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WQ0001817_Monitoring - 03-2021_20210419 (2)
Monitoring Report Submittal ............................................................................................................................................ Permit Number #* WQ0001817 Name of Facility:* Albemarle Utility Company Month:* March Year:* 2021 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR March MR's.pdf 8.63MB PDF Cnly GW-59 March MW's.pdf 14.36MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address:* danny.perry@albemarleplantation.com Name of Submitter:* Danny S Perry Signature: Date of submittal: 4/19/2021 This will be filled in autocratically Initial Review Reviewer: Williams, Kendall Is the project number correct?* WQ0001817 Is the monitoring report Yes r No accepted?* Regional Office* Washington Accepted Date: 4/19/2021 SUBMIT FORM ON YELLOW PAPER ONLY , • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Comapany Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island RD TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford N.0 27944 County Perqimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: North of Holding Lagoon _ No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -1 Date sample collected: 3/26/2021 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 6.67 units Temp. 000lo: 1 5.9 °C DRY at Depth to Water Level 82546: 9.4 ft. below measuring point Screened Interval: -5 ft. to -20 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Strong Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance White/Tan/Turb here:❑ Samples for metals were collected unfiltered: ❑ YES Ml NO and field acidified: ❑ YES N NO LABORATORY INFORMATION Date sample analyzed:3/26/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.13 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids -.Total 70300 269 mg/L Al - Aluminum 01105 mg/L pid (Lab) 00403 6.67 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 22 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3 as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCS: mg/L VOC Removal% Shayne Byrum Corporate Secretary Permitter (or Authorized Agent) Name and Title - Please print or type Siq?!Mre bf ROrnittee ((Ir Authorized Agent) G'>rv-59 Rev.05-07-2018 SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 9 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2021 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12324 Site: MW-1 3/26/2021 9:10 AM Water Jay Baker Test Method Results Date Analyzed Color Color White/Tan/Turb 03/26/2021 Depth to water, ft. Depth to Water, Ft. 9.4 feet 03/26/2021 Ammonia Nitrogen EPA 350.1 < 200 pg/L 04/01/2021 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2021 Odor Qualitative Strong Sulfur 03/26/2021 Total Dissolved Solids (TDS) SM 2540 C 269 mg/L 03/29/2021 Temperature SM 2550 B 15.9 C 03/26/2021 Chloride SM 4500 CI E 22 mg/L 03/29/2021 pH SM 4500 H B 6.67 units 03/26/2021 Total Organic Carbon (TOC) SM 5310 B mg/L Fecal Coliform SM 9222D MF <1 Colonies/100ml- 03/26/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 0.13 mg/L 03/26/2021 Nitrate+Nitrite-Nitrogen EPA 3532 0.10 mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/05/2021 Report#:: 2021.04977 Page 1 of 10 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 _ UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name:East of Baffle Lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 3/26/2021 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.60 units Temp. 000lo: 1 6.1 °C DRY at Depth to Water Level 82546: 3.3 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Strong Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Brown here:❑ Samples for metals were collected unfiltered: El YES ® NO and field acidified: [I YES ® NO LABORATORY INFORMATION Date sample analyzed:3/26/2021 Laboratory Name: Environment Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.09 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616� <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 194 mg/L Al - Aluminum o1105 mg/L pH (Lab) 00403 5.60 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride oos4o_ 38 mg/L Cd - Cadmium 01027_ ug/L Arsenic 01002_ ug/L Chromium: Total 01034 ug/L _ Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 3273. ug/L Fe - Iron 01045 ug/L (Specify test and method M ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610_ <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese o1 o55 _ ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum Corporate Secretary Fermittee (or Authorized