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HomeMy WebLinkAboutWQ0010528_Residual Annual Report 2020_20210224Ramseur Where Family and Friends Peet TOWN OF RAMSEUR 2020 Annual Sludge Disposal Report PERMITTEE / PREPARER Town of Ramseur Vicki Caudle P.O. Box 545 724 Liberty St. Ramseur, NC 27316 336-824-8530 Terry Lewallen 336-824-3939 t.lewallenG,town oframseur.ora NCDENR DWR Water Quality Permit Section Non -Discharge Permitting Unit Information Processing Unit 6th Floor, Division of Water Resources 1617 Mail Service Center Raleigh, NC 27699-1617 The Town of Ramseur surface disposed of 3.79 dry tons of water and wastewater plant sludge in 2020. Ramseur used lime stabilization to meet pathogen reduction and vector attraction requirements. The facility was compliant during the past calendar year with all conditions of the land application permit issued by the Division of Water Resources. The 2020 Annual Sludge Disposal Report for the Town of Ramseur is attached. It includes the following: • CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM • WWTP ANNUAL RESIDUAL SAMPLING SUMMARY FORM • Environment 1 Lab Results & Associated Data/Forms • SGS North America Lab Results & Associated Data/Forms • WTP ANNUAL RESIDUAL SAMPLING SUMMARY FORM • Environment 1 Lab Results & Associated Data/Forms • SGS North America Lab Results & Associated Data/Forms • ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) • WWTP Lime Log Sheet • WTP Sludge Disposal Record • WTP Vehicle Inspection Forms CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM` WQ PERMIT #: WQ0010528 FACILITY NAME: Town of Ramseur PHONE: 336-824-3939 COUNTY: Randolph OPERATOR: Town of Ramseur FACILITY TYPE (please check one): (] Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) Distribution and Marketing (complete Parts A, B, and C) Was the facilitv in operation during the past calendar year? Yes 0 No Q —► If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January February WWTP - NCO026565 0.015 0.11 0.125 March April VIay tune Iuly August September October WTP - NCG590019 3.68 3.68 November December Total from FORM DMSDF (sup) .................... totals: Annual (dry tons): 0.015 3.79 3.805 0 Amendment(s) used: Lime Bulking Agent(s) used: If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) Part C: Facility was compliant during the past calendar year with all conditions of the land application permit ,r] Yes ;including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No 0, If No, Explain in Narritive t. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. >_. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. No contravention of Ground Water Quality Standards occurred at a monitoring well. 'I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant )enalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Date Signature f Preparer (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) Z-tl-Zl Date DENR FORM DMSDF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0010528 Laboratory: 1) Environment 1 Facility Name: Town of Ramseur 2) SGS North America Residual Source WQ # or NCO026565 3) NPDES #: 4) WWTP Name: Ramseur WWTP 5) Parameter (mg/kg) Ceiling Cone. Limit Sample or Composite Date 12/10/202 0 Percent Solids (%) NA 0.66 Arsenic 46 <2.5 pH NA 6.3 Copper NA Chromium 300 13 Lead NA Mercury NA Molybdenum NA Nickel 320 14 Selenium NA Zinc NA Total Phosphorus NA TKN NA Ammonia -Nitrogen NA Nitrate and Nitrite NA a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reterence the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Pre arer *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Z -ls- 7—d Date DENR FORM RSSF (12/2006) t flm60 114 0AKM0,'RrbR—fVC:;—` GREENVILLE, N.C. 27858 RPMSMUR MWTP- SLUDGE 7.24. LIBERTY STREET PO BOX 515 'RAMSUER MC 273'16' PARAN MER$ P11, Units. Arsenic (dry- wt.. basjs,�, -mg/kg Chromium, T,(dry wt. basis),mg/kg Nickel (dry wt, basis), mg/kg Total Solids,. % Sludge Analysis M6tbod Sample Date Analyst Cod I e 6.3 12/15/20 TMR 4500HB-11 <24 .12128(20- NAB 311313-44 13 12/11/20, LFJ E M200.1- 14 I2/23/20 LFJ EPA2.00.7 .0.66 12I15/20 T?MM 2540G41 FAX (252) 756-0633 ZD#z 96$ DATE COLLECTEM 12/10/20: DATE REPORTED i 01/08/21 REVIEWED BY. -A - yNIi9 T-L....,. -. . 1 J 1 Environnient 1, Inc. on PnY 7r1RS 11A 0nkmnnt Dr_ CEIAIN OF CUSTODY RECORD Page 1 of I Greenville. NC 27855 environmentline.com CHLORINE NEUTAALIZEDATCOLLECTION DISINFECTIUNT Phone (252} 756-620b - Fax (252) 756-0633 CHLORINE Ij CLIF,�iT: 965 Week: & pHCHECK (LAB) _ UV Lj :UEZ WATER (RAMSEUR WWTP-SLUDGE) L) NONE p p p p p p G G G G COWAINERTYPE, PIG TADINTE BLACKWELL '.O. BOX 1279 CHEMICAL PRESERVATION ;LEMMONS NC 27012 A A A A A A A A A A. r A -NONE D-NACH z 336) 766-0270 B-NNU; E HCL Q o z o v' y a x C-HzSO, F -ZINC ACETATE/NAOH COLLECTION o w 7 G-NATHIOSULFATE a °" so .o L) U F v E SAMPLE LOCATION DATE TIME q o ¢ 7 .. ..,, _.,.., CLASSIFICATION: Sludge Sample l /b -2b (6oD /F 7. ,. lyVASTEINIATER (NPDES) DRINKING :HATER I i CWNGW ( I SOLID WASTE SECTION I CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENTIDELIVERY O N SAMPLES COLLECTED BY: (Pease Print) L %. SAMPLES R ENED IN LAB AT `O R i• } SIi B SIG.