HomeMy WebLinkAboutWQ0004972_Monitoring - 03-2021_20210429Monitoring Report Submittal
............................................................................................................................................
Permit Number #* WQ0004972
Name of Facility:*
Month:* March
Report Information
Forest Lakes Preserve ELS
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
Confirmation Email Address:*
Name of Submitter:*
Signature:
Date of submittal:
Initial Review
Year:* 2021
Upload Document*
Forest Lakes_March.pdf 2.44MB
FDF Cnly
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-t, NDAR-2, NDMLR, GW-59).
Jessica. Mize@pacelabs.com
Jessica Mize
jus l oil
Reviewer: Williams, Kendall N
4/29/2021
This will be filled in automatically
Is the project number correct? * WQ0004972
Is the monitoring report r Yes r No
accepted?*
Regional Office * Winston-Salem
Accepted Date: 4/29/2021
Page I of 2
NON -DISCHARGE WASTE WATER MONITORING REPORT
PERMIT NUMBER: W00004972 MONTH: March YEAR: 2021
FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie
Flow Monitoring Point: Effluent: Influent:
Parameter Monitoring Point: Effluent: Ll Influent: ISurface Water (SW):j (SW):SW Code/Name: LJ
Was There Effluent Flow for this Month Generated At This Facility: Yes: No: Li
D
A
T
Operator
Amval
Time
2400
Gook
Operator
Timean
Sitc
ORC
on
Site?
50050
OD400
50060
o0310
00610
00530
31616
00665
00625
00630
006M
00620
703DO
00940
Daily Rate
(Flow) into
Treatment
System
pH
Residual
Chlorine
1301M
20 C
NH 3-N
TSS
Fecal
Colirorm
IGe menic
Moan-)
Total
Pham
Taal
Kjct(hal
Nitrogen
NO2-NO3
Taal
Nitrogen
Ninate
NO3-N
Taal
DissoWv
Solids
Chloride
HRS
YA
GPD
UNITS
UG,L
\IG,L
SIOL
NIU,L
',I111h1I.
710,L
NtOL
MG L
_MG LL
AIU:L
NI&I.
hIGfL
Conrinna+s
kT=ani+y
Ion= v
ont .
unt v
am y
om+y
ont y
ont v
Nimifily
3,yr
.'year
1
1510
0.25
Y
9.222
6.23
<I0
0915
0.50
Y
9,841
6.09
<10
a
1505
0.25
Y
8,073
6.17
<10
4
154;
11.511
Y
7,688
6.22
<10
5
0707
0.25
Y
7,688
6.27
<I0
a
1
110,049
71
10.049
a
1400
11.25
B
10,049
6.34
<10
v
1550
0.50
B
9.109
6.31
<10
10
1349
0.50
Y
9,287
6.30
<10
11
0730
0.25
Y
9.233
6.28
<10
12
1345
0.25
Y
10,851
6.31
<10
13
1
1
9,763
141
9.763
15
0920
0.25
1'
9,763
6.22
<10
16
0855
(1.25
Y
81822
6.19
<10
17
0900
0.50
Y
8.051
6.28
<10
7.9
45.9
19.3
44110
11.6
51.6
<0d140
51.6
<0.30
212
37.4
18
1550
0.25
B
8.360
6.31
<10
19
1510
6.25
B
8.969
6.27
<10
20
12,004
21
12,004
22
0937
0.25
Y
12,004
6.22
<10
23
1405
0.50
Y
7,530
6,21
<10
24
1422
0.50
Y
6,999
6.20
<10
25
117311
0.25
Y
7,468
6.27
<10
26
080U
0.25
Y
7,697
6.27
<10
27
8.976
28
8.976
29
1318
0.25
Y
8,976
6.24
<10
.10
17 10
0.25
B
111.255
6,19
<10
?t
1425
U.50
B
8,887
6.22
<10
Average
9.207
<10
5.
<
.6
<U,
Daily 4laximum
12,1104
6.34
<10
5.
