WQ0013116_Application_20210511

Gary Caldwell, Mayor
Julia Freeman, Mayor Pro Tem
Jon Feichter, Alderman
Anthony Sutton, Alderman
Chuck Dickson, Alderman
April 1, 2021
Rob Hites Jr., Town Manager
Bill Cannon, Town Attorney
TOWN OF WAYNESVILLE
Distribution of Class A Wastewater Residuals
Permit No. WQ0013116
NCDEQ-DWR
Non -Discharge Permitting Unit
Attn: Nathaniel Thornburg, Unit Supervisor
1617 Mail Service Center
Raleigh, NC 27699-1617
Mr. Nathaniel Thornburg,
For your review and approval is the renewal request of Permit No. WQ0013116 belonging to the Town
of Waynesville. Below is a summary of attachments as requested in the permit application:
• Form: DCAR 06-16 & Supporting Documentation
+ Attachment DCAR Item D
■ Attachment DCAR Item H
• Form: RSC 06-16 Residuals Source Certification
• Attachment RSC Item B
• Attachment RSC Item C
If there are any questions, please do not hesitate to contact the Public Services Operations Center.
in rely
J
Preston Gregg, P
Town Engineer
129 Legion Dr. • P.O. Box 100 • Waynesville, NC 28786 Phone [phone] Fax [phone]
Web Address: www.waynesvillene.gov

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one on final and two copies of the application and
sunoortina documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit wehsile
General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under 15A NCAC 02T .1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
The project name should be consistent on the plans, specifications, etc.
® The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b]. An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(b).
❑ If this project is for a modification of an existing permit, submit one copy of the existing permit.
❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification New Permit
Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310
— --- I [
Finor (residuals permitted for distribution < 3,000 dry tons/year) $810
Major Modification 1 1
f $395
$245
1 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
® List all items included in the application package, as well as a brief description of the requested permitting action.
INSTRUCTIONS FOR FORM: DCAR 06-16 Pagel of 3

D. Program Information (All Application Packages)
® Provide a narrative explaining the following:
® How the materials will be handled and transported from where the residuals were produced to where it will be treated.
® How the residuals will be processed/treated (attach process flow diagram).
® How leachate collection will be handled.
® Where the residuals will be stored until processed.
® How the final product will be distributed (packaging, bulk, etc.)
® What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
® Name and address of the person who prepared the residual that is sold or given away.
® A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
® A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
Information on all, applicable setbacks in accordance with 15A NCAC 02T. I 108(b).
® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A
NCAC 02T .I 104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1108{a) on the plans.
❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15A NCAC 02T .1104 a 2 B , including leakage and pressure testing as appropriate.
❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T
.1104(a).
G. Environmental Assessments (Maybe Required— See 15A NCAC 1 C .0300)
❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3

H. Operation and Maintenance Plan (New and Renewal Application Packages)
For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
® Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum:
® Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
® Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
® Safety measures; may include safety training program, manuals, signs, etc.
® Spill response plan; including control, containment, remediation, emergency contact information, etc.
® Inspection plan including the following information;
® Names and titles of personnel responsible for conducting the inspections.
® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
® Sampling and monitoring plan including the following information;
® Names and titles of personnel responsible for conducting the sampling and monitoring.
® Detailed description of monitoring procedures including parameters to be monitored.
® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special DeliverX:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: Town of WaynesydIe
Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ® Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Title: Town Manager
Applicant's mailing address: 16 S. Main St.
City: Waynesville State: NC Zip: 28786-
Telephone number: 828) 456-3706 Email Address: rhites _ waynesvillenc.go
2. Consultant's name: N/A License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address:
City: State: Zip: -
Telephone number: (_) = Email Address:
3. Fee submitted: (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00013116
Date of most -recently issued permit: 7/20/2016
Date of most -recently certified Attachment A (if different than the permit):
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Town of Waynesville Blend Processing Facility & Distribution Program
City: Waynesville State: NC Zip: 28786-
Coordinates: Latitude: 35' 32' 30" Longitude: 82' 57' 04"
Datum: NAD 83 Level of accuracy: 5 mm
Method of measurement: Haywood GIS
County where facility is located: Haywood
2. Facility contact (person familiar with residuals preparation):
Name: Mark Jones Title: Lab Supervisor
Mailing address: 129 Legion
City: Waynesville State: NC Zip: 28786-
Telephone number: 828) 456-3706 E-mail address: miones waynesvillenc.gov
FORM: DCAR 06-16 Page 1 of 3

3. Is the residual process facility also the generator? ® Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: 90-180 days (Note: the Division requires minimum 30 days storage in units that are
separate from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
® sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
❑ other (explain);
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials
Amounts to be added
er 1.0 dry ton of residuals (dry ton
Lime Kiln Dust
1.1 D Tons
3. Approximate amounts of the residuals received and processed at the facility: 693 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 1,138 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): All treated residuals are stored under sheds at WWTP. Average storage time is
3 months with a maximum of 6 months.
6. Does the facility have a stormwater management plan? ❑ Yes; ® No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Stoma a areas are
located in storaebays under a roof structure.
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ❑ No, Explain;_
I_5)/0-„ G
(Signature Authority's N'�d— PLEASE PRINT)
attest that this application for �� V✓�l OF V121flnU3L11,11 - W wl"
P.
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature:
Date:
FORM: DCAR 06-16 Page 3 of 3

WAYNESVILLE
North Carolina
Pm ,ress with Vision
1871
Attachment DCAR Item D.
(Program Information)
TABLE OF CONTENTS
Narrative.......................................................................................................................................................1
Handlingof Materials................................................................................................................................1
ProcessFlow Diagram .............................................. ........................ ............................... ......... 1
Leachatecollection.....................................................................................................:............... ..........1
StoringResiduals.......................................................................................................................................1
Distribution................................................................................................................................................1
ProcessFlow Diagram..............................................................................................................................2
MarketabilityConsumer Guide.................................................................................................................3-4
DistributionList.....................................................................................................................................5

NARRATIVE DESCRIPTION OF THE TOWN OF WAYNESVILLE
WASTEWATER TREATMENT SLUDGE MANAGEMENT
The Town of Waynesville Wastewater Treatment Plant generates both primary sludge with
primary clarifies and waste activated sludge from the secondary activated sludge process at the
Wastewater Treatment Plant.
The two settled sludges are gravity thickened in primary and secondary gravity sludge
thickeners. The gravity thickened sludges are pumped to an anaerobic digester for further
volatile solids and pathogen reduction. The digested sludge is then dewatered with a 1,5 meter
belt press. The dewatered sludge is blended with lime kiln dust as well as agricultural time (as of
December 2013) to achieve the required vector attraction reduction requirements and is heat
pasteurized to 15$ degrees Fahrenheit or greater for pathogen reduction requirements. The time
stabilization and heat pasteurization ecluipment used is RDP teclunologics thermohlender and 30
minute deten(k)n time pasteurization vessel.
Listed below are facts about The Town of Waynesville Wastewater Treatment Blend Processing
and Distribution: `
• All biosolids produced are stored under a covered shed onsite. The biosolid product is
distributed to the public free of charge.
• The residuals are produced and treated at the same location.
■ All residuals are stored and processed onsite at the Wastewater Treatment Plant.
■ All leachate collected is returned to plan influent.
• Detention time from anaerobic digester through the belt press time sludge blender and
.pasteurization vessel to discharge through the conveyor is approximately one hour.
Occasionally more time is used to turn the processed residuals in the storage shed to
Produce a more workable product and decrease percent moisture.
• All final products are stored onsite under a covered shed.
• The final product is stored for approximately 3 -- b months depending on the season.
During spring and fall, the product is in demand more than suntnier and winter.
• The final product is given away in bulk to the local farmers.
Lich year. approximately 800 — 1,100 dry tons per year are produced and distribuned. The
destination of final product has been to local farmers and local commercial lime spreaders. All
recipients' names are kept on file at the treatment plant.
Page 1 1

TREATMENT PROCESS SCHEMATIC
Pr it71�7
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�IutiC�i
,alas Prodt,r_,

Pollutants of Concern
In 1994 the US Environmental Pio(eclioii Agenc}
Started what is known as the 303 Regulations
These regulations set limits for pndwetn and
vector atlraclon reduction in the disposal of
sewage biosolids and for hravy metal
concentrations such as Mercury. Cadmium,
Arsenic, Chromium, Copper, Lead, Molybdenum
Nickel, Selenium and Zinc Although a few of
these metals can be considered macro nu(rients
when available in tram amounts they can be very
toxic in high concentrations.
The lime stabilization heat pasteurization process
eliminates the pathogen and vector attraction
prublem. The Town of Waynesvilles Sewer Use
Ordinance and Industrial Pretreatment Regulations
limit_+ the amount of heavy metals that can enter the
Waste Water Treatment Plant. Since 1994 all
quarterly analyses of Waynesvilles sewage
biosolids have met the US EPA requirement for
"Exceptional" or "High Quality" for heavy metal's
concentration limits.
Page 13
Questions
Agricultural technical guidance contact
Tom Harvey' Agricultural Agent
North Carolina Cooperative Vxtension Servicc
828-456-3575
Biosolids product information contact
Fred Baker' Director of Public Works
Town of Waynesville
828-456-4410
David Smith' Plant supervisor
Town of Waynesville Waste Water Treatment
Plant
828-452-4685
Consumer
Guide
Town of Waynesville
Agricultural Use
Biosolid Product
Town Of Waynesville
Waste Water Treatment Plant
566 WALNUT TRAIL
WAYNESVILLE NC 28786

Benefits of this product
What is a biosolid Application rates
product?
The Town of Waynesville Biosolid Product
is a combination of equal parts municipal sewage
sludge and lime blended together and heat
pasteurized to produce a class A stabilized biosolid
product that meets F_.PA 503 regulations for
agricultural use.
Why are we doing this?
The three most common methods for sewage
sludge disposal are (1) burial in a landfill,
(2) incineration, and (3) recycling by lime
stabili7ation and heat piisteurization for land
Application.
The Town of Waynesville, hngiuning in 1965,
incinerated its sewage sludge, but rising fuel oil
costs and stricter air pollution regulations in thr
late 1970s ended this method of disposal for the
Town. From the late 19705 to early 199X the
disposal method used was burial in a Town owned
landfill. With the useful life of the landfill ending in
19Qg,the Town of Waynesville opted for a more
environment friendly process for sludge disposal
that is also a major recycling effort for the "ruwu of
Waynesville. The process is known as Lime
Stabilization and Heat Pasteurization.
Page 14
The primary benefit of this product's use is for a
liming agent to adjust soil pH. Other benefits
include value as a low grade fertilizer and as a soil
amendment to help to make clay and other heavy
soils more permeable and improve soil aeration to
promote better root growth. As environmental
regulations toughen and costs for landfill and
incineration disposal methods increase
dramatically every year, recycling of this material
into a safe and very usable product is beneficial
environmentally and economically.
Precautions & Restrictions
Prolonged contact with the eye's shin and mucous
membranes should be avoidcd due to the highly
alkaline nature of line stabilized biosolids and
direct ingestion should also be avoided.
As with agricultural lime this product should not be
applied to any site that is flooded,frozen or snow
covered. Adequate procedures shall be provided to
prevent surface runoff from carrying any applied or
stored biosolids into any surface waters. This
product should not be applied any closer than 10
feet from any public or private water supply
including wells,streams,lakes,rivers or natural
drainage way.
It is recommended that a soil analysis be
performed to determine the amount of agricultural
lime needed. Approximately two ton of this
product will be needed to equal one ton of
agricultural lime.
Product Analysis
Lbs. per ton wet hasis
Available for first crop
Nitrogen
3.3 Lbs.
Phosphate
4.3 Lbs,
Potash
0.87 Lbs.
Magnesium
3.1 Lbs
Iron
8.5 Lbs
Calcium
232.7 Lbs.
Sulfur
2.0 Lbs.
Manganese
0.07Ibs
Zinc
0.19 Lbs.
Copper
0.05 Lbs

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Attachment DCAR Item H.
(Operation and Maintenance Plan)
TABLE OF CONTENTS
Full Operation and Maintenance Plan ....... .............. ...—.................. ........................................ 1-9
SystemDrawings .................................... ........................... ................................................... 10-42
SystemPhotographs............................................................................................. ............. 13-22
Monitoringand Reporting ............................ ........................................................ ................ 23-26
SamplingPlan...............................................................................................................................27

OPERATION AND MAINTENANCE PLAN
BIOSOLIDS PROCESSING PROGRAM
WASTEWATER TREATMENT FACILITY
TOWN OF WAYNESVILLE, NORTH CAROLINA

TABLE OF CONTENTS
I. DESCRIPTION OF BIOSOLIDS PROGRAM.....................1
II. EQUIPMENT MAINTENANCE DATA................................2
III. SAFETY.....................................................................................3
IV. SPILL CONTROL...................................................................4
V. SAMPLING AND MONITORING.........................................5
APPENDICES:
A. BIOSOLIDS SYSTEM DRAWINGS
B. BIOSOLIDS SYSTEM PHOTOGRAPHS
C. MONITORING AND REPORTING REQUIREMENTS

SECTION I. DESCRIPTION OF BIOSOLIDS PROGR�NI
The Town of Waynesville Biosolids Program operates under Permit No. WQ0013116 as issued
by the North Carolina Department of Environment and Natural Resources. After primary and
secondary sludge is processed through the sludge thickeners and the anaerobic digester, the
sludge is fed to a 1.5 meter belt filter press at approximately 2.0% to 2.5% solids. The belt filter
press typically dewaters the sludge to a solids content range of approximately 19% to 21%.
The dewatered sludge from the belt press is discharged into an enclosed screw auger to be
transported for treatment. Agricultural lime can be fed into the process at this point by utilizing a
loader to discharge the lime material into a live bottom bin and screw auger. However, due to
mechanical issues with the auger, Town staff typically blends the agricultural lime manually
after the sludge is treated. The dewatered sludge enters an electrically heated insulated blender
where either quicklime or lime kiln dust (LKD) is added by a volumetric feeder at a controlled
rate and thoroughly mixed with the sludge. After leaving the insulated blender, the lime/sludge
mixture enters a pasteurization vessel where supplemental electric heat is added to maintain the
temperature of the sludge at 158°F (70°C) for thirty minutes to meet the pathogen reduction
requirements of 40 CFR Part 503. Temperature probes monitor the sludge temperature, and the
speed of the conveyor is designed so that the product remains in the vessel for the full thirty
minutes to achieve pasteurization. The vector attraction reduction requirements of 40 CFR Part
503 are met by adding sufficient quicklime or LKD to raise the pH of the sludge to at least 12,
maintain the pH at 12 for two hours and then at 11.5 for an additional 22 hours. After the
product leaves the pasteurization vessel it is discharged into a truck and transported to the
adjacent covered storage area. In order to make the final product more useable for the farming
community, the Town operations staff manually blends agricultural lime with the treated sludge
beneath the covered storage area to increase the solids content to approximately 45% to 50% for
easier spreading. The agricultural lime also adds magnesium content to the final product. The
Town distributes the final product to lime spreading companies, farmers and the general public.
See drawing .schematics in the appendix of this O&M Plan for additional details.

0
TREATMENT PROCESS SCHEMATIC
P.
_'r O. V i t y
wo-, t c, '%: � - --j ',iickener
9tj,lc t, luftks fl �'r,rYt
(W.A,`s.)
:iud(ly l-eed Purrtp
Sik.idge/Acs I_irric
131Lr1de,r� �'rr��w Cwt
L irnc, F tyP(j Cor)VF'y(l
Flc_(dc-cl c rid
'lsulctr '31end .r
KD/Quic{:limr
cod Auger
f lfk0l BiQs 7lldS 1-I odl.•
4.�4-5-50%, sblid�,
L—z
00 0
st•-.urilrrtir�n
1'r_ :ssl to Storage and
ir-ib t+carl
J
,h

SECTION II. E llIPMENT MAINTENANCE DATA
Belt Filter Press
Manufacturer: Enviroquip, Inc.
Model: Series 518, Model 1700
Number: 1
Capacity: 1.5 meter, 1050 lbs dry solids/hour, 75 gpm hydraulic capacity
Service Contact:
517- 536- t644
Lime Pasteur uation_.Eauipuent
Manufacturer: RDP Company
Dewatered Sludge Screw Conveyor: 1500 lb/hr dry solids
Pasteurization Vessel: 4000 lb/hr dry solids
Final Product Screw Conveyor: 4000 lb/hr dry solids
Silo: 30 tons capacity
Service Contact: B rad m/ I /_ ;y, a H
610-G o-c/oo 13
NOTE: $EL++' E UIPtiIEN'I" UPT:RA7'ION AND I�IAIN1'EI�iAa1�CE 1tiIANUALS IN TOWN
OF WAYNESVILLE WASTEWATER TREATMENT PLANT OFFICE FOR
MAINTENANCE DETAILS AND SCHEDULES.

SECTION III. SAFETY
Site Restriction and Security
Only authorized personnel shall be permitted to enter any equipment building or directly access
equipment. The general public shall not be permitted on the site unless accompanied by
authorized Town of Waynesville operations or maintenance personnel.
Personnel Training
Maintenance of Biosolids System Equipment shall be performed only by properly trained
personnel who are thoroughly familiar with the facility, equipment, and safety rules for the Town
of Waynesville Wastewater Treatment Plant. Refer to the operation and maintenance manual for
each individual equipment component prior to beginning any repairs.
Subcontractors
All subcontractors shall be required to register with the Town of Waynesville Operations office
prior to entering any equipment buildings or working on any equipment. Town of Waynesville
maintenance staff shall provide necessary safety information to subcontractors prior to allowing
the subcontractor to enter the equipment site.
Emergency Contacts
In the event of an emergency, contact the following:
1. For All Emergencies: Dial 9-1-1
2. Haywood County Emergency Services: [phone]
3. Haywood County Sheriff: [phone]
4. Town of Waynesville Police: [phone]
5. Town of Waynesville Wastewater Treatment Plant: [phone]
6. Haywood Regional Medical Center: 262 Leroy George Dr., Clyde, NC [phone]

SECTION IV. SPILL CONTROL
In the event of spillage of dry or liquid chemicals or products, or biosolids materials outside of
contained areas, Town maintenance staff shall take immediate actions to contain the spill.
Containment of the spilled material to prevent the material from human contact or from draining
into waterways shall be achieved.
In the event that a hazardous material is spilled and requires containment or disposal, Town
maintenance staff shall contact the Haywood County Emergency Services at [phone]. If
a dangerous situation with hazardous materials occurs, call 9-1-1.

SECTION V. SAMPLING AND MONITORING
Sampling and monitoring of the biosolids shall be in accordance with the NCDENR Permit
issued for the facility. A copy of the Monitoring and Reporting Requirements from the permit
are provided in the Appendix.
The lime/sludge mixture enters a pasteurization vessel where supplemental electric heat is added
to maintain the temperature of the sludge at 158°F (70°C) for thirty minutes to meet the pathogen
reduction requirements of 40 CFR Part 503. Temperature probes monitor the sludge temperature,
and the speed of the conveyor is designed so that the product remains in the vessel for the full
thirty minutes to achieve pasteurization. The vector attraction reduction requirements of 40 CFR
Part 503 are met by adding sufficient quicklime or LKD to raise the pH of the sludge to at least
12, maintain the pH at 12 for two hours and then at 11.5 for an additional 22 hours. Town
operation and maintenance staff shall take samples and perform testing to confirm these
conditions for pathogen and vector attraction are met, and shall record all sampling and test
results in the log book in the Wastewater Treatment Plant laboratory.
Residuals generated shall be analyzed to demonstrate that they are non -hazardous under the
Resource Conservation and Recovery Act (RCRA) at the frequency specified in the NCDENR
permit. The results shall be maintained on file at the Town of Waynesville for a minimum of
five (5) years as required by the permit. A corrosivity, ignitability, and reactivity analysis, as
well as a Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted on
residuals generated. The frequency of testing is dependent upon the amount of product that is
land applied on an annual basis. Refer to the tables in the permit and provided in the Appendix.

APPENDIX A
BIOSOLIDS SYSTEM DRA`VINGS

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APPENDIX B
BIOSOLIDS SYSTEM PHOTOGRAPHS

MDUALS PRO
SSING FACILITY

s7 w
a

AG. LIME FEED AUGER
R
i

,.I— -MEN T.
F]
FIV,

9 ]FINAL PRODU T DISCHARGE
�

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" .

APPENDIX C
MONITORING AND REPORTING REQUIREMENTS

i4. If the land application sites are to be overseeded (e,g., bermuda grass in the summer and rye
grass in the winter with BOTH crops to receive residuals), then the second crop shall receive
an application of PAN at a rate of no greater than SO pounds per acre per year. This practice
shall. be allowed as long as the second crop is to be han•ested. if the second crop is to be
planted for erosion control only and is to be tilted into the soil, then no residuals shall be land
applied to these sites because the PAN will essentially be retumed to the soil.
Prior to application of PAN to permitted sites at rates exceeding the agronomic rate, the
Permittee must submit and receive approval by the Division
15. Should any of the residuals generated by the residuals source -generating facilities listed in the
most recently -certified Attachment A of this permit contain a high salt content (i.e., high
sodium adsorption ratio (SAR) of five (5) or higher), Elie exchangeable sodium percentage
(ESP) or other method as approved by the Division, using the results from the arunual soils
analysis as required by this permit, shall be monitored on all of the land application sites.
The local Cooperative Extension Office, the Department of Agriculture and Consumer
Services, the Natural Resource Conservation Service, a North Carolina -licensed Soil
Scientist, or other agronomist shall review the results and make recommendations regarding
soil amendments (e.g., gypsum, etc.) or other ameliorative mechanism for maintaining the
integrity of the site in terms of suitability for land application of residuals and maintaining
conditions conducive to crop growth. The Perrttittee shall implement such recommendations
accordingly and shall maintain written records of each monitoring event that includes details
of the sites covered and rate of soil amendment application.
M. MONITORING AND REPORTENG RE UIREMENTS
I. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue
analyses) deemed necessary by the Division to insure protection of the environment will be
established and an acceptable sampling and reporting schedule shall be followed.
Residuals generated by each approved residuals source -generating facility shall be analyzed
to demonstrate that they are non -hazardous under the Resource Conservation and Recovery
Act (RCRA) at the frequency specified in the most recently -certified Attachment A of this
permit, and the results shall be maintained on file by the Permittee for a minimum of five
years. A corrosivity, ignitability, and reactivity analysis as well as a Toxicity Characteristics
Leaching Procedure (TCLP) analysis shall be conducted on residuals generated by each
approved residuals source -generating facility. If residuals generated by a particular residuals
source -generating facility are land applied at a frequency less than that which is specified in
the most recently -certified Attachment A of this permit, the analyses shall be required for
each residuals land application event. Only residuals that are generated by the residuals
source -generating facilities that are identified as being exempt from this condition in the most
recently -certified Attachment A of this permit shall not be required to comply with this
monitoring requirement.

The TCLP analysis shall include the following parameters (i.e., note the regulatory level in
milligrams per liter in parentheses):
Arsenic (5.0)
Barium (100.0)
Benzene (0.5)
Cadmium (1.0)
Carbon tetrachloride (0.5)
Chlordane (0.03)
Chlorobenzene (100.0)
Chloroform (6.0)
Chromium (5.0)
m-Cresol (200.0)
o-Cresol (200.0)
p-Cresol (200.0)
Cresol (200.0)
2,4-D (10.0)
1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
1,1-Dichloroethylene (0,7)
Pyridine (5.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Endrin (0.02)
Silver (5.0)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Heptachlor (and its hyd,oxide) (0.008)
Toxaphene (0.5)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Hexachloroethane (3.0)
2,4,5-TrieWorophenol (400.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
Mercury (0.2)
Vinyl chloride (0.2)
Methoxychlor (10.0)
Methyl ethyl ketone (200.0)
After the residuals have been monitored annually for two years, the Permittee may submit a
request to the Division for a permit modification to reduce the frequency of the TCLP
analysis. In no case, however, shall the frequency of TCLP monitoring be less than once per
permit cycle when residuals are sold or given away.
An analysis shall be conducted on residuals generated by each residual source -generating
facility listed in the most recently certified Attachment A of this permit. An analysis shall be
conducted by the Permittee on the Class A EQ residuals product at a frequency that is
dependent on the dry tons of Class A EQ residuals product distributed or expected to be
distributed during the calendar year for application to the land. The monitoring frequency
schedule shall be as stipulated in the following table:
Amount of Product
Amount of Product
Distributed for
Distributed for
Application to the Land
Application to the Land
Monitoring Frequency
(metric tons per
(short tons per
365-day period)
365-day period)
0 < mDT/yr < 290
0 < DT/yr < 319
Once per Year
290 = mDT/yT < 1,500
319 = DT/yr < 1,650
Once per Quarter
(Four Times per Year)
1,500 = mDT/yr < 15,000
1,650 = DT/yr < 16,500
Once per 60 Days
(Six Times per Year)
15,000 = mDT/yr
16,500 = DT/yr
Once per Month
(12 Times per Year)

The results shall_ be iaintained on file by the Permittee for a minimum of five years. The
analysis shall include, but shall not necessarily be limited to, the following parameters:
Aluminum
Magnesium
Phosphorus
Ammonia -Nitrogen
V
Mercury
Potassium
Arsenic
Molybdenum
Selenium
Cadmium
Nickel
Sodium
Calcium
Nitrate -Nitrite Nitrogen
Total Kjeldahl Nitrogen
Copper
pH
Total Solids (Percent)
Lead
Plant Available Nitrogen
(By Calculation)
Zinc
After the residuals have been monitored as specified above for two years at the frequency
specified in the most recently -certified Attachment A of this permit, the Permttee may
submit a request to the Division for a permit modification to request a reduction of this
monitoring requirement, In no case, however, shall the frequency of monitoring be less than
once per year when residuals are sold or given away.
4. Residuals generated by each residuals source -generating facility listed in the most recently -
certified Attachment A of this permit shall be monitored for compliance with Condition I. 7,
at a frequency that is dependent on the dry tons of Class A EQ residuals product distributed
or expected to be distributed during the calendar year for application to the land. The
monitoring frequency schedule shall be as stipulated in the following table:
Amount of Product
I Amount of Product
Distributed for
V Distributed for
Application to the Land
Application to the Land
Monitoring Frequency
(metric tons per
(short tons per
365-day period)
` 365-day period)
0 < mDT/yr < 290
0 < DT/y,r < 319
Once per Year
290 = mDT/yr < 1,500
319 = DT/yr < 1,650
Once per Quarter
(Four Times per Year)
1,500 = mDT/yr < 15,000
1,650 = DT/yr < 16,500
Once per 60 Days
(Six Times per Year)
J
15,000 = mDT/yr 1
16,500 = DT/yr
Once per Month
(12 Times per Year)
The results of all analyses and records of all operational data shall be maintained on file by
the Permittee for a minimum of five years. Data to verify pathogen and vector attraction
reduction of the residuals shall be maintained on file by the Permittee for a minimum of five
years. The required data shall be specific to the stabilization process utilized, but also shall
be sufficient to demonstrate clear compliance with the Class A pathogen requirements and
site restrictions in 15A NCAC 02T .1106 (a) and (b), and one vector attraction reduction
requirements in 15A NCAC 02T .1107 (a) shall be met.

Town of Waynesville WWTP
503 Biosolid Sampling Plan
1.) Vector Attraction ph
Sampling Point — conveyor from pasteurization vessel to truck
Frequency — each shift biosolids are processed
Type — grab samples
Certified Lab — Waynesville WWTP lab
Staff— Ronnie Norris, Plant Superintendent
Mark Jones, Lab Manger
Jeff Evans, Lab Analyst
2.) Pathogen Reduction and all other required parameters
Sampling Point — biosolids storage area
Frequency — bimonthly
Type —12-24 grab samples composited
Certified Lab. — Environmental Testing Solutions Inc.
Pasteurization vessel temperatures are continuously monitored to ensure all material
reaches a minimum of 158 degrees Fahrenheit.
Pasteurization vessel also has a 30 minute detention time.
Page 127

State of North Carolina
Department of Environmental Quality
PXDivision of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
® For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Town of Wajy-nesville
Status
Code e
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current b
Proposed
R
Town of Waynesville
Waynesville WWTP
Haywood
WQ0013116
1,065
1,065
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Town of Waynesville
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or Q Private.
Facility permit issued by: ® Div. of Water Resources, Div. of Environmental Health,
or ❑ Other (explain: 1).
3. Facility contact person and title: Jeff Evans, WWTP Daily Supervisor
Complete mailing address: 129 Legion Dr.
City: Waynesville State: NC Zip: 28786-
Telephone number: [phone] E-mail address: ievans _ waynesyillenc.go
4. Facility physical address: 56.6 Walnut Trail Rd.
City: Waynesville State: NC Zip: 28785
Coordinates: Latitude: 350 32' 30" Longitude: 82. 57' 04"
Datum: NAD 83 Level of accuracy: 5 mm
Method of measurement: Haywood GIS
5. Purpose of the facility:
® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: % industrial and % domestic)
0 other (explain: ! ).
6. Does the facility have an approved pretreatment program: ❑ Yes ❑ No
7. Facility permitted/design flow: 6_0 MGD and facility average daily flow: 3_4 MGD
8. Average amount of residuals being generated at this facility 800 — 1,100 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Anaerobic digested sewage sled a that is lime stabilized and heatasteurized
Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
® 40 CFR Part 503 or ❑ 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102f 6) as:
Biological ❑ Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes is no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Environmental Testing Solutions and Date of analysis: May 2019
Passed corrosivity test: yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: . OF (> 140°F)
Passed reactivity test: E yes ❑no. HCN: 0.338 mg/kg (<250) & 112S: 9.63 mg/kg (<500)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
.25
Hexachlorobenzene
0.13
.1
Barium
100.0
2.50
Hexachloro-1,3-Butadiene
0.5
.1
Benzene
0.5
.10
Hexachloroethane
3.0
.1
Cadmium
1.0
.05
Lead
5.0
.25
Carbon Tetrachloride
0.5
.10
Lindane
0.4
.0005
Chlordane
0.03
.005
Mercury
0.2
.002
Chlorobenzene
100.0
.10
Methoxychlor
10.0
.0005
Chloroform
6.0
.10
Methyl Ethyl Ketone
200.0
.20
Chromium
5.0
.10
Nitrobenzene
2.0
.10
m-Cresol
200.0
.10
Pentachlorophenol
100.0
.10
o-Cresol
200.0
.10
Pyridine
5.0
.10
p-Cresol
200.0
.10
Selenium
1.0
.25
Cresol
200.0
.20
Silver
5.0
.10
2,4-D
10.0
.10
Tetrachloroethylene
0.7
.10
1,4-Dichlorobenzene
7.5
.10
Toxaphene
0.5
.0005
1,2-Dichloroethane
0.5
.10
Trichloroethylene
0.5
.10
1,1-Dichloroethylene
0.7
.10
2,4,5-Trichlorophenol
400.0
.10
2,4-Dinitrotoluene
0.13
.10
2,4,6-Trichlorophenol
2.0
.10
Endrin
0.02
.0005
214,5-TP (Silvex)
1.0
.10
Heptachlor and its Hydroxide
0.008
.0005
Vinyl Chloride
0.2
.10
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Disti-lbution/Lanrl Applicatioti: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Environmental Testing Solutions and Date of analysis: November 2019
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
6.07
Cadmium
85
39
1.32
Copper
4,300
1,500
183
Lead
840
300
15.1
Mercury
57
17
0.59
Molybdenum
75
n/a
3.65
Nickel
420
420
13.10
Selenium
100
100
3.90
Zinc
7,500
2,800
490
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: N/A and Date of analysis: N/A
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg1kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 55 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Environmental Testing Solutions and Date of analysis: November 2019
Parameter
Result
(mg/kg) Dry
Aluminum
6,875
Ammonia -Nitrogen
247.5
Calcium
144,650
Magnesium
4,004
Nitrate -Nitrite Nitrogen
7.70
pH (Standard Unit)
12.0
Phosphorus
3,096.50
Potassium
924
Sodium
243.10
Total Kjeldahl Nitrogen
91.90
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1.20
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1") Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
651.34
929.53
Injection/Incorporation
695.34
973.53
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: N/A
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02TA 106, specify how residuals will meet the pathogen reduction requirements:
a. Far Distrihutiorr/Larrd A licatiorr o C7ass A or F uivalent:
® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
® Alternative 5 [15A NCAC 02T. 1 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, Q heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or Z pasteurization.
b. For Land Avvlicadon of Class B:
❑ Alternative 1 [15A NCAC 02T. 1 106(c)(1)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, 2 anaerobic digestion,
0 composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt - If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
® Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T. 1 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

Attachment RSC Item S.
(Generating Facility Information)
TABLE OF CONTENTS
VicinityMap..............................................................................
Process Flow Diagram and Narrative.. ................................ ......
QuantitativeData..........................................................................
SamplingPlan................................................................................
......................................... I
.............. 2-3
.........................................4
........................ 5

lop,
W ui
LL,
u.cc
O
64

NARRATIVE DESCRIPTION OF THE TOWN OF WAYNESVILLE
WASTEWATER TREATMENT SLUDGE MANAGEMENT
The Town of Waynesville Wastewater Treatment Plant generates both primary sludge with
primary clarifies and waste activated sludge from the secondary activated sludge process at the
Wastewater Treatment Plant.
"The two settled sludges are gravity thickened in primary and secondary gravity sludge
thickeners. The gravity thickened sludges are pumped to an anaerobic digester for further
volatile solids and pathogen reduction. The digested sludge is then dewatered with a 1.5 meter
belt press. The dewatered sludge is blended with lime kiln dust as well as agricultural lime (as of
December 2013} to achieve the required vector attraction reduction requirements and is heat
pasteurized to 158 degrees Fahrenheit or greater for pathogen reduction requirements. The lime
stabilization and heat pasteurization equipment used is RDP technologies thermoblender and 30
minute detention time pasteurization vessel.
Listed below are facts about The Town of Waynesville Wastewater Treatment Blend Processing
and Distribution:
• All biosolids produced are stored under a covered shed onsite. The biosolid product is
distributed to the public free of charge.
• The residuals are produced and treated at the same location.
• All residuals are stored and processed onsite at the Wastewater Treatment Plant.
• All leachate collected is returned to plan influent.
• Detention time from anaerobic digester through the belt press lime sludge blender and
pasteurization vessel to discharge through the conveyor is approximately one hour.
Occasionally more time is used to turn the processed residuals in the storage shed to
produce a more workable product and decrease percent moisture.
• All final products are stored onsite under a covered shed.
• 'The final product is stored for approximately 3 — 6 months depending on the season.
During spring and fall, the product is in demand more than summer and winter.
• The final product is given away in bulk to the local farmers.
Each year, approximately 800 — 1,100 dry tons per year are produced and distributed. The
destination of final product has been to local farmers and local commercial lime spreaders. All
recipients' names are kept on file at the treatment plant.
Page 1 2

TREATMENT PROCESS SCHEMATIC�
VV L
(MM-
f'iiir.:I
Mu li ibu t ion

V, .
TING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
CLASS A ANNUAL DISTRIBUTION AND MARK
Town of Wati'nesville Mark Jones
W 00131 10 FACILITY NAME: 1iarvood OPERATOR:
WQ PERi411T �: Q COLINTI'. "Residual ln" Volume only) and Part C)
PHONE: [82R)452-4685
'FACILITY TYPE (please check one): 0 Surface Dis}3osa! (complete Part A [Sourarts1 , and C)
0 Distribution and Marketing (complete P�rtsif No skip parts A, B, C and certify form below
Ye_s No Part B*:
Was the facility in operation [luring the past callenrtd,,*year' Reci lent Information
Volume (dry tons) Name(s) Volume (dry) tons Intended use(s)
Sources(s) (include NPDES # if Amendment/ Residual In Product Out
Month applicable) 131.6 Liming Agent
} p Bulking Agent 67.2 Brandon James for
46.91 20.29 05 50.4 Tim Kelley 84
106.4 f ia•
.lanuary 24.35 26.64.4 Adrian Presnell
February 45.28 19.12 Doyle Smith 448
March 48.41
7.59 56 2.24 Siila�;e
112 Bart Casnphei!
68.02 240.8 Fields
April 43.98 117.6 Cod}• Worley
1•Iay 70.41 47.19 Johnny James 112
54.08 126 11.2
,tune 71.92 156.8 James Robinson
3 ul�• 70.48 86.32
64.99 120.4
:august 55.41 61.6
September 49.75 11.85
0
October 0 0 0
November 0 0
December 1136.24
Total from FORM DMSDF (sup} 526.9 4l}5.5 932.4
Annual (dry tons):
i otnls: Lime Kiln Dust 13ull:in¢ f�gent{sy used:
Amendmcnt(s) used: Total Number of Form D M S D F (Supp
I]MS>]I (suPP)l
* If more space is requirCO. aklul-" wuu - -
Part C: land apEl plication permit 0 Yes If No, Explain in Narritive
No
Facility was compliant during the past
b low) issued by the Division rtof Water Resources: co ies of certified laboratory results are attached.
(including but not limited to items
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3 p
2_ All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources
3. No contravention of Ground Water Quality Standards occurred at a monitoring well. violationsa
"1 certify, under penalty of law, that the above information is, to the best of my knowledge and belief, t `ne, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for now g
_
7,p a.' Date
Date Signature of prepare
Si n ur f mittee (if different fromPermittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

Town of Waynesville WWTP
503 Biosolid Sampling Plan
1.) Vector Attraction ph
Sampling Point — conveyor from pasteurization vessel to truck
Frequency — each shift biosolids are processed
Type — grab samples
Certified Lab — Waynesville WWTP lab
Staff— Jeff Evans, Daily Plant Supervisor
Mark Jones, Lab Supervisor
2.) Pathogen Reduction and all other required parameters
Sampling Point — biosolids storage area
Frequency — bimonthly
Type —12-24 grab samples composited
Certified Lab. — Environmental Testing Solutions Inc.
Pasteurization vessel temperatures are continuously monitored to ensure all material
reaches a minimum of 158 degrees Fahrenheit.
Pasteurization vessel also has a 30 minute detention time.
*Note: See O&M manual for additional sampling procedures and policies.
Page 15

Attachment RSC Item C.
(Residuals Quality Information)
Table of Contents
Laboratory Reports & Operational Data........................................................................................................
PAN (Plant Available Nitrogen) Calculations.......................................................................................... 1-2
LaboratoryData.............................................................................................................................. See Tab
Load& Temperature Log................................................................................................................ See Tab
Vector Attraction Reduction pH Values......................................................................................... See Tab
TCLP................................................................................................................................................ See Tab

PAN Calculations for Residuals
Date
Parameter
mg/kg dry Wt.
Ibs/dry ton
1/7/2015
TKN
8010
17
3/11/2015
TKN
9560
14.8
5/5/2015
TKN
8380
15.4
7/8/20151
TKN
7680
19.2
9/9/20151
TKN
9360
16.4
11/3/20151
TKN
8010
14.2
Average MG/Kg dry WT
Average LBS/Dry Ton
8500
16.16666667
Date
Parameter
mg/kg dry Wt.
Ibs/dry ton
1/7/2015
Ammonia-N
180
0.36
3/11/2015
Ammonia-N
880
1.76
5/5/2015
Ammonia-N
150
0.3
7/8/2015
Ammonia-N
120
0.24
9/9/2015
Ammonia-N
170
0.34
11/3/2015
Ammonia-N
130
0.26
Average MG/Kg dry WT
Average LBS/Dry Ton
271.6666667
0.543333333
Date
Parameter
mg/kg dry Wt.
Ibs/dry ton
1/7/2015
Nitrate -Nitrite
49.7
0.0994
3/11/2015
Nitrate -Nitrite
560
1.12
5/5/2015
Nitrate -Nitrite
64
0.128
7/8/2015
Nitrate -Nitrite
5.5
1 0.011
9/9/2015
Nitrate -Nitrite
26.9
0.0538
11/3/2015
Nitrate -Nitrite
29.1
0.0582
Average MG/Kg dry WT 122.5333333
Average LBS/Dry Ton 0.245066667
Mineralization Rate for Anaerobically Digested Residuals is
M R= 20%
Pan = (MR)*(TKN-NH3) + .5*(NH3) + (Nitrate+Nitrite)
Date
Parameter
Amount
Units
1/10/2012
PAN
3.6074
PPM Dry Wt.
3/6/2n�12
PAN
4.608
PPM Dry Wt.
5/8/2012
PAN
3.298
PPM Dry Wt.
7/10/2012
PAN
3.923
PPM Dry Wt.
9/11/2012
PAN
3.4358
PPM Dry Wt.
11/6/2012
PAN
2.9762
PPM Dry Wt.
Avg. PAN
3.6414
PPM Dry Wt.
IPPM=IMG/KG
Total PAN to be land applied per year
Page 1
PAN Calcs.

