NC0087513_Regional Office Historical File Pre 2018 (2)

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross, Jr., Secretary
Gregory J. Thorpe, Ph.D., Acting Director
April 3, 2002
Mr. Chris Branch
The Boulevard. Company
200 West 1.0th Street
Charlotte, North Carolina 28202
Dear Mr. Branch:
Subject: Permit No. NC0087513
ATC Number 087513A01
The Boulevard Company
Mecklenburg County
The Division received a letter of request for Authorization to Construct on November 1, 2001.
Plans and specifications for the subject project have been reviewed and found to be satisfactory.
Authorization is hereby granted. for the installation of a groundwater remediation system. Specifically,
this ATC allows the installation of:
a transfer tank,
primary and back-up transfer pumps with on/off and high -high float switches,
�► a dual bag filter system,
two liquid -phase granular activated carbon (GAC)vessels,
flow meter, and
• a control panel with an automated phone dialer
This groundwater remediation system will discharge the treated effluent into an urnnarned
tributary of Little Sugar Creek in the Catawba River Basin.
This Authorization to Construct is issued in accordance with Part H1, Paragraph C of NPDES
Pennit No. NCOO87513 issued October 10, 2001. and shall be subject to revocation unless the
wastewater treatment facilities are constructed in accordance with the conditions and limitations
specified in Permit No. NC0087513. Failure to abide by the requirements contained in this
Authorization to Construct may subject the Pernnittee to an enforcement action by the Division of Water
Quality in accordance with North Carolina General Statute 143-215.6A to 143-215.6C. The issuance of
this Authorization to Construct does not preclude the Permittee from complying with any and all
statutes, rules, regulations, or ordinances which may be imposed by other government agencies (local,
state, and federal) which have jurisdiction.
In the event that the facility fails to perform satisfactorily, including the creation of nuisance
conditions, the Permittee shall take immediate corrective action, including those as may be required by
this Division, such as the construction of additional or replacement wastewater treatment or disposal
facilities..
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Permit No. NC0087513
Authorization to Construct
The Boulevard Company
April 3, 2002
Page 2
The Mooresville Regional Office, telephone nurnber [phone], shall be notified at least
forty-eight (48) hours in advance of operation of the installed facilities so that an on -site inspection can
be made. Such notification to the regional supervisor shall be made during the normal office hours from
8:00 a,m. until 5:00 p.m. on Monday through Friday, excluding State Holidays.
Upon completion of construction and prior to operation of this permitted facility, a certification
must be received from a professional engineer certifying that the permitted facility has been installed in
accordance with the NPDES Permit, this Authorization to Construct, and the approved plans and
specifications. Mail the completed certification to: North Carolina DENR-DWQ, NPDES Unit, 1617
Mail Service Center, Raleigh, NC 27699-1617.
One (1) set of approved plans and specifications is being forwarded to you. A copy of the
approved plans and specifications shall be maintained on site by the Permittee for the life of the facility.
If you have any questions or need additional information, please contact Jacquelyn M. Nowell,
telephone number [phone], extension 512.
Sincerely,
Gregory J. Thorpe, Ph.D.
cc: Central Files
NPDES Unit
Mooresville Regional Office, DWQ
Technical Assistance and Certification

Mr. Chris Branch
The Boulevard (a.,, 715 North Church, LLC
200 West 10th. Street
Charlotte, North Carolina. 28202
Dear Mr, Branch;
Michael F, sley
Governor
William G. Ross, Jr., Secretary_ ,
North Ca aline Department of Environment andNatural ResoureeY'll
Gregory J. Thorpe, PhD., Acting Director ,:77
_Division of Water Quality
August 22, 2001
Subject: Draft NPDES Permit
Permit NC0087513
715 North Church site
Mecklenburg County
Enclosed with this letter is a copy of the draft NPDES permit for the above referenced facility. I
encourage you to review the draft carefully to ensure thorough understanding of the information,
conditions, and requirements contained therein.
As this is a new discharge, I would like to draw your attention to the following conditions in your
draft permit:
• Trichloroethylene (TCE), chloroform,. barium, selenium, and chromium shall be
monitored monthly. These requirements are based on the contaminants found on -site, the
results of LAW Engineering's sampling efforts, and the general permit for groundwater.
remechation.
• A daily maximurn limit of 8.85 ug/L for tetrachloroethylene (PCE) has been added to the
permit. Data from your facility indicates that your discharge has the reasonable potential to
cause a violation of the water quality criteria for PCE. Under Division of Water Quality
(Division) policy, this prompts the need for a limit..
• Arsenic limit and monitoring requirement have been included. Reasonable potential
analysis indicated that effluent from your facility may cause a violation of the state arsenic
standard; a 50 ug/L limit and monthly monitoring have been added accordingly.
• A chromium limit of SO ug/L and monthly monitoring has been included. Data from your
facility indicates that potentially high concentrations of chromium may be in your effluent,
thereby requiring a limit..
• Quarterly monitoring for oil and grease and naphthalene has been included. A 550-gallon
storage tank containing fuel oil was found at the subject site. Under the terms of the general
groundwater rernediation permit for site potentially contaminated by fuel oil, these parameters
must be monitored.
• A chronic toxicity test at 90% has been included. Since you are discharging to a biologically'
impaired. stream., it is crucial to include a toxicity test to ensure that the discharge does not
have any further detrimental effects on Little Sugar Creek. In addition, a special condition to
the permit. has been added indicating that chronic non-compliance with the toxicity
requirement may require that the Boulevard cease the discharge.
N. C. Division cif. Water Quality/ NPDES Unit
16'1.7 Mail Service Center, Raleigh, NC 27699-1617
Internet: h2o.enr,state.nc,us
Phone: [phone]
fax: [phone]
DE.NR Customer Service Center: 1 800 623-7748

Please submit any comments or questions concerning this draft permit no later than thirty (30)
days following receipt of this letter, Cornments should be sent to
Ms. Natalie Sierra
NCDENR DWNPDES Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
If you have any questions or comments concerning this draft permit, please contact me at 919-733
5033 extension 551 or is e-mail at NatahnSierra@hcmailmet. 3
Natalie V, Sierra
NPDES Unit
cc: Mooresville Regional Office/Water Quality Section
NPDES Unit
Aquatic Toxicology Unit
Mecklenburg County Department of Environmental Protection

Permit N00087513
STATE OF NORTH CAROLINA
DEPARTMENT OF EIWIRO NiT NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUT ANT DISCHARGE ELIMINATION SYSTEM
(NPDES)
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and restulations
promulgated and adopted by the North Carolina Environmental Management Coaunission, and the Federal Water Pollution
Control Act, as amended,
The Boulevard @ 715 North Church, LLC
is hereby authorized to discharge wastewater from outtalk located at the
715 North Church Site
715 North Church Street
Charlotte
ec enburg County
to receiving waters designated as an unnamed tributary to Little Sugar Creek in the Catawba River Basin
in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts
Ii II, III and IV hereof
This permit shall become effective: November 1, 2001.
This permit and authorization to discharge shall expire at midnight on September 30, 2006.
Shaded this day
Kerr T. Stevens, Director
Division of Water Quality
By Authority of the Ensarournenta 'Management Commission

is hereby authorized to:
SUPPLE T TO PE T CO R, 1.ET
`
The
Permit NC00875 13
After applying for and re en an Authorization orizat to C nstr t try the Division of W t!
Quality, operate a 0.072 MGD r and ater remediat o . facility located
Church Street, Charlotte, MecklenburgCounty, and
the Boulevard, 705 North
discharge fro said treatment facility at the specified locations (see attached map nto an unnamed
tributary to Little Sugar Creek, a %%aterbody classified as C waters within the Catawba River Basin.

NCOOS75 1 3 - The Boulcvard 7 71 North Church. L.LC
-A1:1L1 A": C2/15NE'CharifAtr;.'::
s-lrzarn Snrin Si
TV2,;:i ROW-, 0.072 N1GD
Facility
Lorton
ard 7:5 Nurch Church, LAX
0 rth NCX«87513
Grourclwritcr Rcraccdiaticc

Perm t NC008 i 51i3
A. (I.) EFFLUENT LIMITATIONS AND MONITORING REQi.1I
Beginning on the effective date of the permit and lasting until expiration, the Pern
from Outfall 001. Such discharges shall be limited and monitored by the Permnitte
EFFLUENT
CHARACTERISTICS
How
�otaT Suspended Solids
t kl and Greasel
richloroethylene (.ICE;)
etrac oroet y. ene
oform
Arsenic
Bari
um
Chromium
°aplit a ene-
Monthly
Average
Daily
aximum
1\1easurernent
Frequency
Continuous
tIENTS - DRAFT
a
is authorized to discharge
pecified below:
Sample
Type
urttp o
Meter
Monthly Composite
(uarterly Ciro
Grab
U1REMENTS
plc Location
vent
uent
Effluent
Grab Effluent.
Mvfonthfy Gra
cent
Monthly Composite Effluent
Monthly
Composite
Nfonthly° Composite
Monthly Composite
Effluent
Effluent
Chronic To
Footnotes:
The grab sample for oil and grease should be skimmed from the surface in a quiescent zone,
such as a holding tank, if possible. If oil and grease is not detected above method detection
limits during the first twelve consecutive sampling events, then the pem7ittee may request that
the monitoring requirement be eliminated,
If naphthalene is not detected above m..ethod detection limits during the first twelve consecutive
sampling events, then the permittee may request that the monitoring requirement be eliminated.
Chronic Toxicity (Ceriodaphnia P/F at 90%), monitor quarterly in February, May,, August and
Novernber [see Special Condition A. (?.)].
a
Composite
There shall be no discharge of floating solids or foam visible aft other than trace amounts.
nt

Per xr)it NO0087513
A. (?.) CHRONIC TOXICITY PERMIT LIMIT (QRTRLY)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to Ceriodaphnia
dub/a at an effluent concentration of 90°A.
The permit holder shall perform at a minimum, uarterIv monitoring using test ptacedures outlined in the "North Carolina
Ceriodaphnia Chronic Effluent Bioassay Proce Revi Februarys 1998, or subsequent versions or "North Carolina
Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions. The tests will
be performed during the months of February, May, August and November. Effluent sampling for this testing shall be
performed at the NPDES permitted final effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit limit, then
multiple -concentration testing shall be performed at a minimum, in each of the two following months as described in "North.
Carolina Phase 11 Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest concentration
having no detectable impairment of reproduction or survival and the lowest concentration that does have a detectable
impairment of reproduction or survival. The definition of " detectable impairment," collection methods, exposure regimes,.
and further statistical methods are specified in the "North Carolina Phase II Chronic Whole Effluent Toxicity Test
Procedure" (Revised -February 1.998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring
Form (MR. -I) for the months in which tests were performed, using the parameter code TGP3B for the pass/fail results and
THP3B for the Chronic Value. Additionally. DWQ Form AT-3 (original) is to be sent to the following address;
Attention: North Carolina Division of Water Quality
Environmental Sciences Branch
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Branch no laterthan 30 days after
the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all concentration/response
data, and be certified by laboratory supervisor and ORC or approved designate signature. Total residual chlorine of the
effluent toxicity sample must be measured and reported if chiori.ne is employed for disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the perminee
will complete the information located at the top of the aquatic toxicity (AT) test form indicating the facility name, permit
number, pipe number, county, and the month/year of the report with the notation of "No Flow" in the comment area of the
form. The report shall be submitted to the Environmental Sciences Branch at the address cited above,
Should the perminee fail to monitor during a month in which toxicity monitoring is required,. monitoring will be required
during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water Quality
indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring
requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival,
minimum control organism reproduction, and appropriate environmental controls, shall constitute an invalid test and will
require immediate follow-up testing to be completed no later th a.n the last day of the month following the month of the initial
monitoring,
A.(3.) SPECIAL CONDITION FOR DISCHARGE TO IMPAIRED STREAMS
The proposed discharge conveys effluent to Little Sugar Creel,, which is listed on North Carolina's 2000 303(d)
List as biologically impaired. If this facility is chronically non -compliant with the toxicity limit outlined in Part A..(2.) above
or it is otherwise determined that this discharge poses a threat to the water quality of the receiving stream, the Permitt:ee will
be required by the Division to cease discharge.

NCDENR / DWQ
FACT SHEET FOR NPDES PERMIT DEVELOPMENT
The Boulevard Company
(@ 715 North. Church, LLC)
NPDES No. NC0087513
Facility Information
1.) Facility Name:
(2.) Fermi
d Flow,MGD:
(3.) Facility Class:
715 North Church Si
0.072 MGD
(6.) County:
(7.) Regional Office:
(4.) Facility Status:
Permit S
US:
(.) Receiving Stream:
(2.) Subbasin:
(3.) Index No.:
(4.) Stream
Classification:
5.) 303(d) Lasted:
6.) 305(b) Status:
7.) Use Support:
New
New
(8.) USGS Topo Quad:
Stream Characteristics . .
Sugar Creek
©834
Summer 7t 1© icfs
2.) Average
3.1 IWC f°ail
Conditions Incorporated into New Per:
Proposed Co
incorporate monitoring
parameters and limits resulting.
from monitoring well results and
reasonable potential analysis.
Incorporate cornposite
monitoring for appropriate
parameters, since Qd >30,000
gpd.
Parameters
Effluent limits and monitoring
requirements
Composite sa
Mecklenburg
Mooresville
GI5NE
(Charlotte East)
O0%(
1.6%
st©rnndrain)
(creek)
©n(s)
Monitoring well results will
indicate parameters of concern
fear monitoring. Reasonable
potential analysis indicates
which of these parameters might
pose a water quality problem.
piing requirement 1'er 28,0500 monitoring
regulations.

ppipprwr
NPDES PERMIT FACT SHEET
Pace
Add monthly trichloroe
[ monitoring
Add oil and grease and
naphthalene monthly
monitoring naphthalene limit
Chronic Toxicity at 90%
The Boulevard at 715 North Church
NPDES No. NC008 7 513
Trichloroethene
Oil and grease, naphthalene
Toxici
Tetrachloroethene has been
detected on site at levels
indicating potential to exceed
water quality criterion. Site is
adjacent to a dry cleaning
operation, allowing for the
possibility of detection of
trichloroethene. Applicant will
be notified that if trichloroethene
is not detected after 12 sampling
events, applicant may request
reduction in monitoring
frequency.
A 550-gallon UST containing
heating oil. was found an site.
These parameters should be
- monitored until it can be
adequately demonstrated that no
gw contamination has resulted
from the presence of the UST
after 1.2 sampling events). This
is as per NCG51000 for
groundwater contaminated by
fuel oil.
Per ATU policy
Require continuous flow
order, since Qd> 10,000
Flow
Per NPDES Permitting Policy
PROJECT NOTES
Summary
• This is a new application for discharge of up to 0.072 MGD of treated groundwater from a
construction dewatering operation in downtown Charlotte.
The Boulevard site was operating under an interim discharge permit, with treated
groundwater piped to the CMUD sanitary system. Effective May 1, 2001, all peiuntted
discharges of remediated groundwater, contaminated groundwater, subsurface drainage, or
remediated surface water to the CMUD sanitary sewer were ceased.
The proposed discharge is to a city storm sewer in Charlotte, which indirectly discharges to
Little Sugar Creek. This creek is listed on the Draft 303(d) list as Partially Supporting, with
impaiiuient due to fecal coliform and turbidity. This creek is also listed as biologically
impaired due to unknown causes. The receiving stream has a s7Q10 flow of 0.85 cfs and a
30Q2 flow of 2.18 cfs.
Engineering Alternatives Analysis.
• The applicant briefly evaluated wastewater disposal alternatives, No long-term treatment
options (aside from direct discharge} are available in the downtown Charlotte area.
Treatment System.
▪ The proposed treatment system consists of bag filters and.
ed carbon vessels.
Permit Highlights
• Incorporate monitoring requirements (and, where reasonable potential has been
demonstrated, limits) for parameters detected in samples drawn from the interim treatment
system and monitoring wells. Add composite sampling for appropriate parameters, since Qd
> 30,000 gpd.
Page 2
. August 21,

