NCG510532_Monitoring Report_20150426

NPDES DOCUMENT !MCANNINO COVER SHEET
NCG510532
140 West Franklin remediation
NPDES Permit:
Document Type:
Permit Issuance
Wasteload Allocation
Authorization to Construct (AtC)
Permit Modification
Complete File - Historical
Monitoring
Report
Instream Assessment (67B)
Environmental Assessment (EA)
Permit
History
Document Date:
April 26, 2015
This document is printed on reuse paper - ignore any
content on the re'rerae side

Permit NC0001 121
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby
revoke4 and as of this issuance, any previously issued permit bearing this number is no longer effective.
Therefore, the exclusive authority to operate and discharge from this facility arises under the permit
conditions, requirements, terms, and provisions described herein.
Specialty Product Technologies is hereby authorized to:
1, Continue to operate an existing wastewater treatment facility with design flow of 0.17 MGD for
process -contact wastewater (Outfall 001) that includes the following components:
• Chromium and cyanide batch treatment tanks,
• Acid -alkaline holding tank,
• Clarifier,
• Plate and frame press
2. Continue to operate a 0.152 MGD groundwater-remediation related wastewater treatment system
including a packed tower air stripper (Outfall 003).
3. Continue to combine wastewaters from internal Outfalls 001 and 003 at a final wastewater Outfall
Q04; all outfalls and facilities located at Danaher Sensors and Controls Products (2100 West
Broad Street, north of Elizabethtown) in Bladen County.
4. Continue to discharge from the above -listed facilities, at the locations specified on the attached map,
to the Cape Fear River, currently a Class C stream in the Cape Fear River Basin.
Part 1, Page 2 of 7

ARG
Ammons Resource Group
2040 Peach Grove Lane Zebulon, NC 27597
919-369-5679 fredammons©att.net
April 26, 2015
To Whom It May Concern
Central Files
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RECEIVED
mAY G
CENTRAL FILES
DVVR SECTION
Subject: MARCH 2015 DISCHARGE MONITORING REPORT
140 WLSI- FRANKLIN, LLC;
140 WEST FRANKLIN STREET
CHAPEL HILL, ORANGE COUNTY, NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
Attached is the March 2015 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill, North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Flow rates were recorded and documented and were below the permitted daily maximum limits.
This information is submitted as required by Part II, of Section D. (2.) of its NPDES Permit. Inlet
water samples will be collected and analyzed as requested by the Town of Chapel Hill in
reference to the request to the state from the property owners to rescind the NPDES permit
number NCG510532 in the month of May, 2015. The analytical information will be forwarded to
the Town of Chapel Hill for their approval to decommission the treatment system operation.
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely,
Ammons Resource Group
Fred A
ORC
on
Enclosures: March 2015 DMR
cc: 140 West Franklin, LLC
Mr. Ernest Odei-Larbi, Chapel Hill

NPDES PERMIT NO. NCG5 10532
FACILITY NAME 140 WEST FRANKLIN
EFFLUENT
DISCHARGE NO. 001 MONTH March
CLASS NA COUNTY ORANGE
YEAR 2015
CERTIFIED LABORATORY (1) SGS Environmental Services, Inc CERTIFICATION NO. 481
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons
PERSON(S) COLLECTING SAMPLES Fred Ammons
CHECK BOX IF ORC HAS CHANGED 0
Mail ORIGINAL and ONE COPY to:
ATM: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
GRADE I CERTIFICATION NO. 992126
ORC PHONE [phone]
NO FLOW / DISCHARGE FROM SITE *
(SIGNATUR OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIG ATURE, I CERTIFY THAT THIS REPORT IS
CCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DATE
0
DATE
Operator Arrival Time
2400 Rock
Operator Time
On Site
ORC On Site? **
50050
34030
34371
34010
81551
22417 1
34696
01051
00530
00400
32103
03604
00556
FLOW
BENZENE
ETHYLBENZENE
TOLUEN;
TOTAL XYLENES
METHYL TERT_BUTYL
ETHER (MTBE)
NAPHTHALENE
TOTAL LEAD
TOTAL SUSPENDED
SOLIDS (TSS)
a
1,2 DICHLOROETHANE
(1,2 DCA)
TOTAL PHENOLS
OIL AND GREASE
EFFM
INF 0
.-114
.. a
0
HRS
HRS
Y/BIN
MGD
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
mg/L
UG/L
UG/L
1
0.000000
2
0.000000
3
0.000000
4
1000
2
yes
0.000000
5
0.002056
6
0.002056
7
0.002056
8
,
0.002056
9
0.002056
10
0.002056
11
1430
2
yes
0.002056
12
0.002056
13
0.002056
14
0.002056
15
0.002056
16
0.002056
17
0.002056
18.1100
2
yes
0.002056
19
0.002149
20
0.002149
21
0.002149
22
0.002149
23
0.002149
24
0.002149
25
0.002149
26
0.002149
27
0.002149
28
0.002149
29
0.002149
30
1000
2
yes
0.002149
31
0.002149
AVERAGE
0.001830
_
MAXIMUM
MINIMUM
Comp. (C) / Grab (G)
G
Daily Maximum
1.19
97
11
670
19
12
25
30
6<pH<9
0.38
300
monitor
DWQ Form MR-1 (11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
All monitoring data and sampling frequencies do NOT meet permit requirements
x
�'omhli int
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
tor gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
S
nt or type)
AtrnL ICA'nc. V-eCt
Signature f Permittee(* * Date
(Required unless submitted electronically)
Permittee Address Phone Number e-mail address Permit Expiration Date
126 West Franklin Street, Chapel Hill NC 27516 [phone]
February 28, 2017
ADDITIONAL CERTIFIED LABORATORIES
certified Laboratory (2) t nvironmental 1 esting solutions, Inc L.ertiticatiOn NO.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wgs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per I5A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