19.3
4400
11.6
Daily Minimum
6,999
6.119
<10
7.9
45.9
19,3
440f1
11.6
<0,04U
91.6
<0,311
2t2
37.4
Manthly Urnils Is)
24400
CompositesJ! Grab (G)
Operator in Responsible Charge (ORC): Glenn Price Grade: R Phone: 336-996-2841
Check Box if ORC Has Changed ORC Certification Number: 987931/20771
Certified Laboratories (1): Pace Analytical Serivees (2):
Person(s) Collecting Samples: Glenn Price
Mail ORIGINAL and Two COPIES to:
Arm Non -Discharge Compliance Unit X o A
DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
Division of Water Quality By this signature, 1 cerfify that this report is accurate and
1617 Mail Service Center complete to the best of my knowledge.
RALEIGH, NC 27699-1617
DENR Form NDAR-1 (5/2003)
NON DISCHARGE WASTEWATER MONITORING REPORT
FACILITY STATUS:
Please answer the following question: Compliant (Y,N)
L Does all monitoring data and sampling frequencies meet permit requirements? 1 14 -J
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permitee)* Date
Baron Neal McDuffie (Authorized Agent)
(Permittee-Please print or type)
2N Riverside Plaza Suite 800
Chicago, Il 60606
(Permittee Address)
01002 Arsenic
01022 Boron
00310 BOD5
01027 Cadmium
00916 Calcium
00940 Chloride
50060 Chlorine, Total
Residual
01034 Chromium
00340 COD
31504
Coliform, Total
00094
Conductivity
01042
Copper
00300
Dissolved Oxygen
31616
Fecal Coliform
01051
Lead
00927
Magnesium
71900
Mercury
00610
NH3 as N
01067
Nickel
Baron Neal McDuffie
(Name of Signing Official -Please print or type)
Field Services Director (Pace Analytical Services)
(Position or Title)
3/31/21
(Permit Exp. Date)
00600 Nitrogen, Total
00630 NO2 & NO3
00620 NO3
00556 Oil & Grease
W 09 PAN(Plant Available
00400 pH
32730 Phenols
00665 Phosphorus, Total
00937 Potassium
00545 Settleable Matter
00929
Sodium
00931
SAR
00745
Sulfide
00515
TDS
00010
Temperature
00625
TKN
00680
TOC
00530
TSS/TSR
00076
Turbidity
01092
Zinc
Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529.
The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facilitLs permit for reporting data.
* If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D).
Page 2 of 2
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITE(S)
THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED
PERMIT NUMBER: W 004972 MONTH: March YEAR: 2021
FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie
Formulas:
Dai€y Loading {inches) _ [Volume Applied (gallons) x 0.1336 (cubic feetlgallon) x 12 (inches/foot))1 [Area Sprayed (acres) x 43.560 (square feetlacre} or
_ [Volume Applied (gallons)! [Area Sprayed (acres) x 21,152 (gallonslacre•inch).
Maximum Hourly Loading (inches) = Daily Loading (inches)! [Time irrigated (minuies)160 (minuteslhour)) Monthly Loading (inches) =Sum of Daily Loading (inches)
12 Month Floating Total (inches) = Sum of Ibis month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches}
Average Weekly Loading (inches) = [Monthly Loading (inchosimonth)1 Number of days in the month (dayslmonth )) x 7 (dayshveek)
Did Irrigation Occur At This Facility:
Yes. Na❑
Did Irrigation Occur On This Field:
Y Nv
Did Irrigation Occur On This Field:
YeEl No: ❑
Field Number:
Feld Number:
Area Sprayed (acres):
3.4
Area Sprayed (acres):
Cover Crop:
Cover Crop:
Permitted Hou
y Rate me es :
0.11
PermittedHourly Rate inches):
D
A
j'
)H+
WEATHER CONDITIONS
Storage
Lagoon
Permitted Yearly Rate (inches):
46.6
Permitted Yearly Rate (inches):
Weather
Code'
Temperature
al
arpncali,�n
Plena.
lion
V"to
ArThul
Tim,
rmt.n,il
❑ai€y
l.,a Im,
ldavmwn
Rauch
1-ding
Vol-
Appl,J
Time
1rn.• 1.1
Daily
Lnn!inF
kf
H-ly
U dillg
Fr-hanl
I'FI
aches
1111
pllms
t
I CI
48
0
3.1
2
CI
38
0
2.4
3
CI
66
0
2.2
42`480
300
0.46
0.09
4
C1
67
f1
3.2
q
R
58
1.7
3.0
6
7
C
61
0
2.3
42.480
300
0.46
11
v
C ,
72
0
3.3
In
C
69
0
3.1
11
C
60
0
2.9
33 984
240
0.37
0.09
12
PC
75
0
3.2
u
IJ
15
C1
49
0
2.6
42.480
300
0.46
1 0.09
16
Cl
39
1 II
3._*
17
1 Cl
49
f)
3.0
Is
CI
54
0
2.6
19
C
52
0
2.3
42,480
300
0.46
0.09
2n
21
C
44
11
3,il
rJ
PC
67
(1
2.ti
24
R
76
11,4
2.(,
'-s
R
5')
1).7
2.4
26
CI
57
II
T
27
28
24
PC
70
0
2.0
33,984
240
0-37
0.09
3n
C
72
II
2.4
3t
R
1.2
7a9.1 eallonalnlonmly Lwdlug it I-)
12 nloot3� FlmrinQ rural cloche.)