NPDES PERMIT FACT SHEET The Boulevard at 715 North Church
Page 3
NPDES No. NC0087513
• Peii iit monitoring requirement for trichloroethene since a dry cleaning operation was
forrneriv on -site
• Pei/flit monitoring for oil and grease and naphthalene due to the discovery of a UST of fuel
oil on site. As per the general permit for fuel contaminated groundwater (NCG51000).
• The MR0 prepared a staff report dated 7/18/2001. MR0 recommends permit
Proposed Schedule for Permit Issuance
Draft Permit to Public Notice:
Permit Scheduled to Issue:
State Contact
08/29/01
11/01/01
If you have any questions on any of the above information or on the attached
permit, please contact Natalie Sierra at [phone], extension 551.
Copies of the following are attached to provide further information on the permit
development:
• Draft Peiiuit
NPDES Recommendation by:
Regional Office Comments
/12st:7-7-
7.„.(7-z3f ,c)
. 0
.415,01.4
Regional Recommendation
by:
Reviewed and accepted bv:
AL
Date
Regional Supervisor:
gi:natu
NPDES Unit Supervisor:
Signature
Paa.e 3
Version: August 17, 2001
Date
Date

„Nlontlily ,Vionitoring Report 715 ,Vorth Church Street April 27, 2001
LAW Project 3 0100L1-172 72
TABLE 1
LABORATORY ANALYTICAL RESULTS
715 NORTH CHURCH S"FREET
CHARLOTTE, NORTH CAROLINA
Sample Date 4.7.111oroform letrachloroethene Arsenic Barium Chromium Selenium
Identification Collected flAWIL) (004 Inig/t) (mg/L) iing11,11
FFE1,1115N I
DW-
DW-3
DW-4
3120/01 < V < 1 < 0.010 0,088 < 0.005 <0 010
3/26101 < 1 < 1 ,./. 0 010 0,89 < 0.005 0 012
412101* < [ 1 I 0,037 0,087 < 0..005 0,0 1 3
4/9/01 .-.). 1 IA <0,010 0.10 <0,005 < 0.010
4113101. g:-. 1 < 1 NA NA NA NA
4/16/01 < I < 1 < 0,010 0.093 0.006 < 0 010
4123101 < [ e). I < 0 010 0.081 0.006
/1/27101 <; 1 NA N.A NA
511/01 < V < 1 NA NA NA NA
5/7/01 < I < I < 0 010 0 084 0.005 < 0.010
5/14/01 < I < I < 0,010 0,075 0.006 < 0.010
5/21101 < 1 < 1 < 0.010 0.082 < 0.005 < 0.010
5.129/01 ..e. 1 ‹. 0 010 0.072 < 0.005 < 0.0 I 0
614101 ./.7. [ 4,0 0.035 0,087 0.005 0 1) 1))
5/7101 < i <. I NA NA NA NA
6/1 V A/1 < [ < 1 < 0.0 I 0 0.082 < 0.005 < 0.0 P..1
6/ I. (1001 < 1 0.016 0,051 < 0,005 < 0.010
612.5/01 .:: 1 < 1 0.019 0.080 < 0,005 ''', 0,010
7/2/01 < 1 < 1 < 0.0 I 0 0.086 < 0.005 < 0.010
7 /9,101 0 1 < 1 < 0.0 I () 0.085 < 0.005 < 00.0 I 0
4/1.8/01 < I
5i 1./01
NA NA
NA NA NA NA
4/18/01 3.3 17 NA N,A NA NA.
4/25101 7.9 81 NA NA. N.A N.A
4/27/01 .., 1 72 NA NA NA NA
511101 ‹. 1 5,2 NA NA N.A NA
517/0 I 1.3 2,1 NA NA NA NA
5/14/01 2,1 1.0 NA N.A N.A. .NA
5111101 ,-- 1 ,.,': 1 NA NA NA NA
5129/01 14 4.6 NA NA N.A. NA
6/4/0 I 4.7 61 NA NA NA N.A
61 I 1/01 2.1 24 NA NA NA. NA
6119101 2.7 i 9 NA NA N.A ,N A
6125101 < 1 3.5 NA NA NA NA
1712A)1 24) 5,9 NA NA NA NA.
719/01 2.4 1.7 NA NA NA NA.
4/1 8101 2.0
4118.'01 3.9
< I
<
NA NA NA NA
NA NA NA NA
Notes:
Ttagl, - Micrograms pate LiteT
2) Ma. "' Milligrams pet Liter.
< Sample col [coed p0.01, to the overflinv tank
NA < Not 'mak zed,
5} ISA NCAC 21.. - 111.1e. S'A (.4 the. Nolit Caul] RA )llllfll.11 itive. [ode, Siitichapier 21... Section ,002 Ground- Waier SLIiida[&
(;,[ Coucemations in bold are [n exceed= cc (,,,4 the 15A NUM,' 21... (imm01:-Wa[er Standards.
hi:pared Ibte/
0111N.ked/ Dale'

3/26/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC,
FLA' Sorick-) Analytcar& rvirortrnenta S,71r.,MoR5
Page 1 of 2
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC01691
Login Group: A0323G1A
Sample Collection Date/Time: 3/20/01 11:10
Lab Submittal Date/Time: 3/20/01 12:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
11' -
ARSENIC,: Less than mg/L 0.010 6010B 3/23/01 20:24 PRF
BARIUM 0.088 mg/L 0.010 60108 3/23/01 20:24 PRF
CADMIUM Less than mg/L 0.001 6010B 3/23/01 20:24 PRF
CHROMIUM Less than mg/L 0.005 6010B 3/23/01 20:24 PRF
LEAD Less than mg/L 0.005 60108 3/23/01 20:24 PRF
SELENIUM Less than mg/L 0.010 60108 3/23/01 20:24 PRF
SILVER Less than mg/L 0.005 60106 3/23/01 20:24 PRF
MERCURY, TOTAL Less than mg/L 0,0002 EPA 245.1 3/23/01 15:46 PRF
MERCURY DIGESTION Completed EPA 245.1 3/22/01 14:50 LC2
BROMODICHLOROMETHANE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
BROMOFORM Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
BROMOMETHANE Not detected ug/L 5 EPA 601/602 3/22/01 08:22 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
CHLOROBENZENE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
CHLOROETHANE Not detected ug/L 5 EPA 601/602 3/22/01 08:22 WAD
CHLOROFORM Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
CHLOROMETHANE Not detected ug/L 5 EPA 601/602 3/22/01 08:22 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L, 5 EPA 601/602 3/22/01 08:22 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 6011602 3/22/0108:22 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 3/22101 08:22 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
1,2)DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601/602 3/22/01 08:22 WAD
NC Certification No, 402 - SC Certification No 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No. E87519
449 .tipringbrook Road RO, Box 24054.1 Charlotte, NC 28224-0543
Phone: [phone] Toll Free Number:1-800/529-6364 Fax: [phone]

3/26/01
Law Eng & Env Se
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
es, Inc
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
PRISM
LABORATORIES, INC,
FLd Service Arraivtical N Environment& Suns
Page 2 of 2
Church St
EFFLUENT
AC01691
A0323G1A
3/20/01 11:10
3/20/01 12:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTMG METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
EDB
METHYLENE CHLORIDE
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
1,1,1-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRtCHLOROFLUOROMETHANE
VINYL CHLORIDE
BENZENE
ETHYLBENZENE
IPE
MTBE
TOLUENE
TOTAL XYLENES
CIS-1,2-DICHLOROETHENE
METALS DIGESTION METHOD
Sample Comments:
Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 5 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 1 EPA 601/602 3122/01 08:22 WAD
Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
Not detected Lig& 5 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 5 EPA 601/602 3/220'01 08:22 WAD
Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 5 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 5 EPA 601/602 3/22/01 08'22 WAD
Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
Not detected ug/L 3 EPA 601/602 3/22101 08:22 WAD
Not detected ug/L 1 EPA 601/602 3/22/01 08:22 WAD
Completed SW846-3005 3/22/01 14:15 LC2
Angela D. Overcash V.P. Laboratory Services
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert, No, 37735 - FL Certification No, E87519
449 Springbrook Road P.0, Box 240543 ...Charlotte, NC 28224-0543
Phone: [phone] oll Fret: Number: :I-800/529-6364 Fax: [phone]

TCIRIES, JNC
AnalyticalEnvironmental Solutions
Client
PhyslcatAddress
Phone Fax
P,OftiBilling Reference
Project Name
CLIENT
AMPLE DESCRIPTION
Sampler's Signature
Relinquished Oyi Si Mute)
DATE
COLLECTED
Relinquished By: (Signature)
Relinquished By: (Signature)
Method of Shipmedt
O. Fed Ex J UPS IHrn1-deliveredJ Other:
TIM
OLLECTED
MILITARY
HOURS
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Springbrook Road Charlotte, NC 28217
P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Fax [phone]
REPORT TO: Name
Address
BILL TO: Name
Address
Requested Due Date iJ 1 Day .J 2 Days 6 3 Days 6 4 Days J 5 Days
J 6-9 Days J Standard 10 days
Samples received atter 1500 will he processed the next business day.
Turnaround lime is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
MATRIX SAMPLE CONTAINER
(SOIL,
WATER OR 'TYPE
SLUDGE) SEE BELOW NCI
72,
SIZE
Sampled By (Print Name)
Received By: (Signature
calved By: (Signature)
rism Laboratoriqs
AiTYA2 Altqjt'
f
PRESERVA-
TIVES
ANALY
Da
Group N
TIPDES: UST:
NC LI NC
LI SC
J OTHER
GROUNDWATER:
NC
-0 SC
fT.) OTHER
DRINKING WATER:
CI NC
Ci SC
LJ OTHER
E CODES: A = Amber C Clear
pies INTACT upon arrival? •
eived ON WET ICE? Temp
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed \MOUT READSPACE?
PROPER CONTAINERS used?
State Certification
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
NO N/A
V
SC Other NA
No NA
Yes No
OTHER
PRESS DOWN FIRMLY 3 COPIES
ES REQUESTED
Affiliation
Li
SOLID WASTE: RCRA: CERC A LANDFILL
LI NC 0 NC ' LI NC l':-.1 NC
0 SC 0 SC ' LI SC ILI SC
Li OTHER 0 OTHER . 12.) OTHER CI OTHER
OTHER:
J NC
LI SC
0 OTHER
REMARKS
Additional Comments
A
LAB PRISM
CERT. LAB
I
ID NO. D NO.
Site Arrival Time:
Site Departure Time:
SEE REVERSE FOR
TERMS & CONDITIONS
G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
FINAL REPORT COPY

Full Service Analytical & Environmen
Client
Physical Address
Phone
P.O #/Billing Reference
Project Name
Fax
CLIENT DATE
AMPLE DESCRIPTION i COLLECTED
Sampler's Signature
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OI
SLUDGE)
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Springbrook. Road ,. Charlotte, NC 282 17
P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
REPORT TO: Name _._.
Address
BILL TO: Name
Address
Requested Due ©ate IJ 1 Day IJ 2 Days Li 3 Days J 4 Days LI' 5 Days
tJ 6 9 Days CA Standard 10 days
Samples received alter 15:00 will be processed the next business day.
Turnaround time is based on. business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
SAMPLE CONTAINER
'TYPE
SEE, BELOW
NO..
SIZE
npled By (Print Name)
PRESERVA-
TIVES
ANALY
moles INTACT upon arrival?
Received ON WET ICE? Temp PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?`
CUSTODY SEALS INTACT?
VOLATILES rec'd W/OUT HEADSPACE?
PROPER CONTAINERS used?
Stare Certification
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
YES
SC Other
No NA
Yes No
OTHER
NA
PRESS DOWN FIR
COPIES
RUESTED
Affiliation
Ii dStV UT By: (Signature)
l%ePa uishod Ey: (Sigeealc re)
Haliriquished By: (Signature)
c1 Shiprxrnnl
Ex J UPS -J Hand delivered J Other:
rtecerved thy: (btgna€urey
Received By: (Signature}
Reesived For Prism Laboratories
NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA
Q NC Li NC LI NC U NC iJ NC ID NC LI NC
i SC 'A SC ❑ SC 0 SC iJ SC rJ SC C.J SC
J OTHER LI OTHER LI OTHER LI OTHER J OTHER ka OTHER J OTHER
Date
Date
Data
Group Nrp..
tarvrHo
LANDFILL OTHER:
LINC ID NC
aSC i_JSC
OTHER LI OTHER
REMARKS
Additional Comments:.
SUB
LAB
CERT.
ID NO.
Site Arrival Time:
Site Departure Time:
E REVERSE FOR
tAS & CONDITIONS
`CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P Plastic; TL W Teflon -Lined Cap VOA = Volatile Ortanics Analysis (Zero Head Space)
CUSTOMER COPY

ab Report
4/2/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following analytical resu
TEST
PARAMETER
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
MERCURY, TOTAL
MERCURY DIGESTION
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
DIBROMOCHLOROMETHANE
1.2-DICHLOROBENZENE
1 ,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
DICHLORODIFLUOROMETHANE
1,1-DICHLOROE'THANE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
TRANS-1,2-DICHLOROETHENE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRANS-1,3-DICHLOROPROPENE
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
PRISM
LABORATORIES, INC.
Full Seroce Analytical B Envircna e tat Scr(uki
Page 1 of 2
Church St.
EFFLUENT
ACO2338
AO42G1
3/26/01 11:25
3/26/01 14:00
s have been obtained for the indicated sample which was submitted to this laboratory
TEST
RESULT
REPORTING METHOD DATE/TIME
UNITS LIMIT REFERENCE STARTED ANALYST
Not detected mg/L
0.89 mg.
Not detected mg/L
Not detected mg/L
Not detected mg/L
0.012 mg/L
Not detected mg/L
Le than mg/L
Completed
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug!L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
0.010 6010B 3/29/01 19:08 MSP
0.010 6010B 3/29/01 19:08 MSP
0,001 6010B 3/29/01 19;08 MSP
0,005 6010B 3/29/01 19:08 MSP
0.005 6010B 3/29/01 19:08 MSP
0.010 6010B 3/29/01 19:08 MSP
0.005 6010B 3/29/01 19:08 MSP
0.0002 EPA 245.1 3/29/01 15:49 PRF
EPA 245.1 3/28/01 13:00 LC2
1 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01,55 WAD
5 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
5 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
5 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601✓602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
5 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01,55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
1 EPA 601/602 4/1/01 01:55 WAD
5 EPA 601/602 4/1/01 01:55 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No, 37735 - FL Certification No. F87519
449 Springbrook Road I'.O, Box 240543 .. C,Itarto#te, NC 28224-0543
P'ho,n':704/529-6364 +Toll Free Number:1-800/529-6364,.. Fax:[phone]t19

plir ab Report
4/2/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC,
Fen Service Analykal .61 Erwitercrientai Sir:epees
Page 2 of 2
Customer Project ID: Church St.
Customer Sample ID: EFFLUENT
Prism Sample ID: ACO2338
Login Group: A042G1
Sample Collection Date/Time: 3/26/01 1125
Lab Submittal Date/Time: 3/26/01 14:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
EDB Not detected ug/L 1 EPA 601/602 4/1/01 0155 WAD
METHYLENE CHLORIDE Not detected ug/L 5 EPA 601/602 4/1/01 0155 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 EPA 601/602 4/1/01 0155 WAD
TETRACHLOROETHENE Not detected ug/L 1 EPA 601/602 4/1/01 0155 WAD
1,1,1-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/1/01 01-55 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/1101 01:55 WAD
TRICHLOROETHENE Not detected ug/L 1 EPA 601/602 4/1/01 01:55 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 EPA 601/602 411101 01:55 WAD
VINYL CHLORIDE Not detected ug/L 5 EPA 601/602 4/1/01 01;55 WAD
BENZENE Not detected ug/L 1 EPA 601/602 4/1/01 01;55 WAD
ETHYLBENZENE Not detected ug/L 1 EPA 601/602 4/1/01 01:55 WAD
IPE Not detected ug/L 5 EPA 601/602 4/1/01 0155 WAD
MTBE Not detected ug/L 5 EPA 601/602 4/1/01 01-55 WAD
TOLUENE Not detected ug/L 1 EPA 601/602 4/1/01 01:55 WAD
TOTAL XYLENES Not detected ug/L 3 EPA 601/602 4/1/01 01:55 WAD
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 4/1/01 01:55 WAD
_____....
METALS DIGEST-SURFACE/GROUNDW Completed SW846-3005 3/28/01 1150 LC2
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert, No, 37735 - FL Certification No. E87519
449 SprirOrook Road .... [10 24(1543 ....Charlotte, NC 28224-(15'43
Phony: 704/52'14)364 ...Toll Frey Nun-Aber:1 -8001529-6364 Fax: 7N/525-0409
" ""

