NC0021962_Lab results - 625 Parameters_20201021

Action History (UTC-05:00) Eastern Time (US & Canada)
Subrrit by Anonymous User 10/21/2020 10:26:11 AM (Supplemental Submittal)
Submit by Bennett, Tilman B 5/16/2021 9:05:26 PM (Supplemental Info Submittal)
p Lab sample results for 625 compounds - probably needs a better submittal process
• Bennett, Tilman B assigned the task to Bennett, Tilman B 5/16/2021 9:04 PM
• The task was assigned to Thedford, Wren, Bennett, Bradley 10/21/2020 10:26 AM

Initial Review Information
Updated ID#:* IWORTANf:FEVIBAERSHOLLDVERIFY and revise here ifnecessary.
NC0021962
How should this project be handled?*
r File r Discard
Information Submitted on 10/21/2020
Submitter Information
Name: James Utke
Vft is subrritting the inforrretion?
Email Address:* [e-mail]
Submittal Information
The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental
information associated with discharge monitoring reports (DMR). All DMR data is required to be submitted
electronically through the eDMR system and should not be submitted here. Division staff will reviewall
uploaded documents and will only maintain required information. Documents such as laboratory reports are not required
to be submitted and will not be maintained in the system.
Project Information:
Rease SUDDly the Dernit nun ber for this
Existing ID#* PerrritNurrber
NC0021962
Exarrples: NOKxxxxxx or NO&xxxxx
Facility Name:* CITGO Petroleum Corporation
County: Mecklenburg
Please upload all files that need to be
submited. *
dick the upload button or drag and drop files here to attach docurrent
NPDES625 september2020.pdf 8.63MB
Only pdf files are accepted.
Comments about the attachments:
625 Compound Scan Submittal. September 2020
* V By checking the box and signing box below, I certify that:
o I have given true, accurate, and complete information on this form;

• I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the
NC General Statutes (the "Uniform Electronic Transactions Act)
• I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes
(the "Uniform Electronic Transactions Act');
• I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written
signature; AND
• I intend to electronically sign and submit the Supplemental Information form."
Full Name: James Earl Utke
Signature:
Date Submitted: 10/21/2020

%; aceAnalytical ® ANALYTICAL REPORT
National Center for Testing & Innovation September 14, 2020
5
E
F
CITGO-Charlotte, NC
Sample Delivery Group: L1258804 F
Samples Received: 09/04/2020 s
5r
Project Number: SEMIANN
Description: Treated stormwater rQC
�GI
Report To: Mr. Jim Utke
7600 Mount Holly Road f11
Charlotte, NC 28214
GSc
Entire Report Reviewed By
Reagan Johnson
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the Information.I bvided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME- Parr:

TABLE OF CONTENTS ONE LAB. NATIONWIDE V
Cp: Cover Page
I
Tc: Table of Contents
�
Ss: Sample Summary
3
Cn:Case Narrative
4
000N�
Sr: Sample Results
5
E
OUTFALLDO1 L1258804'01
5
Qc:Quality Control Summary
7
[Cn
Semi Volatile Organic Compounds (GC/K4S)byMethod 6251
7
Er
GI: Glossary ofTerms
12
Al: Accreditationa&Locations
13
E
ScSample Chain ofCustody
14
AocoowT: penJscr soa oArE/nms p^=F:-

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
OUTFALL 001 L1258804-01 WW Rick Patterson 09/03/2008:45 09/04/2009:30
metnod
Semi Volatile-. Organic Compounds (GC/MS) by Method 625.1
Batch
WG1539844
Dilution Preparation Analysis Analyst
date/time date/time
1 09/09/2017:07 09/10/20 02:11 JNJ
Location
Mt. Juliet, TN
ACCOUNT: PROJECT: SDG:
DATF/TtMF-
DA�C

CASE NARRATIVE
ONE LAB. NATIONWIDE. AR
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Lam'
Reagan Johnson
Project Manager
ACCOUNT: PROJECT: SDG:
DATE/TIME-