} (SAb,IPLER) DATEEMME RECEIVED Y (SIG.} t)aATF{tltitE COMMENTS: .�?z- a "I 2�5 RELINQJ HEDBY(SIG.) DATr1TINIE j5 RE Y{SIG.) DATE/TIME `?— = ! to /z_o 3 3 — DATEIRME RELINCXlI.SHt`D BY (SIC,) DATEiTIME RECEIVED BY (Si Sampler must place a `�C" for composite sample or a `G" for PLEASE READ Instructions for completing this farm an the reaerse side. Grab sample in the blocks above for each parameter requested. [ 0 375221 FORM n3 _ f The results set forth herein are provided by SGS North Alneri.ca Inc. e-Hardeopy 2. 0 Automated Repoi-t echii'KlRe 0 or x Environment 1, Inc Suez Water (Ramseur WWTP-Sludge); Clemmons, NC 965 SGS Job Number: FAS1677 Sampling Date: 12/ 10/20 Report to: Environment 1, Inc PO Box 7085 Greenville. NC 27835 1 inc. corn TTN: Ann Brown Total number of pages in report: 14 e- Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Norm Farmer Technical Director Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407425-0707 SGS is the sole authotity for authorizing edits or modifications to this document, Please share your, ideas about Unauthorized ntadificution of this report is strictly prohibited, how we ctut serve you better at: _G, ttavicw stanJard ternts,rt: http;�%+v+vwscs.cont/enitems-and-cunditirnts GIiS.US.CustuntcrC;ut u,�gs.com 1 of 14 FA61677 Table ®f Contents Sections: Section1: Sample Summary ................................................................................................... 3 Section 2: Summary of Hits 4 .................................................................................................... Section3: Sample Results 5 ........................................................................................................ 3.1: FA81677-1: SLUDGE SAMPLE.................................................................................. 6 Section4: Misc. Forms............................................................................................................ 12 4.1: Chain of Custody........................................................................................................... 13 2of14 Fa81677 SOS North America Inc. Sample Summary Environment 1, Inc Job No: FA81677 Suez Water (Ramseur WWTP-Sludge); Clernmons, NC Project No: 965 .... �. t I .. A . , ; , .-.� , : �. Sample Coll•ected Matrix client Number Date Time By Received Code Type Sample ID Atot -w L- Organics ND = Not detected above the MDL FA8 12/1W20 10:00 TL 12/12/20 SO Sludge SLUDGES AMPL Soil samples reported on a dry weight basis unless otherwise indicated on result page, 8,- 3 of 14 FA61677 Summary of Bits Page 1 of 1 Job Number: FA81677 Account: Environment 1, Inc Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC Collected: 12/10/20 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FAS1677-1 SLUDGE SAMPLE Corrosivity as pH Tgnitability (Flashpoint) ° Chromium 0;`6:';?''.?'!,•i.;.;';+ 0.10 (a) Not ignitable, su SW846 CHAP7 Deg. F SW846 1010A MOD mg/l SW846 6010D a of '1 a Gt_. FA61677 t.''tf•� .j :! J t fr",,_ }���� ,{�"yh p�r K '� fin' ��A SG$--4 1 r� y4,}{� �,,�r�' ,e '.s;, '? �'�'i� i�'4s�rvv�� 7 ` S y�p'�1(13��9 { F fI..... JryYfrY A, Orlando, Section 3 e,. Same ' X: R s' Report of Analysis 5of14 FA61677 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA81677-1 Date Sampled: 12/10/20 Matrix: SO - Sludge Date Received: 12/12/20 Method: SW846 8260B SW846 1311 Percent Solids: 0.7 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 5E26306.D 10 12/28/20 14:15 SO 12/14/20 13:50 OP83357 V5E1211 Run #2 Purge Volume .un #1 5.0 ml .un #2 VOA TCLP List CAS No. Compound Result HW# MCL RL 71-43-2 Benzene ND; ; ' ::;;` ? DO18 0.50 0.010. 78-93-3 2-Butanone (MEK) D035 200 0.050 56-23-5 Carbon Tetrachloride ND.'•:r:}':'!;; , D019 0.50 0.010 108-90-7 ChlorobenzeneD.;;'-?i':y:;' D021 100 0.010 67-66-3 Chloroform ND `:;: ;:;; `:'c`r:;`.`" D022 6.0 0.010 106-46-7 1,4-Dichlorobenzene D027 7.5 0.010 107-06-2 1,2-Dichloroethane D028 0.50 0.010 75-35-4 1,1-Dichloroethylene D029 0.70 0.010 127-18-4 Tetrachloroethylene D039 0,70 0.010 79-01-6 Trichloroethylene NZ3;;';;D040 0.50. 0.010 7S-01-4 Vinyl Chloride 'NI};':::';',;i%``':';i:?D043 0.20 0.010 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 1868-53-7 Dibromofluoromethane 9.7%':'.•!;',. 83-118% 17060-07-0 1,2-Dichloroethane-D4 16'6/1— ";'( 79-125% 2037-26-5 Toluene-D8,14%:°:r 85-1120/c 460-00-4 4-Bromofluorobenzene 1a4%;',;;.`•i';. 83-1180/c (a) Outside control limits; however, sample is ND. TCLP Leachate method SW846 1311 MDL Units Q 0,0031 mg/1 0.020 mg/1 0.0036 mg/l 0.0020 mg/l 0.0030 mg/1 0.0026 mg/1 0,0031 mg/l 0.0032 mg/1 0.0022 mg/1 0.0035 mg/l 0.0041 mg/! ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/ 1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6of14 FA81677 SGS North America Inc. Report of Analysis Page 1 of I Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA81677-1 Date Sampled: 12/10/20 Matrix: SO - Sludge Date Received: 12/12/20 Method: SW846 8270D SW846 3510C Percent Solids: 0.7 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC File ID DF AnaIyzed By Prep Date Prep Batch Analytical Batch Run #1 X073996.1) 1 12/24/20 20:20 NJ 12/24/20 12:00 OP83512 SX3015 Run #2 Initial Volume Final Volume ,un # 1 100 ml 1.0 ml .un #2 ABN TCLP List CAS No. Compound 95-48-7 2-Methylphenol 3 &4-Methylphenol 87-86-5 Pentachlorophenol 95-95-4 2,4,5-Trichlorophenol 88-06-2 2,4,6-Trichlorophenol 106-46-7 1,4-Dichlorobenzene 121-14-2 2,4-Dinitrotoluene 118-74-1 Hexachlorobenzene 87-68-3 Hexacblorobutadiene 67-72-1 Hexachloroethane 98-95-3 Nitrobenzene 110-86-1 Pyridine CAS No. Surrogate Recoveries 367-12-4 2-Fluorophenol 4165-62-2 Phenol-d5 118-79-6 2,4,6-Tribromophenol 4165-60-0 Nitrobenzene-d5 321-60-8 2-Fluorobiphenyl 1718-51-0 Terphenyl-d14 TCLP Leachate method SW846 1311 Result HW# MCL RL MDL Units Q ND.;!:`:;:;` : ;!.`,;:, D023 200 0.050 0.0056 mg/1 D024 200 0.050 0.0098 mg/1 D037 100 0.25 0.050 mg/l D041 400 0.050 0.0074 mg/1 -:, D042 2.0 0.050 0,0075 mg/1 D027 7.5 0.050 0.0050 mg/1 D030 0.13 0.050 0.0081 mg/1 D032 0.13 0.050 0.0069 mg/1 D033 0,50 0.050 0.0050 mg/I D034 3.0 0.050. 0.016 mg/I D036 2.0 0.050 0.0093 mg/l D038 5.0 0.10 0.020 mg/1 Run# 1 Run# 2 Limits 54:°Los;;:`;:,. ' 14-67% 149 12%.,'ir: f:':;'.•;:`; 42-108% 69. 40 39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7of14 Faois77 SGS North America Inc. Report of Analysis Page I of 1 s Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA81677-1 Date Sampled: 12/10/20 Matrix: SO - Sludge Date Received: 12/12/20 Method: SW846 8151A SW846 3510C Percent Solids: 0.7 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC072216.1) 1 12/16/20 16:09 JA 12/15/20 09:45 OP83385 GCC1775 Run #2 Initial Volume Final Volume Run #1 10.0 ml 5.0 ml Run #2 Herbicide TCLP List CAS No. Compound 94-75-7 2,4-D 93-72-1 2,4,5-TP (Silvex) CAS No. Surrogate Recoveries 19719-28-9 2,4-DCAA Result HW# MCL RL ND.'ji`:;i:;;;;D016 10 0.050 ND• i. %`.1-:'! D017 1.0 0.0050 Run# 1 Run# 2 Limits 39-135% TCLP Leachate method SW846 1311 MDL Units Q 0.017 mg/l 0.0013 mg/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of '14 FAM77 SGS North America Inc. Page 1 of I s Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA81677-1 Date Sampled: 12/10/20 Matrix: SO - Sludge Date Received: 12/12/20 Method: SW846 8081B SW846 3510C Percent Solids: 0.7 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 ST150573.1) 1 12/15/20 18:48 WH 12/15/20 09:30 OP83384 GST3630 Run #2 Report of Analysis Initial Volume Final Volume Run #1 100 ml 5.0 ml Run #2 Pesticide TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindane) l�?D{'.'::::.::;?: s`:`I)013 0.40 0.00010 0.000022 mg/t 12789-03-6 Chlordane '...'.. D020 0.030 0.0010 0.00038 mg/1 72-20-8 Endrin :; :':!;,< ` D012 0.020 0.00020 0,000021 mg/l 76-44-8 Heptachlor ND,: ' :`',,' ;r; ? •': D031 0.0080 0.00010 0.000026 mg/1 1024-57-3 Heptachlor epoxide ND;;:,:;;.!';, ,: D031 0.0080 0.00014 0.000020 mg/1 72-43-5 Methoxychior ND:`;';;;' `':; ;';i D014 10 0.00020 0.000050 mg/l 8001-35-2 Toxaphene ND, `: D015 0.50 0.0050 0.0021 mg/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 69%,:;.;1+;:;; 42-127% 2051-24-3 Decachlorobiphenyl 92%q"....''.:..i 27-127% (a) Associated BS outside of control limits high, sample was N.D. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/l/ 11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9of14 FAM77 SGS North America Inc, Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA81677-1 Date Sampled: 12/10/20 Matrix: SO - Sludge Date Received: 12/12/20 Percent Solids: 0.7 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC Page 1 of 1 3 Metals Analysis, TCLP Leachate SW8461311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic ; <•Q:;10 • !; ::''' D004 5.0 0.10 mg/l 1 12/18/20 12/18/20 LM SW846 6010D 2 SW846 301OA 4 Barium ,2;0„: `,;} ;. ; D005 100 2.0 mg/l 1 12/18/20 12/18/20 LM SW846 6010D 2 SW846 3010A 4 Cadmium <,0,;0.50.,'.;; D006 1.0 0.050 mg/1 1 12/18/20 12/18/20 LM SW846 6010D 2 SW846 3010A 4 Chromium O66,` a;'.?`!;; : D007 5.0 0.10 mg/1 1 12/18/20 12/18/20 LM SW846 6010D 2 SW846 3010A 4 Lead 0',050,!; ::':,` D008 5.0 0.050 mg/1 1 12/18/20 12/18/20 LM SW846 601OD 2 SW846 3010A 4 Mercury :;''<Q;00$t];`', D009 0.20 0.0050 mg/1 1 12/15/20 12/15/20 JC SW8467470A 1 SW8467470A3 Selenium <Q 1;0' <`:; ; DO10 1.0 0.10 mg/1 1 12/18/20 12/19/20 LM SW846 6010D 2 SW846 3010A 4 Silver ;<OIO.,i.'?:;':•:', DO11 5,0 0.10 mg/1 1 12/18/20 12/18/20 LM SW846 6010D 2 SW846 3010A 4 (1) Instrument QC Batch: MA17315 (2) Instrument QC Batch: MA17322 (3) Prep QC Batch: MP38286 (4) Prep QC Batch: MP38301 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) 10 of 14 FA81677 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA81677-1 Date Sampled: 12/10/20 Matrix: SO - Sludge Date Received: 12/12/20 Percent Solids: 0.7 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC Page 1 of 1 General Chemistry Analyte Result RL Units DF Analyzed By Method Corrosivity as pH su 1 12/21/20 16:40 )B SW846 CHAP? Cyanide Reactivity <210 >. `?;:, .,': 210 mg/kg 1 01/04/21 12:16 AC SW946 CEIAP7 Ignitability (Flashpoint) a >:200.