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HomeMy WebLinkAboutWQ0004972_Monitoring - 03-2021_20210429Monitoring Report Submittal ............................................................................................................................................ Permit Number #* WQ0004972 Name of Facility:* Month:* March Report Information Forest Lakes Preserve ELS Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter:* Signature: Date of submittal: Initial Review Year:* 2021 Upload Document* Forest Lakes_March.pdf 2.44MB FDF Cnly Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-t, NDAR-2, NDMLR, GW-59). Jessica. Mize@pacelabs.com Jessica Mize jus l oil Reviewer: Williams, Kendall N 4/29/2021 This will be filled in automatically Is the project number correct? * WQ0004972 Is the monitoring report r Yes r No accepted?* Regional Office * Winston-Salem Accepted Date: 4/29/2021 Page I of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W00004972 MONTH: March YEAR: 2021 FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie Flow Monitoring Point: Effluent: Influent: Parameter Monitoring Point: Effluent: Ll Influent: ISurface Water (SW):j (SW):SW Code/Name: LJ Was There Effluent Flow for this Month Generated At This Facility: Yes: No: Li D A T Operator Amval Time 2400 Gook Operator Timean Sitc ORC on Site? 50050 OD400 50060 o0310 00610 00530 31616 00665 00625 00630 006M 00620 703DO 00940 Daily Rate (Flow) into Treatment System pH Residual Chlorine 1301M 20 C NH 3-N TSS Fecal Colirorm IGe menic Moan-) Total Pham Taal Kjct(hal Nitrogen NO2-NO3 Taal Nitrogen Ninate NO3-N Taal DissoWv Solids Chloride HRS YA GPD UNITS UG,L \IG,L SIOL NIU,L ',I111h1I. 710,L NtOL MG L _MG LL AIU:L NI&I. hIGfL Conrinna+s kT=ani+y Ion= v ont . unt v am y om+y ont y ont v Nimifily 3,yr .'year 1 1510 0.25 Y 9.222 6.23 <I0 0915 0.50 Y 9,841 6.09 <10 a 1505 0.25 Y 8,073 6.17 <10 4 154; 11.511 Y 7,688 6.22 <10 5 0707 0.25 Y 7,688 6.27 <I0 a 1 110,049 71 10.049 a 1400 11.25 B 10,049 6.34 <10 v 1550 0.50 B 9.109 6.31 <10 10 1349 0.50 Y 9,287 6.30 <10 11 0730 0.25 Y 9.233 6.28 <10 12 1345 0.25 Y 10,851 6.31 <10 13 1 1 9,763 141 9.763 15 0920 0.25 1' 9,763 6.22 <10 16 0855 (1.25 Y 81822 6.19 <10 17 0900 0.50 Y 8.051 6.28 <10 7.9 45.9 19.3 44110 11.6 51.6 <0d140 51.6 <0.30 212 37.4 18 1550 0.25 B 8.360 6.31 <10 19 1510 6.25 B 8.969 6.27 <10 20 12,004 21 12,004 22 0937 0.25 Y 12,004 6.22 <10 23 1405 0.50 Y 7,530 6,21 <10 24 1422 0.50 Y 6,999 6.20 <10 25 117311 0.25 Y 7,468 6.27 <10 26 080U 0.25 Y 7,697 6.27 <10 27 8.976 28 8.976 29 1318 0.25 Y 8,976 6.24 <10 .10 17 10 0.25 B 111.255 6,19 <10 ?t 1425 U.50 B 8,887 6.22 <10 Average 9.207 <10 5. < .6 <U, Daily 4laximum 12,1104 6.34 <10 5. 19.3 4400 11.6 Daily Minimum 6,999 6.119 <10 7.9 45.9 19,3 440f1 11.6 <0,04U 91.6 <0,311 2t2 37.4 Manthly Urnils Is) 24400 CompositesJ! Grab (G) Operator in Responsible Charge (ORC): Glenn Price Grade: R Phone: 336-996-2841 Check Box if ORC Has Changed ORC Certification Number: 987931/20771 Certified Laboratories (1): Pace Analytical Serivees (2): Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: Arm Non -Discharge Compliance Unit X o A DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, 1 cerfify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant (Y,N) L Does all monitoring data and sampling frequencies meet permit requirements? 1 14 -J If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitee)* Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza Suite 800 Chicago, Il 60606 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31/21 (Permit Exp. Date) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN(Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facilitLs permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W 004972 MONTH: March YEAR: 2021 FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie Formulas: Dai€y Loading {inches) _ [Volume Applied (gallons) x 0.1336 (cubic feetlgallon) x 12 (inches/foot))1 [Area Sprayed (acres) x 43.560 (square feetlacre} or _ [Volume Applied (gallons)! [Area Sprayed (acres) x 21,152 (gallonslacre•inch). Maximum Hourly Loading (inches) = Daily Loading (inches)! [Time irrigated (minuies)160 (minuteslhour)) Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of Ibis month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches} Average Weekly Loading (inches) = [Monthly Loading (inchosimonth)1 Number of days in the month (dayslmonth )) x 7 (dayshveek) Did Irrigation Occur At This Facility: Yes. Na❑ Did Irrigation Occur On This Field: Y Nv Did Irrigation Occur On This Field: YeEl No: ❑ Field Number: Feld Number: Area Sprayed (acres): 3.4 Area Sprayed (acres): Cover Crop: Cover Crop: Permitted Hou y Rate me es : 0.11 PermittedHourly Rate inches): D A j' )H+ WEATHER CONDITIONS Storage Lagoon Permitted Yearly Rate (inches): 46.6 Permitted Yearly Rate (inches): Weather Code' Temperature al arpncali,�n Plena. lion V"to ArThul Tim, rmt.n,il ❑ai€y l.,a Im, ldavmwn Rauch 1-ding Vol- Appl,J Time 1rn.