Full Service Analytical & Environmental Soiuions
Client
Physical Address
Phone — Fax
ROA/Billing Reference
Project Name
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE
449 Springbrook Road Charlotte, NC 28217
P.O. Box 240543 4. Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
N FIRMLY - 3 COPIES
REPORT TO: Name
Address
BILL TO: Name
Address
Requested Due Date r
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
TIME
CLIENT DATE COLLECTED
P E DESCRIPTION COLLECTED MiLITARY
HOURS
Sampler's Signature
inquished By: (Signature
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
Sampled By (Print Name)
PRESERVA-
TIVES
Samples INTACT upon arrheal?
Reeved ON WET ICE? Temp
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEAOSPACE?
PROPER CONTAINERS used?
State Certification
Requested NC SC Other NA_
Water Chlorinated Yes No NA
Sample Iced Upon Collection Yes No
Affiliation
Relinquished By: (Sip:Tait-II:U)
y Sig—nTatu e
Method of Shipment
VPDES NC UST:
sc
OTHER
NTAINER TYPE CODES: A = Amber
eceyed By: Signature)
Received By: {Signature)
Reteived.For Prism Laboratories Ety
NC .__,
SC
OTHER
GROUNDWATER: NC
SC
OTHER
C = Clear G Glass P Plastic;
DRINKING WATER:
Date
ate
(„..1
Mika /Hour's
og-In Group No
NC SOLID WASTE,
SC
OTHER „
REMARKS
• SUB
' LAB
CERT.
ID NO.
PRISM
LAB
ID NO.
Additional Comments
OTHER
TL Tellon-Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
OTHER; NC
SC
OTHER__
SEE REVERSE FOR
TERMS & CONDITIONS
FINAL REPORT COPY

lillir
ri-12 —01 10:32A
Lab Report
4/12/01
Law Eng & Env Services, Inc
Attn. Matt Gustis
PO Box 11297
Charlotte, NC 28220
P . 02
PRISM
LASOPATtlni6t,
rug S),,Kvie 1;a4.4WPI,
Customer Project ID: Church St.
Customer Sample ID: EFFLUENT
Priam Semple ID: AC03123
Loon Group: A049G1
Sample Collection Date/Time: 4/2/01
Lab Submittal Date/Time, 4/2101
Page 1 of 2
11:30
14 45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory,
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT uNIT5 LIMIT REFERENCE STARTED ANALYST
ARSENIC 0,037 ms/L 0 010 6010B 4/11/01 2014 PRF
BARIUM 0 067 mg/L 0.010 60106 4/11i01 20:14 PRF
CADMIUM Not deteCted mg/t. 0 001 60108 4J11101 20-14 PRF
CHROMIUM Not detected mg/L 0,005 50106 4//1/01 20 14 PRF
LEAD Not detected mg/L 0.005 60106 4111/01 20 14 PRF
SELENIUM 0 013 mg/L 0,010 60108 4/11/01 20 14 PRF
SILt/R Not detected mg/L 0 005 60106 4/11/01 20 14 PRP
....._,...,..„
MERCURY, TOTAL Less than mg/L 0 0002 EPA 245.1 4/10/01 15 00 PRF
MERCURY DIGESTION Competed EPA 245.1 417/01 11 45 LCZ:
BROMODICHLOROMETHANE Not detected ug/L 1 EPA 60/602 4/6/01 11:35 WAD
BROMOFORM Not detected ug/L 1 EPA 6011602 4/6/01 1135 WAD
8ROMOMETHANE Not detected ugl 5 EPA 601/602 4/6101 11.35 WAD
CARBON TETRACHLORIDE Not detected ug/L. 1 EPA 601/602 4/6/01 11.35 WAD
CHLOROBENZENE Not detected uglt 1 EPA 6011602 4,641 '1,35 WAD
CHLOROETHANE Not detected ug/L 5 EPA 601/602 4/6/01 1135 WAD
CHLOROFORM Not detected ugIL 1 EPA 601/602 4/6/01 11,35 WAD
CHLOROMETHANE Not detected ug/i.. 5 EPA 641/602 4/6/01 1:1,35 WAD
DIBROMOCHLOROMETHANE Not detected ugil 1 EPA 601,502 4/6101 1135 WAD
1,2.D1CHLOROBENZENE Not detected ug/L. 1 EPA 601/802 4/6!01 1105 WAD
1.3•DICHLOROBENZENE Nat detected ug/L 1 EPA 601/602 4/6/01 11 35 WAD
1,4-D1CHLOROBENZENE Not detected ug/L 1 EPA 601/602 4/6/01 1135 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 6011602 4/6/01 11'35 wAu
1,1-OCHLOROETHANE Not detected ug/L 1 EPA 601/602 4/6/01 1135 WAD
1,201CHLOROETHANE Not detected ug/L 1 EPA 601/002 4/6/01 11.35 WAD
11-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 4/6/01 t 1,35 WAD
TRANS-1 2-DICHLOROETHENE Not detected ug/L. 1 EPA 601/602 4/610, 11 35 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 4/6/01 11:35 WAD
CIS-13-DICHLOROPROPENE Not detected ug/L 1 EPA 601/602 415/01 11,35 WAD
TRANS-1,3-DICHLOROPROPENE Not detected Lg/L 5 EPA 601ie02 4/6/01 11:35 WAD
NC Certification No, 402 - SC Certificallon Na.99012 - NC Drinking Water Gen, No. 37735 - FL 'Certification No, E87519
14" .',Pritighrools 1t,hid t). Ili 24041 — tettc, Nt 2822-IA1;11
71-1L,7,211-filt,1 fel11roNumber; 14t1141/;2,4-1416-4 704/525-040y

r.-12--©1 10:32A
Lab Report
4/12/01
Law Eng & Env Services, Inc
Attn. Matt Gustis
PG Box 11297
Charlotte, NC 28220
The fottovartrlg analytical results have been obtai
TEST
PARAMETER
EDB
METHYLENE CHLORIDE
1,1,2,2-TETRACHLCRQETHANE
TETRACHLQROETHENE
1,1,1•TRICHLORQETHANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
BENZENE
ETHYLBENZENE
IPE
NITRE
TOLUENE
TOTAL XYLENES
CIS-1 „2-DICHLOROETHENE
METALS DIGEST- URFACEIGR©UNDW Completed
Sample Comments°
TEST
RESULT
Not detected ug/L
Not detected ug/L
Not detected ug/L
1.1 ugfL
Notdetecta d ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detoctecl ug/L
Not detected ug/L
Angela Q. 0vercash, V.P. Laboratory Services
Customer Project ID: Church St.
Customer Sample ID: EFFLUENT
Prism Sample ID: AC03123
Loin Group: A049G1
Sample Collection date/Time: 4/2/01
P.03
PRISM
t,AGORATOM ES, INC
4 I.rr4�i1+k11f1H �(k�„vl ii°J%YAR,b
Page 2 of 2
1.1:30
Lab Submittal Date!Time: 4/2/01 14:45
d for the indicated sample which was subr111tted to this laboratory:
REPORTING METHOD
UNITS LIMIT REFERENCE
5
5
1
1
5
5
3
DATE/TIME
STARTED ANALYST
EPA 601 /602 4-16/01 11:35 WAD
EPA 601/602 4/6/01 11:35 WAr7
EPA 601/602 4)6/0' 11 35 WAD
EPA 601/602 4/6/01 11-35 WAD
EPA 6010302 4/6/01 11 °35 WAD
EPA 601/602 4/6/01 11:35 WAD
EPA 801/602 4/6/01 11 35 WAD
EPA 601/602 416/01 11:35 WAD
EPA 601/602 4/6101 1 1:35 WAD
EPA 601/602 416101 11:35 WAD
EPA 601/602 4/6/01 11,35 WAD
EPA 801(81)2 4/6101 11:35 WAD
EPA 601/602 416101 11:35 WAD
EPA601/602 4/6/0111,35 WAD
EPA 601/602 446/01 11.35 WAD
EPA 601/1302 4/6/01 11.35 WAD
SW84E-3015 417C0110:20 LC2
NC Certification No; 402 - SC Certification No, 9
012 - NC Drinking Water Cort. No 3T7t _ FL Certification No, E87519
444,N ',-i.ngbrouk r (1, fl& L 24 I;43 Ch rrlottc..'NC 2$224-054ti
7IA4/524.6'164 /S25-J4 N

a
it
C6Ye Y11 ,L�:�" j
Physdcal Address
G.C/f JPtC>e
Ph a 7a1'':3-t "_Ada Fax 7a 7,7„.4
P.O.a/Billing Reference Jc /'d — / o 2 72 /© % q '
Prelims Name C. 4 u rCZ .57
CLIENT DATE
AMPLE DESCRIPTION COLLECTED
Fl drltawi5IWell s wSi;a
r1
Q
N
NPOES:
:I NC
CSC
J OTHER
UST:
J NC
J SC
_I OTHER
GROUNOVarATER:
J N C
SC
Ti OTHER
Y
D
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE 4
449 Springbrook Road .. Or me. NC 282 t 7
P.O. Box 240543 .. Charlotte, NC 28224 -O543
Phone: 7€O4/529-t 364 . Fax: 704/525-O409
— //
REPORT TO: Name
Address
BILL TO: Name
4"r Address
Reuuestvd Due Data .J T Day J 2 Days J Days J 4 Days „i(''° Dar
J 6,9 DaV5 U Stanch-d 10 duy^s
Semplec ruc i d rn'le o 15.00 be p4ocessd Get+ real bu541e.45
Tjrnarry„rani time is ttgsQd Oil NISI/ness days, excluding weekends- mid torichr c.
SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
MA1�Frea4 SAMPLE CONTAINER
(SOIL.
ATER OR 'TYPE
SEE BELOW I NO. SUE
Sampied By (P IAnI Name)
RR'ev.e. ;Sign:,b�reI
DRINKING WATER:
NG
SC
OTHER
SOLID WASTE:
NC
SC
OTHER
PRESERVA
FIVES
RCRA: CERCIA
J NG .0 NC
JSC JSC
Li OTHER i OTHER
ICE7 Temp _0 11
ATIV€S indicated?
O DING TIMES?
INTAC T7
'OUT HEAOSPACE?
RS
rC
Requested EL NC ,
Walei O Hour-o f Yes
Smp.e Iced UTAPI COI LCUon
C'CMUO NPDES
4Cleg
TAINER TYPE CODES: A a Amber C = Clear G = Glass P Ptasue: TL Tellor Lined Cap VOA � Volatile Or
LANDFILL
NC
J SC
] OTHER
s Analysi
oz
Ai4rt,lr-fir
OTHER:
Ti NC
SC
J OTHER
SC
No
Yes
REMARKS
A.^;Tltk r i Crye:Ee':IMs
Zerei Hea© Space)
NA
CERT.
ID NO.
PRrSM
L.AS
ID NO.
SEW REVERSE FOR
TERNS & CONDITIONS
CFTC I

ab Report
RISM
LABORATORIES, INC.
4/23/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
FO Service AinatyScai & Erinvironmentrig Sokirtions
Page 1 of 2
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC03811
Login Group: A0416G1
Sample Collection Date/Time: 4/9/01 14:35
Lab Submittal Date/Time: 4/9/01 15:30
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ARSENIC Not detected mg/L 0.010 6010B 4/20/01 1837 MSP
BARIUM 0.10 mg/L 0.010 6010B 4/20/01 18:37 MSP
CADMIUM Not detected mgiL 0.001 6010B 4/20/01 1837 MSP
CHROMIUM Not detected mg/L 0,005 60106 4/20/01 18:37 MSP
LEAD Not detected mg/L 0.005 6010B 4/20/01 180.37 MSP
SELENIUM Not detected mg/L 0.010 60106 4/20/01 1837 MSP
SILVER Not detected mg/L 0,005 6010B 4/20/01 1837 MSP
MERCURY, TOTAL Less than mg/L 0.0002 EPA 245.1 4/12/01 19:09 PRE
MERCURY DIGESTION Completed EPA 245.1 4/12/01 13:10 LC2
BROMODICHLOROMETHANE Not detected ug/L 1 EPA 601/602 4/1201 1231 WAD
BROMOFORM Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
BROMOMETHANE Not detected ug/L 5 EPA 601/602 4/12/01 12:31 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
CHLOROBENZENE Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
CHLOROETHANE Not detected ug/L 5 EPA 601/602 4/12/01 12:31 WAD
CHLOROFORM Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
CHLOROMETHANE Not detected ug/L 5 EPA 601/602 4/12/01 12:31 WAD
DIBROMOCHLOROMETHANE Not detected uglL 1 EPA 601/602 4/12/01 1231 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 4/12/01 1231 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 4/12/01 1231 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601/602 4/12/01 12:31 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/12/01 1231 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 EPA 601/602 4/12/01 1231 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601/602 4/12/01 12:31 WAD
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No, E87519
449 Springbrook Road r.o. Box 240543 Charlotte, NC 28224-0543
Phone: [phone](14 ...Toll Free Number: 1-800/529-6364 Fax: [phone]

ab Report
4/23/01
Page 2 of 2
Law Eng & Env Services, Inc Customer Project ID: Church St
Attn: Matt Gustis Customer Sample ID: EFFLUENT
PO Box 11297 Prism Sample ID: AC03811
Charlotte, NC 28220 Login Group: A0416G1
Sample Collection DatefTime: 4/9/01 14:35
Lab Submittal Date/Time: 4/9/01 15:30
PRISM
LABORATORIES, INC,
Ftsit Serves': Artayitnat 6. Environmental Solutions
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Not detected ug/L 1 EPA 6011602 4/12/01 1231 WAD
Not detected ug/L 5 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
1.4 ug/L 1 EPA 601/602 4/12101 12:31 WAD
Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 5 EPA 601/602 4112/01 12:31 WAD
Not detected ug/L 5 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 5 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 5 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 1 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/L 3 EPA 601/602 4/12/01 12:31 WAD
Not detected ug/1.. 1 EPA 601/602 4/12/01 12:31 WAD
EDB
METHYLENE CHLORIDE
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
1,1,1-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
BENZENE
ETHYLBENZENE
IPE
MTBE
TOLUENE
TOTAL XYLENES
CIS-1,2-DICHLOROETHENE
METALS DIGEST-SURFACE/GROUNDW Completed
Sample Comments.
D. 0vercash, V.P. Laboratory Services
5toV846-3005 4/17/01 13:00 LC2
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No, E87519
449 Springbrook Road Ea Box 240543 ...Charlotte, NC 28224-0543
Phone: [phone],384 ...Toll Free Number -1-800/529-636.4 .... 1ax: 704/525-0409

