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HomeMy WebLinkAboutWQ0002857_Monitoring - 03-2021_20210429Monitoring Report Submittal ............................................................................................................................................ Permit Number #* WQ0002857 Name of Facility:* Month:* March Report Information Piedmont Custom Meats Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter:* Signature: Date of submittal: Initial Review Year:* 2021 Upload Document* Piedmont Custom 2.63MB Meats_March.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Jessica. Mize@pacelabs.com Jessica Mize Reviewer: Williams, Kendall N 4/29/2021 This w ill be filled in automatically Is the project number correct?* WQ0002857 Is the monitoring report t: Yes r No accepted?* Regional Office* Winston-Salem Accepted Date: 4/29/2021 Page 1 of 3 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W00002857 MONTH: March YEAR: 2021 FACILITY NAME: Piedmont Custom Meats W',VTF COUNTY: Caswell Flow Monitoring Point: Effluent: JllI��1nf1uent: n VON 1pff ■ •._ .. rF r rr•rr rr.s rr r rr. r rr r � r rr sr. r rr. rr•.F rr.rr rr.. r • �o Fir In ------------ Operator in Responsible Charge (ORC): Glenn Price Grade: SI Phone: 336-996-2841 Check Box if ORC Has Changed: El ORC Certification Number: 987931/20771 Certified Laboratories (1): Pace Analvtical Services (2 Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to- ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CW Division of Water Quality By this signature, I certify that this report is accurate and 1617 flail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-I617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant (Y,N) 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is n, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 43 ,z,� W1 d- d { Baron Neal McDuffie (Signature of Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 9683 Kerr"s Chapel Road Gibsonville NC (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD Field Services Director (Pace AnaMcal Services) PARAMETER CODES 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury NH3 as N F00610 01067 Nickel (Position or Title) 336-582-8247 (Phone Number) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 03/31/21 (Permit Exp. Date) 00929 Sodium _ 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 61092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units desiartated in the reporting - facilit,+sgermit for reporting data. * If signed by other than the Penmittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 3 of 3 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W00002857 MONTH: March YEAR: 2021 FACILITY NAME: Piedmont Custom Meats WNVTF COUNTY: Caswell Formulas: Daily Loading (inches) = (Volume Applied (gallons) x 0.1336 (cubic feetfgallon) x 12 (inchesffool)] I (Area Splayed (acres) x 43.560 (squaro feeVacre) or = (Volume Applied (gallons) I (Area Sprayed (acres) x 27,152 (gallonslacre-inch). Maximum Hourly Loading (inches) = Daily Loading (inches) / (Time irrigated (minutes) I60 (minutes/hour)] Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = (Monthly Loading (inches/month) / Number of days in the month (dayslmonth )] x 7 (days.1%eek) N�tion Occur At This Facility� !1 ■ aa Infig—ati-o-n Occu­rOnT_ -his -Field: yen w Did IrTigaticin Occur On This Feld: ■ Permitted Aoufly Rate (inches): . .Permitted Yearly Rate inches)� Permitted Yeady Rate Cinchesy. ®� 1 I I -Weather Codes: Clear, PC-panly cloudy, Cklouds, R-rain, Sn-snux, Sl-sleet Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: El Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHAR ) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) I. The application rate(s) did not exceed the limit(s) specified in the permit. 