Agent) Name and Title - Please print or type Authorized Agent) GW-59 Rev. 06-0 -2018 SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info`a environnientalchemists.com Albemarle Utility Date of Report: Apr 05, 2021 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12325 Site: MW-2 3/26/2021 9:20 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan/Brown 03/26/2021 Depth to water, ft. Depth to Water, Ft. 3.3 feet 03/26/2021 Ammonia Nitrogen EPA 350.1 < 200 pg/L 04/01 /2021 Gallons bailed before sampling Gallons Bailed before sampling 5 (dry) gallons 03/26/2021 Odor Qualitative Strong Sulfur 03/26/2021 Total Dissolved Solids (TDS) SM 2540 C 194 mg/L 03/29/2021 Temperature SM 2550 B 16.1 C 03/26/2021 Chloride SM 4500 Cl E 38 mg/L 03/29/2021 pH SM 4500 H B 5.60 units 03/26/2021 Total Organic Carbon (TOC) sM 5310 B mg/L Fecal Coliform SM 9222D MF <1 Colonies/100mL 03/26/2021 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 0.09 mg/L 03/26/2021 Nitrate+Nitrite-Nitrogen EPA 353.2 0.09 mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/05/2021 Report tt 2021-04977 Page 2 of 10 SUBMIT FORM ON YELLOW PAPER ONLY UNDWATER QUALITY MONITORING: PLIANCE REPORT FORM Please Print Clearly or Type Facility Name: Albemarle Utility CompE Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford NC IContact Person: Danny Shelton Perry ORC Well Location/Site Name: South East of Spray field 27944 WELL ID NUMBER (from Permit): MW - 3 Well Depth: 12 ft. Depth to Water Level 82546: 2.6 ft. below measuring point Measuring Point is 3 ft. above land surface Volume of water pumped/bailed before sampling: 3 Samples for metals were collected unfiltered: ❑ YES County Perquimans Telephone#: 252-426-1007 No. of wells to be sampled: 10 Date sample collected: 3/26/2021 Well Diameter: 2 in. Screened Interval: -2 ft. Relative M.P. Elevation: gallons NO and field acidified: ❑ YES LI DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge W00001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: to -12 ft. ft. Date sample analyzed:3/26/2021 Laboratory Name: Environmental Chemists, Inc PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NOZ) as N 00615 0.76 Coliform: MF Fecal 31616 72 colonies /100mL Nitrate (NO3) as N 00620 <0.02 Coliform: MF Total 31504 / 100mL Phosphorus: Total as P 00665 (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 issolved Solids:Totai 70300 961 mg/L AI -Aluminum oilo5 pH (Lab) 00403 5.81 units Ba - Barium 01007 TOC 00680 mg/L Ca - Calcium o0916 Chloride 00940 15 mg/L Cd - Cadmium 01027 Arsenic 01002 ug/L Chromium: Total 01034 Grease and Oils 00552 mg/L Cu - Copper 01042 Phenol 32730 ug/L Fe - Iron 01045 Sulfate 00945 mg/L Hg - Mercury 71900 Specific Conductance 00095 µMhos K - Potassium 00937 Total Ammonia 00610 <0.02 mg/L Mg - Magnesium 00927 (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn -Manganese 01055 TKN as N 00625 mg/L Ni - Nickel 01067 mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L FIELD ANALYSES: pH 00400: 5.81 units Spec. Cond. 00094: Odor 00085: Slight Sulfur Appearance Brown/Turbid Pb - Lead 01051 Zn - Zinc 01092 Certification No. 94 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary f (____ Permittee (or Authorized Agent) Name and Title - Please print or type a of Kermittef Authorized Agent) GW-59 Rev.06-07-2018 If WELL Temp. 000lo: 15.0 °C DRY at Whos I time of 701 [envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax iiifo@environmentalchemists.com environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2021 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12326 Site: MW-3 3/26/2021 9:35 AM Water Jay Baker Test Method Results Date Analyzed Color color Brown/Turbid 03/26/2021 Depth to water, ft. Depth to water. Ft. 2.6 feet 03/26/2021 Ammonia Nitrogen EPA350.1 < 200pg/L 04/01/2021 Gallons bailed before sampling Gallons Bailed before sampling 3 (dry) gallons 03/26/2021 Odor Qualitative Slight Sulfur 03/26/2021 Total Dissolved Solids (TDS) SM 2540 C 961 mg/L 03/29/2021 Temperature SM 2550 B 15.0 C 03/26/2021 Chloride SM 4500 Cl E 15 mg/L 03/29/2021 pH SM 4500 H B 5.81 units 03/26/2021 Total Organic Carbon (TOC) SM 5310 B mg/L Fecal Coliform SM 92220 MF 72 Colonies/100mL 03/26/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 0.76mg/L 03/26/2021 Nitrate+Nitrite-Nitrogen EPA 353.2 0.55 mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/05/2021 Report # 2021-04977 Page 3 of 10 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South West of Spray field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 4 Date sample collected: 3/26/2021 