Total Dry tons of Residual to be land applied per year
Four year average volume of residuals produced is 960 metric tons
960 metric tons 1057.92 tons
Date
PPM DRY Wt.
LBS/Dry Ton
1/10/2012
0.0072148
1.44296E-05
3/6/2012
0.009216
0.000018432
5/8/2012
0.006596
0.000013192
7/10/2012
0.007846
0.000015692
9/11/20121
0.0068716
1.37432E-05
11/6/20121
0.0059524
1.19048E-05
Avg LBS/Dry ton 1.45656E-05I
Date
Total PAN LBS
1/10/2012
7.632681216
3/6/2012
9.74979072
5/8/2012
6.97804032
7/10/2012
8.30044032
9/11/2012
7.269603072
11/6/20121
6.297163008
Average 7.704619776
Page 2 PAN Calcs.

r'TAR'
Environmental Testing Solutions, Inc. Certificate of Analysis
Project name: Town of Waynesville WWTP
Collection date:
Gate received:
5-Feb-19
5-Feb-19
PO Box 7565
Asheville. NC 28802
Phone: [phone]
Fax: [phone]
Project number:
Sample identification: .503 Lime Sludge - Composite Sample number:
190205.522
165680
Date
Parameter
Method
Result
RL
Units
Analyst Footnotes
Analvzcd
Arsenic
6010 C
7.26
5.34
mg/kg
13-Feb-19
MLR I
Cadmium
6010 C
<2.14
2.14
mg/kg
13-Feb-19
MLR 1
Copper
6010 C
121
2.14
mg/kg
13-Feb-19
MLR I
Chromium
6010 C
24.6
5.34
mg/kg
13-1--eh-19
MLR I
Lead
6010 C
13.0
5.34
mg/kg
13-Feb-19
MLR I
Molybdenum
6010 C
<5.34
5.34
mg/kg
13-hcb-19
MLR I
Nickel
6010 C
18.4
2.14
mg/kg
13-Feb-19
MLR I.
Selenium
6010 C
<5.34
5.34
mg/kg
13-1-6-19
MLR 1
Zinc
6010 C
293
5.34
mg/kg
13-17eb-19
MLR I
Aluminium
6010 C
10500
534
mg/kg
15-Feb-19
MLR I
Calcium
6010 C
249000
2720
mg/kg
19-tar-19
MLR 1
Magnesium
6010 C
5510
267
mg/kg
13-Feb-19
MLR 1
Potassium
6010 C
1700
10.7
mg/kg
13-Feb-19
MLR 1
Sodium
6010 C
510
10.7
mg/kg
13-Feb-19
MLR l
Mercury
7471B
0.63
0.043
mg/kg
11-njer-19
TLT I
Total Kjeldahl Nitrogen
351.2
14700
692
mg/kg
i-n4ar-19
LEW I
Nitrate + Nitrate
300.0
<40.0
40.0
mg/kg
14-Feb-19
JMM I
Total Nitrogen
Calculation
14700
692
mg/kg
I-Niar-17
LEW I
Total Phosphorus
200.7
4180
267
mg/kg
13-Feb-Io
MLR I
Total Solids
SM2540 G
45.5
0.10
%
8-Feb-19
MLR I
pli in Soil
SW 846 9045D
12.2
0.10
S.U.
6-F&19
MS 2
%Total Solid
SM 2540 G
46
0.10
%
6-1`6-19
KF.K
Ammonia Nitrogen
EPA 350.3
630
8.7
mg/kg
7-Feb.19
KEK
Sodium Absorption Ration
CALL
4.14
mg/kg
i9-Mar-19
KEK
Plant Avaliable Nitrogen
CALC
3129
mg/kg
t9-Mar-19
KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Sample analyzed outside holding time.
Date reviewed: ©%J-l�i,��i NC Certification Number: 600
Data reviewed by: [Geller 1•1. Keemm SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
Signature: �,/L-
This report should not be reproduced, cxept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the smnples submitted for analysis.

;. tCCRCn
Rogers &. Callcott
� TNI
ENVIRONMENTAL
toan�p
Laboratory Report
Client
Gnvironmental'resling Solutions
Project: Waynesville WWTP
Kelley E. Keenan
Work Order: 9020293
351 Depot St,
Received: 0206i2019 09:00
Asheville, NC 288014310
Dear CI ienr
Rogers and Cullcott appreciates the opportunity to be of service to you. 'rhe attached laboratory services report includes analytical results and chain of
custody for samples that were received on February 06, 2019. Rogers and Callcou maintains a formal QA/QC program. Unless otherwise noted, all
analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses mel the QA'QC confidence
interval for each test method unless otherwise qualified. Estimated uncertainly is available upon request.
Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. Ifyou receive this message by
mistake, please notify Rogers and Callcou immediately.
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at any.ashleyCarogersandcalIcou.com or
(864)-335-4962 Ifyou have any questions about this report.
Report Approved By:
Amy Ashley
Project Manager
This report nray nor he reproduced, except in/dl, aIdmut nrilren pen -mission fi-nw Rogers & Callcoll, Inc•
-0 Box 5655 Grecnvlflrn, SC 29606 426 € w4 r•�,{t \Vay rer—nviile, ;G 296 r" n 564.23£.1-556 fax 8 4,232.6140 rogersal1dcalleott.Caln
_ .. an.-„� is yv•- , . •:I [.,r , .nY
Page 1 of 11

Rogers & Callcott
ENVIRONMENTAL
Certificate of Analysis
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 288014310
Sample Number Sample Description
9020293-01 Waynesville WWTP 503 Lime Sludge - Comp
South Carolina Greenville Laboratory Idenlific•ation 23105
South C'arnliaa Columbia Laboratory Idenliicarion 40572
Ator'lh Carolina Lahorolor7. C'errifrealion Number 27
North Carolina Drinking 14arer Lab A4unber• 45710
lVFLAP L'lah Certificate Number SC000042014-1
Georgia Drinking 11raler• Lab ID 880
Project: Waynesville WWTP
Work Order: 9020293
Received: 02=06/2019 09:00
Matrix Sampled Type
Sludge 02105'19 08:45 Composite
PO Sax 5655
Greenville, SC 29606 4'6 rziirforexr, MFty Greenxl e, SC 29607
ma-r. 864.232.15 6 r;,. 864,232.6mo
roper-sa dcalICdCC.com
03f19= 2019 14,11
This report mqy nor he reproduced, except in fill/, n ilhuru
written pernussion front Rogers & Culicoa, Inc
Page 2 OI 1 1)

` Rogers & CaRcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 901-0293
Asheville, NC 28801-4310 Reported: 03/19/19 14:11
Sample Data
Sample Number 90'-0293-01
Sample Description Waynesville WWTP 503 Lime Sludge - Comp collected on 02r05119 08:45
Reporting
Parameter Result Limit knits DF Analyzed
Method
Flag Analyst
[latch
General Chemistry Parameters
Nitrate as N
ND
20A
mg kg dn-
1.00
02/14/19 17:11
EPA 300.0
JMM
B9BO707
Nitrite asN
ND
20.0
mg'kgdry
1,00
02/14/19 17:11
EPA300.0
SI JMM
B9130707
Total Kjeldahl Nitrogen
14700
692
mEkg dry
10.0
03101,19 14:14
EPA 3512)
LEW
B9B1205
"total Nitrogen tTKN�Nitrate+Nitrite)
14700
692
mg'kgdry
10.0
01101/19 14:14
-
LEW
B9130468
Total Solids
45.5
0.10
%
1.00
02/08/19 1L20
SM 2540G
MLR
B9130362
Total Metals
Mercury
0.63
0.043
mgkg dry
1.00
02111.119 12:52
EPA 7471 B
TLT
B960275
Aluminum
10500
534
mgkgdry
50.0
02•'15119 16:39
EPA6010D
MLR
B9BO454
Arsenic
7.26
5.34
mg'kg dry
1.00
02/13i 19 21:29
EPA 601OD
MLR
139130454
Cadmium
ND
2.14
mg`kgdry
1.00
02/13/19 21:29
EPA 601OD
MLR
139BO454
Calcium
249000
2720
mg'kgdn
500
03!19i19 13:14
EPA 6010D
LMC
09131139
Chromium
24,6
5.34
mg'kg dry-
1,00
02113/19 211:29
EPA 601OD
MLR
139B0454
Copper
121
2,14
mg`kg dry
1,00
02/13119 21:29
EPA 601OD
MLR
119BO454
Lead
13.0
5.34
mg'kg dry
1.00
021-13119 21:29
EPA 601OD
MLR
B9BO454
Magnesium
5510
267
mg'kgdry
50.0
02/15-19 16:39
FrA60101)
MLR
B9BO454
Molybdenum
ND
5.34
mglcg dry
1.00
02113119 21:29
FPA 601OD
MLR
B9130454
Nickel
18.4
2.14
mg`kg dry
1.00
02/13i 19 21:29
t:w� 6010D
NlLR
B9BO454
Potassium
1700
10.7
mg'kgdry
I
02i13i19 21:29
EPA enloD
MLR
B9130454
Selenium
ND
5,34
mg kgdry
1.00
02/13i19 21:29
EPA 60101)
MLR
B9B0454
Sodium
510
10,7
mg'kgdry
I
02 13/19 21:29
EPA 60101)
MLR
B9130454
Tolal Phosphorus as P
4180
267
mg,kg dry
50.0
02/13/19 2125
ECA601oD
MLR
B9BO454
Zinc
293
5,34
mg1cg dry
1.00
021,13/ 19 21:29
EPA 6010D
MLR
B9110454
PO Rox 5655 c,., t:, i,�, SC 2a60• 4;26 fb rforest'Way Green eie, SC 29607 . ,.ri �� 1,�3- 5 � ti:,E �� Z32.6i lJ rogersandcallcott.cvm
,>,y rmtrt:z.,ir •mvned roxnpirny
03%7912019 14:11 77ik mporimap nor be reproduced. exrepr in jd1, it l7how wriluen permis:rien rnni Rogers & Calleou, Inc. Page 3 of 11

Rogers & Callcott
ENVIRONMENTAL
L"nvironmental Testing Solutions project: Waynesville WWTP
351 Depot St. Work Order: 9020293
Asheville, NC 28801-4310 Reported: 03/19J19 14:11
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source %RFC RPD
Parameter Result Limit Units Level Result %RFC Limits RPD Limit Flags
Batch B9B0362 - General Prep - Solids
Duplicate (B9B0362-DUPI) Source: 9020293-01
Total Solids 45.3 0,10 %
Batch B9B0707 - General Prep - IC
Blank (B9B0707-61,KI)
Nitrate as N
Nitrite as N
Blank (B9B0707-BI,K2)
Nitrate as N
Nitrite as N
1.CS (B9B0707-BSI)
ND 20.0 rng'kgdry
ND 20.0 mg°kkdry
ND 20.0 mg'kgdry
ND 20.0 mgrkg (try
45 5
Nitrate asN
ND
20,0
mgtkgdry
1.50
100
90-110
Nitrite asN'
ND
W
mgrkg dry
0.500
103
90-110
Duplicate (B9B0707-DUPI)
Source: 9020293-01
Nitrate as N
— — ND
20.0
mgrkg dry
ND
--- f�
Nitrite asN
ND
20.0
mg/kgdry
ND
klatris Spike (B9B0707-MS1)
Source: 9020293-01
Nitrate as N
ND
10.0
mgrkg dry
14.1
ND
66
65-130
Nitrite as N
ND
20.11
mgrkg dry
2.95
ND
56
65-130
Reference (B9$0707-SRMI)
Nitrate as N
208
20.0
mg -kg dry
279
75
59,5-110
Reference (B960707-SRM2)
Nitrite as N
ND
20.0
mg/kg dry
4.54
91
70-130
Batch B9B1205 - EPA 351,2-TKN
Blank (B981205-BLKI)
Tool Kjcldahl Nitrogen
ND 8.79 mgrkg wet
0.4 1.5
30
30
SI
Roo 5655 11r-e-enwisie, SC 29606 425 F:urfarest Wiy Greenville, SC 21607 864.73<1556 (,x, 864,232:65to rope -sandCallcc> C cow
03i1912019 14-11 This report tray not he reproduced, eeeepr in fir1l, rrkltnut uririen permission frorn Rogers & Callcon. hit•. Page 4 Ol 1 1

.� Rogers & Cattcott
E NV IRON MENTAL
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9020293
Asheville, NC 28801-4310 Reported-, 03;19/19 14:11
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Unks Level Result %REC Limits RPD Limit Flags
Batch B9B1205 - EPA 351.2=TKN
LCS (B9B1205-BS1)
Total Kjeldahl Nitrogen 254 8-75 mg'kg wet 262 97 0-200
Duplicate (B9B1205-DUP1) Source: 9020293-01
Total Kjeldahl Nitrogen 153010 i 13 mgkg dry 14700 4 30
Reference (B981205-SRNI1)
Total Kjeldahl Nitrogen 100 32.9 mg kg wet 1090 104 53.6-14U
C) Box 5 55 . Greenivi;l . SC 29666 . _ ....rfol est way —i eenv4le, a? 29940 864 232J55 tax S 3,232:6No f ogersrandcal lcott.com
a:ie•titplsy'!). idwnvpirOnIIImIV
03i1912019 14:11 This report man not be reproduced. e cept in ftdl. without woven permission from Hogerr & Callcoo. Me, Page 5 of � 1

Rogers &callcott
ENV IRc"7. NMEN TAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9020293
Asheville, NC: 28801-4310 Reported: 03 19'19 14:1 t
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limil Units Level Result %REC Limits RPD Limit Flags
Batch B9Bo275 - EPA 7471 B
Blank (B9Bt1275-BLKI)
Mercury
Blank (B9110275-BLK2)
ND 0.00020 mgrkg wet
Mercury
ND
0.019
me- kgwet
LCS (B9B0275-BSI)
Mercury
0.0048
0.0001-0
mg -kg wet 0.00500 96 80-120
LCS (B9B0275-BS2)
Mercury - —T T
0.52
0.020
mg'kgwet 0.494 106 80-120
Reference (B9B0275-SRMI)
Mercury
14
0.039
mg -kg wet 11-5 110 60.3.140
Batch B9B0454 - EPA 3050B
Blank (B9B0454-BLKI)
Aluminum 4
ND
0.10
mg'kgwet
Arsenic
ND
0.05
mgkgwo
Cadmium
ND
0.02
mg'kg wet
Chromium
ND
0.05
mg'kg wet
Copper
ND
0.02
mg'kg wet
Lead
ND
0.05
mgkg wet
Magnesium
ND
0.05
mgfkg.wet
Molybdenum
ND
0.05
mg/kg wet
Nickel
ND
0.02
mg%kg wet
Potassium
tiD
010
mg='kgwet
Selenium
ND
0.05
mg.`kgwet
Sodium
ND
0.10
mg/kgwet
Total Phosphorus as P
ND
0.05
mg'kgwet
Zinc
ND
0,05
mg -kg wet
LCS (B9B0454-BSI)
Aluminum
0.59
0,10
mg -kg wet
0.500
117
80-120
Arsenic
0.49
0.05
mgkgwet
0.500
98
80-120
Cadmium
0.50
0.02
mgkgwct
0.500
100
80-120
Chromium
0.51
0.05
mgkgwet
0.500
102
80-11-0
B.�x �t 5
avi!r. - '9606 4M r...Horest fty
Cat ��ef"A
, SC 2?607
noir: 8642332.1556
�-,,x 864.232,614ct
rogersandcallcvtt.com
03t1912019 19.11
This report 'nav not be reproduced, except infill, ill, ivirhour rvripen
penniceion fnm
Rogers & Callc,xr,
Inc.
Page 6 0f 11

Rogers &Callcott
I-NVIRONNMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9020293
Asheville, NC 28801-4310 Reported: 03/19/19 14:11
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPA
Parnmeter Result limit Units Level Result %REC Limits RPI) Limfl Flugs
Batch B9B0454 - E13A 3050B
LCS (B9B0454-BSI)
Copper
0.50
0.02
mg'kg wet
0,500
101
80-120
Lead
0.50
0.05
mg;,kgwet
0.500
99
80-120
Magnesium
0.54
0.05
innIg wet
0,500
107
80-120
M01YMCI om
0.50
0.05
mg,'kL wet
0.500
101
80.120
Nickel
0.50
0.02
mgkgwet
(1.500
99
80-120
Potassium
4.88
0.10
mg`kg wet
5.00
98
80-120
Selenium
0.47
0.05
mgkgwet
0,500
94
80-120
Sodium
0.54
0,10
mgkgwet
0.500
109
80.120
Total Phosphorus as P
0.48
0.05
mgkgwet
0.500
97
80-120
"Zinc
0.50
0.05
ntgkgINTL
0.500
101
80-120
Reference (B9B0454-SRAII)
Aluminum
11300
489
mgkg wet
7900
143
40,71-153.2
Arsenic
152
4,89
mgkgwet
166
92
83.13-116-9
Cadmium
119
1.96
mgkgwet
129
92
82.17-117.1
Chromium
98.0
4.99
mgkgwet
101
97
8-1.67.118.8
Copper
103
1-96
mgkgwet
I10
94
83.55-116.4
Lead
192
4.89
mgkg wet
203
89
82.27-117.'_-
Magnesium
2650
245
mgkgwet
2290
116
75.55-124,5
Molybdenum
30.9
4.89
mgkgwet
32.4
95
78.7-121
Nickel
78.6
1,96
mgkgwet
87,1
90
82.43-117,1
Potassium
1830
9,78
mggkgwel
1990
92
69.35-131.2
Selenium
106
4.89
mgkgwet
117
90
78A6-120.5
Sodium
583
9.78
mgkgwet
621
94
73,75-126.4
Zinc
223
4.89
mgkg wet
240
93
80.83-119 2
Reference (B9B0454-SRN12)
Total Phosphorus as P
770
24.4
mgIg wel
866
89
19-86.159.35
Batch B9B1139 - EPA 3050B
Blank (B9B1139-B1.KI)
Calcium
ND 0.10 mgkg wet
Box cA5 Gt e nville, SC '2` 60r, !2C- `r:,winreSL ", y Gret_nril`•.e. SC -9-07 ..;.j:,, SC4-232 iSSt ;,x R64,232-614o f Ogf'Wrsandcallcott.COI71
cm
0349'1019 14r ll This report moon, not be reproduced. except in fitR, without ,mitten pcmussion from Rogers &- Cullco0. Inc. Page 7 Of 1 1

4 Rogers & Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: 'Waynesville WWTP
351 Depot St. Work Order: 9020293
Asheville, NC 28801.4310 Reported: 03/19/19 14:11
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
I'arar No l'r Result Limit Units Level Result %REC Lindts RPD Limit Flags
Batch 139131139 - EPA 3050B
LCS (89111139-BSI)
Calcium
056
0,10 mg/kg Wei 0.500 113
80-120
Rererence (B9B] 139-SRMI )
Calcium
5280
496 mg%kg wet 4720 112
81.36-1 I8 4
Sample Preparation Data
Parameter
Batch
Sample Ill Prepared
Analvst
EPA 3050B Metal Digestion
CPA3050B
139130454
9020293-01 02/12/2019 08:00
LHB
EPA 3050B
B9131139
9020293-01 02/26,2019 10:18
LHB
EPA 7471B Mercury Digestion
EPA 747113
B9130275
9020293-01 02/07112019 11:40
PO Box 5655 Greonvilie, S�— 2�106 425 i am' r. sr way G dcxvll e' SC '9607 ,. „r. 86 ;.2321556 C-,� 864 232,6!4o roger Sandcaltcott.co1T
03,74.%1019 I4:ll TTris repot may nor be reproduced, eceepi in'till, wilhow arinen pernricrion./roar Rogers & Callcon, Ine. Page 8 of 1 1

kt� Rogers &Cakott
ENVIKONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9020293
Asheville, NC 28801-43 10 Reported: 03/19/19 14:11
Data Qualifiers and Definitions
ND Analyte NOT DETECITI) at or above the reporting limit
NR Not reported
RPD Relative Percent Difference
S1 The matrix spike and' or the matrix spike duplicate sample recovery was not within control limits due to matrix interference, The
Laboratory Control Sample (LCS) was within control limits.
PO Box 5655 Greenvilie, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864,232 1556 ; f;,x 864,232.6140 rogersandcallcott,com
onemployee-owned company
0311912019 14--11 This iy,,poH "ouy not be ivpmdoced, except in full. withal written permission from Rogers & Callaoll, Inc, I Page o

Rogers & Callcott CHAIN OF CUSTODY RECORD
FNVIRONMENTAIL
Mading PO Box 5655 Shipping 426 Fairforest Way 215B Stoneridge Drive
Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210
Phone (VA) 232-1556 Fax [phone] Phone [phone]
Client Name
Address
I^
Cu
Report To:
Y
Email Address
0
,Z
Telephone #
E
41
PO # Project #
Z
p
E
2
R&C
WORK ORDER
YR_
DATE
TIME
SAMPLE DESCRIPTION
— of
AO
Nf
Rb3t
SAMPLER,{- RELQ ISHED BY:
1. �/
RELINQUISHED BY:
ltv
DATE/TIME:
DATE/TI M E:
60J)ra19
RELINQUISHED BY: DATE/TIME:
m RELINQUISHED BY: DATE/TIME
o 7.
0
CJ'
RECEIVED BY:
2. F-rSW
RECE BY:
4.
RECEIVED BY:
6.
RECEIVED BY:
8.
Passible Hazards assoc�ted with samples: ❑ Non -Hazard ❑Flammable EISIdn Irritant ❑ Poison F
WORK ORDER !A i 1� i ,Q L'
Filtered (Yes/No
Cooled es _o)
Container Type (P€astic las:
Container Volume (mL) f
Samp€eType Lrab&o pr-osi
Sample Source (Ww, GW, DW,
Preservation Code(s)
A —None E—HCI I—ZnAcetate
B—HNO3 F—Na2S203 1—H3PO4
C—H2SO4 G—BoricAcid K -MCAA
D — NaOH H —Ascorbic Acid L -
COMMENTS
WLJfo
A aPJ- q 141
DATE%f IM E:
O7.16 b 1 n Composite Start Date:
DATE/TIME: Composite Start Time:
7.10AA OL 60 Time or Flow (Circle one) Initials:
DATEMME:
Temperature of blank or representative sample
DATEITIME: At time of collection °C
At time of lab receipt �} . C
IDDther Form Revised July, 2014 Page of

Rakers &Caticott
ENVIRONMENTAL
Sample Receipt Verification
Date Work
Client: Received: Z. P Order:
Carrier Name: Client FedEx UPS US Mail Courier Field Services Other:
Tracking Number:
Receipt Criteria
Y
e
N
N
`
Comments
a
A
s
Shipping container / cooler intact?
X
X
Damaged Leaking Other:
Custody seals intact?
COC included with samples?
R
Damaged Leaking Other:
COC signed when relinquished and received?
Sample bottles intact?
Sample ID on COC agree with label on bottle(s)?
x
Date / time on COC agree with label on bottle(s)?
Number of bottles on COC agrees with number of bottles received?
Samples received within holding time?
Sample volume sufficient for analysis?
x
VOA vials free of headspace (<6mm bubble)?
Samples cooled? Temp at receipt recorded on COC
p Temeasured with IR thermometer- SN: 97050067
m
Ice Cold Packs Dry Ice None
Samples requiring pH preservation at proper pH? X1 a•il-i1
Note: Samples for metals analysis may be preserved upon receipt in the lab,
v
Now Sam Ica for o&G and VOA anal is— p.rR checked at beach.
n
Samples dechlorinated for parameters requiring chlorine removal at
the time of sample collection?
Note: Chlorine checked at bench for samples requiring Bacterial, VOA, and RAA
Sriat : fS,
HCL
H2SO4
HNO3 -.....
Comments:
If in-house preservation used — record Lot ft
H3PO4
NaOH
Other
Were non-conformance issues noted at sample receipt? Yes or
Non -Conformance issue other than noted above:
Revised February 2018 Completed by:_
Page 11 of 11

•
CHAIN -OF -CUSTODY / Analytical Request
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name:
Client Name; 7{ G�— ;jW- '-':t7V
Address: S&G t,�-(O,,i TrEQ R.4\ 1 C k +r+.) IQ'(t
Report to:t \
Phone: � i1 �S - [o $ Fax: � i� 1 � -;)CI 3
PO Number:
Reouested Analvses
Project Number:
�jij.
/ / pH Checked UponItcc tp[
( I. - 01.mg i UMri Reieip[
Preservatives
Sample Identification
J
J
7Field
Q
z
��
z z z z (°C) Comments
Temperature cc)
Received on Ice:
Y / N�s
Sealed Cooler:
Y / N
Samples Intact:
/
ZY)
/N� /� �y Additional Comments: L� At ! MrKof �L �i � �i �j & � � 6, lio
�f ]� 1 1 f
,
Print d Name of Sampler:
/
r HI (►Mol M' Idr tnta t-fy� 6 k- 1, e41 012 it fug Sa(id�,.
I'l r' �. t"I'
awl
sigmat ampler:
P� l P Pla4 iiv„i:��+j@ n y rr�+ eo, K � e,,,Va jTI R TAN; '�
F t l 1
f'P"

PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Environmental Testing Solutions, Inc. Certificate Of Analysis
Project name: Town of Waynesville WWTP Project number:
Collection date: 7-May-19
Date received: 7-May-19
Sample identification: 503 Lime Sludge -Composite Sample number:
190507.532
168192
Parameter
Method
Result
RL
Units
pate
Analyst
Footnotes
Analyzed
Arsenic
6010 C
<4.29
4.29
mg/kg
15-h1ay-19
LMC
I
Cadmium
6010 C
<1.72
1.72
mg/kg
Is-May-19
LMC
I
Copper
6010 C
87.7
1,72
mg/kg
15-May.19
LMC
I
Chromium
6010 C
12.2
4.29
mg/kg
15-May-19
LMC
I
Lead
6010 C
7.29
4,29
mg/kg
15-may-19
LMC
I
Molybdenum
6010 C
<4.29
4.29
mg/kg
I5-may-19
LMC
I
Nickel
6010 C
7.55
1.72
mg/kg
is-May-t9
LMC
I
Selenium
6010 C
<4.29
4.29
mg/kg
t5-May-i9
LMC
I
Zinc
6010 C
184
4.29
mg/kg
15.May-19
LMC
I
Aluminium
6010 C
8380
42.9
mg/kg
I5-May-i9
LMC
I
Calcium
6010 C
185000
8580
mg/kg
14-May-19
LMC
I
Magnesium
6010 C
3480
42.9
mg/kg
15-May-19
LMC
I
Potassium
6010 C
1220
8.58
mg/kg
15-mtay-19
LMC
I
Sodium
6010 C
336
8.58
mg/kg
15-May-t9
LMC
I
Mercury
7471E
0.50
0.035
mg/kg
Io-A4ay-t<,
TLT
I
Total Kjeldahl Nitrogen
351.2
mg/kg
3
Nitrate + Nitrate
300.0
mg/kg
3
Total Nitrogen
Calculation
mg/kg
3
Total Phosphorus
200.7
3050
42.9
mg/kg
is-may-19
LMC
I
Total Solids
Siv12540 G
56.7
0.10
%
lo-May-19
LBW
I
pli in Soil
SW 846 9045D
12.2
0.10
S.U.
7-May-19
MS
2
% Total Solid
SM 2540 G
58
0.10
%
7-May-19
MS
Ammonia Nitrogen
EPA 350.3
280
6.9
rng/kg
9-may-19
KEK
Sodium Absorption Ration
CALL
1.5
mg/kg
29-May-19
KEK
Plant Avaliable Nitrogen
CALC
mg/kg
KEK
3
Multiple Tube Fermentation
SM 9221-E
<97
97
MPNIG
6-May-19
KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Cal lcott Environmental.
2. Sample analyzed outside holding time. Duplicate result was 12.3 S.U.
3. Cancelled due to sample method. Client is recollecting.
Date reviewed: 117 -AC),I q
Data reviewed by: Kelley C. Keenan
Signature: (/
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis_

Rogers & Callcott
ENVIRONMENTAL
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St,
Asheville, NC 28801-43I0
Dear Client:
Laboratory Report
Project: Waynesville WWTP
Work Order: 9050446
Received: 05108i2019 09:30
Rogers and Callcott appreciates the opportunity to be ofservice to you. "rhe attached laboratory services report includes analytical results and chain of
custody for samples that were received on May 08, 2019. Rogers and Callcott maintains a formal QA-1QC program. Unless otherwise noted, all analyses
performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA'QC confidence imerval
for each test method unless otherwise qualified. Estimated uncertainty is available upon request.
Privileged % Confidential information may be contained in this report and is intended only for the use of the addressee. Ify'ou are not time addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. Ifyou receive this message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at ainy.ashley(ri:rogersandeallcou.com or
(864)-335-4962 if you have any questions about this report.
Report Approved By:
Amy Ashley
Project Manager
This repori mqy not he reproduced, r-wept in fall, without irrifien permission from Rogers R Callcon. htc_
PO Rex 56SS Greenviiio, Sir 29606 42-6 F—,urforzst YV.i Crcenv<Ge, SC 29607 ni,n 864.232.1s56 bx 864.<32.6140 Yogersandcallcott.com
an ernitoyr,:;.�,..,_.^t;a;:y
Page 1 of 10

Rogers &Cakott
d., ENV IItONMENTAI_
Certificate of Analysis
Client Environmental Testing Solutions
Kelley B, Keenan
351 Depot St,
Asheville, NC 28801-4310
Sample Number Sample Description
9050446.01 Waynesville WWTP 503 Lime Sludge - Comp
At
4w
Sarah Carolina Greenville Laboralory Identification 23105
South Carolina Columbia Laboratory Identification 40572
;North Carolina laboralory Certification :Number 27
North Carolina Drinking Mater Lab Number 45710
NELAP Utah Certificate Number SC000042014-1
Georgia Drinking Water Lab ID 880
Project: Waynesville WWTP
Work Order: 9050446
Received: 05108/2019 09:30
Matrix Sampled Type
Sludge 05/07/19 07:41 Composite
PO Box 5655 Grcenvilie, SC 29k06 426 i-airdore%t W-q Greenville, SC 29607 nna:n £b4,232-155b tax 564-232.b140 i-C}gorsif3t ciflcou.CDi13
0511412019 07-50 7745 report may not be reproduced, except infill, without nv7uen permission front Rogers & Callcon, Ine. Page 2 ❑f 1 O

Rogers &CaUcott
ENV IRON MEN'rAt.
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050446
Asheville, NC 28 801-43 10 Reported: 05/24/19 07:50
Case Narrative
Total Nitrogen analysis cancelled as discussed with client 5-23-2019.
I'O Box S655 Greenville, SG 2960C 426 rainforest Way Greenville, SC: 29607 main %4,232 155E tax B64.232_6140 I'Ogei'S-,Ill(iCIilcc)CC.col-il
0512W200 07.,30 This repori mai, nol be reproduced, excepi infid7, wirhoui urruen pormUsion front Rogers t4 C'allcoe, Inc. Pag9 3 Of 1 O

Rogers & Calkott
ENVIRONMFNTAI.
Enviromnental'Vesting Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050446
Asheville, NC28801-4310 Reported: 05124'19 07:50
Sample Data
Sample Number
Sample Description
Parameter
9050446-01
Waynesville WWTP 503 Lime Sludge - Comp collected on 05107119
Reporting
Result Limit Units
07:41
DF Analyzed
Method
Flag Analyst
Batch
General Chemistry Parameters
Total Solids
56.7
0.10
%
1,00
05,10 19 12:00
SM 25400
LBW
B9E0791
'total Metals
Mercury
0.50
0.035
mg'kgdry
1.00
05/10i19 09:56
EPA 747113
TLT
B9P.0503
Aluminum
8380
42,9
mgkgdry
10.0
05/15119 00:03
EPA 601OD
LMC
l39[i0619
Arsenic
ND
4,29
mg/kg dry
1.00
05/15/19 00:07
EPA 60101)
LMC
E9E0619
Cadmium
ND
1.72
lug -kg dry
1,00
05115---19 00:07
EPA 601OD
LMC
A9F0619
Calcium
185000
8580
mg'kgdry
1,000
05/14/19 23:56
EPA 601OD
LMC
B9E0619
Chromium
12.2
4.29
mg --'kg dry
1.00
05•'15119 00:07
EPA 601OD
LMC
139E0619
Copper
87.7
1.72
mg'kg dry
1,00
05/15/19 00:07
EPA 601 OD
LMC
139E0619
Lead
7.29
4.29
mg•'kg dry
1.00
05" 15119 00:W
E1SA 6010D
LMC
139E0619
Magnesium
3480
42.9
inWkg dry
10.0
05115/19 00:03
EPA 6010D
LMC
W0619
Molybdenum
ND
4.29
ni kg dry
1.00
05/15.-19 00:07
EPA60101)
LK4C
1391;0619
Nickel
7.55
1.72
mg!kg dry
1.00
05/15119 00:07
EPik 60101)
LMC
139E0619
Potassium
1220
8.58
mgkg dry
1.00
0515`19 00:07
EPA 60101)
LMC
139EO619
Selenium
ND
4.29
m kg dry
1.00
05115i19 00:07
EPA6010D
LMC
B9E0619
Sodium
336
8.58
mg'kg dry
1.00
05,115119 00:07
EPA 60101)
LMC
139E0619
Total Phosphorus as P
3050
42,9
mg-kgdry
10,0
05/15/19 00:03
F Pik 601OD
LMC
139E:0619
Zinc
184
4.29
mgkgdry
1.00
05,115119 00:07
EPA601OD
LMC
139E0619
i`o Box 5655 Gr-,.enviiie, SI, 29606 4£6 alr -resr. Way G. _envil_., SC: ?9607 m i 864 232.1556 f;,Y 664,232,614o rogersandcallcOtt.com
- a! -,&
05/2412019 07r50 This report nmy not he repivdnecd, owmpt in dl, n iihout written permission from Rogers & Cal/colt, lne. Pale 4 of 10

