NCG510532_Monitoring Report_20121218

NPDES DOCUMENT SCANNINO COVER !MEET
NPDES Permit:
NCG510532
140 West Franklin
remediation
Document Type:
Permit Issuance
Wasteload Allocation
Authorization to Construct (AtC)
Permit Modification
Complete File - Historical
Monitoring Report
Instream Assessment (67B)
Environmental Assessment (EA)
Permit
History
Document Date:
December 18, 2012
This; document Its printed on reuse paper - igrllore any
content on the relirers4B side

EFFLUENT
NPDES PERMIT NO. NCG510532 DISCHARGE NO. 001 MONTH November YEAR 2012
FACILITY NAME 140 WEST FRANKLIN CLASS NA COUNTY ORANGE
CERTIFIED LABORATORY (1) SGS Environmental Services. Inc CERTIFICATION NO. 481
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons GRADE 1 CERTIFICATION NO. 992126
PERSON(S) COLLEC S�LEAmmons ORC PHONE [phone]
CIIECK BOX IF ORC j�"N% 11 LL{,.��� NO FLOW / UISCIIARCE FROM SITE
Mail ORIGINAL and ONE �( b tQ
ATFN: CENTRAL FILES J i �� iv
DIVISION OF WATER QUALITY (SI NATURE OF OPERATOR IN RESPONSIBLE CHARGE)
1617 MAIL SERVICE CENNTRAL FILES BY THIS SIGNATURE, 1 CERTIFY THAT THIS REPORT IS
RALEIGH. NC 27699-1617 fWQ/B 1CCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
- ( 2-
DATE
DATE
Operator Arrir al Time
2400 Clock
Operator Time
On Site
ORC On Site? **
50050
34030
34371
34010
81551
22417
34696
01051
00530
00400
32103
03604
00556
FLOW
BENZENE
ETHYLBENZENE
TOLUENE
TOTAL XYLENES
METHYL TERT_BUTYL
ETHER (MTBE)
NAPHTHALENE
TOTAL LEAD
TOTAL SUSPENDED
SOLIDS (TSS)
x
a
1,2 DICHLOROETHANE
(1,2 DCA)
TOTAL PHENOLS
OIL AND GREASE
EFF EI
INF ❑
DAILY
RATE
IIRS
IIRS
Y/B/N
MGD
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
mg/L
UG/L
UG/L
I
0.000000
2
0.000000
3
0.000000
4
0.000000
5
1200
2
yes
0.000000
6
0.000000
7
0.000000
8
0.000000
9
0.000000
I0
0.000000
I
0.000000
12
0.000000
13
0.000000
14
0.000000
15
900
2
yes
0.005420
16
0.005420
17
0.005420
I8
0.005420
19
0.005420
20
0.005420
21
1000
2
yes
0.005420
22
0.007259
23
0.007259
24
0.007259
25
0.007259
26
0.007259
27
900
2
yes
0.007259
28
0.007259
29
0.007259
30
0.007259
AVERAGE
0.003442
MAXIMUM
MINIMUM
Comp. (C) / Grab (G)
G
Daily Maximum
1.19
97
1 l
670
19
12
25
30
6<pH<9
0.38
300
monitor
DWQ Form MR-1 (11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
A II monitoring data and sampling frequencies do NOT meet permit requirements
x
Compliant
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Jon Keener, 140
st Franklin, LLC
Permittee (Plea • rint or type)
1, I /
126 West Franklin Street, Chapel Hill NC 27516 [phone]
Permittee Address Phone Number
�o Permittee t''
�
unless submittc electronically)
e-mail address
February 28, 2017
Permit Expiration Date
Certified Laboratory (2)
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ADDITIONAL CERTIFIED LABORATORIES
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wgs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data_
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

ARG
Ammons kesource Group
2040 Peach Grove Lane Zebulon. NC 27597
919-369-5679 [e-mail]
November 18, 2012
To Whom It May Concern
Central Files
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RECEIVED
1JLC 052012
CENTRAL FILES
O WQ/BOG
Subject: OCTOBER 2012 DISCHARGE MONITORING REPORT
140 WEST FRANKLIN, LLC
140 WEST FRANKLIN STREET
CHAPEL HILL, ORANGE COUNTY, NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
Attached is the October 2012 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill. North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Water samples were collected from outfall 001 on October 26, 2012 for the quarterly sampling
event as required by the permit. Samples were sent to SGS Environmental Services, Inc. of
Wilmington, North Carolina for analysis. Analytical results indicate that compounds were below
the permitted daily maximum limits. Flow rates were recorded and documented and were below
the permitted daily maximum limits. This information is submitted as required by Part II, of
Section D. (2.) of its NPDES Permit.
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely,
Ammons Res..rce Group
red - ons
ORC
Enclosures: October 2012 DMR
October 2012 Analytical Report
cc: Mr. Jon Keener, 140 West Franklin, LLC
Mr. Mike Taylor, Chapel Hill

EFFLUENT
NPDES PERMIT NO. NCG510532 DISCHARGE NO. 001 MONTH OCTOBER YEAR 2012
FACILITY NAME 140 WEST FRANKLIN CLASS NA COUNTY ORANGE
CERTIFIED LABORATORY (1) SGS Environmental Services, Inc CERTIFICATION NO. 481,
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons GRADE I CERTIFICATION NO. 992126
PERSON(S) COLLECTING SAMPLES Fred Ammons ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED ❑ NO FLOW / DISCHARGE FROM SITE *
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
(SIGNATURE (31: OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DATE
DATE
Operator Arrive! Time
2400 aock
Operator Time
On Site
ORC On Site? **
50050
34030
34371
34010
81551
22417
34696 101051
00530
00400
32103
03604
00556
FLOW
w
Z
N
Z
w
co
ETHYLBENZENE
TOLUENg
TOTAL XYLENES
METHYL TERT_BUTYL
ETHER (MTBE)
NAPHTHALENE
TOTAL LEAD
TOTAL SUSPENDED
SOLIDS (TSS)
=
¢'
1,2 DICHLOROETHANE
(1,2 DCA)
TOTAL PHENOLS
OIL AND GREASE
EFFah1
INF 0
DAILY
RATE
HRS
HRS
Y/B/N
MGD
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
mg/L
UG/L
UG/L
1
0.087684
2
1500
2
yes
0.087684
_
_
3
0.087684
4
0.087684
_
5
900
2
yes
0.087684
6
0.000000
7
0.000000
8
0.000000
9
0.000000
-
10
0.000000
11
0.000000
12
1200
2.00
yes
0.000000
13
0.000000
14
0.000000
15
0.000000
16
0.000000
17
0.000000
18
0.000000
19
0.00 )000
20
0.000000
_
21
1000
2
yes
0.000000
22
0.000000
23
0.000000
24
0.000000
-
,
25
0.000000
26
1600
2
yes
0.000000
ND
ND
ND
ND
2.78
ND
ND
3.00
7.23
ND
ND
NS
27
0.000000
28
0.000000
29
0.000000
30
0.000000
3I
0.000000
AVERAGE
0.014143
MAXIMUM
MINIMUM
Comp. (C) / Grab (G)
G
Daily Maximum
1
1.19
97
11
670
19
12
25
30
6<pH<9
0.38
300
monitor
DWQ Form MR-1(11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
:\lI monitoring data and sampling frequencies do NO'l' meet permit requirements
Compliant
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Jon Keener, 140 est Franklin, LLC
Permittee ' e print o type)
tgna .f etmittee** Date
(Re' ►red unless submitt electronica
Permittee Address Phone Number
e-mail address
Permit Expiration Date
126 West Franklin Street, Chapel Hill NC 27516 [phone] February 28, 2017
Certified Laboratory (2)
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ADDITIONAL CERTIFIED LABORATORIES
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wgs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the pennittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

AMM Yfl •&u IYRa,rC-Tlvr r.
Laboratory Report of Analysis
Fred Ammons
Ammons Resource Group
2040 Peach Grove Lane
Zebulon, NC 27597
Report Number 31203514
Client Project: CA
Dear Fred Ammons,
Enclosed are the results of the analytical services performed under the referenced project for the received samples
and associated QC as applicable. The samples are certified to meet the requirements of the National Environmental
Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be retained in our files
for a period of five years in the event they are required for future reference. All results are intended to be used in their
entirety and SGS is not responsible for use of less than the complete report. Any samples submitted to our
laboratory will be retained for a maximum of thirty (30) days from the date of this report unless other arrangements
are requested.
If there are any questions about the report or services performed during this project, please call Michael D. Page at
[phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you again
on any additional analytical needs.
Sincerely,
SGS North America Inc.
Digitally signed by: Michael Page
Date: 2012.11.13 13:26:38-05'00'
Michael D. Page
Project Manager
[e-mail]
Print Date 11/t3i2013
Date
N.C. Certification # 481
ANALYTICAL PERSPECTIVES IS NOW PART OF SGS, THE WORLD'S LEADING INSPECTION,
VERIFICATION, TESTING AND CERTIFICATION COMPANY.
5500 9usiness Or. US • 29405 - Wilm ingion,1JC t ♦1 910 350 1933 141 910 3501557 www.a a :to
Page 1 of 23
Memrr Di:xSGS G(Du.rSESSAI

Print Date 11/13!
SGt
w�u►mrae r�s�cc�rvrs
Laboratory Qualifiers
Report Definitions
DL Method, Instrument, or Estimated Detection Limit per Analytical Method
CL Control Limits for the recovery result of a parameter
LOQ Reporting Limit
DF Dilution Factor
RPD Relative Percent Difference
LCS(D) Laboratory Control Spike (Duplicate)
MS(D) Matrix Spike (Duplicate)
MB Method Blank
Qualifier Definitions
Recovery or RPD outside of control limits
B Analyte was detected in the Lab Method Blank at a level above the LOQ
U Undetected (Reported as ND or < DL)
✓ Recovery is below quality control limit. The data has been validated based on a favorable signal-to-noise
and detection limit
A Amount detected is less than the Lower Method Calibration Limit
J Estimated Concentration.
O The recovery of this analyte in the OPR is above the Method QC Limits and the reported concentration in
the sample may be biased high
E Amount detected is greater than the Upper Calibration Limit
S The amount of analyte present has saturated the detector. This situation results in an
underestimation of the affected analyte(s)
Q Indicates the presence of a quantitative interference. This situation may result in an
underestimation of the affected analyte(s)
Indicates the presence of a qualitative interference that could cause a false positive or an
overestimation of the affected analyte(s)
DPE Indicates the presence of a peak in the polychlorinated diphenylether channel that could
cause a false positive or an overestimation of the affected analyte(s)
TIC Tentatively Identified Compound
EMPC Estimated Maximum possible Concentration due to ion ratio failure
ND Not Detected
K Result is estimated due to ion ratio failure in High Resolution PCB Analysis
P RPD > 40% between results of dual columns
D Spike or surrogate was diluted out in order to achieve a parameter result within instrument calibration
range
Samples requiring manual integrations for various congeners and/or standards are marked and dated by the analyst. A
code definition is provided below:
M1 Mis-identified peak
Note Results pages that include a value for "Solids (%)" have been adjusted for moisture content.
2012
N C. Certification # 481
5500 Business Or. US - 28405 • Wilmington,14C t 41 9103501903 I.19103501557 www.sgs tom
Page 2 of 23
ldember of the SSS Grog ISGS SAI

ANALYTICAL. !'FRMaic,TYFG
Sample Summary
Client Sample ID Lab Sample ID Collected Received Matrix
Outfall 001 31203514001 10/26/2012 12:00 10/27/2012 09:40 Water
Print Date 11, 1312012
N C. Certification # 481
1 5500 Business 0r. US • 28405 • Wilmington WC t♦19103501903 f .1910350 1557 www.sgscom
Page 3 of 23
Menthe' vl ae SSS Grua MSS Ski

SG$
r
ANALTI1CAL cure noes
Case Narrative
Outfall 001
SM 4500H+ B - The pH was run outside of the method specified hold time.
Print Dale 1 1 /13/2012 N.0 Certification # 481
1 5500 Business Or. US - 28405 - Wilmington, TJC t *1 910 3501903 f [phone] ww•w.sga tom
Page 4 of 23
Manber 1.1 fie SES Grwp 1%5 SA

Results of Outfall 001
Client Sample ID: Outfall 001
Client Project ID: CA
Lab Sample ID: 31203514001-A
Lab Project ID: 31203514
Results by SW-846 8260B
Parameter
12-Dichloroethane
Benzene
Ethyl Benzene
Naphthalene
Toluene
Xylene (total)
tert-Butyl methyl ether (MTBE)
Surrogates
1,2-Dichloroethane-d4
4-Bromofluorobenzene
Toluene d8
Batch Information
Result
ND
ND
ND
ND
ND
ND
2.78
94.0
102
104
Analytical Batch: VMS2693
Analytical Method: SW-846 8260B
Instrument: MSD3
Analyst: BWS
Print Date 11/13/2012
Qual DL
U 0.139
U 0.156
U 0.186
U 0.260
U 0.180
U 0.602
0.195
Collection Date: 10/26/2012 12:00
Received Date: 10/27/2012 09:40
Matrix: Water
i
LOQ/CL Units DF Date Analyzed
1.00 ug/L 1 10/31/2012 16:31
1.00 ug/L 1 10/31/2012 16:31
1.00 ug/L 1 10/31/2012 16:31
1.00 ug/L 1 10/31/2012 16:31
1.00 ug/L 1 10/31/2012 16:31
2.00 ug/L 1 10/31/2012 16:31
1.00 ug/L 1 10/31/2012 16:31
64.0-140 % 1 10/31/2012 16:31
85.0-115 % 1 10/31/2012 16:31
82.0-117 % 1 10/31/2012 16:31
Prep Batch. VXX4249
Prep Method: SW-846 5030B
Prep Date/Time 10/31/2012 08:52
Prep Initial Wt.Nol.: 40 mL
Prep Extract Vol: 40 mL
N C Certification # 481
55CC Business Ur. US • 28405. Wilmington, WC t+1 9103501903 ([phone] areetv.s9s axn
Page 5 of 23
Membr vl The SE S G.aw 1SGS SA,