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.12 units Temp. 000lo: 14.6 °C DRY at Depth to Water Level 82546: 2.9 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Slight/Sulfur check Volume of water pumped/bailed before sampling: 3.0 gallons Appearance Brown/Turbid here:❑ Samples for metals were collected unfiltered: ❑ YES M NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed:3/26/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.16 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 192 mg/L Al - Aluminum 01105 mg/L pil (Lab) 00403 6.12 units Ba - Barium 01007 ug/L TOC oo68o mg/L Ca - Calcium 00916 mg/L Chloride 00940 6 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 _ ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 uglL Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945_ mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095_ µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 6eon Zvi ro c h e mn ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infora environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2021 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12327 Site: MW-4 3/26/2021 9:47 AM Water Jay Baker Test Method Results Date Analyzed Color Color Brown/Turbid 03/26/2021 Depth to water, ft. Depth to water, Ft. 2.9 feet 03/26/2021 Ammonia Nitrogen EPA 350.1 < 200 pg/L 04/01 /2021 Gallons bailed before sampling Gallons Bailed before sampling 3 (dry) gallons 03/26/2021 Odor Qualitative Slight Sulfur 03/26/2021 Total Dissolved Solids (TDS) SM 2540 C 192 mg/L 03/29/2021 Temperature SM 2550 B 14.6 C 03/26/2021 Chloride SM 4500 Cl E 6 mg/L 03/29/2021 pH SM 4500 H B 6.12 units 03/26/2021 Total Organic Carbon (TOC) SM 5310 B mg/L Fecal Coliform SM 9222D MF <1 Colonies/100mL 03/26/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 0.05 mg/L 03/26/2021 Nitrate+Nitrite-Nitrogen EPA 353.2 0.21 mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method 0.16 mg/L 04/05/2021 Report # 2021-04977 Page 4 of 10 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 _ County Perquimans X Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South West of Sprayfield No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 5 Date sample collected: 3/26/2021 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.59 units Temp. 000lo: 14.7 °C DRY at Depth to Water Level 82546: 4.5 ft. below measuring point Screened Interval: 12 ft. to 2 _ ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Turbid here:r Samples for metals were collected unfiltered: ❑ YES © NO and field acidified: ❑ YES ® NO u LABORATORY INFORMATION Date sample analyzed:3/26/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.08 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 365 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.59 units Ba - Barium 01007 ^mg/L ug/L TOG 00680 mg/L Ca - Calcium 00916 _ Chloride 00940 68 rng/L Cd - Cadmium 01027 ug/L .Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NHaas N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only Total • certify that, to the best of my knowledge and belief the information submitted in this report is true. aca DWR-certified laboratory. I am aware that there are significant penalties for submitting false information Corporate Secretary mg/L Effluent Total VOCs: Permiftee (or Authorized Agent) Name and Title - Please print or type SignaitlR—of PernWee (or Vorized Agent) GW-59 Rev.06-07-2018 mg/L VOC Removal% envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax itifo@environmentalchemists.com Albemarle Utility Date of Report: Apr 05. 2021 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12328 Site: MW-5 3/26/2021 10:00 AM Water Jay Baker Test Method Results Date Analyzed Color color Tan/Turbid 03/26/2021 Depth to water, ft. Depth to water, Ft. 4.5 feet 03/26/2021 Ammonia Nitrogen EPA 350.1 < 200 pg/L 04/01 /2021 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2021 Odor Qualitative None 03/26/2021 Total Dissolved Solids (TDS) SM 2540 C 365 mg/L 03/29/2021 Temperature SM 2550 B 14.7 C 03/26/2021 Chloride SM 4500 CI E 68 mg/L 03/29/2021 pH SM 4500 H B 6.59 units 03/26/2021 Total Organic Carbon (TOC) SM 5310 B mg/L Fecal Coliform SM 9222D MF <1 Colonies/100ml- 03/26/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 03/26/2021 Nitrate+Nitrite-Nitrogen EPA 353.2 0.08 mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method 0.08 mg/L 04/05/2021 Report #:: 2021-04977 Page 5 of 10 SUBMIT FORM ON YELLOW PAPER ONLY • . DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-25-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery 001 Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone,#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West Of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 6 Date sample collected: 3/26/2021 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.50 units Temp. 000lo: 14.8 °C DRY at Depth to Water Level 82546: 4.4 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: [Mhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Strong Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here: Samples for metals were collected unfiltered: ❑ YES NO and field acidified: ❑ YES 0 NO LABORATORY INFORMATION Date sample analyzed:3/26/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.04 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 952 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.50 units Ba - Barium 01007 _ 11 TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 363 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 11 Chromium: Total 01034 11 Grease and Oils 00552 ri Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 11 Fe - Iron 01045 11 (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 11 Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 I,tMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 ri method # _ (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 11 , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only • certify that. to the best of my knowledge and belief. the information submitted in this report is true. acct DWR-certified laboratory. I am aware that there are, significant penalties for submitting false information Corporate Secretary mg/L Effluent Total VOCs: Permittee (or Authorized Agent) Name and Title - Please print or type Sig7L!AfdFoXKermitt7r Authorized Agent) GW-59 Rev.06-07-2018 /V/ mg/L VOC Removal% [envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc, 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2021 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12329 Site: MW-6 3/26/2021 10:14 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan/Clear 03/26/2021 Depth to water, ft. Depth to water, Ft. 4.4 feet 03/26/2021 Ammonia Nitrogen EPA 350.1 < 200 pg/L 04/01/2021 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2021 Odor Qualitative Strong Sulfur 03/26/2021 Total Dissolved Solids (TDS) SM 2540 C 952 mg/L 03/29/2021 Temperature SM 2550 B 14.8 C 03/26/2021 Chloride SM 4500 Cl E 363 mg/L 03/29/2021 pH SM 4500 H B 6.50 units 03/26/2021 Total Organic Carbon (TOC) SM 5310 B mg/L Fecal Coliform SM 9222D MF <1 Colonies/100mL 03/26/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 0.04 mg/L 03/26/2021 Nitrate+Nitrite-Nitrogen EPA 353.2 0.04 mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/05/2021 Report #:: 2021-04977 Page 6 of 10 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MQNI T ORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM WON_ 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans M Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location!Site Name: West of Baffle lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 7 Date sample collected: 3/26/2021 FIELD ANALYSES: WAS Well Depth: 16.9 ft. Well Diameter: 2 in. pH 00400: 7.03 units Temp. 000lo: 23.6 °C DRY at Depth to Water Level 82546: 0.5 ft. below measuring point Screened Interval: 11.9 ft. to 16.9 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 10 gallons Appearance Red/Tan here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES NO LABORATORY INFORMATION Date sample analyzed:3/26/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.04 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 rng/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use NSPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 359 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 7.03 units Ba - Barium 01007 ug/L TOC oo68o mg/L Ca - Calcium 00916 mg/L `ug/L Chloride 00940 49 mg/L Cd - Cadmium 01027 A Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552__ mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625� mg/L Ni - Nickel 01os7 ug/L method # For Remediation Systems Only (Attach Lab Reports): influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Pe mittee (or Authorized Agent) Name and Title - Please print or type Agent) GW-59 Rev.06-07-2018 49 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Pax ANALYTICAL & CONSULTING CHEMISTS infolu environtnentalchemists.com Albemarle Utility Date of Report: Apr 05, 2021 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12330 Site: MW-7 3/26/2021 8:55 AM Water Jay