`.';,`•; i`:;:'_•': Deg.F 1 12/23/2007:23 CS SW846 10)0A MOD Solids, Percent 0; 7,;':':;'; ; : `:'':; ::; ;:' % 1 12/15/20 09:11 KSA SM 19 25400 Sulfide Reactivity <'.71-00.%.:`:`r`.'`::;,:7100 mg/kg 1 12/29/2010:03 7C SW846CHAP7 (a) Not ignitable. RL = Reporting Limit - sag,- 11 of 14 FA81677 t•�„�;:i;.t;:kf I,ir a.'`� It a •S'4k1 ��� JY/ x ��.%tl�� j� TTi' ... , s -19 Y,w� V � �u ns, tah 9,Y'� e - ✓ ¢!i'T� Section 4 11!I1ScTOTTTISJ Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody 12 of 14 FAM77 Environment 1,Inc. P.O. Box 7085, 114 Oakmont Dr. Greenvtitn. NC 27RSR CHAIN OF CUSTODY RECORD A $'Mine 1 of i mvirommenU irtc.com :hone (252)72-6208 • Fax (232)'756.0633 CLIENT: 965 Week:s UEZ WATER (RAMSEUR WWTP"SLUDGlt3 iADTNEBLACKWELL .0. BOX 1279 ILEMMONS NC 27012 536) 766-0270 COLLECTION DIS1Ni•'SCTION ❑ CHLORINE uv ❑ NONB ❑ CHLORNENEUTRALIZED ATCOLLECTIQN pHCHECKPB) P P P P P P G. G ': G G COMAINERTYPE,PlG A A A A A A A A. 1 A A CHEM CALPRESERVAiION Y A -NONE D-NAOH S-HNO, E-HCL F - ZINC ACETATE/NAOH G-NATHICSULFATE q• E ur ? U 4 9 :� ¢" a V y F v F Fr SAMPLELOCATION DATE TIME Sludge Sample 1 "Cif b •?D (bDo P 7.,1 7 L CtASSIRCATION: ❑ WASTEWATER(NPDES) ❑ ORINKINGWAMA ❑ GW M SOLIDWASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING_ S�IIPMENTIOELIYERY Y N " } SAMPLESCOU.£CTEDBY: (pk?!s PM, y '~ t✓a! �L� ,i SAMPLES R EIVEDINLASAT -P°C R St) 8 SIG) (SAIAPLEA)) Al'L'� yDATEITIME I REGWED Y (SIG.) �"�1.. -112 DATEMME bo 124 1iJ COMMENTS: y AEJ D'0($IG.) DAIFITIME i .Rfi Isla) � DATSTIME E� 3- REiI ,►1r, t.l r9 EA E ftFA 1 sti t "' s I co tetlhg tli'is form ''the reverse side.. niktler must place a "C'tor composite sample or a "G"for i F Grab sample In the blocks above for each parameter requested, N2 375221 FA81677: Chain of Custody Fate 1 of 2 13 of 14 FA91677 SGS Sample Receipt Summary Jodi Number: FA81677 Client: ENVIRONMENT 1, INC Project: SUFZ WATER (RAMSEUR WWTP-SLUDGE) Date I Time Received: 12/12/2020 10:25:00 AM DeliveryMathod: FEDEX Airbill Vs: 923153814283 Therm ID: IR 1; Therm CF: 0.2; # of Coolers: 1 Cooler Temps (Raw Measured) *C., Cooler 1: (1,6); Cooler Temps (Corrected) °C: Cooler 1t (1.8); A :a CoolerInformation Y or N Samole Information Y or N -NLA_ 1. Custody Seals Present ❑ 1. Sample labels present on bottles R ❑ 2. Custody Seals Intact ❑ 2. Samples preserved properly R ❑ 3. Temp criterle achieved 0 ❑ 3. Sufficient volumelco'Mainers recvd for analysis: 0 ❑ 4. Cooler temp verification jR Gun 4. Condition of sample 5. Cooler media Ica (Ban) S. Sample recvd within HT ❑ 6, Datesfrimes/lDs on CDC match Sample Label R ❑ Trip Blank Information Y or N NfA 7. VOCs have headapace ❑ ❑ []i 1, Trip Blank present! cooler ❑ ® ❑ 8. Bottles received for unspecified tests ❑ 8 2. Trip Blank listed on CDC ❑ ® ❑ 9, Composlting Instructions clear ❑ ❑ W or S NfA 10. Voa Solt KltsMars received past 48hrs? ❑ ❑ R 11. % Solids Jar received? ❑ ❑ 3, Type Of TS Received ❑ ❑ ® 12. Residual Chlorine Present? ❑ ❑ MIsc. Information Number of Encores: 25•Gram 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals: Test Strip Lot #s: pH 0-3 230315 pH 10-12 219813A Other. (Specify) Residual Chlorine Test Strip Lot #: Comments SM001 Technician: KYRASA Date: 12/12/202010:25:00 Reviewer. Date: Rov, safe a524117 FA81677: Chain of Custody Page 2 of 2 14 of 14 __. - FA81677 ANNUAL RESIDUAL SAMPLING SUMMARY FORM ' Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0010528 Laboratory: 1) Environment 1 Facility Name: Town of Ramseur 2) SGS Accutest Residual Source WQ # or NCG590019 3) NPDES #: 4) WWTP Name: Ramseur Water Treatment Plant 5) 77 ,...:.1__,_I A.... 1-, : TA-4- Parameter (mg/kg) Ceiling Cone. Limit Sample or Composite Date 10/28/202 0 Percent Solids (%) NA 2.54 Arsenic 46 <2.5 pH NA 4.9 Copper NA Chromium 300 10 Lead NA Mercury NA Molybdenum NA Nickel 320 50 Selenium NA Zinc NA Total Phosphorus NA TKN NA Ammonia -Nitrogen NA Nitrate and Nitrite NA a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature old Pre -parer * 7, -11-Z 1 Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) [��norra�c��� 90 ��c�op�op�at�dl i ` r' Slk�-c�-� GREENVUE, N <C, 27858 F-AMSEUR WTP-SLUDGE 724 LIBERTY STREET 'PO BOX. 5 4 5 RMSEUR,NC 2731.6. PARAMETERS PH, Units Arsenic (dry wt. basis), mgft.. Chromium, T.{dry wt.. basis),-xng/kg Nickel (dry Nvt. basis),ing/hg Total Solidsi % Sludge Analysts Method Sample Date Analyst Code 4.9 11t03110 IDS 450OBB-11 <2.5 11/16120 X-1TM. 3113B-04 10: 11/12/20 LFJ '3113B-04 so. 11112/20 LFJ EPA752O' 154 11102/2-0 TMR 2540G-11 756-0633 ID# , 950 DATE QQLLECTEDz 1'0/28/20 D= RZPQRTED .71/30/20 REVIEWED, BY: z", ,vironment 1, Inc. CHAIN OF CUSTOg7Y R ECO7 . Box. 7085, 1.14 Oakmont Dr. r T a T Page 1 of. I �fi]v111C.1�!