/— Results of Outfall 001
Client Sample ID: Outfall 001
Client Project ID: CA
Lab Sample ID: 31203514001-F
Lab Project ID: 31203514
%*•- Results by SW-846 6010C
Parameter
Lead
Batch Information
Result
ND
Analytical Batch: MIP1805
Analytical Method: SW-846 6010C
Instrument: ICP1
Analyst: PSW
Print Date: 11 /1312012
Collection Date: 10/26/2012 12:00
Received Date: 10/27/2012 09:40
Matrix: Water
Qual DL LOQ/CL Units DF
U 0.00541 0.0100 mg/L 1
Prep Batch: MXX2443
Prep Method: SW-846 3010A
Prep Date/Time. 10131/2012 08:25
Prep Initial Wt.Nol.: 50 mL
Prep Extract Vol: 50 mL
Date Analyzed
11/1/2012 17:58
N.0 Certification # 481
55CE8uincssDr. US 26405 Wilmington, VC t+19t035C1903 P.19103501557 wwnv.sgscom
Page 6 of 23
Membe- al air SGS Gram rSGS Shc

SG8ANALYTICAL P/•ergy-./VR1
Results of Outfall 001
Client Sample ID: Outfall 001
Client Project ID: CA
Lab Sample ID: 31203514001-E
Lab Project ID: 31203514
Results by SM 2540-D
Parameter
Total Suspended Solids
Batch Information
Analytical Batch. IN02110
Analytical Method. SM 2540-D
Instrument: BAL10
Analyst: MAH
Print Date 11113r2012
Result
3.00
Qual DL
1.25
Collection Date: 10/26/2012 12:00
Received Date: 10/27/2012 09:40
Matrix: Water
LOQ/CL Units DF
1.25 mg/L .5
Prep Batch: INO2110
Prep Method: SM 2540-D
Prep Date/Time. 1110112012 15:00
Prep Initial Wt.Nol.: 1 mL
Prep Extract Vol: 1 mL
Date Analyzed
11 /1 /2012 15:00
N t; Cert f cation # 481
5500 Business Or U5 - 26405 - WilmrngiOn ?iC t «1 9103M 1903 I [phone] www.sgs coin
Page 7 of 23
Rkmbr, o+ enr SGS U.vw lSGS Skt

SG�'
ANAL7TICA. t'6F* IOCTIVFF
- Results of Outfall 001
Client Sample ID: Outfall 001
Client Project ID: CA
Lab Sample ID: 31203514001-H
Lab Project ID: 31203514
%"- Results by SM 4500-H+ B pH
Parameter
pH
pH at Temperature
Batch Information
Result
7.233
21.9
Analytical Batch: INO2091
Analytical Method: SM 4500-H+ B pH
Instrument: ATIT1
Analyst: PSW
Pnnt Date 11 13,2012
Qual DL
0.0100
Collection Date: 10/26/2012 12:00
Received Date: 10/27/2012 09:40
Matrix: Water
LOQ/CL Units
0.0100 S.U.
C
DF
1
1
Prep Batch: INO2091
Prep Method: SM 4500-H+ B pH
Prep Date/Time: 10/30/2012 12:30
Prep Initial Wt.Nol.: 1 mL
Prep Extract Vol: 1 mL
Date Analyzed
10/30/2012 12:30
10/30/2012 12:30
N.C. Certification # 481
5500 Business Dr. US • 28405 • Wilmington. NC t .1 910 3501903 141 910 3501557 ww w.sgs corn
Page 8 of 23
Menbr: vl the SGS Group fSGS sAl

AEI.. IlT:A:
Results of Outfall 001
Client Sample ID: Outfall 001
Client Project ID: CA
Lab Sample ID: 31203514001-G
Lab Project ID: 31203514
Collection Date: 10/26/2012 12:00
Received Date: 10/27/2012 09:40
Matrix: Water
Results by EPA 420.4 (SUB)
Parameter Result Qual DL LOQ/CL Units DF Date Analyzed
Phenol ND U 10.0 ug/L 1 11/9/2012 13:20
Laboratory: Microbac
Analytical Date/Time: 11/09/2012 13:20
Print Date: 11 /13/2012
Prep Method.
Prep Date/Time:
N.C. Certification # 481
5500 Business Dr. US • 28405 • Wilmington, NC t 41 910 3501903 1 [phone] griirw.sgs tom
Page 9 of 23
Membet Di the SES GrewISGSSdI

p Batch Summary
Analytical Method: SW-846 8260B
Client Sample ID
LCS for HBN 31070 [VXX/4249]
LCSD for HBN 31070 [VXX/4249]
MB for HBN 31070 [VXX/4249]
Outfall 001
137-Comp(97095MS)
137-Comp(97095MSD)
Print Date ' 1312012
Prep Method: SW-846 5030B
Prep Batch: VXX4249
Prep Date: 10/31/2012 08:49
Lab Sample ID Analysis Date
97415 10/31/2012 09:57
97416 10/31/2012 10:21
97417 10/31/2012 11:33
31203514001 10/31/2012 16:31
97516 10/31/2012 20:07
97517 10/31/2012 20:31
Analytical Batch
VMS2693
VMS2693
VMS2693
VMS2693
VMS2693
VMS2693
Instrument Ana st
MSD3 BWS
MSD3 BWS
MSD3 BWS
MSD3 BWS
MSD3 BWS
MSD3 BWS
N C Certification # 481
5509 Business tar. US • 28405 • Wilrr mgton, )Jl; t [phone] I [phone] www.sgs corn
j membr= of fnt BBS Grow ISES SAI
Page 10 of 23

SG$
Method Blank
•
ANAI.NflCAI. tossow 6CRVEi
Blank ID: MB for HBN 31070 [VXX/4249]
Blank Lab ID: 97417
QC for Samples:
31203514001
Matrix: Water
Results by SW-846 8260B -
Parameter Result Qual DL LOQ/CL Units DF
tert-Butyl methyl ether (MTBE) ND U 0.195 1.00 ug/L 1
Benzene ND U 0.156 1.00 ug/L 1
1,2-Dichloroethane ND U 0.139 1.00 ug/L 1
Toluene ND U 0.180 1.00 ug/L 1
Ethyl Benzene ND U 0.186 1.00 ug/L 1
Xylene (total) ND U 0.602 2.00 ug/L 1
Naphthalene ND U 0.260 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 95.0 64.0-140 % 1
Toluene d8 103 82.0-117 % 1
4-Bromofluorobenzene 101 85.0-115 % 1
Batch Information
naiyu;;at Batch: VMS2693
Analytical Method: SW-846 8260B
Instrument: MSD3
Analyst: BWS
Prep Batch: VXX4249
Prep Method: SW-846 5030B
Prep DatefTime: 10/31/2012 8:49:16AM
Prep Initial Wt.Nol.: 40 mL
Prep Extract Vol 40 mL
Print Date. 1111.312012 N.C. Certification # 481
5500 Business or. US • 28405 - Wilmington,14C t [phone] [phone] wwwv.ags.com
Member of the SUS Group IS1 SSAg
Page 11 of 23

SG$ANA&JflCAL PWRf a[C1TVIM
Blank Spike Summary
Blank Spike ID: LCS for HBN 31070 (VXX/4249]
Blank Spike Lab ID: 97415
Date Analyzed: 10/31/2012 09:57
QC for Samples: 31203514001
Results by SW-846 8260B
Parameter
Th
Spike Duplicate ID: LCSD for HBN 31070 [VXX/4249]
Spike Duplicate Lab ID: 97416
Date Analyzed: 10/31/2012 10:21
Matrix: Water
tert-Butyl methyl ether (MTBE)
Benzene
1,2-Dichloroethane
Toluene
Ethyl Benzene
Naphthalene
Surrogates
1,2-Dichloroethane-d4
Toluene d8
4-Bromofluorobenzene
Batch Information
Blank Spike (ug/L) Spike Duplicate (ug/L)
Spike Result Rec % Spike Result Rec (%) CL RPD (%) RPD CL
5.00 4.63 93 5.00 5.06 101 47.0-142 8.9 30.00
5.00 4.54 91 5.00 5.32 106 76.0-124 16 30.00
5.00 4.57 91 5.00 4.95 99 76.0-119 8.0 30.00
5.00 4 74 95 5.00 5.36 107 75.0-123 12 30.00
5.00 4.30 86 5.00 4.97 99 76.0-123 14 30.00
5.00 4.33 87 5.00 4.77 95 67.0-122 9.7 30.00
95
103
101
94 64.0-140
103 82.0-117
102 85.0-115
Analytical Batch. VMS2693
Analytical Method: SW-846 8260E
Instrument: MSD3
Analyst: BWS
Prep Batch: VXX4249
Prep Method: SW-846 5030E
Prep Date/Time: 10/31/2012 08:49
Spike Init Wt.Nol.: 40 mL Extract Vol: 40 mL
Dupe Init WI/Vol.: 40 mL Extract Vol: 40 mL
Print Date 11/13/2012
N.C. Certification # 481
5500 Business Or. US • 28405 • Wilmington, NC t «1910 350191)3 f [phone] w ww.sgs cam
Page 12 of 23
Membrr ul the SGS Group ISGS Sal

SGS1
ANKYnGi. r. ,cn,Fs
r Batch Summary
Analytical Method: SW-846 6010C
Client Sample ID
MB for HBN 31047 [MXX/2443]
LCS for HBN 31047 [MXX/2443]
LCSD for HBN 31047 [MXX/2443]
Outfall 001
Outfall 001(97028MS)
Outfall 001(97028MSD)
MW-151(97207DUP)
Print Date 11032012
Prep Method: SW-846 3010A
Prep Batch: MXX2443
Prep Date: 10/31/2012 08:25
Lab Sample ID Analysis Date
97347 11/01/2012 17:44
97348 11/01/2012 17:48
97349 11/01/2012 17:53
31203514001 11/01/2012 17:58
97350 11/01/2012 18:12
97351 11/01/2012 18:16
97352 11/01/2012 18:40
Analytical Batch Instrument Analyst
MIP1805 ICP1 PSW
MIP1805 ICP1 PSW
MIP1805 ICP1 PSW
MIP1805 ICP1 PSW
MIP1805 ICP1 PSW
MIP1805 ICP1 PSW
MIP1805 ICP1 PSW
N.0 Certification # 481
5500 Business Or. US - 28405 • Wilmington, NC t 41 910 3501903 1 ♦1910 3501557 w+A•w.sga cum
Page 13 of 23
%tenter of the SGS Grouo ISO MI

SG gr_
Method Blank
Blank ID: MB for HBN 31047 [MXX/2443]
Blank Lab ID: 97347
QC for Samples:
31203514001
Results by SW-846 6010C
Parameter
Lead
Batch Information
Result
ND
Analytical Batch: MIP1805
Analytical Method: SW-846 6010C
Instrument: ICP1
Analyst: PSW
Print Date: 11/13'2012'
Qual
U
DL
0.00541
Matrix: Water
LOQ/CL Units
0.0100 mg/L
Prep Batch: MXX2443
Prep Method: SW-846 3010A
Prep Date/Time: 10/31/2012 8:25:38AM
Prep Initial Wt.Nol.: 50 mL
Prep Extract Vol: 50 mL
DF
1
N.C. Certification # 481
5500 Business 0r. US.28405 • Wilmington, NC t +i 9103501903 1 [phone] www.sgs com
Page 14 of 23
Umbel Di rrr SGS Grow (SOU,

1111
SG SI Anusne-A1. PFR*PECIIVF%
Blank Spike Summary
Blank Spike ID: LCS for HBN 31047 [MXX/2443]
Blank Spike Lab ID: 97348
Date Analyzed: 11/01/2012 17:48
QC for Samples: 31203514001
Results by SW-846 6010C
Spike Duplicate ID: LCSD for HBN 31047 [MXX/2443]
Spike Duplicate Lab ID: 97349
Date Analyzed: 11/01/2012 17:53
Matrix: Water
Blank Spike (mg/L) Spike Duplicate (mg/L)
Parameter Spike Result Rec (%2 Spike Result Rec (%) CL RPD (%) RPD CL
Lead 0.400 0.393 98 0.400 0.387 97 80.0-120 1.5 20.00
Batch Information
Analytical Batch. MIP1805
Analytical Method: SW-846 6010C
Instrument: ICP1
Analyst: PSW
Print Date: 1111312012
Prep Batch: MXX2443
Prep Method: SW-846 3010A
Prep Date/Time: 10131/2012 08:25
Spike Init Wt.Nol.: 50 mL Extract Vol: 50 mL
Dupe Init Wt.Nol.: 50 mL Extract Vol: 50 mL
N.C. Certification 1481
5500 Business Dr. US - 28405 •Wilmington, NC t r i 910 3501903 f 41910 3501557 www.sgs. com
Page 15 of 23
Memtm o1 the SUS Grow (SUS S41

A4,1,1_ w1 1•r Frrci:rnvrA
Matrix Spike Summary
Original Sample ID: 31203514001 (Outfall 001)
MS Sample ID: 97350
MSD Sample ID: 97351
QC for Samples: 31203514001
Analysis Date: 11/01/2012 17:58
Analysis Date: 11/01/2012 18:12
Analysis Date: 11/01/2012 18:16
Matrix: Water
Results by SW-846 6010C J
Matrix Spike (mg/L) Spike Duplicate (mg/L)
Parameter Sample Spike :esuit Rec (%) Spike Res(„: Rec (%) CL RPD (%) RPD CL
Lead ND 0.400 0.351 88 0.400 0.357 89 75.0-125 1.7 20.00
Batch Information
Analytical Batch: MIP1805
Analytical Method: SW-846 6010C
Instrument: ICP1
Analyst: PSW
Print Date 11/13/2012i
Prep Batch: MXX2443
Prep Method: SW-846 3010A
Prep Date/Time. 10/31/2012 08:25
MS Init Wt.Nol.: 50 mL Extract Vol.: 50 mL
MSD snit Wt.Nol.: 50 mL Extract Vol.: 50 mL
N.C. Certification # 481
5500 Business Or. US • 28405 • Wilmington, ? IC t [phone] [phone] www.sgs cum
Page 16 of 23
Member uI tfir SGS GImjy ISGS SAI