ARG
Ammons Resource Group
2040 Peach Grove Lane Zebulon, NC 27597
919-369-5679 [e-mail]
February 17, 2015
To Whom It May Concern
Central Files
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RECEIVED
MAR 0 4 2015
CENTRAL FILES
DWR SECTION
Subject: JANUARY 2015 DISCHARGE MONITORING REPORT
140 WEST FRANKLIN, LLC
140 WEST FRANKLIN STREET
CHAPEL HILL, ORANGE COUNTY, NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
Attached is the January 2015 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill, North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Water samples were collected from outfall 001 on January 28, 2015 for the quarterly sampling
event as required by the permit. Samples were sent to SGS Environmental Services, Inc. of
Wilmington, North Carolina for analysis. Analytical results indicate that all compounds were
below the permitted daily maximum limits. Flow rates were recorded and documented and were
below the permitted daily maximum limits. This information is submitted as required by Part II, of
Section D. (2.) of its NPDES Permit. Water samples will be collected and analyzed as required
by the permit in February 2014.
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely,
Ammons Resource Group
Fr�d ns `
ORC
Enclosures: January 2015 DMR
cc: Mr. Scott Milke, 140 West Franklin, LLC
Mr. Ernest Odei-Larbi, Chapel Hill

EFFLUENT YEAR 20-=
DISCHARGE NO. 001 MONTH January
NPDES PERMIT NO. NCG510532 --
FACILITY NAME 140 WEST FRANKLIN CLASS �COUNTY ORANGECERTIFICATION NO. 481
CERTIFIED LABORATORY (1) SGS Environmental Services Inc
(list additional laboratories on the backside/page 2 of this form) GRADE IORC CERTIFICATION NO. 992126
OPERATOR IN
RESPONSIBLE CHARGE (ORC) Fred Ammons DONE [phone]
NO FLOW / DISCHARGE FROM SITE *
PERSON(S) COLLECTING} SAMPLES Fred Ammons
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIVISION OF WATER QUALITY
i 17 MAIL SERVICE CENTER
x Li � r• �'�.�
(SIGNA • PE' ' OR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
('('I!uerR AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
2-
DATE
a
RALEIGH, NC 27699-1617
...-..--. _ _ _ _ _ --
00400
32103
TOTAL PHENOLS M
OIL AND GREASE
._.
F
c
I g
II
A
8
8
50050
34030
wz
N
34371
34010
81551
22417
34696
01051
00530
W
vz2
rn�
Cl).l
"�
� o
0
°ice'
a
illFLOW
�,
WI d
O
ac
N
o ry
N
UG/L
W
N
z
m
Gal
w
°
F
O
e
m00
1
a
�c;
EQQ
=GlZ
F
Z
J4s1
Q
F
UG/L !
p
'4
o
U
EFFF1
:, INF
❑
Cd
0
Q�z
gm
c,
HRS
YIB/N
MGD
UG/L
UG/L
UG/L
UG/L I
UG/L
1
H
HRS
0.0018 80
I
2
0.001880
0.001880
3
0.001880
I
4
,
0.001880
5
0.001880
6
1300
2
yes
0.002125
7
0.002125
,
8
0.002125
9
0.002125
10
0.002125
11
12
0.002125
13
0.002125
14
0.002125
15
0.002125
-
16
1300
2
yes
0.002125
17
0.001621
18
0.001621
19
0.001621
20
1300
2
yes
0.001621
21
0.001652
22
0.001652
23
0.001652
24
0.001652
25
0.061652
26
0.061652
27
0.001652
_
28
1300
2
yes
0.001652
ND
ND
ND
ND
ND
ND
ND
ND
8.84
ND
4
NS
29
0.001652
30
0.001652
31
0.001652
AVERAGE
0.001845
,
MAXIMUM
MINIMUM
Comp. (C) / Grab (G)
1 G
Daily Maximum
1.19 97
11
670
19
12 25
30
6<pH<9
0.38
300
monitor
DWQ Form MR-1 (11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
All monitoring data and sampling frequencies do NOT meet permit requirements
Compliant
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Scott Milke, 140 West Franklin, LLC
Permittee (Please print or type)
.17(//41
z Zt-l5�
Signature of Permittee*** Date
(Required unless submitted electronically)
Permittee Address Phone Number e-mail address Permit Expiration Date
126 West Franklin Street, Chapel Hill NC 27516 [phone] February 28, 2017
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Environmental Testing Solutions, Inc Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
37
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

