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Home My WebLink AboutNCG060412_2021 DMR_20210419NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG060000 Food and Kindred Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDFS Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG06 0412 Person Collecting Samples: Parker Cliatt Facility Name: Amazon.com Services LLC - CLT9 Laboratory Name: Eurofins TestAmerica Facility County: Mecklenburg Laboratory Cert. No.: 269 Discharge during this period:❑✓ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes ✓❑ No If so, which Tier (I, II, or III)? A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR ✓❑ Yes ❑ No Date Uploaded: Li Aot (Z.0Zk Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Parameter Outfall001 Outfall002 Outfall Outfall Outfall Code N/A Receiving Stream Class WS WS N/A Date Sample Collected MM/DD/YYYY 3/31/2021 3/31/2021 46529 24-Hour Rainfall in inches 0.44 0.44 C0530 TSS in mg/L (100 or SO*) 5.2 20 00400 pH in standard units (6.0 — 9.0) 8.17 8.33 00556 Oil & Grease in mg/L (30) 4.2 2.2 31616 Fecal Coliform per 100 ml of N/A N/A freshwater (if required) (1000) 61211 Enterococci per 100 ml of saltwater N/A N/A (if required) (500) Chemical Oxygen Demand in mg/L 13 00340 (120) < 5 Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month N/A N/A 00552 Non -Polar Oil & Grease in mg/L (15) N/A N/A * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of SO mg/L. All other water classifications have a benchmark of 100 mg/L Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." J_y (�_� 1-1 I lct 1 TO-24 Signature of Permittee or Delegated Authorized Individual Date Email Address nickensa@amazon.com Phone Number (916) 606-1485 urofins Environment Testing America ANALYTICAL REPORT Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-197118-1 Client Project/Site: Storm Water - Amazon Warehouses (CLT9) rof ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade Authorized for release by: 41912021 3:14:27 PM Lauren Evans, Project Manager 1 (615)301-5034 Lauren.Evans@Eurofinset.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: ERM-West Job ID: 680-197118-1 Project/Site: Storm Water - Amazon Warehouses (CLT9) Qualifiers General Chemistry Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. II Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRIES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins TestAmerica, Savannah Page 2 of 14 4/9/2021 Sample Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (CLT9) Job ID: 680-197118-1 Lab Sample ID Client Sample ID Matrix Collected Received Asset ID 680-197118-1 CLT9_Sample_Point_01_20210331 Water 03/31/2114:08 04/05/2110:20 680-197118-2 CLT9_Sample_Point_02_20210331 Water 03/31/2114:27 04/05/2110:20 Eurofins TestAmerica, Savannah Page 3 of 14 4/9/2021 Case Narrative Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (CLT9) Job ID: 680-197118-1 Laboratory: Eurofins TestAmerica, Savannah Narrative Job ID: 680-197118-1 F47 Job Narrative 680-197118-1 Comments No additional comments. Receipt The samples were received on 4/5/2021 10:20 AM. Unless otherwise noted below, the samples arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 1.50 C. General Chemistry Method SM 2540D: The sample duplicate precision for the following sample associated with analytical batch 680-662840 was outside control limits: (680-197041-A-1 DU). The associated Laboratory Control Sample / Laboratory Control Sample Duplicate (LCS/LCSD) precision met acceptance criteria. Methods 410.4: The native sample, matrix spike, and matrix spike duplicate (MS/MSD) associated with batch 663054 were performed at the same dilution. Due to the additional level of analyte present in the spiked samples, the concentration of COD in the MS/MSD was above the instrument calibration range. The data have been reported and qualified. Methods 1664A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 680-663438. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 4 of 14 4/9/2021 Client Sample Results Client: ERM-West Job ID: 680-197118-1 Project/Site: Storm Water - Amazon Warehouses (CLT9) Client Sample ID: CLT9_ Sample_Point_01_20210331 Lab Sample ID: 680-197118-1 Date Collected: 03/31/21 14:08 Matrix: Water Date Received: 04/05/21 10:20 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac HEM (Oil & Grease) 4.2 J 5.0 1.4 mg/L 04/09/21 06:56 04/09/21 09:06 1 Total Suspended Solids 5.2 5.0 5.0 mg/L 04/05/21 15:03 1 Chemical Oxygen Demand <5.0 10 5.0 mg/L 04/06/21 17:22 1 Eurofins TestAmerica, Savannah Page 5 of 14 4/9/2021 Client Sample Results Client: ERM-West Job I D: 680-197118-1 Project/Site: Storm Water - Amazon Warehouses (CLT9) Client Sample ID: CLT9_ Sam ple_Point_02_20210331 Lab Sample ID: 680-197118-2 Date Collected: 03/31/21 14:27 Matrix: Water Date Received: 04/05/21 10:20 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac HEM (Oil & Grease) 2.2 J 5.0 1.4 mg/L 04/09/21 06:56 04/09/21 09:06 1 Total Suspended Solids 20 10 10 mg/L 04/05/21 15:03 1 Chemical Oxygen Demand 13 10 5.0 mg/L 04/06/21 17:23 1 Eurofins TestAmerica, Savannah Page 6 of 14 4/9/2021 QC Sample Results Client: ERM-West Job I D: 680-197118-1 Project/Site: Storm Water - Amazon Warehouses (CLT9) Method: 1664A - HEM and SGT-HEM Lab Sample ID: MB 680-663438/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 663492 Prep Batch: 663438 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac HEM (Oil & Grease) <1.4 5.0 1.4 mg/L 04/09/21 06:56 04/09/21 09:06 1 Lab Sample ID: LCS 680-663438/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 663492 Prep Batch: 663438 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits HEM (Oil & Grease) 40.0 37.20 mg/L 93 78 - 114 Lab Sample ID: LCSD 680-663438/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 663492 Prep Batch: 663438 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit HEM (Oil & Grease) 40.0 36.40 mg/L 91 78- 114 2 18 Method: 2540 D-2011 - Total Suspended Solids (Dried at 103-105°C) Lab Sample ID: MB 680-662840/1 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 662840 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Total Suspended Solids <2.5 2.5 2.5 mg/L 04/05/21 15:03 1 Lab Sample ID: LCS 680-662840/2 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 662840 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 951 900 mg/L 95 80- 120 Lab Sample ID: LCSD 680-662840/3 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 662840 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 951 910 mg/L 96 80- 120 1 25 Method: 410.4-1993 R2.0 - COD Lab Sample ID: MB 680-663054/3 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 663054 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chemical Oxygen Demand <5.0 10 5.0 mg/L 04/06/21 17:21 1 Eurofins TestAmerica, Savannah Page 7 of 14 4/9/2021 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (CLT9) Method: 410.4-1993 R2.0 - COD (Continued) Lab Sample ID: LCS 680-663054/4 Matrix: Water Analysis Batch: 663054 Job I D: 680-197118-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 50.0 50.6 mg/L 101 90-110 Page 8 of 14 Eurofins TestAmerica, Savannah 4/9/2021 QC Association Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (CLT9) General Chemistry Analysis Batch: 662840 Lab Sample ID 680-197118-1 680-197118-2 MB 680-662840/1 LCS 680-662840/2 LCSD 680-662840/3 Analysis Batch: 663054 Client Sample ID C LT9_Sample_Point_01 _20210331 CLT9_Sample_Point_02_20210331 Method Blank Lab Control Sample Lab Control Sample Dup Prep Type Matrix Total/NA Water Total/NA Water Total/NA Water Total/NA Water Total/NA Water Job ID: 680-197118-1 Method Prep Batch 2540 D-2011 2540 D-2011 2540 D-2011 2540 D-2011 2540 D-2011 Lab Sample ID Client Sample ID Prep Type Matrix Method 680-197118-1 CLT9_Sample_Point_01_20210331 Total/NA Water 410.4-1993 R2.0 680-197118-2 CLT9_Sample_Point_02_20210331 Total/NA Water 410.4-1993 R2.0 MB 680-663054/3 Method Blank Total/NA Water 410.4-1993 R2.0 LCS 680-663054/4 Lab Control Sample Total/NA Water 410.4-1993 R2.0 Prep Batch: 663438 Lab Sample