Futi e Analytical
Client
„
��RAYOrnEs INC
Environmental Solutions
/
Physical Address
Phone
)
Fax;
P.01/Billing Reference
Project Name
CHAIN OF CUSTODY RECORD
PAGE OF_ QUOTE #
449 Springbrook Road Charlotte, NC 28217
P.O. Box 240543 A. Charlotte, NC 28224-0543
Phone: [phone],364 Ai. Fax [phone]
REPORT TO: NaMe
Address
BILL TO: Name
Address
Requested Due Date LI 1 Day Ll 2 Days J 3 Days LI 4 Days /J 5 Days
U 6-9 Days =.1 Standard 10 days
Samples received alter 1500 will be processed the next business day,
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES
USE ONLY
s INTACT upon arrival?
C
Received ON WET ICE? Temp
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
USTODY SEALS INTACT?
VOLATILES rec'd MOUT HEADSPACE?
PROPER CONTAINERS used?
State Certification
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
CLIENT
SAMPLE DESCRIPTION
SaMpIer'S Signature
Relinquished By: (Signaty(
Relinquished By: (Signalure)
rinquished By: (Signature)
hod ol Staprnent:
Fed Ex U UPS D Hand-deiiveied Other
DATE
OLLECTE
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL.
WATER OR
SLUDGE)
SAMPLE CONTAINER
*TYPE
SEE BELOW NO. SIZE
Sampled By (Print Name)
PRESERVA-
TIVES
ANALYSES
N
SC Other NA
No NA
Yes No
OTHER
PRESS DOWN F R Y -3 COPIES
UESTED
Affiliation
NPDES:
ILI NC
UST:
CI NC
SC
0 OTHER
GROUNDWATER:
LI NC
u Sc
:I OTHER
Received
roved By: (Signature)
Recewed0Wi5i1Ort Laboratories By:,
DRINKING WATER: SOLID WASTE:
Li NC Ll NC
SC 1-1 SC
0 OTHER LI OTHER
RCRA:
LI NC
LI SC
ILI OTHER
CERCLA
U NC
LI SC
fLI OTHER
Da
Da
Date,
ogln GrinjP
ilitary/Hours
LANDFILL OTHER:
LI NC LI NC
0 SC LI SC
0 OTHER J OTHER
REMARKS
AdclitiOnai Comments:
SUB
LAB PRISM
LAB
CERT, ID NO.
ID NO.
PRISM USE ONLY
Site Arrival Time:
Site Departure Time;
Field Tech Fee:
ge
SEE REVERSE FOR
TERMS & CONDITIONS
CODES:
A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap
VOA = Volatile Organics Analysis (Zero Head Space)
FINAL REPORT COPY

Fr ,
Report
4/13/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
RISM
LABORATORIES, INC.
Fuji Service Analytical & Environmental Solutions
Page 1 of 2
Customer Project ID: 715 N Church St.
Customer Sample ID: EFFLUENT
Prism Sample ID: AC04386
Loin Group: A0413G1
Sample Collection DateiTime: 4/13/01 12:00
Lab Submittal Date/Time: 4/13/01 12:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
BROMOFORM Not detected ug/L 1 EPA 601/502 4/13/01 14:19 CMB
BROMOMETHANE Not detected ug/L 5 EPA 601/602 4/13/01 14:19 CMB
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 601/602 4/13101 14:19 CMB
CHLOROBENZENE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
CHLOROETHANE Not detected ug/L 5 EPA 601/602 4/13/01 14:19 CMB
CHLOROFORM Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
CHLOROMETHANE Not detected ug/L 5 EPA 601/602 4/13/01 14:19 CMB
DIBROMOCHLOROMETHANE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
1,2-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
1,3-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
1,4-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601/602 4/13/01 14-19 CMB
1,1-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
1,1-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 EPA 601/602 4/13101 14:19 CMB
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601/602 4/13/01 14:19 CMB
EDB Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
METHYLENE CHLORIDE Not detected ug/L 5 EPA 601/602 4/13/01 14:19 CMB
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
TETRACHLOROETHENE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
1,1,1-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/13/01 14:19 CMB
1,1,2-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/13/01 14;19 CMB
TRICHLOROETHENE Not detected ugh_ 1 EPA 601/602 4/13/01 14:19 CMB
TRICHLOROFLUOROMETHANE Not detected ug/L 5 EPA 601/602 4/13/01 14:19 CMB
VINYL CHLORIDE Not detected ug/L 5 EPA 601/602 4/13/01 14:19 CMB
BENZENE Not detected ug/L 1 EPA 601/602 4/13/01 14;19 CMB
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springhrook Road .4. RO. Box 240543 Charlotte, NC 28224-0543
Phone; 704/529-6364 ...... Toll Free Number: 1.-800/529-6364 Fax: [phone]

ab` Report
4/13/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following analytical
TEST
PARAMETER
ETHYLBENZENE
IPE
MTBE.
TOLUENE
TOTAL XYLENES
CIS-1,2-UICHLOROETHENE
Sample Commen
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
PRISM
LABORATORIES, 4NC.
Full Service Arsatytca: w" Envi
Page 2 of 2
715 N Church St.
EFFLUENT
AC04386
A0413G1
4/13/01 12:00
4/13/01 12:45
TT
esults have been obtained for the indicated sample which was submitted to this laboratory:
TEST
RESULT UNITS
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L.
Not detected ug/L
Angela D. ©vercash, V.P. Laboratory Services
REPORTING METHOD DATE/TIME
LIMIT REFERENCE STARTED ANALYST
1 EPA 601/602 4/13/01 14:19 CMB
5 EPA 601/602 4/13/01 14:19 CMB
5 EPA 601/602 4/13/01 14:19 CMB
1 EPA 601/602 4/13101 14:19 CMB
3 EPA 601/602 4/13/01 14:19 CMB
1 EPA 601/602 4/13/01 14:19 CMB
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbr'ouk Road A., P:7, Bo 240543 ... Charlotte, NC 28224-0543
Phone: [phone] ..Toll Free Number.1-800/.529-63&4 Fay: 704/525-0404

,
ATOR1ES INC -
e Analytical & Environmental Solutions
Client 1-
Physical Address 111'
, = ,
Phone
P.0.#/Billing Reference
Project Name
CLIENT
SAMPLE DESCRIPTION
Sampler's Signature
Fax
DATE
COLLECTED
TIME MATRIX
COLLECTED (SOIL,
MILITARY WATER OR
HOURS SLUDGE)
RelingnOhed By: (Signature)
Relinquished By: (Signature)
Relinquished By: (Signature)
Method ot Shipment:
3'J Fed Ex UPS J Hanckdelivered J Other:
NPDES:
J NC
Sc
UST:
LI NC
Lj SC
LI OTHER
GROUNDWATER:
ILI NC
LI SC
LI OTHER
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Springbrook Road AL Charlotte, NC 28217
P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
REPORT TO: Name
Address
BILL TO: Name
Address
Requested Due Datiti LI 1 Day Ll 2 Days DI 3 Days LI 4 Days ID 5 Days
J 6-9 Days `U.1 Standard 10 days
Samples received alter 15,00 will toe processed the next business day
Turnaround time is based on business days, excluding weekends and hold:lays
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
SAMPLE CONTAINER
TYPE 11
SEE BELOW NO- 1 SIZE
. _
Sampled By (Prin( Name)
Received By: (Signature)
Received By: (Signature)
ReneivettinFor F:fiatin Laboratoriepidy:„V
DRINKING WATER:
NC
LI Sc
J OTHER
PRESERVA-
TIVES
SOLID WASTE: RCRA:
Li NC LI NC
SO LI SC
OTHER EJ OTHER
CERCLA
Ll NC
01 SC
LI OTHER
Daio
Dat
ples INTACT upon arrival?
Received ON WET ICE? Ternp
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES rec'd W/OUT HEADSPACE?
PROPER CONTAINERS used?
tate Certification
Requested FL
Water Chlorinated
Sample Iced Upon Collection
CMUD NPDES
YE NO N/A
.?""
NC _ SC Other
Yes No NA
Yes No
OTHER
NA
PRESS DOWN Fl
Y 3 COPIES
ANALYSES REQ
Z1'1
Log -In Group No. ,.
...„ .
T D
1 LAB
REMARKS CERT.
ID NO.
AffiIirion
ht5ry/Hour Additional Comments;
LANDFILL
J NC
'LI SC
LI OTHER
OTHER:
J NC
LI SC
OTHER
PRISM
LAB
ID NO.
PRISM USE ONLY
Site Arrival Time;
Site Departure Time:
SEE REVERSE FOR
TERMS & CONDITIONS
E CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap
VOA = Volatile Organics Analysis (Zero Head Space)
FINAL REPORT COPY

!IF —
Lab heport
4/25/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
PRISM
LABORATORIES, INC,
„,,,,,bbfbbblablbllttAbblihatu,„,
Fub; Service Analytical & Environmental Solutions
Page 1 of 2
Church Street
EFFLUENT
AC04425
A0423G1
4/16/01 08:20
4/16/01 0855
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
MERCURY, TOTAL
MERCURY DIGESTION
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
DIBROMOCHLOROMETHANE
1,2-DICHLOROBENZE NE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
DICHLORODIFLUOROMETHANE
1,1-DICHLOROETHANE
1,2-DICHLOROETHANE
1.1-DICHLOROETHENE
TRANS-1.2-DICHLOROETHENE
1.2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRANS-1,3-DICHLOROPROPENE
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Not detected
0.093
Not detected
0.006
Not detected
Not detected
Not detected
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Less than mg/L
Completed
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected [4/1_
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
0.010
0.010
0.001
0.005
0.005
0.010
0.005
60106
60106
60106
60106
60108
6010B
6010B
4/20/01 18:21
4/20/01 18:21
4/20/01 1821
4/20/01 18:21
4/20/01 18:21
4/20/01 18.21
4/20/01 1821
MSP
MSP
MSP
MSP
MSP
MSP
MSP
0,0002 EPA 245.1 4/24/01 11:23 PRE
EPA 245.1 4/18/01 13:35 LC2
1 EPA 601/602 4117/01 09:14 SHG
1 EPA 601/602 4/17/01 09:14 SHG
5 EPA 601/602 4117/01 09:14 SHG
1 EPA 601/602 4/17/01 09:14 SHG
1 EPA 601/602 4117/01 09:14 SHG
5 EPA 601/602 4/17/01 09:14 SHG
1 EPA 601/602 4/17/01 09:14 SHG
5 EPA 601/602 4/17/01 09:14 SHG
1 EPA 601/602 4/17/01 09:14 SHG
1 EPA 601/602 4/17/01 09:14 SHG
1 EPA 601/602 4117/01 09:14 SHG
1 EPA 601/602 4/17/01 09:14 SHG
5 EPA 601/602 4/17/01 09:14 SHG
1 EPA 601/602 4/17/01 09:14 SHG
1 EPA 601/602 4/17/01 09;14 SHG
1 EPA 601/602 4/17/01 09:14 SHG
1 EPA 601/602 4/17/01 09:14 SHG
1 EPA 601/602 4/17/01 0914 SHG
1 EPA 601/602 4/17/01 09:14 SHG
5 EPA 601/602 4/17/01 09:14 SHG
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert, No, 37735 - FL Certification No. E87519
449 Springbrook Road .6 P.O. Box 240543 .26 Charlotte, NC 28224-0543
Phone: [phone] a Toll Free Number: 1-800/529-6364 .26 Fax: [phone]

Lab Report
Fir
4/25/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following analytica
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
PRISM
LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 2of2
Church Street
EFFLUENT
AC04425
A0423G1
4/16/01 08:20
4/16/01 08:55
esults have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
EDB
METHYLENE CHLORIDE
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
1,1,1-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
BENZENE
ETHYLBENZENE
IPE
MTBE
TOLUENE
TOTAL XYLENES
CIS-1,2-DICHLOROETHENE
METALS DIGEST-SURFACE/GROUNDW Co
Sample Comments:
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE=._. STARTED ANALYST
Not detected ug/L 1 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 5 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 1 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 1 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 1 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 1 EPA 601/602 4/17/01 09:14 SHG
Not detected t1g/L 1 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 5 EPA 601/602 4/17/01 0914 SHG
Not detected ug/L 5 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 1 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 1 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 5 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 5 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 1 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 3 EPA 601/602 4/17/01 09:14 SHG
Not detected ug/L 1 EPA 601/602 4/17/01 09:14 SHG
pleted 5W846-3005 4/17/01 13:00 LC2
Angela D. 0vercash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert. No, 37735 - FL Certification No. E87519
449 Springbrook Road P,O. Box 240543 A. Charlotte, NC 28224-0543
Phone: [phone] . Toll Free Number: 1-800/529-6.364 Fax: [phone]