Rogers & Caticott
ENVIRONMENTAL
NMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050446
Asheville, NC 28801-4310 Reported: 05/24119 07:50
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result f REC Limits RPD limit Flags
Batch B9E0503 - EPA 7471B
Blank (B9E0503-BLKI)
Mercury
ND
0-0001-0
mg -kg feet
LCS (B9E0503-BSI)
Mcrcury
0.0049
0.00020
mg -'kg wet
0.00500
98
90.120
LCS (B9EO503-BS2)
Mercury
0.50
0101-0
mg-kgwet
0.499
99
80-120
Reference (W0503-SRMI )
Mercury
13
0,040
nitAgwet
12.5
105
60.3-140
Batch B9E0619 - EPA 3050B
Blank (B9E06t9-BLKI)
Aluminum
ND
0,05
mckgwet
f
Arsenic
N1)
0,05
mglkgwet
Cadmium
ND
0.02
mgrkg wet
Calcium
ND
oA0
mg/kg wet
Chromium
ND
0.05
me-kgwet
Copper
ND
0.02
mgkg wet
Lead
ND
0,05
mg/kg wet
Magnesium
ND
0,05
mgkg wet
Molybdenum
ND
0.05
mgrkg wet
Nickel
ND
0.02
mgkg wet
Potassium
ND
0,10
mgkgwet
Selenium
ND
0,05
mgkg wet
Sodium
ND
0.10
mgke wci
Total Phosphorus as P
ND
0.05
mgkg wet
Zinc
ND
0,05
mgrkg wet
LCS (B9EO619-BSI)
Aluminum
0,55
O.05
mg=kg w c 1
01500
110
80.120
Arsenic
0.52
"5
mgkg wet
0.500
103
80-120
Cadmium
052
0,02
mgkgwet
0.500
105
80-120
Calcium
0,60
0.10
mg ---kg wet
0,500
119
80-120
Chromium
0,53
0.05
mgrkg wet
0.5011
107
80.120
Copper
0.53
0.02
mg/kg wet
0.500
107
80.120
PC 3,ox =655 Groetwe, SC 9606
A.,:==mot .Wv,
v-eenv;11e,
SC 29607
€,,�w 864-2321556
fa= 864,232
6140 rogersarldcallcott.com
05=24/201 J 07:50 This repot maj, not he reproduced, except in fall, rehhour written permission font Rogers & Callcurr, hre_ Page 5 of 0

Rogers & cattcott
ENV!RON MINTAL
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050446
Asheville. NC 29801-4310 Reported: 05/24119 07:50
Total Metals
Qualih, Control Sumtnaiy
Reporting Spike Source %REC RPD
'Parameter Result limit Units Level Result !RFC limits RPD Limit Flags
Batch B9E0619 - EPA 3050B
L,CS (B9E0619-BSI)
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Total Phosphorus us P
Zinc
Reference (B9E0619-SRM1)
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
yme
Reference (B9E0619-SRM2)
Total Phosphorus as P
0.51
005
mgkg wet
6.500
103
80.120
0.55
0.05
mgkg wet
0.500
111
80-120
0.53
0.05
mg'kgw•et
0.500
106
80-120
0.53
0.02
mg1kg wet
0.500
105
80.120
5.02
0.10
mg'kg wct
5.00
100
80-120
0.51
0.05
mg'kg wet
0,500
101
80420
0,53
0.10
mg/kg wet
0.500
105
80.120
0.52
0.05
mg'kgwet
0.500
t04
80-120
0.55
O.05
mg'kgwet
0.500
110
80-120
9970
249
mgikg wet
7900
125
46.71-153.2
150
4.97
mg -kg wet
166
90
83.13-116.9
116
1.99
mg'kg wet
129
90
92,17-117.1
4620
497
mgkgwci
4720
98
81.36-118.4
101
4.97
mgkgwet
101
100
82.67-118,8
103
1.99
mg kg wet
110
94
83.53-116.4
150
4,47
mg'kgwet
203
89
82,27-117.2
246()
2-49
mgkgwet
2290
108
75.55-124.5
30.8
4,97
mgkgwet
32A
95
78.7-121
78.1
1.99
mg'kgwet
87.1
90
82.43-117.1
1810
9.94
mg/kg wcl
1990
91
69.35-131.2
103
4.97
mgkg wet
W
88
78.46-120,5
529
9,94
mg!kg wet
621
85
73.75-126.4
220
4.97
mg/kg wet
240
92
80,83.119.2
772 24,5 mg/kg wci 966 89 19-86.159.35
PO Box 565E 7reenrilte, SC 2%06 12h Fai,foresLV%y Gree.gv lie, SC 29607 n,s r 864,232J.5S6 �,x 86-4132 6m rogersandcalleott.com
05;'247019 07, 50 This reporl mar not by reproduced, except in full, without written permission fr m Rogers & Culleud, Inc_ Page 6 Of 10

Rogers & Cakott
ENVIRONMENTAL
Enviromnental Testing Solutions Project: Wayncsville WWTP
351 Depot St, Work Order: 9050446 r
Asheville, NC 28801-4310 Reported: 05/24119 07:50
Sample Preparation Data
Parameter Batch Sample Ill Prepared Analvst
EPA 30508 Metal Digestion
EPA 3050B 139E0619 9050446-01 05 13t2019 10:15 LHB
EPA 7471E Mercury Digestion
EPA 7471B B9EO503 9050446-01 05/09/2019 15:30 TCr
PO 13o% S655 Greet,v,lle. SC 29606 426 h;rfaresr Way Greenv:lie, SC 29607 main 1164.232.1556 rogersandcallcott.com
,tI,.oIk1II(PYJT-f-14'..1,•,r.,,•-iy
05t24,10I9 07:50 This report may not he reproduced, except in jdt,, mUhomd IM11011permasion limn Rogers & Ca!/colt, Inc. Page 7 of 1 Q

Rogers & Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St, Work Order: 9050446
Asheville, NC 28 801-43 10 Reported: 05/24/19 07:50
Data Qualifiers and Definitions
ND Analvte NOT DETECTED at or above the reporting limit
NR Not reported
RPD Relative Percent Difference
PO iiox 5655 Greenville, SC 29606 426 Fair forest Way Greenville, SC 29607 main 864.232.1556 fx 864.232.6mo rogersandc:i I lc: )u.com
0512412019 07;50 This report may not he reproduced, except inJidl, withauu w-wen permissiunjrom Rogers & Callcott, Inc. Page 8 Of 1 O

og�rs & Ca�lcott CHAIN
OF
CUSTODY
RECORD
WORI<oRDER
Q O�i�i4(o
ENVIRONMENTAL
Filtered Les/l )
I
Cooled g NO)
Mailing PO Box 5655 Shipping 426 Fairforest Way 215B Stoneridge Drive
Container Type Llastic/ ass
Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210
Phone [phone] Fax [phone] Phone [phone]
Container Volume (mQ 510
Client Name
Sample Type (GrablJgo pasite
Address
Sample Source (WW, GW, DW, S, er
— —��• --
is
'i
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Report TO:
o
Preservation Codes)
Email Address
U
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A —None E—HCI I — ZnAcetate
B—HNO3 F—Na2S203 !—H3PO4
Telephone #
a)
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C—HzsOc G—Boric Add K-MCAA
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G
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D - NaOH H - Ascorbic Acid L -
PO # Project #
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WORK ORDER
YR_
DATE
TIME
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COMMENTS
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SAMPLER—,RWNBY:
DATE/7iME:
RECEIVED BY:
DDAATEEMME:
RELI UISH�E�Q BY:
DATE/TIME:
RECEIV Y:
DATE/TIME:
3. LIJJItA 1'
M61 5
4.
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RELINQUISHED BY:
DATE/TIME:
RECEI BY:
DATE/TIME:
5.
6.
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LCDJ
RELINQUISHED BY:
DATE/TIME:
RECEIVED BY:
DATE/TIME:
j 7.
8.
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Possible Hazards associated with samples: Non -Hazard Flammable ❑Skin Irritant I--] Poison nknown ❑other
7* can w-ed, Q's
d 155G6cWt AA fn C11 Mt,
5ppq 07r.
Composite Start Date:
Composite Start Time:
Time or Flow (Circle one) Initials:
Temperature of blank or representative sample
At time of collection C
At time of lab receipt ®`C
Form Revised July, 2014 Page of

i
Ropirs & Callcott
ENVIRONMENTAL
Sample Receipt Verification
Date Work
Client: r5 _ _ Received:Order: g j _
Carrier Name; Client FedEx UPS US Mail Courier Field Services Other:
Tracking Number:
Receipt Criteria
e
N
N
Comments
o
A
s
Shipping container / cooler intact?
Damaged Leaking Other:
Custody seals intact?
COC included with samples?
COC signed when relinquished and received?
Damaged Leaking Other;
Sample bottles intact?
Sample ID on COC agree with label on bottle(s)?
Date / time on COC agree with label on bottle(s)?
x
Number of bottles on COC agrees with number of bottles received?
Samples received within holding time?
Sample volume sufficient for analysis?
VOA vials free of headspace (<6mm bubble)?
Temp at receipt recorded on COC
Samples cooled?
Ice Cold Packs Dry ice None
Temp measured with rR thermometer - SN: 97050067
Samples requiring pH preservation at proper pH?
Note: Samples for metals analysis may be preserved upon receipt in the lab,
Note: Samples for O&G and VOA analysis — roservatiou checked at bench..
Samples dechlorinated for parameters requiring chlorine removal at
the time of sample collection?
�(
Note: Chlorine checked at bench for samples requiring Bacterial, VOA, and FUA
analysis.
If in-house preservation used — record Lot #
HCL
H3PO4
H2SO4
NaOH
HNO3
Other
Comments:
Were non-conformance issues noted at sample receipt? Yes or No
Non -Conformance issue other than noted above:
Revised February 2018 Completed by:
Page 10 of 10

• CHAIN -OF -CUSTODY / Analytical Request
Client Name: u)1JI
P ET!S Address: 5b (a i,t�a l + I ra i I Rd
287535
Environmental Testing Solutions, Inc. Report to:
PO Box 7565, Asheville, NC 28802 Phone: g Fax: --a013
Phone: [phone], Fax: [phone] PO Number:
ProiectName: rt.l.".wTies Jl �� 1 itenesested.analyses
Project Number:
p1I Checked U Reozipt
CI_ < 0.2 mr l Upul Receipi
Preservatives
Sample Identification �_ > _ }
CJ U
Ld
r i! ( )
= ►'i
Field
Tam . (°C) Comments
S03 C; mL; /5h,4e
C,
lvelal2
S
Si�ila
�''��
�%
y
5I J F
L
v'-
Temperature (°C
Q.�
]e~�tiC it W,4a
tS�
Received on Ice:
Y
6 15 � f✓v lr Teo`
517119
try / Q
N �"
�
vS
C�
� � qt7
Sealed Cooler:
' Y N
Samples Intact
/"Y i N
I
Additional Comments; 1- Amxwt,.e,_i;,-trjo 95y CalCr3(AI CA Pb Mg i i19iM�1
N?7P���+►+ °Is Sz, IjAl S q R
Pri ed Name of Sampler:
I
�7( A
-TKr), to l Plank Rda�Rabi� 1�1;'Fra [4��C•+Ieu����on)
Signature $Ana pler:
1"
V.

Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name:
Town of Waynesville WWTP
Collection date:
10-Jun-19
Date received:
11-Jun-19
PO Box 7565
Asheville. NC 28802
Phone: [phone]
Fax: [phone]
Project number: 190611.514
Sample identification: 503 Lime Sludge- Composite
Sample number: 169372
Parameter
Method
Result
RL Units
bate
Analyst Footnotes
Analyzed
Total Kjcldahl Nitrogen
351.2
69.8
mg/kg
20-Jun-19
ECFIEM l
Nitrate + Nitrate Nitrogen
353.2
16.9
mg/kg
24-Jun-19
ECHEM 1
Total Nitrogen
Calculation
86.7
mg/kg
25-Jun-19
ECHEM I
_
Footnotes:
RL = Reporting Limit. Values are reported dog%;n to the Reporting Limit only.
1. Sample analyzed by Enviro Chemists. Inc.
Date reviewed: .Z-60 NC Certification Number: 600
Data reviewed by: Kellev R. Keenan SC Certification Number: 99053
r� Signature: NC Drinking Water Certification Number: 37786
rw
This report should not be reproduced, exept in its entirety, without the written consent of tinvironmental 'Testing Solutions, Inc
The results in this report relate only to the samples submitted for analysis.

l Environmental Chemists, Inc.
envir1 t {•! .._ �y} _,'1`: :'�';C i'�ii;}i}e} a,%t, .\l, .`5 fir[.,, 9M .Cl '. .22",_,._. „elf" t 0103,02' .421 1-i3I,
... �i.} li{3+.� ,rf1C:-ai [1 ii�!•:,a; �4?,zie:N_7`.1 ,}
J roc s '�'=_�'!.l%_ ,:`' ._l•,� F:eS
Higlvl .ici.`s)IYI `iflc. •V_ .:6iail s iif ..rl^'';� i 1
ANALYTICAL & CONSULTING CHEMIST S
Environmental Testing Solutions, Inc. Date of Report: Jun 25, 2019
Post Office Box 7565 Customer PO #:
Asheville NC 28802 Customer ID: 08100055
Attention: Kelley Keenan (ETS) Report #: 2019-09469
Project ID: Waynesville WTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
19-24232 Site: 503 Lime Sludge 6/10/2019 5:35 PM Solid/Sludge Client
Test Method Results Date Analyzed
Total Nitrogen (calc)
Total Kjeldahl Nitrogen (TKN) EPA351 2 69.8 mg/kg 06/20/2019
Nitrate+Nitrite-Nitrogen EPA 353 2 16.9 mg/kg 06/24/2019
Total Nitrogen Total Nitrogen 86.7 mg/kg 06/25/2019
Comment:
1
Reviewed by:
Rctft 2019,(M469 --
F'-3iJP_ 7 of 1

Env iroot i-iiental Chemists, Inc.
envirochem
'k l6sid_ Vma­� N('�Q�54
10,11N."ington 1 )_ockSzomklc N(_
ANALYTICAL & CONSULTING CHEMISTS
QC ETS- 2019-09469
LCS
parivilefer
True fafue
Resith
?/0 True Jahle
Limils
mgsL
mgL
lzl_lo
N 0 3 - �N, 02)
1.00
0.99
99
90-110
TK_N
4.0
3.8
95
90-110
MS/MSD
True
Parameter
T-11flue
RecoveiT
Recovery
Limits `?/o
Limits
ingl-L
in L
Difkrence
Recovery
D{Jlircnce
N(.)3+NO2
MID
0.60
120
N/A
80-120
<')o
TKN
5,7
114
— N/A
80-120
< 20
DUPLICA'rc SAMPLES
Restills
Parameter
Ing, 1,
X DiJfirence
Limits'XI
NO3,NO_-)
6.27
6.03
+_
6
< 20
TKN
27.6
28.1
1)
<20
BLANKS
Parameter
Results
Limit
Ing. 1.
t)lg,,L
NO3TN-02
<0,01
0,01
TKN
<0.25
0.25

Environmental 7 sting Solutions, Inc.
PO Box 71565, Ashevillu. NC 28802
Mwne- [phone]v Fax.- i 8_18) .3 350-9368
V A -o i e" N -t n It, z
i'voik""t Number;
CHAIN -CUS'TODY Analytical Request
(licill Name:
Address:
Rqwrr to.
Phorw:
PO Ntimber:
Sample Identificdion E
LEz Z
f-I Ifi
Fit k.
Topf Rtcvip;
Te

• F 4
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
CHAIN -OF -CUSTODY / Analytical Request
1
Client Nance: r 10W,'� 44AQ 5o 6 le Wi,3TP
Address: ,j (o 6 [ 1 A V+ i re IZCL
0a ��vc1�e h1c, ��785
Report to: PQ-1 i i r 'k-
Phone: (t.�fq L167a—g655 Fax: FSa5 -,2o 3_
PO Number:
i7-PlfPri Onfah'Cec
Project Number:
lz7n
_9
HChccicdL mRcai
C"I. ^ 0.2 mg}I iron Rrccipt
Preservatives
Sample Identification
E
1 z -
=o
L
0
E
s ,•
A
r
x
Field
Temp.( °Q Comments
503
�1161
�[
70
'_
G �
Temperature (C) l{ ` �'
M
IDLJ {1 P�
I!
7
C- TS C-n
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rw k J D n e
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Received on lce:
Y 1 N
� � S 1
�
j1
r7*✓'71111
f7j..,o
%O
1030
Sealed Cooler:
Y N
Samples Intact:
0/ N
Additional Comments:
Sampler Name and Signature
Pri�ted Name of Sampler:
ync^
P v , r f, i rV
ry
r-'`-5
�q Q
Sigrmture of Sampler-
t
i

Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name: Town of Waynesville WWTP
Collection date: 6-Ma3-19
Date received: 6-May-19
Sample identification: 503 Lime Sludge - Composite
Po Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 190506.503
Sample number: t68081
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%"Total Solid SM 2540 G 54 0.10 % 6-May-11t KEK
Multiple Tube Fermentation SNi 9221-E <97 97 MNN,g 64i18y-19 K1 K
Footnotes:
RL = Reporting Limit. Values are reported down to the Repotting Limit only.
Date reviewed: NC Certification Number: 600
Data reviewed by: Kellev E, Keenan SC Certification Number: 99053
Sianalure: NC Drinking Water Certification Number: 37786
fhis report should not be reproduced, exept in its entirew, without the written consent of I.nvironmental Testing Solutions, Inc
The results in this report relate only to the samples submitted for analysis

•
a
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Proiect Name: U4jcZ11 it L5 V ]
I I C
CHAIN -OF -CUSTODY / Analytical Request
Client Name:
Address:(p!�,[.�
11C. AJC, 25 7 $ S
Report to:
Phone: 6.-)5) L/So2— fo � Fax:
PO Number:
l2euursied Analysis
Project Number:
�] �j
pi Checked 1'pnn Rrrclpl
C6 � 0? rn•;+I I pnn Rccript
Preservatives
-
Sample Identification
-E 47
°
U
I
z
c
ch
�o
c
U
�„
Field
"
L
F
❑ _
[_
z u
- 7 Temp.("C) Comments
So 3 L � �At
1(.8001
S
'vwlcl
1
'
I I - rzo Mel RMI
Mrs in 0
IMIMWMTI��w
l-empCMwre (°C
.� -�
I�C�'ii tifr S,n; �h
T n o fl
S IR
%� � �
j�
t`i
g : a o
Received on Ice:
! (�l�Z
Sealed Cooler:
Y' N
Samples Intact:
Y N
Additional Comments:
Prin 'ame of Sampler:
afri" , dswl. i let ✓19
Signature 0;' ' I pi
mil"

Environmental Testing Solutions, Inc. Certificate of Analysis
Project name: Town or Waynesville WWTP
Collection date: 6-May-19
Date received: 6-May-19
Sample identification: 503 Lime Sludge - Composite
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax, [phone]
Project number: 190506.503
Sample number: 168081
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
% "total Solid SM 2540 G 54 0.10 % 6-May-19 KE K
MUlti le Tube Fermentation SM 9221-E: <97 97 MPNIZ 64v1ay-19 KLK
Footnotes:
RL, = Reporting Limit. Values are reported down to the Reporting; Limit only,
Date reviewed: 0j.Lq,6j NC Certification Number: 600
Data revieNved by: Kelley F. Keenan SC Certification Number: 99053
Signature:NC Drinking Water Certification Number: 37786
this report should not be reproduced. wept in its entirety, without the written conseni arEnvironmental'resung Solutions, Inc
'rho results in this report relate only to the samples submitted for analysis.

Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: S 1
(8JJ2/8�) 350-9368
. Q P,* Norco 1A Ju;,)G'-i) I /c-
CHAIN-OF-CUSTODY / Analytical Request
Client Name: 1�j L�1) A wae `j U� 1 I W by l
Address: P d.
LJavne-6i2s' iirc. AJC F�8785
Report to: a-}- r � �,k
Phone: Fax:
PO Number:
Ii—'—t—i A—l—, I
Project Number:
C1, 0,2 m&I Upon Reeelnl
J
L 1
Field
Temp, l" 0 Comments
r
Sample Identification
u
°
- —
r
o C
-Z
o f
Preservatives
v
+
O,
60 3 L I YYJe 1314,6
bBC701
S
�llo
��
OF
10.7 L i ', � fq'4
% s l l
s Iq
i9a p
Cc mpertture (°C)
. l -C
Received on Ice:
Y N
y
�)
ice' ^ �q,
I �� n
I
v�i5
uoz
Sealed Cooler:
N
Samples Intact:
Y N
Additional Comments:
pri unc ❑fS:ut3plcr:
t'C4
Signature of p!
` -

Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name: Town of Waynesville WNVTP
Collection date:
Date received:
2l-Jan-19
21-Jan-19
110 Box 7565
Asheville. NC 28802
Phone: [phone]
Fax: [phone]
Prgiect number: 190121,501
Sample identifieation: 503 Lime sludge 41 - Composite Sample number:
165223
Parameter Method Result RL Units pate Analvzcd Analyst Footnotes
% "Total Solid SM 2540 G 44 0.10 % 21-Jan-19 KFX
Multiple Tube Fermentation SM 9221-F, <79 79 MPNln t-m,,-io KF:K
Sample identification: 503 Lime Sludge #2 - Composite Sample number: 165224
Parameter Method Result RL Units pale Analvsl Footnotes
Analyzed
ni Total Solid SM 2540 G 46 0,10 % 21 in 19 KI;K
Multiple Tubc Fermentation SM 9221-E <83 83 MPNle 21•,tan•19 KhK
Sample idemification: 503 Lime Sludge #3 - Composite Sample number:
165225
Parameter Method Result RL Units pate Analyst Footnotes
Analvzed
% Total Solid SM 2540 G 46 0.10 % lann•19 KEK
-Multiple Tube Fermentation SM 9221-F., <83 83 MPN g Mann-19 KEK
Sample identification: 503 Time Sludge #4 - Composite Sample number
165226
Parameter Method Result RL Units Date Analyst Footnotes
Auah•zed
% Total Solid SM 2540 G 48 0.10 % 21-Jan-19 KEK
Multiple "rube Fermentation SM 9221-E; <86 86 MPNIg 21ean-19 KEK
Footnotes:
RL = Reporting Limit, Values are reported down to the Reporting Limit only.
Date reviewed: a •as. l q NC Certification Number: 600
Data reviewed by: Kelley E. Keenati SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
Signature:
This report should not be reproduced, exept in its entirely, without the %witten consent orEnvironmental Testing Solutions, Inc
The results in this report relate only 10 the samples submitted for analysis.

•
•
Fmr.
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Proiect Name:
CHAIN -OF -CUSTODY / Analytical Request
Client Name: CL 1'i QT W ASV, 1 jet
Address:
t' GuitEsis t A;L S b
Report to: pi t1 t-' /L 10 Y-�
Phone: � $ a $7 q5a - 'I � 8 Fax: ' 8 L�,j( ",261,3
PO Number:
Reuuested Anahses
Project Number:
L'
H Ciwc1ed Upon Rax*
�
Cl_ < G.2 mg't LTjx. R=ipt
Preservatives
Sample Identification
"
=
uL
u3
d c
C
7 Q
i
i_7
;r J c�a
w w z
c�' C+L
z
T<ield
Temp. (°Q Comments
-
L2 i 1
56NJ
�
J
4-
CYA
[�a5zz;
1 i
v5
5 Ltmpls1 e
C'
(c CZ240
6
i'7jtiq
9"StJ
Temperature (oC)
S•q .L
iM
icrw'n cr
d.ai11
F i(
V
1�
i} lZ%Cq
'( �arZL
, .iC,tC5
taaanY:l
,
Received on lee:
Y / E)
Sealed Cooler:
Y 1�
�.NJ
Samples Intact:
Additional Comments:
<
pler::
=1natureof
,

Environmental Testing Solutions, Inc.
Certificate of Analysis
Projcet name: ',own of 11'avnesville wWTP
Collection date:
Date received:
28-Jan-19
28-Jan-19
Sample identification: 503 Lime Sludge #5 - Composite
1"0 Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 190128.500
Sample number: 165471
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%"Total Solid SM 2.540 G 62 0.10 % 28-aan-i9 KEK
Multiple "Cube Fermentation SM 9221-E <112 112 MPNJg 28-Jan-19 KEK
Sample identification: 503 Lime Sludge #6 - Composite Sample number:
165472
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%'Total Solid SM 2540 G 64 0.10 % 28-Jan-19 KI K
Multiple Tube Fermentation SM 9221-E <115 115 MPN/g 28-JanJ9 KEK
Sample identification: 503 Lime Sludge #7 - Composite Sample number
165473
Parameter Method Result RL Units Date analyst Footnotes
Analyzed
%Total Solid SM 2540 G 46 0.10 % 28-Jan-19 KEK
Multiple Tube Fermentation SM 9221-E <83 83 MPN!g 28-Jan-i9 KEK
Footnotes:
RL - Reporting Limit. Values are reported do�yn to the Reporting Limit only.
Date reviewed: _ O'a�ol •lGI NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
,[ NC Drinking Water Certification Number: 37786
Signature: LA-
Phis report should not be reproduced, exept in its entirely, without the written consent ol'Euvironmental Testing Solutions, Inc
The results in this report relate only to the samples submitted for analysis.

•
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Ili.._.,..♦ !�'........
CHAIN -OF -CUSTODY / Analytical Request
Client Fame: Di.c�lh u r'12 'LI_(,-
-�J—
Address:
Report to: I�a r-Y 17D;ZfC rj
Phone: Fax: y5�!
PO Number:
Project Ntimber:
pH C.'h,&,d Upon Rexi [
0:1 Q.? mc7 Upon Ri.=!ps
Preservatives
�
Sample Identification
C
�
Zr
z �'
=`c
--
r_ +
i s
z
F Z
z
Field
Temp. ["C) Comments
:D:
503 L-WC Aluc
��4�C�3
I S►li i
:a
�1
TemperatureCC) {
�^�`1
leir r� t?
lr3C 45dili
117
���i7,3r
dl[5 Ul'1i tr1 d�'4(J
Received on Ice:
Y ! hl
LJA`I ►�°-_�}J� �
i t� E�
E�
0 k-L&A
I iilL7
Sealed Choler:
Y '
\j
Samples Intact:
(Y ! N
Additional Comments:
Printed Name of Sampler.
r
M a
Signature of 5 mpler-
_t
J

Env IranmentaI Testing 5aIutions, Inc.
Certificate of Analysis
Project name: Town of Waynesville W` TP
Collection date: 6-Aug-19
[late received: 6-Aug-19
Sample identification: 503 Lime Sludge -Composite
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 190806.532
Sample number: 170235
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Arsenic
6010 D
8.80
3.75
mg/kg
13-Aug-19
LMC
1
Cadmium
6010 D
<1.50
1.50
mg/kg
13-Aug-19
LMC
1
Copper
6010 D
136.0
1.50
mg/kg
16-Aug-19
LMC;
1
Chromium
6010 D
21.8
3.75
mg/kg
13-Aug-19
LMC
1
Lead
6010 D
15.0
3.75
mg/kg
13-Aug-19
LMC
1
Molybdenum
6010 D
<3.75
3.75
mg/kg
13-Aag-19
LMC
I
Nickel
6010 D
14.2
1.50
mg/kg
13-Aug-t9
LMC
1
Selenium
6010 D
<3.75
3,75
mg/kg
13-Aug-19
LMC
1
Zinc
6010 D
377
3.75
mg/kg
13-Aug-19
LMC
1
Aluminium
6010 D
16400
375.0
mg/kg
13-Aug-19
I.,MC
I
Calcium
6010 D
228000
3750
mg/kg
16-Aug-19
LMC
I
Magnesium
6010 D
7500
375.0
mg/kg
13-Aug-19
LMC
1
Potassium
6010 D
2570
74.9
mg/kg
13-Aag-19
LMC
1
Sodium
6010 D
675
74.9
mg/kg
13-Aug-19
LMC,
1
Mercury
7471B
0.27
0.039
mg/kg
22-Aag-19
TLT
1
Total Kjeldahl Nitrogen
5M 4500 ORG t3
5680
mg/kg
7-Aug-19
ECHEM
3
Nitrate + Nitrate
353.2
0.25
mg/kg
20-Aag-19
ECHEM
3
Total Nitrogen
Calculation
5680
mg/kg
22-Aug-19
ECHEM
3
Total Phosphorus
200.7
3050
42.9
mg/kg
1s.may-r9
LMC
I
"Total Solids
SM2540 G
50.3'
0.10
%
7-nag-19
MLR
1
PH in Soil
SW 846 9045D
12.2
0.10
S.U.
7-Aug-19
MS
2
%Total Solid
SM 2540 G
63
0,10
%
8-Aug-19
KEK
Ammonia Nitrogen
CPA 350.3
160
6.3
mg/kg
8-Aug-r9
KEK
Sodium Absorption Ration
CALC
2.0
mg/kg
29-Aug-19
KEK
Plant Avaliable Nitrogen
CALC
1184
mg/kg
29-Aug-19
KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Sample analyzed outside holding time, Duplicate result was 12.3 S.U.
3. Sample analyzed by Enviro Chemists, Inc.
Date reviewed: 00'
Data reviewed by: Kelley E. Keenan
Signature: Y
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, lnc-
The results in this repon relate only to the samples submitted for analysis.

Rogers & Callcott
INVIRONMENTA'
Client Fm ironmental Tesling Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Dear Cl icnt
Laboratory Report
Project: Waynesville `,>rWTP
Work Order: 9080402
Received: 08:'0? 2019 11:40
Rogers and Callcott appreciates the opportunity to be orservice to you. The attached laboratory services report includes analytical results and chain of
custody for s:unples that were received on August 07, 2019. Rogers and Callcott maintains a formal QAQC program. Unless otherwise noted, all
analyses performed under NELAP certification have complied with all the requirements for tlieTINI slandard "rhe analyses met the QA/QC confidence
interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request.
Privileged , Confidential information may be contained in this report and is intended only for the use of Ilic addressee. If you are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive Ili is message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at amy.asbley(Nrogersandcalleou.com or
(864)-335-4962 if you have any questions about this report.
Report Approved By:
O/1T J C�vttr
Amy Ashley
Project Manager S
This report ropy not he reptnduced, except in fill. wilhoal nvinen permission from Rogers & Calico if. Inc.
PO Box 5655 Gr= ,_ _, v=i e. £C: 2 606 426 Falrfcrc;t VW .. ,___€:v E'•.e. `;C 29607 . .... 864 232 €556 f?r, 864.232_6 i4o rogersandcallcott.eom
Page 1 of 9

Rogers & Cakott
1=1ti{VIRONMENT L
Certificate of Analysis
Client Environmental Testing Solutions
Kelley 13, Keenan
351 Depot St.
Asheville, NC 28801-4310
Sample Number Sample Description
9080402-01 Waynesville W WTP 503 Lime Sludge - Comp
Soarh Carolina Greenville Laboratnr)• ldentVieation 23105
Soulh Carolina CoAnnbia Labaratart! ldenlilicalion 40-i'Z
North Carolina Laborator' Certification Nrooher?-'
N'nrlh Carolina Drinking 1Fater Lab Nninber 45110
NELel P Utah Cerli icaie Number SC000042014-1
Georgia Drinking Water Lab ID 880
Project: Waynesville WWTP
Work Order: 9080402
Received: 08'0712019 11:40
Matrix Sampled 'Type
Sludge 08'06i19 08:00 Composite
Box f55
G;-eenv'1€r, 4C 2960v
426 N;rforc=.sx way Greenville, 5C 2907
mil r 864 232. =556 rav 8.4-232 5140
rogersanar-allc tt.com
0&i2.V2019 06.41
This
report nrav not be reproduced. except in hill, without
nrinen permission/root Rogers &- Callcon. lnc.
Page 2 Of 9

Rogers & Cakott
NVIRO1~lMEN TAL
Environmental Testing Solutions Project: Waynesville WW'TP
351 Depot St. Work Order: 9080402
Asheville, NC 28801-4310 Reported: 08/23/19 06:41
Sample Data
,Sample Number 9080402-01
Sample Description Waynesville wwTP 503 Lime Sludge - Comp collected on 08;06,'19 08:00
Reporting
Parameter Result Limit Units Dr Analyzed
Nlelhad
Flag Analyst
Balch
General Chemistry Parameters
"Ibtal Solids
50.3
0.10
%
1.00
08/07/19 16:25
SM 2540G
MLR
B91-10455
Total Metals
Mercury
0.27
0.039
mg:kg
2.00
08i22/l9 13:34
EPA 747113
TILT
B9H0866
Aluminum
16400
375
mg=lgdty
50.0
08113'l9 21:28
EPA6010D
LMC
B91-10497
Arsenic
8.80
3.75
mekgd0'
1.00
08/13/19 21:36
EPA 6010D
LMC
B9140497
Cadmium
ND
1.50
mg kg dry
1,00
08/13/19 2)1:36
EPA 60101)
LMC
B9H0497
Calcium
228000
3750
mgkg dry
1.000
08/16/19 15:35
EPA 6010D
LMC
B9H0497
Chromium
21.8
3,75
mg'kgdry
1.00
08/13/19 21:36
PPA601OD
LMC
B9H0497
Copper
136
1.50
mgf$gdry
1.00
081W19 15:41
EPA60101)
LMC
B9H0497
Lead
15.0
3.75
mg!kgdry
1.00
08/13/19 21:36
EPA 601OD
LMC
B91-10497
Magnesium
7500
375
mg kg dry
50.0
08/13/19 21:28
EPA 601OD
LMC
B9H0497
Molybdenum
ND
3.75
mgtkgdry
1.00
08.13119 21:36
EP.A60101)
LNIC
B9H0497
Nickel
14.2
1.50
fnwkg dry
1,00
08/13/19 21:36
EPA 601OD
LMC
B9H0497
Potassium
2.570
74.9
mg,kg dry
10.0
08/13/19 21:32
EPA 601OD
LMC
B9H0497
Selenium
ND
3.75
mg- kg
1.00
08/11-19 21:36
EPA601OD
LMC
B91{0497
Sodium
657
74.9
mg/kgdry
10.0
08/13/19 21:32
EPA6010D
LMC
69140497
Total Phosphorus as 11
5770
187
m-vkg dry
50.0
08/13.119 21:28
EPA 601OD
LMC
B9H0497
Zinc
377
3.75
mgkgdry
1,00
08/13/19 21:36
EPA601OD
LMC
B9140497
p) Box 5655, C'-reenvii1e, _ 2Q6 € -s g µr, $ dC COtt.com
�E a2 � F ,-'c�sc:sx W.t i.}rr;-3rv.,. SC 'z-0= ��.232 i'<36 ., - 86- 1,3".6€ . t'C)��C ill ci
08 23f 2010 06,41 This report may not he mprodurcd. except in full, adfhouf wriften pennia'aian frtm Rogers & Culleolf. 1ne page 3 0t 9

Rogers &Cakott
ENV IR)(vMEN AL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St, Work Order: 9080401
Asheville, NC 28801-4310 Reported: 08123,19 06:41
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPl)
Parameter Result Limit Units Level Result %REC Limits RPI) Lhnit Flags
Batch B9H0497 - EPA 3050E
Blank (B9I10497-Bt,KI)
Aluminum
ND
0.05
mg. -kg wet
Arsenic
ND
0,05
mg:kgwet
Cadmium
ND
0-02
mgkgwet
Calcium
ND
0.05
mgkg%vo
Chromium
ND
0.05
mckgwet
Copper
ND
0,02
mggkg wel
Lead
ND
0.05
Mg kg
Magnesium
ND
0.05
mgkg wet
Molybdenum
ND
0.05
mgtkgwet
Nickel
ND
0.02
mgfkg wet
Potassium
ND
fk10
mg'kgwet
Selenium
ND
0.05
me -,kg wet
Sodium
ND
0.10
mgkgwo
Total Phosphorus as P
ND
0.05
mg. -kg wcl
Zinc
ND
005
mgrkgwet
LC'S (B9H0497-BSI)
Aluminum
0.54
0.05
mg, kgwel
0,500
1(Y)
80-120
Arsenic
0,52
0A5
mgkgwel
0.500
105
80-120
Cadmium
0.53
0,02
rngkg wet
0.500
105
80-120
Calcium
O,19
0.05
rng%kg wet
0.500
118
80-120
Chromium
0.51
0.05
mg'kg%vet
0.500
103
80-120
Copper
0.54
0A2
mgkgwet
0.500
108
80-120
Lead
0.33
0.05
mgkgwet
0.500
106
80-120
Magnesium
0.57
0,05
mg'kgwet
0,500
IN
80-120
Molybdenum
0.52
0.05
mgkgwel
0.500
104
80-I20
Nickel
0.52
0.02
mg'Icg wet
MOO
104
80.120
Potassium
5.00
0.10
ntgkg wet
5.00
100
80-120
Selenium
O1 53
0.05
mg,. --kg wet
0.500
106
80.120
Sodium
059
0.10
mg=kgwet
0,500
117
80-120
'total Phosphorus as P
0,54
0.05
mg -kg wet
0.500
109
80-120
Zinc
0.53
0.05
mgkgwet
0.500
106
80-120
Reference (139I-I0497-SRM 1)
Aluminum
10300
243
mgkgw•et
J 7900
130
46,71-153.2
Arsenic
162-
4,87
mg kg wet
166
98
83.131-116,9y
vv
rO Box 56 s s�.�,`„C;E"... ,., `!C
a-1,60; <u ,F,. - orom
T■ - 4 c-c
,u � h } 0V
na 86 23
I_.. 8 -2
133 i.J!`4o
y C i /�}} ! �ry
I tiger Jat dcallcott.co I �
08123 2019 06:41
Thli' rrpon nu{t nnr Gr.
n pror6r•ei, except
in fdl, withaui
irriurn ycrmisairrn,
T om Rogers & Calleorr. Inc_
Page 4 of 9