Baker Test Method Results Date Analyzed Color Color Red/Tan 03/26/2021 Depth to water, ft. Depth to Water, Ft. 0.5 feet 03/26/2021 Ammonia Nitrogen EPA 350.1 < 200 pg/L 04/01/2021 Gallons bailed before sampling Gallons Bailed before sampling 10 gallons 03/26/2021 Odor Qualitative None 03/26/2021 Total Dissolved Solids (TDS) SM 2540 c 359 mg/L 03/29/2021 Temperature SM 2550 B 23.6 C 03/26/2021 Chloride SM 4500 Cl E 49 mg/L 03/29/2021 pH SM 4500 H B 7.03 units 03/26/2021 Total Organic Carbon (TOC) SM 5310 B mg/L Fecal Coliform SM 9222D MF <1 Colonies/100mL 03/26/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.04 mg/L 03/26/2021 Nitrate+ N itrite-Nitrogen EPA 353.2 < 0.02 mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/05/2021 Report #. 2021-04977 Page 7 of 10 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ001817 UIC_ Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford INC 27944 County Perquimans _ J ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: East of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 8 Date sample collected: 3/26/2021 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.31 units Temp. 000lo: 15.6 °C DRY at Depth to Water Level P2546: 4.2 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: uMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear _ here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed:3/26/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 < 0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.43 mg/L. Zn - Zinc 01092 mg/L Coliform: MF Total 31504 / 100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 R mg/L Other (Specify Compounds and Concentration Units): .issolved Solids:Total 70300 447 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.31 units Ba - Barium 01007 ug/L TOG 00630 mg/L Ca - Calcium 00916 mg/L Chloride 00940 142 mg/L Cd - Cadmium 01027 _ ug/L Arsenic 01002 ug/L Chromium: Total 01034 ^ smg/L ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 ORGANICS: (by GC, GC/MS, HPLC) Pheno! 32730� ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L _ method # (Aminonia Nitrogen; NH,as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N C0625 m� mg/L Ni - Nickel 01067 �a ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Rev. 06-07-2018 GW-59 :envirrochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info aenvironmentalchemists.coiil Albemarle Utility Date of Report: Apr 05, 2021 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12331 Site: MW-8 3/26/2021 10:30 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan/Clear 03/26/2021 Depth to water, ft. Depth to Water, Ft. 4.2 feet 03/26/2021 Ammonia Nitrogen EPA 350.1 < 200 pg/L 04/01 /2021 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2021 Odor Qualitative None 03/26/2021 Total Dissolved Solids (TDS) SM 2540 c 447 mg/L 03/29/2021 Temperature SM 2550 B 15.6 C 03/26/2021 Chloride SM 4500 cl E 142 mg/L 03/29/2021 pH SM 4500 H B 6.31 units 03/26/2021 Total Organic Carbon (TOC) SM 5310 B mg/L Fecal Coliform SM 9222D MF <1 Colonies/100ml- 03/26/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 03/26/2021 Nitrate+Nitrite-Nitrogen EPA 353.2 0.43 mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method 0.43 mg/L 04/05/2021 Report # 2021-04977 Page 8 of 10 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑0 Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 9 Date sample collected: 3/26/2021 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.37 units Temp. 000lo: 14.9 °C DRY at Depth to Water Level 82546: 4.3 ft. below measuring point Screened Interval. 4 ft. to 14 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here: Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed:3/2612021 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.09 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) _/100mL Orthophosphate 70507 �mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 67 mg/L Ai - Aluminum 01105 _ mg/L pH (Lab) 00403 6.37 units Ba - Barium 01007 _ ug/L TOG 00680 mg/L Ca - Calcium 00916 _ mg/L Chloride 00940 6 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method A ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # T ctal Ammonia 00610 <0-2 _ mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese oio55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permittee (or Authorized Agent) Name and Title - P!e3se print or type SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910,392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchetnists.coni Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Apr 05, 2021 Customer