Fu
Client
RATORIES,
Analytical & Environmental Solutions
PhysicatAddress.,'"' '
Phone ' —To
Fax!x
P, 04/Billing Rol —
Project Name
CLIENT .,
SAMPLE DESCRIPTION
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Springbrook Road Charlotte, NC 28217
P.O. Box 24054,3 Charlotte, NC 28224-0543
Phone: 704/529,636.4,.. Fax: [phone]°
REPORT TO; Name
BILL TO: Name/—
Addres
Requested Due Date 1 Day J 2 Days G 3 Days i 4 Days J 5 Days
6-9 Days J Standard 10 days
Samples received after 1500 wiltbe processed the next business day.
Turnaround time is based on business days excluding weekends and holidays,
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
Samples INTACT upon arrival?
eceived ON WET ICE? Temp
PROPER PRESERVATIVES ind(cated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed MOUT HEADSPACE?
PROPER CONTA1NERS used?
Slate Certification
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
DATE
COLLECTED
TIME
ILLECTED
ITARY
HOURS
MATRIX
(SOIL,
WATER OR *TYPE
SLUDGE) SEE BELOW NO. SIZE
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALIYEES RE
Yfd NO
SC Other NA
No NA
Yes No
OTHER
PRESS DOWN FIRMLY 3 COPIES
U STED
REMARKS
SUB
LAB
CERT.
ID NO.
PRISM
LAB
ID NO.
Sampler's Signature /
Sampled By (Print Name)
AftiIiation
turtttLi'''
etthquished By: (Signature)
Raiirlquished By (Signature,
Msthod at Shipment. //
Fed Ex j UPS Y:.') Hand -delivered j Other:
NPDES: UST:
NC LJNC
l';1 SC 1J SC
THER LA OTHER
GROUNDWATER;
CA NC
LJ SC
ILI OTHER
ived By. (Signature
Received By: (Signature)
Reg E'er Oriisi4iortesfly:
DRINKING WATER: SOLID WAST
Li NC LJNC
LI SC LJSC
U OTHER OTHER
ata
�ae
Lo-Ir)
RCRA: CERCLA LANDFILL OTHER':
LI NC LI NC LI NC Li NC
LI SC IJ SC LJSC LI SC
LI OTHER rj OTHER LJ OTHER -J OTHER
Additional Comments
PRI
USE ONLY
Site Arrival Tints:
Site Departure Time:
Field Tech Fee.
9
SEE REVERSE FOR
TERMS & CONDITIONS
R TYPE CODES: A Amber C Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
FINAL REPORT COPY

ab Report
PRISM
4/23/01
Law Eng & Env Services, Inc
Matt Gustis
PO Box 11297
Charlotte, NC 28220
LABORATORIES, INC,
uH Service Analyiica[ & Env.kronmenOl SOutions
Page 1 of 8
Customer Project ID: 715 N. Church Street
Customer Sample ID: DW-i
Prism Sample ID: AC04797
Login Group: A0423G4
Sample Collection Date/Time: 4/18/01 15:30
Lab Submittal Date/Time: 4/18/01 18:25
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
BROMODICHLOROMETHANE Not detected ug/L 1 601 4/19/01 09:27 MP
BROMOFORM Not detected ug/L 1 601 4/19/01 09:27 MP
BROMOMETHANE Not detected ug/L 5 601 4/19/01 09:27 MP
CARBON TETRACHLORIDE Not detected ug/L 1 601 4/19/01 09:27 MP
CHLOROBENZENE Not detected ug/L 1 601 4/19/01 09:27 MP
CHLOROETHANE Not detected ug/L 5 601 4/19/01 09:27 MP
CHLOROFORM Not detected ug/L 1 601 4/19/01 09:27 MP
CHLOROMETHANE Not detected ugh. 5 601 4/19/01 09:27 MP
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 4/19/01 09:27 MP
1,2-DICHLOROBENZENE Not detected ug/L 1 601 4/19/01 09:27 MP
1,3-DICHLOROBENZENE Not detected ug/L 1 601 4/19/01 09:27 MP
1,4-DICHLOROBENZENE Not detected ug/L 1 601 4/19/01 09:27 MP
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 4/19/01 09:27 MP
1,1-DICHLOROETHANE Not detected ug/L 1 601 4/19/01 09:27 MP
1,2-DICHLOROETHANE Not detected ug/L 1 601 4/19/01 09:27 MP
1,1-DICHLOROETHENE Not detected ug/L 1 601 4/19/01 09:27 MP
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 4/19/01 09:27 MP
1,2-DICHLOROPROPANE Not detected ug/L 1 601 4/19/01 09:27 MP
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 4/19/01 09:27 MP
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 4/19/01 09:27 MP
EDB Not detected ug/L 1 601 4/19/01 09:27 MP
METHYLENE CHLORIDE Not detected ug/L 5 601 4/19/01 09:27 MP
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 4/19/01 09:27 MP
TETRACHLOROETHENE Not detected ug/L 1 601 4/19/01 09:27 MP
1,1,1-TRICHLOROETHANE Not detected ug/L 1 601 4/19/01 09:27 MP
1,1,2-TRICHLOROETHANE Not detected ug/L 1 601 4/19/01 09:27 MP
TRICHLOROETHENE Not detected ug/L 1 601 4/19/01 09:27 MP
TRICHLOROFLUOROMETHANE Not detected ugh. 5 601 4/19/01 09:27 MP
VINYL CHLORIDE Not detected ug/L 5 601 4/19/01 09:27 MP
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 601 4/19/01 09:27 MP
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ..... tO. Box 240543 ...Charlotte, NC 26224-0543
Phone: [phone] ..... roll Free N ouribm, I-S00/529-6364 .... Fax: [phone]
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE STARTED ANALYST

4/23/01
Law Eng & Env Services„ Inc
Matt Guses
PO Box 11297
Charlotte, NC 3
Anouutt rns"
Page 2 of 8
Customer Project ID: 715 N. Church Street
Customer Sample ID: r
Print Sample ID: AC04797
Login Group: A0423G4
Sample Collection atelTime:: 4/18/01 15:30
Lab Submittal Date/Time: 4/18/01 18:25
The follow g analyti l results have been obtained for the indicated sample which was submitted to this aboratory
TEST
PARAMETER
Sample o manta:
TEST
RESULT
UNITS
REPORTING METHOD DATErTI tE
LIMIT REFERENCE STARTED ANALYST
Angel "D. Overnash, V,P. Laboratory Services
NC Certification No. 402 - SC rti canon No. 99012T- NC Drinking Water Cert. No. 37735 FL Ce
449 Sl rira t,rtaazk t{oad ,.t„ I30. Box 4t 543 ttit, Charlotte, N 4;
PI re: 704/529-ta to4 Trill Free Nurbee'
lc
ion No. E8751

ab Report
rir
4/23/01
Law Eng & Env Services, Inc
Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC,
Full Se rvie AnivYi.
Page 3 of 8
Customer Project ID: 715 N. Church Street
Customer Sample ID: DW-2
Prism Sample ID: AC04798
Login Group: A0423G4
Sample Collection Date/Time: 4/18/01 16:00
Lab Submittal Date/Time: 4/18/01 18:25
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST
PARAMETER RESULT UNITS
BROMODICHLOROMETHANE Not detected ug/L
BROMOFORM Not detected ug/L
BROMOMETHA.NE Not detected ug/L
CARBON TETRACHLORIDE Not detected ug/L
CHLOROBENZENE Not detected ug/L
CHLOROETHANE Not detected ug/L
CHLOROFORM 33 ug/L
CHLOROMETHANE Not detected ug/L
DIBROMOCHLOROMETHANE Not detected ug/L
1,2-DICHLOROBENZENE Not detected ug/L
1,3-DICHLOROBENZENE Not detected ug/L
1,4-DICHLOROBENZENE Not detected ug/L
DICHLORODIFLUOROMETHANE Not detected ug/L
1,1-DICHLOROETHANE Not detected ug/L
1,2-DICHLOROETHANE Not detected ug/L
1,1-0ICHLOROETHENE Not detected ug/L
TRANS-1,2-DICHLOROETHENE Not detected ug/L
1,2-DICHLOROPROPANE Not detected ug/L
CIS-1,3-DICHLOROPROPENE Not detected ug/L
TRANS-1,3-DICHLOROPROPENE Not detected ug/L
EDB Not detected ug/L
METHYLENE CHLORIDE Not detected ug/L
1,1,2,2-TETRACHLOROETHANE Not detected ug/L
TETRACHLOROETHENE 17 ug/L
1,1,1-TRICHLOROETHANE Not detected ug/L
1,1,2-TRICHLOROETHANE Not detected ug/L
TRICHLOROETHENE Not detected ug/L
TRICHLOROFLUOROMETHANE Not detected ug/L
VINYL CHLORIDE Not detected ug/L
CIS-1,2-DICHLOROETHENE Not detected ug/L
REPORTING METHOD
ATE/TIME
LIMIT REFERENCE STARTED ANALYST
601
601
801
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/011024 MP
4/19/0110:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
4/19/01 10:24 MP
NC Certification No, 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Sprongbrocok Road P.O. Box.. 240543 Charlotte, NC 28224-0543
Phone: [phone] ► Trro11 Free Number: 1-800/529-6364 Fax: [phone]

4/23/01
Law nc & Env Services, Ind
Matt Gustis
PO Box 11297
Charlotte, N 2 220
auk@ Ea }ce Ana t at Envkr :n
Page 4 of 8
Customer Pr ject ID:. 715 N. Church Street
Customer Sample ID: -2
Prism Sample : A04798
Login GrupA0423G4
Sample Collection Date/Time: 4/18/01 1 :00
Lab Submittal Dt/Time 4/18/01 18:25
The followinganalytical results nave been obtained or the indicated sere 1pie which was submitted to this laboratory
TEST
PARAMETER
Sample t crrrar e ts.
TEST REPORTING METHOD UATErnME
RESULT UNITS LIMIT REFERENCE STARTE ANALYST
Angela D. Overcast:, /. a Laboratory Services
NC Certi c bon No. 402 SC Certification No. 99012 - NC Drinking Water Cert. No, 7735 FL Certification No, E 7 19
449 pringbru k i had 4k,170
one: 704a966 4.
: Sc� 24054
Number: 1
harlotte, Nt. "' -054
64 1 ax 70/52

rab Report
4/23/01
Law Eng & Env Services, Inc
Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC.
FUU SeMee Analytical & Environmental Solutions
Page 5 of 8
Customer Project ID: 715 N. Church Street
Customer Sample ID: DW4
Prism Sample ID: AC04799
Login Group: A0423G4
Sample Collection Date/Time: 4/18/01 17:00
Lab Submittal Date/Time: 4/18/01 18:25
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
._.
TEST TEST REPORTING METHOD DATEMME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
---- —
BROMODICHLOROMETHANE Not detected ug/L 1 601 4/19/01 11;33 MP
BROMOFORM Not detected ug/L 1 601 4/19/01 11;33 MP
BROMOMETHANE Not detected ug/L 5 601 4/19/01 11;33 MP
CARBON TETRACHLORIDE Not detected ug/L 1 601 4/19/01 11133 MP
CHLOROBENZENE Not detected uglL 1 601 4/19/01 11:33 MP
CHLOROETHANE Not detected ug/L 5 601 4/19/01 1133 MP
CHLOROFORM 2.0 ug/L 1 601 4/19/01 11:33 MP
CHLOROMETHANE Not detected ug/L 5 601 4119/01 11:33 MP
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 4/19/01 11:33 MP
1,2-DICHLOROBENZENE Not detected ug/L 1 601 4/19/01 11:33 MP
1,3-DICHLOROBENZENE Not detected ug/L 1 601 4/19/01 11.33 MP
1,4-DICHLOROBENZENE Not detected ug/L 1 601 4/19/01 1133 MP
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 4/19/01 11.33 MP
1,1-DICHLOROETHANE Not detected ug/L 1 601 4/19/01 1133 MP
1,2-DICHLOROETHANE Not detected ug/L 1 601 4/19/01 11 33 MP
1,1-DICHLOROETHENE Not detected ug/L 1 601 4/19/01 11:33 MP
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 4/19/01 11:33 MP
1,2-DICHLOROPROPANE Not detected ug/L 1 601 4/19/01 11:33 MP
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 4/19/01 11:33 MP
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 4/19/01 11:33 MP
EDB Not detected ug/L 1 601 4/19/01 11:33 MP
METHYLENE CHLORIDE Not detected ug/L 5 601 4/19/01 1133 MP
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 4/19/01 11:33 MP
TETRACHLOROETHENE Not detected ug/L 1 601 4/19101 11:33 MP
1,1,1-TRICHLOROETHANE Not detected ug/L 1 601 4/19/01 11:33 MP
1,1,2-TRICHLOROETHANE Not detected ug/L 1 601 4/19/01 11:33 MP
TRICHLOROETHENE Not detected ug/L 1 601 4/19/01 11:33 MP
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 4/19/01 11:33 MP
VINYL CHLORIDE Not detected ug/L 5 601 4/19/01 1133 MP
CIS-1.2-DICHLOROETHENE Not detected ug/L 1 601 4/19/01 11.33 MP
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road Box 240543 ...Charlotte, NC 28224-0543.
Phone: [phone]ree Number. 1-800/529-6364 Fax: [phone]

4/ 3/ 1
Law Eng & Env Services, nc
Matt Gustis
PO Box 11297
Charlotte, NC28220
The fallowing analytic
4pie rr»merits:
Angola C. Overcash, V.P. L
{ raiy& Ii➢ttorl-
Page 6 of 8
Custom er Project 7'15 N. Church Street
Customer Sample IC: D _3
Prism Sample ID: AC047'99
Logiki Group: A0423G4
Sample Collection Date!Tirn 4i18/01' 17:00
Lab Submittal Date/Time.4/18/01 18: 5
ned for the indicated sample which was submitted to this laboratory
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Services
NC Certifieatirrn No. 402 - SC Certifica
nN ,99012 NC Drinkingd
=444 Sp n,hrt c�
6'hone; 04/529-63h4
k
r C rt. Noa 3773 - EL arts" tkon Nn.E875
Road Bux 24054
5 t l ark t4
I"ssk[ k ree ur h c. 1-S00k"? -fm364
704/525-0409

ab Report
PRISM
LABORATORIES, INC..
4/23/01
Law Eng & Env Services, Inc
Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following analytical t�esul
TEST —
PARAMETER
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
DIBROMOCHLOROMETHANE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
DICHLOROD I FLUOROMETHANE
1,1-DICHLOROETHANE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
TRANS-1,2-DICHLOROETHENE
1,2-DICHLOROPROPANE
CIS-1,.3-DICHLOROPROPENE
TRANS-1,3-DICHLOROPROPENE
EDB
METHYLENE CHLORIDE,
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
1,1,1-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
CIS-1,2-DICHLOROETHENE
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
Fuli Service Analytical & Environmental Solutions
Page 7 of 8
715 N. Church Street
DW-4
AC04800
A0423G4
4/18/01 17:30
4/18/01 18:25
have been obtained for the indicated sample which was submitted to this laboratory
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Not detected ugfL
Not detected ug/L
Not detected ug/L
Not detected ugfL
Not detected ug/L
Not detected ug/L
3,9 ug/L
Not detected ugfL
Not detected ug/L
Not detected ug/L
Not. detected ug/L
Not detected ugfL
Not detected ug/L
Not detected ugfL
Not detected ugfL
Not detected ugfL.
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ugfL
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
1
1
5
1
1
5
5
1
1
1
1
5
1
1
1
1
1
1
5
1
5
1
1
1
1
5
5
601
601
601
601
601
601
60'1
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
4/20/0108:49 MP
4/20101 08:49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4/20/01 08;49 MP
4/20/01 08;49 MP
4/20/0108;49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4120/01 08:49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4120/01 08:49 MP
4/20/0108:49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4/20/01 08;49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4120/01 08:49 MP
4/20/01 08:49 MP
4/20/01 08;49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4/20/01 08:49 MP
4/2010108:49 MP
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road t'.O. Box 240543 Charlotte. NC 28224-0543
Phone; 704/529-8364 + To11 Free Number:1-800/529-6364 Fax: [phone]

4/23/01
Law Eng & EnvServices, Inc
Matt Eustis
P3 Box 11297
Charlotte, NC 0
Er ,,naytica[ utons.
Page 8 of
Customer Pr ject ID: 715 . Church Street
Customer Sample 1 DW
Prism Sample ID: AC04800
Login Group: A0423G4
Sample Collection Date/Time 4/18/01 17:30
Lab Submittal Date/Time: 4/18/01 1 : 5
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
-TT
PARAMETER
Sample Comment :
TEST
RESULT
Angela D. Ivrbash„ V.P, Laboratory Services
R PO TIN
NITME
LIMIT RERENCE .R
ANALYST
NC erti c tion No. 402 - SC Certification l o. 99012 NC Drinking ing W ter Cart, No. 7735 . FL Certification No. E87!
449 'pringbr a k Casa [ !',C3. Box 240543 .1.
Phone: [phone]
to tither: 1-811 529
NC 2 22 -t05
<<. °525- Jib