A,rnae 15'eekly' Lotdiol; lior6r.1
-
2.58
35.69
. _..
... �•:�
0.52
•%%valher Cade6: C-clrar, PC -parch doudr, CI -cloudy, R-rain, Se-san". SI-sleet
Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Pliant: 336-996-2841
ORC Certification Number: 987931/20771 Check Box if ORC Has Changed:
Mail ORIGINAL and Two COPIES to:
ATTN: Non -Discharge Compliance Unit X
DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
Division of Water Quality By this signature, I certify that this report is accurate and
16I7 Mail Service Center complete to the best of my knowledge.
RALEIGH, NC 27699-1617
DENR Form NDAR-1 (5/2003)
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITE(S)
FACILITY STATUS:
Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant
with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the
compliant box.)
Compliant (Y,N)
1. The application rate(s) did not exceed the limit(s) specified in the permit. I
Z Adequate measures were taken to prevent wastewater runoff from the site(s).
3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit.
4. All buffer zones as specified in the permit were maintained during each application.
5. The freeboard in the treatment and/or storage lagoon(s) was not less than the
limit(s) specified in the permit.
If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
4 cad ( Baron Neal McDuffie
(Signature of Permitee)* Date (Name of Signing Official -Please print or type)
Baron Neal McDuffie (Authorized Agent)
(Permittee-Please print or type)
2N. Riverside Plaza Suite 800
Chicago, II 60606
(Permittee Address)
Field Services Director (Pace Analytical Services)
(Position or Title)
3/31/2021
(Permit Exp. Date)
* If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D).
1�zAnalytical"
www.pacelahs.ram
April 05, 2021
Tracy Overdurf
Forest Lake
192 Thousand Trails Dr.
Advance, NC 27006
RE: Project: Forest Lake MWIEffllnf
Pace Project No.: 92528275
Dear Tracy Overdurf:
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
{704)977-0981
Enclosed are the analytical results for sample(s) received by the laboratory on March 17, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
stephanie.knott@pacelabs.com
704-977-0981
Project Manager
Enclosures
�47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuil.
without the written consent of Pace Analytical Services, LLC.
Page 1 of 26
a 147oilAnalyfi0
cal
WmPacelabs.com
Project: Forest Lake MW/Efflinf
Pace Project No.: 92528275
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/N ELAP Certification # LA1 70028
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification 37712
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky LIST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fu[1,
without the written consent of Pace Analytical Services, I.I.C.