4 Rogers & CaRcott
ENV IROi-4 MENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9080402
Asheville, NC 28801-4310 Reported: 08/23/19 06:41
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPII
Parameter Result Lbnll Units Level Result %REC Limits RPD Limit Flags
Batch B9H0497 - EPA 3050B
Reference (B9H0497-5RM 1)
Codmium
118
L95
mg/kg wet
129
91
82.17-I1"N
Calcium
4710
243
mg'kg wet
4720.
100
81.36-118A
Chromium
103
4.87
mg-Agwer
101
102
82.67-118.8
Copper
110
I95
mgrkgwet
110
100
83.55-116.4
Lead
203
4,87
mg kg wet
203
100
82 27-117.2-
Magnesium
2710
243
mgrkgwet
2290
118
75.55-124.5
Molybdenum
32.3
4.87
mg -kg wet
32-4
100
M17.121
Nickel
81,8
1.95
mg'kgwet
87.1
94
82.43-117.1
Potassium
2060
9,74
mgkgwel
1990
104
69,35.1312
Selenium
113
4-87
mg/kgwet
117
96
78,46.1'-0-5
Sodium
646
487
mg'kgwet
621
104
73-75.126,4
Zinc
278
4,87
mg'kg wet
240
116
80.83-1192
Reference (B91-10497-SRM2)
Total Phosphorus as P
819
1-3.3
mgrkg wet
866
95
19.86-15935
Batch B9H0866 - EPA 7471 B
Blank (B9H0$66-BLKI)
Mercury
ND
0.00020
mg. -kg
Blank (B911-10866-11LK2)
Mercury
L,CS (B9H0866-BSI)
Mercury
Reference (B9H0866-SILN1l)
Mercury
ND 0.020 mg,18
0.0047 0.000-10 mg kg 0.00500
12 0,039 mg -'kg 12.5
94 80-120
96 60.3-140
PO Box S655 Grerinf•,,,,, SC 296,06 46 =a,f-ts• e—t W,'tv Gr•--E'mnfle, SC 29607 , 86 22, f�3 864 232614o rogersa Edcallcott.com
08 23 014 06,41 This )vI)oro no,rv,wl he reltrodnred, except in jrll, wirhou! urirren permir.rinn fimn Rogers & Crolhnm, hoc. Page 5 Of 9

Rogers & caticott
ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9080402
Asheville, NC 28801-4310 Reported: 08/23/19 06:41
Sample Preparation Data
Parameter Batch Sample ID Prepared Analyr
EPA 30508 Metal Digestion
EPA 3050B B9140497 9080402-01 08/12-12019 09:52 LMC
EPA 7471E Mercury Digestion
E11A7471B B9H0866 9080402-01 08/19/2019 15:45 TLT
PO Box 5655 G; eet.vilie, SC 296 426 F�irforest Way G•ee ville, SC 29607 main: S64.232.'556 txx 5G4.232.6?40 f C)gersandCaIICOCt.Co171
0812312019 06,41 This iepory ntay not be reproduced, ercept inJJl, without written perntission front Rogers & C'allcou, lnc, Page 6 0f 9

it, Rogers & Cattcott
E NV IRON ME NTA L
Environmental Testing Solutions Project: Wavnesville W WTP
351 Depot St, Work Order: 9080402
Asheville, NC 28801-4310 Reported: 08/23/19 06:41
Data Qualifiers and Del3nitions
ND Analyle NOTDETECTED at or above the repotting limit
NR Not reported
RPD Relative Percent Difference
PQ Brax 5€a55 GrLenvMe, SC 29606 426 Fatrfcrest V by Greenville, SC 29607 man 964,232.15S6 fax 864,2316140 rogers-andniicott.COrn
- Me1 I.
081231,1019 06; 41 This repon may not he reproduced. except in fi(14 wilhoul urines penuicetrin from Rogers & Callcou• Inc. Page 7 0f

Rogers &Cakott CHAIN OF CUSTODY
41 ENVIRONMENTAL
Malling PO Box5655 shipping 426FairforestWay 215EStonerOgeDrive
Address: Greenvdle,5C29606 Address: Greer ille,SG29607 Columbia,5C29210
Phone [phone] Fax [phone] Phone [phone]
Client Name
Address
f� a,
L— I ht �`
0
ReportTo: o
Email Address o � {
p n�.
Tele hone # z
PO # Project # '
a
WORK ORDER DATE TIME SAMPLE DESCRIPTION CL
RECORD
WORK
ORDER 61M4o2
Filtered &S/9 j
Cooled ��O)
Container TypeLPlastiC lass
Container Volume (mL) �
[ Sample Type Lrablc poslte
tN Sample Source>W, GW, DW, Stlother}
Preservation Code(s)
A —None E—NCI I—ZnAcetate
B—HNO3 F—Na25203 J—H3PDa
C— H25Oa G — Boric Add K- MCAA
D - NaoH H — Ascorbic Acid L-
�3
��
�r
COMMENTS
oaq
oew
3UWZQ 5 bud -Ga
4.,r,4b Lo wtarP
•J-nVJ-- mG I I(q
SAMPLER-i3 Q I ED BY:
1 j/L LX
DATEMME:
.m,1 O,,
RECEIVED BY:
Z 17ede. , I
DATE/TIME-
!i
Composite Start Date:
Composite Start Time:
Time or Flow (Circle one) Initials:
RELINQUISHED BY:
3. F (1��
DATE/TIME:
RECEIVE Y:
4.
DATErfIME:
.1.1a 1140
RELINCI ISHED BY:
5.
DATEMME:
RFC BY:
6.
DATE/TiME:
1
Temperature of blank or representative sample
At time of collection "C
At time of lab receipt 6.7-1 11.0 -C
RELINQUISHED BY:
7,
DATE/•TlME:
RECEIVED BY:
g,
DATE/TIME:
Possible Hazards associated with samples: QNon-Hazard [--]Flammable ❑Skin lrrftant Poison Unknown E]7ther Form Revised July, 2014 Page Page 8 of 9

EN11f`RD(V.M> NTAf
Sample Receipt Verification
Date Work
Client: Received: •� • lg� Order: 0z,
Carrier Name: Client Fed13x UPS US Mail Courier Field Services Other:
Tracking Number: tOT2350 411a ` 2�
Receipt Criteria
Y
e
o
A
Comments
S
Shipping container / cooler intact?
Damaged Leaking Other:
Custody seals intact?
COC Included with samples?
COC signed when relinquished and received?
Sample bottles intact?
Damaged Leaking Other.
Sample ID on COC agree with label on bottle(s)?
X
Date / time on COC agree with label on bottle(s)?
K
Number of bottles on COC agrees with number of bottles received?
Samples received within holding time?
X
Sample volume sufficient for analysis?
X
VOA vials free of headspace (<6mm bubble)? -
x
Temp at receipt recorded on COC
Samples cooled? m measured with SN: 97050067
Te
`
Ice Cold Packs Dry Ice None
Samples requiring pH preservation at proper pH?
Note_ Samples for metals analysis may be preserved upon receipt in the lab.
Note: Samples for 0&G and VOA analysis — mservation checked at bencb...
Samples dechlorinated
for parameters requiring chlorine removal at
the time of sample collection?
x
Note: Chlorine checked at bench for samples requiring Bactorial, VOA, and HAA
aftS.
If in-house preservation used — record Lot #
HCL
H3POa
H2$Oa
NaOH
HNO3
Other
Comments:
Were non-conformance issues noted at sample receipt? Yes or No)
Non -Conformance issue other than noted above:
Revised February2016 Completed by:__
Page 9 of 9

_77
envirochem
ANALY! fGAL & co�jsuurlNG CHENAISIS
Environmental Testing Solutions, Inc.
Post Office Box 7565
Asheville NC 28802
Attention, Kelley Keenan (ETS)
Lab ID Sample ID:
19-33352 Site: 503 Lime Sludge
Environmental Chemists, Inc.
V 279J 04-
14) d,
i Nil- 2 k ',4 7. 5,4­l
is ICIW! R1:'b - "M
Date of Report- Aug 22, 2019
Customer PO #.,
Customer ID: 08100055
Report #: 2019-13014
Project ID. Waynesville WWTP
Collect Date/Time Matrix Sampled by
8/6/2019 8,00 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Nitrogen (caic)
Nitrate+Nitrite-Nitrogen EPA 353 2
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B
Total Nitrogen Tolal Nitrogen
Comment-, Results reported on an as received basis
Reviewed by:
0.25 mglkg
5680 mqlkg
5680 mg/kg
08/20/2019
08/07/2019
08122)2019

Environmental Chemists, Inc.
L envirochem
L!�V-6�­ lei:._
L� 4., Jx
%
ANALYTIC"AL & CONSULTING CHEMISTS
LCS
QC ETS- 2019-13014
Parameter, erne I'Llille IIrLimils
n I i�l
NO3-rNO2 1.00 0.99� 90 -1 io
9
10.0 g.,7 7 90-110
MS/MSD
I lWe
Recove)-v
% RC.-Overlt,
bmiisfli
Lhwii.y ""!'
Ing.1
mg, L
—50—
—10
Dijj&rmcc
RecoVery
Dffirence
0
NIA
80-1210
<
TKN
4.0
Q
98/98
0
80-120
DUPLICATE SAMPLES
Pai-ameter
NO3 i-N5-2--
JR-IN'
BLANKS
Parameter
NO3--NO-')
TKN
Resuhs
Inn! L
<().O" < 0. 021
N1, "A N"'A
Results
)nglL
<0A1
< 0 '2) 5
Limit
ing-1,
0.01
0.22 5
%
NlA

CRIAIN-OF-CL)STODY Analytical Request
("NenN ! a
Am
N
ao n" V sting Solutions, inc, (a'port
PO flax 7565, eksheville, NC 28802 Pbone:
Phone: [phone], Fax- [phone] )IC) Number:
. . . .................
t
5b3
: AIM-alkinpil 4 lkuvrimfs-.
ALLY d -v h
Field Comments
Tmp. ("(
L

k,
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name:
CHAIN -OF -CUSTODY / Analytical Request
Client Name: IDI, A 07 O aglieSUl lle Wl) 71
Address: j (mf a�yl�-� ra ,` [ led
1.Ju e s ;'lie Ak ,?8 785"
Report to: rct4 r ,6
Phone: 414_6-$" Fax: l,6a8] 115-6-aa1,3
PO Number:
[ Requested Analyses
Project Number: 96OWS321
p1l Checked Upon It.CR71 t
CI; <0'_ mg'1 L•tx+1ti Rctrilsl
Preservatives
_
r
V)
QO '�
s Sample Identification
L
e =
—r
-r
a =
v c
u C O �' t,
F= a z o z
Field
Temp. ("CI Comments
5-03 Lime S & u
C
oar,
I
W. 5{►z
�a. a
,j
g (o v9
g;50
�! J laW r
Temperature (T)
Received on Ice:
t� / N
Co���
i 9 (k
`
IW 7
LA_
Ik
(�l#A
Y
iD
Sealed Cooler:/
/ Y )/ ! N
Samples Intact:
Jf% N
Additional Cuntments:'* Al I !'t1Y1&b i'a-104r--API A$ICis Ca
CpN Pb1 M[, Ng I
Mal 1��� M trak-4),-h1 K- �7. � "/0 TL't4 � So1,*J5 nH f r �
j 1 I
Lb �lCte
Printed c of � mplrr.
'►}-in 1
M tYe3Cn I�'f r�+,,
'JR PIC4 A o& %; b j .
SFgfY.itt S 5' CE".

_l Environmental Testing Solutions, Inc. Certificate of Analysis
Project name; Town of Waynesville W WTP
Collection date: 8-Aug-19
Date received: 8-Aug-19
Sample identification: 503 Lime Sludge - Composite
PO BoN 7565
Asheville. NC 28802
Phone: [phone]
Pax: [phone]
Project number: 190808.500
Sample number:
171422
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
°i Total Solid SM 2540 G 63 0.10 % 8-Aug.19 KI K
Multiple "Tube Fermentation SM 9221-I <113 113 MPN/9 n-Au.-19 KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting; Limit only.
Date reviewed: � � (�j 1' 5 NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
p NC Drinking Water Certification Number: 37786
Signature: V
l$is reportshould not he reproduced, exept in its entirely, without the written consent ol'Environmental Testing Solutions. Inc
The results in this repon relate only to the samples submitted for analysis.

•
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name:
CHAIN -OF -CUSTODY / Analytical Request
p
Client Name: d: ie E 1
Address: 6 On
Report to: pal ' nMi
Fax:g
PO Number:
}Requested Anair-sea
Project
Number:
pH Checked Litm Reoci
Cl: 02 rng3 Upm Rcwipt
�
9
Preservatives
Sample Identification
E
a
rZ>zC7
E
_
�.
,
E
`o
C
rnld
z
v
z
ti'Dz
z.
("Cy Comments
G
*-+Hzz
I
1
C
'Temperature ('C)
O • j �/
'C�t (.�. �7 ;
91 911
$t �TS �a.r�•al
/a/ (�
$ �'�
Received on Ice:
Y N
f/ 5 ('
I'li(l4
1
m4 f
CDs
{J��
pqy
Sealed Cooler:
! N
Samples Intact:
N
Additional Comments:
Pri, amr of Sant Err
`Ck w� i -�. f-���.M `7 S
Si ^ a ' Sampl �^
f/

t
Environmental Testing Solutions, Inc. Certificate of Analysis
Pro_jeet name: Town of Waynesville WWTP
Collection date:
Date received:
4-Nov-19
4-Nov-19
Sample identification: 503 Lime Sludge - Composite
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 191104.509
Sample number: 193805
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Arsenic
6010 D
6.07
3.31
mg/kg
12-Nov-19
LMC
1
Cadmium
0010 D
<1.32
1.32
mg/kg
12-Nov---19
LMC
1
Copper
6010 D
183
1.32
mg/kg
12-Nov-19
LMC
1
Chromium
6010 D
24.4
3.31
mg/kg
12-Nov-19
LMC
1
Lead
6010 D
15.1
3.31
mg/kg
12-Nov-19
LMC
1
Molybdenum
6010 D
3.65
3.31
mg/kg
12-Noe-19
LMC;
1
Nickel
6010 D
13.1
1.32
mg/kg
12-Noe-19
LMC
l
Selenium
6010 D
3.9
3.31
mg/kg
12-Nov-19
LMC
1
Zinc
6010 D
490
33.1
mg/kg
12-Nov-19
LMC
I
Aluminium
6010 D
12500
331
mg/kg
12-Nov-19
LMC
I
Calcium
6010 D
263000
6610
mglkg
12-Nov-19
LMC
1
Magnesium
6010 D
7280
331.0
mg/kg
12-Nor-19
LMC
1
Potassium
6010 D
1680
66.1
mg/kg
12-Noy--19
LMC
1
Sodium
6010 D
442
66.1
mg/kg
12-Nor-19
LIv1C
1
Mercury
747113
0.59
0.068
mg/kg
18-Nov-19
TLT
I
Total Kjeldahl Nitrogen
SM 4500 ORG B
167
mg/kg
28-Noy-19
ECHEM
3
Nitrate + Nitrate
353.2
14.0
mg/kg
18-Nov-19
ECHEM
3
Total Nitrogen
Calculation
181
mg/kg
29-\ov-19
ECHEM
3
Total Phosphorus
2003
5630
331.0
mg/kg
12-Nov-19
LMC
I
Total Solids
SM2540 G
57.2
0.10
%
6-Noy--19
JND
l
PH in Soil
SW 8469045D
12.0
0.10
S.U.
4-Nov-19
MS
2
% Total Solid
SM 2540 G
55
0.10
%
4-Nov-19
MS
Ammonia Nitrogen
EPA 350.3
450
7.3
mglkg
,-Nov-19
KEK
Sodium Absorption Ration
CALC
1.2
mg/kg
21-Nov-19
KEK
Plant Avaliable Nitrogen
CALC
182.4
mg/kg
2-Dec-19
KEK
Footnotes:
RE, = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Sample analyzed outside holding time. Duplicate result was 12.3 S.U.
3. Sample analyzed by Enviro Chemists, Inc,
Date reviewed: /9.02- 1 q
Data reviewed by: Kelley E. Keenan
Signature:
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exepl in its entirety, without the written consent or Environmental Testing Solutions, Inc,
The results in this report relate only to the samples submitted for analysis_

Rogers & Callcott
ENVIRONMENTAL
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St_
Asheville, NC 288014310
Dear Client
°BorrriR+'�`
Laboratory Report
Project: Waynesville WWI?
Work Order: 9110190
Received: 111052019 11:45
Rogers and Callcott appreciates the opportunity to be of service to you. -]'he attached laboratory services report includes analytical results and chain of
custody for samples that were received on November 05.2019. Rogers and Callcott maintains a formal QAQC program. Unless otherwise noted, all
analyses performed under NELAP certification have complied with all the requirements for the TNI standard The analyses met the QA"QC confidence
interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request.
Privileged., Confidential information may be contained in this report and is intended only for the use of the addressee. Ifyou are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. if you receive this message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients, please contact Sarah Baker, your project Manager, at samh.baker(a,rogersandcallcott.coin or
(864)-232-1556 if you have any questions about this report.
Report Approved By:
Sarah Baker
Project Manager
This mporl mqv not be reproduced, except in fidl, ❑ flhow a rilien pcimissimr /rmn Rogers & Callcou. Inc -
PO 0ctx 5635 tarecnvirc, SC 29606 42 , forest Wxr Grce-wAkn, SC 29647 .,,,,.,, 864.232 `S56 fax 864,231614o rQgersaf)deallcott,corrl
Page 1 of 9

Rogers & Catleott
ENVIRONMENTAL.
Certificate of Analysis
Client Environmental Testing Solutions
Kelley L. Keenan
151 Depot St.
Asheville, NC 28801-4310
Sample Number Sample Description
9110190-01 Waynesville WWTP 503 Lime Sludge - Comp
Son& Carolina Greenville Laboralmy Identificalion 23105
South Carolinas Columbia Laborarmy !dent fcaiion 40571
North Carolina Laboralorr Cerlificalion ltanber 17
North Carolina Drinking Wafer Lab Nrtniber 45710
NEI 9A Utah CeriVicate Number SC000042014-1
Georgia Drinking Water Lab ID 880
Project: Waynesville wwrP
Work Order: 9110190
Received: 11f05/2019 I L45
Matrix Sampled 7�pe
Sludge 11/04/19 08:18 Composite
PC? Box 5655 Gs-eenvi[le, SC 2%06 426 Fairfarest Way Greenville, SC 29607 main 864.232.1556 fix 96-232.61.10 rogersandCallcott,com
._ _..-- -_.- _. -_ ,�n r. rnl•nnyrw •mvnr•I r;trnt�any
11t1911019 14:39 Thtr n pori rnuy nor be m-pmduced. except in jdl. wilhow wrinen permission f bm Roger & C'a0col41nc,
Page 2 of 9

G Rogers & Cakott
LNVIIkQNMLN IAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9110190
Asheville. NC 28801-4310 Reported: 11119 19 14:39
Sample Data
Sample Number 9110190-01
Sample Description vvaynesvi11e Wei'"rP 503 Lime Sludge - Comp
Reporting
Parameter Result Limit
collecied on I U04.' 19 08:18
Units Dp Analyzed
Method
Fing Analyst
Batch
General Chemistry Parameters
'Total Solids
57.2
0.10
gn
1.00
11'06119 10:45
SN1 25400
JND
B9K0235
Total Metals
Mercury
0.59
0.068
mg`kgdry
2.00
11'18'19 11:18
EPA 7471f3
TAT
139K0756
Aluminum
12500
331
mg`kgdry
100
11'12'19 23:18
l"iPA6010D
LMC
139K0292
Arsenic
6.07
3.31
mgAgdD^
1.00
11'12119 23:25
ERA 00100
LMC
139K0292
Cadmium
ND
1.32
mgftdry
1.00
11'121,19 23:25
EPA6010D
LMC
139K0292
C'nlcium
263000
6610
ing,'kg dn'
1.000
11! 15'19 17:18
EPA 601OD
LMC
139K0292
Chromium
24.4
3.31
mgkg dry
k00
11'12!19 23:25
F,PA 60101)
LMC
B9K0292
Copper
183
1.32
mk'kg dry
1.00
11212119 23:25
EPA 601 OD
LMC
B9K0292
Lead
15.1
3.31
mg'kgdry
1,00
I1'12119 23:25
EP11,60101)
LMC
B9K0292
Magnesium
7280
331
mgrkgdry
100
11!12'19 23:18
EVA601OD
LMC
B9K0292
Molybdenum
3.65
3.31
mg'kgdry
1.00
11.-12!19 23:25
EPA60101)
LMC
B9K0292
Nickel
13.1
1.32
mg'kgdry
1.00
11112119 23:25
EPA 601OD
LMC
1391(0292
Potassium
1680
66.1
mg'kg dry
10.0
111.12/19 23:21
EPA 601OD
LMC
139K0292
Selenium
3.88
3.31
mgkgdry
1.00
11112/19 23:25
EPA60100
LMC
139K0292
Sodium
442
66.1
in6,kg dry
10.0
11'12119 23:21
EPA 601OD
LMC
B9K0292
Total Phosphorus as I'
5630
331
mg kg dry
100
11112/19 23:18
EPA 601 OD
LMC
139K0292
Zinc
490
33.1
rnWAg dry
10.0
11/12/19 23:21
FPA601OD
LMC
B9K0292
PC) Box 5655 (3r �,ervi; , SC '29606 426 Fa:r, _, sr VV-ay C: c"en..,. _. SC NO' .,.,r 864,212 i S 50 ..= 864 731.6140 rope "SandcaIICOtt.com
at»o Ipviy�-n uwnerf t wl 1p.e ny
111,19r2019 1 d:39 This mpori muy nni he reprvduced, except in fitlf, wirhoid wrWen permission from Rogers & Callcolr. Inc. Page 3 Of 9

Rogers & Caleott
FNVIRONMEEINTAL
Environmental Testing Solutions Project; Waynesville WWTP
351 Depot St. Work Order: 9110190
Asheville, NC 28801-4310 Reported: 1 I'19119 14:39
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPU
Parameter Result limit Units Level Result %REC Limits RPD Limit Flags
Batch B9K0292 - EPA 3050B
Bluuk (B9K0292-BI,K1)
Aluminum
ND
0,05
mg kg wet
.Arsenic
ND
0.05
mgkg wet
Cadmium
ND
0.02
mgkgwet
Calcium
ND
0.10
rogkgwet
Chromium
ND
0.05
ntgkg wct
Copper
ND
0.02
mgkgwet
Lead
ND
0.05
ingkg wet
klagnesium
ND
0.05
mg'kgwet
Molybdenum
ND
0.05
nigkgwo
Nickel
ND
0.02
mgkgwet
Potassium
ND
0,10
mg'kg wet
Selenium
ND
0.05
mgkg wet
Sodium
ND
0,10
mgkgwet
Total Phosphorus as P
ND
0.05
mg -kg wet
Zinc
ND
0.05
mgkg wei
LCS (B9K0292-BSI)
Aluminum
0,46
0,05
mgkg wet
0,500
91
80-120
Arsenic
0,47
0.05
mg=kg wet
0.500
94
80-120
Cadmium
0.47
002
mgkgwet
0,500
95
80.1'--0
Calcium
OAK
0,10
mgkgwet
0,500
97
80-120
Chromium
0.47
0.05
mg1l;wet
0.500
94
80-120
Copper
0.47
0.02
mgkgwet
0300
95
80-120
Lead
0.47
0,05
mgOcgwet
0.500
94
80-120
Magnesium
0A8
0,05
mg'kg wet
0.500
97
80.120
Molybdenum
0,48
0.05
mgkgwet
0,500
95
80-120
Nickel
0,46
0.02
mg'kg wcr
0.500
93
80.120
Potassium
4A9
0.10
mgtkg wet
5,00
90
80.120
Selenium
0.46
0.05
mgfkgwet
0.500
91
80-120
Sodium
0.51
0.10
mg,kg wet
0.500
102
80-120
'rural Phosphorus as P
0,44
0.05
ntgkg wet
0.500
89
80-120
Zinc
0.49
0.05
mglcgwet
0.500
97
80420
Reference (89K0292-SR_1ll)
Aluminum
11700
243
mgkgwet
8490
138
50.41-149.59
Arsenic
97-7
4,86
migkg wet
91.6
100
59.98-130.12
C
' -,r? #C,y 9C "xt'•Y""Ii; .Ti< �.*e JC'iT
eB�.-, i';ii rE;r v?L �inY
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... ..^. 864,s32 "5i :34
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614�; I d � o1_C.com roge san ca c
W19/2019 14:39 This mlio r mu3• nor be rrpnithiced. except in JuIL ❑dthoni mriilen permusion from Rogens & Callcnu, Inc Page 4 0f J

Rogers & CaRcatt
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9110190
Asheville, NC 28801-4310 Reported: I1.19i19 14:39
Total Metals
Quality Control Summary
Reporting Spike Source %RFC RPD
Parameter Result Limit Units Level Result %REC Limits RPI) Umil Flags
Batch B9K0292 - EPA 3050B
Reference (B9K0292-SRM1)
Cadmium
Calcium
Chromium
Copper
I -cad
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Reference (B9K0292-SM12)
Total Phosphorus as P
Batch B9K0756 - EPA 7471E
Blank (B9K0756-BLK1)
Mercury
Blank (B9K0756-BLK2)
Mercury '
L,CS (B9K0756-BSI)
Mercury
I CS (B9K0756-BS2)
114
1.95
mg1gwe[
114
100
75-125.4
5130
486
mg g. wet
4730
108
72.52-127.3
156
4.86
mg kg wet
147
106
70.07-129.9
100
1,95
mg/kg wet
97,7
102
75,03-124.9
lot
4.86
mgkg wet
105
96
70.48-128.6
2860
243
mg -kg wet
2310
124
60-138.1
82.5
06
mg kg wet
78.8
105
69.54-130.7
120
1,95
mgkgwet
119
101
69,92-1302
2730
486
mgikgwct
2040
134
58.82-140.7
90.3
4.96
mg'kg wet
93.1
97
64.55-135.3
176
9.73
mg Ica wot
t54
115
39.68-161
216
4.86
rn 'kg wet
212
102
69.81-129,7
711 24.3 mg kg wc[ 776 92 ",16.177.84
ND 0.0001-0 mgkg wot
ND 0.020 mg'kg wc1
0.0046 0,00020 mgkgwet 0.00500 92 80.120
Mercury 0.47 0.020 mg -kg wet 0 497 94 80.120
Reference (B9K0756-SRMI)
Mercury 16 0.040 mg'kg wet 12.5 130 60.3.140
PO ROX r655 i recr ss;_ ., SC _ 06 4 A'airfo: est%i G,eevil .. <t~ 2907 :;„;; 564.232.15,56 _,x 13 ,2.32.61 o rogersandc-01catt.com
111) 9VM9 l4r39 This report tnar tint be reproduced, except in fin't, Page 5 4f J

Rogers & Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9110190
Asheville, NC 28801-4310 Reported: 11/19/19 14:39
Sample Preparation Data
Parameter Batch Sample ID Prepared Analvst
EPA 3050B Metal Digestion
EPA 3050B 139K0292 9110190-01 11111/2019 0930 LMC
EPA 7471 B Mercury Digestion
EPA 7471B B9K0756 9110190-01 11/15/2019 08:00
PC? 0ox 5655 Greenville, SC 29606 25 K irlcsrest Wiy Greenville, SC 39607 main 864,232.I556 fix 864,1132 6140 rogersandcaUcntt.corn
an • .
HY1912019 14,39 This report may nor he mprodneed, except InJtd1. without wrillen perwission from Rogers & C'ollcoll. Inc. Page 6 of 9

Rogers &Caticott
ENVIRONMENTAL
Frivirommental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9110190
Asheville, NC 28801-4310 Reported: 11119114 14:39
Data Qualifiers and Definitions
ND Analyte NOT DETFCTED at or above the reporting limit
NR Not reported
RI'D Relative Percent Difference
PO Box 5655 Greenville, SC 29606 426 F-airfore-st %A&y i Greenville, SC 29607 r-,wr,, 864-232-ISS6 fax 864,232,6140 rogersandcailcott.com
1111912019 14:39 This report may not be reproduced, Lreept in fill, nlihont written permissionfromRogers & Callcort. hie,
I Page 7 of

Rnaprs J�. C nIlrott CHAIN OF CUSTODY RECORD WORK ORDER �11 A
- 7!- — ENVIRONMENTAL
mailing PO Box 5655 Shipping 426 Fairforest Way 2158 Stoneridge Drive
Address: Greenville,5C29606 Address: Greenville,SC296D7 Columbla,SC29210
Phone [phone] Fax [phone]-M40 Phone [phone]M9
Client Name
Address
Report To:
Email Address
Telephone #
PO # Project #
c
o
v
o
E
Z
.I
E
Filtered Lesj o)
Cooled, e�No)
ContainerTypeLiastic/v5S
Container Volume (ml.) :�lQ
Sample Type (Grab/ mpos(te)
Sample Source (WW, GW, DW, 5W 5, ther)
Preservation Code(s)
A —None E—HCI I—ZnAcetate
B—HNO3 F—NazSzO3 J—H3PO4
C— H2SO4 G—Boric Add K- MCAA
D-N20H H-AscorbIcAcid L-
��
C�~
~ r
i
r
�'
R&C
WORKORDER
YR
DATE_
TIME
SAMPLE DESCRIPTION
COMMENTS
n
tjw,c
L016
3C;yV objelor__ tors-p
L
)L
y-
rQor,ftD
WWTP
WeJ Alq t
_
M
i�)T�1 rnrirotl� vu-� t.t'�o►nis
SAMPLER -RE(((��� HED BY:
I
1.
DATE/TIME:
'f
RECEIVED BY:
Z. R �ry - ^
(Y�€_-Y
DATE/TIME:
/ f ) (,J Q
7
l
Composite Start Date:
Composite Start Time:
Time or Flow (Circle one) Initials:
REf,141Q�DBY;
3. t �
DATE/TIME:
RECEIVED
4'
DATE%TlME:
II _ C,-1 Li 144-S
RELINQUISHED BY:
S•
DATE/TIME:
RECEIVE
6•
DATE/TIME:
Temperature of blank or representative sample
At time of collection "C
At time of lab receipt t_ 4 sC
RELINQUISHED BY:
7.
DATE/TIME:
RECEIVED BY:
B.
DATE/TIME:
PossibfeHazards associated with samples: Non -Hazard ❑Flammable ❑Sk[nirrltant LIPoison nknown �ther Form Revised July,2014 Page Page 8 of 9

Rogers:&C[[cott
Sample Receipt Verification
Date Work
Client: — -- - Received: 11. . I Order: 4 I I p
Carrier Name: Client FedEx UPS US Mail Courier Field Services Other: _
Tracking Num en. 2 3 a
Receipt Criteria e o .A Comments
s
Shipping container / cooler intact?
Custody seals intact?
COC included with samples? .r
COC signed when relinquished and received?
Sample bottles intact? V
Sample ID on COC agree with label on bottle(s)? Ij
Date / time on COC agree with label on bottle(s)?
Number of bottles on COC agrees with number of bottles received? V
Samples received within holding time? h
Sample volume sufficient for analysis?
VOA vials free of headspace (<6mm bubble)?
Samples cooled? Temp at receipt recorded on COC
Tamp measured with tR thermometer • SN: 97050a67
Samples requiring pH preservation at proper pH?
Note: Samples for metals analysis may be preserved.upon receipt in the lab.
Note.' S=V[eSfOrO&GaMdVOAMIdY$iS—DmcrvationcheckMathpneh.
Samples dechlorinated for parameters requiring chlorine removal at
the time of sample collection?
Note: Chlorine checked at bench for samples requiring Bacterial, VOA, and HAA
Damaged Leaking Other;
Damaged Leaking Other:
lee ) Cold Packs Dry Iee None
_ If in-house preserVOtiDrI used -- record %ot #
HCL H3POq'
H2SO4 NaOH
HNO3 Other
Comments:
Were non-conformance issues noted at sample; receipt? Yes or No
Non -Conformance issue other than noted above:
Revised February 2018
Completed by:
Page 9 of 9 1

L envirochem
%J
ANALYTIC
AL & CONSULTNG CHPAJS�I S
Environmental Testing Solutions, Inc,
Post Office Box 7565
Asheville NC 28802
Attention:
Lab ID Sample ID-
19-47776 Site, 503 Lime Sludge
Test
Total Solids (%)
Total Kjeldahl Nitrogen (TKN)
Total Nitrogen (calc)
Nitrate+ N itrite-Nitrog en
Total Nitrogen____
Etivirotimental Chemists, Inc.
I 1 1 !,�h)j I - i 1 1,3 2-4,124 f
1"' d, Mayavofk� - 'J'.
'4 Fa\
3 U- b
Date of Report: Nov 29, 2019
Customer PO #:
Customer ID: 08100055
Report #,- 2019-18769
Project ID: Waynesville WWTP
Collect Date/Time Matrix Sampled by
11/412019 8:18 AM Solid/Sludge Client
-Method--- - --Results Date Analyzed
SM 2540 B 53.5% 11 /11 /2019
SM 4500 Org B 167 mg/kg 11/28/2019
EPA 353 2
'rota! Nitrogen
Comment: Results reported on a dry weight basis.
Reviewed by-
14,0 mg/kg 11118/2019
181 mglkg 11/2912019
Remrt4l: --11C-187139 Page': of I

CHAIN -OF -CUSTODY I Analytical Request
Clielit Name: —70
Addi.
A
EAvironmental Testing Solutions. Inc. Report to:
PO Mix 74565, Asheville, N"C' 28802 Pbone. Fax-:
Plume� (828) 3-50--q364, Fm [phone]
Pro � ��W"r1j!)VJ1(40 LOL4 rho
PwjL�,l N u n be r
Y11
Comments
j
LT
���LAL
S��A�,d Coolet

•
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name: 1A64M-.Md1&
CHAIN -OF -CUSTODY / Analytical Request
Client Name: B� W�r1ltSli,`��G �wY
Address:
vhqy
Report to: Thh OL�ri
Phone: ($;4C) �{Sa.y(ard y Fax: (1?'aQ-)C4Sb a013
PO Number:
Requested Analyses
Project Number:
KY
D1I ['htzka i t:p:n Rc[eipl
CI, ' 0.2 rnpl Upon RL•ccipl
U
Sample Identification
_
._
r
i
F S
Preservatives
Field
Temp. ("C) Comments
z"
z
J
z
z
A-03 Li,hr_ Sludtot
C
IA3a)s
11(y lq
9:14
3
✓
✓
33°F
I
Milli!
Temperature('C)
�'
IM11mi
falfr W . f�l
W�Re9w�
11I�I�q
$J�rf�Q
g-3�
Received on Ice:
Y N
ZT.5 (o[.i. c�
! 1l lq 11 q
/ �
✓ k
6D)
I//c/5
/636
Sealed Cooler:
Y N
Samples Intact:
Y N
Additional Comments_ 41 1 A"anl0.NilAkaalr, t Js, cA, c r, Ca � CAI ft, Mj t 145, Ma
11Pe t Iral AI+4r� 4Al-"tnt Va T-6a rjol�, fal P, Kt Ce AL, SA9, TKAv�
ZYl , I)14nI cLv., ,%Wf- APA oqe- �-b1J CAW'�= o�,
�
Printed Name o 4ntpler:
til ttif�'- lei:
}

Load & Temperature

LOAD TEMPERATURE LOG
YEAR
MONTH
PASTEURIZATION PASTEURIZATION OPERATOR
nATF LOADS IN TEMP. OF OUT TEMP. OF INITIAL
fn
Ll
Jo
Lc
Inc t-c
I LA
CA 5
ly
15
Cl
fnc-
KEEP SEPERATEDFROM
MAN DISTRIBUTION PILE ANY
LOADS THAT DONOT REACH
AND MAINTAIN 158oF.
|TTAKES AMINIMUM OF
3OMINUTES TOGOFROM
PASTER|ZAT|{}N|NTD
PASTER|ZAT|ONOUT.
t- As~~ 2q
revised: 2/7-25105

LOAD TEMPERATURE LOG
MONTH
PA8TEUR|ZATlONPA8TEUR|ZATON OPERATOR
DATE #LOADS IN TEMP. OF OUT TEMP. OF INITIAL
ol
KEEP SEPERATED FROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT DDNOT REACH
AND MAINTAIN 158~F.
|TTAKES AMINIMUM OF
3OMINUTES TOGOFROM
PASTER|ZATON|NTO
PAGTER|ZAT|ONOUT.
�06�� 1,6
revised: 2/7-25/05

LOAD TEMPERATURE LOG
MDNTH
PASTEURIZATION PASTEURIZATION OPERATOR
DATF |OAOS |NTEMP- »F OUT TEMP. »F INITIAL
o
72)
cl
J,
t, c k )-V-)
c)
1-c
I -A
KEEP 8EPERATEDFROM
MAN O|8TR|8UTlDN PILE ANY
LOADS THAT DONOT REACH
AND MAINTAIN 158OF.
[TTAKES AMINIMUM OF
3UMINUTES TOGOFROM
PASTER|ZAT|ON|NTO
PASTER|ZAT}C>N{}UT.
)
revised: 2/7-25/05

LOAD TEMPERATURE LOG
YEAR C� MONTH
PASTEURIZATION PASTEURIZATION OPERATOR
DATE #LOAOG |NTEMP. oF OUT TEMP. »F INITIAL
CAW
Ll
117
4�2
KEEP 8EPERAJEDFROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT DONOT REACH
AND MAINTAIN 158^F.
|TTAKES AMINIMUM OF
3OMINUTES TOGOFROM
PAGTER|ZAT|[)N|NTO
PA8TER|ZAT|(]N[)UT.
revised: 2/7-25/05

LOAD TEMPERATURE LOG
YEAR
MONTH:j`�
PASTEURIZATION PASTEURIZATION OPERATOR
DATE # LOADS IN TEMP. OF OUT TEMP. OF INITIAL
rn
i..
��
1
N 1hi
.f^
F741
t.
d
gYa f�
,yq n
,fj
KEEP SEPERATED FROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT DO NOT REACH
AND MAINTAIN 158 OF.
IT TAKES A MINIMUM OF
30 MINUTES TO GO FROM
PASTERIZATION IN TO
PASTERIZATION OUT.
revised: 2/7-25/05