Laboratory Report of Analysis
To: Fred Ammons
Ammons Resource Group
2040 Peach Grove Lane
Zebulon, NC 27597
Report Number: 31500185
Client Project: 140 West
Dear Fred Ammons,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. All results are
intended to be used in their entirety and SGS is not responsible for use of less than the complete report. Any
samples submitted to our laboratory will be retained for a maximum of thirty (30) days from the date of this report
unless other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Michael D. Page
at [phone]. We will be happy to answer any questions or concems which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America Inc.
Digitally signed by: Michael Page
DN: CN = Michael Page C = US O = SGS North
America OU = Environmental Services
Date: 2015.02.16 14:32:04 -04'00'
Michael D. Page
Project Manager
[e-mail]
Date
N.C- Certification # 481
This document is issued by the Company under its General Conditions of Service accessible at hup-ovr.v;, sgs comfen!f erns-and-Cow:1'lons hlm. Attention is drawn
to the limitation of liability, indemnification and jurisdiction issues defined therein.
Any holder of this document is advised that information contained hereon reflects the Company's findings at the time of its intervention only and within the limits of
Client's instructions, if any. The Company's sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their
rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful
and offenders may be prosecuted to the fullest extent of the law.
SGS 5500 Business Drive Wi4nnator', NC 28405 [phone] I [phone] www.sgs.com
Msrnbor or the SOS Group (SOS SA)
Page 1 of 26

Laboratory Qualifiers
Report Definitions
DL Method, Instrument, or Estimated Detection Limit per Analytical Method
CL Control Limits for the recovery result of a parameter
LOQ Reporting Limit
DF Dilution Factor
RPD Relative Percent Difference
LCS(D) Laboratory Control Spike (Duplicate)
MS(D) Matrix Spdce (Duplicate)
MB Method Blank
Qualifier Definitions
Recovery or RPD outside of control limits
B Analyte was detected in the Lab Method Blank at a level above the LOQ
U Undetected (Reported as ND or < DL)
J Estimated Concentration.
E Amount detected is greater than the Upper Calibration Limit
TIC Tentatively Identified Compound
ND Not Detected
P RPD > 40% between results of dual columns
D Spike or surrogate was diluted out in order to achieve a parameter result within instrument calibration
range
Samples requiring manual integrations for various congeners and/or standards are marked and dated by the analyst. A
code definition is provided below:
M1 Mis-identified peak
M2 Software did not integrate peak
M3 Incorrect baseline construction (i.e. not all of peak included; two peaks integrated as one)
M4 Pattern integration required (i.e. DRO, GRO, PCB, Toxaphene and Technical Chlordane)
M5 Other - Explained in case narrative
Note Results pages that include a value for "Solids (%)" have been adjusted for moisture content.
Print Date: 02/16i20 iN C Certification # 481
Page 2 of 26

Sample Summary
Client Sample ID Lab Sample ID Collected Received Matrix
OUTFALL
Print Date 02/16/2015
31500185001 01/28/2015 12:00 01/29/2015 10:15 Water
N.C. Certification # 481
Page 3 of 26

Case Narrative
OUTFALL
SM4500H-B: This sample was analyzed outside of the method specified hold time for pH.
Print Dale: 02/16/2015
N.0 Certification # 481
Page 4 of 26

SG$
Detectable Results Summary
Client Sample ID: OUTFALL
Lab Sample ID: 31500185001-E Parameter Result Units
EPA 420.1 (SUB) Phenol 0.004 mg/L
SM 4500-H+ B pH pH 8.84 S.U.
pH at Temperature 7.7 C
Print Date: 02/16/2015
•
N.0 Certification # 481
Page 5 of 26