\. GlPJO vironn-ientl inc.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION .one (252) 756-6208 4 Fax (252) 756-0633 (� CHLORINE I'"� ' — qS 0 Week: $ LJENT: pH CHECK (LAB) 410EE; UV LA (RAMSEUR WTP-SLUDGE) NONE P P P P P P G G G G G CONTAINER TYPE, PiG VNE BLACKWELL h� CHEMLCALPRESERVAII(AV . BOX 1279 i;MKONS NC 27"012 A A A A A A A A A A: A A -NONE D-NAOH G 766-0170 t✓ ac z' H C B HNC3 E - HCL 0cc c> Q w ¢ x z C - H SQ, F -ZING ACEfATE/NAOH COLLECTION CJ 4 ¢ ...i o n G-NATHIOSULFATE ¢ o tR a_ t=• �` o N� :° T� E+ F t� E- ci )AMPLE LOCATION DATE 1IME lu a Sample ag p %� 8 ,.v....... '� , � CLASSIFICATION. VIASTEWATER (NPDES) DRINKJNGWATER DININGW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURINGEN IYDELIVERY N SAMPLES COLLECTED BY (Please Print) SAMPLES REMVED IN LAB AT,_ °C LINQUISHED (5' ;) (SAM?LE8) bAWR M E RECEIVED Y (SI .) j DATEfi1ME� COMMENTS: Vit Z, aS LINQUI D BY (Sly.) i DATI=MME t)a RE ' D BY (S( . DATt MME w1 7 if r cg , � " /036 LINQUISHED15Y(SIG.) DATEMME RECEI` (SIC DA`TEliltfE, Sampler most place a "C" for composite sample or a V for PLEASE READ Instructions for completing this form on the reverse side. a�n 5 Grab sample in the blocks above for each parameter requested. N Q 375237 The results set faith herein are provided by SGS North America Inc, e—Htlydcopy 2. Auloinated Report eC 1t . ,e off.' . T brie.. R..........%z::'.:,::'.,`. Environment 1, Inc Suez Water (Ramseur WWTP-Sludge); Clemmons, NC 950 SGS Job Number: FA80347 Sampling Date: 10/28/20 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environmentline.com ATTN: Ann Brown Total number of pages in report: 14 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Norm Farmer Technical Director Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327),1L(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, TA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc, - 4405 Vineland Road - Suite C-15 - Orlando, FL 32811 - tel: 407.425-6700 • fax: 407-425-0707 SGS is the sole authority (.or alithod7in- edits or modifieatiom to this ducum(,mc, Please share your ideas about _ - t.Mauthorind modification of this report is strictly prohihitocl, liow the can serve you better at: Review slundardtetraslit: 13ttp:'•'t�ntysgs.cutnleni[crtns-nnd-conditions EItS.[1S.CustumetCareust .cum 1 of 14 FA80347 Table of Contents > -1- Section1: Sample Summary................................................................................................... Section2: Summary of Hits.................................................................................................... Section3: Sample Results........................................................................................................ 3.1: FA80347-1: SLUDGE SAMPLE.................................................................................. Section4: Misc. Forms............................................................................................................ 4.1: Chain of Custody........................................................................................................... Sections: 3 4 5 6 12 13 2of14 FA80347 dk StS North America Inc. Sample Summary Environment 1, Inc Job No: FA80347 Suez Water (Ramseur WWTP-Sludge); Clemmons, NC Project No: 950 Sample toilec:,ted: Matrix Client Number Date Time By Received Code Type Sample ID Organics ND = Not detected above the MDL FA803477110/28/20 10:30 TL 10/.31/20 SO Sludge SLUDGE SAMPLE Soil samples reported on a dry weight basis unless otherwise indicated on result page. I 3 of 14 FA80347 Summary of Hits Page I of 1 Job Number: FA80347 Account: Environment 1, Inc Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC Collected: 10/28/20 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA80347-I. SLUDGE SAMPLE Corrosivity as pH b.1 ; ',:.,,;'..;'::'::`:; su Ignitability (Flashpoint) a > 200 ::`:' Deg. F (a) Not ignitable. SW846 CHAP? SW846 1010A MOD L 4of14 FAC0347 t , i t 4 q.. �•ia t°"i'. ���c°,fa tr��'r 4f�•j�� , n. t '' '•'' i . •.�� tl � 4'�� ti �{� i�i Yy✓ryy � �.,�nfs . :.:..........¢,;.q,�u,;p..,;Y, ) ASf9 y y�ME 7m .. i._._• Q� , t i t�dti'L Ka i ` i k+, , 'i'+`t't'�.5•* "!'7 OdOdoy,F�.�,�,tit Section 3 �Sam•'�1e.`Resu�Its �:��� � � � �>�+;` Report of Analysis nJPY!:. 4 � 5of14 FAS0347 SGS North America Inc. Report of Analysis Page I of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA80347-1 Date Sampled: 10/28/20 Matrix: SO - Sludge Date Received: 10/31/20 Method: SW846 8260B IN HOUSE Percent Solids: 3.5 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC Pile ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 5E25249.D 10 11/05/20 15:44 SO 11/03/20 14:00 OP82796 V5E1162 Run #2 Purge Volume mn # 1 5.0 ml ,un #2 VOA TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 71-43-2 Benzene ND:?•':::';i`:;;'.;:.:•;' D018 0.50 0.010 0.0031 mg/1 78-93-3 2-Butanone (MEK) ND.:.:,`::..:;.';..;: D035 200 0.050 0.020 mg/I 56-23-5 Carbon Tetrachloride ND..