• 1.1 Daily Lnn!inF kf­ H-ly U dillg Fr-hanl I'FI aches 1111 pllms t I CI 48 0 3.1 2 CI 38 0 2.4 3 CI 66 0 2.2 42`480 300 0.46 0.09 4 C1 67 f1 3.2 q R 58 1.7 3.0 6 7 C 61 0 2.3 42.480 300 0.46 11 v C , 72 0 3.3 In C 69 0 3.1 11 C 60 0 2.9 33 984 240 0.37 0.09 12 PC 75 0 3.2 u IJ 15 C1 49 0 2.6 42.480 300 0.46 1 0.09 16 Cl 39 1 II 3._* 17 1 Cl 49 f) 3.0 Is CI 54 0 2.6 19 C 52 0 2.3 42,480 300 0.46 0.09 2n 21 C 44 11 3,il rJ PC 67 (1 2.ti 24 R 76 11,4 2.(, '-s R 5') 1).7 2.4 26 CI 57 II T 27 28 24 PC 70 0 2.0 33,984 240 0-37 0.09 3n C 72 II 2.4 3t R 1.2 7a9.1 eallonalnlonmly Lwdlug it I-) 12 nloot3� FlmrinQ rural cloche.) A,rnae 15'eekly' Lotdiol; lior6r.1 - 2.58 35.69 . _.. ... �•:� 0.52 •%%valher Cade6: C-clrar, PC -parch doudr, CI -cloudy, R-rain, Se-san". SI-sleet Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Pliant: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 16I7 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. I Z Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. 5. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4 cad ( Baron Neal McDuffie (Signature of Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N. Riverside Plaza Suite 800 Chicago, II 60606 (Permittee Address) Field Services Director (Pace Analytical Services) (Position or Title) 3/31/2021 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). 1�zAnalytical" www.pacelahs.ram April 05, 2021 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lake MWIEffllnf Pace Project No.: 92528275 Dear Tracy Overdurf: Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 {704)977-0981 Enclosed are the analytical results for sample(s) received by the laboratory on March 17, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures �47 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuil. without the written consent of Pace Analytical Services, LLC. Page 1 of 26 a 147oilAnalyfi0 cal WmPacelabs.com Project: Forest Lake MW/Efflinf Pace Project No.: 92528275 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/N ELAP Certification # LA1 70028 North Carolina Drinking Water Certification M 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification 37712 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky LIST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fu[1, without the written consent of Pace Analytical Services, I.I.C. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Page 2 of 26 1�5a'uceAnalyfical j www.pacolabs.com I SAMPLE ANALYTE COUNT Project: Forest Lake MW/Effilnf Pace Project No.: 92528275 Pace Analytical Services, LLC 1377 South Park Drive Kernersvtlle. NC 27284 (704)977-0981 Lab ID Sample ID Method Analysts Analyses Reported Laboratory 92528275001 MW-1 HACH 10206 AMI 1 PASI-E SM 9222D-2006 AMI 1 PASI-E EPA 300.0 Rev 2.1 1993 JLH 1 PASI-A SM 531OB-2011 ECH 1 PASI-A 92528275002 MW-2 HACH 10206 AMI 1 PASI-E SM 9222D-2006 AMI 1 PASI-E EPA 300.0 Rev 2.1 1993 JLH 1 PASI-A SM 531OB-2011 ECH 1 PASI-A 92528275003 MW-3 HACH 10206 AMI 1 PASI-E SM 9222D-2006 AMI 1 PASI-E EPA 300.0 Rev 2.1 1993 JLH 1 PASI-A SM 531 OB-2011 ECH 1 PASI-A 92528275004 MW-4 HACH 10206 AMI 1 PASI-E SM 9222D-2006 AMI 1 PASI-E EPA 300.0 Rev 2.1 1993 JLH 1 PASI-A SM 531OB-2011 ECH 1 PASI-A 92528275005 Effluent HACH 10206 AMI 1 PASI-E SM 254OC-2011 MLS1 1 PASI-E SM 254OD-2011 MLS1 1 PASI-E SM 521OB-2011 MWF 1 PASI-E SM 92220-2006 AMI 1 PASI-E TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 300.0 Rev 2.1 1993 JLH 1 PASI-A EPA 350.1 Rev 2.0 1993 NAL 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MFO 1 PASI-A 92528275006 Influent SM 254OC-2011 MLS1 1 PASI-E SM 254OD-2011 MLS1 1 PASI-E SM 521OB-2011 MWF 1 PASI-E EPA 1664B CJM 1 PASI-C TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 350.1 Rev 2.0 1993 NAL 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MFO 