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in, the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoons) was not less than the limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below -the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for subm,,it�ting ffan alse information, including the possibility of fines and imprisonment for knowing violations." -1 Z-'11- Baron Neat McDuffie (Signature of Permttee)* V Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent (Permittee-Please print or type) 9683 Keres Chapel Road Gibsonville. NC (Permittee Address) Field Services Director ( Pace Analytical Services_ (Position or Title) 336-582-8247 (Phone Number) 03/31/21 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). DENR Form NDAR-1 (5/2003) Page 2 of 3 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUINIBER: WQ0002857 MONTII: March YEAR: 2021 FACILITY NAME: Piedmont Custom Meats WWTF COUNTY: Caswell Formulas: Daily Loading (inches) = [Volume Applied (gallons) x 0.1336 (cubic feet/gallon) x 12 (inchosRool)] 1 {Area Sprayed (acres) x 43,560 (square feellacre) or = (Volume Applied (gallons)! [Area Sprayed (acres) x 27,152 (gallonslacre-inch). Maximum Hourly Loading (inches) = Daily Loading )inches) I [Time irrigated )minutes)160 (minuteslhour)[ Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = IMonfty Loading (fichesimonth)1 Number of days in the month (days/month )] x 7 (daystweek) bid WIrngation Occor At This Facifity� yes:[:[ 'Did Irrigation Occur On This Field: Yea ■ Did Irrigation Occur On This Field: ■ • ■ • Permitted Yearly Rate Cinches)� Permitted Yearly Rate (inchaEy. flm film®�®----�--- •Weather Codes: C-clear, PC -partly cloudy, CI -cloudy. R-rain, Sri-snwy, 51-sleet Spray Irrigation Operator in Responsible Charge (ORQ: Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORS Has Changed Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X c t DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to llte best of my knoN ledge. RALEIG] NC 27699-1617 DENR Form NDAR-1 (5/2003) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (SignatGe of Permitee)* Date Baron Neal MCDUffe (Authorized Agent) (Permittee-Please print or type) 9683 Keres Chapel Road Gibsonville NC (Permittee Address) Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 336-582-8247 (Phone Number) 03/31/21 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). DENR Form NDAR-1 (5/2003) /55'ceAnaljdical' www.pactiabi.com March 29, 2021 Larry Moore Piedmont Custom Meats 430 NC Highway 49 South Asheboro, NC 27205 RE: Project: Piedmont Custom Meats 3/17121 Pace Project No,: 92528140 Dear Larry Moore: Pate Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977.0981 Enclosed are the analytical results for sample(s) received by the laboratory on March 17, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 1�l5aceAna1j6ca( wnrw.pacelabs.com Pace Analytical Services, LLC 1377 South Park Drive Kemersviile, NC 27284 (704)977-0981 Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 2 Of 21 aceAnalytical wuiw.pacelabs.eom SAMPLE ANALYTE COUNT Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92528140001 Effluent HACH 10206 AMI 1 PASI-E SM 254OC-2011 MLS1 1 PASI-E SM 254OD-2011 MLS1 1 PASI-E SM 4500-H+B-2011 MWF 1 PASI-E SM 521OB-2011 MWF 1 PASI-E SM 9222D-2006 AMI 1 PASI-E TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 300.0 Rev 2.1 1993 JLH 1 PASI-A EPA 350.1 Rev 2.0 1993 NAL 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MFO 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 3 of 21 1�5a'ucntoi Analytical www.pacelaba.eom 1 ANALYTICAL RESULTS Project: Piedmont Custom Meats 3/17121 Pace Project No.: 92528140 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: Effluent Parameters Lab ID: 92528140001 Collected: 03/17/21 10:49 Results Units Report Limit DF Received: 03/17/21 12:30 Matrix: Water Prepared Analyzed CAS No. Qual HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206 Pace Analytical Services - Eden Nitrogen, Nitrate 28.5 mg/L 7.5 25 03/17121 17:46 14797-55-8 2540C Total Dissolved Solids Analytical Method: SM 254OC-2011 Pace Analytical Services - Eden Total Dissolved Solids 394 mg/L 25.0 1 03/18/21 13:49 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Eden Total Suspended Solids 192 mg/L 62.5 1 03118/21 08:46 4500H+ pH, Electrometric EDN Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Eden pH at 25 Degrees C 6.0 Sid. Units 0.10 1 03/18/21 12:51 H3 5210B BOD, 5 day EDN Analytical Method: SM 521OB-2011 Preparation Method: SM 52106-2011 Pace Analytical Services - Eden BOD, 5 day 368 mg/L 2.0 1 03/18/21 10:27 03/23/21 10:48 M1310 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Eden Fecal Conforms 69.0 CFU/100 mL 1.0 1 03/17/21 14:40 03/18/21 15:14 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 98.4 mg/L 0.52 1 03/25/21 15:36 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 57.9 mg/L 10.0 10 03/20/2122:12 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 42.5 mg/L 1.0 10 03/28/21 15:38 766441-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 65.1 mg/L 2.5 5 03/24/21 20:15 03/25/21 06:04 7727-37-9 353.2 Nitrogen, NO2IN03 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 33.3 mg/L 0.40 10 03/23/21 12:41 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 21 aceAnalytical wanspacelata.com ANALYTICAL RESULTS Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: Effluent Lab ID: 92528140001 Collected: 03/17121 10:49 Received: 03/17/21 12:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 2.4 mg/L 0.050 1 03/25/2122:57 03/26/2104:08 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 21 1�l5aceAnalytical'D www.paeelabucm i { QUALITY CONTROL DATA Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 QC Batch: 607369 Analysis Method: HACH 10206 QC Batch Method: HACH 10206 Analysis Description: 10206 Nitrogen, Nitrate Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528140001 METHOD BLANK: 3199828 Associated Lab Samples: 92528140001 Parameter Units Nitrogen, Nitrate mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.30 03/17/2117:43 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3199829 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 5 5.1 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3199830 3199831 MS MSD 92527185017 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L ND 5 5 5.0 5.0 100 100 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE. 3199905 3199906 MS MSD 92527185018 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L ND 5 5 5.0 5.0 100 100 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 21 1�;a'cmnalyticalq) j www.pacelabs=rt i QUALITY CONTROL DATA Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 QC Batch: 607644 Analysis Method: SM 254OC-2011 QC Batch Method: SM 254OC-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528140001 METHOD BLANK: 3201017 Matrix: Water Associated Lab Samples: 92528140001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L NO 25.0 03/18/21 13:49 LABORATORY CONTROL SAMPLE: 3201018 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 236 94 90-110 SAMPLE DUPLICATE: 3201019 92527772001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 510 514 1 SAMPLE DUPLICATE: 3201020 92527777001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L ND ND Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 21 aceAna1j&al www.pacelabs.com Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QUALITY CONTROL DATA Project: Piedmont Custom Meats 3/17121 Pace Project No.: 92528140 OC Batch: 607482 Analysis Method: SM 254OD-2011 OC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528140001 METHOD BLANK: 3200298 Associated Lab Samples: 92528140001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 3200299 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 03/18/2108:44 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 252 101 90-110 SAMPLE DUPLICATE: 3200300 92528276001 Dup Parameter Units Result Result Total Suspended Solids mg/L 343 255 SAMPLE DUPLICATE: 3200301 92528164001 Dup Parameter Units Result Result Total Suspended Solids mg/L 371 367 RPD Qualifiers 30 D6 RPD Qualifiers 1 Results presented on this page are In the units Indicated by the "Units" column except whore an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, I.I.C. Page 8 of 21 acmnalytical wiumpacelat it= 1 i QUALITY CONTROL DATA Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 QC Batch: 607616 Analysis Method: SM 4500-H+B-2011 QC Batch Method: SM 4500-H+B-2011 Analysis Description: 4500H+B pH EDEN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528140001 SAMPLE DUPLICATE: 3200841 92528140001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.0 6.0 0 H3 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 21 1�5a'cmnalyfical'D t www.pacelabs.com I Pace Analytical Services, LLC 1377 South Park Drive Kemersviile, NC 27284 (704)977-0981 QUALITY CONTROL DATA Project: Piedmont Custom Meats 3117/21 Pace Project No.: 92528140 QC Batch: 607502 Analysis Method: SM 521OB-2011 QC Batch Method: SM 521OB-2011 Analysis Description: 52108 SOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528140001 METHOD BLANK: 3200368 Associated Lab Samples: 92528140001 Parameter Units B00, 5 day mg/L LABORATORY CONTROL SAMPLE: 3200369 Parameter Units BOD, 5 day mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 03/23/2110:10 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 226 114 84.6-115A SAMPLE DUPLICATE: 3200371 92528042002 Dup Parameter Units Result Result BOD, 5 day mgiL 116 114 RPD Qualifiers 2 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 21 5ticeAnalyticaI www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats 3117/21 Pace Project No.: 92528140 QC Batch: 607404 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF)-EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92528140001 METHOD BLANK: 3200119 Matrix: Water Associated Lab Samples: 92528140001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFUI100 mL NO 1.0 03/18/21 15:14 SAMPLE DUPLICATE: 3200120 92528275003 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 13.0 13.0 0 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977.0981 Results presented on this page are to the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 21 aceAnalytical wpw.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 Pace Analytical Services, LLC 1377 South Park Drive Kemersviile, NC 27284 (704)977-0981 QC Batch: 607982 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92528140001 METHOD BLANK: 3202733 Matrix: Water Associated Lab Samples: 92528140001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 03/20/2117:54 LABORATORY CONTROL SAMPLE: 3202734 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 50 51.7 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3202737 3202738 MS MSD 92528140001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 57.9 50 50 105 105 94 94 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3203204 3203205 MS MSD 92528440001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 319 50 50 332 332 26 27 90-110 0 M6 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, I.I.C. Page 12 of 21 aceAnalytical j WW pacetab=M l QUALITY CONTROL DATA Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 QC Batch: 609785 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92528140001 METHOD BLANK: 3211680 Associated Lab Samples: 92528140001 Parameter Units Nitrogen, Ammonia mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 03/28/2114:45 Paco Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3211681 Spike LCS LCS % Rec Parameter Units Conc. Result %e Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 4.8 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211682 3211683 MS MSD 92529274006 Spike Spike MS MSD MS MSD %e Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.2 5.2 103 103 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211684 3211685 MS MSD 92528059001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result %e Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.3 5.3 103 103 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, L.I.C. Page 13 of 21 aceAnalytical " www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 QC Batch: 608918 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92528140001 METHOD BLANK: 3207275 Associated Lab Samples: 92528140001 Parameter Units Nitrogen, Kjeldahl, Total mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 03/25/2104:29 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3207276 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.8 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3207277 3207278 MS MSD 92528612001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 9.6 10 10 22.2 21.4 126 118 90-110 4 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3207279 3207280 MS MSD 92528699001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 3.4 10 10 15.2 15.0 118 116 90-110 1 M1 Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, I.I.C. Page 14 of 21 QD aceAna1j6ca1 www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 608427 Analysis Method: EPA 353.2 Rev 2.0 1993 OC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92528140001 METHOD BLANK: 3204914 Matrix: Water Associated Lab Samples: 92528140001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L NO 0.040 03/23/21 12:01 LABORATORY CONTROL SAMPLE: 3204915 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mgiL 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3204916 3204917 MS MSD 92528672004 Spike Spike MS MSD MS MSD eke Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.17 2.5 2.5 2.4 2.4 88 88 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3204918 3204919 MS MSD 92528672005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.24 2.5 2.5 2.5 2.5 91 92 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/2912021 12:01 PM without the written consent of Pace Analytical Services, I.I.C. Page 15 of 21 aceAnalWical www.pacelabs.com i QUALITY CONTROL DATA Project: Piedmont Custom Meats 3117/21 Pace Project No.: 92528140 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 609341 Analysis Method: EPA 365.1 Rev 2.0 1993 OC Batch Method: EPA 365.1 Rev 2.01993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92528140001 METHOD BLANK: 3209674 Matrix: Water Associated Lab Samples: 92528140001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 03/26/2104:00 LABORATORY CONTROL SAMPLE: 3209675 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.6 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3209676 3209677 MS MSD 92528059006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.6 2.6 101 102 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3209678 3209679 MS MSD 92528059007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.6 2.6 101 102 90-110 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 21 Pace Analytical Services, LLC 1377 South Park Drive lanema0calm Kemersville, NC 27284 www.pacelab GM (704)977-0981 QUALIFIERS Project: Piedmont Custom Meats 3/17/21 Pace Project No.: 92528140 314JIZ511L•7.�� DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2021 12:01 PM without the written consent of Pace Analytical Services, I.L.C. Page 17 of 21 acemalytical Wale 1 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats 3117/21 Pace Project No.: 92528140 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92528140001 Effluent HACH 10206 607369 92528140001 Effluent SM 254OC-2011 607644 92528140001 Effluent SM 254OD-2011 607482 92528140001 Effluent SM 4500-H+B-2011 607616 92528140001 Effluent SM 521OB-2011 607502 SM 521OB-2011 607559 92528140001 Effluent SM 9222D-2006 607404 SM 9222D-2006 607405 92528140001 Effluent TKN+NO3+NO2 609311 Calculation 92528140001 Effluent EPA 300.0 Rev 2.11993 607982 92528140001 Effluent EPA 350.1 Rev 2.0 1993 609785 92528140001 Effluent EPA 351.2 Rev 2.0 1993 608918 EPA 351.2 Rev 2.0 1993 609091 92528140001 Effluent EPA 353.2 Rev 2.0 1993 608427 92528140001 Effluent EPA 365.1 Rev 2.0 1993 609341 EPA 365.1 Rev 2.0 1993 609417 Date: 03/29/2021 12:01 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 21 528140 0 0) /�� eAn, 71 CHAIN -OF -CUSTODY Analytical Requpst Document Chain -of -Custody is a LEGAL DOCUMENT- Complete adrelevent fields MU,'��I������i'��I�`I'��,''CL company: 66 Billing Information: ALL -SHADED.Af 925,20 Container PreservativelLa Type P Address: I Report To; Email r-; Preservative Types" III riltdc acid, t4I "c auu, tal mfulOCIlloric aQu, IJ sodium fly. � (I nc acetate, j6) methanol, (7) sodium bisulfate, (8) sodium thiosidbte, (9) hexane, (A) ascorbic add, (a) am monlum sulfate, JQ ammonium hydroxide. (D)TSP, (U) Unpreserved, 10) Other Copy TO; Site Collection Info/Address: Analyses Prpfile/Liher. Customer Project Name/Number: State. County/City: Time Zone C61lected. U f JPTJ J�k�-.JCT I JET Phone. Site/Facility ID #: Compliance Monitoring? Email: Yes Nd si l- Present XIll NA tiesA 11' NA nrrect'Bottles Cullect d By print): Purchase Order DW PWS ID It: Quate #: W D Location Code... Sufficiehi %ir,61 um o-llcct&d By (signature}: Turnaround Date Required; Immediately Packed an Ice: [ ]Yes I I NO -4p. - I alp� -.44-.'5014 -11\ 14 N1- V., & IN. -- Sample Disposal: I Dispose s" Same Day Next Day Field Filtered (if applicable): as apprupriate I Return E12 Yes ]No a= C, 1;9 N I& I Archive: I 0 11f 13Day I 14Day 1 5 Day Analysis: X (Expedite Charges Apply} Matrix Codes (Insert in Matrix box below). Drinking Water (DW), Ground Water (GW), Wastewater (WW). Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (Ak), TIssue (5), Bloassay (B), Vapor IV), other (OT) -M tiIW'PfQ,4 Customer Sample ID Matrix• Comp Grab Collected (or Composite Start) Composite End N of Ctns Da te, I Time Date e ie Time Customer Remarks/ Special Conditions/ Possible Hazards: ITyp Relinquished by/Copparly: (Signature) by/Company. (Signature) Inate/Time. ko A 7 r. Lab Sample Temperai* Blank R "hii'm iE .��Coo rA Temp Upon gecelpt::. c Wr, ofe(s) Y;, -N S 'I 1,fi'livid Wi:� er irrn-rlc�ii.:facfR)ir.-**�*1!!h,%4C�' 5 Xg C r, let 'Comments- R (Signature} Comparlyf(Sl Date/n Al Acclnurm *- TEmpfate �?Valture) Ae e6*dbpComparbi; (Sig 'Trip, Blank Recelved:. "Y N HCL MeOR TSR Othei Prelokin" PM; Received by/Company- (Signature) Date/Time! onicorif Page: YES /. No, of: 'Cfttk mark top half of boat if pH and/or dechterin3U. is ao��.fo�2Maa• - - SMALL- &UpdmL' VDA, CaUb% MC CH and grew, GW/W jg fwater) CCr "80 tarm haN od box is tO fiat 44Mker of bottle t LI& tam '�8 '�i a . aL z 3 4 S U 9 pN Adjustment tog for Preserved pH Ypca ticrtpt Cato cra,.,wo�...w_.� .�_ �t�d � :dQitd Oo••�.•,•�.�urrawmw��t�otampli;itapyorthi�latmwiN�euettathe6arJ+CudtnaOEkNRC�a1Ca�@enClitcapa 1 ucalhatd,etCarpnpresarnGve eutGttQmA.cnrr[¢conpNp� page '20 aceAnafyflcaf ­ r •*•+.pbocwca.m+. r Sam le Receiving Non -Conformance Form (NCF) _ 1-1 _ Affix Workarderl>;ogitt Label Here or List Pace C Q� > "- U"I" Workorder Nurrtber or MiJLlog-in Number ;.. ;� ,r$ ~ r r Here 1. If Chain -of -Custody (COC) Is not received; contact client and if necessary, fill out a COC and indicate that it was filled out by lab personnel. Note issues on this NCF. 7- if CCIr'. rc Incmmninta ,hcrk nnnlin*klo i ii k..l.,... ­4 .AA A-# -a.- ...- Collection dateltime miss#ng or Analyses or anaiytes: missing or I Samples listed on COC'do not match samples incorrect ciarificat'on needed racoived missin , additional. etc. Sample IDs on COC do not I match samole labels Required trip blanks were not received Required si natures are missin wrrrrrenrsruetairsrutner issues no[ jisiea above: 3. Sample integrity issues: check a0plIcable Issues below and add details where appropriate: Samples: Condition needs to be brought to Sam fes: Past holding time lab ersonnel's attention details below Preservation: Improper Temperature: not within acceptance criteria (typicailt Samples: Not fleid filtered Containers: Broken or compromised n-a(,,) received I Containers. Incorrect I Tem eraturs: Samples arrived frozen -Samples: Coole, damaged or Custody Seals: Missing or compromised on compromised samples, trip blanks or coolers Vials received with Improper heads ace Samples contain chlorine or sulfides Packing Material: InsufncienUlm arn er Other: 'Comments/Detail �C���� can's C �Ccr,r�_ G �IGt 0. SDttL1 4. If Samples not preserved proparly and Sample Receiving ad usts, H add details below: Sample ID: Date/Time: Amount/type prei added: Preserved by: Initial and Final pR Lot * of ones added: Sample ID: Date/Time: Arnount/type pres added: Presented by: Initial and Final H: Lot # of pres added: Sample 10: Daterrime. Amount/type pres added: Preserved by: Initial and Final 2R Lot * of pres added: 5. Client Contact: If client is contacted for anv issue listed above. fill in details below: PM Inilials: I Date/Time: Client Comments IInstructions: 1=-ALL-C-011-rev.00, 05Ju12018 Page 21 of 2