70 0 .....::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 1 11.1 19 0.000 Lime Applied Annuallbs/acre 0.226 0.014 5.441 1.636 0.195 0.004 0.287 0.747 0.066 7.672 160.557 :::::::::::::::::::::::::::: .................. :: Date lbs/ac Prior Years Cumulative lbs/ac 0.968 0.103 18.292 12.918 1.745 0.0244 1.615 3.673 1.512 49.419 July 18 2165 Current Cumulative lbs/ac 1.194 0.117 23.733 14.554 1.940 0.029 1.902 4.420 1.578 57.091 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit l st/2nd Crop 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation M ° / i ;t a **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 15.00 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Henry Myers Owner: Same Predominant Soil Series: BdB2-Badin Acres Used: 2.5 Acres Permitted: 2.5 Site #: NC-LJN31 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date 7/1/20 8/12/20 % Solids 31.5 23.9 Arsenic 32.1 14.5 Cadmiumi 2.21 0.828 Copper 1 394 473 Chromium 228 106 Lead 4.76 20 Mercury 0.0485 0.448 Molyb- denum 42.9 17.7 Nickel 37.8 70.3 Selenium 15.9 2.09 Zinc 168 795 Total I Phos- 3330 16700 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ITotal DT/Ac./ App. Event I 1 I L2J L3J L4J L5JL6J L7JL8J 1.49 4.51 L9J LOJ 11 J 12 0 Arsenic 0.000 1 0.000 0.000 0.000 0.000 0.000 0.096 1 0.131 0.000 0.000 0.000 0.000 0.226 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.007 0.000 0.000 0.000 0.000 0.014 Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.174 4.266 0.000 0.000 0.000 0.000 5.441 ^hromium 0.000 0.000 0.000 0.000 0.000 0.000 0.679 0.956 0.000 0.000 0.000 0.000 1.636 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.014 0.180 0.000 0.000 0.000 0.000 0.195 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.128 0.160 0.000 0.000 0.000 0.000 0.287 Nickel 0.000 0.000 0.000 0.000 1 0.000 0.000 0.113 1 0.634 0.000 0.000 0.000 0.000 0.747 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.047 0.019 0.000 1 0.000 0.000 0.000 0.066 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.501 7.171 0.000 0.000 0.000 0.000 7.672 ITotal Phos- 0.000 0.000 0.000 0.000 0.000 0.000 9.923 150.634 0.000 0.000 0.000 0.000 160.56 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z z Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Henry Myers Operator: Same WQ Permit #: WQ0001346 Field #: 4 Annual Dry Tons Applied: 21.5175 Site #: NC-UN31 Acres Utilized: 4.7 Acres Permitted: 4.7 Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 ., o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) SO1i Cond. D Wet Moist) Precip. Past 24 Hrs. inches Y co � o 0 m 0. * o -- * o' -, cc '� * w TKN mg/kg Z. Y El o El �. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Sept20 70 23.9 2.998 WWTP Cake D 0 S 0.5 0.3 33,800 2,120 91.6 63.886 NA Fescue Sept 20 28 31.5 1.580 WTP Cake D 0 S 0.5 0.4 12,500 317 28.4 15.994 NA Fescue 0•000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0•000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 98 0[ As Cd Cu Cr Pb H Mo Ni Se Zn P 79.880 0.000 Lime Applied Annuallbs/acre 0.188 1.098 1.286 36 0.012 0.115 0.127 1 34 4.081 21.065 25.146 1 1338 1.356 14.592 15.948 X 0.135 1.94 2.075 267 0.003 0.031 0.034 15 0.242 1.883 2.125 X 0.541 4.034 4.575 1 374 0.063 0.386 0.449 1 89 5.298 54.918 60.216 1 2498 110.656::::.:.::::::::::::::::::::::::::: ................. Date lbs/ac Prior Years Cumulative lbs/ac 2-17 1904 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop .. 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation IZ-l.tl f ,Z� L/ **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loadin1l Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 21.52 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Henry Myers Owner: Same Predominant Soil Series: BdB2-Badin Acres Used: 4.7 Acres Permitted: 4.7 Site #: NC-UN31 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- positeMENNENDate 1 Lo1 • 11 Total � • •. © Mn MODEM 0 n •- 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1: 1 111 1 111 1 111 1 111 1 :: .• 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 11 1 111 1 111 1 111 1 111 1 1 •••• 1 111 1 111 1 111 1 111 1 111 1 111 � • 1 111 1 1 1 1 111 1 111 � 1: • 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1• • 1 111 1 111 1 111 1 111 .. 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1® - 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 11 1 111 1 11 � � • 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1 1• 1 111 1 111 1 111 1 111 1 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1� 1 111 1 111 1 111 1 111 1 1 111 1 111 1 111 1 111 1 11 1 111 1 1 1 1 1 1 111 1 111 1 111 1 111 1 1• 1111 1 111 1 111 1111 1111 1111 � � • 1111 1111 1111 1111 •: ••, 1 111 1 111 1 111 1 111 1 111 1 111 � 11 1 111 1 111 1 111 1 111 1 • • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) Volatile Solids Reduction 2020 Van Kleek equation In (RAS) - Out (digested sludge) _ In (RAS) - (In * Out) (digested sludge) _ 1st Quarter RAS digested sludge IN- OUT 0.6230 0.6210 0.002 IN- (IN -OUT) 0.623 0.386883 0.236117 2nd Quarter IN - OUT 4/1 /2020 0.6950 0.6500 0.045 Reduction IN- (IN -OUT) 1 18.50% 0.695 0.45175 0.24325 IN- OUT 4/16/2020 0.7110 0.6460 0.065 lReduction IN- (IN -OUT) 1 25.83% 0.711 0.459306 0.251694 IN- OUT 5/18/2020 0.7130 0.4580 0.255 Reduction IN- (IN -OUT) 1 65.99% 0.713 0.326554 0.386446 3rd Quarter IN- OUT 7/1 /2020 0.6740 0.5880 0.086 lReduction IN- (IN -OUT) 1 30.97% 0.674 0.396312 0.277688 IN- OUT 7/22/2020 0.6830 0.5920 0.091 lReduction IN- (IN -OUT) 1 32.66% 0.683 0.404336 0.278664 IN - OUT 8/12/2020 0.7130 0.5470 0.166 lReduction IN- (IN -OUT) 1 51.39% 0.713 0.390011 0.322989 Volatile Solids Reduction 2020 4th Quarter IN- OUT 10/5/2020 0.7200 0.5640 0.156 Reduction IN- (IN -OUT) 49.69% 72 0.40608 0.31392 PLIR PROM PT- A CCU RATE -RE L [AS LE LABORA-rORIES, INC WWWPARLABS.CON1 I-'--EPCRT OF ANALYSES Attn: STEVE POLDEN 2717 OF MONROE WASTEWATEPFLANT PROJE(-T NAME: JAN :O PO BOX t59 DATE: '11/24/20 MONROE, NC -A1,11 I F NUMBER, 1 3-79(-.