SGALEF=--
wmurncm.Poormarrvir,
•
Batch Summary
Analytical Method: SM 2540-D
Client Sample ID
MB for HBN 31150 [INO/2110]
LCS for HBN 31150 (INO/21101
1245 Edwards Tank...(96887DUP)
Outfall 001
Print Date 11/13/2012
Prep Method: SM 2540-D
Prep Batch: INO2110
Prep Date: 11/01/2012 15:00
Lab Sample ID Analysis Date
97674 11/01/2012 15:00
97675 11/01/2012 15:00
97676 11/01/2012 15:00
31203514001 11/01/2012 15:00
Analytical Batch Instrument Analyst
INO2110 BAL10 MAH
INO2110 BAL10 MAH
INO2110 BAL10 MAH
INO2110 BAL10 MAH
N C Certification k 481
550081Sine-SSOr US 28405•Wilmington. HC t [phone]+19103501557 wAsv.sgs=an
laembr al the SGS Gfvu, ISGS Sdi
l
Page 17 of 23

SG$
,r- Method Blank
r�-
Blank ID: MB for HBN 31150 [INO/2110]
Blank Lab ID: 97674
QC for Samples:
31203514001
Results by SM 2540-D
Parameter
Total Suspended Solids
Batch Information
Result Qual
ND U
DL
2.50
Matrix: Water
LOQ/CL Units
2.50 mgl&
DF
1
Analytical Batch: IN02110
Analytical Method: SM 2540-D
Instrument: BAL10
Analyst: MAH
Prep Batch. IN02110
Prep Method: SM 2540-D
Prep Date/Time: 11/1/2012 3:00:02PM
Prep Initial Wt.Nol.: 1 mL
Prep Extract Vol: 1 mL
Pant Date 11/13'2012 N C Certitcal:on S 481
5500 Business Dr. US • 28405 • Wilmington, NC t [phone] 1.1910 3501557 www.sgs tom
Member of the SES Gravy fSES Sit
Page 18 of 23

SG$
Blank Spike Summary
Blank Spike ID: LCS for HBN 31150 [INO/2110J
Blank Spike Lab ID: 97675
Date Analyzed: 11 /01 /2012 15:00
QC for Samples: 31203514001
• Results by SM 2540-D
Parameter
Total Suspended Solids
Batch Information
Analytical Batch. INO2110
Analytical Method: SM 2540-D
Instrument: BAL10
Analyst: MAH
Print Date. tin 3/201
Blank Spike (mg/L)
Spike Result Rec (%)
500 436 87
Matrix: Water
CL
80.0-120
Prep Batch: IN02110
Prep Method: SM 2540-D
Prep Date/Time: 11 /01/2012 15:00
Spike Init Wt.Nol.: 1 mL Extract Vol: 1 mL
Dupe !nit Wt.Nol.: Extract Vol:
N.C. Certification # 481
5500 Business Dr. US - 28405 • Wilmington, NC t [phone] I .1910 3501557 www.sgs corn
Page 19 of 23
Memo a t sss Grwg4SGS sar

Microbac
SGS - Wilmington
Mr. Michael Page
5500 Business Drive
Wilmington NC, 28405
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: Water Samples
Date Reported: November 09, 2012
Date Received: October 31, 2012
Date Sampled: October 26, 2012
Sampled By: M. Page
31203514001
1210728-01
Analyze
Result
MDL Units Analyzed
Analyzed By
Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Phenolics. Total Recoverable <10
State Certifications:
NCDNR #11
NCDOH #37714
USDA #3787
5.00
.tgIL
11/9/12 13:20
GOEHL
EPA 420.4 Rev 1.0
Respectfully Submitted
�.C.2IL.r1^ fJcViLG.�`�tc�
Jeanne Overstreet, Project Manager
Page 20 of 23
Page 1 of 2

SGS
1
CLIENT:565.-,Er
CONTACT /G 4'?
SGS Environmental Services Inc.
CHAIN OF CUSTODY RECORD
/(4(cr ba C
Locations Nationwide
• Alaska • Maryla
• New Jersey • New
• North Carolina • Ohio
• West Virginia
www.us.sgs.com
*1210728*
yl�ll
PHONE NO: Cfe)�
SGS Reference #:
ao3$/y
Page/ofj
PROJECT. / Z, c`�"/ (/ SITEIPWSID#,:
REPORTS TO:
/41,c-4 W-
/
INVOICE TO:
/� EMAIL:
QUOTE #:
P.O. #:
LAB NO.
SAMPLE IDENTIFICATION
DATE
TIME
MATRIX/
MATRIX
CODE
0
T
A
I
N
E
R
S
SAMPLE
TYPE
COMP
GRAB
MI.
Mufti
Incremental
Samples
Peatiffathiedi
Used
REMARKS/
LOC ID
3�22357ra5l
lv�zite.
/ co
w
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Collected/Relinquished By:(1)
i
R •uls
R =fqulsh By:( )
ed 3
Date
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Date
Time
1325-
Time
3:33
Date
Time
R : • = Ived By:
R lved By:
CIL9fulSA _AAA'
ecelved By:
DOD Project? YES NO
Cooler ID
Special Deliverable Requirements:
Requested Tumaround Time and -or Special Instructions:
sr) S�, >fr LeveJ7JS
Samples Received Cold? YES NO
Chain of Custody Seal: (Circle)
Relinquished By: (4)
Date
Time
Received For Laboratory By:
Cooler TB
Temperature°C: 1 •D •
0 200 W. Potter Drive Anchorage, AK 99518 Tel: [phone] Fax: [phone]
0 660 Business Drive Wilmington, NC 28408 Tel: [phone] Fax: [phone]
I1tto:/Avww.sgs.eom/terns and conditlons.ht
INTACT BROKEN ABSENT
I Page 2 of 2
White - Retained by
Pink - Retained by Client

SGS1
CHAIN OF CUSTODY RECORD
SGS North America Inc.
Locations Nationwide
• Alaska • Maryland
• New Jersey • New York
• North Carolina • Ohio
www.ua.egs.00m
107227
,q/I('fo/li 0.0a tc � eget/ACLIENT:SGS
Reference:3/2-05.5
CONTACT: 1PHONE NO:( gip 365 . S?79Pressva
ko
��
PAGE OF/
£4 ,7
dvas
-
PROJECT: /%'Ck'JS 7 SITEIPWSID# :
N o
sPELE
Used
i
•
Analysis
REPORT8 TO: A
)
N
0NO.:(
T
C.
COMP
Requited
INVOICE TO:0N mz.-- PQOUOTENUtf:
.. MBER:
2
A
N
E
GRAB
`
` /
�+ t7 �`
LAB NO.
SAMPLE IDENTIFICATION
DATE
TIME
.
MATRIX
R S
,OikQ
REMARKS
0u7 -Pf L OO/
/61-26-/2
AM,
//Z0
7
6
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417-4.0•1
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_
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Collecte. e
quished By:(1
Time
Received By: tie/Shipping
Carrier:
Samples Received Cold? (Gird ES
/
fDatee
' 2-
fAV
Shipping Ticket No:
Temperature°C: e
Relinqul: ed By: (2)
Date
Time
Received By:
Special Deliverable Requirements:
Chain of Custody Seal: (Circle)
INTACT BROKEN 1p
Relinquished By: (3)
—
Date
lime
Received By:
Special Instructions:
Relinquished By: (4)
Da
�t�/� la
Time
0�
Received By:
Requested Tumaround Time:
■ RUSH YrD
Date Needed
C
0
Q
N
W
O 200 W. Potter Drive Anchorage, AK 99518 Tel: [phone] Fax: [phone]
O 5500 Business Drive Wilmington, NC 28405 Tel: [phone] Fax: [phone]
White - Retained by Lab
Pink - Retained by Client

SGS North America Inc.
Sample Receipt Checklist (SRC)
Client Ammons Resource Group
1. XShipped
Hand Delivered
2. X COC Present on Receipt
No COC
Additional Transmittal Forms
3. _ Custody Tape on Container
X' No Custody Tape
4. X Samples Intact
Samples Broken / Leaking
Work Order No.: 31203514
Notes:
5. X Chilled on Receipt Actual Temp.(s) in °C: 4.7
- Walk-in on Ice; Coming down to temp.
- Received Outside of Temperature Specifications
Ambient on Receipt
6. X Sufficient Sample Submitted
Insufficient Sample Submitted
7. Chlorine absent
X HNO3 < 2
HCL < 2
X Additional Preservatives verified (see notes)
8. X Received Within Holding Time
Not Received Within Holding Time
9. X No Discrepancies Noted
Discrepancies Noted
NCDENR notified of Discrepancies*
10. No Headspace present in VOC vials
Headspace present in VOC vials >6mm
Comments:
H2SO4
Inspected and Logged in by: JJ
Date: Mon-10/29/12 00:00
`NCDENR must be notified when collection, holding time or preservation requirements are not met Ml_11.6
Page 23 of 23

ARG
2040 Peach Grove Lane Zebulon. NC 27597
919-369-5679 fredammons @att_ne:
October 16. 201=. 73
rn
To Whom It May Concern am
Central Files
North Carolina Division of Water Quality f ..n
1617 Mail Service Center G ,
Raleigh. North Carolina 27699-161- Or'
iin.) rE
cn
Subject: SEPTEMBER 2012 DISCHARGE MONITORING REPORT
140 WEST FRANKLIN, LLC
1,40 WEST FRANKLIN STREET
CHAPEL HILL, ORANGE COUNTY, NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
Attached is the September 2012 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill. North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Water samples will be collected from outfall 001 during October 2012 for the quarterly sampling
event as reauired by the permit. Flow rates were recorded and documented and were below the
permitted daily maximum limits. This information is submitted as required by Part II, of Section
D. (2.1 of its NPDES Permit
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely,
Ammons R9source Group
•
red
ORC
ns
Enclosures: September 2012 DMR
cc: Mr. Jon Keener. 140 West Franklin, LLC
Mr. Mike Taylor, Chapel Hill

EFFLUENT
NPDES PERMIT NO. NCG510532 DISCHARGE NO. 001 MONTH SEPT
FACILITY NAME 140 WEST FRANKLIN
CLASS NA COUNTY ORANGE
YEAR 2012
CERTIFIED LABORATORY (11 SGS Environmental Services. Inc CERTIFICATION NO. 481
(list additional laboratories on the backside/page 2 of this form
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons
PERSON(S) COLLECTING SAMPLES Fred Ammons
CHECK BOX IF ORC HAS CHANGED 0
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
�TIJ ERATOR 1 RESPONSIBLE CHARGE)
GRADE I CERTIFICATION NO. 992126
ORC PHONE [phone]
NO FLOW / DISCHARGE FROM SITE *
/0- J40 - /&
DATE
lir
THIS SIGNA I CERTIFY THAT THIS REPORT ISCCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
_._.
rao
0
Operator Arrival Time
2400 Clock
Operator Time
On Site
ORC On Site? **
50050 l
34030 1
34371 1
34010 '
81551 1
22417 1
34696 1
01051 1
00530 1
00400
32103 103804 100558 I
FLOW
BENZENE
ETHYLBENZENE
z
cal
0
F
TOTAL XYLENES
METHYL TERT BUTYL
ETHER (MTBE)
NAPHTHALENE
TOTAL LEAD
TOTAL SUSPENDED
SOLIDS (TSS)
1,2 DICHLOROETHANE
(1,2 DCA)
TOTAL PHENOLS
OIL AND GREASE
EFF 13
INF Dcaa
DAILY
RATE
HRS
HRS
Y/B/N
MGD
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
VGA.
a1L
UG/L
UGIL
1
0.000000
2
0.000000
3
0.000000
4
0.000000
,
5
0.000000
_
.
61400
2
yes
0.000000
,
7
0.000000
_
8
0.000000
9
0.000000
10
0.000000
11
0.000000
12
1100
2.00
yes
0.000000
13
0.000000
14
0.000000
15
0.000000
.
16
0.000000
,
_
_
17
0.000000
18
1200
2.00
yes
0.000000
_
19
0.000000
20
0.000000
21
0.000000
22
0.000000
23
0.000000
24
0.000000
25
I200
2
yes
0.000000
,
26
0.000000
27
0.000000
28
0.000000
_
29
0.000000
30
0.000000
AVERAGE
0.000000
MAXIMUM
MINIMUM
Comp. (C) / Grab (G)
G
Daily Maximum
1.19
97
11
670
19
12
25
30
6<pH<9
038
300
monitor
DWQ Form MR-1(11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
All monitoring data and sampling frequencies do NOT meet permit requirements
x
1
Compliant
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance mai pores€__
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
perms :tee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions -being taken and a time -table for
improvements to be made as required by Part H.E.6 of the NPDES permit.
;ertuv, under penaity or law, that this document and all attachments were prepared under my direction or supervision
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and better, true, accurate. and
complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations.'"
Jon Keener. 140 West Franklin. LLC
Perrnitt (Please p 'nt or type)
Permittee*** Date
(Required unless submitted electronically )
126 West Franklin Street. Chapel Hill NC 27516 [phone]
Permittee Address Phone Number e-mail address Permit Expiration Date
February 28, 2017
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Certification Nu.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) _ Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/was and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result. there are no data to
enteredifor all of the parameters on the DMR for the entire monitoring period.
x* ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(bX2)(D,.
Page 2