`, :.::`::.'::`:.::<.' D019 0.50 0.010 0.0036 mg/1 108-90-7 Chlorobenzene ND. >::`':?..:', i;. D021 100 0.010 0.0020 mg/l 67-66-3 Chloroform NI) :::::::i:`` i ,'; D022 6.0 0.010 0.0030 mg/l 106-46-7 1,4-Dichlorobenzene ND ;;?:?.;;'.,';,;:: D027 7.5 0.010 0,0026 mg/1 107-06-2 1,2-Dichloroethane ND,•;::,(:i;, ,`1(,i! D028 0.50 0.010 0.0031 mg/1 75-35-4 I,1-Dichloroethylene ND';:::''::;'!.':,7; ,; D029 0.70 0.010 0.0032 mg/l 127-18-4 Tetrachloroerhylene ND:.`:`:.:: :;::: D039 0.70 0.010 0.0022 mg/1 79-01-6 Trichloroethylene ND;.'':;`:.•:'::;:.,D040 0.50 0.010 0.0035 mg/1 75-01-4 Vinyl Chloride ND,:':•::":'.1:`<`;:.D043 0.20 0.010 0.0041 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane i Ok.:'•:. ':';:`. 83-118% 17060-07-0 1,2-Dichloroethane-D4 1160W-:.;':;`.:: 79-125% 2037-26-5 Toluene-138 I03%:!;';::;.;f. 85-112% 460-004 4-Bromofluorobenzene 104%`;!'!.;::' 83-118% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/ 11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6of94 --.r- FA00347 to 4 6GS North America Inc. Report of Analysis Page 1 of I Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA80347-1 Date Sampled: 10/28/20 Matrix: SO - Sludge Date Received: 10/31/20 Method: SW846 8270D SW846 3510C Percent Solids: 3.5 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run 41 91010525.1) 1 11/12/20 13:12 MV 11/11/20 10:00 OP82907 S9I382 Run #2 Initial Volume Final Volume Run # 1 100 ml 1.0 ml Run #2 ABN TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 95-48-7 2-Methylphenol ND.:`';,; `:;j .:; :.i, D023 200 0.050 0.0056 mg/l 3&4-Methylphenol ND `; ::`;::.'';`;i D024 200 0.050 0.0098 mg/1 87-86-5 Pentachlorophenol ND, :.`:'.i•:';!,:::', D037 100 0.25 0.050 mg/1 95-95-4 2,4,5-Trichloropbenol N17, i,:;`.'.`.;; ::,:!; D041 400 0.050 0.0074 mg/1 88-06-2 2,4,6-Trichlorophenol1D.` ;;:;'.``;.;: D042 2.0 0.050 0.0075 mg/I 106-46-7 1,4-Dichlorobenzene ND ;..;:,:. .',:,: D027 7.5 0.050 0.0050 mg/1 121-14-2 2,4-Dinitrotoluene ND.;'':';'+`; `, ;';';' D030 0.13 0.050 0.0081 mg/l 118-74-1 Hexachlorobenzene D032 0.13 0A50 0.0069 mg/1 87-68-3 Hexachlorobutadiene ND ',: !..::;';: ;`, , D033 0.50 0.050 0.0050 mg/1 67-72-1 Hexachloroethane ND;.=;;;;i;; ;` D034 3.0 0.050 0.016 mg/1 98-95-3 Nitrobenzene ND,':; ,';':,;; i!D036 2.0 0.050 0.0093 mg/l 1I0-86-1 Pyridine ND.<.:i;;:."'.`;: D038 5.0 0.10 0.020 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 30% :'::�':::::..:: 14-67% 4165-62-2 Phenol-d5 24%0 { .i`s`< 10-50% 118-79-6 2,4,6-Tribromophenol 7.80°;;,:`': 33-118% 4165-60-0 Nitrobenzene-d5 69%C,'i.`•.., 42-108% 321-60-8 2-Fluorobiphenyl 40-106°1° 1718-51-0 Terphenyl-d14 78%i,',.:;'':`,: 39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/l/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound nt7of14 FAU0347 SGS North America Inc. Report of Analysis Page 1 of 1 a� Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA80347-1 Date Sampled: 10/28/20 Matrix: SO - Sludge Date Received: 10/31/20 Method: SW846 8151A SW846 3510C Percent Solids: 3.5 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC071657.D 1 11/12/20 16:46 SH 11/11/20 12:00 OP82909 GCC1757 Run #2 Initial Volume Final Volume Run #I 10.0 ml 5.0 ml Run #2 Herbicide TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 94-75-7 2,4-D ND„.';!.`,`?,':, D416 10 0.050 0.017 mg/1 93-72-1 2,4,5-TP (Silvex) ND..;>'' ::::'.: `D017 1.0 0.0050 0,0013 mg/I CAS No. Surrogate Recoveries Run# 1 Rung 2 Limits 19719-28-9 2,4-DCAA 7. mo .:`:' .' `.; 39-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound .....3L6._ 8 of 14 FABO347 • ` SGS North America Inc. Report of Analysis Page I of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA80347-1 Date Sampled: 10/28/20 Matrix: SO - Sludge Date Received: 10/31/20 Method: SW846 8081B SW846 3510C Percent Solids: 3.5 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 ST150180,D 1 11/11/20 20:44 WH 11/11/20 08:00 OP82908 GST3617 Run #2 Initial Volume Final Volume mn #1 100 ml 5,O ml '.un #2 Pesticide TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindane) ND,:`.:.:'.:.:';: ; DO13 0.40 0.00010 0.000022 mg/1 12789-03-6 Chlordane h(D.,;.'',! ., ::. ;'` D020 0.030 0.0010 0,00038 mg/l 72-20-8 Endrin a D012 0.020 0.00020 0.000021 mg/1 76-44-8 Heptachlor ND ':::,:: ':':'::;:'::;, D031 0.0080 0.00010 0,000026 mg/1 1024-57-3 Heptachlor epoxide ND::''::.�;.'::-:`:` D031 0.0080 0.00010 0.000020 mg/1 72-43-5 Methoxychlor a ND,; "; ;;,; ?,`'! DOi4 10 0,00020 0.000050 mg/1 8001-35-2 Toxaphene ND.:.:`.' ;i`, `:'`:' DO15 0.50 0.0050 0.0021 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 460:;'.; 42-127% 2051-24-3 Decachlorobiphenyl 'I04%.;'f:`.:;:. 