LOAD TEMPERATURE LOG
YEAR
�
MONTH
PASTEURIZATION PASTEURIZATION OPERATOR
DATE #LDAD3 |NTEMP. vF OUT TEMP. «F INITIAL
ky
ocj
KEEP 8EPERATEOFROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT DONOT REACH
AND MAINTAIN 158~F.
|TTAKES AMINIMUM DF
3OMINUTES TOGOFROM
PA8TER|ZAT|[)N|NTO
PA8TER|Z\T|ON[)UT.
�
��
�0d��^ °x��
revised: 2/7-25/05

LOAD TEMPERATURE LOG
YEAR I CA
MONTH IA�-i
PASTEURIZATION PASTEURIZATION OPERATOR
DATE #LDAO8 |NTEMP. "F OUT TEMP. ^F INITIAL
411
62
KEEP SEPERATEDFROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT DONOT REACH
AND MAINTAIN 158^F.
IT TAKES A K8|N|KAUM OF
3OMINUTES TOGOFROM
PASTER|ZAT|ON|NTO
PA8TER|3AT|ONC>UT.
revised: 2/7-25/05

LOAD TEMPERATURE LOG
PASTEURIZATION PASTEURIZATION OPERATOR
DATE #LOADS IN TEMP. OF OUT TEMP. OF INITIAL
mc-
rnc
c"
pyn
Ic 11-c
in
KEEP SEPERATED FROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT D{}NOT REACH
4NDMAINTAIN 158OF.
TTAKES AMINIMUM OF
}OMINUTES TOGOFROM
zASTER|ZATON|NTJ
zAGTER|ZAT|ONOUT.
mvisod:2/7-250S
h 3[) \c 'l \/.\ 1
-l'4 'Jo7 /y)&

LOAD TEMPERATURE LOG
YEAR 3u q -
r_l
MONTH D (-PW()'l bC"(
PASTEURIZATION PASTEURIZATION OPERATOR
DATE #LOADS IN TEMP. OF OUT TEMP. OF INITIAL
loi
L(
I Cl
j J
AIL,
rr
f 7 -
cl
Gl q
9,01
L C.
210
U3
67
�i -� ,.,
:z.
t e C
i��a
4/1,
-19
'),00
KEEP SEPERATED FROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT DO NOT REACH
AND MAINTAIN 158 OF.
IT TAKES A MINIMUM OF
30 MINUTES TO GO FROM
PASTERIZATION IN TO
PASTERIZATION OUT.
revised: 2/7-25/05

LOAD TEMPERATURE LOG
YEAR ')A�9
MONTH OCt
PASTEURIZATION PASTEURIZATION OPERATOR
DATE #LOADS IN TEMP. OF OUT TEMP. OF INITIAL
16
Cie
KEEP SEPERATEDFROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT O{JNOT REACH
AND MAINTAIN 158~F.
TTAKES AMINIMUM OF
}OMINUTES TOGOFROM
PA8TER|ZAT0N|NTO
DAGTER|ZAT|C>NOUT.
revisod:2/7-2505

Vector
Attraction

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-"q ID: NC01119
Certification #: 194
.strument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:UO3EO21
Exp. Date:OCT. 2020
pH 13.00 Lot #:
Exp. Date: __
Checked with Traceable Thermometer Serial 480410124 Cal Due Date:10/2/2023
ATE
pij
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIAL
rg
.� 7
! '
o-
,
f/
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
1910
CORRECTED PH SU: a; ^ .
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
tRECTED PH SU: 1 Z- U i
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: ,o— ` -- o' , ? `; f z T11
Post Calibration VPrifiratinn
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
the initial pH reading is taken after the lime is mixed with the 503 sludge,
fhe pH of this initial reading has to be above a pH of 12.
the second pH reading is taken 2 hours after the initial reading.
off of this second reading has to be above a pH of 12.
pH of the final reading (24 hours latter) has to be above a pH of 11.5.
cument changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
SPA ID: NC01119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
PH 10.01 Lot #:
PH 13.00 Lot#:UO3EO21
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. OC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SLI
BUFFER
PH 13.0 SU
BUFFER
INITIAL
Qa
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
—jRRECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
i
CORRECTED PH SU: � y' : f'= ` .e F
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
1 ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FPA ID: NC01119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot#:UO3EO21 Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial * 180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
7
i0
g
I
—
.
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. oC
INITIAL
-rZRECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
Tric pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FPA ID: NC01119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot#:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:UO3EO21
Exp. Date:OCT. 2020
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:180410124 Cal Due Date:1 r12/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
/fl'
1 Y,.'L1
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
i
CORRECTED PH SU: /'), `: 'I /..`."I
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
(,zRECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: ° ')' ' f - )) "
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
!.
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
,alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Dorrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
Fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
fhe pH of this initial reading has to be above a pH of 12.
fhP second pH reading is taken 2 hours after the initial reading.
f H of this second reading has to be above a pH of 12.
the pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
=PA ID: NC01119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
pH 10.01 Lot #:
pH 13.00 Lot#:UO3E021
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. oC OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
N
,..
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
LJRRECTED PH SU: /;q t..( -- ,'
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:,.
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
p
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
,alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
-orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
I ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

VH Mt I tK GALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F :. ID: NC01119
N ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot#:UO3EO21 Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
FI
W' 2i
9
�L ' �L� i.
x �°'.)
IaJ . is
.. ; 66
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU:'-
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
J
i.-.
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
-orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
Fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
Fhe pH of this initial reading has to be above a pH of 12.
Fh— second pH reading is taken 2 hours after the initial reading.
.)H of this second reading has to be above a pH of 12.
Fhe pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH Mt I ER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-PAID: NC01119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
pH 10.01 Lot #:
pH 13.00 Lot #:UO3EO21
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
/
a' ei
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
t
i
<
0
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
uJRRECTED PH SU: �—;1' . ' li"- i;N . H
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FPA ID: NC01119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot*UO3EO21
Exp. Date:OCT. 2020
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
IJ
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU:��
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
—JRRECTED PH SU
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
-alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
4ctual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
I tie pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
IPA ID: NC01119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot#:UO3EO21 Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
,,ORRECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
f > -
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
fl �
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
-alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F`"`-` ID: NC01119
1. ;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
PH 10.01 Lot #:
PH 13.00 Lot#:UO3EO21
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU: , �-' ' 1*"� 1=' - q "'i
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
{
CORRECTED PH SU: 4<
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
F x
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th- second pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
IPA ID: NC01119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
PH 10.01 Lot #:
PH 13.00 Lot #:UO3EO21
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. oC OF
QC
TEMP. oC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 1o.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
1 3;�
t ,`i c�.
a� Ti
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: � = ; - -- 0 • I "' - i <2 .,
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
c � e
uORRECTED PH SU: l� ,� - IN, 6 - i 3
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
` g
CORRECTED PH SU: 0. (ra
Post Calibration Verification
TIME
INITTIAL
Ph
10 SU
Temp.
°C
��'yd
l)' n
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
' "fA ID: NCO1119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
PH 10.01 Lot #:
PH 13.00 Lot*UO3EO21
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial *180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DA)TE!!
TIME
EFF.
PH 7.0 SU
BUFFETRgi
PH 10.0 SLI
UFFER
BUFFER
PH 13.0 SU
BUFFER
INITIAL
j
/'
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU: l �•�� . `1 I 'r 1 �� `. ��
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
0, G
f l ..) I G
CORRECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
AQ, s
j .. , p"C
, S.
CORRECTED PH SU: j ;7 -� 0.:� 7 " /a . %.
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
I�r
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
1 ;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance: �]ltve�!,,o
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:UO3E021
Exp. Date:OCT. 2020
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. C OF
QC
TEMP. °C OF
CAL
TEMP. OC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SLI
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
ri q)
CORRECTED PH SU: t')," , tl i
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
G.-, <RECTED PH SU: i :2' I — C) , ,') � - ter t I
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
CORRECTED PH SU: ��'° d -9 0
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
�"M�')
'0 ..
fe.�
D�" 0,.,
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The.second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
P ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
pH 10.01 Lot #:
pH 13.00 Lot#:UO3EO21
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. oC OF
QC
TEMP. C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
TIME
PH7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER}
INITIAL
pDATE
YEFF.
//
;',(��c`.
f s
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU: �• �a ; �w2,
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
C, ..RECTED PH SU: 0'- . S _ e.)- -) -7 � I J, G ,3
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
49
CORRECTED PH SU: ;;.: - t -,' "=
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
7 )H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA_ ID: NC01119
I ',�rtification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
pH 10.01 Lot #:
pH 13.00 Lot#:UO3E021
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. OC OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SLI
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU: tp
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
C -—RECTED PH SU: '�) _ �c __. 6 ` J J , -3
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
4u `�
t � `
� vo , (
d � , �-0
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
T -)H of this second reading has to be above a pH of 12.
Tim pH of the final reading (24 hours latter) has to be above a pH of 11.5
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FPA ID: NC01119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:UO3EO21
Exp. Date:OCT. 2020
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
* 180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PHp)7.0 SU
BUFFER
PHj 10.0 SU
BUFFER
PH 113..0 SU
BUFFER
INITIAL
7,
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
-7 "�j I)Ah
7 .. 'y
CORRECTED PH SU: ., - C,
2 HR
PH^p SU
2 HR
TEMP. OC
ANALYST
INITIAL
C..,.RECTED PH SU: id,'� -. t . Ii . � , (01cri
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
/)- e,
� 7, �"p ,li
* p
CORRECTED PH SU: j,;JJ k, _- c., 1
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
0.
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
r ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:UO3EO21 Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFERp
PH 10.0'/ SLI
BUFFER
PH 13.0 SU
BUFFER
INITIAL
6 kR �4%
.•� �' �
�Srl�j:�
"�a h_�l
� 3� i 4."-.'
��� • 4
G '�d �`3".
�'.,�"�"'��
� �'A°H p�_
�' .`!.,
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: �f R ` -
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
C,,, ERECTED PH SU: _r��).) -- ell, v- .Sb,
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
17 S' t'
CORRECTED PH SU: /,- o' -1 & 11 _ r .
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
I` ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:UO3EO21
Exp. Date:OCT. 2020
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
�J1Ccc
ls'oe
,4' �I 7c
r•j
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIMEa
DATE
TIME
INITIAL
PH SU
TEMP. °C
's
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
&—.-,RECTED PH SU: I.1. '? — ," ( d. &1'1 9
24 HR
PH
24 HR
TEMP.
ANALYST
INITIAL
�SU
sOC
CORRECTED PH SU: / ._ 6)_ P /J 1 "-t
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The -second pH reading is taken 2 hours after the initial reading.
H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EP.A ID: NC01119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E08421
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:UO3EO21 Exp. Date:OCT. 2020
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial *180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7:0 SU
BUFFER
PH 10.0 SU
BUFFER
PH® 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU: �..3 • r /,-
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
C�.,:RECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU
/3ti : - o , I t�,0-2-
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
ThQ second pH reading is taken 2 hours after the initial reading.
- )H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F— ^ ID: NC01119
I .,ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:UO3E021 Exp. Date:OCT. 2020
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
INITIAL
PH SU
TEMP. °C
)DATE
gTIME
CORRECTED PH SU: 6/1"6 n 41j>
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:.�
24 HR
SU
24 HR
TEMP. °C
ANALYST
INITIAL
KPH
t a
CORRECTED PH SU: ,,< >R ;. X.
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Tr second pH reading is taken 2 hours after the initial reading.
jH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
pH 10.01 Lot #:
pH 13.00 Lot #:UO3E021
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
5.
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
A
TIME
INITIAL
PH
TEMP. °C
{Ta/E
ySU
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: -') — 0 I ;' '— � .,2. i.
24 HR
24 HR
ANALYST
PH SU
TEMP. oC
INITIAL
CORRECTED PH SU: A'), �, 1' ,)l < /).X
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F -- ID: NCO1119
I•. .;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
PH 10.01 Lot #:
PH 13.00 Lot #:UO3E021
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2020
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
TIME
DAyy>>TE+$pyJ
TIME
INITIAL
PH SU
TEMP. oC
)DATE
CORRECTED PH SU: r':;i ` d S !>` 5
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
0. 3
993
CORRECTED PH SU:.>..0
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
i 14
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
PH readir.�s must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F'' ID: NCO1119
N certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot#:UO3EO21 Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PHA SU
TEMP. oC
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:�'
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: 1.1) - `' I ) -1 , ff li
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T' second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F—. ID: NCO1119
N certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot* Exp. Date:
pH 13.00 Lot#:UO3E021 Exp. Date:OCT. 2020
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. oC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
I
, .
CORRECTED PH SU: /'),. 5 — 6,1 /,).
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: 12,14 w- fia. >a 1 7 l') , I ci
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: ) i - % L 1
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
!
gg°C
L
I;�4
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T' second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F�-' ID: NC01119
K .;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:UO3E021 Exp. Date:OCT. 2020
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
)/
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: /� cl. `I' — .I 5 `(,.)..)
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: o k d;
24 H R
24 H R
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: id S
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
it iz'
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T' second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA_ ID: NC01119
P ertification #: 194
Instrument ID: ORION DualStar pHASE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot#:A8165 Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:UO3EO21 Exp. Date:OCT. 2020
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. OC OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU: t.' -,;) - a'' i `
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
C�— <RECTED PH SU: ) '-)' )- -- �„I 9 :,), 0) _,)-
�, �
I -,
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
CORRECTED PH SU: �' V< ` :7 '
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
CA
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
T H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FPq_ ID: NCO1119
I ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:UO3EO21
Exp. Date:OCT. 2020
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. C OF
QC
TEMP. oC OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
b;'jI
"'
Sri, 3C-
CORRECTED PH SU: ✓ L' ��-.��-. =>�.
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
C,-.<RECTED PH SU: [)-to — 0_)'�' -:�- !,), 9
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: . q -- 0, '-) � "' I A 1 ei
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Thf second pH reading is taken 2 hours after the initial reading.
H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 12/21/16

IJH MITER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F",- ID: NC01119
. ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:UO3EO21
Exp. Date:OCT. 2020
pH 13.00 Lot #: 971-7<21U
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SLI
BUFFER
PH 13.0 SU
BUFFER
INITIAL
L-d J.z`
K
(i�, �
�' >`t
"�
Hai
ft� a`4
¢ 0
0
qqq% v"
'
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
r
CORRECTED PH SU:
- a
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
G,jRRECTED PH SU: / "'I. ) 0. 0 9, 0, 51,�
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
i% 9,
CORRECTED PH SU: I �-6' - f : 0',� �"®
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FBI. ID: NCO1119
:ertification #: 194
• • ••••- .. '"LJ1w 1 wig rvR OU3 LIIVIC/JLUILIUL
SW-846-9040C
Instrument ID: ORION Dua(Star pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF,
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
'Vlh(i
. 6"
3
CORRECTED PH SU: 4(0 a t = if j- q S-
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
s-
CurtRECTED PH SU: �'•. ,�"
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
•r l�
y
8 � * a: J�..
B
� S
CORRECTED PH SU: ._ 0—) 1 '" 0, 3 j
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Thp.second pH reading is taken 2 hours after the initial reading,
,H of this second reading has to be above a pH of 12.
the pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F--". ID: NC01119
certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance: C. t�i( (,ff,��� �����z•�;��,
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
I
'
�'E`.
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
A
CORRECTED PH SU:'' Q- / _'
2 HR
PHj SU
2 HR
TEMP. oC
ANALYST
INITIAL
CORRECTED PH SU: / . 7 -- '' • � 1( " 0' 4
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 1 „••' w'• r' `'
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Tom, second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
E^" ID: NCO1119
N ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
`u's.
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU:•-'>
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
i-/7°(
PS
CORRECTED PH SU: f q o, j I - 19
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
TI—second pH reading is taken 2 hours after the initial reading.
dH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Er'^ ID: NCO1119
N artification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
pH 7.00 Lot #:A8165
CAL.
TEMP. °C OF
QC
TEMP. OC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU: �J �, - 0,'A X /e', f-� I
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
a'7
C
CVr<RECTED PH SU: 12,41
'— 0, J J 7 l lfl
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
�4
CORRECTED PH SU: , _ —C) -2 1 12i ?�i
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T"— second pH reading is taken 2 hours after the initial reading.
'jH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 603 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F"^ ID: NCO1119
I 'ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. OC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE,
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
D
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
��
.13�
CORRECTED PH SU:a
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
3q r
CORRECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: i .? :
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
`i,
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T�,-. second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EP-°- ID: NC01119
N 3rtification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. C OF
QC
TEMP. OC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
3333
i
i
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE,
TIME
DATE
TIME
INITIAL
PH SU
TEMP..�°C
9
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
4 ;
'Vt
�-
Cur<RECTED PH SU: 0- w �- — C ; � �,/, 12 U-
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
INITIAL
Ph
SU
Temp.
°C
9//TIME
0 i.) z.
J10
A V'S
ry)
(1S ( c
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Tl--second pH reading is taken 2 hours after the initial reading.
jH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Er-', ID: NCO1119
r ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
PH 10.01 Lot #:
PH 13.00 Lot #:Y27E016
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date: _
Exp. Date:OCT. 2021
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. OC OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
0..
COLLECT
DATE
COLLECT
TIME
ANALYSIS
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
DATE
CORRECTED PH SU:-
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
24 HR
SU
24 HR
TEMP.
ANALYST
INITIAL
PPH
1 2' ,
61 :
1C
CORRECTED PH SU: OR" '0 ° 1
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
sD
1} I•
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction' Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T1, second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
E'er° ID: NC01119
N ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. OC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
too
C)d
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: 1,9, : (, '.__. f", K 12, q tj
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 11141,^ L', I S, - 4, q .
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
ICj �ii
. dT`
I P I
iia• i
,/ 7 '&
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T1 second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
El— ID: NC01119
N. artification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
g .;
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
��}/ c5 Jg ��
�.. -..,�
.a� ����
1 .'�S�n
•�/- �•
y
® °'lam" y
CORRECTED PH SU:�-�,
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: i 2 , " 1 — C'1K ,._ 12)
24 HR
24 HR
ANALYST
PH SU
TEMP. oC
INITIAL
:,ORRECTED PH SU: 42, --o: "? ./),;..
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
'.orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
\ctual pH = Measured pH +/- the correction Factor.
Fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
Fhe pH of this initial reading has to be above a pH of 12.
F'--,-second pH reading is taken 2 hours after the initial reading.
,)H of this second reading has to be above a pH of 12.
Fhe pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EP-'- ID: NC01119
N artification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. C OF
QC
TEMP. C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
di
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
f'
CUr(RECTED PH SU: 1.� > , 1 -- o' t (�r —•y /2 .61
24 HR
24 HR
ANALYST
PH SU
TEMP. oC
INITIAL
i
CORRECTED PH SU: 13 1�0 '� e-1 Q a`� 6
Post Calibration Verification
INITIAL
Ph
SU
Temp.
°C
/TIMEj`
j110
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th-^second pH reading is taken 2 hours after the initial reading.
,)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Ems" ID: NC01119
N ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
DA/TE
SLOPE
EyyyI/nFF.
BUFFER
PH8^/7�.0 SU
PH 7.0 SU
BUFFER
BUFFER
PH 10(.0 SU
PH 10.0 SU
BUFFER
BUFFER
PH 13.0hSU
PH 13.0 SU
BUFFER
INITIAL
��'�<;' <'
(/TIME{j
`` ,•`�•.'"
�L y{.V
fiJ7 *�"
��','��C'++__
�V �9I
d �: U}`
1 �, 4
c:� �j
�C
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
r�
CORRECTED PH SU:� n' � 11'� �{
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
Uc
Cur<RECTED PH SU:'-
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
1-1--second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
fhe pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Ems-' ID: NC01119
N ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
10.0
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
Dy�A(1Ty�1E
TIME
INITIAL
PH
TEMP. o®C
J\Dyy§§A}]TE
�+}TIME
.�\
A...i
!
✓�SU.
" :
CORRECTED PH SU:.
2 HR
PH SU
2 HR
TEMP. OC
ANALYST
INITIAL
CORRECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 12,' '._ C`i) I 1, % t�
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
: orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
the initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
the pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
I',. ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
TI
PH 7.0
7.0 SU
PH 10.0 SU
PH� 13.0E SU
BUFFER
INITIAL
Jsl j f 1
{ME
%�
1EFF.
0 1 I e'L
% l
fBUU{FFER
: ' � r.,�"'
� � �%
gB�UFFER
�� t��
�.r�
�S t��_.�
r.:l
d
�
i
( D'
i o l'
17,
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE)
TIME
DATE
INITIAL
PH SU
TEMP. °C
1/ N
1TIME
..2
CORRECTED PH SU: ;> ..w__
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
C�t1RECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: 0- Ll -
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
-alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:.orrectio.°i factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
4ctual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
*H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

IJH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ERA ID: NC01119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:'l�tr';
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial * 180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
a
c;
.....-2
y
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
TIME
INITIAL
PH SU
TEMP. °C
DATE
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
G—, RECTED PH SU: � � :.� /, i r_ !'?
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
/7
CORRECTED PH SU: /')' ( - 6,.)/ = % z, :'a vi
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FpA ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
kqit'?
�-1 . - �
� h�.
A �
� � � �
y
( 41
13- 1 ��i
r� �
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORREC I-ED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
is
t a���C
P65•
(,.,RRECTED PH SU: ,,fit 1J, 3'0
24 HR
PH SU
24 HR
TE^MP. °C
ANALYST
INITIAL
lia
CORRECTED PH SU: /,'), � W 0, . a 4 /'1.3 G,
Post Calibration Verification
TIME
INITIAL
.Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FPA ID: NC01119
:ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
DATE
TIME
INITIAL
PH SU
TEMP. °C
�> �� i (l
jTIME )
\(1 , .} ,✓'
^n� 3I a i.�
.,A'�
?
dy' /a j
gp s
CORRECTED PH SU: 0, — O u f = /M
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
d,lo
IT `�"(
fa ;.
G.,r- RECTED PH SU: lj-(�) -- "),I � -7 1,9,
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
I `T, C
1.4 'r-
CORRECTED PH SU: 12 `> ' - 0. Z 1 % 11, ) j
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
1 ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FPA ID: NC01119
,'ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09:96
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot *A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. oC OF
QC
TEMP. oC OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
E
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP*. OC
j
14 r
J ,'
� ��
•,� "^ •
CORRECTED PH SU: 12-a, °" I �D/ ----29.1
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
u,jRRECTED PH SU: 1 (0 c it °u III I
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:af
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
I ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

FN Mt I tR GALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
pH 7.00 Lot #:A8165
CAL.
TEMP. oC OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: 0- la -- 6), /'�m /.. q t;
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
19,21
U—,-�RECTED PH SU: - 6
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: ��:. ��5
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
,alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
;,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPAID: NCO1119
i . ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
((
ll ppyyyy
1a
*Jr ,
L 16� �
A
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
®
CORRECTED PH SU: A'4 -
2 H R
2HR
ANALYST
PH SU
TEMP. °C
INITIAL
its—
eve 1 9-
'� .
C,.,,:RECTED PH SU: 1, -s-_ e, I� � : .'j
24 H R
24 H R
ANALYST
PH SU
TEMP.. °C
INITIAL
CORRECTED PH SU: 2 , `� 0 , ,Z - 12, T-1
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
15
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
1 lie pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NCO1119
R artification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. OC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
%)
Y9I�... pyi 9 ��
C Q !f�
%'�� (�
��i4 �.A
��e� / '",
V
$ 'rY
a./ {�•
...,} .a y.._.
3 �9 P17
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
SU
INITIAL
TEMP. °C
'...
yPH
9 a 6
i �, C
CORRECTED PH SU: 1'1, » C - 7 12 , 3 a)
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
1 ,�'"3(
(,�,<RECTED PH SU:,
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
47 ls"--
1'7,1 °C_
S .
CORRECTED PH SU: ./d,'5 " 0, Pi ✓ 2J 6
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
Tne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Fp4 ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot#:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SLl
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oCI
Ail
I S.,
I
)a 1.
CORRECTED PH SU: /:).ram .. 0, 0, = 0•q
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
G�rtRECTED PH SU:
24 HR
PH SU
24 HR
TEMP. OC
ANALYST
INITIAL
CORRECTED PH SU: a :5 ,— ') ; i �r zq. '-)
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12..
Tho second pH reading is taken 2 hours after the initial reading.
iH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Fr' -AID: NC01119
i ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot*
pH 10.01 Lot #:A8172
pH 10.01 Lot #:
pH 13.00 Lot #:Y27E016
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial *180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE.
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
=M-Ili
il' ; S -
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
N
.
, . / a
CORRECTED PH SU: /J V. 157y M"4
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: �; : --(c). rs�
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
y
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Tb-- second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FD-,.ID: NC01119
i ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: %-?. �6 �--Co rs ' ";' �
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
Cur1RECTED PH SU: p� Y.. 6I, ;5- ""-
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: /-) y '../ '- 1,;�""u
Post Cnlihration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
10'.:4a
f'j`),
io'-0
1 r`i')
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Tf— second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH Mt I tR CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Ep4 ID: NC01119
1 ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. OC OF
QC
TEMP. C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
EE��,.,
)��h,
� 0) }
6t� �ny
110,Q
i<is t
Ci 1
o P9
a
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIMEINITIAL
ANALYST
INITIAL
PH SU
INITIAL
TEMP. °C
I�I f
I'fn1
, I I
P a
42. &
i')d 6.
CORRECTED PH SU: 12�'y�;-
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
0, G
I'�®("
e- �;f
CurCRECTED PH SU: 0- G Q �T-- /-),0
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Thp second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Ws.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C '
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
I ;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. OC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
DATE
q
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
p
A' d �d
��Ja��p
�'
pq '
�^ d
� C_
1
/ C
,
CORRECTED PH SU: all '- 1:, 4)
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
Cam,<RECTED PH SU: _ _aa(I c IS :'0'q5-
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 1-2, 5— (9, N C I?, S 2-
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
rA
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The -second pH reading is taken 2 hours after the initial reading.
f H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
E-PA ID: NC01119
1 ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
911,10 _.(__ .
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
l ° )- ?
N ,�_
1 �? ,
0'? C-
CORRECTED PH SU: 12-
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
Cu.<RECTED PH SU: 0o .3 M- q '7
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
f ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
TIME
EFF.
PH 7.0 SU
BUFFER
PHg 10.0 SU
B[UF�F/ER
PH 13.0 SU
BUFFER
INITIAL
gD,A+�TE
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
Ea
-7, ol
CORRECTED PH SU: /),) ., r� 6 5- - /')'"5
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
7 f J " �"'
� ('
it .
CvrcRECTED PH SU: 1 _ � C.% �'> , 1.) ,4�
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Thp-second pH reading is taken 2 hours after the initial reading.
1 )H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

r1l mt I tK UALILSKATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot *A8165 Exp. Date:JUNE. 2020
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
Fp,A ID: NC01119 pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
'artification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
FITIME
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
EFF.
PH'*7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
JD/)ATE
1'� 0
Qf' �Ap
c
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU: 0' �- e), /q
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
l'J.3
CVr<RECTED PH SU: Q, I - ^:`,1 5 1. —
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: �r �,)• !l �'
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
{'?
t
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Ti- ,econd pH reading is taken 2 hours after the initial reading.
1 H of this second reading has to be above a pH of 12..
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

VN Mt I tK GAILIUKATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer serial #:180410124 Cal Due Date:10/2/2023
DATE
/r
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 7.0 SU
TEMP. oC OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
/0-
TEMP. oC OF
PH 10.0 SU
BUFFER
dam/� JA .' C C_ `
�^ �/
CAL
BUFFER
PH 13.0 SU
^ry 'q
TEMP. oC OF
PH 13.0 SU
BUFFER
INITIAL
dg
COLLECT
COLLECT
TIME
ANALYSIS
-DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
/DATE
N 1-
'
�'
CORRECTED PH SU12 , 3
2 HR
PH SU
2 HR
TEMP..oC
ANALYST
INITIAL
u�r<RECTED PH SU: 5 r 4)"
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
�c
14
CORRECTED PH SU: i2�� — 0,) ( 7 1 �. !
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T' second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12..
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FeA ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar PHASE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: /'� ` sI„C,," 1 `? ° o � j
2 HR
PH SU
2 HR
TEMP..oC
ANALYST
INITIAL
CVrtRECTED PH SU: 3 o' : P`-'- • �, Y
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
r,
CORRECTED PH SU: i'; -� � ��� o� ' 9
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
TI-econd pH reading is taken 2 hours after the initial reading.
1 ,H of this second reading has to be above a pH of 12..
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
7— A ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date: J U N E. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFERpL
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
DATE
TIME
INITIAL
PH SU
TEMP. oC
TIME
7
CORRECTED PH SU: __ �' f, �'', /� �✓.`
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
a'`
G v
s
Cur�RECTED PH SU: f 9, 3 1, 0: /9, j
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: --i <. ��'w, .;1i
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12..
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rM Mt I tK CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-FRA ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
PH 10.01 Lot*: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
DATE
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP.
PH 13.0 SU
BUFFER
INITIAL
�' �a
R�'e ," E
�.�1a
- '
!1q Ili,
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: V• i'C" d q � t'll
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
u,-.r<RECTED PH SU: I _ +^ �r� 3.6-
24 HR
PH/i) SU
24 HR
TE/)fM/qP. °C
ANALYST
INITIAL
CORRECTED PH SU: 12 '
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
r� F
3H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
fhe pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12,
Fhe pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

rM Mt I tK CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FPA ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
DATE
?r'p
TIME
CAL.
SLOPE BUFFER
EFF. PH 7.0 SU
��A9
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. oC OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIAL
�d.
-
i
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
COR ECTED PH SU: 12,
2 HR
PH SU
=TEMP..00
ANALYST
INITIAL
CVr<RECTED PH SU: �, _ ,�.I`i 60•_��" '
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
3`
:,ORRECTED PH SU: /')- � _ 0 , I � _ 0. 1
Post Calibration Verification
INITIAL
Ph
10 SU
Temp.
°C0
)TIME
-all
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
;orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade),
kctual pH = Measured pH +/- the correction Factor.
'he initial pH reading is taken after the lime is mixed with the 503 sludge.
'he pH of this initial reading has to be above a pH of 12.
" second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5
)ocument changes in lot #'s.
revised: 12/21 /16

rrl mt I tR UALIbRAT1UN FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F'14 ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
DATE
TIME
SLOPE
Ep{FF.
CAL.
BUFFER
PH7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIAL
ad
W
1' ,Y\ ; `i
4.+ iN
.*. P�'��.
�`SJ
.87:("o
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU: CM' .' 0--3 j,
E2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
p
CurtRECTED PH SU: q_
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
Jc
.
CORRECTED PH SU: i4), i -= Qi' erg
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
-orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
Fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
Fhe pH of this initial reading has to be above a pH of 12.
r' second pH reading is taken 2 hours after the initial reading.
I )H of this second reading has to be above a pH of 12,
fhe pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-gn4n(-.
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F�a ID: NCO1119
;ertification #: 194
I,;-irument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:DUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
DATE TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
24
�'
e
F' i C
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
/
CORRECTED PH SU:
2 HR
PHq/ SggU
2 HR
TEMP..°C
ANALYST
INITIAL
C` ,RECTED PH SU: _j,..) -? . 0,: u 5._ - /) "
ESUTEMP.
E
24 HR
°C
ANALYST
INITIAL
CORRECTED PH SU: - z-/. 61, K-'— 42., )z
Post Calihration Varifirn inn
TIME
INITIAL
Ph
10 SU
Temp.
°C
CAL TEMP. °C OF
BUFFER PH 13.0 SU
PH 13.0 SU BUFFER
INITIAL
34
0
DH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
Fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
f he pH of this initial reading has to be above a pH of 12.
,econd pH reading is taken 2 hours after the initial reading.
ri of this second reading has to be above a pH of 12.
-he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot Vs.
revised: 12/21 /16

„-IoXAI 1UN t-UH 503 LIME/SLUDGE
T SW-846-9040C
own of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F"\ ID: NC01119
:ertification #: 194
i,,,nment ID. ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot*.
Exp. Date:
PH 13.00 Lot AME016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. �C OF
CAL
SLOPE
DATE TIME EFF,
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
F' � �.
a `b
COLLECT:CO4CTNALYSISANALYSIS
DA(gTEpdDATE
f B Id 1:1.��
�
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: /�). 6, t:'7 6' -- /,), 4[,2
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
„ Tic
P<1
RECTED PH SU: 1 7 /fit 49
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: ✓'2-( •-&I g ' 0. it
Post Calibration Verifiratinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
TEMP. "C OF
PH 13.0 SU
BUFFER INITIAL
S e.c7 �- S
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T'-=-second pH reading is taken 2 hours after the initial reading.
H of this second reading has to be above a pH of 12,
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

ff" Mt I tR CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
E^' ID: NC01119
,ertification #: 194
j,._,rument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
SLOPE
DATE TIME EFF.
PH 7.00 Lot #:A8165
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2�20
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
BUFFER
PH 7.0 SU
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
TEMP. " C OF
CAL
TEMP. °C OF
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
^
's
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
8
ip
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP..oC
ANALYST
INITIAL
G_ .RECTED PH SU: l: _(�j °_ r., () _, (�- �-j Uz
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
CORRECTED PH SU:
Post Calihrntinn \/arifirratinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
"C_d
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,'orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
kctual pH = Measured pH +/- the correction Factor.
-he initial pH reading is taken after the lime is mixed with the 503 sludge.
he pH of this initial reading has to be above a pH of 12.
-second pH reading is taken 2 hours after the initial reading.
H of this second reading has to be above a pH of 12,
-he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-84(!-An4nr'.
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F17'11 ID: NC01119
;ertification #: 194
i—trument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:DUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date. --
Checked with Traceable Thermometer Serial *180410124 Cal Due Date:10/2/2023
CAL. TEMP. °C OF
QC
TEMP. °C OF
SLOPE
BUFFER PH 7.0 SU
BUFFER
PH 10.0 SU
DATE TIME EFF.
PH 7.0 SU BUFFER
PH 10.0 SU
BUFFER7,0
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU: JJ 0 . 0,a I <� --- /.), q2
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
C... ,RECTED PH SU: 0"' )v'
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: ) l 3 µ $ 9 T � /.). I <)
Post Calibration Verific:atinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
CAL
TEMP. °C OF
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFFER
INITIAL
13, co
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
;orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
\ctual pH = Measured pH +/- the correction Factor.
'he initial pH reading is taken after the lime is mixed with the 503 sludge.
he pH of this initial reading has to be above a pH of 12.
- second pH reading is taken 2 hours after the initial reading.
rl of this second reading has to be above a pH of 12.
-he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F1_1\ ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance: (� i , ,, „ `t
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF CAL
TEMP. °C OF
SLOPE BUFFER
DATE TIME EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU BUFFER
PH 13.0 SU
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER PH 13.0 SU
BUFFER
INITIAL
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
HCOLLECT
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
J 117 ' , C
CORRECTED PH SU: 13, -- C 6 L 014
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
(_..-<RECTED PH SU:
24 H R
PH SU
24 H R
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 1;.), f� 01,�. L
Post Calibration VPrifinntinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
;orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
\ctual pH = Measured pH +/- the correction Factor.
-he initial pH reading is taken after the lime is mixed with the 503 sludge.
he pH of this initial reading has to be above a pH of 12.
-second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
'he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 12/21 /16

rrt Mt rER CALIBRATION FOR 503 LIME/SLUDGE
SW-84n-gn4nr.
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F�I ID: NCO1119
;ertification #: 194
i,—Lrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date-JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:,: v2/2023
CAL.
TEMP. °C OF
QC
SLOPE BUFFER
PH 7.0 SU
BUFFER
DATE
TIME
EFF. PH 7.0 SU
BUFFER
PH 10.0 SU
TEMP. "C OF
CAL
PH 10.0 SU
BUFFER
BUFFER
PH 13.0 SU
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATEME
;COLLECT
DATE
TIME
INITIAL
PH SU
TEMP. °C
r
i I
reX61
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
/ ,% . ({
X i
(....RECTED PH SU:
ffPHSU
MTIEMP.
ALYST
;INITIAL
CORRECTED PH SU: _J'J, q -y, II A)
Calibration VPrifiratinn
Ph
Temp.
10 SU
°C
LT!MEJ1NITIAL
TEMP. "C OF
PH 13.0 SU
BUFFER INITIAL
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
kctual pH = Measured pH +/- the correction Factor.
'he initial pH reading is taken after the lime is mixed with the 503 sludge.
'he pH of this initial reading has to be above a pH of 12.
-econd pH reading is taken 2 hours after the initial reading.
r-I of this second reading has to be above a pH of 12.
'he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
>ocument changes in lot #'s.
revised: 12/21/16

rn Mt i the CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Fr'a ID: NC01119
:ertification #: 194
.„.trument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
DATE
'IS
TIME
11
SLOPE
EFF.
{ , r
CAL.
BUFFER
PH 7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
�_
QC
BUFFER
PH 10.0 SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
I��'�
f,° : �..��
�.���gf1P °Q
�i' •, C� 1�a
�� �•
�rica d
� �> �J �C-
CORRECTED PH SU: /s., 1
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
C _. , tRECTED PH SU: . 01 IS -.an. / 1.lj...5
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
d
;`�l
CORRECTED PH SU:
Post Calibration Verification
TIME
INIITIAL
Ph
1]0 SU
Temp.
°C
le ^. J
iI Y
9 , I
\ x o..
:)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
: orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
the initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
F'- second pH reading is taken 2 hours after the initial reading.
I )H of this second reading has to be above a pH of 12:
Fhe pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F1A ID: NCO1119
;ertification #: 194
lijocrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2020
pH 7.00 Lot #: Exp. Date:
PH 10.01 Lot#:A8172 Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
PH 7.00 Lot #:A8165
DATE
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SLI
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °T
PH 13.
BUFFi'TAL
u
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
6/
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
G�.,RECTED PH SU:
HSTEEMP.
EPH
24 HR
°C
ANALYST
INITIAL
CORRECTED PH SU: ? f-'. � I ij. s
Post Calibration Verification
Ph
Temp.
TIME
IN
10 SU
°C
N
o
10.E
ICi K.'
.I<,
DH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
,alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
r, _,econd pH reading is taken 2 hours after the initial reading.
i ,H of this second reading has to be above a pH of 12.
fhe pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
T SW-846-9040C
own of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Fes'+ ID: NCO1119
;ertification #: 194
Iliotrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
SLOPE
DATE gTIME p EFF.
CI
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date: JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date: OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date: 3
CAL. TEMP. °C OF QC
BUFFER PH 7.0 SU BUFFER
PH 7.0 SU BUFFER PH 10.0 SU
-/A 0'- i', '( "(' I I(", o
TEMP. C OF
CAL
TEMP. °C OF
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
IT"`i
COLLECT
DATE
COLLECT ANALYSIS ANALYSIS
TIME DATE TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP..°C
INITIAL
r /
,r�ECTED PH SU: r
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: ;' ', I 1,"), 2 1-1
Post Calibration Verification
TIME INITIAL
Ph
10 SU
Temp.
°C
H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
ctual pH = Measured pH +/- the correction Factor.
he initial pH reading is taken after the lime is mixed with the 503 sludge.
he pH of this initial reading has to be above a pH of 12.
cond pH reading is taken 2 hours after the initial reading.
A of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
ocument changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Fri ID: NCO1119
;ertification #: 194
il,,,Lrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
SLOPE
DATE /TIME EFF.
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL. TEMP. °C OF QC
BUFFER PH 7.0 SU BUFFER
PH 7.0 SU BUFFER PH 10.0 SU
TEMP. " C OF CAL
PH 10.0 SU BUFFER
BUFFER I PH 13.0 SU
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATES
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP..°C
INITIAL
i
C._ .,lECTED PH SU: �.. ; '� (Sr,
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
3ORRECTED PH SU:
Post Calihratinn Varifiratinn
TIME
INITIAL
Ph
SU
Temp.
°C
I10
a 3 ..
B3(r(c
TEMP. "C OF
PH 13.0 SU
BUFFER I INiTIAL
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
'he initial pH reading is taken after the lime is mixed with the 503 sludge.
'he pH of this initial reading has to be above a pH of 12.
cond pH reading is taken 2 hours after the initial reading.
„i of this second reading has to be above a pH of 12.
"he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
>ocument changes in lot #'s.
revised: 12/21/16