ARG
Ammons Resource Group
2040 Peach Grove Lane Zebulon, NC 27597
919-369-5679 [e-mail]
September 23, 2012
To Whom it May Concern
Central Files
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: AUGUST 2012 DISCHARGE MONITORING REPORT
140 WEST FRANKLIN, LLC
140 WEST FRANKLIN STREET
CHAPEL HILL, ORANGE COUNTY, NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
VC,:vD
OCT 052012
CENTRAL FILEc
DWQ(BQG
Attached is the August 2012 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill, North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Water samples will be collected from outfall 001 during October 2012 for the quarterly sampling
event as required by the permit. Flow rates were recorded and documented and were below the
permitted daily maximum limits. This information is submitted as required by Part II, of Section
D. (2.) of its NPDES Permit.
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely,
Ammons Resoprce Group
Enclosures: August 2012 DMR
cc: Mr. Jon Keener, 140 West Franklin, LLC
Mr. Mike Taylor, Town of Chapel Hill

r,
EFFLUENT
NPDES PERMIT NO. NCG510532 DISCHARGE NO. 001 MONTH August YEAR 2012
FACILITY NAME 140 WEST FRANKLIN CLASS NA COUNTY ORANGE
CERTIFIED LABORATORY (1) SGS Environmental Services, Inc CERTIFICATION NO. 481
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons GRADE I CERTIFICATION NO. 992126
PERSON(S) COLLECTING SAMPLES Fred Ammons ORC PHONE [phone]
CHECK BOX IF OR43 HAS CHANGED ❑
Mail ORIGINAL and OI TIo2012
ATTN: CENTRAL FILES
DIVISION OF WATER Q1Y AI,ITY
1617 MAIL SERVICE CE114TER
RALEIGH, NC 27699-1617
NO FLOW / DISCHARGE FROM SITE *
F 25- /z
(S A '. O • ' ERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DATE
0
W
F
A
Operator Arrival Time
2400 pock
Operator Time
On Site
ORC On Site? **
50050
34030
34371
34010
81551
22417
34696
01051
00530
00400
32103
03604
00556
FLOW
BENZENE
ETHYLBENZENE
TOLUENE
TOTAL XYLENES
METHYL TERT_BUTYL
ETHER (MTBE)
NAPHTHALENE
TOTAL LEAD
TOTAL SUSPENDED
SOLIDS (TSS)
7-1a
1,2 DICHLOROETHANE
(1,2 DCA)
TOTAL PHENOLS
OIL AND GREASE
EFFNII
INF ❑
j
a WQ
a
HRS
HRS
Y/B/N
MGD
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
mg/L
UG/L
UG/L
1
0.016290
2
0.016290
3
0.016290
4
0.016290
5
0.016290
6
700
2
yes
0.016290
7
0.019080
8
0.019080
9
0.019080
10
0.019080
11
0.019080
12
0.019080
13
0.019080
14
1600
2
yes
0.019080
15
0.001 141
16
0.001141
17
0.001141
18
0.001141
19
0.001141
20
0.001141
21
1000
2
yes
0.001141
22
0.000000
23
0.000000
24
0.000000
25
0.000000
26
0.000000
27
1700
2
yes
0.000000
28
0.000000
29
0.000000
30
0.000000
31
1000
2
yes
0.000000
AVERAGE
0.008334
MAXIMUM
MINIMUM
Comp. (C) /Grab (G)
G
Daily Maximum
1.19
97
11
670
19
12
25
30
6<pH<9
0.38
300
monitor
DWQ Form MR- (1 I/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
All monitoring data and sampling frequencies do NOT meet permit requirements
x
Compliant
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becores aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Jon Keener, 140 West Franklin, LLC
Perm - {Please pri or type)
ee*** Date
submitted electronically)
126 West Franklin Street, Chapel Hill NC 27516 [phone] February 28, 2017
Permittee Address Phone Number
e-mail address
Permit Expiration Date
Certified Laboratory (2)
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
l)DITIONAL CERTIFIED LABORATORIES
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

ARG
Ammons Resource Group
2040 Peach Grove Lane Zebulon, NC 27597
919-369-5679 fredammons©att. net
August 20, 2012
To Whom It May Concern
Central Files
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: JULY 2012 DISCHARGE MONITORING REPORT
140 WEST FRANKLIN, LLC
140 WEST FRANKLIN ST
CHAPEL HILL, ORANGgICOUNTY NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
Attached is the July 2012 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill, North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Water samples were collected from outfall 001 on July 1, 2012 for the quarterly sampling event
as required by the permit. Samples were sent to SGS Environmental Services, Inc. of
Wilmington, North Carolina for analysis. Analytical results indicate that compounds were below
the permitted daily maximum limits. Flow rates were recorded and documented and were below
the permitted daily maximum limits. This information is submitted as required by Part II, of
Section D. (2.) of its NPDES Permit.
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely,
Ammons Resource Group
red ons
ORC
Enclosures: July 2012 DMR
July 2012 Analytical Reports
cc: Mr. Jon Keener, 140 West Franklin, LLC
Mr. Mike Taylor, Chapel Hill
AUG 302012
WATER QUALITY SECTION
INFORMATION PROCESSING UNIT

EFFLUENT
NPDES PERMIT NO. NCG510532 DISCHARGE NO. 001 MONTH JULY YEAR 2012
FACILITY NAME 140 WEST FRANKLIN CLASS NA COUNTY ORANGE
CERTIFIED LABORATORY (1) SGS Environmental Services. Inc CERTIFICATION NO. 481
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons GRADE I CERTIFICATION NO. 992126
PERSON(S) COLLECTING SAMPLES Fred Ammons ORC PHONE [phone]
NO FLOW / DISCHARGE FROM SITE *
CHECK BOX IF ORC HAS CHANGED ❑
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIVISION OF WATER QUAL1TY [SI OPERATOR [N RESPONSIBLE CHARGE)
1617 MAIL SERVICE CENTER Y THIS SIGNATURE, 1 CERTIFY THAT THIS REPORT IS
RALEIGH, NC 27699-1617 ICCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
g-2o- /Z
DATE
DATE
Operator Arrival Time
2400 aock
Operator Time
On Site
ORC On Site? **
50050
34030
34371
34010
81551
22417
34696
01051
00530 100400
32103
03604
00556
FLOW
BENZENE
ETHYLBENZENE
TOLUEN;
TOTAL XYLENES
METHYL TERT_BUTYL
ETHER (MTBE)
NAPHTHALENE
TOTAL LEAD
TOTAL SUSPENDED
SOLIDS (TSS)
a
1,2 DICHLOROETHANE
(1,2 DCA)
TOTAL PHENOLS
OIL AND GREASE
EFFX 1
INF 0
DAILY
RATE
HES
HRS
Y/B/N
MGD
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
mg&
UG/L
UG/L
1
1100
2
yes
0.002150
ND
ND
ND
ND
2.94
ND
0.0071
4
8.75
ND
0.0078
NS
2
0.002150
3
0.002150
4
0.002150
5
0.002150
6
1000
2
yes
0.002150
7
0.011450
8
0.011450
9
0.00450
10
0.011450
11
0.011450
12
0.011450
13
0.011450
-
14
0.01,1450
15
1800
2
yes
0.01.1450
16
0.002320
17
1800
2
yes
0.002320
18
0.026200
19
0.002980
20
0.002980
21
0.002980
22
0.002980
23
0.002980
24
1600
2
yes
0.002980
25
0.014160
26
0.014160
27
0.014160
28
1500
2
yes
0.014160
29
0.014160
30
0.014160
31
0.014160
_
AVERAGE
0.008509
MAXIMUM
MINIMUM
_
Comp. (C) / Grab (G)
G
Daily Maximum
1.19
97
11
670
19
12
25
30
6<pH<9
0.38
300
monitor
DWQ Form MR-1 (11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
All monitoring data and sampling frequencies do NOT meet permit requirements
Compliant
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Jon Keener, 140 West Franklin, LLC
Permittee (Please print or type)
Si
ee Date
(Required unless submitted electronically)
Permittee Address Phone Number
126 West Franklin Street, Chapel Hill NC 27516 [phone]
e-mail address Permit Expiration Date
February 28, 2017
Certified Laboratory (2)
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ADDITIONAL CERTIFIED LABORATORIES
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per I5A NCAC 2B .0506(b)(2)(D).
L
Page 2

1
Laboratory Report of Analysis
To: Fred Ammons
Ammons Resource Group
2040 Peach Grove Lane
Zebulon, NC 27597
Report Number:
Client Project: 1
31202078
40 West
Dear Fred Ammons
Enclosed are the re
samples and assoc
Environmental Labc
retained in our files
intended to be used
samples submitted
unless other arrang
If there are any que
at [phone].
suits of the analytical services performed under the referenced project for the received
iated QC as applicable. The samples are certified to meet the requirements of the National
fratory Accreditation Conference Standards. Copies of this report and supporting data will be
for a period of five years in the event they are required for future reference. All results are
in their entirety and SGS is not responsible for use of less than the complete report. Any
to our laboratory will be retained for a maximum of thirty (30) days from the date of this report
ements are requested.
stions about the report or services performed during this project, please call Michael D. Page
We will be happy to answer any questions or concems which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America Inc.
Barbara A. Hager
2012.07.17 15:07:45-05'00'
Michael D. Page
Project Manager
michael.page@sgs.c
om
Date
Print Date 07: 1 '2012
NC
ANALYTICAL PERSPECTIVES IS NOW PART OF SGS, THE WORLD'S LEADING INSPECTION,
VERIFICATION, TESTING AND CERTIFICATION COMPANY.
5500 Business Dr_ US • 1B405 • Wilmington, NC t.t 910 3501903 f .1910 350 1557 www.sgs.com
{ Page-1 of 3
Member of ere SGS G ,Ln fSG S S4r

SG iIL-
Laboratory Qualifiers
Report Definitions
DL Method, Instrument, or Estimated Detection Limit per Analytical Method
CL Control Limits for the recovery result of a parameter
LOQ Reporting Limit
DF Dilution Factor
RPD Relative Percent Difference
LCS(D) Laboratory Control Spike (Duplicate)
MS(D) Matrix Spike (Duplicate)
MB Method Blank
Qualifier Definitions
' Recovery or RPD outside of control limits
B Analyte was detected in the Lab Method Blank at a level above the LOQ
U Undetected (Reported as ND or < DL)
✓ Recovery is below quality control limit. The data has been validated based on a favorable signal-to-noise
and detection limit
A Amount detected is less than the Lower Method Calibration Limit
J Estimated Concentration.
O The recovery of this analyte in the OPR is above the Method QC Limits and the reported concentration in
the sample may be biased high
E Amount detected is greater than the Upper Calibration Limit
S The amount of analyte present has saturated the detector. This situation results in an
underestimation of the affected analyte(s)
Q Indicates the presence of a quantitative interference. This situation may result in an
underestimation of the affected analyte(s)
Indicates the presence of a qualitative interference that could cause a false positive or an
overestimation of the affected analyte(s)
DPE Indicates the presence of a peak in the polychlorinated diphenylether channel that could
cause a false positive or an overestimation of the affected analyte(s)
TIC Tentatively Identified Compound
EMPC Estimated Maximum possible Concentration due to ion ratio failure
ND Not Detected
K Result is estimated due to ion ratio failure in High Resolution PCB Analysis
P RPD > 40% between results of dual columns
D Spike or surrogate was diluted out in order to achieve a parameter result within instrument calibration
range
Samples requiring manual integrations for various congeners and/or standards are marked and dated by the analyst. A code
definition is provided below:
M1 Mis-identified peak
M2 Software did not integrate peak
M3 Incorrect baseline construction (i.e. not all of peak included; two peaks integrated as one)
M4 Pattern integration required (i.e. DRO, GRO, PCB, Toxaphene and Technical Chlordane)
M5 Other - Explained in case narrative
Note Results pages that include a value for "Solids (%)" have been adjusted for moisture content.
Print Date: 07/17/2012
N C Certification # 481
5500 Business Dr US • 29405 - Wilmington, NC t 41 910 3501903 141 910 3501557 wwwsgs corn
j Page 2 of 33
MemberdtheSG5G+Quo ISGSSAI

Client Sample ID
Outfall 001 7-12
Oo
ANAL YT(=A1 I'I RfiaiCRVri
Sample Summary
Lab Sample ID Collected Received Matrix
31202078001 07/01/2012 11:15 07/02/2012 15:08 Water
Print Date' 07/17/2012 N C Certification # 481
5500 Business Dr. US • 29405 • Wilmington, NC 1,1 910 3501903 141 9103501557 www.sgs cum
Page-3-af'33
Member at tha SOS Group (SGS SAI

ANALYTICAL ICAL wIMree+ws
Case Narrative
Outfall 001 7-12
The temperature of the sample at the time of pH analysis was 22.6 degrees C.
Print Date: 07/17/2012
N C Certification # 481
15500 Business Dr. US • 28405 • Wilmington, NC t +t 910 3501903 f [phone] w•nw.sgs com
Page 4 of 33
Member of the SGS Groin ISG S SA1

Client Sample ID: 1
Lab Sample ID: 31:
EPA 420.4 (SUB)
SM 2540-D
SM 4500-H+ B pl-
SW-846 6010C
SW-846 8260B
Quality Control Sa
Client Sample ID: I
Lab Sample ID: 79'
SW-846 6010C
Detectable Results Summary
)utfall 001 7-12
:02078001-D Parameter Result Units
Phenol 0.0078 mg/L
Total Suspended Solids 4.00 mg/L
pH 8.756 S.U.
Lead 0.00713 mg/L J
tert-Butyl methyl ether (MTBE) 2.94 ug/L
mples
NB for HBN 25297 [MXX/2143)
64
Parameter Result Units
Lead 0.00597 mg/L J
Pant Date 07.17 2012 N C Cer • ... :
5500 Business Dr. US • 28405 • Wilmington, NC t+19103501903 t+19103501557 www.sgs corn
Page 5 0
Plembr• of ne SGS Gaup ISGS S41

SG.q
Ate. PRIIIPPECTIVICS
r- Results of Outfall 001 7-12
Client Sample ID: Outfall 001 7-12
Client Project ID: 140 West
Lab Sample ID: 31202078001-A
Lab Project ID: 31202078
`- Results by SW-846 8260B
Parameter
1,2-Dichloroethane
Benzene
Ethyl Benzene
Naphthalene
Toluene
Xylene (total)
tert-Butyl methyl ether
Surrogates
1,2-Dichloroethane-d4 102 64.0-140 % 1 07/6/2012 16:01
4-Bromofluorobenzene 99.0 85.0-115 % 1 07/6/2012 16:01
Toluene d8 103 82.0-117 % 1 07/6/2012 16:01
Collection Date: 07/01/2012 11:15
Received Date: 07/02/2012 15:08
Matrix: Water
Result Qual DL LOQ/CL Units OF Date Analyzed
ND U 0.167 1.00 ug/L 1 07/6/2012 16:01
ND U 0.113 1.00 ug/L 1 07/6/2012 16:01
ND U 0.0877 1.00 ug/L 1 07/6/2012 16:01
ND U 0.0855 1.00 ug/L 1 07/6/2012 16:01
ND U 0.133 1.00 ug/L 1 07/6/2012 16:01
ND U 0.182 2.00 ug/L 1 07/6/2012 16:01
(MTBE) 2.94 0.144 1.00 ug/L 1 07/6/2012 16:01
Batch Information
Analytical Batch: V
Analytical Method'
Instrument MSD3
Analyst: BWS
Analytical Date/Tim
MS2352 Prep Batch: VXX3590
SW-846 8260E Prep Method: SW-846 5030E
Prep Date/Time: 07/06/2012 09:53
Prep Initial Wt.Nol.: 40 mL
e: 07/06/2012 16:01 Prep Extract Vol: 40 mL
Pnnt Date: 07/17/2012 N.0 Certification # 481
5500 Business Dr. US • 28405 • Wilmington, NC t [phone] f [phone] w•ww.sgs corn
j Pdge6of33
Member or the SGS Glow !SGS SAI