r Results of OUTFALL
Client Sample ID: OUTFALL
Client Project ID: 140 West
Lab Sample ID: 31500185001-A
Lab Project ID: 31500185
Results by SW-846 8260E
Parameter
1,2-Dichloroethane
Benzene
Ethyl Benzene
Naphthalene
Toluene
m,p-Xylene
o-Xylene
tert-Butyl methyl ether (MTBE)
Surrogates
1,2-Dichloroethane-d4
4-Bromofluorobenzene
Toluene d8
Result
ND
ND
ND
ND
ND
ND
ND
ND
100
95.0
103
Batch Information
Analytical Batch: VMS3506
Analytical Method: SW-846 8260E
Instrument: MSDB
Analyst: BWS
Print Date: 02/16/2015
Collection Date: 01 /28/2015 12:00
Received Date: 01/29/2015 10:15
Matrix: Water
♦
i
gig' DL LOQ/CL Units DF
U 0.0910 1.00 ug/L 1
U 0.136 1.00 ug/L 1
U 0.224 1.00 ug/L 1
U 0.120 1.00 ug/L 1
U 0.149 1.00 ug/L 1
U 0.401 2.00 ug/L 1
U 0.209 1.00 ug/L 1
U 0.0960 1.00 ug/L 1
64.0-140
85.0-115
82.0-117
0/0
Prep Batch: VXX5499
Prep Method: SW-846 5030B
Prep Date/Time: 02/04/2015 15:20
Prep Initial VVt.Not.: 40 mL
Prep Extract Vol: 40 mL
Date Analyzed
02/4/2015 12:34
02/4/2015 12:34
02/4/2015 12:34
02/4/2015 12:34
02/4/2015 12:34
02/4/2015 12:34
02/4/2015 12:34
02/4/2015 12:34
02/4/2015 12:34
02/4/2015 12:34
02/4/2015 12:34
N.C. Certification # 481
Page 6 of 26

Results of OUTFALL
Client Sample ID: OUTFALL
Client Project ID: 140 West
Lab Sample ID: 31500185001-F
Lab Project ID: 31500185
Results by SW-846 6010C
Parameter
Lead
Batch Information
Result
ND
Analytical Batch: MIP2719
Analytical Method- SW-846 6010C
Instrument: ICP1
Analyst: PSW
Print Date 02/16/2015
Collection Date: 01/28/2015 12:00
Received Date: 01/29/2015 10:15
Matrix: Water
DL
0.00794
LOQ/CL Units DF
0.0100 mg/L 1
Prep Batch: MXX3844
Prep Method: SW-846 3010A
Prep Date/Time. 01/30/2015 08:24
Prep Initial Wt.Nol 50 mL
Prep Extract Vol'. 50 mL
Date Analyzed
02/2/2015 14:56
N.0 Certification # 481
Page 7 of 26

r Results of OUTFALL
Client Sample ID: OUTFALL
Client Project ID: 140 West
Lab Sample ID: 31500185001-D
Lab Project ID: 31500185
Results by SM 2540-D
Parameter
Total Suspended Solids
Batch Information
Analytical Batch: INO3632
Analytical Method: SM 2540-D
Instrument: BAL10
Analyst: VML
Print Date: 02/16/2015
Result
ND
♦
Collection Date: 01/28/2015 12:00
Received Date: 01/29/2015 10:15
Matrix: Water
ual DL
3.60
LOQ/CL Units OF
25.0 mg/L 1
Prep Batch: INO3632
Prep Method: SM 2540-D
Prep Date/Time: 01/29/2015 15:01
Prep Initial Wt./Vol.: 1 mL
Prep Extract Vol: 1 mL
Date Analyzed
01/29/2015 15:01
N.C. Certification # 491
Page 8 of 26

r Results of OUTFALL - •
Client Sample ID: OUTFALL
Client Project ID: 140 West
Lab Sample ID: 31500185001-A
Lab Project ID: 31500185
Results by SM 4500-H+ B pH
Parameter
pH
pH at Temperature
Batch Information
Analytical Batch: 1
Analytical Method:
Instrument: PH1
Analyst: VML
Print Date: 02/16/2015
Result
8.84
7.7
Collection Date: 01/28/2015 12:00
Received Date: 01/29/2015 10:15
Matrix: Water
ual DL LOQ/CL Units DF Date Analyzed
0.0100 0.0100 S.U. 1 02/2/2015 10:41
C 1 02/2/2015 10:41
N03636
SM 4500-H+ B pH
Prep Batch: IN03636
Prep Method: SM 4500-H+ B pH
Prep DatefTime: 02/02/2015 10:41
Prep Initial Wt.Nol.: 1 mL
Prep Extract Vol: 1 mL
N.0 Certification # 481
Page 9 of 26

Results of OUTFALL
Client Sample ID: OUTFALL
Client Project ID: 140 West
Lab Sample ID: 31500185001-E
Lab Project ID: 31500185
Collection Date: 01/28/2015 12:00
Received Date: 01/29/2015 10:15
Matrix: Water
Results by EPA 420.1 (SUB)
Parameter Result Qual DL LOQ/CL Units DF Date Analyzed
Phenol 0.004 mg/L 1 02/12/2015 0:00
Laboratory: Envirochem
Analytical Date/Tirne: 02/12/2015 00:00
Print Date: 02/16/2015
Prep Method:
Prep Date/Time•
N.C. Certification # 481
t
Page 10 of 26

r Batch Summary
Analytical Method: SW-846 8260B
Prep Method:
Prep Batch:
Prep Date:
SW-846 5030B
VXX5499
02/04/2015 09:12
Client Sample ID
LCS for HBN 64855 [VXX/5499]
LCSD for HBN 64855 [VXX/5499]
MB for HBN 64855 [VXX/5499]
OUTFALL
6168 MS
6168 MSD
Lab Sample ID Analysis Date
158563 02/04/2015 10:31
158564 02/04/2015 10:55
158565 02/04/2015 11:45
31500185001 02/04/2015 12:34
31500193030 02/04/2015 20:33
31500193031 02/04/2015 20:58
Analytical Batch Instrument Analyst
VMS3506
VMS3506
VMS3506
VMS3506
VMS3506
VMS3506
MSD8 BWS
MSD8 BWS
MSD8 BWS
MSD8 BWS
MSD8 BWS
MSD8 BWS
Print Date: 02i16/2015 N.C. Certification # 481
1
Page 11 of 26