27-127% (a) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/ 1 / 11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9of14 FA80347 SGS North America Inc. Report of Analysis 'lient Sample ID: SLUDGE SAMPLE ,ab Sample ID: FA80347-1 Date Sampled: 10/28/20 vlatrix: SO - Sludge Date Received: 10/31/20 Percent Solids: 3.5 ?roject: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC Metals Analysis, TCLP Leachate SW846 1311 Page 1 of 1 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic 0 ..j 0 ';j D004 5.0 0.10 mg/1 1 11/11/20 11/11/20 LM SW9466010C2 SW846301OA4 Barium <2,0•„.':;:.'::. `: D005 100 2.0 mg/1 1 11/11/20 11/11/20 LM SW846 6010C 2 SW846 3010A 4 Cadmium <..0:050.';!D006 1.0 0,050 mg/1 1 11/11/20 11/11/20 LM SW8466010C2 SW8463010A4 Chromium <,O..10., r.` :'::'.: D007 5.0 0.10 mg/l 1 11/11/20 11/11/20 LM SW846 6010C 2 SW846 3010A 4 Lead <0..050 :';;;;< D008 5.0 0.050 mg/1 I 11/11/20 11/11/20 LM SW846 dOIOC 2 SW846 3010A 4 Mercury <,0.0050::' D009 0.20 0.0050 mg/1 1 11/04/20 11 /04/20 ie SW846 7470A 1 SW846 7470A 3 Selenium <0.::10,. ;'.. ` •'' DO10 1.0 0.10 mg/l 1 11/11/20 11/11/20 LM SW846 6010C 2 SW846 3010A4 Silver <.0;`1Q;;`:;';'.';;D011 5.0 0.10 mg/l 1 11/11/20 11/11/20 LM SW8466010C2 SW846301OA4 (1) Instrument QC Batch: MA17201 (2) Instrument QC Batch: MA17220 (3) Prep QC Batch: MP38085 (4) Prep QC Batch: MP38122 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/l 1) �'!' 10 of 14 Bdlm. FA60347 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA80347-1 Date Sampled: 10/28/20 Matrix: SO - Sludge Date Received: 10/31/20 Percent Solids: 3.5 Project: Suez Water (Ramseur WWTP-Sludge); Clemmons, NC General Chemistry Analyte Corrosivity as pH Cyanide Reactivity Ignitability (Flashpoint) a Solids, Percent Sulfide Reactivity (a) Not ignitable. RL = Reporting Limit Page I of 1 P is Result RL Units DF Analyzed By Method su 1 11/12/20 12:09 JB SW846 CHAP? <43 43 mg/kg 1 11/16/20 13:51 AC SW846CHAP7 Deg. F 1 11/13/2009:04 CS SW8461010AMOD % 1 11/03/2013:17 JB SM192540G 1400 mg/kg 1 I1/10/20 12:32 Jc SW846 CHAP? 11 of 14 FA80347 CHAIN OF CV i'ODY RECOV FMS41 Page 1 of I Environment 1,Inc, P.O. Box 7083, 114 Oalonont Dr. Greenville, NC 27858 ;uviwutttcatl itta.com Phone 452)756-6208 " Fax (252) 796.0633 DISINPP.CTION CHLORINENEUTRAU2EDATCOLLECTION CLIENT: . Week:8 Ci 5j " IDCHLORINC ❑ UV pHCHECS((LAB) P P P P P P G G G G G CMNTAINERTYPE,P/G 411I29biA-WIA RAMSUUR WTRSLUDGE) ADINE BLACIVNELL NONE, .0. BOX 1279 LEMMONS NC 27012 A A A A A A A A A A A CHEMICAL PRESERVATION 136) 766 0270 A -NONE, D-NAOH u�F Sa 3 8-HMO, E•HCL g s A 'S p° pm : W C • H'SO' F • ZINC ACETATE/NAOH COLLECTION 8 tR 4 $ a 13. a 4. a '�' c d a =� t G•NATHIOSLUATE LOCATION I SAMPLE DATE TIME Fo o 0- a, SludgeSatepte ?a�g.T � : t 30 _'�'• CLASSIFICATION: WASTEWATER(NMES) . ............ . DRINKING WATER DWRiW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DU RING yiHlPhjENTIDELIVERY (L / N SAMPLES COLLECTED BY: lfl SAMPLESRECENEDWLABAT_L_°C RELNCUISHED (S ,) (SAMPLER) DATETRME R'M ) DA ME COMMENTS; DBYG) RETJNDU15�1 ` f/ �' 4 DATVV4E OD �2 EY D EITME Z REU SHED BY ICI) ` D TfjTIME kE ($IG DATETTI ••L " •/IS�O^ ?Li x0 -.. �• OTWO I i " r plating this for , Sampler must place m on the , verso sfde. e a "C" for composite sample or a "G" for F LO i $ I/moo "13o Grab sample In the blocks above for each parameter requested, N U 375237 FA80347: Chain of Custody Page I of 2 13 of '14 FAB0347 SGS Sample Receipt Summary Jab Number., FA80347 Client: ENVIRONMENT 1, INC, Project: 950 Date / Time Received: 10/31/2020 9:30:00 AM Delivery Method: FEDEX Airblil Ws: 900433727312 Therm ID: IR 1; Therm CF: 0.2; Cooler Temps (Raw Measured) °C: Cooler 1: (0,6); Cooler Temps (Corrected) °C: Cooler 1: (0.8): # of Coolers: 1 Cooler Information —X--QL--tL Sample Information Y or N N!A 1. Custody Seals Present R ❑ 1. Sample labels present on bottles 0 ❑ 2. Custody Seats Intact FVJ ❑ 2, Samples preserved property �Ji ❑ 3. Temp criteria achieved ® ❑ 3. Sufficient volume/containers read for analysis: ® ❑ 4. Cooler temp verification IR Gun 4, Condition of sample jet 5. Cooler media 101121191 S. Sample recvd within HT ❑ 6. Dales/Times/IDS on COC match Sample Label ® ❑ Trio Blank Information Y or N N/A 7, VOCs have headspace ❑ ❑ 0 1. Trip Blank present / cooler Cl ❑ R 8. Bottles received for unspecified tests ❑ 2. Trip Blank listed on COC ❑ ❑ R 9. Composifing Instructions clear ❑ ❑ 0 W or S NIA 10. Vos SoR Kits/Jars received past 48hrs? ❑ ❑ 0 3, Type Of TB Received ❑ ❑ 11. % Solids Jar received? Cl ❑ 12, Residual Chlorine Present? Cl ❑ R Misc. information y Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals: Test Strip Lot #s: pH 0.3 230315 10-12 219813A Other. (Specify) Residual Chlorine Test Strip Lot#: J _ `pH Comments _ ROt Reev.v.Date 0524117 Technician: BRYANG Date: 10/31/2020 9:30:00 A Reviewer: Date: FA80347: Chain of Custody Page 2 of 2 14 of 14 FA80347 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Ramseur WQ Permit Number: WQ0010528 W.W. Name: Ramseur WWTP Monitoring Period: From l/l/2020 NPDES Number: NCO026565 To 12/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)[] A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying El Treatment ElThermophilic El Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ .......... Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens Cl If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": . Lime Stabilization 0 Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- dences Frequency of Analysis Sample Type Analytical Tech - ni Minimum Geo. Mean Maximuml Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization L] Alt 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ C.;EK11FIC;ATHON STATEMENT (please check the appropriate statement) 21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." eT-ry_ lrewct le►-i � Preparer Aame and Title (type or print) Signatur4 of Preparer* Land Applier Name and Title (if applicable)(type or print) 7-/1-Z6 Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) f1FNR PnRAA P\/RF n?T (19/,)nnrn) 4 • Month LIME LOG SHEET �19 Year 2b Z (] DATE 2- GAL. WASTED *OO Initial TEMP °C 05. Initial pH, SU b•9 LBS OF LIME d TIME lbD� pH, SU 12 •� TEMP °C �•3 Temp Corrected pH, SU �Z. Z pH after 2 HRS � 2•`f TEMP °C after 2 HRS 5 Temp Corrected pH, SU Z . pH after 24 HRS ' If TEMP °C after 24 HRS Temp Corrected pH, SU pH Correction Temp°C Correction 40 Plus 0.45 39 Plus 0.42 38 Plus 0.39 37 Plus 0.36 36 Plus 0.33 35 Plus 0.30 34 Plus 0.27 33 Plus 0.24 32 Plus 0.21 31 Plus 0.18 30 1 Plus 0.15 29 1 Plus 0.12 28 Plus 0.09 27 Plus 0.06 26 Plus 0.03 25 0 24 Minus 0.03 23 Minus 0.06 22 Minus 0.09 21 Minus 0.12 20 Minus 0.15 19 Minus 0.18 18 Minus 0.21 17 Minus 0.24 16 Minus 0.27 15 Minus 0.30 14 Minus 0.33 13 Minus 0.36 12 Minus 0.39 11 Minus 0.42 10 Minus 0.4S "I certify, under penalty of law, that the Class B pathogen requirements in 40 CFR, Part 503.32(b) have been met and the vector attraction reduction requirement in 40 CFR, Part 503.33(b)(4) and (6) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Printed Name & Title �e L Iti �GZ {/ �� [n O RI Signature RAMSEUR WATER TREATMENT PLANT SLUDGE DISPOSAL RECORD YEAR: .2 Q a o Prior to 1 st disposal event 1 Collect a sludge sample from the drying beds and test for Percent Solids, Arsenic, Chromium, Nickel, and TCLP 2 Measure the pH on -site and record result on Chain of Custody Label the sample location as "Sludge to Disposal" On Hauling Event Days 1 Complete "Vehicle Inspection" form 2 Complete bottom portion Date of Hauling Volume Tank Size # Loads Gallons a7/ot0 3 /G o ti p a 8 zo 3 11co 3 I(o0 Z 3 "i 6-0 a 2 (p ZD o i 3� 76v I n �: 15 VEHICLE INSPECTION* FORM LIQUID WASTE Pumping Company . __ _ P0,4, Sc I eA f: Address 71 _ o M .MahPJCity _f,_.r`1 h �'71% Zip Code 283� ? Telephone Name of pumper or representative present d1 ring inspection (please print)f- Make and Model 5�4f1:n License ?Number n Gallons YA 91782 3.IG o ����' satisfactory U = nn i Egn?i� rent Condat�Ion )inspected Vehicles G j 2 3 4 5 eneral Cleanliness {Ali equipment maintained and ' cleaned of spillage i 5 Vehicle lYFechanics j Lights, Horn, Tires, Brakes, Mirrors, Steering Wheel `5 5 } Tank Container j Leak proof, no dents or corrosion Tank Cover Tight fitting, spill proof € s Release Val ve and ' Valve, hose, fittings goodno Hose , leaks Sewage Suction Sound condition, drained after ' { Hose ; each use, sanitary storage ' S ` Copy of SPCC PIan ? Located in vehicle f Spill Cleanup Equipment !Water Bose, disin€ectant, hand ` sanitizer, 5 gal. of absorbent*, 5 galbucket, broom & shovel ! Over ill Protection j Positive check valve present or _ I Lem Indicator contents level gauge 5 S vel ? Recommended, but not requik ed k �� if check valve used ! Purnp Type, condition (able to handle ( septage without intake st-ainer) S S Complete if any item is marked "'UnEsatisfactorf> in columns at left Date /o/a7/ao Inspected byso,, (print name) i�tature) *� VEHICLE INSPECTION FORM LIQUID WASTE PUMPING AND HAULING Pumping Company: T or -moo,-Jn. < Address I I ct DIJ %taut"City _ 1"iewc 6p-ok e Zip Code 37 Z Telephone Name of pumper or representative present during inspection (pleaseprint) i b -4-1- r COLLECTION VEHICLES: Make and Model License Number Tanker Capacity in Gallons Y -81'2f? 3 ICo 2 o yA -/ J 9G 7 3 /G9 EQUIPMENT INSPECTION: S = satisfactory iJ = unsatisfactory Equipment Condition Inspected Vehicles Complete if any item is marked "unsatisfactory" in 1 2 3 4 5 columns at left General All equipment maintained and S Cleanliness cleaned of spillage Vehicle Mechanics Lights, Horn, Tires, Brakes, S Mirrors, Steering Wheel Tank Container Leak proof, no dents or corrosion s S Tank Cover Tight fitting, spill proof S Release Valve and Valve, hose, fittings good, no Hose leaks Sewage Suction Sound condition, drained after Hose each use, sanitary storage Copy of SPCC Plan Located in vehicle Spill Cleanup Water hose, disinfectant, hand Equipment sanitizer, 5 gal. of absorbent*, 5 al. bucket, broom & shovel Overfill Protection Positive check valve present or S contents level gauge Level Indicator Recommended, but not required s S if check valve used Pump Type, condition (able to handle S s septae without intake strainer Date ZO/2JZc20 Inspected by cli SOn Ye-ll-j i (print name) (Signature)