AH.*I VTCAL rnna.[cnv¢i
Results of Outfall 001 7-12
Client Sample ID: Outfall 001 7-12
Client Project ID: 140 West
Lab Sample ID: 31202078001-H
Lab Project ID: 31202078
Results by SW-846 6010C
Parameter Result
Lead 0.00713
Batch Information
Analytical Batch: MIP1613
Analytical Method: SW-846 6010C
Instrument: ICP1
Analyst: NTM
Analytical Date/Time: 07/03/2012 17:38
Print Date. 0T17i2012
Qual
J
DL
0.00541
Collection Date: 07/01/2012 11:15
Received Date: 07/02/2012 15:08
Matrix: Water
LOQ/CL Units DF
0.0100 mg/L 1
Prep Batch: MXX2143
Prep Method: SW-846 3010A
Prep Date/Time: 07/03/2012 09:38
Prep Initial Wt./Vol.: 50 mL
Prep Extract Vol: 50 mL
Date Analyzed
07/3/2012 17:38
N C Certification # 481
5500 Business 0r. US 28405 • Wilmington, NC t +1 910 35C 1903 1 [phone] www.sgs corn
Page 7-of-3
Member of the SGS Grow ISGS S4 f

Results of Outfall 001 7-12
Client Sample ID: Outfall 001 7-12
Client Project ID: 140 West
Lab Sample ID: 31202078001-F
Lab Project ID: 31202078
Results by SM 2540-D
Parameter Result
Total Suspended Solids 4.00
Batch Information
Ana,yucai Batcn. IN01778
Analytical Method: SM 2540-D
Instrument: BAL70
Analyst: MAH
Analytical Date/Time: 07/06/2012 10:01
Print Date. 0707/2012
Qual DL
2.50
Collection Date: 07/01/2012 11:15
Received Date: 07/02/2012 15:08
Matrix: Water
LOQ/CL Units DF
2.50 mglL 1
Prep Batch: IN01778
Prep Method: SM 2540-D
Prep Date/Time: 07/06/2012 10:01
Prep Initial Wt.Nol.: 1 mL
Prep Extract Vol: 1 mL
Date Analyzed
07/6/2012 10:01
N C. Certification # 481
5500 Business Dr. US 28405 • Wilmington, NC t+i 910 3501903 f [phone] www.sgs com
Page 8 of 33
Menthe, p1 the Sr1S Group 1SGS 541

A 4. IVT ::AI I•r Ax=r::rvcc
Results of Outfall 001 7-12
Client Sample ID: Outfall 001 7-12
Client Project ID: 140 West
Lab Sample ID: 31202078001-G
Lab Project ID: 31202078
Results by SM 4500-H+ B pH
Parameter
pH
Ratrh Infnrmatinn
Result
8.756
Qual DL
0.0100
Collection Date: 07/01/2012 11:15
Received Date: 07/02/2012 15:08
Matrix: Water
LOQ/CL Units DF
0.0100 S.U. 1
Date Analyzed
07/3/2012 15:28
Analytical Batcn IN01779
Analytical Method: ISM 4500-H+ B pH
Instrument: PH2
Analyst: NTM
Analytical Date/Time: 07/03/2012 15:28
Prep Batch: IN01779
Prep Method: SM 4500-H+ B pH
Prep Date/Time: 07103/2012 15:28
Prep Initial Wt.Nol.: 1 mL
Prep Extract Vol: 1 mL
Print Date: 07/17/2012
N C Certification # 481
5500 Business 0r US • 28405 • Wilrningtan, NC t it 910 3501903 141 910 3501557 www.sgs corn
j f'dge9of3 Member ofttmSGSGIpin ISO SA

MALITCAL.. ,WE
r- Results of Outfall 001 7-12
Client Sample ID: Outfall 001 7-12
Client Project ID: 140 West
Lab Sample ID: 31202078001-D
Lab Project ID: 31202078
�— Results by EPA 420.4 (SUB)
Parameter
Phenol
Laboratory: Pace
Analytical Date/Time
Result
0.0078
: 07/13/2012 15:26
Collection Date: 07/01/2012 11:15
Received Date: 07/02/2012 15:08
Matrix: Water
Qual DL LOQ/CL Units DF Date Analyzed
0.00500 mg/L 1 07/13/2012 15:26
Prep Method.
Prep Date/Time:
Print Date 07/17/2012 N.C. Certfiication # 481
1
5500 Business Dr. US • 28405_ Wilmington, NC 1+1910 3501903 1+1910 3501557 www.sgs coin
Page 10 0"
MemDr vl rve SGS Group ISGSSAI

_SGS1
,•— Batch Summary
Analytical Method: SW-846 8260E
Prep Method: SW-846 5030E
Prep Batch: VXX3590
Prep Date: 07/06/2012 08:52
Client Sample ID
LCS for HBN 25376 [VXX/3590]
LCSD for HBN 25376 [VXX/3590)
MB for HBN 25376 [VXX/3590]
Outfall 001 7-12
MW-5(79515MS)
MW-5(79515MSD)
Lab Sample ID Analysis Date
79452 07/06/2012 10:06
79453 07/06/2012 10:31
79454 07/06/2012 11:22
31202078001 07/06/2012 16:01
79537 07/06/2012 20:41
79538 07/06/2012 21:06
Analytical Batch
VMS2352
VMS2352
VMS2352
VMS2352
VMS2352
VMS2352
Instrument Ana st
MSD3 BWS
MSD3 BWS
MSD3 BWS
MSD3 BWS
MSD3 BWS
MSD3 BWS
Print Date. 07 t
5500 Business Drive, Wilmington, NC 28405
t 910350.1903 f 910.350.1557 www.ussgs.com
Member of SGS Group
Page 11 of 33

AHAIVTC-AI 1'GRs'F:.nvF4
Method Blank
Blank ID: MB for HBN 25376 [VXX/3590]
Blank Lab ID: 79454
QC for Samples:
31202078001
Results by SW-846 8260E
Matrix: Water
Parameter Result Qual DL LOQ/CL Units DF
tert-Butyl methyl ether (MTBE) ND U 0.144 1.00 ug/L 1
Benzene ND U 0.113 1.00 ug/L 1
1,2-Dichloroethane ND U 0.167 1.00 ug/L 1
Toluene ND U 0.133 1.00 ug/L 1
Ethyl Benzene ND U 0.0877 1.00 ug/L 1
Xylene (total) ND U 0.182 2.00 ug/L 1
Naphthalene ND U 0.0855 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 102 64.0-140 % 1
Toluene d8 103 82.0-117 % 1
4-Bromofluorobenzene 100 85.0-115 % 1
Batch Information
-.. : MS2352
Analytical Method: SW-846 82606
Instrument: MSD3
Analyst BWS
Analytical Date/Time. 7/6/2012 11:22:OOAM
Prep Batch: VXX3590
Prep Method: SW-846 5030E
Prep Date/Time: 7/6/2012 8:52:54AM
Prep Initial Wt.Nol.: 40 mL
Prep Extract Vol: 40 mL
Print Date 07/17/2012 N C Certification # 481
15500 Business Dr. US • 28405- Wilmington, NC t [phone] t .1 910 3501557 www sgs com
Page 12 of 33
Member of the SGS Group ISGS SA)

CGS
r Blank Spike Summary
Blank Spike ID: LCS for HBN 25376 [VXX/3590]
Blank Spike Lab ID: 79452
Date Analyzed: 07/06/2012 10:06
QC for Samples: 31202078001
♦� Results by SW-846 8260E
Parameter
tert-Butyl methyl ether (MTBE)
Benzene
1,2-Dichloroethane
Toluene
Ethyl Benzene
Naphthalene
Surrogates
1,2-Dichloroethane-d4
Toluene d8
4-Bromofluorobenzene
Batch Information
Blank Spike (ug/L)
Spike Duplicate ID: LCSD for HBN 25376 [VXX/3590]
Spike Duplicate Lab ID: 79453
Date Analyzed: 07/06/2012 10:31
Matrix: Water
Spike Duplicate (ug/L)
Spike Result Rec (%) Spike Result Rec % CL RPD (%) RPD CL
5.00 4.17 83 5.00 4.57 91 47.0-142 9.2 30.00
5.00 4.62 92 5.00 4.95 99 76.0-124 6.9 30.00
5.00 4.33 87 5.00 4.88 98 76.0-119 12 30.00
5.00 4.76 95 5.00 5.02 100 75.0-123 5.3 30.00
5.00 4.33 87 5.00 4.78 96 76.0-123 9.9 30.00
5.00 4.36 87 5.00 4.63 93 67.0-122 6.0 30.00
Analytical Batch. VMS2352
Analytical Method: SW-846 8260E
Instrument: MSD3
Analyst BWS
Print Date 07/17i2017 '
100 100 64.0-140
103 101 82.0-117
102 99 85.0-115
Prep Batch: VXX3590
Prep Method: SW-846 5030E
Prep Date/Time: 07/06/2012 08:52
Spike Init Wt.Nol.. 40 mL Extract Vol: 40 mL
Dupe Init WI.NoI.: 40 mL Extract Vol: 40 mL
N C Certification # 481
5500 Business Dr US • 28405 Wilmington. NC t .1 910 3501903 1.1910 3501557 www.sgs corn
Page 13 of 33
Membe• of the SGS 4i oup iSGS SAr

Batch Summary
AN LMC LL PerM=ce.'nVR.
Analytical Method: SW-846 6010C
Prep Method: SW-846 3010A
Prep Batch: MXX2143
Prep Date: 07/03/2012 09:38
Client Sample ID Lab Sample ID Analysis Date Analytical Batch Instrument Analyst
MB for HBN 25297 [MXX/2143] 79164 07/03/2012 17:15 MIP1613 ICP1 NTM
LCS for HBN 25297 [MXX/2143] 79165 07/03/2012 17:20 MIP1613 ICP1 NTM
LCSD for HBN 25297 [MXX/2143] 79166 07/03/2012 17:34 MIP1613 ICP1 NTM
Outfall 001 7-12 31202078001 07/03/2012 17:38 MIP1613 ICP1 NTM
Outfall 001 7-12(79065MS) 79168 07/03/2012 17:43 MIP1613 ICP1 NTM
Outfall 001 7-12(79065MSD) 79169 07/03/2012 17:47 MIP1613 ICP1 NTM
70IW-02 (dissolved)(78895DUP) 79167 07/03/2012 18:02 MIP1613 ICP1 NTM
MB-F1 for HBN 25297 [MXX/2143] 79170 07/03/2012 18:06 MIP1613 ICP1 NTM
Print Date 07: t ; 20 ; 2. N C Certification # 461
5500 Business Drive, Wilmington, NC 28405
t 910350.1903 f 910.350.1557 vmvw.ussgs.com
Member of 5GS Group
Page 14 of 33

Method Blank
AN*1 VT.^Al 1•rRfiarr rrvn
Blank ID: MB for HBN 25297 [MXX/2143]
Blank Lab ID: 79164
QC for Samples:
31202078001
• Results by SW-846 6010C
Parameter
Lead
Batch Information
,•la ca. 1•:'613
Analytical Method: SW-846 6010C
Instrument: ICP1
Analyst: NTM
Analytical Date/Time
Result ual
0.00597 J
Print Date: 07/17/2012 1
: 7/3/2012 5:15:41PM
DL
0.00541
Matrix: Water
LOQ/CL Units
0.0100 mg/L
Prep Batch: MXX2143
Prep Method: SW-846 3010A
Prep Date/Time: 7/3/2012 9.38:37AM
Prep Initial Wt.Nol.: 50 mL
Prep Extract Vol: 50 mL
DF
1
N C Certification # 481
5500 Business Dr. US • 28405 • Wilmington, NC t 41 910350 1903 141 9103501557 www.sgs can
aye is 0
Memae+ of etie SGS Grow ISGS S4I

Ann
Matrix Spike Summary
Original Sample ID: 31202078001 (Outfall 001 7-12)
MS Sample ID: 79168
MSD Sample ID: 79169
QC for Samples: 31202078001
Results by SW-846 6010C
Analysis Date: 07/03/2012 17:38
Analysis Date: 07/03/2012 17:43
Analysis Date: 07/03/2012 17:47
Matrix: Water
Matrix Spike (mg/L) Spike Duplicate (mg/L)
Parameter Sample Spike Result Rec (%) Spike Result Rec (%) CL RPD (%) RPD CL
Lead 0.00713 0.400 0.370 92 0.400 0.351 88 75.0-125 5.3 20.00
Batrh Information
Analytical Batch: MIP1613
Analytical Method: SW-846 6010C
Instrument: ICP1
Analyst: NTM
Prep Batch: MXX2143
Prep Method: SW-846 3010A
Prep Date/Time: 07/03/2012 09:38
MS Init Wt.Nol.: 50 mL Extract Vol.: 50 mL
MSD Init Wt.Nol.: 50 mL Extract Vol.: 50 mL
Print Date 07/17/2012 N C CertiticaUon # 481
5500Business Dr. US • 20405- Wilmington, NC t [phone]+19103501557 www.sgs corn
Page 18 of33
Member of the SCS Group ISO SAI

SG$
f— Method Blank
w►w.nem Ana
Blank ID: MB-F1 for HBN 25297 [MXX/2143]
Blank Lab ID: 79170
QC for Samples:
31202078001
Results by SW-846 6010C
Matrix: Water
Parameter Result Qual DL LOQ/CL Units DF
Lead ND U 0.00541 0.0100 mg/L 1
Batch Information
Analytical Batch: M
Analytical Method:
Instrument: ICP1
Analyst: NTM
Analytical Date/Tim
IP1613 Prep Batch: MXX2143
SW-846 6010C Prep Method: SW-846 3010A
Prep Date/Time: 7/3/2012 9:38:37AM
Prep Initial Wt.Nol.: 50 mL
s: 7/3/2012 6:06:33PM Prep Extract Vol: 50 mL
Print Date 07;17-2012 N.0 Certification # 481
5500 Business Dr. US • 26405 Wilmington, NC t+1 9.10 35C 1903 1.1 910 350:557 w•ww.sgs corn
Peye t8-of 33
Member of the SGS GI OUP ISGS S41