ID Client Sample ID Prep Type Matrix Method 680-197118-1 CLT9_Sample_Point_01_20210331 Total/NA Water 1664A 680-197118-2 CLT9_Sample_Point_02_20210331 Total/NA Water 1664A MB 680-663438/1-A Method Blank Total/NA Water 1664A LCS 680-663438/2-A Lab Control Sample Total/NA Water 1664A LCSD 680-663438/3-A Lab Control Sample Dup Total/NA Water 1664A Analysis Batch: 663492 Prep Batch Prep Batch Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-197118-1 CLT9_Sample_Point_01_20210331 Total/NA Water 1664A 663438 680-197118-2 CLT9_Sample_Point_02_20210331 Total/NA Water 1664A 663438 MB 680-663438/1-A Method Blank Total/NA Water 1664A 663438 LCS 680-663438/2-A Lab Control Sample Total/NA Water 1664A 663438 LCSD 680-663438/3-A Lab Control Sample Dup Total/NA Water 1664A 663438 Page 9 of 14 Eurofins TestAmerica, Savannah 4/9/2021 Lab Chronicle Client: ERM-West Job ID: 680-197118-1 Project/Site: Storm Water - Amazon Warehouses (CLT9) Client Sample ID: CLT9_ Sample_Point_01_20210331 Lab Sample ID: 680-197118-1 Date Collected: 03/31/21 14:08 Matrix: Water Date Received: 04/05/21 10:20 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 1664A 501 mL 500 mL 663438 04/09/21 06:56 JAS TAL SAV Total/NA Analysis 1664A 1 663492 04/09/21 09:06 JAS TAL SAV Instrument ID: NoEquip Total/NA Analysis 2540 D-2011 1 500 mL 1000 mL 662840 04/05/21 15:03 PG TAL SAV Instrument ID: NOEQUIP Total/NA Analysis 410.4-1993 R2.0 1 2 mL 2 mL 663054 04/06/21 17:22 MCL TAL SAV • Instrument ID: SPC7 Client Sample ID: CLT9_ Sam ple_Point_02_20210331 Lab Sample ID: 680-197118-2 Date Collected: 03/31/21 14:27 Matrix: Water Date Received: 04/05/21 10:20 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 1664A 496 mL 500 mL 663438 04/09/21 06:56 JAS TAL SAV Total/NA Analysis 1664A 1 663492 04/09/21 09:06 JAS TAL SAV Instrument ID: NoEquip Total/NA Analysis 2540 D-2011 1 250 mL 1000 mL 662840 04/05/21 15:03 PG TAL SAV Instrument ID: NOEQUIP Total/NA Analysis 410.4-1993 R2.0 1 2 mL 2 mL 663054 04/06/21 17:23 MCL TAL SAV Instrument ID: SPC7 Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 10 of 14 4/9/2021 Accreditation/Certification Summary Client: ERM-West Job I D: 680-197118-1 Project/Site: Storm Water - Amazon Warehouses (CLT9) Laboratory: Eurofins TestAmerica, Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (VWV/SVV) State 269 12-31-21 Eurofins TestAmerica, Savannah Page 11 of 14 4/9/2021 Method Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (CLT9) Job ID: 680-197118-1 Method Method Description Protocol Laboratory 1664A HEM and SGT-HEM 1664A TAL SAV 2540 D-2011 Total Suspended Solids (Dried at 103-105°C) SM TAL SAV 410.4-1993 R2.0 COD MCAVWV TAL SAV 1664A HEM and SGT-HEM (Aqueous) 1664A TAL SAV Protocol References: 1664A= EPA-821-98-002 MCAVVW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 12 of 14 4/9/2021 H 4- d A v` c r w ai 0 Z ,0,. ,$�E Q. h t = z v, a =aziz o ° Fo E A 2zOn.p¢v,�»3n, 2 � ° � ci cg ci 0 C d a Q U a, y� Q a, �J z m y Im rn m h n a v m c._ R E ❑ p w 2 2N22S Q Q $�jw W w` ` t O O 1L Q m 2j j l -O j 'y 2 L*u)ejuoo}oiagwnNRiol m OD 1 d E .� V z � I �� Q ro E m ❑ ❑ S ❑ — � as F E 6i a q m U Q d h m O a� w 5 H O 8 R U c �cp w m a V o \ o E (SS1) sPlloS paPuadsng leiol OOt9l 0 {° a a c �� t n--_. a E w J003) pucw&a u*8Ax0 leolwo40. 00ZZ9 O $ m a: cc 0 (02eu0 y 110) W3H - MU n v� �n E (ON A) Oswm Moped > > i- (ON jo ssA) gdwe$ Pajinl!d PIBId 1 a N ❑ L M 8 `8 g m c O E 0 E 0 EEp U N N m E 2 CL E 5, a V iJ m 1.- 11 a a �1 d) co p ❑ � Z o h u, ❑' �a 0.N0 N a 0 0 0 � d O M 0 N O z° (0 co v a ' p a E 0 o y a y aDi — 2i R co _ o �' Q{ m t a m y Viz° a n (D v (d U c1 = c l Nto m m d � a, a d N 0 � 2 - c 04 3 Z Z y a 7 'j Q� 'j N U V OO w a° I v Z umi U a c w a a Q N cn 4� 0 w U Page 13 of 14 4/9/2021 Login Sample Receipt Checklist Client: ERM-West Job Number: 680-197118-1 Login Number: 197118 List Number: 1 Creator: Banda, Christy S Question List Source: Eurofins TestAmerica, Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins TestAmerica, Savannah Page 14 of 14 4/9/2021