Method Blank
Blank ID: MB for HBN 64855 [VXXI54991
Blank Lab ID: 158565
QC for Samples:
31500185001
"— Results by SW-846 8260B
Parameter
Matrix: Water
Result Qual DL LOQ/CL Units DF
tert-Butyl methyl ether (MTBE) ND U 0.0960 1.00 ug/L 1
Benzene ND U 0.136 1.00 ug/L 1
1,2-Dichloroethane ND U 0.0910 1.00 ug/L 1
Toluene ND U 0.149 1.00 ug/L 1
Ethyl Benzene ND U 0.224 1.00 ug/L 1
m,p-Xylene ND U 0.401 2.00 ug/L 1
o-Xylene ND U 0.209 1.00 ug/L 1
Naphthalene ND U 0.120 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 102 64.0-140 % 1
Toluene d8 100 82.0-117 % 1
4-Bromofluorobenzene 94.0 85.0-115 % 1
Batch Information
Analytical Batch: VMS3506 Prep Batch: VXX5499
Analytical Method: SW-846 8260E Prep Method: SW-846 5030E
Instrument: MSD8 Prep Date/Time: 2/4/2015 9:12:59AM
Analyst: BWS Prep Initial Wt.Nol.: 40 mL
Prep Extract Vol: 40 mL
Print Date: 02/16/2015
N.C. Certification # 481
Page 12 of 26

Blank Spike Summary
Blank Spike ID: LCS for HBN 64855 [VXX/5499]
Blank Spike Lab ID: 158563
Date Analyzed: 02/04/2015 10:31
QC for Samples: 31500185001
Results by SW-846 8260E
Spike Duplicate ID: LCSD for HBN 64855 [VXX/5499]
Spike Duplicate Lab ID: 158564
Date Analyzed: 02/04/2015 10:55
Matrix: Water
Parameter
tert-Butyl methyl ether (MTBE)
Benzene
1,2-Dichioroethane
Toluene
Ethyl Benzene
m,p-Xylene
o-Xylene
Naphthalene
Surrogates
1,2-Dichloroethane-d4
Toluene d8
4-Bromofluorobenzene
Batch Information
Blank Spike (ug/L)
Spike Result Rec (%) Spike
5.00 4.97 99 5.00
5.00 5.03 101 5.00
5.00 5.01 100 5.00
5.00 4.49 90 5.00
5.00 4.85 97 5.00
10.0 9.55 96 10.0
5.00 4.60 92 5.00
5.00 5.01 100 5.00
Analytical Batch: VMS3506
Analytical Method: SW-846 8260E
Instrument: MSD8
Analyst: BWS
Print Date: 02/16r2016
101
94
101
Spike Duplicate (ug/L)
Result Rec (%1 CL RPD (%) RPD CL
4.98 100 47.0-142 0.20 30.00
5.02 100 76.0-124 0.20 30.00
5.20 104 76.0-119 3.7 30.00
5.16 103 75.0-123 14 30.00
4.95 99 76.0-123 2.0 30.00
9.81 98 76.0-124 2.7 30.00
4.73 95 75.0-124 2.8 30.00
4.97 99 67.0-122 0.80 30.00
100
104
98
64.0-140
82.0-117
85.0-115
Prep Batch: VXX5499
Prep Method: SW-846 5030E
Prep Date/Time: 02/04/2015 09:12
Spike Init Wt.Nol.: 40 mL Extract Vol: 40 mL
Dupe Init Wt.Nol.: 40 mL Extract Vol: 40 mL
N.C. Certification # 481
Page 13 of 26

Batch Summary
Analytical Method: SW-846 6010C
Prep Method: SW-846 3010A
Prep Batch: MXX3844
Prep Date: 01/30/2015 08:24
Client Sample ID
MB for HBN 63753 [MXX/3844J
LCS for HBN 63753 [MXX/3844]
LCSD for HBN 63753 [MXX/3844]
BT-SW-01(157958MS)
BT-SW-01(157958MSD)
OUTFALL
OUTFALL(157990DUP)
Print Date: 02/16/2015
Lab Sample ID Analysis Date
158133 02/02/2015 11:00
158134 02/02/2015 11:07
158135 02/02/2015 11:14
158136 02/02/2015 11:27
158137 02/02/2015 11:33
31500185001 02/02/2015 14:56
158138 02/02/2015 15:02
Analytical Batch Instrument Analyst
MIP2719
MIP2719
MIP2719
MIP2719
MIP2719
MIP2719
MIP2719
ICP1 PSW
ICP1 PSW
ICP1 PSW
ICP1 PSW
ICP1 PSW
ICP1 PSW
ICP1 PSW
N.C. Certification # 481
Page 14 of 26

r Method Blank
Blank ID: MB for HBN 63753 [MXX/3844]
Blank Lab ID: 158133
QC for Samples:
31500185001
`Results by SW-846 6010C
Parameter Result
Lead ND
Batch Information
Analytical Batch. MIP2719
Analytical Method: SW-846 6010C
Instrument: ICP1
Analyst: PSW
Print Date: 02/16/2015
Qual
Matrix: Water
DL
0.00794
LOQ/CL Units
0.0100 mg/L
Prep Batch: MXX3844
Prep Method: SW-846 3010A
Prep DatefTime: 1/30/2015 8:24:00AM
Prep Initial Wt.Nol.: 50 mL
Prep Extract Vol: 50 mL
DF
1
N.C. Certification # 481
Page 15 of 26

a.anr pie summary
Blank Spike ID: LCS for HBN 63753 [MXX/3844)
Blank Spike Lab ID: 158134
Date Analyzed: 02/02/2015 11:07
QC for Samples: 31500185001
Results by SW-846 6010C
Parameter Spike
Lead 0.400
Batch Information
Analytical Batch: MIP2719
Analytical Method: 1 SW-846 6010C
Instrument: ICP1
Analyst: PSW
Spike Duplicate ID: LCSD for HBN 63753 [MXX/38441
Spike Duplicate Lab ID: 158135
Date Analyzed: 02/02/2015 11:14
Matrix: Water
Blank Spike (mg/L) Spike Duplicate (mg/L)
Result
Rec (%) Spike Result Rec % CL RPD (%)
0.389 97 0.400 0.392 98 80.0-120 0.77
Prep Batch: MXX3844
Prep Method: SW-846 3010A
Prep Date/Time• 01/30/2015 08:24
Spike Init Wt.Nol.: 50 mL Extract Vol: 50 mL
Dupe Init Wt.NoI.: 50 mL Extract Vol: 50 mL
RPD CL
20.00
rnnl uaie uUlbrzulb
N C Certification # 481
Page 16 of 26

e - Duplicate Sample Summary
Original Sample ID: 31500185001-F
Duplicate Sample ID: 158138
QC for Samples: Moot 85001
�- Results by SW-846 6010C
PARAMETER
Lead
Batch Information
Analysis Date: 02/02/2015 14:56
Analysis Date: 02/02/2015 15:02
Matrix: Water
Original (mo/L) Qual Duplicate (ma/L) gtal RPD (%1 RPD CL
ND U ND U 20.00
Analytical Batch: MIP2719
Analytical Method: SW-846 6010C
Instrument: ICP1
Analyst: PSW
Print Date 02/16/2015
Prep Batch: MXX3844
Prep Method. SW-846 3010A
Prep Date/Time: 01/30/2015 08:24
N.C. Certification # 481
Page 17 of 26

Batch Summary
Analytical Method: SM 2540-D
Prep Method: SM 2540-D
Prep Batch: INO3632
Prep Date: 01/29/2015 15:01
Client Sample ID
MB for HBN 63664 [INO/3632]
LCS for HBN 63664 [INO/3632]
OUTFALL(157990DUP)
OUTFALL
Print Date: 02/16/2015
Lab Sample ID Analysis Date
158044 01/29/2015 15:01
158045 01/29/2015 15:01
158046 01/29/2015 15:01
31500185001 01/29/2015 15:01
Analytical Batch
INO3632
INO3632
INO3632
INO3632
Instrument Ana st
BAL10 VML
BAL10 VML
BAL10 VML
BAL10 VML
N C Certification # 481
Page 18 of 26

r Method Blank
Blank ID: MB for HBN 63664 [INO/3632]
Blank Lab ID: 158044
QC for Samples:
31500185001
Results by SM 2540-D
Parameter
Total Suspended Solids
Batch Information
Analytical Batch: IN03632
Analytical Method: SM 2540-D
Instrument: BAL10
Analyst: VML
Print Date: 02/16/2015
Result
ND
ual
Matrix: Water
DL
3.60
LOQ/CL Units
25.0 mg/L
Prep Batch: IN03632
Prep Method: SM 2540-D
Prep Date/Time: 1/29/2015 3.01:33PM
Prep Initial Wt.Nol.: 1 mL
Prep Extract Vol: 1 mL
OF
1
N.C. Certification # 481
Page 19 of 26