AH-11 R%OR(`.m1fl
Blank Spike Summary
Blank Spike ID: LCS for HBN 25297 [MXX/21431
Blank Spike Lab ID: 79165
Date Analyzed: 07/03/2012 17:20
QC for Samples: 31202078001
Results by SW-846 6010C
Parameter
Lead
Batch Information
Blank Spike (mg/L)
Spike Duplicate ID: LCSD for HBN 25297 [MXX/2143]
Spike Duplicate Lab ID: 79166
Date Analyzed: 07/03/2012 17:34
Matrix: Water
Spike Duplicate (mg/L)
Spike Result Rec (%) Spike Result Rec % =! RPD (%) RPD CL
0.400 0.392 98 0.400 0.388 97 1-0
Analytical Batch: MIP1613
Analytical Method: SW-846 6010C
Instrument. ICP1
Analyst: NTM
Print Date. 07/17/2012
Prep Batch: MXX2143
Prep Method: SW-846 3010A
Prep Date/Time 07/03/2012 09:38
Spike Init Wt.Nol : 50 mL Extract Vol: 50 mL
Dupe Init Wt./Vol.: 50 mL Extract Vol: 50 mL
N.C. Certification # 481
5500 Business Dr. US - 28405 Wilmington, NC t f t 910 35C 1903 1 -1 910 350 7557 www.sgs corn
Page 17-of-33
Membrr of the SGS Gloua ISGS S41

r- Batch Summary
Analytical Method: SM 2540-D
Prep Method: SM 2540-D
Prep Batch: IN01778
Prep Date: 07/06/2012 09:54
Client Sample ID
MB for HBN 25344 LINO/1778]
LCS for HBN 25344 [INO/1778]
LCSD for HBN 25344 [INO/1778]
Outfall 001 7-12
Outfall001 7-12(79065DUP)
Lab Sample ID Analysis Date
79336 07/06/2012 09:54
79337 07/06/2012 09:57
79338 07/06/2012 09:59
31202078001 07/06/2012 10:01
79339 07/06/2012 10:03
Analytical Batch Instrument Analyst
IN01778 BAL10 MAH
IN01778 BAL10 MAH
IN01778 BAL10 MAH
INO1778 BAL10 MAH
IN01778 BAL10 MAH
Print Date 07,17:2012
5500 Business Drive, Wilmington, NC 28405
t 910.350.1903 f 910.350.1557 www.ussgs.com
Member of SGS Group
Page 19 of 33

AN .LV7,r I ITRR'c;.nvc4
Method Blank
Blank ID: MB for HBN 25344 [INO/1778]
Blank Lab ID: 79336
QC for Samples:
31202078001
Results by SM 2540-D
Parameter
Total Suspended Solids
Batch Information
Result
ND
a;ch. INO1778
Analytical Method: SM 2540-D
Instrument: BAL10
Analyst: MAH
Analytical Date/Time: 7/6/2012 9:54:50AM
Print Date: 137117 /2012
Qual
U
DL
2.50
Matrix: Water
LOQ/CL
2.50
Units
mg/L
Prep Batch: INO1778
Prep Method: SM 2540-0
Prep Date/Time: 7/6/2012 9:54:50AM
Prep Initial Wt.Nol.: 1 mL
Prep Extract Vol: 1 mL
DF
1
N C Certification # 481
5500 Business Or US • 20405 • Wilmington, NC t +i 910 3501903 1 +19i0 3501557 www.sgs com
Page-20d1:f33
Member of the SGS Gaup ISGSSAI

sGt
wrwnraararr.errva
r• Blank Spike Summary
Blank Spike ID: LCS for HBN 25344 [INO/1778]
Blank Spike Lab ID: 79337
Date Analyzed: 07/06/2012 09:57
QC for Samples: 31202078001
�. Results by SM 2540-D
Parameter
Total Suspended Solids
Rafe Infnnnafinn
Spike Duplicate ID: LCSD for HBN 25344 [INO/1778]
Spike Duplicate Lab ID: 79338
Date Analyzed: 07/06/2012 09:59
Matrix: Water
Blank Spike (mg/L) Spike Duplicate (mg/L)
Spike Result Rec (%) Spike Result Rec (%) __ RPD (%) RPD CL
500 484 97 500 483 97 000-I20 0.21
Analytical Batch IN01778
Analytical Method. SM 2540-D
Instrument: BAL10
Analyst: MAH
Prep Batch: IN01778
Prep Method: SM 2540-D
Prep Date/Time: 07/06/2012 09:57
Spike Init Wt.Nol.: 1 mL Extract Vol: 1 mL
Dupe Init Wt.Nol.: 1 mL Extract Vol: 1 mL
Print Date 07/17/2t712
N:C Certification # 481
5500 Business Dr US • 18405 Wilmington. NC t41 910 35C 1903 I.1910350'557 www.egscorn
_r Page 21 of-33—
Membe- of t,e SGS Group ISG s S4i

scS
10
ANAIVTIc:At I•F R4�FC.T`V F4
Duplicate Sample Summary -1
Original Sample ID: 31202078001-F
Duplicate Sample ID: 79339
QC for Samples: 31202078001
Analysis Date: 07/06/2012 10:01
Analysis Date: 07/06/2012 10:03
Matrix: Water
Results by SM 2540-D
PARAMETER Original (mg/L) Qual Duplicate (mg/L) Qual RPD (%) RPD CL
Total Suspended Solids 4.00 ND 20.00
aatcn mtormauon
Analytical batcn lN0 1 7 78
Analytical Method: SM 2540-D
Instrument: BAL10
Analyst: MAH
Print Date: 07/17/2012
N.C. Certification # 481
5500 Business Dr. US - 28405 • Wilmington, NC t +i 910 3501903 141 910 3501557 www.sgs cam
Pdye 22 u
Member of the SGAS 6roue ISGS SAI

art
ANUVIICAL P[nvfcrrvi.*
Batch Summary
Analytical Method: EPA420.4
Prep Method: SM 4500-H+ B pH
Prep Batch:INO1779
Prep Date: 07/03/2012 15:28
Client Sample ID Lab Sample ID Analysis Date Analytical Batch Instrument Analyst
Outfall 001 7-12 31202078001 07/13/2012 15:26 Pace
Print Date 07117/2012 M C Certification # 481
5500 Business Drive, Wilmington, NC 28405
t 910.350.1903 f 910.350.1557 Www.us.sgs.com
Member of SGS Group
Page 23 of 33

aceAnalytica!®
wwwpace/abs.c %n
July 17, 2012
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
Mr. Michael Page
SGS Environmental Services Inc
5500 Business Drive
Wilmington, NC 28405
RE: Project: 31202078
Pace Project No.: 92123151
Dear Mr. Page:
Enclosed are the analytical results for sample(s) received by the laboratory on July 03, 2012. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Renee Spencer
[e-mail]
Project Manager
Enclosures
cc: Ms. Barbara Hager, SGS Environmental Services Inc.
REPORT OF LABORATORY ANALYSIS Page 1 of 8
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 24 of 33

W /'UlGViVCU 0I
M.wwacefabs.com
Project: 31202078
Pace Project No.: 92123151
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 iGncey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
CERTIFICATIONS
Asheville Certification Ms
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification]#: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia Certification #: 00072
West Virginia Certification #: 356
VirginaNELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS Page 2 of 8
This report shall not be reproduced, except in full,
without the written consent of PaceAnalytical Services, Inc..
Page 25 of 33

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kncey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
SAMPLE SUMMARY
Project: 31202078
Pace Project No.: 92123151
Lab ID Sample ID Matrix Date Collected Date Received
92123151001 31202078001
Water 07/01/12 11:15 07/03/12 17:05
REPORT OF LABORATORY ANALYSIS Page 3 of 8
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 26 of 33

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 7795 Riverside Dr. 9800 ICncey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersvilte, NC 28078
[phone] [phone] [phone]
SAMPLE ANALYTE COUNT
Project: 31202078
Pace Project No.: 92123151
Lab ID Sample ID
Analytes
Method Analysts Reported Laboratory
92123151001 31202078001 EPA 420.4 SDH 1 PASI-A
REPORT OF LABORATORY ANALYSIS Page 4 of 8
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 27 of 33

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 IGnceyr Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
ANALYTICAL RESULTS
Project: 31202078
Pace Project No.: 92123151
Sample: 31202078001
Parameters
Lab ID: 92123151001 Collected: 07/01/12 11:15 Received: 07/03/12 17:05 Matrix: Water
Report
Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
420.4 Phenolics, Total
Phenol
Date: 07/17/2012 12:59 PM
Analytical Method: EPA 420.4
0.0078 mg/L 0.0050 0.0050 1 07/13/12 15:26 108-95-2
REPORT OF LABORATORY ANALYSIS Page 5 of 8
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 28 of 33

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Klncey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: 31202078
Pace Project No.: 92123151
QC Batch: WETA/12606 Analysis Method: EPA 420.4
QC Batch Method: EPA 420.4 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92123151001
METHOD BLANK: 793161
Associated Lab Samples: 92123151001
Matrix: Water
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenol mg/L ND 0.0050 07/13/12 15:32
LABORATORY CONTROL SAMPLE: 793162
Parameter
Units
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
Phenol mg/L .05 0.051 102 90-110
MATRIX SPIKE SAMPLE: 793164
92122888001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Phenol mg/L 0.099 .05 0.21 225 90-110 M1
MATRIX SPIKE SAMPLE: 793166
92123151001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Phenol mg/L 0.0078 .05 0.12 214 90-110 M1
SAMPLE DUPLICATE: 793163
92122888001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Phenol mg/L 0.099 0.11 11 20
SAMPLE DUPLICATE: 793165
Parameter Units
92123151001 Dup Max
Result Result RPD RPD Qualifiers
Phenol mg/L 0.0078 0.0093 18 20
Date: 07/17/2012 12:59 PM
REPORT OF LABORATORY ANALYSIS Page 6 of 8
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 29 of 33

es
Analytical
wwwpacetabs.com
Project: 31202078
Pace Project No.: 92123151
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 IGnceyr Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALIFIERS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethytvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anatytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
Date: 07/17/2012 12:59 PM
REPORT OF LABORATORY ANALYSIS Page 7 of 8
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 30 of 33

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite 2225 Riverside Dr. 9800 KnceyAve. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 31202078
Pace Project No.: 92123151
Lab ID
Analytical
Sample ID QC Batch Method QC Batch Analytical Method Batch
92123151001 31202078001 EPA 420.4 WETA/12606
Date: 07/17/2012 12:59 PM
REPORT OF LABORATORY ANALYSIS Page 8 of 8
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 31 of 33

SGS1
CHAIN OF CUSTODY RECORD
SGS North America Inc.
Locations Nationwide
• Alaska • Maryland
• New Jersey • New York
• North Carolina • Ohlo
www.us.ags.com
104348
1 CLIENT. 4#1�(9l)5 !\ .. L PC80- 6E0 op
SGS Reference:
/
/ /
CONTACT. HONE N0: ) 6171
l 3202.078'
PAGE OF
wumz-a-izoo
Prawn
/4/7�g�LE361
PRO.lECT.SITEIPWSID# :
,
REPORTS TO:
•
P€o , f \!a 1,5AX NO.:( )
COMP
5:
Refired
o V
1/4.'
INVOICE TO: QUOTE 9:
/f �
D/e Kt Llr P.O. NUMBER:
GRABG
I
LAB NO.
SAMPLE IDENTIFICATION
DATE
TIME
MATRIX
�,
0-I
REMARKS
6ingsk t O/ 7- /Z
?'i—/Z
/%1 S
Waitr
`I
Gr
✓
,i
,.--
.�7 (3'MX
gJel C.
,_
/IA r 6 g ,
/ Z rc�4
_
NQpihvt l
go s, , •—
0 r&,- Nay
.
,
_
keDu/ket,./
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co
_
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co, : - ... R u7 • • = y:(1)
Date
N
Z
limo�j�
it •)
`• ((•/ 0 a
R rued B • ,
IL
T
Shipping Carrier:
Shipping Ticket No:
Samples Received Cold? (Orel YES O
Temperature°C: •�i l 0C •
Reli quishe ' : (2)
64 , r
Date
74-1712
Timo
y 2..
Re ved By:
k't �, j^A.-/
Special Deliverable Requirements:
Chain of Custody Seal: (Circle)
INTA BROKEN ABSENT
Relinquished
By: (3)
PCiff//L.
Date
9' XI;
Timo
/503'
Received By:
ti,,,,..e...........
Special Instructions:
Relinquished By: (4)
Date
Timo
cel a t. 8y:
Requested Turnaround Timo:
■ RUSH XSTD
Data Needed
C
CD
CO
0
w
O 200 W. Potter Drive Anchorago. AK 99518 Tel: [phone] Fax: [phone]
0 5500 Business Drive Wilmington, NC 29405 Tel: [phone] Fax: [phone]
White • Retained by Lab
Pink - Retained by Client

SGS North America Inc.
Sample Receipt Checklist (SRC1
Client Ammons Resource Group Work Order No.: 31202078
1. Shipped Notes:
1( Hand Delivered
2. X COC Present on Receipt
No COC
Additional Transmittal Forms
3. X Custody Tape on Container
No Custody Tape
4. X Samples Intact
Samples Broken / Leaking
5. X Chilled on Receipt Actual Temp.(s) in °C: 2.1
Ambient on Receipt
X Walk-in on Ice; Coming down to temp.
Received Outside of Temperature Specifications
6. )(', Sufficient Sample Submitted
Insufficient Sample Submitted
7. Chlorine absent
X HNO3 < 2
HCL<2
X Additional Preservatives verified (see notes)
8. X', Received Within Holding Time
Not Received Within Holding Time
9. X No Discrepancies Noted
Discrepancies Noted
NCDENR notified of Discrepancies*
10. X No Headspace present in VOC vials
Headspace present in VOC vials >6mm
Comments:
H2SO4
Inspected and Logged in by: JJ
Date: Mon-7/2/12 00:00
Page 33 of 33
*NCDENR must be notified when collection, holding time or preservation requirements are not met. Ml_11.6