' 1 11v11_- 1 cK I-HLIUKATION FOR 503 LIME/SLUDGE
SW84
Town -
of Waynesville WWTP 6-9040C
566 Walnut Trail
Waynesville, NC 28785
E^ ID: NC01119
:ertification #: 194
I+,,irument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
DATE
COLLECT
DATE
I SLOPE
TIME EFF.
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot#:A8172 Exp. Date:DUNE. 201g
pH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date: OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due -Date: 10/2/2023
CAL. TEMP. °C OF[PH
QC
BUFFER PH 7.0 SUUFFER
PH 7.0 SU BUFFER 10.0 SU
. ,co I )0. Lill
COLLECT I ANALYSIS I ANALYSIS
TIME DATE TIME
CORRECTED PH SU: i-'Z u, "o,-I ) _' o_46
0
TEMP. " C OF
PH 10.0 SU
CAL
BUFFER
TEMqFFERI
PH
BUFFER
PH 13.0 SU
BUITIAL
ANALYST INITIAL INITIAL
INITIAL PH SU I TEMP. °C
2 HR 2 HR ANALYST
PH SUjTEMP..oC INITIAL
�� -�
G,.,+�ECTED PH SU:
24 HR 24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
(ej Ll
Post Calibration Verification
Ph Temp.
TIME INITIAL 10 SU °C
Q.�.,
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,orrection factor (CF) = 0.03 pH units k (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
-he initial pH reading is taken after the lime is mixed with the 503 sludge.
he pH of this initial reading has to be above a pH of 12.
pond pH reading is taken 2 hours after the initial reading.
+1 of this second reading has to be above a pH of 12.
-he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 12/21/16

1-N MITER CALIBRATION FOR 503 LIME/SLUDGE
T SW-846-9040C
own of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FD,q ID: NC01119
;ertification #: 194
li„rrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date: JUNE. 201_-_9
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date: OCT.
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
SLOPE
CAL.
BUFFER
TEMP. °C OF
PH 7.0 SU
QC
BUFFER
TEMP. °C OF
CAL
TEMP. °C OF
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
PH 10.0 SU
BUFFER
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFFER IN
n
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
TIME
TM E
INITIAL
PHL SU
TEMP. °C
i,DATE
)
t_ � i (('f
�I �l
�... e ,�,1 �'J�
6'DATE
CORRECTED
PH SU:
2 HR 2 HR ANALYST
PH SU TEMP..°C INITIAL
C, .,RECTED PH SU:
24 HR ANALYST
ff
TEMP. °C
INITIAL
3ORRECTED PH SU:
Post Calibration Verification
Ph Temp.
TIME INITIAL 10 SU °C
,H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
ctual pH = Measured pH +/- the correction Factor.
he initial pH reading is taken after the lime is mixed with the 503 sludge.
he -oH of this initial reading has to be above a pH of 12.
:cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
ocument changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F11A ID: NCO1119
;ertification #: 194
li-,,crument ID: ORION DualStar pH/ISE Benchtop
S/N: E09696
In Lab
Equipment Maintenance: e g
PH 7.00 Lot #:A8165
Exp. Date.JUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot#:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date: OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial *180410124 Cal Due Date:10/2/2023
CAL.
SLOPE BUFFER
TEMP. °C OF
PH 7.0 SU
QC
BUFFER
TEMP. °C OF
PH 10.0 SU
CAL
BUFFER
TEMP. °C OF
DATE TIME EFF. PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFFER
5-47ife 97
s
COLLECT I
DATE
COLLECT I
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
17/
UUHHECTED PH SU: I>j- � M 0, a S- �= /' „ .3'5__
2 HR
PH SU
2 HR
TEMP..°C
ANALYST
INITIAL
RECTED PH SU: o" ,5
24 HR
MPH SU
24 HR
TEMP. °C
ANALYST
INITIAL
P r.➢
,ORRECTED PH SU:
Post Calibration VPrifiratinn
INITIAL
Temp.TIME
°C
EP
yp �y-yA
U 4 3q �Y...
H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
ctual pH = Measured pH +/- the correction Factor.
he initial pH reading is taken after the lime is mixed with the 503 sludge.
he pH of this initial reading has to be above a pH of 12.
cond pH reading is taken 2 hours after the initial reading.
,rl of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
ocument changes in lot #'s.
INITIAL
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-84F-anan(,
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F"\ ID: NC01119
;ertification #: 194
Inc,irument ID: ORION DualStar pH/ISE Benchtop
S/N: E09696
In Lab
Equipment Maintenance:
SLOPE
DATE TIME EFF.
PH 7.00 Lot #:A8165
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2v20
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:1012/2023
CAL. TEMP. "C OF QC
BUFFER
PH 7.0 SU
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
7'4
`9
TEMP. "C OF CAL TEMP. °C OF
PH 10.0 SU BUFFER PH 13.0 SU
BUFFER PH 13.0 SU BUFFER INiTIAL
XCOLLECT
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: �:?. , A fS'-zi %I
2 HR
H,+ SU
2 HR
TEMP..°C
ANALYST
,INITIAL
C,,.RECTED PH SU: f' ,`% ;: 1'2_ 7— / �', �' ;
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 12, 6
Post Calibration Verifiration
TIME
INITIAL
Ph
10 SU
Temp.
°C
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
-he initial pH reading is taken after the lime is mixed with the 503 sludge.
he -pH of this initial reading has to be above a pH of 12.
�cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12:
-he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 12/21 /16

r'M mt I ER CALIBRATION FOR 503 LIME/SLUDGE
Town of W SW-846-9040C
aynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ID: NC01119
:ertification #: 194
ln�(rument ID: ORION DualStar pH/ISE Benchtop
S/N: E09696
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
PH 7. 0 Lot Exp. Date:
10.
PH 10.01 Lott #:A8172 ExpDate: JUNE. 2019
PH 10.01 Lot*: . Exp. Date: _^
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Dat 3
CAL.
TEMP. °C OFRQq—TEMP.'COF
DATE
TIME
SLOPE
EFF.
BUFFER
PH 7.0 SU
PH 10.0 SU
PH 7.0 SU
BUFFER
P
BUFFER
1
:.o.
COLLECT
COLLECT3777
INITIAL
DATE
TIME
TEMP. °C
If
CORRECTED PH SU: j- t. t� �.3, d�g j� q "
2 HR 2 HR ANALYST
PH SU
TEMP..°C
INITIAL
C-.,RECTED PH SU:
24 HR 24 HR ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
1 10, fit,
Post Calibration Verification
Ph Temp.
TIME INITIAL 10 SU °C
CAL TEMP. °C OF
BUFFER PH 13.0 SU
PH 13.0 SU BUFFER INITIAL
1H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
,ctual pH = Measured pH +/- the correction Factor.
he initial pH reading is taken after the lime is mixed with the 503 sludge.
h nH of this initial reading has to be above a pH of 12.
�cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
ocument changes in lot Vs.
revised: 12/21/16

rn Mt I ER CALIBRATION FOR 503 LIME/SLUDGE
Tow f SW-846-9040C
n o Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FP 11 ID: NC01119
;ertification #: 194
ii,ocrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165 Exp. Date.-JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date: JUNE. 2019
pH 10.01 Lot #: Exp. Date: _
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
DATE
TIME
SLOPE
EFF.
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
).' i�'`3
CORRECTED PH SU: /d 6 C)..® -� -Li S
2 HR 2 HR ANALYST
PH SU TEMP..°C INITIAL
C,`,,RECTED PH SU: L2,k�_P,e di --19, �;d
24 HR
PH SU
24 HR
TEMP. °C
�I I.
Tel
�ORRECTED PH SU:
j,), �,
� C: 4 y ii- ,- ;;,, l `
Post Calibration Verifiratinn
Ph
Temp.
TIME
INITIAL 10 SU
°C
/61., 'S
,fn
(I` �" /V,�
a a� 6c
CID_
CAL TEMP. °C OF
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFFER INITIAL
1H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
,ctual pH = Measured pH +/- the correction Factor.
he initial pH reading is taken after the lime is mixed with the 503 sludge.
h- )H of this initial reading has to be above a pH of 12.
�cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
ocument changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
To f SW-846-9040C
wn o Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ID: NC01119
,'ertification #: 194
Ii,,crument ID: ORION DualStar pH/ISE Benchtop
S/N: E09696
In Lab
Equipment Maintenance:
PH 7.00 Lot#:A8165 Exp. Date.JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot#:A8172 Exp. Date:JUNE. 2p19
PH 10.01 Lot #: Exp. Date: pH 13.00 Lot #:Y27E016 Exp. Date: OCT. 202- ___1
PH 13.00 Lot #:
Date- Checked with Traceable Thermometer Serial #:1804101124Cal Due Dat 3
SLOPE
CAL.
BUFFER
TEMP. oC OF
PH 7.0 SU
QC
TEMP. °C OF
CAL
TEMP. oC OF
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER INiTIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
f,
J
".X� (/
;'�
®pn pe)
j
i ('off,
CORRECTED PH SU: d')., 6),/, -:� /"J, ,;
2 HR 2 HR ANALYST
PH SU
TEMP..°C
INITIAL
+•
G,.,RECTED PH SU:
, ��
, , . 11
M
24 H RANALYSTTEMP. °C INITIAL
CORRECTED PH SU: p J).,` 1e
Post Calibration Verificatinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
,q
kl
2 3 rj �
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
he initial pH reading is taken after the lime is mixed with the 503 sludge.
nH of this initial reading has to be above a pH of 12.
�cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
locument changes in lot #'s.
revised: 12/21/16

rH METER CALIBRATION FOR 503 LIME/SLUDGE
Town o f W SW-846-9040C
aynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ID: NC01119
;ertification #: 194
li„(rument ID: ORION DualStar pH/ISE Benchtop
S/N:E00696
In Lab
Equipment Maintenance:
DATE
COLLECT
DATE
ii
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date: _
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 20 12
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Dat 3
CAL.
TEMP. °C OF
QC
TEMP. °C OF
SLOPE BUFFER
TIME
PH 7.0 SU
BUFFER
PH 10.0 SU
EFF. PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
:G N �. ,w
)i
COLLECT ANALYSIS ANALYSIS ANALYST
TIME DATE TIME INITIAL
CORRECTED PH SU: 41. . 011. W [ )41�
2HR 2HR ANALYST
PH SU TEMP..°C INITIAL
62
C-.,RECTED PH SU:
24 HR 24 HR ANALYST
PH SU TEMP. °C INITIAL
Y I C
3ORRECTED PH SU:
Post Calibration Verification
Ph Temp.
TIME INITIAL 10 SU °C
jt."C.1t., �� . I' 'n,e"c,
INITIAL I INITIAL
PH SU TEMP. °C
/ 11 , ( ), I . I I'c'
CAL TEMP. °C OF
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFF/ER INITIAL
�H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
,ctual pH = Measured pH +/- the correction Factor.
he initial pH reading is taken after the lime is mixed with the 503 sludge.
h" -H of this initial reading has to be above a pH of 12.
:cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
ocument changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
T SW-846-9040C
own of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ID: NC01119
;ertification #: 194
hj3irument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot#:A8165 Exp. Date.JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot#:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:Y27E016 Exp. Date: OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
OFSLOPE
BUFFER
DATE TIME
PH7.0SU
BUFFER
0 SU
EFF. PH 7.0 SU
BUFFER
PH 10.0 SUER
F[TTEEMiP.0
q
COLLECT COLLECT ANALYSIS
DATE TIME DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
cd ev
CORRECTED PH SU:
EHR
2 HR
TEMP..°C
ANALYST
INITIAL
1
C,`,,RECTED PH SU: Q3.7- Yt, C, af1a
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verifinatinn
TIME
INITIAL
Ph
10 SU
Temp,
°C
/t',3
r.
�`0 , d;
CAL TEMP. °C OF
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFFER INITIAL
j.
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
;orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
'he initial pH reading is taken after the lime is mixed with the 503 sludge.
'h - -,H of this initial reading has to be above a pH of 12.
,cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
-he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
locument changes in lot #'s.
revised: 12/21/16

rh not I I:R CALIBRATION FOR 503 LIME/SLUDGE
T SW-846-9040C
own of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ID: NCO 1119
;ertification #: 194
li„crument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2p2p
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot#:A8172 Exp. Date: JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date: OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due -Date: 3
CAL.
TEMP. °C OF
QC
TEMP C OF
SLOPE BUFFER
DATE TIME EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
a
COLLECT COLLECT ANALYSIS ANALYSIS ANALYST
DATE TIME DATE TIME INITIAL
CORRECTED PH SU: /� , bI j' 7, x/1
i2HR
TEMP..°C
ANALYST
INITIAL
a1 11
` f/
;� _
C-.,RECTED PH SU: __19:( c)<G'j. "j- , gi)
a
LYST
TIAL
m
CORRECTED PH SU:
Post Calibration Verificatinn
TIME
INITIAL
Ph
10 SU
TempL.
°C
INITIAL
INITIAL
PH SU
TEMP. oC
CAL TEMP. °C OF
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFFER INITIAL
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
\ctual pH = Measured pH +/- the correction Factor.
-he initial pH reading is taken after the lime is mixed with the 503 sludge.
h, ,H of this initial reading has to be above a pH of 12.
�cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
-he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised:12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
T SW-846-9040C
own of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
rn.q ID: NC01119
;ertification #: 194
Ino(rument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date.JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot#:A8172 Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEM17+OC
TEMP. CP ° OF
SLOPE BUFFER
TIME EFF.
PH
FFER
PH 10.0 SUDATE
PH 7.0 SU
BU
10.0 SU
BUFFER
F %
COLLECT
COLLECT ANALYSIS ANALYSIS
ANALYST INITIAL
INITIAL
DATpyE
TIME DATE TIMEy
INITIAL SU
TEMP. °C
gP7H
UUNNLU I LD PH SU: /,). ( z); 4' s
ff
PHSU ETEMP-OC
INITIAL
C,-.,RECTED PH SU: 0, 1�
R4HM4HANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verifirntinn
TIME
Ph
INITIAL 10 SU
Temp.
°C
a
CAL TEM.00
OF
BUFFER PH0 SU
PH 13.0 SU BUFFER INITIAL
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
-he initial pH reading is taken after the lime is mixed with the 503 sludge.
h-.,H of this initial reading has to be above a pH of 12.
:cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
'he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Iocument changes in lot Vs.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
T SW-846-9040C
own of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
r n ID: NC01119
;ertification #: 194
iijocrument ID.- ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot#:A8172 Exp. Date:JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due -Date: 3
CAL.
TEMP. °C OF
QC
SLOPE
BUFFER
PH 7.0 SU
BUFFER
DATE TIME EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
TEMP. " C OF CAL TEMP. °C OF
PH 10.0 SU BUFFER PH 13.0 SU
BUFFER PH 13.0 SU BUFFER INITIAL
COLLECTI
DATE
COLLECT
TIME
I ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
U U K H E C I ED PH SU: 1, ; , r.
2 HRFR
ANALYST
PH SU..°C
INITIAL
C`.,RECTED PH SU.-
/ ?; gip'. / .°" /,>,
TMANALYST
INITIAL
CORRECTED PH SU:
v
Post Calibration Verifiratinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
;orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
\ctual pH = Measured pH +/- the correction Factor.
'he initial pH reading is taken after the lime is mixed with the 503 sludge.
h H of this initial reading has to be above a pH of 12.
:cond pH reading is taken 2 hours after the initial reading.
H of this second reading has to be above a pH of 12,
'he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
To f SW-846-9040C
wn o Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FP ID: NC01119
,ertification #: 194
Inocrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date: JUNE. 2019
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
SLOPE
CAL.
BUFFER
TEMP. °C OF
PH 7.0 SU
QC
TEMP. °C OF
CAL
TEMP. °C OF
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER INITIAL
s
�I` .? �
��y�o �tj
�
:�1�
9 J•. {","l'z.3
oti.f' e ��.,.�_ �,) �-'
COLLECT
COLLECTZMEM7AL
IAL
INITIAL
DATE
TIMEU
TEMP. oC
s
CORRECTED PH SU: �, d r), r 2
2 HR 2 HR ANALYST
PH SU
TEMP..°C
!IINITIAL
C_.,RECTED PH SU:
24 H R
24 H R ANALYST
PH SU
TEMP. °C INITIAL
CORRECTED PH SU: _ /2DI._ y fg :),i
Post Calibration Verification
Ph Temp.
TIME INITIAL 10 SU °C
co � b
� '? Q: h6E.t �p• (
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
'he initial pH reading is taken after the lime is mixed with the 503 sludge.
'h---H of this initial reading has to be above a pH of 12.
:cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
locument changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
T SW-846-9040C
own of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Fr'' ID: NC01119
;ertification #: 194
I11c)(rument ID: ORION DualStar pH/ISE Benchtop
S/N: E09696
In Lab
Equipment Maintenance:
CAL. ITEMP. °C O
SLOPE
BUFFER
PH 7.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
DATE
TIME
DATE
TIME
INITIAL
CORRECTED PH SU:
ANALYST
T J!R
..oC INITIAL
G,,,RECTED PH SU:
24 HR 24 HR
PH SU TEMP. °C
ANALYST
INITIAL
en
:�ORRECTED PH SU:,.z�
Post Calibration Verifirntinn
TIME
INITIAL
T9�,,
4,'�
EP
,d
PH 7.00 Lot #:A8165 Exp. Date.JUNE. 2020
PH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date: JLINE. 20 99
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
PH 13.00 Lot*: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due -Date: 3
QC TEMP. oC OF
BUFFER PH 10.0 SU
PH 10.0 SU BUFFER
INITIAL I INITIAL
PH SU TEMP. °C
d, 3 'c
CAL TEMP. °C OF
BUFFER
PH 13.0 SU
:1NIAL
PH 13.0 SU
BUFFER
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
,ctual pH = Measured pH +/- the correction Factor.
he initial pH reading is taken after the lime is mixed with the 503 sludge.
h---H of this initial reading has to be above a pH of 12.
,cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
locument changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
T SW-846-9040C
own of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ID: NC01119
;ertification #: 194
hiocrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09696
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165 Exp. Date.JUNE, 2020
PH 7.00 Lot #: Exp. Date:
PH 10.01 Lot #:A8172 Exp. Date:JUNE. 20 99
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:Y27E016 Exp. Date: OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due —Date: 3
CAL.
TEMP. °C OF
QC
TEMP. °C OF
DATE
TIME
SLOPE
EFF.
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
ter
:1
7 "
COLLECT
COLLECT
ANALYSIS
ANALYSIS
TIME
DATE
TIME
'yD{jAT/JE
=INITIAL
CORRECTED PH SU:
_ �, �-, I�.:'/). V
2 HR 2 HR ANALYST
PH SU TEMP..00 INITIAL
C-.,RECTED PH SU: 0_7 —0,, I r / SJ,
24 H R 24 H R ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calibration Verification
7��c
aIHE.,�
CAL TEMP. °C OF
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFFER INITIAL
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade, At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
'he initial pH reading is taken after the lime is mixed with the 503 sludge.
*h,-- H of this initial reading has to be above a pH of 12.
;cond pH reading is taken 2 hours after the initial reading.
,H of this second reading has to be above a pH of 12,
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
locument changes in lot #'s.
revised: 12/21/16

PH Mt I tK CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
I` ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SLl
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
a1
CORRECTED PH SU: 1,), ,3 ,._ ex,,) Q�2 Q
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
A]
Y �y9
2 2,5
/l1
C�-.RECTED PH SU: 12,1 — 0 -n 6
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: /,21'— 0" t12- �7 (2, 1
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
lei,
)
/tat
I� ,1
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
1 H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
N ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09696
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: P , j '6i09 '= 12.. y
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
g2,7
CVO-RECTED PH SU:�¢-
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Thp second pH reading is taken 2 hours after the initial reading.
l ,H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH Mt I ER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Epp, ID: NCO1119
N ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
PH 7.00 Lot #:
PH 10.01 Lot #:A8172
PH 10.01 Lot #:
PH 13.00 Lot #:Y27E016
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2021
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial M 180410124 Cal Due Date:10/2/2023
CAL.
TEMP. C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SLI
BUFFER
PH 13.0 SU
BUFFER
INITIAL
e 11cibi
14�r ..li/
�
r
T/.�t�y^m�
Y
4 VtI
� G Y...I
P. S.
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
a
CORRECTED PH SU: 1 (0 -. C' el 9 (;2, fs-�
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
Cur<RECTED PH SU: d .. P - 6) o .- 1';q
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
G 5 e 4.
,
CORRECTED PH SU: jj, t m 1)�qr
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Tory second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
E^- ID: NC01119
N ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:A8172
pH 10.01 Lot #:
pH 13.00 Lot #:Y27E016
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:JUNE. 2019
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. oC OF
QC
TEMP. °C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
Jd\.
l e%
tX
1-1
'oV
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PHr� SU
TEMP. oC
CORRECTED PH SU: �,, � a .rc
2 HR
PHSUTEMP.
2 HR
°C
ANALYST
INITIAL
V Y
i^1;�. , (
n
CORRECTED PH SU: �, `� C' V3 ;
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: i -6 -C� , j J ; 19 -i6
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10. SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th—secondpH reading is taken 2 hours after the initial reading.
dH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FP-4 ID: NC01119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
pH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
^7
/
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU: 1-9,� - 't),oC', ..- 0, 1
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
C
P5-
CCiHRECTED PH SU: -Q • C
24 HR
24 HR
ANALYST
PH SU
TE/jMP./°C
INITIAL
CORRECTED PH SU: 11, 6 "- e, (1- 2 s y
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
m'"fo I
V3, 1
(3, 1
j.3
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T�--- second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FP4 ID: NC01119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
PH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot. #:Y27E016
Exp. Date:OCT. 2021
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. oC
INITIAL
_ a'
Wr
CORRECTED PH SU: Ja) � -� - 6, 0. (:f) - t 6 q
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: IQ. � - 0. ) 'i /'-)." x j
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th second pH reading is taken 2 hours after the initial reading.
.)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

SW-846-9040G
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NCO1119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. oC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
}
6; t �i 1�Y�
' `���'
Jd
7_.ib
�7•.ro
/c'y��
.;"Z�r3
E3
,/``,L-, C
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
o�
r,1''>
CORRECTED PH SU: Al - i- al,-o , - L2- 9"
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
GuHRECTED PH SU:
24 HR
PH SU
24 HR^
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: j,), q V- C7 /2 S �
Post Calibration Verifiratinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th second pH reading is taken 2 hours after the initial reading.
dH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

SW-846-9040C ._.�_..��..
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
GJ24 ID: NC01119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A8165
Exp. Date:JUNE. 2020
pH 7.00 Lot #:
Exp. Date:
PH 10.01 Lot #:A8172
Exp. Date:JUNE. 2019
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:Y27E016
Exp. Date:OCT. 2021
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. oC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP.'C
��� � �
'' iN�
� .•� dui
� . � �
®-�
�'� ��
,�,� : � 0...---
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
)k
'PZ,
f'j�7
CCRRECTED PH SU: 1 `4' (e, 0 'o � `: / "�,
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
CORRECTED PH SU: jai.,_"�,�,
Post Calihratinn VPrificatinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T`- second pH reading is taken 2 hours after the initial reading.
dH of this second reading has to be above a pH of 12.
The pH c the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FP4 ID: NCO1119 e�
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date.-JUNE. 2020
pH 7.00 Lot #: Exp. Date:
pH 10.01 Lot #:A8172 Exp. Date:JUNE. 2019
pH 10.01 Lot #: C. N Exp. Date: IV
pH 13.00 Lot #:Y27E016 Exp. Date:OCT. 2021
pH 13.00 Lot #: ') ) �t't, Jl do Exp. Date: d; !, ;k� )- i
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
pH 7.00 Lot #:A8165
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
OLLECTANALYSIS
FTIME
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: / 2. ` -0 , f,� , L Q. Y 7
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
_
CORRECTED PH SU: °=-a �
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
TIME
TIITIAL
Ph
10 SU
Temp.
°C
nH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
-alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Nctual pH = Measured pH +/- the correction Factor.
Fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
Fhe pH of this initial reading has to be above a pH of 12.
Fh second pH reading is taken 2 hours after the initial reading.
rH of this second reading has to be above a pH of 12.
-he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 12/21 /16

rh Mt I tK GALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A8165
Waynesville, NC 28785 pH 7.00 Lot #:
FRA ID: NC01119 pH 10.01 Lot #:WP2
;ertification #: 194 pH 10.01 Lot #:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009
S/N: E09596 pH 13.00 Lot #: � �I/�,�,
In Lab Checked with Traceable Thermometer Serial #:180410124
Equipment Maintenance:
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:NOV. 2020
Exp. Date:
Exp. Date:OCT. 2021
Exp. Date: 0,- ,j ;x c_
Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. OC OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. OC
())/DJjATJ,yE
yl i 7
fTIME
�" 1
i �e
r3 a�
1 1 / jJ
�✓'# 9 71i"
l �I A e"` A'_.
CORRECTED PH SU: '12 o 6
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
..
C;ur1RECTED PH SU: � d Y o V n 9 " i)-Ci I
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
"
CORRECTED PH SU:._
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
ThP second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F-P-A, ID: NC01119
i ;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:WP2
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:NOV. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
r
d
1
C3,00
1
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
(" ;. �-�
-7/1 h q
P 5.
b?
rl (.
CORRECTED PH SU: 1'4 C -- ()o% = /)
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
Cur1RECTED PH SU: is Z;-- d1 0 1 r 0, 1
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 0 3 0 , 6 - z /' 1 "5__
Post Calibration Verification
TI((M��E��'^^pp
INyITIAL
Ph
10aSU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th--second pH reading is taken 2 hours after the initial reading.
i ,H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

I'M Mt I tK UALUSKA I ION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
F-�14, ID: NC01119
1 ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:WP2
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
pH 13.00 Lot #:
Checked with Traceable Thermometer Serial #:180410124
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:NOV. 2020
Exp. Date:
Exp. Date:OCT. 2021
Exp. Date:
Cal Due Date:10/2/2023
CAL.
TEMP. oC OF
QC
TEMP. oC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
C1 a
7c
-�(_
'lo.c'
I 1,9"'ry
3'do
jo
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
m
CORRECTED PH SU: e 12,6�
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
n -"A .
r
GuRRECTED PH SU: /!'.I� 7 .- C , 9 0
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: G')-(" -v,6 fi - 7 %
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot MA8165
pH 7.00 Lot #:
pH 10.01 Lot #:WP2
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:NOV. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
r,ti,
4
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU: 1a
2 HR
2 HR
ANALYST
PH SU
TEMP. oC
INITIAL
Cu,<RECTED PH SU: (3,(2 _Y-7
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
b
✓
CORRECTED PH SU: j': 7 .m- & I T I t j;
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
r"
1 V 1
,j� k
2 Q
y
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Thjo second pH reading is taken 2 hours after the initial reading.
l H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Documem changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FPA ID: NCO1119
i ;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
pH 7.00 Lot #:A8165
pH 7.00 Lot #:
pH 10.01 Lot #:WP2
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2020
Exp. Date:
Exp. Date:NOV. 2020
Exp. Date:
Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot M Exp. Date: _
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. oC OF
CAL
TEMP. OC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE.
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
j
® en IL
c` � Y..�
kr,
y,
CurtRECTED PH SU: p 4 q .- () 4 9 � -, /' , ej
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: i .115 -- 6, I iJ; , 0-3 "S)
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th--.second pH reading is taken 2 hours after the initial reading.
aH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

• • • •••� • d•� VI"•VIY.\Al IVl• I WIN :JVJ LIIVIC/JLUUUC
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
F"'A. ID: NC01119 pH 10.01 Lot #:WP2 Exp. Date:NOV. 2020
! ;ertification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. C OF
QC
TEMP. oC OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
'�✓/'J �yf) 5
/—. A l+C�
4 J
c V
`
`r.
y f]
1� (/
(
C9 Lr �d t`'—
_
M
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DAT{Eg(
INITIAL
PH SU
Tp/EMP.'C
-pTIMgpEa
/7DAT(E
�y@TIME
6C
CORRECTED PH SU: f ,._ms' , 1-12
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
p
Cu,<RECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: r . Q "` ` -�j ;1 "3
Post Calihratinn VPrifiratinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th—second pH reading is taken 2 hours after the initial reading.
t )H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rn IVIC 1 CK I.ALIMKAI IUN 1-UK 9U.i LIMO/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A8165 Exp. Date:JUNE. 2020
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
E.RA ID: NC01119 pH 10.01 Lot #:WP2 Exp. Date:NOV. 2020
i ;ertification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. oC OF
QC
TEMP. OC OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
1 PI l�.°
;�.
�Y ���
Dom®
6��u
°'
/
a
�y/
^r,
I
0
Qe
.��;,.,..,
C39sI�;
/f-'^'•`_
ova �1''
r�-a�f
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
7&/�
OR,RECTED PH SU: 12 , C� "m t > `'t
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
CurlRECTED PH SU: �. - 'Ana ' I o 3 5
24 HR
24 HR
ANALYST
PH SU
TEMP. oC
INITIAL
5
_
CORRECTED PH SU: 0-j - ("' � 9 �' w /I • o -)-
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th,- second pH reading is taken 2 hours after the initial reading.
i ,H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EpA ID: NC01119
I ;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot MA8165 _
PH 7.00 Lot #: /3'l j �
PH 10.01 Lot #:WP2
PH 10.01 Lot #: s%I)11d
PH 13.00 Lot #:M28F009
PH 13.00 Lot #:
Checked with Traceable iThermometer Serial #:180410124
,,?Vie', is " s t 0 t'1
Exp. Date:JUNE. 2020
Exp. Date: .9c, i c c v i
Exp. Date:NOV. 2020
Exp. Date:
Exp. Date:OCT. 2021
Exp. Date: _
Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.P'gH
7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIMEy
DATE
INITIAL
PH SU
TEMP. oC
-7dg+
^'TIME
CORRECTED PH SU:..
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
C--,<RECTED PH SU:
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
I')..t
M.,i"C
'��
CORRECTED PH SU: j Ica ... an, l �' = /j, ':
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
fl < k/-)
,
t.' a
do ,'. C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
ThP second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
PH 7.00 Lot #:A9155
Waynesville, NC 28785 pH 7.00 Lot #:
E-PA ID: NC01119 pH 10.01 Lot #:A9142
:ertification #: 194 pH 10.01 Lot #:
Insirument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009
S/N: E09596 pH 13.00 Lot #:
In Lab Checked with T bl Th
race. a ermometer Senal #.180410124
Equipment Maintenance:
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
Ep. Date:
Cal Due Ite:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE ,
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
IF, T
-7
J(
CORRECTED PH SU: I J, T- -Vrt N� = V, ,
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
i ..) :
" .. ''c•
f ? � .
C,—.<RECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: 42, y, I I = 01 qq _
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
dtel_6("_I
IV _.
/04
a • ) 11(
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 Iio pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

rn mt I tK t;AL.IbKAI IUN FUR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
,ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot MA9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
CAL.
TEMP. °C OF
QC
TEMP. oC OF
CAL
TEMP. OC OF
DATE
TIME
SLOPE
EFF.
BUFFER
PH 7.0 SU
PH 7.0 SU
BUFFER
BUFFER
PH 10.0 SU
PH 10.0 SU
BUFFER
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: °, -:i-0o 11 := 11%)
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
C,.. RECTED PH SU: /IC, q « a I a ' 1,9,,°�;�
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 1 ie pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH Mt I tK GALIURNHUN FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
Certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot MA9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date: _
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. C OF
QC
TEMP. oC OF
CAL
TEMP. OC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 1{0.0SU
BUFFER
PH 13.0 SU
BUFFER
1041
1 .� y ._
�(✓l ^ Gn
�`�) � ..
< �a
tiT6e{,� y
gINITIAL
®� ..
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
o'
Y
,RRECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: (z , f
NX-
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculatib,n, may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
, pH of this second reading has to be above a pH of 12.
ie pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