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 3 of 26 aceAnalj cal www.pocelabs.com 1 , Project: Forest Lake MWlEffllnf Pace Project No.: 92528275 Lab ID Sample ID PAST -A = Pace Analytical Services -Asheville PAST-C = Pace Analytical Services - Charlotte PASI-E = Pace Analytical Services - Eden Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 SAMPLE ANALYTE COUNT Analytes Method Analysts Reported Laboratory REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 26 /5a'ceAna1j6ca1' i www.pacelabs.com 1 ANALYTICAL RESULTS Project: Forest Lake MW/Eff/lnf Pace Project No.: 92528275 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MWA Lab ID: 92528275001 Collected: 03/17/21 08:54 Received: 03/17121 12:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg/L 0.30 1 03/17/21 17:46 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1.0 1 03/17/21 14:40 03/18/21 15:14 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 1.1 mg/L 1.0 1 03/21/2121:28 16887-00-6 5310B TOC Analytical Method: SM 531OB-2011 Pace Analytical Services -Asheville Total Organic Carbon 2.5 mg/L 1.0 1 04/03/21 16:31 7440-44-0 Date: 04/05/2021 03:15 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 26 58CeAnalytical 1�1( www.pacelabsxom I ANALYTICAL RESULTS Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 Pace Analytical Services, LLC 1377 South Park Drive Kemersvilie, NC 27284 (704)977-0981 Sample: MW-2 Parameters Lab ID: 92528275002 Collected: 03/17/21 08:24 Results Units Report Limit OF Received: 03/17/21 12:30 Matrix: Water Prepared Analyzed CAS No. Qual HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206 Pace Analytical Services - Eden Nitrogen, Nitrate 0.96 mg/L 0.30 1 03/17/21 17.47 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2006 Preparation Method: SM 922213-2006 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1.0 1 03/17/21 14:40 03/18/21 15:14 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 5.1 mg/L 1.0 1 03/21/2122:09 16887-00-6 5310E TOC Analytical Method: SM 531 OB-2011 Pace Analytical Services -Asheville Total Organic Carbon NO mg/L 1.0 1 04/03121 16:51 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 26 1C0 eAnalXical www.pacelabs.com i i ANALYTICAL RESULTS Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MW-3 Lab ID: 92528275003 Collected: 03/17/21 07:47 Received: 03/17/21 12:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206 Pace Analytical Services - Eden Nitrogen, Nitrate 8.5 mg/L 0.30 1 03/17/21 17:47 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Eden Fecal Coliforms 13.0 CFU1100 mL 1.0 1 03/17/21 14:40 03/18/21 15:14 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 26.8 mg/L 1.0 1 03121/2122:22 16887-00-6 5310E TOC Analytical Method: SM 531OB-2011 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 04/03/21 17:09 744044-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 26 aceAnalXical www.pacelabs.com 1 ANALYTICAL RESULTS Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 Sample: MW-4 Lab ID: 92528275004 Collected: 03/17/21 08:08 Received: 03/17/21 12:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg/L 0.30 1 03/17/21 17:47 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Eden Fecal Coliforms NO CFU/100 mL 1.0 1 03/17/21 14:40 03/18/21 15:14 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 3.4 mg/L 1.0 1 03/21/2122:36 16887-00-6 5310E TOC Analytical Method: SM 531OB-2011 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 04/03/21 17:29 7440-44-0 Date: 04/05/2021 03:15 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.L.C. Page 8 of 26 Pace Analytical Services, LLC 1�55'ceAnalytical m 1377 South Park Drive Kemersville, NC 27284 www.pacelabs.com (704)977-0981 i f ANALYTICAL RESULTS Project: Forest Lake MW/Efflinf Pace Project No.: 92528275 Sample: Effluent Parameters Lab ID: 92528275005 Collected: 03/17/21 08:33 Results Units Report Limit DF Received: 03/17/21 12:30 Matrix: Water Prepared Analyzed CAS No. Dual HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg/L 0.30 1 03/17121 17:46 14797-55-8 2540C Total Dissolved Solids Analytical Method: SM 254OC-2011 Pace Analytical Services - Eden Total Dissolved Solids 212 mg/L 25.0 1 03/18/21 13:49 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Eden Total Suspended Solids 19.3 mg/L 8.3 1 03/18/21 08:48 5210E BOD, 5 day EDN Analytical Method: SM 521OB-2011 