OUTFALL 001 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 09/03/20 08:45 L1258804
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Analyte
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
Bis(2-chloroethyl)ether
2,2-Oxybis(1-Chloropropane)
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene
Di benz(a,h)anthracene
3,3-Dichlorobenz idine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
1,2-Diphenylhydrazine
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachloro-1,3-butad iene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Ndrosodimethylamine
n-Nitrosodiphenylamine
n-N itrosodi-n-propylamine
Phenanthrene U
Benzylbutyl phthalate U
Bis(2-ethylhexyl)phthalate U
Di-n-butyl phthalate U
Diethyl phthalate U
Dimethyl phthalate U
Di-n-octyl phthalate U
Pyrene U
1,2,4-Trichlorobenzene U
4-Chloro-3-methylphenol U
2-Chlorophenol U
2,4-Dichlorophenol U
2,4-Dimethylphenol 0
4,6-Dinitro-2-methylphenol U
2,4-Dinitrophenol U
2-Nitrophenol U
4-Nitrophenol U
Pentachlorophenol U
Phenol U
2,4,6-Trichlorophenol U
(S) Nitrobenzene-d5 7
(S) 2-Fluoroblphenyi 6
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
6.4
4.8
Qualifier MDL
mg/I
mg/1
U
0.0000886
U
0.0000921
U
0.0000804
U
0.00374
U
0.000199
U
0.000130
U
0.000120
U
0.000121
U
0.0000381
U
0.000116
U
0.000137
U
0.000210
U
0.0000877
U
0.0000648
U
0.0000926
U
0.000130
U
0.0000644
U
0.000212
U
0.0000983
0.000250
0.000105
0.000102
0.0000844
0.0000755
0.0000968
0.0000598
0.000127
0.000279
0.000143
0.000159
0.000297
0.000998
0.00237
0.000261
0.000112
0.000765
0.000895
0.000453
0.000287
0,000260
0.000932
0.000107
0.0000698
0.000131
0.000133
0.000102
00126
B J 0.0000636
0.00112
0.00593
0.000117
0.000143
0.000313
0.00433
0.000100
RDL Dilution
mg/I
0.00100 1
0.00100 1
0.00100 1
0.0100 1
0.00100 1
0.00100 1
0.00100 1
0.00100 1
0,00100 1
0.0100 1
0.0100 1
0.0100 1
0.0100 1
0.00100 1
0.0100 1
0.00100 1
0.00100 1
0.0100 1
0.0100 1
0.0100 1
0.0100 1
0.00100 1
0.00100 1
0.00100 1
0.0100 1
0.0100 1
0.0100 1
0.00100 1
0.0100 1
0.00100 1
0.0100 1
0.0100 1
0.0100 1
0.0100 1
0.00100 1
0.00300 1
0.00300 1
0,00300 1
0.00300 1
0.00300 1
0.00300 1
0.00100 1
0,0100 1
0.0100 1
0.0100 1
0.0100 1
0.0100 1
0,0100 1
0.0100 1
0.0100 1
0.0100 1
0.0100 1
0.0100 1
0,0100 1
15.0-374
22.0-127
Analysis
ddte / time
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
09/10/2020 02:11
0911012020 02.11
0911012020 02:11
Batch
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
WG1539844
ACCOUNT: PROJECT: SDG:
DATEfrlMF-
oert:-

OUTFALL 001 SAMPLE RESULTS - 01
Collected date/time: 09/03/20 08:45 L1258804
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
ONE LAB, NATIONWIDE. JR
Result Qualifier MDL
RDL
Dilution Analysis
Analyte
_..mg/I mg/I
mg/I
date/time
(S) p-Terphenyl-d14
75.2
29. 0-141
0911012020 02:11
(S) Phenol-d5
32.6
S. 00-424
0911012020 02:11
(S) 2-Fluorophenol
52.5
10.0-120
0911012020 02.11
(S)2,4,6-Tribromophenol
75.0
10.0-153
0911012020 02:11
Batch
WG1539844
WG1539844
WG1539844
WG1539844
ACCOUNT: PROJECT: SDG:
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a

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. AR
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit,
RDL
Reported Detection Limit.
Rec.
Recovery,
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
J
The identification of the analyte is acceptable; the reported value is an estimate.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
ACCOUNT: PROJECT: SDG:
DATE/TIME
PAr,F

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
State Accreditations
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TN002
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky's
90010
South Carolina
84004
Kentucky'
16
South Dakota
n/a
Louisiana
A130792
Tennessee' °
2006
Louisiana'
LA180010
Texas
T104704245-18-15
Maine
TN0002
Texas'
LAB01152
Maryland
324
Utah
TN00003
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
460132
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A2LA
Third Party
Federal Accreditations
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2LA— ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
' Drinking Water ' Underground Storage Tanks ' Aquatic Toxicity ° Chemical/Microbiological s Mold a Wastewater n/a Accreditation not applicable
QUr Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
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