Full Service Analytical & Environmental Solutions
Client
Physical Ltd
Phone'
P,O,#1Bflling Reference:
Project Name
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #_--
449 Springbro©k. Road .. Charlotte, NC 28217
P.O. Box 240543 . Charlotte, NC 28224--0543
Phone: [phone]," Fax [phone]
REPORT TO: Name
Address
BILL TO: Name
Address .._.
Requested Due Date U 1 Da`y;,
Days _i 4 Days U 5 Days
C] 6-9 Days Standard 10 days
mples received after 15:00 will be processed lie next business day.
Turnaround lime is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
pips INTACT upon e
ived ON WET ICE? Temp �' I
PROPER PRESERVATIVES indicated?
eceived WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
State Certification
Requested FL NC SC _ Other
Water Chlorinated Yes No NA
Sample Iced Upon Collection Yes No
OTHER.
CMUD NPDES
NA.
CLIENT
SAMPLE DESCRIPTION
Sampler's Signature
IlrttdUk>Elrred' B
y tSignature)
nqui ed By (Signs
DATE
COLLECTED
Method of ,shipment)
J Fed Ex a UPS `j Hand -delivered s_i Other:
NPDES:
J NC
SC
UST:
J NC
U SC
ID OTHER
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OI
SLUDGE)
SAMPLE CONTAINER
"TYPE
SEE BELOW
NO.
SIZE
Sampled By (Print Name)
Received By (Signature)
ved By: (Signature)
sm Laboratorta
PRESERVA-
TIVES
Date
Date
ANA
YSES REQUEST
Affiliation
itary(Heul's
OTHER:
J NC
rJSC
J OTHEH
TYPE CODES: A Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
REMARKS
Additional Comments:
GI3OLINDWATER: DRNKING I
C
LI SC DSC
LI OTHER ❑ OTHER
ATER: SOLID WASTE: RCRA:
LI NC LI NC
J SC J SC
U OTHER U OTHER
CERCLA
u NC
ID SC
LI OTHER
LANDFILL
NC
ID SC
LI OTHER
PRISM
LAB
ID NO.
SUB
LAB
CERT.
ID NO,
Arrival Time:
Site Departure Time;
Field Tech Fee:
SEE REVERSE FOR
TERMS & CONDITIONS
FINAL REPORT COP

irReport
5/1/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following anal
TEST
PARAMETER
ICI resu
Fun Service Analytical & Environmental Solutions
Page 1 of 2
Customer Project ID: Church St.
Customer Sample ID: EFFLUENT
Prism Sample ID: AC05228
Login Group: A0430G1
Sample Collection Date/Time: 4/23/01 16:50
Lab Submittal Date/Time: 4/23/01 17:30
have been obtained for the indicated sample which was submitted to this laboratory:
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
MERCURY, TOTAL
MERCURY DIGESTION
BROMODICHLORQMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
DIBROMOCHLOROMETHANE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE.
1,4-DICHLOROBENZENE
DICHLORODIFLUOROMETHANE
1,1-DICHLOROETHANE
1,2-DICHLOR©ETHANE
1,1-DICHLOROETHENE
TRANS-I,2-DICHLOROETHENE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRANS-1,3-DICHLOROPROPENE
TEST REPORTING METHOD
DATE/TIME
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Not detected mg/ 0.010 6010B 4/30/01 14:51 MSP
0,081 mg/L 0.010 6010B 4/30/01 14:51 MSP
Not detected mg/L 0.001 6010B 4/30/01 14:51 MSP
0.006 mg/L 0.005 6010B 4/30/011.4.51 MSP
Not detected mg/L 0.005 6010B 4/30/01 14:51 MSP
Not detected mg/L 0,010 6010B 4/30/01 14:51 MSP
Not detected mg/L 0.005 6010B 4/30/01 14:51 MSP
Less than mg/L 0.0002 EPA 245.1 4/26/01 15.35 PRF
Completed EPA 245.1 4/24/01 11:30 LC2
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 5 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 5 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 5 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05.03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 5 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
Not detected ug/L 5 EPA 601/602 4/27/01 05:03 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No, 37735 - FL Certification No. E87519
449 Springbrook Road . PO. Box 240543 .w. Charlotte, NC 28224-0543
Phone: [phone] Toll Free Number: 1-800/529-6364 416 Fax: [phone]

5/1/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PG Box 11297
Charlotte, NC 28220
Full Service Anatytical 8 Erwlronmental Solutions
Page 2 of 2
Customer Project ID: Church St.
Customer Sample ID: EFFLUENT
Prism Sample ID: AC05228
Login Group: A0430G1
Sample Collection Date/Time: 4/23/01 16.50
Lab Submittal Date/Time: 4/23/01 17:30
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
EDB Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
METHYLENE CHLORIDE Not detected ug/L 5 EPA 601/602 4/27/01 05:03 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 EPA 601/602 4/27/01 0503 WAD
TETRACHLOROETHENE Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
1,1,1-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
TRICHLOROETHENE Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 EPA 601/602 4/27/01 05:03 WAD
VINYL CHLORIDE Not detected ug/L 5 EPA 601/602 4/27/01 05:03 WAD
BENZENE Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
ETHYLBENZENE Not detected ug/L 1 EPA 6011602 4/27/01 05:03 WAD
IPE Not detected ug/L 5 EPA 601/602 4/27/01 05:03 WAD
MTBE Not detected ug/L 5 EPA 601/602 4/277/01 05:03 WAD
TOLUENE Not detected ug/L 1 EPA 601/602 4/27101 05:03 WAD
TOTAL XYLENES Not detected ug/L 3 EPA 601/602 4/27101 05:03 WAD
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 4/27/01 05:03 WAD
METALS DIGEST-SURFACE/GROUNDW Completed
Sample Comments:
Angela D. 0vercash, V,P. Laboratory Services
SW846-3005 4/26/01 12:00 LC2
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road _ P.O. Box 240543 . Charlotte, NC 28224-0543
Phone: [phone] .,. Toll Free Number: 1-800/529-6364 Fax: [phone]

$�A NC
Full Service .Analytical & Environmental Solutions
Client
Physical Address,
Phonic'
PA1#/BillIng Reference
Prolect Name
Fax
CLIENT DATE
SAMPLE DESCRIPTION COLLECTED
Sampler's Signature
itinquished B. (SIyna1urij
dirqubr1d By; (Signature)
elinquisihed By: (Si tyre)
.;:
TIME
OLLECTED
MILfTARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
CHAIN OF CUSTODY RECORD
PAGE / OF QUOTE #
449 Springbrook Road Alb. Charlotte, NC 28217
P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
REPORT TO: Name
Address
BILL TO; Name
Address
Requested Due Date 1 Day J 2 Days l 3 Days IJ 4 Days Li 5 Days
U 6-9 Days .71 Standard 10 days
Samples received atter 15:00 will be processed the next business day
Turnaround time is based on business days, excluding weekends and holidays
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES}
SAMPLE CONTAINER
'TYPE
SEE BELOW Na SIZE
Sampled By Print Name)
PRESERVA-
TIVES
LAB USE
mples INTACT uporvettlivat?
eived ON WET ICE? Temp
PROPER PRESERVATIVES indicated?
Recssved WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed MOUT HEADSPACE?
PROPER CONTAINERS used?
State Certification
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
YE NO
SC Other NA
No NA
Yes No
OTHER
PRESS DOWN FIRMLY 3 COPIES
ANALYSES REOUESTED
Affiliation
Method of Shipman':
Ex UPS J Hand-dellverod IJ Other:
R iy: ig
C V ti d
y: (Signature)
heceivporfor POsnytaiboratoeus
PDES: UST: GROUNDWATER: DRINKING WATER:
C LI NC U NC LI NC
LI SC CJ SC LI SC
J OTHER L OTHER U OTHER
PE CODES: A = Amber C = Clear G = Glass
SOLID WASTE:
U NC
Li SC
LI OTHER
RCRA:
LI NC
'0 SC
LI OTHER
CERCLA
Li NC
0 SC
OTHER
Date
Date
itary/liours
Date
Irlt.gPLv1?„No
" .
LANDFILL
0 NC
Li SC
LI OTHER
OTHER:
(LI NC
01 SC
OTHE.R .
REMARKS
Additional Comments:
P = Plastic; TL Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
SUB
LAB
CERT.
lo NO.
PRISM
LAB
D NO.
PRISM USE ONLY
Site Arrival Time:
Site Departure Time:
Field Tech Fee:
SEE REVERSE FOR
TERMS & CONDITIONS
FINAL REPORT COPY

FrReport
4/26/01
Law Eng & Env Services, Inc
Attn: Matt Gust's
PO Box 11297
Charlotte, NC 28220
SM
LA ATONES, INC.
Fultl SaMce Aoalyticatl & Eavittlonntltlental Soluliona
Page 1 of 2
Customer Project ID: Church St
Customer Sample ID: DW-2
Prism Sample ID: AC05412
Login Group: A0426G1
Sample Collection Date/Time: 4/25/01 15:00
Lab Submittal Date/Time: 4/25/01 15:25
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Not detected ug/L 1 601 4/25/01 18:55 WAD
BROMOFORM Not detected ug/L 1 601 4/25/01 18:55 WAD
BROMOMETHANE Not detected ug/L 5 601 4/25/01 18:55 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 4/25/01 18:55 WAD
CHLOROBENZENE Not detected ug/L 1 601 4/25/01 18:55 WAD
CHLOROETHANE Not detected ug/L 5 601 4/25/01 18:55 WAD
CHLOROFORM 7%9 ug/L 1 601 4/25/01 18:55 WAD
CHLOROMETHANE Not detected ug/L 5 601 4/25/01 18:55 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 4/25/01 18:55 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 601 4/25/01 18:55 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 601 4/25/01 18:55 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 4/25/01 18:55 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 4/25/01 18:55 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 4/25/01 18:55 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 601 4/25/01 18:55 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 601 4/25/01 18:55 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 4/25/01 18:55 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 601 4/25/01 18:55 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 4/25/01 18:55 WAD
TRANS •1,3-DICHLOROPROPENE Not detected ug/L 5 601 4/25/01 18:55 WAD
EDB Not detected ug/L 1 601 4/25/01 18:55 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 4/25/01 18:55 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 4/25/01 18:55 WAD
TETRACHLOROETHENE 81 ug/L 1 601 4/25/01 18:55 WAD
1,1 J-TRICHLOROETHANE Not detected ug/L 1 601 4/25/01 18:55 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L 1 601 4/25/01 18:55 WAD
TRICHLOROETHENE Not detected ug/L 1 601 4/25/01 18:55 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 4/25/01 18:55 WAD
VINYL CHLORIDE Not detected ug/L 5 601 4/25/01 18:55 WAD
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 601 4/25/01 18:55 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cut, No, 37735 - FL Certification No. E87519
449 Springbrook Road P.O. Box 240543 Ai. Charlotte, NC 28224-0543
Phone: [phone] a Toll Free Number: 1-800/529-6364 a, Fax: [phone]

4/26/01
Law Eng & Env Services, Inc
Attn: Matt Asti
PO Box 11297
Charlotte, NC 28220
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection DaterLime:
Lab Submittal Date/Time:
LASORA *niES,INC
t sett tAntr „246.
Full Service Ana t & Environmental Solutions
Page 2 of 2
Church St
AC05412
A0426G1
4/25/01 15:00
4/25/01 15:25
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
Sample Comments:
,22
TEST REPORTING METHOD DATETrME I --
RESULT UNITS LIMIT REFERENCE STARTE* ANALYST
Angela D. Overcash, V.P. Laboratory Services
NC Cerlificatbn No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No, 37735 - FL Certification No: E87519
449 Springbreck Road at, PO, Box 240543 „Au. Charlotte, NC 28224-0543
Phone: [phone] Toll Free Number: 14 1/529-6364 .„,*, Fax: [phone]

Analytical Environmental So
Client
Physical Addre
Phone
P_t].#7BIIII'ng Referepce
Project Name
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Springbrook Road .. Charlotte, NC. 28217
P.O. Box 240543 .. Charlotte, NC 28224-0543
Phone: [phone] A. Fax: [phone]
REPORT TO: Name
Address
TO: Name
Address
Requested Due Date. 'J 1 Day ill Days LI 3 Days J 4 Days : 1 5 Days
6-9 Days J Standard 10 days
Samples received atter 15.`00 will be processed the next business day.
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
LAB USE ONLY
Samples INTACT upon arrival?
Received ON WET ICE? Temp
PROPER PRESERVATIVES 'indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES rec`d 4V/OUT HEADSPACE?
PROPER CONTAINERS used?
anon
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
SC
No
Yes
Other ..
NA
No
OTHER
NA..
N FIRMLY - 3 COPIES
CLIENT
SAMPLE DESCRIPTION
pi er''s Signature
n
Reldritluished By. (Signature)
Relinquished By; (Signature)
Method GI Shipmeult:,u
_J Fed Ex J UPS ?J Hand-<.lellvered Ji Other:
DATE
COLLECTED
!PDES: UST:
U NC
J SC
l0 OTHER
TIME
COLLECTED
MILITARY
HOURS
GROUNDWATER:
U NC
Li SC
U OTHER
ATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PE
0
Sampled By
Received By;
Received By: (Signetur
Recov ar Pria
DRINKING WATER:
it NC
U SC
U OTHER
a
Print Name)
SOLID WASTE:
U NC
U SC
Lt OTHER
PRESERVA-
TIVES
RCRA:
U NC
U SC
Ll OTHER
CERCLA
OI NC
SC
U OTHER
ANALYSES REQUESTED
Gruu
LANDFILL
LJ NC
U SC
CJ OTHER
Affiliation
Ours
OTHER:
U NC
J SC
U OTHER
REMARKS
Additional Comments;
PRISM
LAB
ID NO.
SUB
LAB
CERT.
ID NO.
Site Arrival Time:
Site Departure Time:
REVERSE FOR
IS &CONDITIONS
ODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile
Organics Analysis (Zero Head Space)
FINAL REPORT COPY

Report
IIIF
4/27/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
Full Service Analytical 8 Environmental Solutions
Page 1 of 4
Customer Project ID: Church St.
Customer Sample ID: DW-2
Prism Sample ID: AC05693
Login Group: A0427G2
Sample Collection Date/Time: 4/27/01 09:15
Lab Submittal Date/Time: 4/27/01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING METHOD DATE/TIME
LIMIT REFERENCE STARTED ANALYST
1tROMODICHLOROMETHANE Not detected ug/L 1 601 4/27/01 14:51 WAD
BROMOFORM Not detected ug/L 1 601 4/27/01 14:51 WAD
BROMOMETHANE Not detected ug/L 5 601 4/27/01 14:51 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 4/27/01 14:51 WAD
CHLOROBENZENE Not detected ug/L 1 601 4127/01 14:51 WAD
CHLOROETHANE Not detected ug/L 5 601 4/27/01 14:51 WAD
CHLOROFORM Not detected ug/L 1 601 4/27/01 14:51 WAD
CHLOROMETHANE Not detected ug/L 5 601 4/27/01 14:51 WAD
DtBROMOCHLOROMETHANE Not detected ug/L 1 601 4/27/01 14:51 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 601 4/27/01 14.51 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 601 4/27/01 14:51 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 4/27/01 14:51 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 4/27/01 14:51 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 4/27/01 14:51 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 601 4/27/01 14:51 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 601 4/27/01 14:51 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 4127/01 14:51 WAD
1 „2-DICHLOROPROPANE Not detected ug/L 1 601 4/27/01 14:51 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 4/27/01 14:51 WAD
TRANS--1,3-DICHLOROPROPENE Not detected ug/L 5 601 4/27/01 14:51 WAD
EDB Not detected ug/L 1 601 4/27/01 14.51 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 4/27/01 14:51 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 4/27/01 14:51 WAD
TETRACHLOROETHENE 72 ug/L 1 601 4/27/01 14:51 WAD
1,1,1-TRICHLOROETHANE Nat detected ug/L 1 601 4/27/01 14:51 WAD
11,2-TRICHLOROETHANE Not detected ug/L 1 601 4/27/01 14:51 WAD
TRICHLOROETHENE Not detected ug/L 1 601 4/27/01 14:51 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 4/27/01 14:51 WAD
VINYL CHLORIDE Not detected ug/L 5 601 4/27/01 14:51 WAD
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 601 4/27/01 14:51 WAD
NC Certification No. 402 SC Certification No. 99012 - NC Drinking Water Cert, No, 37735 - FL Certification No, E87519
449 Springbrook Road _ P.O. Box 240543 r►. Charlotte, NC 28224-0543
Phone: [phone] Toll Free Number: 1-800/529-6364 Ab. Fax: `704/525-0409

TEST
RESULT"
4/27/01
Law Eng & EnvServices, In
Attn: N att Gustis
PO Box 11297
Charlotte, NC"2 22
Fink Service ArratytIa
Page 2 of 4
Customer Project I Church St
Customer Sample I -2
Prim Sample ID: A Q 69
Login i roup.: A042702
rrtpie Collection tion Date/Time: 4/27 r 1 09:1
Lab Submittal Date/Time: 4/27/01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
tory:
TEST
AR.AR RTR
pie Cr
gale D. Overcash, . l laeretci
yes
REF OFMNG
U MTS _ LIMIT F .v...., TART i ANALYST
METHOD DAT /T1M
NC Certif ation No, 402 - SC Certitl ation No, 99012 - CSC Drinking p Wster Cart. No. 37735 - RL Car
9 Sprmg root Cent ? D. Box 240343 Chart tre, C 252 4-.054
Phone: 704/52 - a3 i4 Tol treeNumber: 1- 52 - 364 As. Fax: 7 d4/525-ir4ir9
ion Po. E87519

b Report
Fir
4/27/01
Law Eng & Env Services, irlc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following analytic
TEST
PARAMETER
Full Service Analy cat & Environmental Solutions
Page 3 of 4
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC05694
Login Group: A0427G2
Sample Collection DatelTime: 4/27/01 09:25
Lab Submittal Date/Time: 4/27/01 10:00
esults have been obtained for the indicated sample which was submitted to this laboratory:
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
DI BROMOCHLOROMETHANE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
DICHLORODIFLUOROMETHANE
1,1-DICHLOROETHANE
1,2-DICHLQROETHANE
1„1-DICHLOROETKENE
TRANS-1,2-DICHLOROETHENE
1,2-DICHLOROPROPANE
CIS-1 „3-DICHLORQPROPENE
TRANS-1,3-DICHLOROPROPENE
EDB
METHYLENE CHLORIDE
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
1,1,1-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
CISµ1,2-DICHLQROETHENE
TEST
RESULT
UNIT
Not detected ug/L
Not detected ug/L.
Not detected ug/L.
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L.
Not detected ug/L.
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
REPORTING METHOD DATE/TIME
I JMIT REFERENCE __. STARTED ANALYST
1
5
1
1
1
1
1
5
5
1
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13;54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13;54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/2.7101 13:54 WAD
4/27/01 13:54 WAD
4/27101 13;54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13;54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
4/27/01 13:54 WAD
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road AIL P.O. Box 240543 .a. Charlotte, NC 28224-0543
Phone: [phone] ,► Toll Free Number: 1-800/529-6364 Fax: [phone]

IFReport
4/27/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
Pa Box 11297
Charlotte, NC 28220
The following analytical results h
TEST
PARAMETER
Sample Comments:
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
Page 4 of 4
Church St
EFFLUENT
AC05694
A0427G2
4/27/01 09:25
4/27/01 10:00
ve been obtained for the indicated sample which was submitted to this laboratory:
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Angela D, ©vercash, V.P. Laboratory Services
NC Certification No. 402 - SC Ce
cation No. 99012 - NC Drinking Water Cert. No, 37735 - FL Certification No. E87519
449 Springbrook Road a P.O. Box 240543 a. Charlotte, NC 28224.0543
Phone: [phone] a Toll Free Number: 1-800/529-6364 . Fax [phone]

LAB Report
5/3/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
Pp Box 11297
Charlotte, NC 28220
The following an
TEST
PARAMETER,__..,,,.,....
BROMODICHLOROMETHANE
Not detected ug/L
BROMOFORM Not detected ug/L
BROMOMETHANE Not detected ug/L
CARBON TETRACHLORIDE Not detected ug/L
CHLOROBENZENE Not detected ug/L
CHLOROETHANE Not detected ug/L
CHLOROFORM Not detected ug/L
CHLOROMETHANE Not detected ug/L
DIBROMOCHLOROMETHANE Not detected tag/L.
1,2-DICHLOROBENZENE Not detected ug/L
1,3-DICHLOROBENZENE Not detected ug/L
1,4-DICHLOROBENZENE Not detected ug/L
DICHLORODIFLUOROMETHANE Not detected ug/L
1.1-DICHLOROETHANE Not detected ugh..
1,2-DICHLOROETHANE Not detected ug/L
1,1-DICHLOROETHENE Not detected ug/L
TRANS-1,2-DICHLOROETHENE Not detected ug/L.
1,2-DICHLOROPROPANE Not detected ug/L
CIS-1,3-DICHLOROPROPENE Not detected ug/L
TRANS-1,3-DICHLOROPROPENE Not detected ug/L
EDB Not detected ug/L
METHYLENE CHLORIDE Not detected ug/L
1,1,2,2-TETRACHLOROETHANE Not detected ug/L
TETRACHLOROETHENE Not detected ug/L
111-TRICHLOROETHANE Not detected ug/L
1,1,2-TRICHLOROETHANE Not detected ug/L
TRICHLOROETHENE Not detected ug/L
TRICHLOROFLUOROMETHANE Not detected ug/L
VINYL CHLORIDE Not detected ug/L
CIS-1,2-DICHLOROETHENE. Not detected ug/L
Full Service Analytical & Ernoronmental Solutions
Page 1 of 6
Customer Project lD: Church St
Customer Sample ID: DW-1
Prism. Sample ID: AC06108
Login Group: A053G3
Sample Collection Date/Time: 5/1/01 14:35
Lab Submittal DatelTime: 5/1/01 15:40
ults have been obtained for the indicated sample which was submitted to this laboratory:
TEST REPORTING METHOD DATE/TIME
RESULT UNITS _.. LIMIT REFERENCE STARTE© __..._ ANALYST
1 601 5/2/0121°°17 WAD
1 601 5/2/01 21:17 WAD
5 601 5/2/01 21:17 WAD
1 601 5/2/0121:17 WAD
1 601 5/2/01 21:17 WAD
5 601 5/2/01 21:17 WAD
1 601 512/01 21:17 WAD
5 601 5/210121:17 WAD
1 601 5/2/01 21:17 WAD
1 601 5/2/0121:17 WAD
1 601 5/2/01 21 ° 17 WAD
1 601 5/2/01 21:17 WAD
5 601 5/2/01 21;17 WAD
1 601 5/2/01 21:17 WAD
1 601 5/2/01 21:17 WAD
1 601 512/012117 WAD
1 601 5/2/01 21.17 WAD
1 601 5/2/01 21:17 WAD
1 601 5/2/01 21;17 WAD
5 601 5/2/01 21:17 WAD
1 601 5/2/01 21;17 WAD
5 601 5/2/01 21:17 WAD
1 601 5/2/01 21:17 WAD
1 601 5/2/01 21:17 WAD
1 601 5/2/01 21:17 WAD
1 601 5/2/01 21:17 WAD
1 601 5/210121.17 WAD
5 601 5/2/01 21:17 WAD
5 601 5/2/01 21;17 WAD
1 601 5/2/01 21:17 WAD
NC Certification. No. 402 - SC Certification. No, 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbronk Road n. P.O. Box 240543 . Charlotte, NC 28224-0543
Phone: [phone]. Toll Free Number: 1-800/529-6364. Fax: [phone]

Lab Report
5/3/01
Law Eng & Env Services, Inc
Attn: Matt Gusts
PG Box 11297
Charlotte, NC 28220
Full Service Analytical & Environmental Solutions
Page 2 of 6
Customer Project ID: Church St
Customer Sample ID: DW-1
Prism Sample ID: AC06108
Login Group: .A053G3
Sample Collection Date/Time: 5/1/01 14:35
Lab Submittal Date/Time: 5/1/01 15:40
The following analytical results have been obtained for the indicated sample which was submitted to this laborato
TEST
PARAMETER
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LPMIT REFERENCE STARTED ANALYST
Sample Comments:
Anger D. ©vercash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Spring -brook . Road . P.O. Box 240543 .. Charlotte, NC 28224-0543
Phone: [phone] .► Toll Free Number: 1-8001529-6364 A.. Fax: [phone]

5/3/01
Law Eng & Env Services, inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
SM
ATORIES, INC,
Full SerW,e Ana/ricall Erivironrnental Sohltiorts
Page 3 of 6
Customer Project ID: Church St
Customer Sample ID: DW-2
Prism Sample ID: AC06109
Login Grow. A053G3
Sample Collection Daterrime 5/1/01 13:55
Lab Submittal Date/Time. 5/1/01 15:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Not detected ug/L 1 601 5/2/01 22:13 WAD
BROMOFORM Not detected ug/L 1 601 5/2/01 22113 VVAD
BROMOMETHANE Not detected ug/L 5 601 5/2/01 2213 WAD
CARBON TETRACHLORIDE Not detected ugl 1 601 5/2/01 2213 WAD
CHLOROBENZENE Not detected ug/L 1 601 512/01 22:13 WAD
CHLOROETHANE Not detected ug/L 5 601 5/2/01 22:13 WAD
CHLOROFORM Not detected ug/L 1 601 512/01 2213 WAD
CHLOROMETHANE Not detected ug/L 5 601 512/01 2213 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 5/2/01 2213 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 601 5/2/01 22:13 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 601 5/2/01 22:13 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 5/2/01 2213 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 5/2/01 22:13 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 5/2/01 2213 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 601 512/01 22:13 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 601 5/2/01 22:13 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 5/2/01 2213 WAD
1,2-DtCHLOROPROPANE Not detected ug/L 1 601 5/2/01 22:13 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 5/2/01 2213 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 5/2/01 2213 WAD
EDB Not detected ug/L 1 601 5/2/01 2213 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 5/2/01 2213 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 5/2/01 22:13 WAD
TETRACHLOROETHENE 5,2 ug/L 1 601 5/2/01 2213 WAD
1,1,1-TRICHLOROETHANE Not detected ug/L 1 601 5/2/01 22;13 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L 1 601 5/2/01 2213 WAD
TRICHLOROETHENE Not detected ug/L 1 601 512/01 22:13 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 5/2/01 22:13 WAD
VINYL CHLORIDE Not detected ug/L 5 601 5/2/01 22:13 WAD
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 601 5/2/01 2213 WAD
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No. E87519
449 Springbrook Road P,O, Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Toll Free Number: 1-800/529-6364 Fax: [phone]

5/
Lave Eng & Env Services, Inc
Attni Matt Gustis
PO Box 11297
Charlotte, NC 28220
Full Ecaiirce Analytiva & Environmenred alutUnns
Page 4 of
Customer Project ID': Church St
Customer Sample ID: D
Prism Sample IDa AC06109
Login Group: :
Sa is lls t.inn Dat /Tim : /1/ 1 13:55
Lab Submittal Date/Time: 5/1/01 1 :4t
The fol o ing analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
Tale Co Comments:
TEST
RESULT
UNIT
Angela D. °verge h, 1/".P. Laboratory Services
REPORTING AETHOO OATEITi tE
LIMIT
REFERENCE STARTED.
ANALYST
NCertificakicn No. 402 - SC CertrfieatNon No. 9012 - NC Drinking Water Cert. No. 3773 FL ertihcation No E3 19
449 prin brook R.oad,.a. P.0, Box 240543 Chador NC 2 224-0543
Phone: [phone] kik Toll Free Number. , i /5 -63 4 are 7041525

Fr
Lab Report
5/3/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
ISM
ATORES,INC
Full Service AriatytKal & Environmenta9 Solutions
Page 5 of 6
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC06110
Login Group: A053G3
Sample Collection Date/Time: 5/1/01 13:40
Lab Submittal Date/Time: 5/1/01 15:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Not detected ug/L 1 601 5/2/01 2308 WAD
BROMOFORM Not detected ug/L 1 601 5/2/01 2308 WAD
BROMOMETHANE Not detected ug/L 5 601 5/2/01 23:08 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 5/2/01 23:08 WAD
CHLOROBENZENE Not detected ug/L 1 601 5/2/01 23:08 WAD
CHLOROETHANE Not detected ug/L 5 601 5/2/01 2308 WAD
CHLOROFORM Not detected ug/L 1 601 5/2/01 23:08 WAD
CHLOROMETHANE Not detected ug/L 5 601 5/2/01 2308 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 5/2101 2308 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 601 5/2/01 2308 WAD
1,3-DICHLOROBENZENE Not (detected ug/L 1 601 5/2/01 23:08 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 5/2/01 23:08 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 5/2/01 23:08 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 5/2/01 23:08 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 601 5/2/01 23:08 WAD
1,1-DtCHLOROETHENE Not detected ug/L 1 601 5/2/01 23:08 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 5/2/01 23:08 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 601 5/2101 23:08 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 512/01 2308 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 5/2/01 23:08 WAD
EDB Not detected ug/L 1 601 5/2/01 2108 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 5/2/01 2308 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 5/2/01 23:08 WAD
TETRACHLOROETHENE Not detected ug/L 1 601 5/2/01 23:08 WAD
1,1„1-TRICHLOROETHANE Not detected ug/L 1 601 5/2/01 23:08 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L 1 601 5/2/01 2308 WAD
TRICHLOROETHENE Not detected ug/L 1 601 5/2/01 23:08 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 5/2/01 2308 WAD
VINYL CHLORIDE Not detected ug/L 5 601 5/2/01 23:08 WAD
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 601 5/2/01 23:08 WAD
NC Certification No 402 - SC Certification No. 99012 - NC Drinking Water Cert. N©. 37735 - FL Certification No. E87519
449 Springbrook Road 411. P.O. Box 240543 Alb. Charlotte, NC 28224-0543
Phone: [phone] Ai. Toll Free Number: 1-800/529-6364 .,r, Fax: [phone]

Lat Report
5/3/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
Fult Service Analytical 8. Environmental Solutions
Page 6 of 6
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC06110
Login Group: A053G3
Sample Collection Date/Time: 5/1/01 13:40
Lab Submittal Date/Time: 5/1/01 15:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments.
Angola D. Overcash, VP, Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No. E87519
449 Springbrook Road PO. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] A.. Toll Free Number: 1-800/529-6364 Fax:, 704/525-0409