Preparation Method: SM 521OB-2011 Pace Analytical Services - Eden BOD, 5 day 7.9 mg/L 2.0 1 03/18/21 10:27 03/23/21 10:29 R6 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 922213-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Eden Fecal Coliforms 4400 CFU/100 mL 1.0 1 03/17/21 14:40 03/18/21 15:14 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 51.6 mg/L 0.52 1 03/25/21 15:39 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 37.4 mg/L 1.0 1 03121/2122:49 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 45.6 mg/L 1.0 10 03/28/21 13:57 766441-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 51.6 mg/L 2.5 5 03/24/21 21:35 03/25/21 06:16 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 ND mg/L 0.040 1 03/25/21 10:28 M1 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 11.6 mg/L 0.25 5 03/29121 17:40 03/30/2102:20 7723-14-0 M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 26 /5a'ceAnalyfical' www.pacelabs.ccm i ANALYTICAL RESULTS Project: Forest Lake MW/Effllnf Pace Project No.: 92528275 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: Influent Lab ID: 92528275006 Collected: 03117/21 08:39 Received: 03/17/21 12:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2011 Pace Analytical Services - Eden Total Dissolved Solids 225 mg/L 25.0 1 03/18/21 13:49 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Eden Total Suspended Solids 132 mg/L 25.0 1 03/18/21 08:49 5210B BOD, 5 day EON Analytical Method: SM 521 OB-2011 Preparation Method: SM 5210B-2011 Pace Analytical Services - Eden BOD, 5 day 195 mg/L 2.0 1 03/18/21 10:27 03/23/21 10:31 HEM, Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Oil and Grease 18.7 mg/L 5.0 1 03/30/21 13:13 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 52.6 mg/L 0.52 1 03/25/21 15:39 350.1 Ammonia Analytical Method: EPA350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 37.2 mg/L 1.0 10 03/28/21 15:29 7664- 1-7 M6 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 52.4 mg/L 2.5 5 03/24/21 21:35 03/25121 06:17 7727-37-9 353.2 Nitrogen, NO2/NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 0.20 mg/L 0.040 1 03/25/21 10:34 M1 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.01993 Pace Analytical Services -Asheville Phosphorus 10.6 mg/L 0.25 5 03/2912117:40 03/30/21 02:22 7723-14-0 Date: 04/05/2021 03:15 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.L.C. Page 10 of 26 1�5acIeAnalyticalo lwww.pacelab.eam t QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 QC Batch: 607369 Analysis Method: HACH 10206 QC Batch Method: HACH 10206 Analysis Description: 10206 Nitrogen, Nitrate Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005 METHOD BLANK: 3199828 Matrix: Water Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L NO 0.30 03/17/21 17:43 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3199829 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 5 5.1 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3199830 3199831 MS MSD 92527185017 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L NO 5 5 5.0 5.0 100 100 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3199905 3199906 MS MSD 92527185018 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen. Nitrate mg/L ND 5 5 5.0 5.0 100 100 90-110 0 Results presented on this page are in the units Indicated by the 'Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 26 aceAnalytical r www.patelabs.eom f QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 QC Batch: 607644 Analysis Method: SM 254OC-2011 QC Batch Method: SM 254OC-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528275005, 92528275006 METHOD BLANK: 3201017 Matrix: Water Associated Lab Samples: 92528275005, 92528275006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 03/18/21 13:49 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3201018 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 236 94 90-110 SAMPLE DUPLICATE: 3201019 92527772001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 510 514 1 SAMPLE DUPLICATE: 3201020 92527777001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L ND ND Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04105/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 26 aceAnalytical m www.pacetabs.ccm f QUALITY CONTROL DATA Project: Forest Lake MW/Effllnf Pace Project No.: 92528275 QC Batch: 607482 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528275005, 