VM Mt I tK GALIbKAI IUN I -UK 511.113 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, INC 28785
EPA ID: NC01119
'ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
pH 7.00 Lot MA9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
pH 13.00 Lot #:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. OC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
M1010
0
e,
YS
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
Li
CORRECTED PH SU: 0, 3 -01 / k3 ':. 01 11)
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
(-.:RECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 0, ' - 4", o d � 1, 6,9
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
off of this second reading has to be above a pH of 12.
i tie pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH Mt I ER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
FRA ID: NC01119
;ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
pH 7.00 Lot MA9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp, Date:
Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date: _
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. C OF
CAL
TEMP. C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
P�Hy 7.0 SU
BUFFER
PH1/0.0 SU
BUFFER
PH®p13.0r�SU
BUFFER
INITIAL
}7
-A � `)
JTIME
5 .
lEjF•F.
P.7 tl fl
d aM '!J
'-A ',
�6e
•11 e� u�,
U 3.0
191 , `�._.
S"
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
`� e,,•j ri %
v� •�, .,.�
� e:d`'#
TTIME
' 4 t � �
9 • � _
�� ��
O 1� �jP' 1, `�
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
(—RECTED PH SU: I'Ti .._ 61 / - ["2— -- <S-
24 HR
24 HR
ANALYST
PH SU
TEMP. oC
INITIAL
.9
CORRECTED PH SU: 1),' M 6, Q 42'C S
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
A°C g
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 rye pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
FPA ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date:. May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. oC OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
4 7 "e.
CORRECTED PH SU: /)— o 4 -=
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
v.�M1 J
g` Sop ,� •.T �
a,n
u,)RRECTED PH SU:
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
CORRECTED PH SU: $s_
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
to
�a
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
-I ne pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

rri IVIC I CK WALIMMA I IUIV rum 3U.3 LIIVIC/OLUUUt:
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
certification #: 194
In6crument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
�q()
. 51'v
V', )..`'('
/our
1,7, 6 0�.
U ,r '��c�
/?ja �'�
� ,.
COLLECT
DATE
COLLECT
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
aTIME
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
1. . <RECTED PH SU: E _ .. �) , ( - n / j .3 S-
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 1 2,"Y - 0, f'' �= 12 , 2 7
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
- nH of this second reading has to be above a pH of 12.
1 I pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
Certification #: 194
li istrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. C OF
QC
TEMP. °C OF
CAL
TEMP °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH�$10.0 SU
BUFFER
PH,q¢ 13.000)ySU
INITIAL
yg
16 , 0
1 tIA a�.
N � *nJ
ypBtUFFER
i �7 3,
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
&`f
CORRECTED PH SU: n"
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
,iRECTED PH SU: _ 1_ - ._ C. 9 ) <—"" � �
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: q,l
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
, „e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

r-rl Mr- i tK I,AL1t3KA I IUN I -UK 5U3 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
:,ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date: _
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. C OF
QC
TEMP. C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
` �
L,_7t
a,P �,
t- iRECTED PH SU: a -3 e, --. 0,1,9
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 7;:%• t'Y ��a "a
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
1 t •' �a
e'� •
qp
N 1
,
9 A v I '1.,,
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i . .e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rrrl mtI CK GALIESKAI IUN FUR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
I-11\ ID: NC01119
'ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N:E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A9155
PH 7.00 Lot #:
PH 10.01 Lot #:A9142
PH 10.01 Lot #:
PH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
PH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. C OF
QC
TEMP. oC OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
91:1
it
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
1721a.,
/26
CORRECTED PH SU:; ?: GP --'>
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
�- ,iRECTED PH SU: L2 '?,- 0,1.2 [9 - '
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
41
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
M
r/
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T..., second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
I r ra pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

rn not I tR CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
1-4 ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 2020
:,ertification #: 194 pH 10.01 Lot #: Exp. Date: _
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 202-1
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
FTIME
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
C i
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: 4 A11
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
iRECTED PH SU: ,.e -r -- (D), I•.o M
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calihratinn VPrifirntinn
TIME
INITIAL
Ph
10 SU
Temp.
a°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T` second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
I ..a pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
.PA ID: NC01119
certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date: _
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. oC OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
ANALYSIS
DATE
ANALYSIS
TIME-g
ANALYST
INITIAL
INITIAL
PHSUTEMP.
INITIAL
oC
a�TIME
CORRECTED PH SU: % -' , C �' -
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
L ERECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: 013 - � s 19 a / 9' i "'�
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
�y
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
..a pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rr1 not I tK UALIUMAI ION FOR 503 LIMEISLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
Wirt'\ ID: NC01119
3ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot MA9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot* Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. OC OF
[DATE
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
py /,✓
/
V�
CORRECTED PH SU: id.�
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
12la
C::,
tYe
ERECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
INITIAL
10 SU
°C
pqTIME
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T"—second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
. ,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

rn not I tK k ALlbKAI IUN 1-UK 5U3 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155
Waynesville, NC 28785 pH 7.00 Lot #:
-I-PA ID: NC01119 pH 10.01 Lot MA9142
:,ertification #: 194 pH 10.01 Lot #:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot * Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIMEg
E9FF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SpU°"'
INITIAL
TEMP. oC
.,DATE
NTIME
is
J ( r
CORRECTED PH SU: fir. --� a 9 x�
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
P
�- �RECTED PH SU: /;)_4-- 0-(;-�' = /,j J I
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:..
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T` second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
.,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
'77'q ID: NCO1119 pH 10.01 Lot #:A9142 Exp. Date: May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:1012/2023
Equipment Maintenance:
F-T
CAL.
TEMP. °C OF
QC
TEMP. OC OF
CAL
TEMP. 0C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATEf/JJ
D]JATE��"
TIMEnn
PH SU
TEMP. oC
y/TIME
�@INITIAL
CORRECTED PH SU: jid.i%.
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
1RECTED PH SU:
24 HR
PH SU
24 HR
I TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: �.�� �,,✓= �:�., t�_
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
9 ' I
i�) r M,
C as�''
rf � j
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
I ..a pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH ME FER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ID: NC01119
certification #: 194
Insirument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 20?..0
Exp. Date:
Exp. Date:OCT. 2021
Pry -i,J.uu not 4: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
DATE
TIME
SLOPE
CAL.
BUFFER
PH 7.0
7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 1/�0.0`SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIAL
tf / p
/ 6S
(EFF.
0{. l G •
% ' 41
.^"' e 0
�6,�
f l A � L....
� ♦ -0v
�`.%
COLLECT
DA%TE/
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: /")j -7 — c, I 'V-- )j-)
2 HR
2 HR
ANALYST
PH SU
TEMP. oC
INITIAL
�- �RECTED PH SU: _(?, I.-) A 1 .6-7.
24 HR
PHppSU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T :econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ,.e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155
Waynesville, NC 28785 pH 7.00 Lot #:
P�''A ID: NC01119
PH 10.01 Lot #:A9142
certification #: 194 pH 10.01 Lot #:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M281`009
S/N: E09596 pH 13.00 Lot #:
In Lab Checked with Traceable Thermometer Serial #:180410124
Equipment Maintenance:
Exp. Date:JUNE. 2C21
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
Exp. Date: ^
Cal Due Date:10/2/2023
DATE
TIME
SLOPE
EFF.
CAL.
BUFFER
PH"g7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIAL
i5t�l
Yr,�,�>...4,A'
a�s.9
t,:a
.j e9b,t _
7'e*•6i
i" figs
Roo
COLLECT
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
:.:D�AT4'E
'q
^TIME
QG
f1
�'dlc
CORRECTED PH SU: ' :, r ; y -
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
AI .� . L
'-s ,
t ERECTED PH SU: �j,,j- c -(%, J) ' jj14e
2:4H R
PSU
24HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
?' record pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
..a pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
"\ ID: NC01119
certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #'A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
ph 'i U.UU Lot It: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
DATE
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 7.0 SU
TEMP. C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
/TIME
Xv
CORRECTED PH SU: /2s .7 —t;,I � r �. —
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
jc ,'t
ERECTED PH SU: _'7 -0 j I A Id,5
:2:4:H:R
24 HR
TEMP. oC
ANALYST
INITIAL
CORRECTED PH SU:: 3 •-io
w��
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
iG `.t 5'"
0- S .
16 i
_ "'�_
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ..a pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rt1 not t tH CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
"A ID: NC01119
certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
PH 7.00 Lot #:A9155
PH 7.00 Lot #:
PH 10.01 Lot #:A9142
PH 10.01 Lot #:
PH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 20?..0
Exp. Date:
Exp. Date:OCT. 2021
pri .(,J.uu t-ot 1;: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
8.00
6<k��
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: / , q_ tI, , j -
2HR
ANALYST
ESU2H
TEMP. °C
INITIAL
' RECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU:,
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
y
�/
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
(,,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
r-,q ID: NC01119
certification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
`N6 i,
is
3, ev
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: (" > 8 e� • - C ,
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
p
iRECTED PH SU:
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
�c
CORRECTED PH SU:
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
,econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ,,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

VH Mt I tR GALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
GSA ID: NCO1119
'3ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 202..0
Exp. Date:
Exp,
Date:OCT. 2021
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
pH 13.00 Lot #:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: id-(o o r f T' ,
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
Ia, a
-'� �- 4"c
g? .5
�- -ERECTED PH SU: /1(1,- o,t -,I w / a.14
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
:10 ,
,
CORRECTED PH SU: I),:-0s9S` ,:= /). /6—
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
/0:a
e"��
10.1
4q" C'
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
,econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ..a pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
`-"�A ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
FD7ATETIME
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
160
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
It��;1ITo
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
U-
J6',` 0(
P-5 -y
�- 1RECTED PH SU: 1.1 3 " 0. /A -': ) �, f
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
�t' �
ju)"
; 31
CORRECTED PH SU: I I-'" - 0 , t ,y 19.4 5—
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
lc --t I
e-5-1
' 0,�
'ab •91(
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
j ,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 W
alnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
r'A ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
DATE
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
�131/q
CORRECTED PH SU: % ,6 -t ( �? - / ;), 3 �
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
12%�
y�
�_ ;RECTED PH SU: Q, C, — 0, 12 ::- (2.4(�l
HR
24 HR
ANALYST
FP24
H SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calibration VPrifiration
FTIME
INITIAL
Ph
10 SU
Temp.
°C
l°U,�z(�
-
� i. 3 C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i , ,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rrt Mt t tK CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
r r'A ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
In6irument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
EFF�y.
PH 7.0 SU
BUFFER
PH(J0110.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
dTIMgE
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: /)-6 w()� fq1: J0.913
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
�- ERECTED PH SU: _ / 2- -1 --0 1 t�- a 0, 15,-
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
d
-r<
CORRECTED PH SU: /), -
Post Calibration Verifi(-.atinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
0)'
�v1� .
/0.
a0, "9
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The -pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ,,a pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

• .. ...� �.w v. .r.r... ...Y.� . Y.� VVV a�1111 vI.I L. .I F/VV
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
--111% ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 2020
: ertification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
B3UFF�/ER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
`�t
F
T.
CORRECTED PH SU: M, ? - 046 t1 25'
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
Q---?
ca.(I� "'
1015,
�- iRECTED PH SU: 1 t, I - 0 � (r-- / .
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
.
CORRECTED PH SU: 12. v f - Q, -�S-
Post Calihration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The., pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'S. revised. 12121116

PH METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot#: Exp. Date:
-�A ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 202..0
certification #: 194 pH 10.01 Lot #: Exp. Date:
Insirument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
IN! I IAL
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
�I III
�� °
y
/
d i• �C-
CORRECTED PH SU: U (v -oi P e 7, ff , q�2
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
�- ERECTED PH SU: a 7 -- 'l , /9,
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: t'�- � ()��'��
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
/'t "oy
e'�.
jo.(
�d,(' 0(-
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The -pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rn 1VIC 1 tK UAL MIKA I IUN FUR 503 LIME/SLUDGE
S W-846-9040 C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
?A ID: NC01119 H 10.01 Lot #:A9142
p Exp, Date: May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
Insrrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
DATE
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIAL
�.m
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: 11 — 0.167 == 12,q5-
2 HR
2 HR
ANALYST
P/pH SU
TEMP.oC
INITIAL
ERECTED PH SU: �,`� R 15T
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
IV> � "C-
-?. i,
CORRECTED PH SU:-, r fa- 55
Post Calibration Verifir ntinn
INITIAL
Ph
10 SU
Temp.
°C
jTIME
e'1 �C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rrh net I tR CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
pH 7.00 Lot #:A9155
Exp. Date:JUNE. 2021
Waynesville, NC 28785
pH 7.00 Lot #:
Exp. Date:
�:PA ID: NC01119
pH 10.01 Lot #:A9142
Exp. Date: May. 2020
certification #: 194
pH 10.01 Lot #:
Exp. Date:
In6irument ID: ORION DualStar pH/ISE Benchtop
pH 13.00 Lot #:M28F009
Exp. Date:OCT. 2021
S/N: E09596
pH 13.00 Lot #:
Exp. Date:
In Lab Checked with Traceable
Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. oC OF
CAL
TEMP. oC OF
DATE
PIM
SLOPE
EFF.
BUFFER
PH 7.0 SU
PH 7.0 SU
BUFFER
BUFFER
PH 10.0 SLI
PH 10.0 SU
BUFFER
BUFFER
PH 13.0 SU
PH 13.0 SU
BUFFER
INITIAL
z /
3C-
mo
,
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU:
2 HR
PH SU
2 HR
TEMP. oC
ANALYST
INITIAL
N' (f
A-VIC
•5
L ERECTED PH SU: /0a (.� — (n / w Q. V
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
La
CORRECTED PH SU: MJ d 6, of a d 1il 71
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The_ pH of this initial reading has to be above a pH of 12.
,econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rr1 Nit I r-K UALIbKAI ION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
PQA ID: NC01119
certification #: 194
Insirument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
PH 'I J.uu I_ot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
AL.
TEMP. °C OF
QC
TEMP. oC OF
CAL
TEMP. °C OF
SFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
TEFF.PH
7.0 SU
BUFFER
PH 10.0 SLI
BUFFER
PH 13.0 SU
BUFFER
INITIAL
I-JI
�tTOOJ.
a c llc I��
� ..
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: /�2. , -
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
�- iRECTED PH SU: 9. G Y-0.' 9 49'�A
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITp^IIAL
•
CORRECTED PH SU: 19. 6--a ) I - o ) I
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
o,9 (V
.S,
10. R
1 I r q06
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
- econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i �.e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rrt not I t:K CALIBRATION FOR 503 LIME/SLUDGE
Town of Waynesville WWTP S W-846-9040C
566 W
alnut Trall pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
r-:`'A ID: NC01119 H 10.01 Lot #:A9142 Exp. Date: p May. 2020
certification #: 194 pH 10.01 Lot #: Ex Date:
,...,Lrument ID: ORION DualStar H/ISE Benchto p
P p pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
D/ApTE TIME
4F.
CAL.
UFFER
SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. oC OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
INITIAL
t
yH/y7.0
9�B'/U/F/FER
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. °C
CORRECTED PH SU: % _ � — C ':z 11 M
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
/12(l
11, 711C
5.
�_ RECTED PH SU: d,J.. 6 - 0, f fir::' Id.
y .
:24 H R
H SU
24 H R
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 0, ,- 60 V z /),7
Post Calibration VPrificatinn
TIMIE
INIHTIAL
Ph
SU
Temp.
°C
910
p
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T ,coral pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
i , ,a pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rn Iwci r-K t-ALIbKAI ION FOR 503 LIME/SLUDGE
Town of Waynesville WWTP S W-846-9040 C
566 Waln t T N
u ral
Waynesville, NC 28785
pH 7.00 Lot #:A9155
Exp. Date:JUNE. 2021
�:-'A ID: NC01119
pH 7.00 Lot #:
Exp. Date;
Certification #: 194
p H 10.01 Lot #:A9142
Exp. Date: May. 20?..0
_,rument ID: ORION DualStar pH/ISE Benchtop
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:
Exp. Date:OCT. 2021
S/N: E09596
In Lab
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial-.180410124 Cal Due
Equipment Maintenance:
Date:10/2/2023
SLOPE
TIME EFF.
CAL.
BUFFER
PH 7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.o SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
°C OF
TEMP��
PH 0 SUDATE
BUFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
6,1/11 r `t
�I ft dt ` l
� d T,
! a
/7a
CORRECTED PH SU: / , e V .2 4 :. Od 6
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
RECTED PH SU: gg., 0,: a '
H R
SU
P
24 H R
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: 0. - 0, I � /1 a .2
Post Calibration VPrifiratinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T econd pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
i ,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised:12/21/16

HN ML I LR CALIBRATION FOR 503 LIME/SLUDGE
Town of Waynesville WWTP S W-846-9040C
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
PDA ID: NC01119 H 10.01 Lot #:A9142 Exp. Date: May. y. 202..0
certification #: 194 pH 10.01 Lot #: Exp. Date:
crument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
SLOPE
CAL. TEMP. °C OF
BUFFER PH 7.0 SU
QC
:BLIFFER
TEMP. °C OF
PH 10.0 SU
CAL
BUFFER
TEMP. °C OF
PH 13.0 SU
DATE
TIME EFF.
PH 7.0 SU BUFFER
00.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
Aft, 1(
lit
y
,
COLLECT
DATE
COLLECT
TIME
ANALYSIS
DATE
ANALYSIS
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
'1E I
�,'o
I�
�yTIME
i Vg
`'5,-,
��r�&
CORRECTED PH SU: /d. (0 — 0 1 � q y /�'?
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
]
1),(
/ "C
e.s.
RECTED PH SU:
FP24 HR
24 HR
TE{>MP. °CJ
ANALYST
INITIAL
/H})SU
s'�
CORRECTED PH SU: d �Y— 0191y 11 11
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
b0119 3 1
P�5' 1
/ ,/
1�'1
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
r Qcond pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
j ,.e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rn Nit i tK UALWHATION FOR 503 LIME/SLUDGE
Town of Waynesville WWTP S W-846-9040C
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
AID: NC01119 pH 10.01 Lot #:A9142
Exp. Date: May. 202..0
certification #: 194 pH 10.01 Lot #: Exp. Date:
rument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:1012/2023
Equipment Maintenance:
DA,pTE
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 7.0 SU
TEMP. °C OF:PH
PH 7.0 SU
BUFFER
QC
FFER
10.0 SU
TEMP. °C OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
MP. °C OF
H 130 SU
!BUFFER
INITIAL
. 69 4Y
9 9. C
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
(�1T.-j
CORRECTED PH SU: % 2.-2 - 6. a -�_ (, LfQ,
2 H R
PH SU
2 H R
TEMP. °C
ANALYST
INITIAL
/)-
doy � O
.5 .
�_ RECTED PH SU: N'(o -0, L� n /gjg',_
::1:4 HR
SU
24 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: ldg_o jyS - l ,�)
Post Calibration Verificntinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
"f )?
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
r econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ..0 pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised:12/21/16

I'll METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot#:
r-°A ID: NC01119 Exp. Date:
2020
PH 10.01 Lot #:A9142 Exp. Date: Mv.a
Certification #: 194 pH 10.01 Lot #:
..rument ID: ORION DualStar pH/ISE Benchto Exp. Date;
p pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #:
In Lab Exp. Date:
Equipment Maintenance:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
SLOPE BUFFER
DATE TIME EFF. PH 7.0 SU
TEMP. °C OF
PH 7.0 SU
BUFFER
QC
BUFFER
PH 10.0 SU
TEMP. oC OF
PH 10.0 SU
BUFFER
CAL
BUFFER
PH 13.0 SU
TEMP. °C OF
PH 13.0 SU
BUFFER
INITIALIj
ECOLLECT[ICOLLECT
ME
ANALYSIS
DATE
ANALYSIS
TIME
ANALYST
INITIAL
INITIAL
PH SU
INITIAL
TEMP. oC
CORRECTED PH SU: & 7 - o., d 41:: f,?, q 6
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
� RECTED PH SU: M-7
L24 HR
SU
24 HR
TEMP. °C
ANALYST
INITIAL
�.3
9I,
A 5 .
CORRECTED PH SU: 12. p S'-
Post Calibration VPrifiratinn
TIME
INITIAL
Ph
10 SU
Temp.
°C
i 3
/0,1
4c,
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The_,pH of this initial reading has to be above a pl-I of 12.
' econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 lid pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #is.
revised:12/21/16

t-HL113KAi 1UN FOR 503 LIME/SLUDGE
To f SW-846-9040C
wn o Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155
Waynesville, NC 28785 Exp. Date:JUNE. 2021
FDA ID: NC01119 PH 7.00 Lot #: Exp. Date:
certification #: 194 pH 10.01 Lot #:A9142 Ex Date: Ma . 2020
PH 10.01 Lot #: p. �— —
_�rument ID: ORION DualStar PHASE Benchto Exp. Date:
S/N: E09596 p pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
In Lab pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
SLOPE
CAL.
BUFFER
TEMP. °C OF
PH 7.0 SU
QC
BUFFER
TEMP. °C OF
PH 10.0 SU
C AL
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
BUFFER
PH 13.0 SU
j
a00
�.�
dl/+�
�td`3�Ir
S 3.00
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU: /). (0 - a, p 1).q5,-
2 HR 2 HR ANALYST
SU
TEMP. °C INITIAL
KPH
/ B$�,
RECTED PH SU:
�,), -- 0, g .!�fg ,
24 HR
24 HR ANALYST
PH SU
TEMP. °C INITIAL
CORRECTED PH SU:
12` 3
Post Calibration Verification
Ph Temp.
TIME
INITIAL
10 SU °C
.
,0 X 1 a C
TEMP. "C OF
PH 13.0 SU
BUFFER INITIAL
Aft i?
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
r econ.d pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised:12/21/16

Nt-I METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot#: Exp. Date:
i"A ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
—rument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. oC OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
Cyr a'ir't
°' :; `
� 1 .i
.{ l
f T `}
1, s
� 3 f3 ✓
%:, .i�"L
M. t '
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
.' / .� S
/ '
i . '
�Sd i l
2
., f�
'Ys`� ,
s� yn.�d . „"
X K`�ir :8...4if.
f
CORRECTED PH SU: �e< .:i 0= i S /") i S
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
RECTED PH SU: 1 � t),
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0,03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
1 „e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised:12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2i_ -,1
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
FDA ID: NC01119 pH 10.01 Lot#:A9142 Exp. Date: May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
-rument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PHly10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
' 0u)
>
z;
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE{
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
11
A
1
l.r
CORRECTED PH SU.- j,f2.,l eti
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
RECTED PH SU: /.t 3
24 HR
24 HR
ANALYST
PH SU
TEMP. oC
INITIAL
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
26,
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
ThP pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised:12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
ID: NC01119 pH 10.01 Lot MA9142 Exp. Date: May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
_.rument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFp(FER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
/ 3
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
,
sRa,.
CORRECTED PH SU: 13> ' o 1 u"' °-
2 H R
2HR
ANALYST
PH SU
TEMP. °C
INITIAL
(.✓
i, .f
.RECTED PH SU:
HR
24 HR
ANALYST
�24
PH SU
TEMP. °C
INITIAL
�0 a .
CORRECTED PH SU:t.I `
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
i ,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised:12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot#: Exp. Date:
I':'1A ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 2020
certification #: 194 pH 10.01 Lot #: Exp. Date:
—rument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
F
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
L✓ 1
e a SA
27 i`\
ob. C? `,,-
� �,1
�
� �Y
� r�.. �' TM�
� <� ✓ y
P"#
f l
.
.� .
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
r t,'
CORRECTED PH SU: /=f�:j:, t s
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
RECTED PH SU: I j) , ' ., t" , (�
24 HR
PH SU
24 HR
TEMP. oC
ANALYST
INITIAL
�j
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
I ,z pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised:12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
P°A ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 202.0
certification #: 194 pH 10.01 Lot #: Exp. Date:
.,rument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 12.00 Lot #: Exp. Date: _
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
PDAT.,E
TIME
EFF.
PH 7.0 SU
BUFFER
PH 1o.o SU
BUFFER
PH 13.01 SU
BUFFER
INITIAL
IcdY.�J,
...
v- .
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
SU
TEMP. oC
., `
/PHj
CORRECTED PH SU: ) 4 (" -,oI I / I, `t�")
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
RECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. oC
INITIAL
CORRECTED PH SU: ,/ ,� •" /- o' I "' ` /„ . "2
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12,
i „e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised:12/21/16

PN METER CALIBRATION FOR 503 LIME/SLUDGE
S W-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
pH 7.00 Lot #:A9155
Exp. Date:JUNE. 2021
Waynesville, NC 28785
pH 7.00 Lot #:
Exp. Date:
�:°A ID: NC01119
pH 10.01 Lot #:A9142
Exp. Date: May. 20.20
certification #: 194
pH 10.01 Lot #:
Exp. Date:
.,rument ID: ORION DualStar pH/ISE Benchtop
pH 13.00 Lot #:M2817009
Exp. Date:OCT. 2021
S/N: E09596
pH 13.00 Lot #:
Exp. Date:
In Lab Checked with Traceable
Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PHy10.o SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
b 6
.5 •L/"�
`'.i+ i
,._.. :...
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
7�� f
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
RECTED PH SU: �:'�. Ica "0 /
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
econd pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
I J,e pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail pH 7.00 Lot #:A9155 Exp. Date:JUNE. 2021
Waynesville, NC 28785 pH 7.00 Lot #: Exp. Date:
EPA ID: NC01119 pH 10.01 Lot #:A9142 Exp. Date: May. 2020
I ertification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009 Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
o,?
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
I
CORRECTED PH SU: 1 I 1
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
Cv.-�RECTED PH SU: %� s /= ), # ' ) Utz;
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU
Dnct (`alihrntinn Varifinntinn
Ph
Temp.
TIME
INITIAL
10 SU
°C
,, a
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
TK- second pH reading is taken 2 hours after the initial reading.
dH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA. ID: ":!'-01119
P, artification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 202Q
Exp. Date:
Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. oC OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
� f
ft)/21
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. eC
CORRECTED PH SU: •�J "• �'/ -
2 HR
2 HR
ANALYST
PH SU
TEMP. oC
INITIAL
Cu.-,RECTED PH SU: , : '`>> 1 d Jd 05
24 HR
PH SU
24 HR
TEMP. °C
ANALYST
INITIAL
)
3C 9
CORRECTED PH SU:
Pest Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th- second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NCO1119
N 3rtification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. oC OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
//
77
z>p .n'
J. ovar
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU: ''t " o .
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
c_.
Cu,.RECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: I / J, '(
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH cl this initial reading has to be above a pH of 12.
ThP second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot *A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. oC OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. oC
INITIAL
0— ERECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. oC
INITIAL
CORRECTED PH SU: 1 z!
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
ThP second pH reading is taken 2 hours after the initial reading.
>H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
N artification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot MA9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
pH 13.00 Lot #:
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
Exp. Date:
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. oC OF
QC
TEMP. °C OF
CAL
TEMP. oC OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
t
0,0
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
TIME
INITIAL
PH SU
TEMP. °C
j.��'
DATE
I 11
5
•C—
F.l�.�.�
4i
a ✓
�
CORRECTED PH SU: �'L 0, l 1 sI.'
2 HR
2 HR
ANALYST
PH SU
TEMP. oC
INITIAL
Cu,-�RECTED PH SU: Wi) Ia' 1,1.`Y'
24 HR
24 HR
ANALYST
PH SU
TEMP. oC
INITIAL
y
CORRECTED PH SU: a.;�' � � � /�� o
Post Calibration Verification
TIME
INITIAL
Ph
10 SU
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th- second pH reading is taken 2 hours after the initial reading.
-,,H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
S/N: E09596 pH 13.00 Lot #: Exp. Date: _
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
1t I
�`� 3 1 j
Krc y
t3 :✓'
qs� �. l,i
/
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
��P.1/•/y
�' � 7
"�.;A.
0) 7
,J c;
t
rp. ��'
:'i� iii 3
)',Y�s..�
F7 iii
CORRECTED PH SU: ;'.: rr c" 1 Q?
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
Cu.-,RECTED PH SU:
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU: H. 211
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
/
r
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
ThP second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NCO1119
ertification #: 194
Instrument ID: ORION DualStar pH/ISE Benchtop
S/N: E09596
In Lab
Equipment Maintenance:
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
pH 13.00 Lot #:M28F009
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
pH 13.00 Lot #: Exp. Date: _
Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
2
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. °C
r)
CORRECTED PH SU:.:. - Via,?; - ' •-,...
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
C,,..RECTED PH SU: ' ? t2,18 3/<?. il "'I
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
`a„ z)
/
CORRECTED PH SU: F.=>� ==99
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
)H of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

rr7 IVIC I CM W MLIDMAI IVIV rum DU3 LIIVIC/0LUUl7C
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
pH 7.00 Lot #:A9155
Exp. Date:JUNE. 2021
Waynesville, NC 28785
pH 7.00 Lot #:
Exp. Date:
`—'\ ID: NC01119
pH 10.01 Lot #:A9142
Exp. Date: May. 2020
1.. _ ,:ertification #: 194
pH 10.01 Lot #:
Exp. Date:
Instrument ID: ORION DualStar pH/ISE Benchtop
pH 13.00 Lot #:M28F009
Exp. Date:OCT. 2021
S/N: E09596
pH 13.00 Lot #:
Exp. Date:
In Lab Checked with Traceable Thermometer Serial #:180410124 Cal Due Date:10/2/2023
Equipment Maintenance:
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
BUFFER
INITIAL
kp
x
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
T ola-A
iy
b
d . . �5—
f' �K 0 so
CORRECTED PH SU:
2 HR
2 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CC)RREL ', ED PH SU: '$;.,_:` . j w..y �u
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calihration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
4' ,
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pl-, Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T' second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21/16

PH METER GALIMAIIUN 1-UR 5U3 LIME/5L000t
SW-846-9040C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
ID: NC01119
I .;ertification #: 194
pH 7.00 Lot #:A9155
pH 7.00 Lot #:
pH 10.01 Lot #:A9142
pH 10.01 Lot #:
Instrument ID: ORION DualStar pH/ISE Benchtop pH 13.00 Lot #:M28F009
S/N: E09596 pH 13.00 Lot*
In Lab Checked with Traceable Thermometer Serial #:180410124
Equipment Maintenance:
Exp. Date:JUNE. 2021
Exp. Date:
Exp. Date: May. 2020
Exp. Date:
Exp. Date:OCT. 2021
Exp. Date: _
Cal Due Date:10/2/2023
CAL.
TEMP. °C OF
QC
TEMP. °C OF
CAL
TEMP. °C OF
SLOPE
BUFFER
PH 7.0 SU
BUFFER
PH 10.0 SU
BUFFER
PH 13.0 SU
DATE
TIME
EFF.
PH 7.0 SU
BUFFER
PH 10.0 SLI
BUFFER
PH 13.0 SU
BUFFER
INITIAL
61
COLLECT
COLLECT
ANALYSIS
ANALYSIS
ANALYST
INITIAL
INITIAL
DATE
TIME
DATE
TIME
INITIAL
PH SU
TEMP. oC
CORRECTED PH SU: k� Y v 9 / t `)
2 HR
PH SU
2 HR
TEMP. °C
ANALYST
INITIAL
CORRECTED PH SU: > U, )�"'? ': �'9 r3
24 HR
24 HR
ANALYST
PH SU
TEMP. °C
INITIAL
CORRECTED PH SU:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
10 SU
°C
Wn
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Th., second pH reading is taken 2 hours after the initial reading.
l aH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 12/21 /16

TCLP

t
N
-` Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name: Town of Waynesville WWTP
Collection date: 7-May-19
Date received: 7-May-19
Sample identification: 503 Lime Sludge - Composite
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 190507.531
Sample number: 168191
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Reactive Cyanide
335.4
0.338
mg/kg
23-Nlay-1g
ECHEM
2
Reactive Sulfide
SM 4500 S D
9.63
mg/kg
24-May-19
ECHEM
2
Ignitability
SW 846 1030
<0.8
0.8
min/sec
23-May-19
ECHEM
2
pH in Soil
9045 C
12.2
S.U.
7-May-19
MS
3
Arsenic - TCLP
6010 C
<0.25
0.25
mg/L
17-May-19
LMC
1
Barium - TCLP
6010 C
<2.50
2.50
mg/L
17-May-19
LMC
I
Cadmium -TCLP
6010 C
<0.05
0.05
mg/L
17-May-19
LMC
I
Chromium - TCLP
6010 C
<0.10
0.10
mg/L
17-May-19
LMC
I
Lead - TCLP
6010 C
<0.25
0.25
mg/L
17-May-19
LMC
1
Selenium - TCLP
6010 C
<0.25
0.25
mg/L
17-May-1q
LMC
1
Silver - TCLP
6010 C
<0.10
0.10
mg/L
17-May-19
LMC
l
Mercury - TCLP
7470A
<0.0020
0.0020
mg/L
22-May-19
TLT
1
Full Scan TCLP Organics
See attached sheets
1,2
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Sample analzyed by Enviro Chemists, Inc.
3. Sample analzyed outside holding time. Duplicate result was 12.3 S.U.
Date reviewed: (H-30
Data reviewed by: Kelley E. Keenan
Signature: V a
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.

Rogers& Callcott
ENVI RON MENTAL
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Dear Client:
x mod,.
%
Laboratory Report
Project: Waynesville WWTP
Work Order: 9050445
Received: 05/08/2019 09:30
Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of
custody for samples that were received on May 08, 2019. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses
performed under NELAP certification have complied with all the requirements for the TNI standard The analyses met the QA/QC confidence interval
for each test method unless otherwise qualified. Estimated uncertainty is available upon request.
Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at amy.ashley cDrogersandcallcott.com or
(864)-335-4962 if you have any questions about this report.
Report Approved By:
R-J'4-vl�'> 9
Amy Ashley
Project Manager
This report may not be reproduced, except in f dl, without written permission fi-orn Rogers & Callcott, Inc.
110 Box 565 S Gwe xnville, SC 29606 426 Fairforesr Vl/ay G evnry llo, SC 29607 niJn 864.232,1556 fax 86, 11.232-6i4o ri?�Tyersa dcallcott.com
a;r rrrnplayee-o;.�rred coralmny
Page 1 of 21

ti
oge
oR"
Certificate of Analysis
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Sample Number Sample Description
9050445-01 Waynesville W WTP 503 Lime Sludge - Comp
e PCcft""
41
South Carolina Greenville Laboratory Identification 23105
South Carolina Columbia Laboratory Identification 40572
North Carolina Laboratory Certification Number 27
North Carolina Drinking Water Lab Number 45710
NELAP Utah Certificate Number SC000042014-1
Georgia Drinking Water Lab ID 880
Project: Waynesville WWTP
Work Order: 9050445
Received: 05/08/2019 09:30
Matrix Sampled Type
Sludge 05/07/19 07:41 Composite
PO Box 5655 Greonville, 8CC 29606 426 r lr o~esr Vv4ay Greenvillo, 5C' 29607 rnaEn 864.232.1556 fax 864.232.614J Y'ogerSaT-idcallcott.com
an (ompany
0512812019 16.30 This report may not be reproduced, except in fill, without written permission from Rogers & Callcot(. Inc. Page 2 of Z 1

rRogers &Cakott
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
Sample Data
Sample Number
Sample Description
Parameter
9050445-01
Waynesville W WTP 503 Lime Sludge - Comp collected on 05/07/19 07:41
Reporting
Result Limit Units DF Analyzed
Method
Flag Analyst
Batch
TCLP Metals
Mercury
ND
0.0020
mg/L
10.0
05/22/19 11:57
EPA7470A
TLT
B9E0976
Arsenic
ND
0.25
mg/L
5.00
05/17/19 00:48
EPA 6010D
LMC
B9E0681
Barium
ND
2.50
mg/L
5.00
05/17/19 00:48
EPA 6010D
LMC
B9E0681
Cadmium
ND
0.05
mg/L
5.00
05/17/19 00:48
EPA 601OD
LMC
B9E0681
Chromium
ND
0.10
mg/L
5.00
05/17/19 00:48
EPA 60t0D
LMC
139E0681
Lead
ND
0.25
mg/L
5.00
05/17/19 00:48
EPA 6010D
LMC
B9E0681
Selenium
ND
0.25
mg/L
5.00
05/17/19 00:48
EPA 60101)
LMC
B9E0681
Silver
ND
0.10
mg/L
5.00
05/17/19 00:48
EPA 601OD
LMC
B9E0681
TCLP Volatile Organics
Benzene
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
B9E1134
2-Butanone(MEK)
ND
0.200
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
B9E1134
Carbon tetrachloride
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
B9E1134
Chlorobenzene
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
B9EI134
Chloroform
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
B9E1134
1,2-Dichloroethane
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
B9E1134
1,4-Dichlorobenzene
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA 8260B
LDM
B9E1134
1, 1 -Dichloroethene
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
B9E1134
Tetrachloroethene
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
B9E1134
Trichloroethene
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
139E1134
Vinyl chloride
ND
0.100
mg/L
50.0
05/21/19 17:44
EPA8260B
LDM
B9E1134
Surrogates
%REC
% REC Limits
Flag
1,2-Dichloroethane-D4
94
70-130
Toluene-D8
122
70-130
4-Brorno/luorobenzene
109
70-130
TCLP Semi -Volatile Organics
2-Methylphenol(o-Cresol)
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA8270D
RJM B9E0691
3/4-Methylphenol(m,p-Cresol)
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA8270D
RJM B9E0691
total Cresol
ND
0.200
mg/L
50.0
05/15/19 15:21
EPA8270D
RJM B9E0691
2,4-Dinitrotoluene
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA8270D
RJM B9E0691
Hexachlorobenzene
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA 8270D
RJM B9E0691
Hexachlorobutadiene
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA8270D
RJM B9E0691
Hexachloroethane
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA8270D
RJM B9E0691
Nitrobenzene
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA8270D
RJM B9E0691
P Box 5655 Gr�:ofmlle, SC: 29606
426 Fair'fore t Way
Greerrvifio,
SC 29607
main WA.232.1556 ' fax [phone]
1
1 ogerSaridcallcott,com
an einployee ok^rrred company
0512812019 16.30 This report pray not he reproduced, except in full, without written perurission front Rogers d Callcoft, Inc. Page 3 Of 21

la Rogers& Cal[cott
ENV IRONMEN.1AI_
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
Sample Number 9050445-01
Sample Description Waynesville W WTP
503 Lime Sludge
- Comp collected on 05/07/19
07:41
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag
Analyst
Batch
TCLP Semi -Volatile Organics
Pentachlorophenol
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA 8270D
RJM
B9E0691
Pyridine
ND
0.100
nng/L
50.0
05/15/19 15:21
EPA 8270D
RJM
139E0691
2,4,5-Trichlorophenol
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA 8270D
RJM
139E0691
2,4,6-Trichlorophenol
ND
0.100
mg/L
50.0
05/15/19 15:21
EPA 8270D
RJM
139E0691
Surrogates
%REC
% REC Limits
Flag
Nitrobenzene-D5
81
15-314
2-Flaorobiphenyl
68
32-118
2-Fluorophenol
67
20-110
Phenol-D5
55
8-424
2,4,6-Tribromophenol
110
39-130
Terphenvl-DN
106
26-173
TCLP Pesticides
Gamma-BHC (Lindane)
ND
0.00050
mg/L
10.0
05/24/19 06:16
EPA 8081B
RKH
B9E0848
Chlordane
ND
0.0050
nng/L
10.0
05/24/19 06:16
EPA 8081B
RKH
139E0848
Endrin
ND
0.00050
mg/L
10.0
05/24/19 06:16
EPA 8081B
RKH
139E0848
Heptachlor
ND
10.00050
rng/L
10.0
05/24/19 06:16
EPA 8081B
RKH
139E0848
Heptachlor epoxide
ND
0.00050
mg/L
10.0
05/24/19 06:16
EPA 8081B
RKH
B9E0848
Toxaphene
ND
0.0050
mg/L
10.0
05/24/19 06:16
EPA 8081B
RKH
139E0848
Methoxychlor
ND
0.00050
ing/L
10.0
05/24/19 06:16
EPA 8081B
RKH
B9E0848
Surrogates
% REC
% REC Limits
Flag
2,4,5,6-Tetrrichloro-m-xylerre
89
60-130
Decachlorobiphenyl
56
30-150
PO Box 5655 (,: oonvbc, SC 29606 426 FairloresE \A/ay G eonw:€le, SC 29607 main €164.232,1556 ' fax E64 232.6I40 rogerSc'1Cldcallcott,com
an empi« yee-cnvned cornpt)ny
0512812019 16.30 This report may not be reproduced, except in Jidl, without iwritten permission from Rogers & Callcott, Inc Page 4 Of 21