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Page 2 of 26
1�5a'uceAnalyfical
j www.pacolabs.com
I
SAMPLE ANALYTE COUNT
Project: Forest Lake MW/Effilnf
Pace Project No.: 92528275
Pace Analytical Services, LLC
1377 South Park Drive
Kernersvtlle. NC 27284
(704)977-0981
Lab ID
Sample ID
Method
Analysts
Analyses
Reported
Laboratory
92528275001
MW-1
HACH 10206
AMI
1
PASI-E
SM 9222D-2006
AMI
1
PASI-E
EPA 300.0 Rev 2.1 1993
JLH
1
PASI-A
SM 531OB-2011
ECH
1
PASI-A
92528275002
MW-2
HACH 10206
AMI
1
PASI-E
SM 9222D-2006
AMI
1
PASI-E
EPA 300.0 Rev 2.1 1993
JLH
1
PASI-A
SM 531OB-2011
ECH
1
PASI-A
92528275003
MW-3
HACH 10206
AMI
1
PASI-E
SM 9222D-2006
AMI
1
PASI-E
EPA 300.0 Rev 2.1 1993
JLH
1
PASI-A
SM 531 OB-2011
ECH
1
PASI-A
92528275004
MW-4
HACH 10206
AMI
1
PASI-E
SM 9222D-2006
AMI
1
PASI-E
EPA 300.0 Rev 2.1 1993
JLH
1
PASI-A
SM 531OB-2011
ECH
1
PASI-A
92528275005
Effluent
HACH 10206
AMI
1
PASI-E
SM 254OC-2011
MLS1
1
PASI-E
SM 254OD-2011
MLS1
1
PASI-E
SM 521OB-2011
MWF
1
PASI-E
SM 92220-2006
AMI
1
PASI-E
TKN+NO3+NO2 Calculation
EWS
1
PASI-A
EPA 300.0 Rev 2.1 1993
JLH
1
PASI-A
EPA 350.1 Rev 2.0 1993
NAL
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA353.2 Rev 2.0 1993
KDF1
1
PASI-A
EPA 365.1 Rev 2.0 1993
MFO
1
PASI-A
92528275006
Influent
SM 254OC-2011
MLS1
1
PASI-E
SM 254OD-2011
MLS1
1
PASI-E
SM 521OB-2011
MWF
1
PASI-E
EPA 1664B
CJM
1
PASI-C
TKN+NO3+NO2 Calculation
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993
NAL
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
1
PASI-A
EPA 365.1 Rev 2.0 1993
MFO
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C. Page 3 of 26
aceAnalj cal
www.pocelabs.com
1
,
Project: Forest Lake MWlEffllnf
Pace Project No.: 92528275
Lab ID Sample ID
PAST -A = Pace Analytical Services -Asheville
PAST-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
SAMPLE ANALYTE COUNT
Analytes
Method Analysts Reported Laboratory
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 26
/5a'ceAna1j6ca1'
i www.pacelabs.com
1
ANALYTICAL RESULTS
Project: Forest Lake MW/Eff/lnf
Pace Project No.: 92528275
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: MWA
Lab ID: 92528275001 Collected: 03/17/21 08:54
Received: 03/17121 12:30 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
HACH 10206 Nitrogen, Nitrate
Analytical Method: HACH 10206
Pace Analytical Services - Eden
Nitrogen, Nitrate
ND mg/L 0.30
1
03/17/21 17:46
14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/17/21 14:40 03/18/21 15:14
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
1.1 mg/L 1.0
1
03/21/2121:28
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon
2.5 mg/L 1.0
1
04/03/21 16:31
7440-44-0
Date: 04/05/2021 03:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 26
58CeAnalytical
1�1( www.pacelabsxom
I
ANALYTICAL RESULTS
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
Pace Analytical Services, LLC
1377 South Park Drive
Kemersvilie, NC 27284
(704)977-0981
Sample: MW-2
Parameters
Lab ID: 92528275002 Collected: 03/17/21 08:24
Results Units Report Limit OF
Received: 03/17/21 12:30 Matrix: Water
Prepared Analyzed CAS No. Qual
HACH 10206 Nitrogen, Nitrate
Analytical Method: HACH 10206
Pace Analytical Services - Eden
Nitrogen, Nitrate
0.96 mg/L 0.30 1
03/17/21 17.47
14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2006 Preparation Method: SM 922213-2006
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU/100 mL 1.0 1
03/17/21 14:40 03/18/21 15:14
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
5.1 mg/L 1.0 1
03/21/2122:09
16887-00-6
5310E TOC
Analytical Method: SM 531 OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon
NO mg/L 1.0 1
04/03121 16:51
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 26
1C0
eAnalXical
www.pacelabs.com
i
i
ANALYTICAL RESULTS
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: MW-3 Lab ID: 92528275003 Collected: 03/17/21 07:47 Received: 03/17/21 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206
Pace Analytical Services - Eden
Nitrogen, Nitrate 8.5 mg/L 0.30 1 03/17/21 17:47 14797-55-8
MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services - Eden
Fecal Coliforms 13.0 CFU1100 mL 1.0 1 03/17/21 14:40 03/18/21 15:14
300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride 26.8 mg/L 1.0 1 03121/2122:22 16887-00-6
5310E TOC Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1.0 1 04/03/21 17:09 744044-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 26
aceAnalXical
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1
ANALYTICAL RESULTS
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville. NC 27284
(704)977-0981
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
Sample: MW-4 Lab ID: 92528275004 Collected: 03/17/21 08:08 Received: 03/17/21 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
HACH 10206 Nitrogen, Nitrate
Analytical Method: HACH 10206
Pace Analytical Services - Eden
Nitrogen, Nitrate
ND mg/L 0.30 1
03/17/21 17:47 14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services - Eden
Fecal Coliforms
NO CFU/100 mL 1.0 1
03/17/21 14:40 03/18/21 15:14
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
3.4 mg/L 1.0 1
03/21/2122:36 16887-00-6
5310E TOC
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0 1
04/03/21 17:29 7440-44-0
Date: 04/05/2021 03:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.L.C.