-j 1 1 _ SAMPLE 11�� MONROE WWTP SAMPI,E TvWrP7X WW " j _' T ME 01 -1 '' SAMP-ED- SAMP,,F�. � Rz('EI VED PE I c BY, of M F RE2E1VE 0 7.')HLJ.VEZED BY- Eli TYPE SAMPLE- C-,«an ANAJ.',/SiS _NAT 23S METHOD DATF Ti ME BY RESULT UNITS 01/06Z20 16s0 RE 8 4 , 0, MIPNi BORA""OPY DTPECr)-,�< 2217 Graham Park Drive - Charlotte. NC 28273 Phone: (704) 588-8333 - Fax: (704) 588-8335 AM R PROMPT•ACCIJRRTE• RE{ -TABLE LABORATORIES, INC 137967 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CITY OF MONROE MONROE WWTP 01 /06120 FECAL COLIFORM, GEOMETRIC MEAN • SM 9221 E # 1 F. Coliform 10,007 T. SolidsSample 12.27% 81,557.45 2 10,642 12.25% 86,867.83 3 11,996 12.38% 96,928.68 4 9,907 12.35% 80,221.82 5 9,936 12.22% 81,304.89 6 9,964 12.08% 82,449.91 7 1 10,088 1 12.56% 1 80,314.42 Fecal Coliform Geometric Mean= • L R aTpRr, INC. www.parfabs.com CHAIN OF CUS TOD Y pAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 Shiopinc. r0ailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 t s essenval that wi information De recorded on ;his Chain o' Custody docur,.>_n, :or acceptance by PAR Laboratories, Inc. and the North Carolina Department o: Environmental and Mural Resources. Ccnpany Name (bitrrng) Comments! Special Instructions City of Monroe Addres3 PO Box 69 503 BI®SOLIDS i i� T 1�IlvT city, Stale & zip code ^A �r- 1.. 2Q1I 1 I R' POR 1 f `CT OIZtOe_ �Point of Contact & Telephone Steve Hoiden I; 704) 252-4679 sllolden,'cumonroeiic.ol-�,, Sample Taken By: —J�'/ �y� l/ ►���f�✓ IS THIS FOR STATE or EPA REPORTING? YE_S .j- NO *Sample type: DW WW )C GWMW _ HW _ Soil _ other Sample Temp at time of sampling: *7,9 OC Sample Temp upon receipt: /"-�7 --C- Preserved: Yes — No X Teflon Liner/ Zero Headspace: Yes _ No N/A X Cii n Sample I.D. Sample Location ;Number) Comp Grab Preserv. Set Up Date / Time I I Collection Date / Time Analyes Reyuesled a I WwTP X NONE 1, G _ p ,vv FECAL COLIFORM 2 wvv rP ; x NONE v l0: �� FECAL COLIFORM ? WWTP , X NONE p % v FECAL COLIFORM r 4 )"7P - X NONE FECAL COLIFORM 4 5 WvvTP X NONE r J FECAL COLIFORM a 6 WWTP X NONE _L _ o : FECAL COLIFORM R7 wwTP t i X NONE Z 3 FECAL COLIFORM I 2eiinquishe Date/rime Received by: j Date/Time 41 - Oc:, . elir,pvished by: Datei i ime Peceived by: DaterTme C=Ccrnposrte G=Grab DW=Drinkino_ Water WW=Wastewater GWMW = Groundwater Monitoring Well H'.V=Hazardous Waste ' See 0-her Side 1 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: Monroe WWTP cake NPDES Number: NCO024333 Monitoring Period: From l/l/2020 To 3/31/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization Class B: Alternative 1 21 Alternative 2 C If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Ai Drying❑ Composting ❑ Aerobic Digestion Sd Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data. Parameter Allowable Level in Sludge Pathogen Density Number of Excee- c Frequency of Analysis Sample Type Analytical Tech - ni oue MinimumGeo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 80,221.82 84,061 96,928.68 MGN/g 0 quarterly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) rj Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) [l Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable) Alt. 9 (Injection) L] Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) 21 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) rIMKID rr)DRA D\/DG rnl /1')1')nna\ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WWTP Name: WWTP cake Monitoring Period: From l/1/2020 WQ Permit Number: WQ0001346 NPDES Number: NCO024333 To 3/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment Cl Thermophilic Beta Ray 01 Gamma Ray ❑ Pasteurization Class B: jAlt. (1) Fecal Density Rl Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion Cl Anaerobic Digestion ❑ _. ........... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- -dencesg Frequency of Analysis Y Sample Type Analytical Tech- ni oue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 80,221.82 84,061 96,928.68 MPN/g 0 quarterly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal colifonn) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) G Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization Cy Alt 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) C Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) Ej "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) /� Ir— y1>g1,-w �K, . m -,v, a a -2,, Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) npKip rnPKA CA/Pr mT /17/')fV)9\ I PROMPT- A CCU RATE -RELIABLE LABORATORIES, INC WW'%V.PARLABS.COM REPORT ()iANAlY.7"" 11-..1 n: 1— '-"PEVE F."'LDEN i.Y OF MONROE WASTEWATEPPT_,ANT 1PROJECT t.IAMIE: APR 2"' EOX '_1 4 / I 69 'DATF: MONROE, Ni' : 8 1I I �'.MPLF NUMBER.- ,866 SAI'47:E ID- MONROE WW7P ISAMPLE MATRIX WW 0 4 /Gj i l TIME SAMPLED- RECEIVED- 041/00.1/20 SAMPLER SH RECEIVED IbY Dj '."VE RE-ETVED 102" DELIVERED BY- SH TYPE SAMPLE- G.-a", ANALYSIS MET, H OD TIME BY F.FStT!,T IW77S _AI 8, 1 " 1 MPN/g C(Di IP'01�1,1 (GEOM. M-EAN) S V, R T.' 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 f-I F'14OMf'T-ACCURATE• RELIACiLE T,AB(DR-ATORIES, INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20, SC Cert # 99003001 CLIENT NAME: CITY OF • ' • SAMPLE ID: = kyj [01 ki I ' * SAMPLE DATE: 1 ANALYSIS: • • " • ' ANALYSIS METHOD: • 7-138636 Fecal Coliform Geometric Mean= # 1 F. Coliform 1.139 T. SolidsSample 14.74% 7,726.86 2 1,106 14.38% 7,696.03 3 1,366 15.33% 8,912.67 4 1,101 14.43% 7,631.38 5 1,302 14.52% 8,964.12 6 1,117 15.03% 7,432.54 7 1 1,240 1 14.47% 1 8,571.92 ij f �A jq iA50RArORIES, INC. www.partabs.com CHAIN OF CUS TOD Y PAR Laboratories, Inc Phone (704) 588-8333 Fax (704 588-8335 Shippinc Mailing. 2217 Graham Park Drive PO Box 4, 1483 Charione, NC 28273 Charlotte, NC 28241-1483 s esen:.ai that all information be recorded on this Chain of Custody docur-ent for acceptance by PAR Laboratories. Inc, and the North Carolina soariment of Environmentai and Natural Resources. Ccmpeny Name IbMin9) City of Monroe IAddress City. Stata S zip code Instru i 503 BIOSOLDDS i Monroe. NC 28111 1 REPORTING r'Oint of Contact SS Teiephor>E'� ...'- _. j PO Box 69 Steve Holden ( 704 ) 282-4679 sholden(ir.monroenc.orc �� Sample Taken By: IS THIS FOR STATE or EPA REPORTING? YES NO 'Sample type: DW WW Y GWMW _ HW _ Soil _ other--t— Sample Temp at time of sampling.j� °C Sample Temp upon receipt: / �,� °-C— Preserved: Yes _ No X Teflon Liner/ Zero Headsoace: Yes No N!A X Client Sample I.D. ( Sample Location ! Number) Comp Grab Preserv. ` Set Up Date / Time Collectiou Date / Time Analyes Requested X NONE _ v -'rq FECAL COLIFORM 2 WWTp i X NONE , LJ , o FECAL COLIFORM k 3 �'WTPX 4 W%k7P I NONE j X NONE FECAL COLIFORM FECAL COLIFORM 0 5 1XrWrP X NONE _ ^ Lv i FECAL COLIFORM 6 WWTP X NONE _ Zv FECAL COLIFORM -- - 7 WWTP X NONE i FECAL COLIFORM ,FI ;^u red by: efinquished by: Dateltime Received I �► 2 Dater -lime Received by: tellime Date/1 une zl�-01-)_o//02_7 =G=Grab DW=Drinking Water WW=WaSlewater GWMW=Groundwater Monitoring Well WV -Hazardous Warn ' See Dther Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WWTP Name: Monroe WWTP cake NPDES Number: WQ0001346 NCO024333 Monitoring Period: From 4/1/2020 To 6/30/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 �J Alternative 2 ❑ .................. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Au Drying❑ 1Composting ❑ jAerobic, Digestion Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data. Parameter Allowable Level in in Sludge Pathogen Density Number of Excee- n Frequency of Analysis Y Sample Type Analytical Tech - ni gue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 7,432.54 8,111 8,964.12 MGN/g 0 quarterly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) D Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ 1Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) Fl Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed C CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) Ken Morris, Residuals Coordinator Land Applier Name and Title (if applicable)(type or print) I %lam Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WWTP Name: WWTP cake WQ Permit Number: NPDES Number: Monitoring Period: From 4/l/2020 To 6/30/2020 WQ0001346 NCO024333 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)Cl Alt. C (Prior Testing)[] A1t.D (No Prior Test) ❑F Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density 211 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Cl Air Drying ❑ Composting ❑ jAerobic Digestion 21 Anaerobic Digestion Cl If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- deuces Frequency of Analysis y Sample Type Analytical Tech - ni ue Minimum Minimu Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 7,432.54 8,111 8,964.12 MPN/g 0 quarterly grab SM9221 E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) Rl Alt. 2 (40-day bench) ❑ Alt. 3 (30-daybench) ❑ 1 Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Q "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) Ken Morris, Residuals Coordinator Land Applier Name and Title (if applicable)(type or print) SijAature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) MCKIM moue odor n)T PAOkR PROM PT- ACCU RATE• REL.I AS LE LABORATORIES, INC WVbWPARLABS.COM REPORT OF ANALYSES Attn: KEN MORRIS ' CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JUN 20 PO BOX 69 DATE: 07/21/20 MONROE, NC 28111- SAMPLE NUMBER- 139302 SAMPLE ID- MONROE WWTP SAMPLE MLATRIX- WW DATE SAMPLED- 07/01/20 TIME SAMPLED- 101E DATE RECEIVED-- 07/01/2.0 SAMPLER- KM RECEIVED BY DJ TIME RECEIVED- 1230 DELIVERED BY- KM TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 07/01/20 1630 RE 4,744 MPN/g I LABORATORY DIRECTOR 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 1 PA&R PROMPT•ACCU RATE'• RELIABLE LAI30I2ATORIES, INC 139302 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CITY OF MONROE MONROE WWTP 07/01 /20 FECAL COLIFORM, GEOMETRIC MEAN • SM 9221 E 1 869 17.56% 4,946.01 2 704 17.45% 4,035.53 3 810 17.30% 4,679.98 4 841 17.41 % 4,832.21 5 868 17.18% 5,049.57 6 798 17.16% 4,649.25 7 1 886 1 17.35% 1 5,105.27 Fecal Coliform -7 Geometric Mean= ";=AJR CHAIN OF CUSTODY WaRAMR►BS.lNC. PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www.parfabs.cam Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charfo-zie, NC 28273 Charlotte, NC 28241-1483 it l; cuicnVal that all Informaion be recorded on this Chain or Custody document fur acceptance by PAR Laboratodw. Inc. and the North Carolirm Deoarlment of EnvirorR enzal and Naluml Resources. ' Company Name tbining) City of Monroe Comments/ Special Instructions tlddtaas ' PO Box 69 503 BXOSOLZDS city. stA:a rip coda RFPOR.TING i Monroe, NC 2$111 �rp nl of .ontaot & TulapAooa _. — _ -r S '7 o oZ - SCOM00 Taken By: KA— fWaA lA— IS 'His FOR STATE or EPA REPO�TlNG? YES NO 'Sample type: DW __ WWr GWMW _ HW _ Soil _ other Sample 'Comp at time of saMPF1ng_,2$,,2 °C Sample Temp upon receipt: _/ '• °KZ- Proserved: Yes ` No .A,, Teflon Liner/ Zero Headspace: Yes _ No [A X clicot Sample I.D. Comp Grab Prescrv. Set Up Collection Analym Requeitad f Sine union /Number Date /Time Date /Time N I W WTP NONE .1 ,. 10 FECAL COLIFORM 1 o p f) 2 W WTI' X NONE ti 1.2 FECAL COLIFORM a o' to 3 WW'IT X NONE .7/11 FECAL COLIFORMAl a o 1p, 167 A WWTP NONE _ t7 FECAL. COLIFORM r VIrWTP X NONE ' i o2 a : 02o FECAL COLIFORM 'rP X NONE FECAL COLIFORM j N 7 WWTH X NONE r �,� a FECAL COLIFORM +ellnquished by: ;t.lir,quished by: Date[Time 7 g2 Datefiime Received by: Received by: �J Daterrlme C "Gcnposrte G=Grab DW—Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well WV -Hazardous Wasta See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: Monroe WWTP cake (7/l/2020 sample) NPDES Number: NCO024333 Monitoring Period: From 7/l/2020 To 9/30/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 El If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 SJ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Ai Drying❑ Composting ❑ Aerobic Digestion 0 Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data. Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dences Frequency of Analysis Sample Type Analytical Tech - ni oue Minimum Geo. Mean Maximumi Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 4,035.53 4,744 5,105.27 MGN/g 0 bimonthly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) 1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) DI Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) Ef No vector attraction reduction alternatives were performed 01 CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." r "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) ��� 2154-- �, K.-,,. )o � l-- -21 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nr=NR FnPKA P\/RF 1;ni (17/9nnR) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) 1 Facility Name: City of Monroe WWTP Name: WWTP cake (7/l/2020 sample) Monitoring Period: From 7/1/2020 To WQ Permit Number: NPDES Number: 9/30/2020 WQ0001346 NCO024333 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment)❑ Alt. C (Prior Testing)[] A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density Rl Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion i� Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number ot Excee- n Frequency of Analysis y s Sample Type Analytical Tech- i e Minimum Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 4,035.53 4,744 5,105.27 MPN/g 0 quarterly Grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) 21 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." n "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) Ken Morris, Residuals Coordinator Land Applier Name and Title (if applicable)(type or print) Si nature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) nGr%iD GnQnn D%/Q� n7T /17/7nnR\ PAiR PROM PT•ACCU RATE -RE LIABLE LABORATORIES, INC WWW.PARLABS.COM REPORT OF ANALYSES Attu: KEN MORRIS ' CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JUL 20 PO BOX 69 DATE: 08/17/20 MONROE, NC 28111- SAMPLE NUMBER- 139475 SAMPLE ID- MONROE WWTP SAMPLE MATRIX WW DATE SAMPLED- 07/22/20 TIME SAMPLED- '1715 DATE RECEIVED- 07/22/20 SAMPLER- KM RECEIVED BY- DJ TIME RECEIVED- i1i5 DELIVERED BY KM TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 07/22/2.0 1650 RE 81,733 MPN/g LABORA^ORY DIRECTOR r 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 PAFZ PROM PT•ACCU RATE• RELIADLE L.ABC)PLATORIES, INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CLIENT NAME: CITY OF • ' • SAMPLE ID: Ru, I " • SAMPLE DATE: WIFIFTUTim ANALYSIS: • • ' • ANALYSIS METHOD: • 139475 Fecal Coliform Geometric Mean= 1 18,111 19.32% 93,736.60 2 19,648 19.50% 100,778.32 3 13,911 19.80% 70,267.53 4 14,959 19.80% 75,558.73 5 14,369 19.11 % 75,177.87 6 16,506 19.27% 85,652.17 7 14,490 1 19.21 % 75,443.48 M CHAIN OF CUSTODY 1ASOAATOArES,wC. PAR Laboratories, Inc Phone (704) 588-8333 Fax (7041 588-8335 wwrf.parfabs-com Shippinc: Mailing: 2- 1 7 Graham Park Drive PO Box 411483 Ctharftttte, NC 282-73 Charlotte, NC 28241-1483 ' is c33cnval Thai all inrormazion be recorded on this Chain or Custody documem for acceptance by FAR Laboratories. Inc. and the North �4rolfna �tDdrtT Vrtt of Environmental and Natural Rcsouree5_ ~Ccrnpany Name (billing) Comments/ Special Instructions City of Motuoe -- Address PO Bo 69 503 BIOSOLIDS Ghy. State &zip coda REPORTING Monroe, NC 28111 �I"ornt of ConUaet & �akpbone'� _____ Sample Taken By:1 IS THIS FOR STATE or EPA REPO$TING? YES NO "i—Ple type: DW WW y' GWMW _ HW _ Soil _ other Sample Temp at time of sampfing: 2 7 • I °C Sample Temp upon receipt: __ °C_ Preserved: Yes _ No X Teflon Liner/ Zero Headspace_ Yes No NIA Client Sample I.D_ ( Sample Location / Number' Comp I Grab , Preserv. Set Up Date i Time Collection Date I Time Analyes Requested a i wwTp i X NONE ,?►-tea -�� .' 16 FECAL COLIFORM 2 WWTP f X NONE 7-'!7 FECAL COLMORM 3 WWTP A WWTP _ S WWTP X X NONE NONE NONE -� a -ao 7_ -ao 'j: he rj� t FECAL COLIFORM FECAL COLIFORM FECAL COLIFORM ! 6 wWTF �. j X NONE 7' as - �e '� : t 7 FECAL COLIFORM _i NONE FECAL COLIFORM Reiinqui-het: by Datee[Tirne� relinquished by: Date/ i ime Receiv b 1. ti Received by: Da te/Tmc / /// i 5 Da terl itme -Composite G=Grab DW=Drinking Waier WW=Wastewater GWMW=Groundwater Monitoring Well WV=Hazardous Waste See Ciher ode ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: Monroe WWTP cake (7/22/2020 sample) NPDES Number: NCO024333 Monitoring Period: From 7/l/2020 To 9/30/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 © Alternative 3 El Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 R1 Alternative 2 0 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion Anaerobic Digestion El If applicable to alternative performed (Class A or Class B) complete the following monitoring data. Parameter Allowable Level in in Sludge Pathogen Density um er o Excee- ence Frequency of Analysis y Sample Type Analytical Tech - nioue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 70,267.53 81,733 100,778.32 MGN/g 0 bimonthly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) 21 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) L; Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ lAlt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nFNR FnRM P\/RF .ri(1:i (17/9nnR) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WWTP Name: WWTP cake (7/22/2020 sample) NPDES Number: Monitoring Period: From 7/1/2020 To 9/30/2020 WQ0001346 NCO024333 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) El Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) El Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density Z Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization n Air Drying ❑ Composting ❑ jAerobic Digestion ',ii Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number ot Excee- nces Frequency of Analysis Y Sample Type Analytical Tech- ni aue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 70,267.53 81,733 100,778.32 MPN/g 0 quarterly Grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) Ej Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ jAlt. 4 (Spec. OZ uptake) ED Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed n CERTIFICATION STATEMENT (please check the appropriate statement) Cl "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) Ken Morris, Residuals Coordinator Land Applier Name and Title (if applicable)(type or print) 44 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nFNR FORM PVRF 02T (12/2006) p AM UR PROM PT•ACCU RATE -RELIABLE LABOPATORIES, INC \N N%AV.PARLA8S.00:%7 REPORT OF ANALYSES Attu: KEN MORRIS CITY OF MONROE WASTEWATERPLANT PROJECT NAME: AUG 20 PO BOX 69 DATE: 08/17/20 MONROE, NC 28111. Si�MFLE NUMBER- 139657 SAMPLE ID- MONRCE WWTP SAMPLE MATRIX- WW DATE SAMPLED- 08i ' 2/20 TIME SI-14PLED- 0'753' DATE RECEIVED- 08/12/20 SAMPLER- KM RECEIVED BY- DJ TIME RECEIVED- 1020 DELIVERED BY- KM, TYPE SAMPLE Grab Page 1 of ANALYSIS ANALYSIS METHOD DATE 'TIME BY RE;SUL"UNTTS FECAL COLIFORM iGEOM. MEAN) SM 9221 E 08/12:/20 1730 RE 147,064 MPN/g LABORA-ORY DIRECTOR- f 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 PAR "Rom PT•ACCU RATE• REL.I AO LC I.ABOR.A70aIES, INC 139657 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20: SC Cert # 99003001 CITY OF MONROE MONROE WWTP 08/12120 FECAL COLIFORM, GEOMETRIC MEAN SM 9221 E 1 37,042 25.11 % 147,514.53 2 37,045 25.33% 146,247.99 3 37,109 24.91 % 148,979.33 4 36,941 24.09% 153,331.91 5 37,056 25.09% 147,708.43 6 36,684 25.11 % 146,091.00 7 36,618 26.17% 139,902.62 Fecal Coliform Geometric Mean= •' MAR CHAIN OF CUSTOD Y LAA"710ftc.WC. PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www,partaD.sxom ShiFRirfq. Mailing: 2217 Graham Park Crive PO Box 411483 Chariorre, NC 28273 Charlotte, NC 28241-1483 l% 17 epantlaa INt #A lntofmat on be recorded on this Chain of CuatodY document for acceptanct by PAR Laboretoo". Inc. end #* Ndtte �+Kt1i Cf, fanviwormwral and Natural Resour`cs. pmesny Nwme Wong) Commonts/ Sp9cial IaciPUG City of MOM-0c, Ard�lffff� w PO Box 69 503 B10SO IDS r O 1 ftip A",% Monroe, NC 28111�dR�T Ufnpl® Taken Ry, 14 THIS FOR STrATE or eA R TING? YES NO *$*Mpw type: Dw__ Ww GWMW _ HW _ soil other SOMPle � e np at time of sa�mrpling: ooi'7.9 °C Sample Temp upon receipt- ° Pf'"499vtd. 'tires .___ Na .A, Teflon Liner! Zero Headspace: Yes No N/A_j =1 a� sap at I.Y.- Atfll 1 Location ( Number Comp Grab Preserv. Set Up Date / Time Collection Date ; Time Analyes Requ M �► a W _X NONE f FECAL COLIFORM A 2 wwrP X NONE o FECAL. COLiFORM NONE � l a a� 'i. 7 FECAL COLIFORM v1► X NONE ,,� FECAL, COLIFORM X NONE-2 o •� , . f FECAL COLIFORM # Q WWTP X NONE fit; FECAL COLIFORM X NON B $ ap �_ �� FECAL COLIFORM rtslirf 1711190 Ay: Datemme Roceiv OotelTrcno A l'2 0? � '-� -2 lolinquisbad by: DutCrrinx� Received by: DateMme ' C-CotnpoaAe G-Crab DW=Drinking Water WW-Wastewater MAW-Groundwator Monitoring Well H',V-HaaardOvs Vivas Sae Ot W Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 1 WWTP Name: Monroe WWTP cake (8/12/2020 sample) NPDES Number: NCO024333 Monitoring Period: From 7/1/2020 To 9/30/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray 01 Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 Cl Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Au Drying;_] Composting ❑ Aerobic Digestion r Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number ot Excee- encesy Frequency of Analysis Sample Type Analytical Tech- ni age Minimu Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 139,902.62 147,064 153,331.91 MGN/g 0 bimonthly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) 1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. OZ uptake) Alt. 5 (14-Day Aerobic) G Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) El Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." r ` "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator Prep/a'rer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WWTP Name: WWTP cake (8/12/2020 sample) WQ Permit Number: WQ0001346 NPDES Number: NCO024333 Monitoring Period: From 7/l/2020 To 9/30/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAIt. (1) Fecal Density J Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion 21 Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- nces Frequency of Analysis Sample Type Analytical Tech - ni aue MinimumGeo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 139,902.62 147,064 153,331.91 MPN/g 0 quarterly Grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) R1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑I Alt. 4 (Spec. Oz uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Wt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed' CERTIFICATION STATEMENT (please check the appropriate statement) C1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator - Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) P AIL UR PROM PT- A CCU RATE -RE LIA©LE LABORATORIES, INC WWW.PARLABS.00M REPORT OF ANALYSi S KEN MORRIti .