Rogers &Caticott
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B9E0681 - EPA 3005A
Blank (B9E0681-BLK1)
Arsenic
ND
0.05
rng/L
Barium
ND
0.50
mg/L
Cadmium
ND
0.01
mg/L
Chromium
ND
0.02
mg/L
Lead
ND
0.05
mg/L
Selenium
ND
0.05
mg/L
Silver
ND
0.02
mg/L
Blank (B9E0681-BLK2)
Arsenic
ND
0.25
mg/L
Barium
ND
2.50
mg/L
Cadmium
ND
0.05
mg/L
Chromium
ND
O.10
mg/L
Lead
ND
0.25
mg/L
Selenium
ND
0.25
mg/L
Silver
ND
O.10
mg/L
Blank (B9E0681-BLK3)
Arsenic
ND
0.25
mg/L -- - - ----------
Barium
ND
2.50
mg/L
Cadmium
ND
0.05
mg/L
Chromium
ND
0.10
mg/L
Lead
ND
0.25
mg/L
Selenium
ND
0.25
mg/L
Silver
ND
0.10
mg/L
LCS (B9E0681-BSI)
Arsenic
0.47
0.05
mg/L
0.500
94
80-120
Barium
ND
0.50
mg/L
0.500
96
80-120
Cadmium
0.47
0.01
mg/L
0.500
94
80-120
Chromium
0.49
0.02
mg/L
0.500
98
80-120
Lead
0.49
0.05
mg/L
0.500
98
80-120
Selenium
0.47
0.05
mg/L
0.500
94
80-120
Silver
0.47
0.02
mg/L
0.500
94
80-120
PC) 3,:;x 5655 ` Gr eerivi8ea, SC 29606 426 [airforest. Way = Greenville, SC 29607 -nam 864,232,15.,56 fax [phone] rogerSc"1ndcallcott.co 1i
an ewplay orat ed company
0512812019 16:30 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 5 Of 21

Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B9E0681 - EPA 3005A
LCS (B9E0681-BS2)
Arsenic
2.23
0.05
mg/L
2.50
89
80-120
Barium
2.25
0.50
mg/L
2.50
90
80-120
Cadmium
2.14
0.01
mg/L
2.50
86
80-120
Chromium
2.28
0.02
mg/L
2.50
91
80-120
Lead
2.28
0.05
mg/L
2.50
91
80-120
Selenium
2.22
0.05
ing/L
2.50
89
80-120
Silver
2.18
0.02
mg/L
2.50
87
80-120
Matrix Spike (B9E0681-MS5)
Source: 9050445-01
Arsenic
2.41
0.25
mg/L
2.50
ND
96
75-125
Barium
3.58
2.50
mg/L
2.50
ND
87
75-125
Cadmium
2.34
0.05
mg/L
2.50
ND
94
75-125
Chromium
2.30
0.10
mg/L
2.50
ND
92
75-125
Lead
2.22
0.25
mg/L
2.50
ND
89
75-125
Selenium
2.38
0.25
mg/L
2.50
ND
95
75-125
Silver
2.49
0.10
mg/L
2.50
ND
99
'75-125
Batch B9E0976 - EPA 7470A
Blank (B9E0976-BLKI)
Mercury
ND
0.0002
mg/L
Blank (B9E0976-BLK2)
Mercury
ND
0.0020
mg/L
Blank (B9E0976-BLK3)
Mercury
ND
0.0020
mg/L
Blank (B9E0976-BLK4)
Mercury
ND
0.0020
mg/L
LCS (B9E0976-BSI)
Mercury
0.0052
0.0002
mg/L
0.00500
103
85-115
110 Box 5655 G ur,,dl= S 29606 426 Fm orest 'Way G i een HIe, SC 29607 n .:n 864.232.1556 fax [phone] rogersandcallcott,CCJm
ern ernp(oym:-«a.�riece r:ornpany
0512812019 16.30 This report may not be reproduced, except in fill, without written permission from Rogers & Callcott, Inc. Page 6 of 21

ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Metals
Quality Control Summary
Reporting Spike Source °/REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B9E0976 - EPA 7470A
LCS (B9E0976-BS2)
Mercury 0.0507 0.0020 mg/1. 0.0500 101 85-115
Matrix Spike (B9E0976-MS5) Source: 9050445-01
Mcrcury 0.0391 0.0020 mg/L 0.0500 ND 78 75-125
Post Spike (139E0976-PS5) Source: 9050445-01
Mercury 3.93
ug/L 4.00 0.0415 97 80-120
PO Box 5655 C3i eenvillt, Si(-'.29606 426 Faiirforest vAl y GreerivHlo, ACT 29607 nn.im 864.1-32.1556 fix 864.232.614o roge °5randcallco t.co'i"i
are
0512812019 16:30 This report may not be reproduced, except in full, without written permission fiom Rogers & Callcott, Inc. Page 7 Of 27

Rogers &Caticott
ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B9E1134 - EPA 5030
Blank (B9E1134-BLKI)
Benzene
ND
0.00200
mg/L
2-Butanone (MEK)
ND
0.00400
mg/L
Carbon tetrachloride
ND
0.00200
mg/L
Chlorobenzene
ND
0.00200
mg/I.
Chloroform
ND
0,00200
mg/L
1,2-Dichlorocthane
ND
0.00200
mg/L
1,4-Dichlorobcnzcnc
ND
0.00200
mg/L
1,1-Dichlorocthcnc
ND
0.00200
mg/L
Tctrachlorocthcnc
ND
0.00200
mg/L
Trichloroetliene
ND
0.00200
mg/L
Vinyl chloride
ND
0.00200
mg/L
Surrogate: 1.2-Diehloroethane-D4
103
70-130
Surrogate: Toluene-D8
127
70-130
Surrogate. 4-BromoJluorobenzene
117
70-130
Blank (B9E1134-BLK2)
Benzene
ND
0.100
mg/L
2-Butanonc (MEK)
ND
0.200
mg/L
Carbon tetrachloride
ND
0.100
mg/L
Chlorobenzene
ND
0.100
mg/L
Chloroform
ND
0.100
mg/L
1,2-Dichlorocthane
ND
0.100
mg/L
1,4-Dichlorobcnzcnc
ND
0.too
mg/L
I,1-Dichlorocthcnc
ND
0.100
mg/L
Tctrachlorocthcnc
ND
0.100
mg/L
'richloroethenc
ND
0.100
mg/L
Vinyl chloride
ND
0.100
mg/L
Surrogate 1,2-Dichloroethane-D4
89
70-130
Surrogate: Toluene-D8
117
70-130
Surrogate: 4-Braznojhuorobenzene
105
70-130
LCS (B9E1134-BS1)
Benzene
0.0203
0.00200
tng/L
0.0200
101
70-130
2-Butanonc (MEK)
0.0195
0M400
mg/L
0.0200
98
60-140
Carbon tetrachloride
0.0187
0.00200
mg/L
0.0200
94
70-130
Chlorobenzene
0.0183
0.00200
mg/L
0.0200
92
70-130
PO Box 5655 C: f�cn
rlk�, SC:' 29606 426 Fan f ; c, Way
<at �r>
vi(l , ` C 29607
' main 864.232,ISS6
fax 864.232.614J
rogeI"Scandcallcott.com
a;y p,mtultt�+....�t-t>v;ht><:! corvipaat:y
0512812019 16. 30 This report may not be reproduced, except in Jidl, without written permission from Rogers & Callcott, [tic. Page 8 of Z 1

Rogers &Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B9E1134 - EPA 5030
LCS (B9E1134-BSI)
Chloroform
0.0198
0.00200
mg/L
0.0200
99
70-130
1,2-Dichlorocthanc
0.0181
0.00200
mg/L
0.0200
90
70-130
1,4-Dichlorobcnzcnc
0,0186
0.00200
mg/t,
0.0200
93
70-130
1,1-Dichlorocthcnc
0.0197
0.00200
mg/L
0.0200
99
70-130
Tctrachlorocthcnc
0.0182
0.00200
mg/L
0.0200
91
70-130
Trichlorocthene
0.0198
0.00200
mg/L
0.0200
99
70-130
Vinyl chloride
0.0227
0.00200
mg/L
0.0200
114
60-140
Surrogate:l,2-Dichloroethane-D4
93
70-130
Surrogate: Toluene-D8
104
70-130
Surrogate. 4-Brotno luorobenzene
105
70-1.30
Matrix Spike (139E1134-MSI)
Source: 9050445-01
Benzene
1.09
0.100
mg/l.
1.00
ND
109
70-130
2-Butanone (MEK)
1.05
0.200
mg/L
1.00
ND
105
60-140
Carbon tetrachloride
1.25
0.100
mg/L
1.00
ND
125
70-130
Chlorobenzene
0.973
0.100
mg/L
1.00
ND
97
70-130
Chloroform
t.09
0.100
mg/L
L00
ND
109
70-130
1,2-Dichlorocthanc
0.924
0.100
mg/L
1.00
ND
92
70-130
1,4-Dichlorobcnzcnc
0.972
0100
mg/L
1.00
ND
97
70-130
I,t-Dichlorocthcnc
1.21
0.100
mg/L
1.00
ND
121
70-130
Tctrachlorocthcnc
1.13
0.100
mg/L
1.00
ND
113
70-130
Trichlorocthcne
1.05
0.100
mg/L
1.00
ND
105
70-130
Vinyl chloride
1.28
0.100
mg/L
1.00
ND
127
60-140
Surrogate: 1,2-Dichloroethane-D4 96 70-130
Surrogate: Toluene-D8 119 70-130
Surrogate:4-Bromo/luorobenzene 106 70-130
Matrix Spike Dup (139E1134-MSD1) Source: 9050445-01
Benzene
1.10
0.100
mg/L
1.00
ND
I10
70-130
1 20
2-13manonc (MEK)
0.971
0.200
mg/L
1.00
ND
97
60-140
8 20
Carbon tetrachloride
1.23
0.100
mg/L
1.00
ND
123
70-130
2 20
Chlorobenzene
0.986
0.100
mg/L
1.00
ND
99
70-130
1 20
Chloroform
1.10
0.100
mg/L
1.00
ND
1l0
70-130
1 20
1,2-Dichlorocthanc
0.924
0.100
mg/L
1.00
ND
92
70-130
0.05 20
1,4-Dichlorobenzenc
1.01
0.100
mg/L
1.00
ND
101
70-130
4 20
1,1-Dichloroctliene
1.16
0.100
mg/L
1.00
ND
116
70-130
5 20
PO Box 5655
Groonv.flo, SC 29606 426 F wfoe-tn.sz. V14-a?` !
C i ,.k nvilk
, SC 29607
,Hann 864232,1556
fax 864. 22.6i40
rope sandCallCott.ct7m
Ml r_omporly
0512812019 16.30
This report may not be reproduced,
except in full, without
written permission fiom
Rogers & Callcott, Inc.
Page 9 Of Z 1

Rogers &Callcott
1".VIRC)NM N FA
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B9E1134 - EPA 5030
Matrix Spike Dup (B9E1134-MSDI) Source. 9050445-01
Tctrachlorocthcnc
1.12
0.100
mg/L
1.00
ND
Ill
70-130
0.9
20
Trichloroethene
1.06
0.100
mg/L
1.00
ND
106
70-130
0.9
20
Vinyl chloride
1.29
0.100
mg/L
1.00
ND
127
60-I40
0.2
20
Surrogate: 1, 2-Dichlaroethane-D4
Surrogate. 7oluene-D8
Surrogate: 4-13rorn of uor obenzene
97 70-130
118 70-130
110 70-130
PO Box 655 Grocnvilke, SC 29606 426 lair`crrast VVay Greranvilke, K. 29607 =nain 864.232.1556 fax [phone]mo rogersan callcott.com
an employee -owned coonpany
05128/2019 16:30 This report may not be reproduced, except in fidl, without written permission from Rogers & Callcott, Inc Page 10 of 21

Rogers &Caltcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B9E0691 - EPA 3510C - GCMS
Blank (B9E0691-BLK1)
2-Mcthylphcnol (o-Cresol)
ND
0.0100
mg/L
3/4-Mcthylphcnol (m,p-Cresol)
ND
0.0100
mg/L
total Cresol
ND
0.0200
mg/L
2,4-Dinitrotoluc11c
ND
0.0100
mg/L
Hcxachlorobenzene
ND
0.0100
mg/L
Hexachlorobutadiene
ND
0,0100
mg/L
Hcxachloroethanc
ND
0.0100
mg/L
Nitrobenzene
ND
0.0100
mg/L
Pcntachlorophcnol
ND
0.0100
mg/L
Pyridine
ND
0.0100
mg/L
2,4,5-Trichlorophcnol
ND
0.0100
mg/L
2,4,6-Trichlorophcnol
ND
0.0100
mg/L
Surrogate: Nihrobenzene-D5
84
15-314
Surrogate. 2-Fluorobiphenyl
78
32-118
Surrogate: 2-Fluorophenol
66
20-110
Surrogate: Phenol-D5
62
8-424
Surrogate:2,4,6-Tribronrophenol
77
39-130
Surrogate: Terphenyl-D14
119
26-173
Blank (B9E0691-BLK2)
2-Mcthylphcnol (o-Cresol)
ND
0.100
mg/L
3/4-Mcthylphenol (nt,p-Cresol)
ND
0.100
mg/L
total Cresol
ND
0.200
mg/L
2,4-Dinitrotohrcuc
ND
0.100
mg/L
Hexachlorobenzene
ND
0.too
mg/L
Hexachlorobutadiene
ND
0.100
mg/L
Hexachloroethane
ND
0.100
mg/L
Nitrobenzene
ND
0.100
mg/L
Pcntachlorophcnol
ND
0.100
mg/L
Pyridine
ND
0.100
mg/L
2,4,5-Trichlorophcnol
ND
0.100
mg/L
2,4,6-Trichlorophcnol
ND
0.100
tng/L
Surrogate.Nitrobenzene-D5
74
15-314
Surrogate: 2-Fluorobiphenyl
65
32-118
Surrogate. 2-Fluorophenol
47
20-110
Surrogate: Phenol-D5
47
8-424
PC) &x 5655 Gr-ecnvfl8#=, SC 29606 426 Fah,f<)resc Wary Greonvilk,,, SC 29007 main 864.2.32.1556 fax 864.232,6140 rogersandcallcott.com
an emplo_yeo-ov"' ted Company
0512812019 16:30 This report may not be reproduced, except in fill, without written permission from Rogers & Callcott, Inc. Page 11 of 21

Rogers &Caltcott
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B9E0691 - EPA 3510C - GCMS
Blank (B9E0691-BLK2)
Blank (B9E0691-BLK3)
2-Mcthylphcnol (o-Cresol)
3/4-Mcthylplicrrol (m,p-Cresol)
total Cresol
2,4-Dinitrotoluene
Hexachlorobenzenc
Hcxachlorobutadicne
Hexachlorocthane
Nitrobenzene
Pcntachlorophcnol
Pyridine
2,4,5-Trichlorophcnol
2,4,6-Trichlorophcnol
Surrogate: 2, 4, 6-Tribromophenol
Surrogate: 7', phenyl-D14
ND
0.100
mg/L
ND
0.100
mg/L
ND
0.200
mg/L
ND
0.100
mg/L
ND
0100
mg/L
ND
0.100
mg/L
ND
0.100
mg/L
ND
0.100
mg/L
ND
0.100
mg/L
ND
0.100
mg/L
ND
0.100
mg/L
ND
0,100
mg/L
63 39-130
123 26-173
Surrogate: Nitrobenzene-D5
68
15-314
Surrogate:2-Fluorobiphenyl
57
32-118
Surrogate. 2-Fluorophenol
53
20-110
Surrogate: Phenol-D5
44
8-424
Surrogate. 2,4,6-Tribromophenol
76
39-130
Surrogate: Tophenyl-D14
119
26-173
LCS (B9E0691-BSI)
2-Methylphenol(o-Cresol)
0.659
0.100
mg/L
0.800
82
40-110
3/4-Mcthylphcnol (m,p-Cresol)
1.21
0.100
mg/L
1.60
76
40-110
2,4-Dinitrotoluenc
0.595
0.100
mg/L
0.800
74
52-I10
Hexachlorobenzenc
0.742
0.100
mg/l.
0.800
93
52-121
Hcxachlorobutadicne
0.460
0.100
mg/L
0.800
57
30-110
Hexachlorocthanc
0.605
0.100
mg/L
0.800
76
24-I10
Nitrobenzene
0.778
0.100
mg/L
0.800
97
36-110
Pcntachlorophcnol
0.592
0.100
mg/L
0,800
74
43-125
Pyridine
0.578
0.100
mg/L
0.800
72
24-110
2,4,5-Trichlorophenol
0.652
0,100
mg/L
0,800
82
53-115
4,6-Trichlorophenol
0.644
0.100
mg/L
0.800
80
53-110
Surrogate: Nitrobenzene-D5 86 15-314
PO Box. 5655 Gr senv.11e, SC 29606 426 Fan-florese. VVay Creonvifiia, 5C - 29607 ' Miin 8611,232.1556 fx 864.232.61.4t} ii3gE'f"Sai1dCalfCC}1 t.CC)9i1
an om rloy c� own td cw"p'ny
05/28/2019 16:30 This report may not be reproduced, except in fill, without written permission from Rogers & Callcott, Inc. Page 12 of 21

Rogers
ger i
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Tags
Batch B9E0691 - EPA 3510C - GCMS
LCS (B9E0691-BSI)
Surrogate: 2-Fluorobiphenyl 81 32-118
Surrogate: 2-Fluo ophenol 70 20-110
Surrogate: Phenol-D5 57 8-424
Surrogate: 2,4,6-Tribroneophenol 72 39-130
Surrogate: Terphenyl-1)14 97 26-173
LCS (B9E0691-BS2)
2-Methylphenol(o-Cresol)
0.630
0.100
mg/L
0.800
79
40-110
3/4-Mcthylphenol (m,p-Cresol)
1.30
0.100
mg/L
1.60
81
40-110
2,4-Dinitrotoluene
0.506
0.100
mg/L
0.800
63
52-110
Hexachlorobenzenc
0.774
0.100
mg/L
0.800
97
52-121
Hcxachlorobutadicnc
0.558
0.100
mg/L
0.800
70
30-110
Hexachlorocthane
0.621
0.100
mg/l,
0.800
78
24-I10
Nitrobenzene
0.878
0.100
mg/L
0.800
110
36-110
Pentachlorophenol
0.516
0.100
mg/L
0.800
65
43-125
Pyridine
0.642
0.100
mg/L
0.800
80
24-110
2,4,5-Trichlorophcnol
0.512
0.100
mg/L
0.800
64
53-115
2,4,6-Tr ichlorophcnol
0.490
0.100
mg/L
0.800
61
53-110
Surrogate: Nitrobenzene-D5
83
15-314
Surrogate: 2-Fluorobiphenyl
62
32-118
Surrogate. 2-Fluorophenol
68
20-110
Surrogate. Phenol-D5
60
8-424
Surrogate: 2,4,6-Tribromopherml
82
39-130
Surrogate: Terphenyl-D14
98
26-173
LCS (B9E0691-BS3)
2-Mcthylphenol (o-Cresol)
0.0516
0.0100
mg/L
0.0800
64
40-110
3/4-Methylphcnol(m,p-Cresol)
0.124
0.0100
mg/L
0.160
77
40-110
2,4-Dinitrotolucne
0.0549
0.0100
mg/L
0.0800
69
52-110
Hexachlorobenzene
0,0660
0,0100
mg/L
0.0800
82
52-121
Hcxachlorobutadicnc
0.0431
0.0100
mg/L
0.0800
54
30-110
Hexachloroethane
0.0469
0.0100
mg/L
0.0800
59
24-110
Nitrobenzene
0.0697
0.0100
mg/L
0.0800
87
36-110
Pentachlorophenol
0.0693
0.0100
mg/L
0.0800
87
43-125
Pyridine
0.0504
0.0100
ntg/L
0,0800
63
24-110
2,4,5-Trichlorophcnol
0.0662
0.0100
tng/L
0.0800
83
53-115
2,4,6-Trichlorophenol
0.0600
0.0100
mg/L
0.0800
75
53-110
PCB Box 5655 ` Gw onviile, S" 29606
26 Fairfore.st Way
GreonvNl;.,
SC: 29637
afn 86A.232.1556
fax 864,232.61 to
rC3gersrandcallcott.com
ate errtL>ioY•:�t-�,-ob.nets company
0512812019 16.30 This report pray not be reproduced, except in fidl, without written permissionfrom Rogers & Callcott, Inc Page 13 of 211

ENV IRON MEN TA L
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B9E0691 - EPA 3510C - GCMS
LCS (B9E0691-BS3)
Surrogate: Nitrobenzene-D5
68
15-314
Surrogate:2-Fhuorobipheyl
62
32-118
Surrogate: 2-Fluorophenot
61
20-110
Surrogate: Phenol-D5
49
8-424
Surrogate. 2,4,6-Tribrotnophenol
76
39-130
Surrogate: Terphenyl-D14
115
26-173
Matrix Spike (B9E0691-MS2) Source: 9050445-01
2-Methylphenol (o-Cresol)
0.498
0 l00
mg/L
0.800
ND
62
30-110
3/4-Methylphenol (m,p-Cresol)
1.10
0.100
mg/L
1.60
ND
69
26-110
2,4-Dinitrotolucne
0.646
0.100
mg/L
0.800
ND
81
43-120
Hcxachlorobcnzcnc
0.857
0.too
mg/L
0.800
ND
t07
45-120
Hcxachlorobutadicne
0.625
0.100
mg/L
0.800
ND
78
12-110
ticxachlorocthane
0.505
0.100
mg/L
0.800
ND
63
15-110
Nitrobenzene
0.714
0.100
mg/L
0.800
ND
89
25-112
Pentachlorophcnol
0.788
0.100
mg/L
0.800
ND
99
30-140
Pyridinc
0.502
0,100
mg/L
0.800
ND
63
17-110
2,4,5-Trichlorophcnol
0.696
0.100
mg/L
0.800
ND
87
46-125
2,4,6-Trichlorophcnol
0.652
0.100
mg/L
0.800
ND
82
43-120
Surrogate: Nitrobenzene-D5
65
15-314
Surrogate: 2-Fluorobiphenyl
78
32-118
Surrogate: 2-Fhrorophenol
57
20-110
Surrogate: Phenol-D5
46
8-424
Surrogate: 2,4,6-Tribrotnophenol
100
39-130
Surrogate: Terphenyl-D14
105
26-173
PO Box 5655 C r e,, rnvillo, SC 29606 426 Faiirk)resr Vvlap Careen fll , SC 29607 ,Hain €364,232.1556 tax 861. 32.6140 ['0ge'i"Sr"1ndcallcott.com
an wmpany
0512812019 16:30 This report may not be reproduced, except in full, without written permission fronr Rogers & Callcott, Inc. page 14 of 21

1& Rogers& Callcott
F-.NVIR0NNENI TAL
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Pesticides
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch MOM - EPA 3510C - GC
Blank (B9E0848-BLKI)
Gamma-BHC (Lindanc)
ND
0.000050
mg/L
Chlordane
ND
0.00050
mg/L
Endrin
ND
0.000050
mg/L
Hcptachlor
ND
0,000050
mg/L
Hcptachlor epoxide
ND
0.000050
mg/L
Toxaphcnc
ND
0.00050
mg/L
Methoxychlor
ND
0.000050
mg/L
Surrogate:2,4,5,6-Tetrnchloro-m-sylene
85
60-130
Surrogate: Decachlorohiphenyl
69
30-150
Blank (B9E0848-BLK2)
Gamma-BHC (Lindanc)
ND
0.00050
mg/L
Chlordane
ND
0.0050
mg/L
Endrin
ND
0.00050
mg/L
Heptachlor
ND
0.00050
mg/L
Hcptachlor epoxide
ND
0.00050
mg/L
Toxaphcnc
ND
0.0050
mg/L
Methoxychlor
ND
0.00050
mg/L
Surrogate. 2,4,5,6-Tetrnchloro-na-xy1ene
86
60-130
Surrogate: Decachlorobiphenyl
86
30-150
Blank (B9E0848-BLK3)
Gamma-BHC (Lindanc)
ND
0.00050
mg/L
Chlordane
ND
0.0050
mg/L
Endrin
ND
0.00050
mg/L
Hcptachlor
ND
0,00050
mg/L
Heptachlor epoxide
ND
0.00050
mg/L
Toxaphcnc
ND
0.0050
mg/L
Mctlioxychlor
ND
0.00050
mg/L
Surrogate:2,4,5,6-Tehnchloro-nr-.cylene
88
60-130
Surrogate: Decachlorobiphenyl
72
30-150
LCS (B9E0848-BSI)
Gamma-BHC (Lindanc)
0.0037
0.00050
mg/L
0.00400
91
70-130
Endrin
0.0038
0.00050
mg/L
0,00400
96
70-130
Heptachlor
0.0034
0.00050
mg/L
0,00400
85
70-130
PO B(cx 5654 Gi c onville,
SC 29606 42/6 Fiiil arc, Way
Greenville,
SC: 29607
maIn 86423).1556
fax 864.232,6140
roge "'sandcallc tt.com
an r mploy—I owned Company
0512812019 16:30 This report may not be reproduced, except in full, without written permission f oar Rogers & Callcott, lac. Page 15 Ot 21

ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Pesticides
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B9E0848 - EPA 3510C - GC
LCS (B9E0848-BSI)
Heptachlor epoxide
0.0037
0.00050
mg/L
0.00400
94
70-130
Mcthoxychlor
0.0041
0.00050
mg/L
0.00400
103
70-130
Surrogate: 2, 4, 5, 6-Tctrcrchloro-tn-sylene
81
60-130
Surrogate: Decachlorobiphenyl
86
30-150
LCS (B9E0848-BS2)
Ganuna-BHC (Lindanc)
0.0037
0.00050
ntg/L
0.00400
93
70-130
Endrin
0.0039
0,00050
mg/L
0.00400
97
70-130
Heptachlor
0.0035
0.00050
mg/l,
0.00400
88
70-130
Hcptachlorcpoxidc
0.0038
0.00050
mg/L
0.00400
95
70-130
Mcthoxychlor
0.0042
0.00050
mg/L
0,00400
105
70-130
Surrogate: 2, 4, 5, 6-Tetrachloro-n7-.rylene
81
60-130
Surrogate: Decachlorobiphenyl
77
30-150
Matrix Spike (B9E0848-MS2)
Source: 9050445-01
Gamma-BHC (Lindane)
0.0039
0.00050
mg/L
0.00400
ND
98
60-140
Endrin
0.0040
0.00050
mg/L
0.00400
ND
99
60-140
feptachlor
0,0034
0.00050
mg/L
0,00400
ND
85
60-140
Hcptachlorcpoxidc
0.0038
0.00050
mg/L
0,00400
ND
94
60-140
Mcthoxychlor
0.0040
0.00050
mg/L
0.00400
ND
100
60-140
Surrogate. 2,4,5,6-Tetrachloro-m-sylene
86
60-130
Surrogate: Decachlorobiphenyl
67
30-150
PO Box 56 tS Greenville, SC ')1)606 426 _ atn:ure=.st Way Greerivill,, SC. 29607 rna,n 864.232.1556 fax 864.232,6140 rogersandcallcott.com
In ernpl< /e10 OMlecl cornlrJny
0512812019 16:30 This report Wray not he reproduced, except in fill, without written perutission from Rogers & Callcott, [tic. Page 16 of 21
1 g

Rogers &Callcott
FNVIRC3l MEN 'Al -
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP Bottle Extraction
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B9E0586 - EPA 1311
Blank (B9E0586-BLKI)
TCLP Bottle Extraction Complete
Blank (B9E0586-BLK2)
TCLP Bottle Extraction Complete
PCB, Bo;x 5655 Greanv;k, S' 29606 426 Riw oresC,/Vay Greenvilke, SC. 29607 864,232.1556 fax 864.232_614o rogersandcallcott.com
an ely l y.q nsvned cornpony
0512812019 16.30 This report may not be reproduced, except in fidl, without written permission from Rogers & Callcott, Inc. Page 17e 17 Of 21
L g

Rogers &Callcott
FNIVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
TCLP ZHE Extraction
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B9E0944 - EPA 1311 - ZHE
Blank (B9EO944-BLKI)
TCLP ZHE Extraction Complete
Sample Preparation Data
Parameter
Batch
Sample ID
Prepared
Analyst
EPA 3005A 1CP Digestion
EPA.3005A
139E0681
9050445-01
05/14/2019 08:47
LMC
EPA 3510 Extraction
EPA 351OC - GC
139E0848
9050445-01
05/16/2019 08:15
DBB
EPA 3510 Extraction
EPA 351OC - GCMS
B9EO691
9050445-01
05/14/2019 09:30
DBB
EPA 7470A Mercury Digestion
EPA 7470A
B9EO976
9050445-01
05/21/2019 14:06
TLT
TCLP Extraction Data
Parameter
Extraction Initial
Batch Sample ID Started Finished Fluid # pH
Final
pH
EPA 1311 - TCLP Extraction
EPA 1311
B9E0586 9050445-01 5/8/2019 at 1635 5/9/2019 at 1040 2 11.86
12.01
EPA 1311- TCLP ZHE
EPA 1311 - ZHE
139E0944 9050445-01 5/16/2019 at 1714 5/17/2019 at 1038 1 N/A
N/A
"? Box 6655 Care r=.vane, SC 29606 =126 df} re nV 11x, S�, 2'607 min 864.232.1556 fax 8i64,2 32.6mo rogersandCallcotteco9'3`t
an employ<3e-owned company
0512812019 16:30 This report may not be reproduced, except in fidl, without written permission from Rogers & Callcott, [tic. Page 18 of 21

Rogers &Callcott
Environmental Testing Solutions Project: Waynesville W WTP
351 Depot St. Work Order: 9050445
Asheville, NC 28801-4310 Reported: 05/28/19 16:30
Data Qualifiers and Definitions
ND Analyte NOT DETECTED at or above the reporting limit
NR Not reported
RPD Relative Percent Difference
PC) Box 5655 Grounville, SC 29606 426 e,m forest Way Grecnvillr., SC.. 29607 main 864.2.32,1556 ' fax [phone] rogersandc llcott.com
'In en�plcyee-r>v✓tiF <1 corrape:ny
O512812019 16:30 This report may not be reproduced, except in fidl, without written permission from Rogers & Callcott, Inc. Page 19 of 21
1 g

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to
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Total Number of Containers
Pararneter(s)
A
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Sample Receipt Verification
Date Work
Client: �� Received: �' fi Order:
Carrier Name: Client Fed( x IJPs US Mail Courier field Services Other:
— —
Tracking Number:
Receipt Criteria
e
o
A
Continents
s
Shipping container 1 cooler intact'?
Damaged Leaking Other:
Custody seats intact?
COC- included with samples?
COC signed when relinquished and received?
Sample bottles intact?
Damaged Leaking Other:
Sample 11) on COC agree with label on bottle(s)?
3
Date I time on COC agree with label on bottles)?
Number of bottles on COC agrees with number of bottles received?
�(
Samples received within holding time?
Sample volume sufficient for analysis?
VOA vials free of headspace (<6mm bubble)?
temp at receipt recorded on C'O<.'� _ ._.._....-.. __
Samples cooled?
Ice Cold Packs Dry Ice None
temp measured with tx thermometer - slvr: y7t15oo67
Samples requiring pH preservation at proper pH?
Notes Samples for metals analysis may be preserver( upon receipt in the lab.
Samples dechtorinated for parameters requiring chlorine removal at�
the time of sample collection?
Note: Chlorine checked at bench for samples requiring Bacterial, VOA, and HAA
analis.
1f in-house preservation used — record Lot i
1-lCL H3POi
F-IzsOa �� ItiaOfl
ITN03 Other
C;o ments:
Were non-conformance issues noted at sample receipt? Yes or No
Non -Conformance issue other than noted above:
Revised February 2013 Completed by:_.__
Page 21 of 21

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc®
6602 Windmill Way, Wilmington, NC 28405 - 910.391 022.3 Lab 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473 5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
info(i�environmentalchemists.com
Environmental Testing Solutions, Inc. Date of Report: May 29, 2019
Post Office Box 7565 Customer PO #:
Asheville NC 28802 Customer ID: 08100055
Attention. Kelley Keenan (ETS) Report #: 2019-07469
Project ID: Waynesville WWTP
Lab ID Sample ID: Waynesville WWTP Collect Date/Time Matrix Sampled by
19-18917 Site: 503 Lime Sludge 5/7/2019 7:41 AM Solid/Sludge Client
Test Method Results Date Analyzed
2,4,5-TP (TCLP) SW846 Method 8151A
<0.003 mg/L
05/16/2019
2,4-D (TCLP) SW846 Method 8151A
<0.003 mg/L
05/16/2019
RCI
Ignitability EPA 1030
<0.8 mm/sec
05/23/2019
Cyanide EPA 335.4
0.338 mq/kq
05/23/2019
Sulfide SiM 4500 S D
9.63 mg/kg
05/24/2019
Comment:
Reviewed by: �o
Report #:: 2019-07469 Page 1 of 1

ANALYTICAL & CONSULTING CHEMISTS
LCS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab t 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax
info(i'environmentalchemists.eoni
QC ETS- 2019-07469
Parameter
True Value
aTI giL.
Result
ingl
% True Value
Limits
Ignitability
N/A
N/A
N/A
N/A
Cyanide
0.125
0.121
97
90-110
Sulfide
0.50
0.53
106
90-110
MS/MSD
True
Recovery,
% Recovery
%
Limits %
Limits°
Parameter
Value
tngiL
mgL
Difference
Recovery
Difference
Ignitability
N/A
N/A
N/A
N/A
N/A
N/A
Cyanide
0.125
1 0.126/0.125
1 101 /100
1 1
80-120
< ?0
Sulfide
N/A
I N/A
I N/A
I N/A
I N/A
N/A
DUPLICATE SAMPLES
Parameter
Results
mg/L
% Difference
Limits
Ignitability
N/A
N/A
N/A
N/A
Cyanide
N/A
N/A
N/A
N/A
Sulfide
<0.01
<0.01
0
< 10
BLANKS
Parameter
Results,
mg/L
Limit
mg/L
Ignitability
N/A
N/A
Cyanide
<0.0025
0.0025
Sulfide
<0.005
0.005

ANALYTICAL & CONSULTING CHEMISTS
Column 1
LCS
t
6602 Windmill Way, Wilmington, NC 28405 ., 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 = 910.347.5843 Lab/Fax
infoikenvironmen taIchemist s.corn
Environmental Chemists Inc.
8151 LCS Recovery Summary
Batch 19-155
LCSD
%RPD
Compound
Spk Amt.
(ug/L)
Calc. Amt.
(ug/L)
% REC.
QC Limits
*
Calc. Amt.
(ug/L)
% REC.
QC Limits
*
40%
**
2,4-D
0.10
0.1108
111
70
-
130
0.0946
95
70
130
16
2,4,5-TP
0.10
0.1113
111
70
-
130
0.0986
99
70
130
12
Column 2
LCS
LCSD
%RPD
Compound
Spk Amt.
(ug/L)
Calc. Amt.
(ug/L)
% REC.
QC Limits
*
Calc. Amt.
(ug/L)
% REC.
QC Limits
*
40%
**
2,4-D
0.10
0.1143
114
70
130
0.0999
100
70
-
130
13
2,4,5-TP
0.10
0.1046
105
70
130
0.0932
93
70
130
12

T-14
Finvironmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 2840-5 - 910.392.0223 Lab e 910.392.4424 Fax
1
710 Bowsertown Road, Wnteo, NC 27954 -, 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists Inc.
8151 Herbicide Surrogate (DCAA) Recovery
Batch 19-155
Column I Column 2
Sample u2/L %R tjp/I %R
MB
0.2295
114.8
0.1994
99.7
LCS
0.2319
116.0
0.2012
100.6
LCSD
0.2162
108.1
0.1876
93.8
19-18917
0.2084
104.2
0.2246
112.3
Control Charts Used for control limits. Est 02272019
DCAA C1 65.36% - 144.37% DCAA C2 63.44% - 132.14%

PO Box 7565, Asheville, NC 28802
Phone: [phone], ,Pax: [phone]
Project Name
CHAIN -OF -CUSTODY l Analytical Request
Client Name:
Address:
Report to:
Phone:
l"O Number:
C l'
Fax:
Requested Analyses
rroject iNttntner:
pt-1 Checked upon Receipt
1
(7h <0--mg/1 1-pon Receipt
.�
j
!
'I Preservatives
Sample Identification
y
z
a
r
,7
,J
s
Field
--
c
i
x
.�
�`
Tcmp. (°C) Comments
t
M71
I
Company Date Time
Temperature CQ t- —_
/}
�j
Received on Ice:
Y N
y
Sealed Cooler:
Y N
Samples Intact:
Y N
Additional Comments:Sampler
Name
and Signature
Printed
Name of.SampJtl�: �
Signature of Sampler.

•
•
•
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Proiect Name:nts� t ��
CHAIN -OF -CUSTODY / Analytical Request
Client Name: ro r� p 4 r �;` 1 �� (,c� GcS T
Address:
rJ,2Ine5u IIe, /L)(- 715*7a
T5pn �-
Report to: , f
Phone: 1ba8) iJSa-q(Q85" Fax: (baS) q5'6—.10)3
PO Number:
ltenumtM Annlvicee
Project
V
Number:
pH Checked C Rtc
Preservatives
C1- < 0.2 mga Upon Reccip[
e
Sample Identification
a
o
d
0
�
?
b
'p
o
A
^�►
a
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aNJ
U
QO w
A
H
x
x z
z
Field
Temp.{°Cj Comments
503 time/sIHIg-
i 1oe191
5
5h114
-:'A`
S
J
✓
►!
✓
51 �F
6-Am"Mimlia
L
Temperature (°C) 2a .(0 WC,t��
(1 CL �. Om"
I�
8S
�T5
s 'I`g
Received
Received on Ice:
Y / N
T S
CoU i l e ✓
MMQI
y�f►'1
, 1—
1/
�—+�
09-111
v r 1
1 Oq$
Sealed Cooler:
Y N
Samples Intact:
91 N
Additional Comments: ,, 6Ce
Prince l acne of Sampler
6- w S
l�
Signature ler: