HomeMy WebLinkAboutNCG030499_2021 DMR_20210425Anchor QEA of North Carolina, PLLC ANCHOR
231 Haywood Street�z Asheville, North Carolina 28801 QEA �i
828.281.3350
April 23, 2021
Attn: DEMLR Stormwater
Asheville Regional Office
Division of Energy, Mineral, and Land Resources
North Carolina Department of Environmental Quality
2090 U.S. 70 Highway Swannanoa, North Carolina 28778-8211
Re: Stormwater Sample Analytical Results, Period 1 2021
Crane Resistoflex
Marion, North Carolina
Certificate of Coverage No. NCG030499
To Whom It May Concern,
Anchor QEA of North Carolina, PLLC (Anchor QEA), is pleased to present the following stormwater
sample analytical results. On behalf of Crane Resistoflex, Anchor QEA collected two stormwater
samples on March 31, 2021, for the referenced facility covered by National Pollutant Discharge
Elimination System Stormwater General Permit No. NCG030000 (Stormwater General Permit). This
sampling event fulfills the compliance sampling requirement for Period 1 of 2021.
In the samples collected from sampling locations OF-001 and OF-002, one monitoring parameter
was not within the range of benchmark values specified in the general permit. All other parameters
and constituent concentrations detected were below or within the acceptable ranges of the
benchmark values specified in the general permit. This letter provides background information and
describes the methods, findings, and conclusions regarding the stormwater sample collection and
analysis.
Background
The most recent Stormwater General Permit for metal fabrication activities was issued by the North
Carolina Department of Environmental Quality with an effective date of November 1, 2018, and it will
expire at midnight on May 31, 2021. Sample collection and reporting protocol for this event followed
the current permit requirements.
The Stormwater General Permit indicates that the permittee shall complete analytical sampling on
a semiannual schedule, once during the first half of the year (January 1 to June 30; Period 1) and
once during the second half of the year (July 1 to December 31; Period 2), at a minimum, allowing
at least 60 days between sample collection dates.
Stormwater Sample Analytical Results, Period 1 2021.docx
April 23, 2021
Page 2
The general location of the facility is indicated in Figure 1. The facility's two permitted outfalls and
sample locations are labeled OF-001 and OF-002, as identified in Figure 2.
Methods
On March 31, 2021, Anchor QEA mobilized to the Crane Resistoflex facility to collect stormwater
samples during a measurable storm event of approximately 0.99 inches of rainfall'. There had not
been a measurable storm event in the 72 hours preceding this sampling event.
The stormwater samples were collected from two outfalls labeled OF-001 and OF-002 (Figure 2).
Samples were collected as indicated in the surface water sampling logs (Attachment 1) from the
approximate center of the discharge streams and were transferred to laboratory -supplied containers.
The containers were placed in a cooler on ice and delivered to Pace Analytical Services, Inc. (Pace), in
Asheville, North Carolina, for laboratory analyses specified in the General Permit. Total Toxic Organic
(TTO) analysis is not required for the Crane Resistoflex facility per Section B, Table 1, Footnote 6 of
the General Permit, which states that Total Toxic Organics sampling is applicable only for those
facilities that perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes.
The pH measurement was obtained in the field by placing a probe within the flow of the respective
outfall. The pH measurement was recorded once stabilization occurred. Anchor QEA's equipment
documentation and instrument calibration data sheet is included as Attachment 2.
Anchor QEA also performed a stormwater discharge outfall (SDO) qualitative monitoring event
during the stormwater analytical sampling event. The associated SDO qualitative monitoring reports
are included as Attachment 3.
Findings
The laboratory analytical results are summarized in the Semiannual Stormwater Discharge Monitoring
Report (Attachment 4). The samples contained concentrations lower than or within the range of the
specified benchmark values for all constituents analyzed by Pace.