-TY OF MONROE W:ASTEWATER.PLANT PR.j'JF;C 7 NAMF: OCT 20 BOX 69 A u% 0 / 2 0 AONROE, NC 28111- i:E NUMBER- 1 401 5 SAh4FLE ID ;;:it�1'` '.; WGiT, SPMPL.E MA_f- X WW AMPLER_ SA['1P ECEIVED- J`_, r'iJ SAMi�. ER -,M RECEIVED1 Y� . - ..ECE'IVED 1 2401 DELIVERED BY FM TYPE SAMPLE- rat; 3C7c 1.of i NA1,YS::., .NALYSIS MFT?C-:-'. E-ATF: 7--ME BY RESt7'.T T..1Tv?TS _; AL COLAORM (Gr;OM. MEAN SM 9:'_[' ._ /_.. .'0 4C RE /9,'(19 MPN!9 f/_ LAPORATCPY 21217 Graliam Park Drive • Charlotte. NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 Am P PROM PT•AC GU RATE• RELIABLE L.ABC7 EtAiORI1-S, IWC IM140153 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CITY OF MONROE MONROE WWTP 10/06/20 FECAL COLIFORM, GEOMETRIC MEAN • SM 9221 E 1 17,351 22.11 % 78,474.99 2 17,648 21.60% 81,704.69 3 16,739 21.49% 77,893.11 4 17,338 20.80% 83,358.74 5 17,413 22.30% 78,086.21 6 17,808 21.68% 82,137.86 7 17,022 22.04% 77,233.69 Fecal Coliform Geometric Mean= • : • � I PA� � CHAIN OF CUSTODY t.natswvr,�ar�s.�rc, PAR Laboratories, Inc Phone (704) 580-8333 Fax (704) 588-8335 WWw.parfabs.t:om shipping: Mailing: 2217 Graham Park Drive PO Box 4114$3 Chariorte, NC 28273 Charlotte, NC 28241-1+483 fi A easaM141 that ah inion wWn 4a recorded on this Chain or Custody documsm for acccutancc by PAR Laubratorlrc. Inc. and #* Nom �2:1" Pwg aWrnet" of Ett�aonnmral and Natural f sourcaa. y Name ItAl1ing) f Commantx! specill Ingt PO Box 64 Mmrue, NC 2811) 503 BZ05OLDDS REPORTING 14 THI-S FUR STATE or EPA REPO TING? YES . NO *UMPN type- Dw __ WW GWMW _ HW _ Soil ether -sample Tginp at time of sampling: 17, ( °C Sampte Temp upon receipt: 111z. pr+ow'Ve(j, Yes No X Tefion Liner/ Zero Headspace: Yes No NlA X �GI[�Rt semple b. 5—a mp la Location ! Numhe. Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analya R" 0 i WWTP X NONE a 5 ae 1',1 FECAL COLIFORM N i VJwtf X NONE j I FECAL COLIFORM 3 X NONE . t o �o Sf '. ((Q FECAL COLIFORM _. X NONE ! o S _ l to FECAL COLIFORM X NONE t a� $ : t 7 FECAL COLIFORM it P X NONE t FECAL COLIFORM X NONE tD 5 8' ' t g FECAL COLIFORM ' 4011rfquiAhoo by Daterrime Roceivedby: DtatolTime wtt*, 15 S o)o (� % ingtaighad by: DatcrTime Received by: Uate/Tinta ' r.—Carnpaaite GRGrab DW=Dnrking Water WW=Wastewater GWMW-Groundwater Monitoring Well HW-Ha2nrdotrs Waste . Sete Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) u Facility Name: City of Monroe WWTP Name: Monroe WWTP cake WQ Permit Number: WQ0001346 NPDES Number: NCO024333 Monitoring Period: From 10/1/2020 To 12/31/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 L Alternative 3 El Alternative 4 ❑ Alternative 5 �r Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 111 Heat Drying ❑ Heat Treatment ❑ Thermophilic Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 J Alternative 2 C .................... ......................... If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization '❑ Air Drying❑ I Composting ❑ jAerobic Digestion Dv Anaerobic Digestion El If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dences Frequency of Analysis Sample Type Analytical Tech - m aue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 77,233.69 79,809 83,358.74 MGN/g 0 bimonthly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) 1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAIL 4 (Spec. 02 uptake) 7-' Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ 1Alt. 8 (Drying - Unstable) D Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." r "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: WWTP cake NPDES Number: NCO024333 Monitoring Period: From 10/1/2020 To 12/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) C: 1 Alt B (Alk Treatment) Q Alt. C (Prior Testing)[] Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: lAlt. (1) Fecal Density v1 Alt. (2) Process to Significantly Reduce Pathogens G If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization C1 Air Drying El Composting ❑ jAerobic Digestion 21 Anaerobic Digestion EJ If applicable to alternative performed (Class A or Class B) complete the following monitoring data. Parameter Allowable Level in in Sludge Pathogen Density Number of Excee- dence Frequency of Analysis y Sample Type Analytical Tech - niaue Minimum Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 77,233.69 79,809 83,358.74 MGN/g 0 quarterly grab sm9221 e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) Alt. 2 (40-day bench) Cj Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) 711 [ Alt. 6 (Alk. Stabilization 1 Alt 7 (Drying - Stable) ❑ lAlt. 8 (Drying - Unstable) r': Alt. 9 (Injection) Ca Alt. 10 (Incorporation) Ej No vector attraction reduction alternatives were performed r CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) Ken Morris, Residuals Coordinator Land Applier Name and Title (if applicable)(type or