PO #: Customer ID: 09110024 Report#: 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12332 Site: MW-9 3/26/2021 11:00 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/26/2021 Depth to water, ft. Depth to Water, Ft 4.3 feet 03/26/2021 Ammonia Nitrogen EPA 350.1 < 200 pg/L 04/01/2021 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2021 Odor Qualitative None 03/26/2021 Total Dissolved Solids (TDS) SM 2540 C 67 mg/L 03/29/2021 Temperature SM 2550 B 14.9 C 03/26/2021 Chloride SM 4500 Cl E 6 mg/L 03/29/2021 pH SM 4500 H B 6.37 units 03/26/2021 Total Organic Carbon (TOC) SM 5310 B mg/L Fecal Coliform SM 9222D MF <1 Colonies/100ml- 03/26/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 03/26/2021 Nitrate+Nitrite-Nitrogen EPA353.2 0.09mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method 0.09 mg/L 04/05/2021 Report #:: 2021-04977 Page 9 of 10 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford N.C. 27944 County Perquimans 0 Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10 Date sample collected: 3/26/2021 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.48 units Temp. 000lo: 15.1 °C DRY at Depth to Water Level 82546: 6.0 ft. below measuring point Screened Interval: 5 ft. to 14 ft. Spec. Cond. 00094: µ time ofMhos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/tan here:r-� Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed:3/26/2021 Laboratory Name: Environmental Chemists„ Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.59 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 140 mg/L Al - Aluminum oil o5 mg/L pH (Lab) 00403 6-48 units Ba - Barium 01007 ug/L TOC 00680� mg/L Ca - Calcium 00916 mg/L Chloride 00940 35 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 i mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen. Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: i certify that. to the best of my knowledge and belief. the information submitted in this report is true. aca DWR-certified laboratory. I am aware that there are significant penalties for submitting false information CorporateShayne Byrum mg/L Effluent Total VOCs: Permittee (or Authorized Agent) Name and Title - Please print or type Signatl"_- ermWe (or Vorized Agent) GW-59 Rev.06-07-2018 mg/L VOC Removal% envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2021 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report M 2021-04977 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-12333 Site: MW-10 3/26/2021 10:45 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/26/2021 Depth to water, ft. Depth to water, Ft. 6.0 feet 03/26/2021 Ammonia Nitrogen EPA350.1 < 200pg/L 04/01/2021 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2021 Odor Qualitative None 03/26/2021 Total Dissolved Solids (TDS) SM 2540 C 140 mg/L 03/29/2021 Temperature SM 2550 B 15.1 C 03/26/2021 Chloride SM 4500 CI E 35 mg/L 03/29/2021 pH SM 4500 H B 6.48 units 03/26/2021 Total Organic Carbon (TOC) SM 5310 B mg/L Fecal Coliform SM 9222D MF <1 Colonies/100ml- 03/26/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 03/26/2021 Nitrate+Nitrite-Nitrogen EPA 353 2 0.59 mg/L 03/30/2021 Nitrate Nitrogen Subtraction Method 0.59 mg/L 04/05/2021 Comment: Reviewed by: Report # . 2021-04977 Page 10 of 10 GW-59A COMPLIANCE REPORT FORM Permit #W6�0O )9)'1 (Submit one each monitoring period with GW-59 forms.) I Enter date monitoring results were due. Will this monitoring report (GW-59 and GW-59A) be submitted after the established due date? YES NO� 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES'; list in the space provided below the well identification number(s) and i explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? ff the answer is "Yes ", contact the Regional Office. for guidance. 4 Are any monitored constituents equal to or above the established standards? YE NO If the answer to question 4 is "NO'; skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: L, U/ M�'� MW 3 �Gb! Mw Co 53_ Io 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? YES NO If the answer to question 5 is `NO'; skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). h ec+ 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly 1 located; contact the Regional Office. I 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES kNO If the answer to question 7 is "YES'; describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. wwdge Perm' a (or Authorized Agent) ate GW-59A 12/8/2003 o LA-3 P14 Grc. d- & , gDol I � qs� 0-q i NIO L L: 6 k-4.; p 9 Ii - --\ Jgj 1-4 zf lu lor, tj e- ypn -77 Lo G 9 nw «,,37 TG N.5 hi 71(p os co