Blank Spike Summary
Blank Spike ID: LCS for HBN 63664 [INO/3632]
Blank Spike Lab ID: 158045
Date Analyzed: 01/29/2015 15:01
QC for Samples:
31500185001
Results by SM 2540-D
Parameter
Total Suspended Solids
Batch Information
Analytical Batch: INO3632
Analytical Method: SM 2540-D
Instrument: BAL10
Analyst: VML
Print Date: 02/16/2015
Matrix: Water
Blank Spike (mg/L)
Spike Result Rec
500 496 99
CL
80.0-120
Prep Batch: INO3632
Prep Method: SM 2540-D
Prep Date/Time: 01/29/2015 15:01
Spike Init Wt.Nol.: 1 mL Extract Vol: 1 mL
Dupe Init Wt.Nol.: Extract Vol:
N.C. Certification # 481
Page 20 of 26

Duplicate Sample Summary
Original Sample ID:
Duplicate Sample ID
31500185001-D Analysis Date: 01/29/2015 15:01
: 158046 Analysis Date: 01/29/2015 15:01
Matrix: Water
QC for Samples: 31300185001
Results by SM 2540-D
PARAMETER
Original (mg/L) ual Duplicate (mq/L) ual RPD (%) RPD CL
Total Suspended Solids ND ND 20.00
Batch Information
Analytical Batch: INO3632
Analytical Method: SM 2540-D
Instrument: BAL10
Analyst: VML
Print Date: 02/16/2015
N.C. Certification # 481
Page 21 of 26

e— Batch Summary
Analytical Method: EPA 420.1 (SUB)
Prep Method:
Prep Batch: SUB
Prep Date:
Client Sample ID
Lab Sample ID Analysis Date Analytical Batch Instrument Analyst
OUTFALL 31500185001 02/12/2015 00:00 SUB MDP
Print Date: 02/16/2015
N.C. Certification # 481
Page 22 of 26

ANALYTICAL & CONSULTING
CHEMISTS
Environmental. Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
NCDENR DWQ CERTIIIICATE DIS CERTIFICATE #37729
SGS Environmental Services, Inc.
5500 Business Drive
Wilmington I1C 28405
Attention: Michael Page
Date of Report: Feb 16, 2015
Customer PO #:
Customer ID: 08100111
Report #;. 2015-01198
Project ID: 31500185
Lab ID Sample ID:
15-02699 Site: 31500185001
Test
Method
Collect Date/Time Matrix Sampled by
1/28/2015 12:00 PM Water Client
Results
Date Analyzed
Inorganic Phenols
EPA 420.1
0.004 mg/L 02/12/2015
Comment
Reviewed by:
Report*: 2015401198
Page 23 of 26
Page 1 of 1

SPECIAL INSTRUCTIONS / COMMENTS:
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TURN AROUND TIME: � L1171 i5 EMAIL: `M(V + 565.coM
REPORT LEVEL: (see reverse! 0 Level 1 0 Level 11 0 Level IV INVOICE TO: (CHECK IF SAME)
SPECIAL DELIVERABLES: ❑ State of Origin: COMPANY: CONTACT
❑ EDD: ❑ Other:
ADDRESS:
PHONE:
EMAIL:
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ENVIRONMENTAL SERVICES 5500 Business Drive
SOS NORTH AMERICA INC.
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Page 24 of 26

9Z Jo SZ 06ed
SG$
ANALYTICAL PtaRPCCTIVIR
.0
CHAIN OF CUSTODY
SOS ANALYTICAL PERSPECTIVES
5500 Business Drive
Wilmington, NC 28405
[phone]
w, Ma8 .CON
CLIENT: AIokoNS kc-SoURCE ( QjUA
SOSRefetaneee:
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CONTACT; FkPHONE Nth q1Q (9
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EMAIL
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COMP
ewna
Iowa
INVOICE TO: QUOTE E
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I
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file
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//
MM.
SAMPLE IDENTIFICATION
DATE
TIME
MATRIX
--,)
RCS
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REPORT LEVEL
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REQUESTED TURNAROUND TIME ,
❑ Rush• Standard
Relinquished
Date
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SPECIAL DELIVERABLE& State of Origin' D Trust Fund
0 Do0 0 EDO Other:
Relinquished By: 13)
Date
Time
Received By;
SPECIAL INSTRUCTIONS:
Recelved For Laboratory By:
• i
Date
Tine
CoC Seel: INTACT BROKEN ABSENT
Semple Receipt Temp: C
Shipping Carrier,
Shipping Ticket No:
Notes. •
SGS-000st (e 121
ANALYTICAL PERSPECTIVES IS NOW PART OF SZIS, THE WORLD'S LEADING INSPECTION.
VERIICATION, TESTING AND CERTIFICATION COMPANY
Whip • Relined M Lee
riUow• Retained by OWt