Page 8 of 26
Pace Analytical Services, LLC
1�55'ceAnalytical m 1377 South Park Drive
Kemersville, NC 27284
www.pacelabs.com (704)977-0981
i
f
ANALYTICAL RESULTS
Project: Forest Lake MW/Efflinf
Pace Project No.: 92528275
Sample: Effluent
Parameters
Lab ID: 92528275005 Collected: 03/17/21 08:33
Results Units Report Limit DF
Received: 03/17/21 12:30 Matrix: Water
Prepared Analyzed CAS No. Dual
HACH 10206 Nitrogen, Nitrate
Analytical Method: HACH 10206
Pace Analytical Services - Eden
Nitrogen, Nitrate
ND mg/L 0.30 1
03/17121 17:46 14797-55-8
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services - Eden
Total Dissolved Solids
212 mg/L 25.0 1
03/18/21 13:49
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Eden
Total Suspended Solids
19.3 mg/L 8.3 1
03/18/21 08:48
5210E BOD, 5 day EDN
Analytical Method: SM 521OB-2011 Preparation Method: SM 521OB-2011
Pace Analytical Services - Eden
BOD, 5 day
7.9 mg/L 2.0 1
03/18/21 10:27 03/23/21 10:29 R6
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 922213-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services - Eden
Fecal Coliforms
4400 CFU/100 mL 1.0 1
03/17/21 14:40 03/18/21 15:14
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Total Nitrogen
51.6 mg/L 0.52 1
03/25/21 15:39
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
37.4 mg/L 1.0 1
03121/2122:49 16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
45.6 mg/L 1.0 10
03/28/21 13:57 766441-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
51.6 mg/L 2.5 5
03/24/21 21:35 03/25/21 06:16 7727-37-9
353.2 Nitrogen, N021NO3 pres.
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/L 0.040 1
03/25/21 10:28 M1
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
11.6 mg/L 0.25 5
03/29121 17:40 03/30/2102:20 7723-14-0 M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 26
/5a'ceAnalyfical'
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i
ANALYTICAL RESULTS
Project: Forest Lake MW/Effllnf
Pace Project No.: 92528275
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: Influent
Lab ID: 92528275006 Collected: 03117/21 08:39
Received: 03/17/21 12:30 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Dual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services - Eden
Total Dissolved Solids
225 mg/L 25.0 1
03/18/21 13:49
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Eden
Total Suspended Solids
132 mg/L 25.0 1
03/18/21 08:49
5210B BOD, 5 day EON
Analytical Method: SM 521 OB-2011 Preparation Method: SM 5210B-2011
Pace Analytical Services - Eden
BOD, 5 day
195 mg/L 2.0 1
03/18/21 10:27 03/23/21 10:31
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease
18.7 mg/L 5.0 1
03/30/21 13:13
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Total Nitrogen
52.6 mg/L 0.52 1
03/25/21 15:39
350.1 Ammonia
Analytical Method: EPA350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
37.2 mg/L 1.0 10
03/28/21 15:29 7664- 1-7 M6
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
52.4 mg/L 2.5 5
03/24/21 21:35 03/25121 06:17 7727-37-9
353.2 Nitrogen, NO2/NO3 pros.
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, NO2 plus NO3
0.20 mg/L 0.040 1
03/25/21 10:34 M1
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.01993
Pace Analytical Services -Asheville
Phosphorus
10.6 mg/L 0.25 5
03/2912117:40 03/30/21 02:22 7723-14-0
Date: 04/05/2021 03:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.L.C.