.ARG
Ammons Resource Group
2040 Peach Grove Lane Zebulon, NC 27597
919-369-5679 [e-mail]
July 23, 2012
To Whom It May Concern
Central Files
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: JUNE 2012 DISCHARGE MONITORING REPORT
140 WEST FRANKLIN, LLC
140 WEST FRANKLIN STREET
CHAPEL HILL, ORANGE COUNTY, NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
Attached is the June 2012 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill, North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Water samples will be collected from outfall 001 during July 2012 for the quarterly sampling
event as required by the permit. Flow rates were recorded and documented and were below the
permitted daily maximum limits. This information is submitted as required by Part II, of Section
D. (2.) of its NPDES Permit.
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely,
Ammons Resource Group
Fre mops
ORC
Enclosures: June 2012 DMR
cc: Mr. Jon Keener, 140 West Franklin, LLC
Mr. Mike Taylor, Chapel Hill

ARG
2040 Peach Grove Lane Zebulon, NC 27597
919-369-5679 [e-mail]
July 23, 2012
To Whom It May Concem
Central Files
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: JUNE 2012 DISCHARGE MONITORING REPORT
140 WEST FRANKLIN, LLC
140 WEST FRANKLIN STREET
CHAPEL HILL, ORANGE COUNTY, NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
Attached is the June 2012 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill, North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Water samples will be collected from outfall 001 during July 2012 for the quarterly sampling
event as required by the permit. Flow rates were recorded and documented and were below the
permitted daily maximum limits. This information is submitted as required by Part II, of Section
D. (2.) of its NPDES Permit.
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely,
Ammons Resource Group
tI'i
mons
ORC
Enclosures: June 2012 DMR
cc: Mr. Jon Keener, 140 West Franklin, LLC
Mr. Mike Taylor, Chapel Hill

EFFLUENT
NPDES PERMIT NO. NCG510532 DISCHARGE NO. 001
MONTH June YEAR 2012
FACILITY NAME 140 WEST FRANKLIN CLASS NA COUNTY ORANGE
CERTIFIED LABORATORY (1) SGS Environmental Services. Inc CERTIFICATION NO. 481
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons GRADE 1 CERTIFICATION NO. 992126
PERSON(S) COLLECTING SAMPLES Fred Ammons
CIIECK BOX IF ORC IIAS1 F'V
Mail ORIGINAL and ONE COPY to: 1J
ORC PHONE [phone]
NO FLOW / DISCHARGE FROM SITE *
ATI iN: CENTRAL FILES
DIVISION OF WATER QUALITY AU G 0 6 2012 (S1 NATURE OFOPERATOR IN RESPONSIBLE CHARGE)
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH, NC 27699-1617 CENTRAL FILES ACCURATE AND COMPLETE TOTHE BEST OF MY KNOWLEDGE.
(1LAl/l11lt�11:
2- 2.F--/z
DATE
34010
81551
22417
34696
01051 l
00530
00400
32103
03604
00556
50050
34030
34371
FLOW
UP
4:7
o
TOTAL XYLENES
NIE'I'►IYL TERT BUTYL
ETIIER (NITRE)
='
-
sc
Q
z
TOTAL LEAD
'I'O'1'AL SUSPENDED
SOLIDS ('I'SS)
1,2 DICIILOROETIIANE
fl (1,2 DCA)
TOTAL P1iENOLS
OIL AND GREASE
Z
=s
=
2
cs.EFFN5
`
INF ❑
v
W
a
i.. u
�
s-
co�
m
p
c
. -.
7_
L.
y
I
IIRS
HRS
V/B/N
MILD
UC/l.
UG/L
UC/l.
UG/L
UG/L
UGIL
11G/I.
m;1L
UG/L
VGA.
1
0.009570
2
0.009570
3
0.009570
4
0.009570
5
0.009570
6
2100
2
yes
0.009570
7
0.010820
8
0.010820
9
1100
2
yes
0.010820
10
0.010650
11
0.010650
12
0.010650
13
0.010650
14
0.010650
15
1400
2
ycs
0.010650
16
0.007450
17
0.007450
18
0.007450
19
0.007450
20
0.007450
21
0.007450
22
0.007450
23
0.007450
24
0.007450
25
1800
3
yes
0.007450
26
1500
3
yes
0.009818
27
0.009818
28
0.009818
29
0.009818
30
0.009818
AVERAGE
0.009246
MAXIMUM
MINIMUM
Comp. (C) / Grab (G)
G
Daily Maximum
1.19
97
11
670
19
12
25
30
6<pH<9
0.38
300
monitor
DWQ Form MR -I (11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
All monitoring data and sampling frequencies do NOT meet permit requirements
Compliant
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part ll.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Jon Keener, 140 West Franklin, LLC
Permittee (Please print or type)
Signa o� i e Dat
(Required unl s submitted electronically)
Permittee Address Phone Number
126 West Franklin Street, Chapel Hill NC 27516 [phone]
e-mail address
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Permit Expiration Date
February 28, 2017
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No F1ow/D charge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

EFFLUENT
NPDES PERMIT NO. NCG510532 DISCHARGE NO. 001 MONTH June
FACILITY NAME 140 WEST FRANKLIN CLASS NA COUNTY ORANGE
YEAR 2012
CERTIFIED LABORATORY (1) SGS Environmental Services, Inc CERTIFICATION NO. 481
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons
PERSON(S) COLLECTING SAMPLES Fred Ammons
CHECK BOX IF ORC HRE' IV E 19
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES BUG 0 6 201Z
DIVISION OF WATER QUALI (SI A OF PERATOR IN RESPONSIBLE CHARGE)
1617 MAIL SERVICE CENT BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH, NC 27699-1617kJ ENTRAL F I<_ES ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
OWQ/BO
GRADE 1 CERTIFICATION NO. 992126
ORC PHONE [phone]
d
NO FLOW / DISCHARGE FROM SITE *
9- 2$s-yZ
DATE
a
A
Operator Arrival Time
2400 Clock
Operator Time
On Site
ORC On Site? **
50050
34030
34371
34010
81551
22417
34696
01051
00530
00400
32103
03604
00556
FLOW
BENZENE
ETHYLBENZENE
TOLUENI6
TOTAL XYLENES
METHYL TERT_BUTYL
ETHER (MTBE)
NAPHTHALENE
TOTAL LEAD
TOTAL SUSPENDED
SOLIDS (TSS)
Ti
1,2 DICHLOROETHANE
(1,2 DCA)
TOTAL PHENOLS
OIL AND GREASE
EFF7431
INF 0
DAILY
RATE
HRS
HRS
Y/BIN
MGD
UG/L
UG/L
11C/I.
l'Gil,
UG/L
UGII.
1'C/1,
mglL
UG/L
UG/L
1
0.009570
2
0_009570
3
0_009570
4
0_009570
5
0_009570
6
2100
2
yes
0_009570
7
0.010820
8
0.010820
9
1100
2
yes
0.010820
10
0.010650
11
0.010650
12
0.010650
13
0.010650
14
0.010650
15
1400
2
yes
0.010650
16
0.007450
17
0.007450
18
0.007450
19
0.007450
20
0.007450
21
0.007450
22
0.007450
23
0.007450
24
0.007450
25
1800
3
yes
0.007450
26
1500
3
yes
0.009818
27
0.009818
28
0.009818
29
0.009818
30
0.009818
AVERAGE
0.009246
MAXIMUM
MINIMUM
Comp. (C) / Grab (G)
G
Daily Maximum
1.19
97
11
670
19
12
25
30
6<pH<9
0.38
300
monitor
DWQ Form MR-1 (11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
All monitoring data and sampling frequencies do NOT meet permit requirements
x
Compl iant
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part I I.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Jon Keener, 140 West Franklin, LLC
Permittee (Please print or type)
Signu_twe oo
ee** Dat
(Required unle3's submitted electronically)
Permittee Address Phone Number
126 West Franklin Street, Chapel Hill NC 27516 [phone]
Certified Laboratory (2)
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
e-mail address
ADDITIONAL CERTIFIED LABORATORIES
Certification No.
Certification No.
Certification No.
Certification No.
Permit Expiration Date
February 28, 2017
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per I5A NCAC 2B .0506(b)(2)(D).
Page 2

ARG
2040 Peach Grove Lane Zebulon, NC 27597
919-369-5679 [e-mail]
June 23, 2012
To Whom It May Concern
Central Files
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: MAY 2012 DISCHARGE MONITORING REPORT
140 WEST FRANKLIN, LLC
140 WEST FRANKLIN STREET
CHAPEL HILL, ORANGE COUNTY, NORTH CAROLINA
NPDES PERMIT NO. NCG510532
Dear Sir/Madam:
Attached is the May 2012 Discharge Monitoring Report for the 140 West Franklin site on
Franklin Street in Chapel Hill, North Carolina. This work was conducted under NPDES Permit
No. NCG510532. Discharge from site dewatering activities to outfall 001 began May 17, 2012.
Water samples will be collected from outfall 001 during June 2012 for the quarterly sampling
event as required by the permit. Flow rates were recorded and documented and were below the
permitted daily maximum limits. This information is submitted as required by Part II, of Section
D. (2.) of its NPDES Permit.
If you have any questions or need additional information, please feel free to contact me at 919-
369-5679.
Sincerely,
Ammons Resource Group
Fred bmmons
ORC
Enclosures: May 2012 DMR
cc: Mr. Jon Keener, 140 West Franklin, LLC
Mr. Mike Taylor, Chapel Hill

EFFLUENT
NPDES PERMIT NO. NCG510532 DISCHARGE NO. 001 MONTH MAY YEAR 2012
FACILITY NAME 140 WEST FRANKLIN CLASS NA COUNTY ORANGE
CERTIFIED LABORATORY (1) SGS Environmental Services. Inc CERTIFICATION NO. 481
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Fred Ammons
PERSONS) COLLECTING SAMPLES Fred Ammons
CHECK BOX IF ORC HAS CHANGED ❑
Mail ORIGINAL and ONE COPY to:
ATI'N: CENTRAL FILES
GRADE I CERTIFICATION NO. 992126
ORC PHONE [phone]
NO FLOW / DISCHARGE FROM SITE *
DIVISION OF WATER QUALITY (S A P RA7'OR IN RESPONSIBLE CHARGE)
1617 Milli, SERVICE CENTER Ii THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH, NC 27699-1617 CCURATE AND COMPLETE. TO THE BEST OF MY KNOWLEDGE.
C .2?.
DATE
W
F
CI
Operator Arrival Time
2400 Clock
Operator Time
On Site
#
s,
WI
0
O
50050
34030 1 343711 34010 181551
1 22417
1 34696 101051
I 00530 J 00400 132103 103604
00556
FLOW
BENZENE
ETHYLBENZENE
TOLUENg
TOTAL XYLENES
METHYL TERT_BUTYL
ETHER(MTBE)
NAPHTHALENE
TOTAL LEAD
TOTAL SUSPENDED
SOLIDS (TSS)
a
1,2 DICHLOROETHANE
(1,2 DCA)
TOTAL PHENOLS
OIL AND GREASE
EFFXII
INFO
-
E�
it :IS
C a
rota
HRS
Y/B/N
MGD
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
mg/L
UG/L
UG/L
I
2
_
3
4
5
-
-
6
7
8
9
10
11
_
_
12
13
14
15
_
1
16
17
1600
4
yes
0.013700
nd
nd
ad
nd
nd
nd
nd
18
1100
3.00
yes
0.013700
19
0.013700
20
0.013700
21
0.013700
22
0.013700
23
-
0.013700
24
1000
2
yes
0.013700
25
0.002350
26
0.002350
27
0.002350
28
0.002350
29
1100
3
yes
0.002350
30
0.009580
31
0.009580
AVERAGE
0.009367
MAXIMUM
MINIMUM
Comp. ((.. / Grab (G)
I G
Daily Maximum
1
1.19 1
97
11
670
19
12
25
30
6<p14<9
0.38
300
monitor,
DWQ Form MR-1 (11/94)

Fatally St (Please cheek one ante a following)
All monitoring data and sampling frequencies meet permit ruiuinunents
(including weddyav if applicable)
ComFdiant
All monitoring data and sampling frequencies do NOT meet permit requirements J7
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office
tiMatars pithily health or the environment. Any noncompliance first potentially
information shall be provided orally within 24 hours from the time the
penmittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
pc/mince Warn= aware of thy. einamatesnces.
if the facility is noncompliant, please attar a list of corrective actions being takes and a thne-tabk for
Improvements to be made as required by Part lLE.6 of the NPDES permit.
"1 certify, under penalty of law, that this document and all attachments were pied under my diversion or supervis or
in accordance with a system designed to assure that qualified personnel propeaiy gam and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those pexsots directly responsible
for gathering the infiimmtion, the information submitted is, to the best of my knowledge and belief true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, inducting the possibility of
fates and imptiscmment for knowing violations."
Pennine* Address Phmus Number anted strokes Pannit Espbetian Dose
lab West Franklin Street, Chapel Ell NC 27516 t919) 868-1678 Feb ua 28,, 2017
ADDmONAL CERIUM LABORATORIES
Certified Laboratory (2) Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at (9l 9) 733-5083 or by visiting the Surface
Water Protection Section's web site at h2u en state e.its/wgs and linking to the unit's information pages.
Use: only emit! ofmeasurement designated in the reporting facility's NPDFS permit kw reporting cbra
* No P w!Diaebarge Prone Site: (heck this born into urge aeons s and, as a result, there are no data to be
anard for ell of ale: pares an the Diofft tithe emote moniftaing paint
*' ORC Oa Site?: ORC must visit sty and doomed visitation tian afreeily as required per lMA NCAC 8G .U204.
"* Signature of Pcrmitte= tfsigned by ounce than the pe rmintee. than the Megaton adze signatory authority must be on
file with the state per l5A NCAC 2B .0506(bX2)(D).
Page 2

Laboratory Report of Analysis
To: Fred Ammons
Ammons Resource Group
2040 Peach Grove Lane
Zebulon, NC 27597
Report Number. 31201469
Client Project: 140 West
Dear Fred Ammons,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. All results are
intended to be used in their entirety and SGS is not responsible for use of less than the complete report. Any
samples submitted to our laboratory will be retained for a maximum of thirty (30) days from the date of this report
unless other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Michael D. Page
at [phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America Inc.
5
Digitally signed by: Michael Page
Date: 2012.05.15 14:01:32-05'00'
Michael D. Page
Project Manager
[e-mail]
Pr' Rate: C! ' _ ...
Date
'3A-M P o(,ctED sm
�
5500 Business Drive, Wilmington, NC JR405
t 910.350.1903 f 910.350.1557 www.us.sgs.com
Member of SGS Group
Page 1 of 11

SGS
C
Report Definitions
Laboratory Qualifiers
DL Method, Instrument, or Estimated Detection Limit per Analytical Method
CL Control Limits for the recovery result of a parameter
LOQ Reporting Limit
DF Dilution Factor
RPD Relative Percent Difference
LCS(D) Laboratory Control Spike (Duplicate)
MS(D) Matrix Spike (Duplicate)
MB Method Blank
Qualifier Definitions
• Recovery or RPD outside of control limits
B Analyte was detected in the Lab Method Blank at a level above the LOQ
U Undetected (Reported as ND or < DL)
✓ Recovery is below quality control limit. The data has been validated based on a favorable signal-to-noise
and detection limit
A Amount detected is less than the Lower Method Calibration Limit
J Estimated Concentration.
O The recovery of this analyte in the OPR is above the Method QC Limits and the reported concentration in
the sample may be biased high
E Amount detected is greater than the Upper Calibration Limit
S The amount of analyte present has saturated the detector. This situation results in an
underestimation of the affected analyte(s)
Q Indicates the presence of a quantitative interference. This situation may result in an
underestimation of the affected analyte(s)
Indicates the presence of a qualitative interference that could cause a false positive or an
overestimation of the affected analyte(s)
DPE Indicates the presence of a peak in the polychlorinated diphenylether channel that could
cause a false positive or an overestimation of the affected analyte(s)
TIC Tentatively Identified Compound
EMPC Estimated Maximum possible Concentration due to ion ratio failure
ND Not Detected
K Result is estimated due to ion ratio failure in High Resolution PCB Analysis
P RPD > 40% between results of dual columns
D Spike or surrogate was diluted out in order to achieve a parameter result within instrument calibration
range
Samples requiring manual integrations for various congeners and/or standards are marked and dated by the analyst. A code
definition is provided below:
M1 Mis-identified peak
M2 Software did not integrate peak
M3 Incorrect baseline construction (Le. not all of peak included; two peaks integrated as one)
M4 Pattern integration required (Le. DRO, GRO, PCB, Toxaphene and Technical Chlordane)
M5 Other - Explained in case narrative
Note Results pages that include a value for "Solids (%)" have been adjusted for moisture content.
N C Certification # 481
5500 Business Drive, Wilmington, NC 28405
t 910.3.50.1903 t910.350.1557_0.m.us.sgs.com
www.ussgs.com
Member of SGS Group
Page 2 of 11

Client Sample ID
Intake
Outfall
Pant Date. Oe
Sample Summary
Lab Sample ID Collected Received Matrix
31201469001 05/11/2012 08:00 05/12/2012 10:00 Water
31201469002 05/11/2012 08:00 05/12/2012 10:00 Water
S500 Business Drive, Wilmington, NC 2&105
t 910.350.1903 f 910.350.1557 www.us.sgs.com
Member of SGS Group
Page 3 of 11

Results of Intake
Client Sample ID: Intake
Client Project ID: 140 West
Lab Sample ID: 31201469001-A
Lab Project ID: 31201469
Results by SW-846 8260B
Parameter
1,2-Dichloroethane
Benzene
Ethyl Benzene
Naphthalene
Toluene
Xylene (total)
tert-Butyl methyl ether (MTBE)
Surrogates
1,2-Dichtorcelhane-d4
4-Bromofluorobenzene
Toluene d8
Batch Information
Result
ND
3.11
0.690
0.440
0.390
1.88
18.5
98.0
101
101
^alytic.,l Meti;oc+: SW-846 8260E
instrument: 4SO4
Anaiysl. DVO
Analytical Date.; i me: 05/14/2012 12:06
Pint Dale 05.'
Qual
U
J
J
J
J
DL
0.167
0.113
0.0877
0.0855
0.133
0.182
0.144
Collection Date: 05/11/2012 08:00
Received Date: 05/12/2012 10:00
Matrix: Water
LOQ/CL
1.00
1.00
1.00
1.00
1.00
2.00
1.00
64.0-140
85.0-115
82.0-117
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DF
1
1
1
1
1
1
1
Prep Balch: VXX3304
Prep Method: SW-846 5030E
Prep Date:Time: 05/ 1412012 00:00
Prep Intel Wt.JVol.: 40 mL
Prep Extract Vol: 40 mL
5500 Business Drive, Wilmington, NC 28405
t 910.350.1903 f 910.350.1557 w'W.us.sgs.com
Date Analyzed
05/14/2012 12:06
05/14/2012 12:06
05/14/2012 12:06
05/14/2012 12:06
05/14/2012 12:06
05/14/2012 12:06
05/14/2012 12:06
05/14/2012 12:06
05/14/2012 12:06
05/14/2012 12:06
Memberaf5G5 Group
Page 4 of 11

Results of Outfall
Client Sample ID: Outfall
Client Project ID: 140 West
Lab Sample ID: 31201469002-A
Lab Project ID: 31201469
Results by SW-846 8260B
Parameter
1,2-Dichloroethane
Benzene
Ethyl Benzene
Naphthalene
Toluene
Xylene (total)
tert-Butyl methyl ether (MTBE)
Surrogates
1,2-Dichloroethane-d4
4-Bromofluorobenzene
Toluene d8
Batch Information
Result
ND
ND
ND
ND
ND
ND
ND
98.0
100
103
ticai La, ... 1.00622 10
Anaiyt cal Method: SW-846 8260E
Instrument iy1SO4
Analyst: DVC
Anaivt cai vaterT me: 05/14/2012 11:42
Print Date C•,-:. .
Collection Date: 05/11/2012 08:00
Received Date: 05/12/2012 10:00
Matrix: Water
Qual DL LOQ/CL Units DF Date Analyzed
U 0.167 1.00 ug/L 1 05/14/2012 11:42
U 0.113 1.00 ug/L 1 05/14/2012 11:42
U 0.0877 1.00 ug/L 1 05/14/2012 11:42
U 0.0855 1.00 ug/L 1 05/14/2012 11:42
U 0.133 1.00 ug/L 1 05/14/2012 11:42
U 0.182 2.00 ug/L 1 05/14/2012 11:42
U 0.144 1.00 ug/L 1 05/14/2012 11:42
64.0-140 % 1 05/14/2012 11:42
85.0-115 % 1 05/14/2012 11:42
82.0-117 % 1 05/14/2012 11:42
Prep Batch VXX3304
Prep Method: SW-846 5030E
Prep DatefTime: 05/14/2012 08:00
Prep Initial `. i./Von.. 40 rnt-
Prep Extras Voi. 40 mt.
5500 Business Drive, Wilmington, NC 28405
t 910.350.1903 f 910.350.1557 www.us.sgs.com
N C Certification 4 481
Member of SG5 Group
Page 5 of 11

,.- Batch Summary
Analytical Method: SW-846 8260E
Client Sample ID
LCS for HBN 23580 [VXX/3304]
LCSD for HBN 23580 [V=3304]
MB for HBN 23580 [VXX/3304]
Outfall
Intake
Intake(71481DUP)
SW-03(71401 MS)
Prep Method: SW-846 5030E
Prep Batch: VXX3304
Prep Date: 05/14/2012 08:19
Lab Sample ID Analysis Date
71497 05/14/2012 09:17
71498 05/14/2012 09:41
71499 05/14/2012 10:53
31201469002 05/14/2012 11:42
31201469001 05/14/2012 12:06
71783 05/14/2012 19:42
71784 05/14/2012 20:06
5500 Business Drive, Wilmington, NC 2&105
't 910.350.1903 f 910.350.1557 www.us.sgs.com
Analytical Batch
VMS2210
VMS2210
VMS2210
VMS2210
VMS2210
VMS2210
VMS2210
Instrument Ana st
MSD4 DVO
MSD4 DVO
MSD4 DVO
MSD4 DVO
MSD4 DVO
MSD4 DVO
MSD4 DVO
Member of SGS Group
.121
Page 6 of 11

,--- Method Blank
Blank ID: MB for HBN 23580 [VXX/3304]
Blank Lab ID: 71499
QC for Samples:
31201469001, 31201469002
... Results by SW-846 8260B
Matrix: Water
Parameter Result gL._ial DL LOQ/CL Units DF
tert-Butyl methyl ether (MTBE) ND U 0.144 1.00 ug/L 1
Benzene ND U 0.113 1.00 ug/L 1
1,2-Dichloroethane ND U 0.167 1.00 ug/L 1
Toluene ND U 0.133 1.00 ug/L 1
Ethyl Benzene ND U 0.0877 1.00 ug/L 1
Xylene (total) ND U 0.182 2.00 ug/L 1
Naphthalene ND U 0.0855 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 98.0 64.0-140 % 1
Toluene d8 102 82.0-117 % 1
4-Bromofluorobenzene 101 85.0-115 % 1
Batch Information
•,strumentD4
Analysii
8/14/2012 10:53:00Atvl
Prep Batch VXX3304
Prep Method: SW-845 5039B
Prep Dale/Time: 5/14/2012 8:19:48AM
Prep initial Wt.Nol.: 40 mL
Prep Extract Vol40 mt..
5500 Business Drive, Wilmington, NC 28405
t 910350.1903f 910.3501557 inAv.us.qsnm
Member of SGS Group
Page 7 of 1 1

-• Blank Spike Summary
Blank Spike ID: LCS for HBN 23580 [VXX/3304]
Blank Spike Lab ID: 71497
Date Analyzed: 05/14/2012 09:17
QC for Samples: 31201469001, 31201469002
Results by SW-846 8260E
Parameter
tent -Butyl methyl ether (MTBE)
Benzene
1,2-Dichloroethane
Toluene
Ethyl Benzene
Naphthalene
Surrogates
1,2-Dichloroethane-d4
Toluene d8
4-Bromofluorobenzene
Batch Information
Ens..
Spike Duplicate ID: LCSD for HBN 23580 [VXX/3304]
Spike Duplicate Lab ID: 71498
Date Analyzed: 05/14/2012 09:41
Matrix: Water
Blank Spike (ug/L) Spike Duplicate (ug/L)
Saike Result Rec (%), S ike Result Rec (%) CL RPD (%) RPD CL
5.00 4.56 91 5.00 4.69 94 47.0-142 2.8 30.00
5.00 4.90 98 5.00 5.00 100 75.0.124 2.0 30.00
5.00 4.47 89 5.00 4.64 93 76.0-119 3.7 30.00
5.00 3 101 5.00 5.06 101 75.0-123 0.0 30.00
5 00 4 77 95 5.00 4.74 95 76.0-123, 0.63 30.00
5.00 4.73 95 5.00 4.78 96 07.0- ` 1.1 30.00
VMS2210
:::;thoc: SW-846 32606
gfSO4
99 100 :i4.0-140
103 103 82.0-117
101 102 35.0-1 15
Prep Batch: VXX3304
Prep Method: SW-846 5030E
Ptep Dale/Time: 05/14/2012 08:18
Spike trait `MJVol.: 40 mL Extract Vol: 40 mL
Dupe 'nit Wt.fVol.: 40 mt. Extract \/oi: 40 mL
5500 Business Drive, Wilmington, NC 28405
t 910.350.1903.f 910.350.1557 www.us.sgs.com
N.C. Certitir atien tF 481'
Member of SGS Group
Page 8 of 11

Duplicate Sample Summary
Original Sample ID: 31201469001-A
Duplicate Sample ID: 71783
QC for Samples: 31201469001, 31201469002
Analysis Date: 05/14/2012 12:06
Analysis Date: 05/14/2012 19:42
Matrix: Water
Results by SW-846 8260B
PARAMETER Original (uq/L) Qual Duplicate (uq/L) Qual RPD (%) RPD CL
1.2-Dichloroethane ND U ND 30.00
Benzene 3.11 3.01 3.3 30.00
Ethyl Benzene 0.690 J 0.670 J 2.9 30.00
Naphthalene 0.440 J 0.460 J 4.4 30.00
tert-Butyl methyl ether (MTBE) 18.5 18.0 2.7 30.00
Toluene 0.390 J 0.400 J 2.5 30.00
Xylene (total) 1.88 J 1.76 J 6.6 30.00
Surrogates
1,2-Dichloroethane-d4 98.0 99.0 0.68
4-Bromofluorobenzene 101 102 0.99
Toluene d8 101 100 1.3
Batch Information
1p:162210 Prep Batch: VXX3304
od: SW-846 8260B Prep Method SW-846 5030B
Prep Date/TiMe! 05/14/2012 08:00
N.C. Certification # 481
5500 Business Drive. Wilmington, NC 28405
t 910.350.1903 f 910.350.1557 vivew.us.sgs.com
Member of 5G5 Group
Page 9 of11

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Page 10 of 11

SGS North America Inc.
Sample Receipt Checklist (SRC)
Client Ammons Resource Group Work Order No.: 31201469
1. X Shipped Notes:
Hand Delivered
2. X COC Present on Receipt
No COC
Additional Transmittal Forms
3. Custody Tape on Container
X No Custody Tape
4. X Samples Intact
Samples Broken / Leaking
5. X Chilled on Receipt Actual Temp.(s) in °C: 5.9
Ambient on Receipt
Walk-in on Ice; Coming down to temp.
Received Outside of Temperature Specifications
6. X Sufficient Sample Submitted
Insufficient Sample Submitted
7. Chlorine absent
HNO3 < 2
HCL<2
Additional Preservatives verified (see notes)
8. X Received Within Holding Time
Not Received Within Holding Time
9. X No Discrepancies Noted
Discrepancies Noted
NCDENR notified of Descrepancies'
10. X No Headspace present in VOC vials
Headspace present in VOC vials >6mm
Comments:
Inspected and Logged in by: JJ
Date: Sat 5f12/12 00:00
'NCDENR must be notified when collection, holding time or preservation requirements are not met. MI 11.6
Page 11 of 11