print) A41— Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DFNR FORM PVRF 02T N2/2006) Date/ Sample % Solids, decimal Sodium Na, mg/kg Na, mg/I Na, meq/L Calcium Ca, mg/kg Ca, mg/I Ca, meq/L Magnesium Mg, mg/kg Mg, mg/I Mg, meq/L SAR 1-6-2020 / WWTP 0.157 510 80.07 3.48 18900 2967.3 148.37 2500 392.5 32.17 0.37 4-1-2020 / WWTP 0.137 737 100.97 4.39 16500 2260.5 113.03 2160 295.92 24.26 0.53 4-16-2020 / WWTP 0.138 855 117.99 5.13 17700 2442.6 122.13 2340 322.92 26.47 0.60 5-18-2020 / WWTP 0.155 716 110.98 4.83 9030 1399.65 69.98 1520 235.6 19.31 0.72 7-1-2020 / WWTP 0.177 633 112.04 4.87 14500 2566.5 128.33 2150 380.55 31.19 0.55 7-22-2020 / WWTP 0.193 741 143.01 6.22 14900 2875.7 143.79 2200 424.6 34.80 0.66 8-12-2020/WWTP 0.239 628 150.09 6.53 121001 2891.9 144.60 1810 432.59 35.46 0.69 10-5-2020/WWTP .... _ 1-6-2020 / WTP 0.205 .. �_- 0.285 7321 ....-... .. 198 150.06 ._. 56.43 6.52 2.45 15500 2640 3177.5 752.4 158.88 37.62 2240 663 459.2 188.955 37.64' 15.49 0.66 0.48 4-1-2020 / WTP 0.205 610 125.05 5.44 1900 389.5 19.48 433 88.765 7.28 1.49 7-1-2020 / WTP 0.315 397 125.06 5.44 2010 633.15 31.66 352 110.88 9.09 1.20 10-5-2020 / WTP 0,334 374 124.92 01 5.43 0.00 1950 651.3 0 0 32.57 0.00 0.00 404 134.936 0 11.06 0.00 1.16 #DIV/0! 0 0.00 0 0.00 #DIV/01 0 0.00 0.00 0 0.00 0 0.00 #DIV/0! 0 01 0.00 0 0.00 #DIV/0! Exchangeable Sodium Percentage ESP = {(Na)/ (Ca+Mg+K+Na)} x 100 Field {(Na) /(Ca+Mg+K+Na)}x100 ESP NC-UN-18-1 A/ (65.6+12.3+2.8+.4) X 100 .47 NC-UN-18-2 .5 / (65.4+14.8+1.9+.5) X 100 .61 NC-UN-18-7 .8 / (54.8+18.1+2.3+.8) X 100 1.05 NC-UN-18-8 .8/ (62.7+16.0+2.0+.8) X 100 .98 NC-UN-29-3 .6 / (59.0+18.6+4.5+.6) X 100 .73 NC-UN-29-4 .4 / (60.2+23.9+7.1+.4) X 100 .44 NC-UN-30-1 .5 / (56.7+19.8+6.2+.5) X 100 .60 NC-UN-30-5 .6 / (59.6+19.3+1.2+.6) X 100 .74 NC-UN-31-3 .4 / (47.8+13.9+3.8+.4) X 100 .61 NC-UN-31-4 .5 / (57.6+17.3+3.7+.5) X 100 .63 no Page 1 of 2 Report Number: 21-007-0588 Account Number: 46205 Send To: City of Monroe Ken Morris 775 Treeway Dr Monroe NC 28110 Waypoint ANALYTICAL "Every acre... Every year. "rM 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Ben Myers 3208 Helms Pond Rd Monroe NC 28110 Farm: UN18 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Date Received: 01/07/2021 Date Of Analysis: 01/08/2021 Date Of Report: 01/08/2021 NC = North Carolina Fertilitv Index Value Sample ID Field ID Lab Number OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A M3 ppm Rate ppm Rate ppm Rate K pp m Rate M g ppm Rate Ca ppm Rate Na ppm Rate Soil P H Buffer Index H me /100 q g me /100 q g UN18-1 13005 9.2 VH 150 575 VH NC = 479 157 H NC = 80 216 M 1915 M 12 VL 5.8 6.65 2.8 14.6 M-O UN18-2 13006 8.6 VH 150 188 VH NC = 157 92 L NC = 47 1 219 M 11610 M 13 VL 5.9 6.72 2.1 12.3 MIN UN18-7 13008 4.2 M 122 145 VH NC = 121 75 L NC = 38 185 H 1 932 M 15 VL 5.6 6.73 2.0 8.5 MIN UN18-8 13009 4.4 M 126 275 VH NC = 229 64 L NC = 33 161 H 1054 M 16 VL 5.8 6.77 1.6 8.4 MIN Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts K % Mg % Ca ova Na off, H off, NO, N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate UN18-1 2.8 12.3 65.6 0.4 19.2 19 M NC = 40 41.1 VH NC = 1027.5 24 H NC = 150 343 VH 13.3 VH NC = 665.0 0.9 M UN18-2 1.9 14.8 65.4 0.5 17.1 15 L NC=31 24.9 VH NC=622.5 22 H NC=138 328 VH 7.6 VH NC=380.0 0.7 M UN18-7 2.3 18.1 54.8 0.8 23.5 18 M NC=37 10.2 VH NC=255.0 18 M NC=113 517 VH 1.8 H NC=90.0 0.5 L UN18-8 2.0 16.0 62.7 0.8 19.0 16 M NC=33 12.2 VH NC=305.0 24 H NC=150 305 VH 5.8 VH NC=290.0 0.5 L Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc. Pauric Mc Groary Ph.D., CPAg Page 2 of 2 Report Number: 21-007-0588 Account Number: 46205 Send To: City of Monroe Ken Morris 775 Treeway Dr Monroe NC 28110 Date Received: 01/07/2021 Date Of Report: 01/08/2021 0 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743.9401 (Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com "Every acre... Every year. "TM Grower: Ben Myers 3208 Helms Pond Rd Monroe NC 28110 Farm: UN18 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Yield Goal Lime Field ID Intended Crop Tons Tons/A N P205 KO Mg S Zn Mn Fe Cu B Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A UN18-1 Pasture 3 0.5 50 0 40 0 9 0 0 0 0 0 U N 18-2 Pasture 3 0.5 50 0 94 0 14 0 o 0 0 0 U N 18-7 Pasture 3 1.3 50 0 94 0 10 T- 0 2 0 0 0 UN18-8 Pasture 3 1.0 50 0 107 0 13 0 0 0 0 0 Comments: Sample(s) : UN18-2,UN18-7,UN18-8 Crop: Pasture For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer. For soils low in sulfur, apply 20-40 Ibs of sulfur as a sulfate in the spring with the nitrogen. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric Mc Groary Ph.D., CPAg Page 1 of 2 Report Number: 21-007-0589 Account Number: 46205 Send To: City of Monroe Ken Morris 775 Treeway Dr Monroe NC 28110 o Waypoint ANALYTICAL "Every acre... Every year. "tM 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: William Griffin 6705 Austin Grove Rd Marshville NC 28103 Farm: UN29 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Date Received: 01/07/2021 Date Of Analysis: 01/08/2021 Date Of Renort: n1lnAl9n91 nlr = N rth InA %/oI Sample ID Lab OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Field ID Number % Soil lbs/A M3 K Mg Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg1100g meq/100g UN29-3 13010 5.6 145 274 VH 204 VH 259 H 1369 M 16 VL 5.9 6.73 2.0 11.6 MIN H 1 1 NC = 228 -7UN29-4 NC = 104 13011 7.6 150F207 VH 383 VH 1 396 H M 14 VL 6.4 6.81 1.2 13.8 MIN VH NC = 172 NC = 196 11661 1 1 1 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID Field ID K Mg Ca Na H NO, N S Zn Mn Fe Cu B SS ova % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate UN29-3 4.5 18.6 59.0 0.6 17.2 18 M 19.7 VH 21 H 225 VH 13.5 VH 0.6 M NC=37 NC=492.5 NC=131 NC=675.0 UN29-4 7.1 23.9 1 60.2 1 0.4 1 8.7 19 M 29.0 VH 32 H 289 VH 12.7 VH 0.8 M NC = 40 NC = 725.0 NC = 200 NC = 635.0 values un uus repurt represent me plant avauaDle nutrients In the Lxplanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc. Pauric Mc Groary Ph.D., CPAg Page 2 of 2 Report Number: 21-007-0589 Account Number:46205 Send To: City of Monroe Ken Morris 775 Treeway Dr Monroe NC 28110 Date Received: 01/07/2021 Date Of Report: 01/08/2021 0 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com "Every acre... Every year.".M Grower: William Griffin 6705 Austin Grove Rd Marshville NC 28103 Farm: UN29 SOIL FERTILITY RECOMMENDATIONS Sample ID Yield Goal Lime Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Field ID Intended Crop Tons Tons/A N P205 K20 Mg S Zn Mn Fe Cu B Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A UN29-3 Pasture 3 1.3 50 0 0 0 10 0 0 0 0 0 UN29-4 Pasture 3 0.0 50 0 0 0 9 0 0 0 0 0 Comments: Sample(s) : UN29-4 Crop: Pasture For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer. For soils low in sulfur, apply 20-40 Ibs of sulfur as a sulfate in the spring with the nitrogen. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric Mc Groary Ph.D., CPAg Page 1 of 2 Report Number: 21-007-0591 Account Number: 46205 Send To: City of Monroe Ken Morris 775 Treeway Dr Monroe NC 28110 • Waypoint ANALYTICAL "Every acre... Every year. "TM 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Tom Appenzeller 830 Clover Rd Marshville NC 28103 Farm: UN30 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Date Received: 01/07/2021 Date Of Analysis: 01/08/2021 Date Of Report: 01/08/2021 NC = North Carolina Fertilitv Index Value Sample ID Field ID Lab Number OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate M g ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H megl100g meq/100g UN30-1 13014 6.5 150 248 VH 269 VH 264 H 1259 M 14 VL 5.9 6.74 1.9 11.1 MIN H NC = 207 NC = 138 UN30-5 13015 5.9 [__� 150 70 H 38 VL 192 H 989 M 11 VL 5.8 6.77 1.6 8.3 MIN H NC=58 NC=19 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID Field ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate UN30-1 6.2 19.8 56.7 0.5 17.1 17 M 20.2 VH 23 H 287 VH 11.1 VH 0.7 M NC=35 NC=505.0 NC=144 NC=555.0 UN30-5 1.2 1 19.3 1 59.6 0.6 19.3 13 L 13.9 VH 25 H 204 VH 4.6 VH 0.5 L NC=27 NC=347.5 NC=156 NC=230.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. by. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric Mc Groary Ph.D., CPAg Page 2 of 2 Report Number: 21-007-0591 Account Number: 46205 Send To: City of Monroe Ken Morris 775 Treeway Dr Monroe NC 28110 Date Received: 01 /07/2021 Date Of Report: 01/08/2021 • Waypoint ANALYTICAL "Every acre... Every year. "rM Farm: UN30 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Tom Appenzeller 830 Clover Rd Marshville NC 28103 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Yield Goal Lime Field ID Intended Crop Tons Tons/A N P205 K20 Mg S Zn Mn Fe Cu B Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A UN30-1 Pasture 3 1.0 50 0 0 0 11 0 0 0 0 0 UN30-5 Pasture 3 1.0 50 30 120 0 16 0 0 0 0 0 Comments: Sample(s) : UN30-5 Crop: Pasture For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer. For soils low in sulfur, apply 20-40 Ibs of sulfur as a sulfate in the spring with the nitrogen. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric Mc Groary Ph.D., CPAg Page 1 of 2 Report Number: 21-007-0590 Account Number:46205 Send To: City of Monroe Ken Morris 775 Treeway Dr Monroe NC 28110 Waypoint ANALYTICAL "Every acre... Every year.'4M 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Henry Myers 3809 Farmwood Dr Monroe NC 28110 Farm: UN31 SOIL ANALYSIS REPORT AnalyticalMethod(s): Mehlich3 SMPBuffer pH Loss On Ignition Water pH Date Received: 01/07/2021 Date Of Analvsis: 01/08/2021 oatra Of Rannrt• m ma/?n,)1 nlr Sample ID Field ID Lab Number OM wN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H meq/100g meq/100g UN31-3 13012 6.8 H 150 148 VH NC = 123 147 H NC = 75 165 M 947 L 10 VL 5.2 6.59 3.4 9.9 MIN UN31-4 13013 6.9 H 150TNC 174 VH = 145 158 H NC = 81 228 H 1267 M 12 VL 5.7 6.70 2.3 11.0 MIN Sample ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Field ID K % Mg % Ca % Na % H % NON ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate UN31-3 3.8 13.9 47.8 0.4 34.3 15 L NC=31 15.4 VH NC=385.0 22 H NC=138 367 VH 4.7 VH INC =235.0 0.5 L UN31-4 3.7 1 17.3 57.6 0.5 1 20.9 17 M INC = 35 19.9 VH NC = 497.5 20 M NC = 125 337 VH 5.7 VH NC = 285.0 11.7 M �.,r.,, � w, ���, •� �= v— , a�a.�a��e i iu —...w u i u is mxpianauun or symoois: io (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = lbs/A, Soluble by C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc. Pauric Mc Groary Ph.D., CPAg r Page 2 of 2 Report Number: 21-007-0590 Account Number: 46205 Send To: City of Monroe Ken Morris 775 Treeway Dr Monroe NC 28110 Date Received: 01/07/2021 Date Of Report: 01/08/2021 o Waypoint ANALYTICAL "Every acre... Every year. "- Farm: UN31 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Henry Myers 3809 Farmwood Dr Monroe NC 28110 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A lb/A UN31-3 Pasture 3 2.2 50 0 40 0 14 0 0 0 0 0 UN31-4 Pasture 3 1 1.3 50 0 40 F 0 11 0 2 0 0 0 Comments: Sample(s) : UN31-4 Crop: Pasture For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer. For soils low in sulfur, apply 20-40 Ibs of sulfur as a sulfate in the spring with the nitrogen. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric Mc Groary Ph.D., CPAg