Page 10 of 26
1�5acIeAnalyticalo
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t
QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
QC Batch: 607369 Analysis Method: HACH 10206
QC Batch Method: HACH 10206 Analysis Description: 10206 Nitrogen, Nitrate
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005
METHOD BLANK: 3199828 Matrix: Water
Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L NO 0.30 03/17/21 17:43
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
LABORATORY CONTROL SAMPLE: 3199829
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 5 5.1 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3199830 3199831
MS MSD
92527185017 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L NO 5 5 5.0 5.0 100 100 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3199905 3199906
MS MSD
92527185018 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen. Nitrate mg/L ND 5 5 5.0 5.0 100 100 90-110 0
Results presented on this page are in the units Indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 26
aceAnalytical
r www.patelabs.eom
f
QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
QC Batch: 607644 Analysis Method: SM 254OC-2011
QC Batch Method: SM 254OC-2011 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92528275005, 92528275006
METHOD BLANK: 3201017 Matrix: Water
Associated Lab Samples: 92528275005, 92528275006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L ND 25.0 03/18/21 13:49
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
LABORATORY CONTROL SAMPLE: 3201018
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids mg/L 250 236 94 90-110
SAMPLE DUPLICATE: 3201019
92527772001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Dissolved Solids
mg/L
510
514 1
SAMPLE DUPLICATE: 3201020
92527777001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Dissolved Solids
mg/L
ND
ND
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04105/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 26
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f
QUALITY CONTROL DATA
Project: Forest Lake MW/Effllnf
Pace Project No.: 92528275
QC Batch: 607482 Analysis Method: SM 254OD-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92528275005, 92528275006
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville. NC 27284
(704)977.0981
METHOD BLANK: 3200298 Matrix: Water
Associated Lab Samples: 92528275005, 92528275006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 03/18/21 08:44
LABORATORY CONTROL SAMPLE: 3200299
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 252 101 90-110
SAMPLE DUPLICATE: 3200300
92528276001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 343 255 30 D6
SAMPLE DUPLICATE: 3200301
92528164001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 371 367 1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 26
/5a'ceAna/jdica1 QD
J wpw.pacelabs.com
i
QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
QC Batch: 607502 Analysis Method: SM 5210B-2011
QC Batch Method: SM 521OB-2011 Analysis Description: 5210E BOD, 5 day Final EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92528275005, 92528275006
METHOD BLANK: 3200368 Matrix: Water
Associated Lab Samples: 92528275005, 92528275006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
BOD, 5 day mg1L ND 2.0 03/23/21 10:10
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977.0981
LABORATORY CONTROL SAMPLE: 3200369
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 226 114 84.6-115.4
SAMPLE DUPLICATE: 3200371
92528042002 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg1L 116 114 2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date. 04105/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 26
5ac ie A na ly No / a
7 www.pacelabs.eom
I
QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
QC Batch: 607404 Analysis Method: SM 9222D-2006
QC Batch Method: SM 92220-2006 Analysis Description: 9222D Fecal Coliform( MF)-EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005
METHOD BLANK: 3200119 Matrix: Water
Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL NO 1.0 03/18/21 15:14
SAMPLE DUPLICATE: 3200120
92528275003 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFU/100 mL 13.0 13.0 0
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04105/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 26
/5a'ceAnalXicalo
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r`
QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
QC Batch: 610185 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92528275006
METHOD BLANK: 3213147
Associated Lab Samples: 92528275006
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 3213148
Parameter Units
Oil and Grease mg/L
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 03/30/2113:13
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
40 35.3 88 78-114
MATRIX SPIKE SAMPLE: 3213149
35620840001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 23.6 40 14.9 -22 78-114 M1
Results presented on this page are In the units Indicated by the "Units" column except where an attemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, I.I.C.