92528275006 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977.0981 METHOD BLANK: 3200298 Matrix: Water Associated Lab Samples: 92528275005, 92528275006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/18/21 08:44 LABORATORY CONTROL SAMPLE: 3200299 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 3200300 92528276001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 343 255 30 D6 SAMPLE DUPLICATE: 3200301 92528164001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 371 367 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 26 /5a'ceAna/jdica1 QD J wpw.pacelabs.com i QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 QC Batch: 607502 Analysis Method: SM 5210B-2011 QC Batch Method: SM 521OB-2011 Analysis Description: 5210E BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528275005, 92528275006 METHOD BLANK: 3200368 Matrix: Water Associated Lab Samples: 92528275005, 92528275006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg1L ND 2.0 03/23/21 10:10 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977.0981 LABORATORY CONTROL SAMPLE: 3200369 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 226 114 84.6-115.4 SAMPLE DUPLICATE: 3200371 92528042002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg1L 116 114 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date. 04105/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 26 5ac ie A na ly No / a 7 www.pacelabs.eom I QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 QC Batch: 607404 Analysis Method: SM 9222D-2006 QC Batch Method: SM 92220-2006 Analysis Description: 9222D Fecal Coliform( MF)-EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005 METHOD BLANK: 3200119 Matrix: Water Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL NO 1.0 03/18/21 15:14 SAMPLE DUPLICATE: 3200120 92528275003 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 13.0 13.0 0 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04105/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 26 /5a'ceAnalXicalo www.pacelabs com r` QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 QC Batch: 610185 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92528275006 METHOD BLANK: 3213147 Associated Lab Samples: 92528275006 Parameter Units Oil and Grease mg/L LABORATORY CONTROL SAMPLE: 3213148 Parameter Units Oil and Grease mg/L Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 03/30/2113:13 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 40 35.3 88 78-114 MATRIX SPIKE SAMPLE: 3213149 35620840001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 23.6 40 14.9 -22 78-114 M1 Results presented on this page are In the units Indicated by the "Units" column except where an attemate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, I.I.C. Page 16 of 26 aceAnalytical www.pacelaba.core i , QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 QC Batch: 607984 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005 METHOD BLANK: 3202745 Matrix: Water Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004, 92528275005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg1L ND 1.0 03/21/2119:26 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3202746 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg1L 50 52.2 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3202747 3202748 MS MSD 92527234030 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L ND 50 50 51.8 50.4 104 101 90-110 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3202749 3202750 MS MSD 92527612006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 1.6 50 50 52.6 51.8 102 100 90-110 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 26 1�5a'cmnalyficalm tvtrw.pacelabs.eom f Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 QC Batch: 609781 QC Batch Method: EPA 350.1 Rev 2.0 1993 Associated Lab Samples: 92528275005 QUALITY CONTROL DATA Analysis Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville METHOD BLANK: 3211656 Matrix: Water Associated Lab Samples: 92528275005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 03/28/21 13:14 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3211657 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 4.9 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211658 3211659 MS MSD 92525439002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L NO 5 5 5.3 5.3 106 106 