The field measurement of pH obtained from OF-001 was not within the specified benchmark range
of 6.0 to 9.0 standard units. The field measurement of pH for OF-002 was within the acceptable
benchmark value range. The field measurement results are listed in the surface water sampling logs
(Attachment 1), and pH results are shown in Attachment 4. The Pace analytical report and chain -of -
custody form are included in Attachment 5.
Rainfall amount was obtained from the Weather For You online database records for the MID_F4683 gauge station in Marion,
North Carolina. Available at: https://www.weatherforyou.com/
April 23, 2021
Page 3
Conclusions
The stormwater sample results for outfalls OF-001 and OF-002 showed one result not within the
specified benchmark range for pH in OF-001. All other parameters and concentrations were below or
within the range of the benchmark values specified in the general permit for all constituents. Per the
Stormwater General Permit, response activities included the following.
1. Conduct a stormwater management inspection of the facility within two weeks of receiving
sampling results (results were received April 6, 2021). A stormwater inspection was completed
on April 13, 2021.
2. Identify and evaluate possible causes of the benchmark value exceedance. This inspection did
not indicate any obvious source of pH issues related to facility operations. However, low pH
could be due to highly concentrated stormwater surge at the collection site. For future
analytical monitoring events, field measurement of pH will be obtained directly from
ambient precipitation if pH within either outfall exhibits a value outside of the specified
benchmark range.
3. Identify potential, and select the specific feasible: source controls, operational controls, or
physical improvements to reduce concentrations of the parameters of concern, and/or to bring
concentrations within the benchmark range. Due to the cause of this parameter result, which
was not within the specified range of benchmark values, new controls should not be
necessary.
4. Implement the selected feasible actions within two months of the inspection. Not applicable.
5. Record each instance of a Tier One response in the Stormwater Pollution Prevention Plan (SPPP).
Include the date and value of the benchmark exceedance, the inspection date, the personnel
conducting the inspection, the selected actions, and the date the selected actions were
implemented. This activity has been completed.
The next analytical monitoring of stormwater discharges will be performed during another
measurable storm event between July 1 and December 31, 2021, to satisfy the Period 2 of 2021
compliance period.
April 23, 2021
Page 4
If you would like additional information, please contact me at (828) 281-3350, or contact Victoria
Boyer at (828) 724-2316.
Sincerely,
Robert Cork PE, MEng
Managing Engineer
cc: Victoria Boyer, Crane Resistoflex
Duplicate, Central Files
Attachments
Figure 1 Site Location Map
Figure 2 Stormwater Discharge Outfall Locations
Attachment 1 Surface Water Sampling Logs
Attachment 2 Equipment Documentation and Instrument Calibration Data Sheet
Attachment 3 Stormwater Discharge Outfall Qualitative Monitoring Reports
Attachment 4 Semiannual Stormwater Discharge Monitoring Report
Attachment 5 Laboratory Analytical Report and Chain -of -Custody Form
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Filepath: Q:\Jobs\Crane_Resistoflex_2062\Maps\AQ_Fig01_SiteLocationMap.mxd
kZANCHOR
QEA
Figure 1
Site Location Map
Stormwater Sample Analytical Results
Crane Resistoflex, Marion, North Carolina
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Attachment 1
Surface Water Sampling Logs
tzANCHOR
QEA
Surface Water Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name:
Loan"E,s;rfo�/e_x
Date: 5131 Zo?1
Project Number:
Sampling Personnel:
G 1" 6 _ q`. 0/ 74.rlf 070/
C PA. merlon
/
Weather: 5S`F Overcpsll It;
Facility Permit #: ■ y C 0 3 0 O 0 0-0-
Sample Name:
Q)C, QU/
Comments:
Sample Method:
Grab Syringe Pump
Bailer-Disp. Other:
Oxidation
Dissolved Specific Cond.
pH (S.U.)
Reduction Turbidity
Time Temp (°C)
Oxygen (mg/L) (PS/cm)
report to 0.1 S.U.
Potential (mV) (NTU) Comments
0135 / Lf 5
— — 5, if
5. aS
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
:2 v✓/ HA103
AlI eWs- 01 f� isSo/Vu! /�'le ids �l�
125 mL Plastic
40 mL Glass
1 L6hrss Plartl`G
/ '��csen��
TS.S
Other / L G last(A-le.-)
2 w/ Hc. t
TPJI Oil a.J 6reafe.
Vegetation: C-7,0u
Sampling Personnel Signature:
Notes:
Samples are analyzed immediately upon collection.
°C: degrees Celsius
pS/cm: micro-Siemen per cubic centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Method Reference:
Access: G00J
Date: 3/3 // 2, 0 2 /
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H' B-2011
Page 1 of 1
kZANCHOR
QEA
Surface Water Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name:
0'¢n C R CS/sfG flex
Date: 313Y 202 /
Project Number:
Sampling Personnel:
q ZU 62 - 0 /. 0 % Tom% 0 70/
C-Px-Ite/-run
Weather: CCoF/ �1. JI-rf'R
Facility Permit #: / VG 0 30 00 0 0
Sample Name:
OF - 0 02
Comments:
sa✓►+�`e l wke t Pole (.[.Sed -h
C-'Ilea/1 (dC Con1'AAti/1a.P-J AA/
Sample Method: Grab Syringe Pump
Bailer-Disp. Other:
Oxidation
Dissolved Specific Cond. pH (S.U.)
Reduction Turbidity
Time Temp (°C)
Oxygen (mg/L) (PS/cm) report to 0.1 S.U.
Potential (mV) (NTU) Comments
141 S /1f. 5
.3 L
- 7. 62
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
Z w . 11 Ko
125 mL Plastic
40 mL Glass
1 L C-class plRl iv'G
u n�'�ere/VG�
TSS
Other / L C6 /arc AMb,, -2 w� 14L �
li 0d a/td
Vegetation: G001
Access: F&tI- rnct JWY dt4 -s4ic
Sampling Personnel Signature: � Date: 3131Z.2021
Notes:
Samples are analyzed immediately upon collection.
°C: degrees Celsius
pS/cm: micro-Siemen per cubic centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
pH: SM 4500-H' B-2011
Page 1 of 1
Attachment 2
Equipment Documentation and
Instrument Calibration Data Sheet
kzANCHOR
QEA
Equipment Documentation and Instrument libration Data Sheet `
Project Name: /��^, �C _ Analyst Conducting Calibration: CLPA-H-VA0
Project Number:r Zp G2 — Q/, Q/ %li Q7o / Date of Calibration:
Project Location: All a/-r(W I)UFf Date of Field Measurements: 'Z(fZi
Facility ID or Permit # (if applicable): )VC-
EQUIPMENT DOCUMENTATION
Rental sample analysis equipment or meters used to take measurements:
I Eauioment Tvoe 1 Brand I Serial Number I Date of Use 1 Rental Comuanv I
Select Turbidimeter.� Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPW (s/n 200601045)
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Instrument Readings
(Hach 21000)
Instrument Readings
(HF Scientific MicroTPM
Cal Std Information
10 NTU
20 NTU.
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
Lot #-
A
Q
Expiration Date:
/
/
21721
Cal (NTU)-
Cal (NTU b • 7
(S�
Cal (NTU):,, t
Cal (NTU):
Cal (NTU):
Cal (N
Time: Q V 9 f L
T
Time:Q
Time: Gs i
Time:
Time:
Time:
Calibration
Verification:
*Pre -Analysis
Check (10 NTU):
Result (NTU):
/ Q * 3
Time: /`
ON S Z
*Pre -Analysis
Check (10 NTU):
Result ):
Time:
*Post -Analysis
Check (10 NTU):
Result (NTU):
/UiZ
Time: !l
V 6 91
*Post -Ana
ICI,.k [ ):
Result (NTU):
Time: C�4P
YSI Professional Plus Multiparameter Meter (s/n 4200006W 1ilItgJ01J13
Instrument Readings
Cal Std Information
Lot #
Date
Opened
Exp. Date
Dissolved Oxygen
(% saturation)
Initial (%):
Cal (%):
7
Time:
DO (Site #2,
if applicable)*
QC** Chec
Initial (%):
Time:
Cal (%):
Result (%):
mmHg:
Time:
Temperature (°C):
Result (%):
Time:
Time:
Result [%1:
PH 7 S.U.
report to 0.1 S.U.
Initial- Q Q
9/ . -(U
pHmV:
`�) • D
Cal (S.U.):
, U
pHmV: (j �%
" "r ' `
Time: �1
L•6
0d6VC
'2 A
PH 4 S.U.
reportto 0.1 S.U.
Initial:
pHmV:
%
Cal (S.U.):
•a
pHmV//�:
J IO , Z
Time:
6830
66117
7/Z)
PH 10 S.U.
report to0.1S.U.
Initial: /y
(/,
pHmV:
—JR.
Cal (S.U.)/: ;
,V/
pHmV:
.,/�R•
Time:
,•
GBgBC
2122
QC** pH 7 S.U.
re;ortto0.1S.U.
Tim/3�,4
33
Result (S.U.):
7,OZ
Time: �j
1130
Result (S.U.):
.
(,0 4
Time:
Result
CAP `
066Z7C
[ L
Spec. Cond.
Initial:
Cal (pmhos/cm):
Time:
1,000 pmhos/cm
% Recove =
QC** Spec. Cond.
1,000 pmhos/cm
Time:
Result (pmhos/cm):
Time:
Result (pmhos/cm):
Time:
esu t (pmhos/cm):
Recovery=
ORP
al:
Temperature ('C):
Time:
Analyst Signature: Analyst Name: <fA,,jr�,an 110,1 Date: 3 A
Notes:
Revision 6, 12/20/20, MAK
1. Instruments shall be calibrated in accordance with the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks.
4. *When performing DO analyses at multiple sample sites (i.e. project/facility locations), the DO probe must be calibrated at
each sample site prior to analysis.
S. QC Acceptable Ranges: pH */- 0.1 S.U. and Specific Conductivity 10%of the true value. If QC readings are out of range, the
instrument needs to be recalibrated.
6. ** QC check must be performed prior to sampling and following completion of sampling, at a minimum. QC checks must be performed with calibration standard from a separate lot # as the initial QC.
7. % Recovery = (Value Obtained, pmhos/cm . True Value, pmhos/cm) x 100
8. NC Field Laboratory Certificate Number 5445
9. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
10. Unless otherwise noted, all DO calibrations and measurements are performed at 0 ppt Salinity.
11. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
pmhos/cm: micromhos per centimeter NTU: nephelometric turbidity units
Temperature: SM 2550 B-2010
*C: degrees Celsius OFF: oxidation reduction potential
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: dissolved oxygen s/n: serial number
DO: SM 4500 O G-2011
mg/L: milligrams per liter S.U.: standard units
PH: SM 4500-H` B-2011
mV: millivolt Spec. Cond, Specific Conductivity
Turbidity. SM 2130 B-2011
Page 1 of 1
Attachment 3
Stormwater Discharge Outfall Qualitative
Monitoring Reports
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ 0 / 3 /0 /0 /0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0/3/0/4/9/9 /
Facility Name:
County: McDowell
Crane Resistoflex
Inspector: Christian Patterson (Anchor QEA)
Date of Inspection: 03-31-21
Time of Inspection: 9:35
Total Event Precipitation (inches): 0.99
Phone No. 828-771-0375
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. of-001
Receiving Stream:
Catawba River
a�oa� C oa�P"" ' A —A IC o,-roc,,aa, ama b 9 �a cbm �US
Structure (pipe, ditch, etc.): Pipe
Describe the industrial activities that occur within the outfall drainage area: Metal fabrication
Page 1 of 2
SWU-242, Last modified 06/01/2018
N/A
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear
N/A 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
N/A and 5 is very cloudy:
lO 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
N/A stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
Ol 2 3 4 5
N/A 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 O2 3 4 5
N/A 7. Is there any foam in the stormwater discharge? Q Yes o No.
N/A g, Is there an oil sheen in the stormwater discharge? QYes Q No.
N/A 9. Is there evidence of erosion or deposition at the outfall? Q Yes Q No.
N/A 10. Other Obvious Indicators of Stormwater Pollution:
List and describe No obvious indicators of stormwater pollution
Notes:
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ 0 / 3 /0 /0 /0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0/3/0/4/9/9 /
Facility Name:
County: McDowell
Crane Resistoflex
Inspector: Christian Patterson (Anchor QEA)
Date of Inspection: 03-31-21
Time of Inspection: 10:15
Total Event Precipitation (inches): 0.99
Phone No. 828-771-0375
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. of-002
Receiving Stream:
Catawba River
a�oa� C oa�P"T ' A —A IC o,-roc,,aa, ama b 9 �a cbm �US
Structure (pipe, ditch, etc.): Pipe
Describe the industrial activities that occur within the outfall drainage area: Metal fabrication
Page 1 of 2
SWU-242, Last modified 06/01/2018
N/A
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear
N/A 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
N/A and 5 is very cloudy:
lO 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
N/A stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
Ol 2 3 4 5
N/A 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
Ol 2 3 4 5
N/A 7. Is there any foam in the stormwater discharge? Q Yes a No.
N/A g, Is there an oil sheen in the stormwater discharge? QYes Q No.
N/A 9. Is there evidence of erosion or deposition at the outfall? Q Yes Q No.
N/A 10. Other Obvious Indicators of Stormwater Pollution:
List and describe No obvious indicators of stormwater pollution
Notes:
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018
Attachment 4
Semiannual Stormwater Discharge
Monitoring Report
NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG03 0 4 9 9� Person Collecting Samples: Christian Patterson
Facility Name: crane Resistoflex Laboratory Name: Pace analytical
Facility County: McDowell Laboratory Cert. No.: 40
Discharge during this period: X Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes *No
If so, which Tier (I, II, or III)?
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in
Parameter
Parameter
Outfall 1
Outfall 2
Outfall
Outfall
Outfall
Code
N/A
Receiving Stream Class
C
C
N/A
Date Sample Collected MM/DD/YYYY
03/31/2021
03/31/2021
46529
24-Hour Rainfall in inches
0.99
0.99
00552
Non -Polar Oil & Grease in mg/L (15)
<5.0
<5.0
C0530
TSS in mg/L (100 or 50*)
17.8
7.6
00400
pH in standard units (6.0-9.0)
5.4
6.3
NCOIL
New Motor/Hydraulic Oil Usage in
0
0
gal/month
<0.005
01119
Copper, total recoverable in mg/L
<0.005
(0.010 FW, 0.005 SW)
01051
Lead, total recoverable in mg/ L
<0.005
<0.005
(0.075 FW, 0.220 SW)
01094
Zinc, total recoverable in mg/ L (0.126
0.0491
0.0712
FW, 0.095 SW)
78141 1
Total Toxic Organics (TTO) in mg/L(1)
NO
ND
Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L.
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations,Yi r � n
2� �f
Signature of ermitte it'rri-ited Authorized Individual Dat
Attachment 5
Laboratory Analytical Report and
Chain -of -Custody Form
(�Ia'ne Analytical
www.pacelabs.com
April 06, 2021
Mr. Robert Cork
Anchor QEA
231 Haywood Street
Asheville, NC 28801
RE: Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
Dear Mr. Cork:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
Enclosed are the analytical results for sample(s) received by the laboratory on March 31, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
C'�e -
Lorri Patton
lorri.patton@pacelabs.com
1(828)254-7176
Project Manager
Enclosures
cc: Mr. Christian Patterson, Anchor QEA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16
(�Ia'ne Analytical
www.pacelabs.cem
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 16
Pace Analytical Services, LLC
(�Ia'ne Ashevihevi Analytical ® Riverside lle, NC 2880404
www.pacelabs.cem (828)254-7176
SAMPLE SUMMARY
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
Lab ID Sample ID Matrix Date Collected Date Received
92530541001 OF-001 Water 03/31/2109:35 03/31/2112:05
92530541002 OF-002 Water 03/31/2110:15 03/31/2112:05
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 16
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SAMPLE ANALYTE COUNT
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92530541001 OF-001 EPA 1664B
CJM
1
PASI-C
EPA200.7 Rev 4.4 1994
SH1
4
PASI-A
EPA200.7 Rev 4.4 1994
SH1
1
PASI-A
SM 254OD-2011
ZMC
1
PASI-A
92530541002 OF-002 EPA 1664B
CJM
1
PASI-C
EPA200.7 Rev 4.4 1994
SH1
4
PASI-A
EPA200.7 Rev 4.4 1994
SH1
1
PASI-A
SM 254OD-2011
ZMC
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
Lab Sample ID Client Sample ID
Method Parameters
92530541001
OF-001
EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 234013)
EPA 200.7 Rev 4.4 1994
Zinc
EPA 200.7 Rev 4.4 1994
Zinc, Dissolved
SM 2540D-2011
Total Suspended Solids
92530541002
OF-002
EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 234013)
EPA 200.7 Rev 4.4 1994
Zinc
EPA 200.7 Rev 4.4 1994
Zinc, Dissolved
SM 2540D-2011
Total Suspended Solids
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
SUMMARY OF DETECTION
Result
Units
Report Limit
Analyzed
2950
ug/L
662
04/02/2118:56
49.1
ug/L
10.0
04/02/2118:56
52.4
ug/L
10.0
04/05/2121:13
17.8
mg/L
2.5
04/03/2112:01
2270
ug/L
662
04/02/2118:59
71.2
ug/L
10.0
04/02/2118:59
68.8
ug/L
10.0
04/05/2121:23
7.6
mg/L
2.5
04/03/2112:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 5 of 16
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
Sample: OF-001
Lab ID: 92530541001 Collected:
03/31/21 09:35
Received: 03/31/21 12:05 Matrix: Water
Parameters
Results Units PQL
MDL
DF
Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L 5.0
5.0
1
04/06/21 13:02
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
ND ug/L 5.0
4.3
1
04/01/2101:49 04/02/2118:56 7440-50-8
Lead
ND ug/L 5.0
4.5
1
04/01/2101:49 04/02/2118:56 7439-92-1
Hardness, Total(SM 234013)
2950 ug/L 662
131
1
04/01/21 01:49 04/02/21 18:56
Zinc
49.1 ug/L 10.0
9.5
1
04/01/2101:49 04/02/2118:56 7440-66-6
200.7 MET ICP, Dissolved
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Zinc, Dissolved
52.4 ug/L 10.0
2.5
1
04/05/21 11:20 04/05/21 21:13 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
17.8 mg/L 2.5
2.5
1
04/03/21 12:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/06/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
Sample: OF-002
Lab ID: 92530541002 Collected:
03/31/21 10:15
Received: 03/31/21 12:05 Matrix: Water
Parameters
Results Units PQL
MDL
DF
Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L 5.0
5.0
1
04/06/21 13:02
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
ND ug/L 5.0
4.3
1
04/01/2101:49 04/02/2118:59 7440-50-8
Lead
ND ug/L 5.0
4.5
1
04/01/2101:49 04/02/2118:59 7439-92-1
Hardness, Total(SM 234013)
2270 ug/L 662
131
1
04/01/21 01:49 04/02/21 18:59
Zinc
71.2 ug/L 10.0
9.5
1
04/01/2101:49 04/02/2118:59 7440-66-6
200.7 MET ICP, Dissolved
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Zinc, Dissolved
68.8 ug/L 10.0
2.5
1
04/05/21 11:20 04/05/21 21:23 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
7.6 mg/L 2.5
2.5
1
04/03/21 12:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/06/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16
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QUALITY CONTROL DATA
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
QC Batch: 611730 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92530541001, 92530541002
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
METHOD BLANK: 3220085 Matrix: Water
Associated Lab Samples: 92530541001, 92530541002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.0 5.0 04/06/21 13:02
LABORATORY CONTROL SAMPLE:
3220086
Spike 1-CS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 19.9
100
64-132
MATRIX SPIKE SAMPLE:
3220087
35621139001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
5.01-1 20
11.2
40
64-132 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/06/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
QC Batch: 610647
Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4
1994
Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92530541001, 92530541002
METHOD BLANK: 3215554
Matrix: Water
Associated Lab Samples: 92530541001, 92530541002
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Copper
ug/L
ND 5.0
4.3 04/02/2117:21
Hardness, Total(SM 2340B)
ug/L
ND 662
131 04/02/21 17:21
Lead
ug/L
ND 5.0
4.5 04/02/2117:21
Zinc
ug/L
ND 10.0
9.5 04/02/2117:21
LABORATORY CONTROL SAMPLE:
3215555
Spike 1-CS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits Qualifiers
Copper
ug/L
500 515
103
85-115
Hardness, Total(SM 2340B)
ug/L
33100 32700
99
85-115
Lead
ug/L
500 489
98
85-115
Zinc
ug/L
500 473
95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3215556 3215557
MS MSD
92529415001
Spike Spike MS
MSD
MS MSD
% Rec
Max
Parameter Units
Result
Cone. Cone. Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
Copper ug/L
30.6
500 500 547
558
103 105
70-130
2
20
Hardness, Total(SM 2340B) ug/L
39500
33100 33100 70200
71500
93 97
70-130
2
20
Lead ug/L
ND
500 500 489
495
97 99
70-130
1
20
Zinc ug/L
53.1
500 500 534
540
96 97
70-130
1
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3215558 3215559
MS MSD
92530269001
Spike Spike MS
MSD
MS MSD
% Rec
Max
Parameter Units
Result
Cone. Cone. Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
Copper ug/L
0.022
500 500 566
556
109 107
70-130
2
20
mg/L
Hardness, Total(SM 2340B) ug/L
25100
33100 33100 58500
59000
101 102
70-130
1
20
Lead ug/L
ND
500 500 506
496
101 99
70-130
2
20
Zinc ug/L
76.3
500 500 572
556
99 96
70-130
3
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/06/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
QC Batch: 611106 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Dissolved
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92530541001, 92530541002
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
METHOD BLANK: 3217579 Matrix: Water
Associated Lab Samples: 92530541001, 92530541002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Zinc, Dissolved ug/L ND 10.0 2.5 04/05/21 21:06
LABORATORY CONTROL SAMPLE: 3217580
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Zinc, Dissolved ug/L 500 481 96 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3217581 3217582
MS MSD
92530541001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Zinc, Dissolved ug/L 52.4 500 500 523 525 94 94 70-130 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/06/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
QC Batch: 611302 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92530541001, 92530541002
METHOD BLANK: 3218451
Matrix:
Water
Associated Lab Samples: 92530541001, 92530541002
Blank
Reporting
Parameter
Units
Result
Limit
Total Suspended Solids
mg/L
ND
2.5
LABORATORY CONTROL SAMPLE:
3218452
Spike
LCS
Parameter
Units
Conc.
Result
Total Suspended Solids
mg/L
249
226
SAMPLE DUPLICATE: 3218468
92530458009
Dup
Parameter
Units
Result
Result
Total Suspended Solids
mg/L
7400
7900
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
MDL Analyzed Qualifiers
2.5 04/03/2111:58
LCS % Rec
% Rec Limits Qualifiers
91 90-110
Max
RPD RPD Qualifiers
7 25
SAMPLE DUPLICATE: 3218469
92530458011 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 3070 2770 10 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/06/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 16
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QUALIFIERS
Project: Crane Resistoflex C92062-01.01
Pace Project No.: 92530541
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 04/06/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
Project:
Pace Project No.:
Crane Resistoflex C92062-01.01
92530541
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical
Method
Batch
92530541001
OF-001
EPA 1664B
611730
92530541002
OF-002
EPA 1664B
611730
92530541001
OF-001
EPA 200.7 Rev 4.4
1994
610647
EPA 200.7
Rev 4.4
1994
610686
92530541002
OF-002
EPA 200.7 Rev 4.4
1994
610647
EPA 200.7
Rev 4.4
1994
610686
92530541001
OF-001
EPA 200.7 Rev 4.4
1994
611106
EPA 200.7
Rev 4.4
1994
611421
92530541002
OF-002
EPA 200.7 Rev 4.4
1994
611106
EPA 200.7
Rev 4.4
1994
611421
92530541001
OF-001
SM 254OD-2011
611302
92530541002
OF-002
SM 254OD-2011
611302
Date: 04/06/2021 04:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 16
_ aceAna lyfrcal
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: October 28, 2020
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.07
Issuing Authority:
Pace CaroEinas quality Office
Laboratory rec iving samples:
Asheville 7 Eden❑ Greenwood ❑ Huntersville ❑
Raleigh❑
Mechanicsville❑ Atlanta[-] Kernersville❑
ConditionSample Client Name:
Wo: 92530541
##
Upon Receipt
Project
�.�
I
I
Courier: []Fed Ex ❑UPS ❑USPS
❑C ent
I III 11
III
❑ Commercial ❑Pace ❑Other:
92530541
Custody Seal Present? ❑Yes V() Seals Intact? Des
Vo
pate/Initials Person Examining Contents:13�
Packing Material: ❑Bubble Wrap 08ubble Sags ❑None
Other
Biological Tissue Frozen?
[�N/A
[]Yes❑No
Thermomete .
IRGunID:
eXP t []Blue
❑None
�O%l Type of Ice:
2, S S -7 Correction Factor:
Cooler Temp:Add/subtract {°Cj (]
Temp should be above freezing to 5°C
❑Samples out of temp criteria. Samples an ice, cooling process
Cooler Temp Corrected {°C)• Z s s, —]
USDA Regulated Soil N/A,
hasbegun
( water sample)
Did samples oriRinatt5 in a quarantine zone within the United States: CA, NY, or SC (check maps)?
Did samples originate from a foreign source (internationally,
❑Yes [Wo
including Hawaii ano Fuerro wcuir Dries .�
Comments/Discrepancy:
Chain of Custody Present?
es
[-]NO
❑N/A
1.
Samples Arrived within Hold Time?
es
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
jyJNa
❑N/A
3.
Rush Turn Around Time Requested?
❑/Yes
ND
❑NIA
4,
Sufficient Volume?
❑Yes
[-]No
❑N/A
5.
Correct Containers Used?
[]No
[-]NIA
6.
-Pace Containers Used?
DN.
❑N/A
Containers Intact?
frvrY"Ps
❑ND
❑N/A
7.
Dissolved analysis: samples Field Filtered?
❑No
❑NIA
8•
Sample Labels Match COC?
Rl�yes
❑No
❑NIA
9.
�r
-Includes Date/Time/ID/Analysis Matrix:
Vt
Headspace in VOA Vials (>5-6mm)?
El Yes
❑No
[�JN,A
10.
Trip Blank Present?
[]Yes
❑No
N/A
11.
Trip Blank Custody Seals Present?
Dyes
❑No
PN/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager 5RF Review:
pate/Time:
Field Data Required? ❑Yes ❑No
tot ID of split containers:
Date:
Date: =i--)-
Page 14 of 16
Document Name: Document Revised: October 28, 2020
Sample Condition Upon Receipt(SCUR) Page 2 of 2
/!2ceAnalXical' Document No.: Issuing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project #
verified and within the acceptance range for preservation
samples,
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
wo#:9253ob41
PM: UP Due Date: 04/07/21
CLIENT: 93—ALTAMONT
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