Page 16 of 26
aceAnalytical
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,
QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
QC Batch: 607984 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005
METHOD BLANK: 3202745 Matrix: Water
Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg1L ND 1.0 03/21/2119:26
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
LABORATORY CONTROL SAMPLE: 3202746
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chloride mg1L 50 52.2 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3202747 3202748
MS MSD
92527234030 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L ND 50 50 51.8 50.4 104 101 90-110 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3202749 3202750
MS MSD
92527612006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 1.6 50 50 52.6 51.8 102 100 90-110 1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 26
1�5a'cmnalyficalm
tvtrw.pacelabs.eom
f
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
QC Batch: 609781
QC Batch Method: EPA 350.1 Rev 2.0 1993
Associated Lab Samples: 92528275005
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
METHOD BLANK: 3211656 Matrix: Water
Associated Lab Samples: 92528275005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.10 03/28/21 13:14
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville. NC 27284
(704)977-0981
LABORATORY CONTROL SAMPLE: 3211657
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/L 5 4.9 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211658 3211659
MS MSD
92525439002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L NO 5 5 5.3 5.3 106 106 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211660 3211661
MS MSD
92528059006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L ND 5 5 5.2 5.2 103 103 90-110 0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 26
1eAnalj6cals
www.pacelabs.cam
QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
Pace Analytical Services, LLC
1377 South Park Drive
Kemersvilie, NC 27284
(704)977.0981
QC Batch: 609784
Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92528275006
METHOD BLANK: 3211674
Matrix: Water
Associated Lab Samples: 92528275006
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/L
ND 0.10
03/28/21 13:58
LABORATORY CONTROL SAMPLE: 3211675
Spike LCS
LCS % Rae
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Nitrogen, Ammonia mg/L
5 4.8
97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211676 3211677
MS MSD
92527508015
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone, Cone. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/L 0.032J
5 5 5.2
5.2 103 103
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211678 3211679
MS MSD
92528275006
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/L 37.2
5 5 42.6
42.8 108 112
90-110 1 M6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 26
1�5a'ne Analytical
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,
QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 608921
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92528275005, 92528275006
METHOD BLANK: 3207313
Matrix: Water
Associated Lab Samples: 92528275005, 92528275006
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/L
ND 0.50
03/25/21 05:06
LABORATORY CONTROL SAMPLE: 3207314
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg1L
10 9.4
94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3207315 3207316
MS MSD
92528244003
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Oual
Nitrogen, Kjeldahl, Total mg/L 18A
10 10 45.3
45.8 269 274
90-110 1 M1
MATRIX SPIKE 8, MATRIX SPIKE DUPLICATE: 3207317 3207318
MS MSD
92528268001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 1.5
10 10 23.8
26.7 223 252
90-110 11 M1,R1
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 26
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QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 609118 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved
Laboratory: PaceAnalyticalServices-Asheville
Associated Lab Samples: 92528275005, 92528275006
METHOD BLANK: 3208246 Matrix: Water
Associated Lab Samples: 92528275005, 92528275006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L ND 0.040 03/25/21 10:25
LABORATORY CONTROL SAMPLE: 3208247
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3208250 3208251
MS MSD
92528275005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 1.7 1.7 66 65 90-110 2 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3208261 3208262
MS MSD
92528275006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.20 2.5 2.5 2.4 2.4 89 89 90-110 0 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, I.I.C.
Page 21 of 26
aceAnalytical"
www.pacelaba.ccm
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
QC Batch: 610010
QC Batch Method: EPA 365.1 Rev 2.0 1993
Associated Lab Samples: 92528275005, 92528275006
METHOD BLANK: 3212591
Associated Lab Samples: 92528275005, 92528275006
Parameter Units
Phosphorus mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.050 0313012101:27
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
LABORATORY CONTROL SAMPLE: 3212592
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/L 2.5 2.5 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3212593 3212594
MS MSD
92528268001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 0.13 2.5 2.5 2.6 2.6 100 99 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3212595 3212596
MS MSD
92528275005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 11.6 2.5 2.5 15.6 15.3 161 151 90-110 2 M1
Results presented an this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 26
acmnalytical m
www,pacelabs.com
QUALITY CONTROL DATA
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
QC Batch: 611248 Analysis Method: SM 531OB-2011
QC Batch Method: SM 5310E-2011 Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004
METHOD BLANK: 3218336 Matrix: Water
Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L ND 1.0 04/03/21 08.44
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
LABORATORY CONTROL SAMPLE: 3218337
Spike LCS LCS % Rec
Parameter Units Conc. Result efo Rec Limits Qualifiers
Total Organic Carbon mg/L 25 24.2 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3218338 3218339
MS MSD
92527508001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec efo Rec Limits RPD Qual
Total Organic Carbon mg/L 23.1 25 25 47.1 47.0 96 95 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3218340 3218341
MS MSD
92527508011 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 25.4 25 25 49.5 49.5 96 96 90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, I.L.C.
Page 23 of 26
Pace Analytical Services, LLC
a 1377 South Park Drive
aceAnalytical Kemersvllie, NC 27284
www.pacelaba.ccm (704)977-0981
E
QUALIFIERS
Project: Forest Lake MW/Eff/Inf
Pace Project No.: 92528275
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte In a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current fist of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
R6 The RPD between valid sample dilutions exceeded 30%.