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211660 3211661 MS MSD 92528059006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.2 5.2 103 103 90-110 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 26 1eAnalj6cals www.pacelabs.cam QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 Pace Analytical Services, LLC 1377 South Park Drive Kemersvilie, NC 27284 (704)977.0981 QC Batch: 609784 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92528275006 METHOD BLANK: 3211674 Matrix: Water Associated Lab Samples: 92528275006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 03/28/21 13:58 LABORATORY CONTROL SAMPLE: 3211675 Spike LCS LCS % Rae Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 4.8 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211676 3211677 MS MSD 92527508015 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 0.032J 5 5 5.2 5.2 103 103 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211678 3211679 MS MSD 92528275006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 37.2 5 5 42.6 42.8 108 112 90-110 1 M6 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 26 1�5a'ne Analytical www.pacelabs.com i , QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 608921 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92528275005, 92528275006 METHOD BLANK: 3207313 Matrix: Water Associated Lab Samples: 92528275005, 92528275006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 03/25/21 05:06 LABORATORY CONTROL SAMPLE: 3207314 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg1L 10 9.4 94 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3207315 3207316 MS MSD 92528244003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Oual Nitrogen, Kjeldahl, Total mg/L 18A 10 10 45.3 45.8 269 274 90-110 1 M1 MATRIX SPIKE 8, MATRIX SPIKE DUPLICATE: 3207317 3207318 MS MSD 92528268001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.5 10 10 23.8 26.7 223 252 90-110 11 M1,R1 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 26 /5a'ceAna1j6r,a1v www.pacelabs.eom QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 609118 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: PaceAnalyticalServices-Asheville Associated Lab Samples: 92528275005, 92528275006 METHOD BLANK: 3208246 Matrix: Water Associated Lab Samples: 92528275005, 92528275006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 03/25/21 10:25 LABORATORY CONTROL SAMPLE: 3208247 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3208250 3208251 MS MSD 92528275005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 1.7 1.7 66 65 90-110 2 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3208261 3208262 MS MSD 92528275006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.20 2.5 2.5 2.4 2.4 89 89 90-110 0 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, I.I.C. Page 21 of 26 aceAnalytical" www.pacelaba.ccm Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 QC Batch: 610010 QC Batch Method: EPA 365.1 Rev 2.0 1993 Associated Lab Samples: 92528275005, 92528275006 METHOD BLANK: 3212591 Associated Lab Samples: 92528275005, 92528275006 Parameter Units Phosphorus mg/L QUALITY CONTROL DATA Analysis Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 0313012101:27 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3212592 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3212593 3212594 MS MSD 92528268001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.13 2.5 2.5 2.6 2.6 100 99 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3212595 3212596 MS MSD 92528275005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 11.6 2.5 2.5 15.6 15.3 161 151 90-110 2 M1 Results presented an this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 26 acmnalytical m www,pacelabs.com QUALITY CONTROL DATA Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 QC Batch: 611248 Analysis Method: SM 531OB-2011 QC Batch Method: SM 5310E-2011 Analysis Description: 5310E TOC Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004 METHOD BLANK: 3218336 Matrix: Water Associated Lab Samples: 92528275001, 92528275002, 92528275003, 92528275004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 04/03/21 08.44 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3218337 Spike LCS LCS % Rec Parameter Units Conc. Result efo Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.2 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3218338 3218339 MS MSD 92527508001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec efo Rec Limits RPD Qual Total Organic Carbon mg/L 23.1 25 25 47.1 47.0 96 95 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3218340 3218341 MS MSD 92527508011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L 25.4 25 25 49.5 49.5 96 96 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, I.L.C. Page 23 of 26 Pace Analytical Services, LLC a 1377 South Park Drive aceAnalytical Kemersvllie, NC 27284 www.pacelaba.ccm (704)977-0981 E QUALIFIERS Project: Forest Lake MW/Eff/Inf Pace Project No.: 92528275 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte In a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current fist of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. R1 RPD value was outside control limits. R6 The RPD between valid sample dilutions exceeded 30%. REPORT OF LABORATORY ANALYSIS This report shall not to reproduced, except in full. Date: 04/05/2021 03:15 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 26 /5a'ceA17a1j4ica1 wrww.pacelaba.cam i QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lake MWtEffllnf Pace Project No.: 92528275 Lab ID 92528275001 92528275002 92528275003 92528275004 92528275005 92528275005 92528275006 92528275005 92528275006 92528275005 92628275006 92528276001 92528275002 92528275003 92528275004 92528275005 92528275006 92528275005 92528275006 92528275001 92528275002 92528275003 92528275004 92528275005 92528275005 92528275006 92628275005 92528275006 92628276005 92528275006 92528275005 92528275006 92528275001 92528275002 92528275003 92528275004 Sample ID MW-1 MW-2 MW3 MW-4 Effluent Effluent Influent Effluent Influent Effluent Influent MW4 MW-2 MW3 MW-4 Effluent Influent Effluent Influent MW-1 MW-2 MW3 MW-4 Effluent Effluent Influent Effluent Influent Effluent Influent Effluent Influent MW-1 MW 2 MW3 MW-4 Date: 04/05/2021 03:15 PM QC Batch Method HACH 10206 HACH 10206 HACH 10206 HACH 10206 HACH 10206 SM 2WC-2011 SM 254OC-2011 SM 254OD-2011 SM 254OD-2011 SM 521 OB-2011 SM 521 OB-2011 SM 9222D-2006 SM 9222D-2006 SM 9222D-2006 SM 9222D-2006 SM 9222D-2006 EPA1664B TKN+NO3+NO2 Calculation TKN+NO3+NO2 Calculation EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 350.1 Rev 2.0 1993 EPA 350.1 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993 SM 531OB-2011 SM 531OB-2011 SM 531OB-2011 SM 531 OB-2011 QC Batch 607369 607369 607369 607369 607369 607644 607644 607482 607482 607502 607502 607404 607404 607404 607404 607404 610185 609314 609314 607984 607984 607984 607984 607984 609781 609784 608921 608921 609118 609118 610010 610010 611248 611248 611248 611248 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Analytical Method SM 521OB-2011 SM 521OB-2011 SM 9222D-2006 SM 9222D-2006 SM 9222D-2006 SM 9222D-2006 SM 9222D-2006 Analytical Batch 607559 607559 607405 607405 607405 607405 607405 EPA 351.2 Rev 2.0 1993 609092 EPA 351.2 Rev 2.0 1993 609092 EPA 365.1 Rev 2.0 1993 610095 EPA 365.1 Rev 2.0 1993 610095 Page 25 of 26 Allaly,#IGai ' CHAIN -OF -CUSTODY Analytical Request Document Chain of -Custody 3s a LEGAL DOCUMENT - Cumpletu all re)event fields Forest Lakes 1811iinglnforrnation: Report To: Emal l To: Copy Tm She Coliecticin Info/Address- Customer Project Name/Number: State: County/City: Time Tone Collected: 1 [ JPTI 1MT( ICT [ JET Phone: Site/Facility ID #. Compliance Monitoring? Email: [ /Yes [ IN. Collected By vrint): Purchase order 8: Ow pWS ID III:� Quote rf: Dw Location Code: Collected By (signature): Turnaround Bate Sequined: Imme rate y Pace on Ice: r [ ] Yes I IN Sample Disposal: Rush: Fieid Filtered (if applicable): I I Dispose as appropriate I I Retum I j SamP Day [ I Next Day I I Yes [ ]No I I Archive: () 2 Day 1 13 Day [ 14 Day (15 Day I ) Hold:_ (Expedite Charges Apply) Analysis: " Matrix Codes (Insert in Matrix box below): Drinking Water(DW), Ground Water (GW), Wastewater(Ww), Product (11), Soil/Solid (SQ, O)I (OL), Wipe (WPI, Air (AR), Tissue (TS), Bioassay (B), Vapor M, Other (OT( CustomCrSample fD Matrix • Comp / Grab Collected {or Composites.... Composite End Res q of Cl Ctns Date I Time Date Tirne f YlV V"J 9W 9 2�,�774 '1-71�7 gw g 3 J')HCJ Oif6 �i Effluent 9 s /-7 r c,JfJ » 2r le2(3`l Customer Remarks / Special Conditions / Possible Hazards: Groundwater Monitoring Relinquished by/Company: (Signature) pF 3. 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