SGS North America Inc.
Sample Receipt Checklist (SRC)
Client: Ammons Resource Group
Work Order No.: 31500185
1. X Shipped Notes:
Hand Delivered
2. X COC Present on Receipt
No COC
Additional Transmittal Forms
3. _ Custody Tape on Container
X No Custody Tape
4. X Samples Intact
Samples Broken / Leaking
5. X Chilled on Receipt Actual Temp.(s) in °C: 4.4 Thermometer ID#: Login 1 D
_Ambient on Receipt
_ Walk-in on Ice; Coming down to temp.
Temperature Blank Present
6. X Sufficient Sample Submitted
Insufficient Sample Submitted
7. Chlorine absent
X HNO3 < 2
HCL<2 14E504,q
yo_Additional Preservatives verified (see notes)
8. X Received Within Holding Time
Not Received Within Holding Time
9. _ No Discrepancies Noted
_ Discrepancies Noted
NCDENR notified of Discrepancies'
10. X No Headspace present in VOC vials
Headspace present in VOC vials >6mm
Comments:
Inspected and Logged in by: Amalie Walker
Date: 1/29/2015
*NCDENR must be notified when collection, holding time or preservation requirements are not met. MI_11.9
Page 26 of 26

ARG
Ammons kesource Group
2040 Peach Grove Lane Zebulon, NC 27597
919-369-5679 [e-mail]
January18, 2015
To Whom It May Concern
Central Files
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: DECEMBER 2014 DISCHARGE MONITORING REPORT
140 WEST FRANKLIN, LLC
140 WEST FRANKLIN STREET
CHAPEL HILL, ORANGE COUNTY, NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
RECEIVED
JAN292015
CENTRAL. FILES
DWR SECTION
Attached is the December 2014 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill, North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Flow rates were recorded and documented and were below the permitted daily maximum limits.
This information is submitted as required by Part II, of Section D. (2.) of its NPDES Permit.
Water samples will be collected and analyzed as required by the permit in the first quarter of
2014.
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely.
Ammons F esour'ce Group
V
Fred Arrim j/
ORC
Enclosures: December 2014 DMR
cc: Mr. Scott Milke, 140 West Franklin, LLC
Mr. Ernest Odei-Larbi, Chapel Hill

EFFLUENT
NPDES PERMIT NO. NCG510532 DISCHARGE NO. 001 MONTH December
FACILITY NAME 140 WEST FRANKLIN
CERTIFIED LABORATORY (1) SGS Environmental Services, Inc CERTIFICATION NO. 481
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons GRADE I CERTIFICATION NO. 992126
CLASS NA COUNTY ORANGE
YEAR 2014
PERSON(S) COLLECTING SAMPLES Fred Ammons
CHECK BOX IF ORC HAS CHANGED 0
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIVISION OF WATER QUALITY L
CHARGE)
1617 MAIL SERVICE CENTER THIS SIGNATURE, I CERTIFY THAT TEAS REPORT IS
RALEIGH, NC 27699-1617 CCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
ORC PHONE [phone]
NO FLOW / DISCHARGE FROM SITE *
/'/8-76
DATE
0
L DATE I
Operator Arrival Time
2400 Clock
Operator Time
On Site
ORC On Site? **
50050
34030
34371
34010
81551
22417
34696
01051
00530
00400
32103
03604
00556
FLO%1
BENZENE
ETHYLBENZENE
ITD
z
Cal
O
E-•
TOTAL XYLENES
METHYL TERT_BUTYL
ETHER (MTBE)
NAPHTHALENE
TOTAL LEAD
TOTAL SUSPENDED
SOLIDS (TSS)
a
1,2 DICHLOROETHANE
(1,2 DCA)
TOTAL PHENOLS
OIL AND GREASE
EFFX 1
INF ❑ I
DAILY
RATE
HRS
HRS
Y/BJN
MGD
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/E,
mg/L
UG/L
' UG/L
1
1000
2
yes
0.000852
2
0.000852
3
0.000852
4
0.000852
5
0.000852
6
0.000852
7
0.000852
8
0.000852
9
0.000852
10
0.000852
11
1300
2
yes
0.000852
12
0.001015
13
0.001015
14
0.00115
_
15
0.001015
16
1200
2
yes
0.001015
17
0.000883
18
0.000883
19
0.000883
20
0.000883
21
0.000883
22
1400
2
yes
0.000883
23
0.001840
24
0.001840
25
0.001840
26
0.001840
27
0.001840
28
0.001840
29
0.001840
30
1400
2
yes
0.001840
31
0.001840
AVERAGE
0.001171
MAXIMUM
MINIMUM
Comp. (C) / Grab (G)
G
Daily Maximum
I
1.19
97
11
670
19
12
25
30
6<pH<9
0.38
300
monitor
DWQ Form MR-1 (11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weeldy averages, if applicable)
All monitoring data and sampling frequencies do NOT meet permit requirements
x
Compliant
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is n ncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Scott Milke, 140 West Franklin, LLC
Permittee (Please print or type)
Sign •ice' ermittee***( ‘5 /5
Date
(Req ed unless submitted electronically)
Permittee Address Phone Number e-mail address Permit Expiration Date
126 West Franklin Street, Chapel Hill NC 27516 [phone] February 28, 2017
Certified Laboratory (2)
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ADDITIONAL CERTIFIED LABORATORIES
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wgs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2