REPORT OF LABORATORY ANALYSIS
This report shall not to reproduced, except in full.
Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 26
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Forest Lake MWtEffllnf
Pace Project No.: 92528275
Lab ID
92528275001
92528275002
92528275003
92528275004
92528275005
92528275005
92528275006
92528275005
92528275006
92528275005
92628275006
92528276001
92528275002
92528275003
92528275004
92528275005
92528275006
92528275005
92528275006
92528275001
92528275002
92528275003
92528275004
92528275005
92528275005
92528275006
92628275005
92528275006
92628276005
92528275006
92528275005
92528275006
92528275001
92528275002
92528275003
92528275004
Sample ID
MW-1
MW-2
MW3
MW-4
Effluent
Effluent
Influent
Effluent
Influent
Effluent
Influent
MW4
MW-2
MW3
MW-4
Effluent
Influent
Effluent
Influent
MW-1
MW-2
MW3
MW-4
Effluent
Effluent
Influent
Effluent
Influent
Effluent
Influent
Effluent
Influent
MW-1
MW 2
MW3
MW-4
Date: 04/05/2021 03:15 PM
QC Batch Method
HACH 10206
HACH 10206
HACH 10206
HACH 10206
HACH 10206
SM 2WC-2011
SM 254OC-2011
SM 254OD-2011
SM 254OD-2011
SM 521 OB-2011
SM 521 OB-2011
SM 9222D-2006
SM 9222D-2006
SM 9222D-2006
SM 9222D-2006
SM 9222D-2006
EPA1664B
TKN+NO3+NO2
Calculation
TKN+NO3+NO2
Calculation
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
SM 531OB-2011
SM 531OB-2011
SM 531OB-2011
SM 531 OB-2011
QC Batch
607369
607369
607369
607369
607369
607644
607644
607482
607482
607502
607502
607404
607404
607404
607404
607404
610185
609314
609314
607984
607984
607984
607984
607984
609781
609784
608921
608921
609118
609118
610010
610010
611248
611248
611248
611248
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Analytical Method
SM 521OB-2011
SM 521OB-2011
SM 9222D-2006
SM 9222D-2006
SM 9222D-2006
SM 9222D-2006
SM 9222D-2006
Analytical
Batch
607559
607559
607405
607405
607405
607405
607405
EPA 351.2 Rev 2.0 1993 609092
EPA 351.2 Rev 2.0 1993 609092
EPA 365.1 Rev 2.0 1993 610095
EPA 365.1 Rev 2.0 1993 610095
Page 25 of 26
Allaly,#IGai ' CHAIN -OF -CUSTODY Analytical Request Document
Chain of -Custody 3s a LEGAL DOCUMENT - Cumpletu all re)event fields
Forest Lakes 1811iinglnforrnation:
Report To:
Emal l To:
Copy Tm
She Coliecticin Info/Address-
Customer Project Name/Number:
State: County/City: Time Tone Collected:
1 [ JPTI 1MT( ICT [ JET
Phone:
Site/Facility ID #.
Compliance Monitoring?
Email:
[ /Yes [ IN.
Collected By vrint):
Purchase order 8:
Ow pWS ID III:�
Quote rf:
Dw Location Code:
Collected By (signature):
Turnaround Bate Sequined:
Imme rate y Pace on Ice:
r
[ ] Yes I IN
Sample Disposal:
Rush:
Fieid Filtered (if applicable):
I I Dispose as appropriate I I Retum
I j SamP Day [ I Next Day
I I Yes [ ]No
I I Archive:
() 2 Day 1 13 Day [ 14 Day (15 Day
I ) Hold:_
(Expedite Charges Apply)
Analysis:
" Matrix Codes (Insert in Matrix box below): Drinking Water(DW), Ground Water (GW), Wastewater(Ww),
Product (11), Soil/Solid (SQ, O)I (OL), Wipe (WPI, Air (AR), Tissue (TS), Bioassay (B), Vapor M, Other (OT(
CustomCrSample fD
Matrix •
Comp /
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Groundwater Monitoring
Relinquished by/Company: (Signature) pF
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(6) methanol, 17) sodium Wsuefete, (9) sodium thlosulfate, (9j hexi)ne, (A) ascorbic acid, (B) ammunium sullare,
tC) ammonium hydroxide, (D) TSP, (U) Unpreserved, (D) other
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