Full Service Analytical Environmental Solutions
Client
Physical Address
Phone
PO.#/Billing Reference ,.
Project Name
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Springbrook Road .. Charlotte, NC 28217
P.C). Box 240543 — Charlotte, NC 28224-0543
Phone: 704/529-f 364 - Fax: [phone]
REPORT TO: Name
Address
BILL TO: Name . .
Address
Requested. Due Date J 1 Day "3 2 Days C) 3 Days ❑ 4 Days 5 Days
CJ 6-9 Days "J Standard 10 days
Samples received after 15:00 will be processed the next business day.
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
LAD USE ONLY
INTACT upon arrival?
ved ON WET ICE? Temp
PROPER PRESERVATIVES' indicated?
ceived WITHIN HOLDING TIMES?
USTODY SEALS INTACT?
VOLATILES rec'd WMOUT HEADSPACE?
ROPER CONTAINERS used?
State Certification
Requested FL
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
NC
PRESS DOW
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
119ILITARY
HOURS
NtATRIX.
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
'TYPE .„
SEE BELOW
Sample
ure
d By: (Signature)
usitied By: (Signature)
linnetshed By: ('Signature)
'shod of Ship
Fed Ex J UN
NRDES:
t. ,NC
and-del+voted rl' Other`
UST:
J NC
J SC
ER U OTHER
GROUNDWATER:
LJ NC
U SC
)J OTHER
NO.
SIZE
PRESERVA-
TIVES
ANALY
SES R
UESTED
SC Other ..
No NA
Yes No
OTHER
REMARKS
NA
SUB
LAB
CERT.
ID NO.
PRISM
LAB
ID NO.
Sampled By (Print Name)
very may:
u
ved By: (Signature)
ecetved'For Prisfn Laboraa
DRINKING WATER:
IJ NC
LJ SC
LI OTHER
SOLID WASTE:
IJ NC
Li SC
rJ OTHER
RCRA: CERCLA
:J NC :J NC
CJ SC LI SG
J OTHER U OTHER
TYPE CODES: A = Amber C = Clear G = Glass P = Plastic, TL = Teflon -Lined Cap VOA = Volatile
Affiliation
LANDFILL
rJ NC
l"J SC
lJ OTHER
Organics Analysis
Additional Comments:
OTHER:
IJ NC
lJ SC
L:I OTHER
(Zero Head Space)
PI:1SM USE ONLY
Site Arrival Time
Site Departure Time:
Field Tech Fee:
SEE REVERSE FOR
TERMS & CONDITIONS
FINAL REPORT COPY

Fr'al) Report
5/14/01
Law Eng & Env Services, Inc
Matt Gustis
PO Box 11297
Charlotte, NC 28220
ISM
A TORIES INC
Full Service Analytical & EnviTonmental Solutions
Page 1 of 4
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC06728
Login Group: A0514G2
Sample Collection Date/Time: 5/7/01 14;00
Lab Submittal Date/Time' 5/7/01 15:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ARSENIC Not detected mg/L 0,010 6010B 5/9/01 23:14 MSP
BARIUM 0,084 mg/L (1010 6010B 5/9/01 23:14 MSP
CADMIUM Not detected mg/L 0,001 6010B 5/9/01 23:14 MSP
CHROMIUM 0.005 mg/L 0,005 60108 5/9/01 2314 MSP
LEAD Not detected mg/L 0,005 60108 5/9/01 23:14 MSP
SELENIUM Not detected mg/L 0010 6010B 5/9/01 23:14 MSP
SILVER Not detected mg/L 0,005 6010B 5/9/01 23:14 MSP
MERCURY, TOTAL Less than mg/L 0,0002 EPA 245.1 5/11/01 13:22 PRF
MERCURY DIGESTION Completed EPA 245.1 5/9/01 13:30 LC2
BROMODICHLOROMETHANE Not detected ug/L 1 EPA 601/602 5/11/01 23;50 WAD
BROMOFORM Not detected ug/L 1 EPA 601/602 5/11/01 23:50 WAD
BROMOMETHANE Not detected ug/L 5 EPA 601/602 5/11/01 2350 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 60141602 5/11/01 23:50 WAD
CHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/11/01 23:50 WAD
CHLOROETHANE Not detected ug/L 5 EPA 601/602 5/11/01 2350 WAD
CHLOROFORM Not detected ug/L 1 EPA 601/602 5/11/01 23:50 WAD
CHLOROMETHANE Not detected ug/L 5 EPA 601/602 5/11/01 23:50 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 EPA 601/602 5/11/01 23:50 WAD
1,2-DICHLOROBENZENE Not detectad ug/L 1 EPA 601/602 5/11/01 23:50 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/11/01 23:50 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/11/01 23:50 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601/602 5/11/01 23:50 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/11/01 23:50 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/11101 2350 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 5/11/01 23:50 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 5/11/01 2350 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 5/11/01 2350 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 EPA 601/602 5/11/01 2350 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601/602 5/11101 2350 WAD
NC Certification No, 402 - SC Certification No. 99012 - NC Drinking Water CertNo. 37735 - FL Certification No, E87519
449 Springbrook Road Ak, P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Toll Free Number: 1-800/529-6364 -a. Fax: [phone]

Fr,
b Report
5/14/01
Law Eng & Env Services, inc
Matt Gustis
Pa Box 11297
Charlotte, NC 28220
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time'
Full Service Analytical & Environmental Solutions
Page 2 of 4
Church St
EFFLUENT
AC06728
A0514G2
5/7/01 14:00
5/7/01 15:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
EDB
METHYLENE CHLORIDE
1„1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
1,1,1-TRICHLOR©ETHANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
BENZENE
ETHYLBENZENE
IPE.
MTBE
TOLUENE
TOTAL XYLENES
CIS-1,2-DICHLOROETHENE
METALS DIGEST-SURFACE/GROUNDW Completed
TEST
RESULT
REPORTING METHOD DATE/TIME
UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Angela D, Overcash, V.P. Laboratory Services
1 EPA 601/602 5/11/01 23:50 WAD
5 EPA 601/602 5/11/01 23.50 WAD
1 EPA 601/602 5/11101 23:50 WAD
1 EPA 601/602 5/11/01 23:50 WAD
1 EPA 601/602 5/11/01 23:50 WAD
1 EPA 601/602 5/11/01 23:50 WAD
1 EPA 601/602 5/11/01 23:50 WAD
5 EPA 601/602 5/11/01 23.50 WAD
5 EPA 601/602 5/11/01 23:50 WAD
1 EPA 601/602 5/11/01 23:50 WAD
1 EPA 601/602 5/11/01 23:50 WAD
5 EPA 601/602 5/11/01 23:50 WAD
5 EPA 601/602 5/11/01 23:50 WAD
1 EPA 601/602 5/11/01 23:50 WAD
3 EPA 601/602 5/11/01 23:50 WAD
1 EPA 601/602 5/11/01 23:50 WAD
SW846-3005 5/8/0110:15 LC2
NC Certification No. 402 - SC Certification No
9012 - NC Drinking Water Cert, No, 37735 - FL Certification No, E87519
449 Springbrook Road a P.O. Box 240543 a Charlotte, NC 28224-0543
Phone: 7'(14/529-6364 a Toll Free Number: 1-800/529-6364 a Fax: [phone]

Fr'alp Report
5/14/01
Law Eng & Env Serv[ces„ Inc:
Matt Gustis
PO Box 11297
Charlotte, NC 28220
SM
1ES, INC
Full Service Analytical & Environmental Solutions
Page 3 of 4
Customer Project ID: Church St
Customer Sample ID: OW-2
Prism Sample ID: AC06729
Login Group: A0514G2
Sample Collection Date/Time: 5/7/01 14:45
Lab Submittal Date/Time: 5/7/01 15:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATETTIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLORCMETHANE Not detected ug/L 1 EPA 601/602 5/12/01 0046 WAD
BROMOFORM Not detected ug/L 1 EPA 601/602 5/12/01 00:46 WAD
BROMOMETHANE Not detected ug/L 5 EPA 601/602 5/12/01 00:46 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 601/602 5/12/01 00:46 WAD
CHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/12/01 00:46 WAD
CHLOROETHANE Not detected ug/L 5 EPA 601/602 5/12/01 00:46 WAD
CHLOROFORM 1,3 ug/L 1 EPA 601/602 5/12/01 00:46 WAD
CHLOROMETHANE Not detected ug/L 5 EPA 601/602 502/01 0046 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 EPA 601/602 5/12/01 0046 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/12/01 0046 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/12/01 0046 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/12/01 00,46 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601/602 5/12/01 0046 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/12/01 00:46 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/12/01 00:46 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 5/12/01 00:46 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 5/12/01 0046 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 5/12/01 00:46 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 EPA 601/602 5/12/01 00:46 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601/602 5/12/01 00.46 WAD
EDB Not detected ug/L 1 EPA 601/602 5/12/0100:46 WAD
METHYLENE CHLORIDE Not detected ug/L 5 EPA 601/602 5/12/01 0046 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 EPA 601/602 5/12/01 00:46 WAD
TETRACHLOROETHENE 2.1 ug/L 1 EPA 601/602 5/12/01 00.46 WAD
1,1,1-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/12/01 00,46 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/12/01 0046 WAD
TRICHLOROETHENE Not detected ug/L 1 EPA 601/602 5/12/01 0046 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 EPA 601/602 5/12/01 00:46 WAD
VINYL CHLORIDE Not detected ug/L 5 EPA 601/602 5/12/01 0046 WAD
BENZENE Not detected ug/L 1 EPA 601/602 5/12/01 00,46 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification NolE87519
449 Springbrook Road a. P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] IL Toll Free Number: 1-800/529-6364 Fax: [phone]

ab Report
Fr
5114/01
Law Eng & Env Sere
Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following anal
TEST
PARAMETER
ETHYLBENZENE
IPE
MTBE
TOLUENE.
TOTAL XYLENES
CIS-1 w2-DICHLOROETHENE
Sample Comments:
s
nc
Page 4 of 4
Customer Project ID: Church St
Customer Sample ID: DW-2
Prism Sample ID: AC06729
Login Group: A©514G2
Sample Collection Date/Time: 5/7/01 14:4.5
Lab Submittal Date/Time: 5/7/01 15:20
ults have been obtained for the indicated sample which was submitted to this laboratory
TEST
RESULT UNITS
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
P. Laboratory Services
REPORTING METHOD DATE/TIME
LIMIT REFERENCE STARTED ANALYST
1
5
5
1
3
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
5/12/01 00:46 WAD
5/12/01 00:46 WAD
5/12/0100:46 WAD
5/12/01 00:46 WAD
5/12/01 00:46 WAD
5/12/01 00:46 WAD
NC Certification No, 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Sprij
Phone: 704/5
gbrook Road .. P.O: Box 240543 ► C,harlotte,NC 28224-0543
9-6364 . Toll Free Number 1-800/529-6364 Fax: [phone]

Full Servie Analytical & Environmental Solutions
Client
Physical Address
Phone
P.O.a/Billing Reference
Project Name
Fax
• ' -"" " •
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE 1
449 Springbrook Road 41,. Charlotte, NC 28217
P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
REPORT TO: Name
Address
BILL TO: Name
Address
Requested Due Dale J 1 Day J 2 Days iD 3 Days ij 4 Days ti 5 Days
6-9 Days J Standard 10 days
Sarnples received after 1500 will be processed the next business day.
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
TIME MATRIX SAMPLE CONTAINER
CLIENT DATE COLLECTED (SOIL,
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE
NO, SIZE
Sampler's Signatu
Relinquished By: (Signature}
Relinquished By: (Signature)
Retiogilished By: (Signature)
Method ot Shipment:
J Fed Ex :J` UPS J Rand-de.livered Ut Other:
NPDES:
J NC
u SC
• OTHER
UST:
LJ NC
U SC
J OTHER
HOURS SLUDGE) SEE BELOW
GROUNDWATER:
• NC
'U SC
• OTHER
Sampled Sy (Print Name)
Received By: (Signature}
oceived by: (signature)
Rectaved e6.1: Prism Laboratories By:
DRINKING WATER: SOLID WASTE: RCRA:
LI NC U NC U NC
Li SC U SC L:1 SC
LI OTHER J OTHER Li OTHER
CERCLA
(:1 NC
SC
J OTHER
Dale
Dale
Dalt'
LAB USE ONLY
Samples INTACT upon arrival?
Received ON WET ICE? Ternp Y?'
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
State Certification
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
SC Other NA
No ' NA
Yes No
OTHER
PRESS DOWN FIRMLY.3 COPIES
ANALYSES REOUESTE1D
„ —
Log -in Group N „
Attiliabon
Miltlaty/Hours
LANDFILL. OTHER:
CI NC LI NC
0 Sc IJ SC
0 OTHER 3 OTHER
Additional Comments:
SUB
PRISM
LAB
CERT% LAB
/
N.C:K 0 NO.
Site Arrival Time:
Site Departure Time:
geld Tech Fee
SEE REVERSE FOR
TERMS & CONDITIONS
*CONTAINER TYPE CODES: A = Amber C.= Clear G Glass P = Ptastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
FINAL REPORT GOPY

!Lab Report
5/21/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following analytical
TEST
PARAMETER
BROMODICHLOROMETHANE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
BROMOFORM Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
BROMQMETHANE Not detected ug/L 5 EPA 601/602 5118/01 04:48 CMB
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
CHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
CHLOROETHANE Not detected ug/L 5 EPA 601/602 5/18/01 04:48 CMB
CHLOROFORM 2.1 ug/L 1 EPA 601/602 5/18/01 04:48 CMB
CHLOROMETHANE Not detected ug/L 5 EPA 601/602 5/18/01 04:48 CMB
DIBROMOCHLOROMETHANE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
1.2-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
1 EPA 601/602 5/18/01 04:48 CMB
Not detected
1,3-t31CFiLOROBENZENEug/L
1.4-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
©ICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601/602 5/18/01 04:48 CMB
9
1,1-DICHLOROETFiANE
Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/18/01 04,48 CMB
ug/L Not detected U /L 1 EPA 601/602 5/18/01 04:48 CMB
TRANS-I,2-DICHLOROETHENE Not detected ug/L
1 EPA 601/602 5/18/01 04:48 CMB
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
CIS-1,3-DICHLOROPR©PENS Not detected ug/L
1 EPA 601/602 5/18/01 04:48 CMB
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601/602 5/18/01 04:48 CMB
EDB Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
METHYLENE CHLORIDE Not detected ug/L 5 EPA 601/602 508/01 04:48 CMB
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
TETRACHLOROETHENE 1,0 ug/L 1 EPA 601/602 5/18/01 04:48 CMB
1,1,1 TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
1,1,2-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
TRICHLOROETHENE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
TRICHLOROFLUOROMETHANE Not detected ug/L 5 EPA 601/602 5/18/01 04:48 CMB
VINYL CHLORIDE Not detected ug/L 5 EPA 601/602 5/18/01 04:48 CMB
BENZENE Not detected ug/L 1 EPA 601/602 5/18/01 04:48 CMB
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Sprintbrook Road P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] a Toll Free Number: 1-800/529-6364 .► Fax: [phone]
Full Service Analytical E. Environmental Solutions
Page 1 of 4
Customer Project ID: Church St
Customer Sample ID: DW-2
Prism Sample ID: AC07441
Login Group: A0521G2
Sample Collection Date/Time: 5/14/01 12:30
Lab Submittal Date/Time: 5/14/01 13:15
esults have been obtained for the indicated sample which was submitted to this laboratory
TEST REPORTING METHOD DATE/TIME
ARTED ANALYST
RESULT UNITS LIMIT REFERENCE ST mm..mm

Lab Report
5/21/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
SM
ABORATORIES, INC.
Full Service Analytical & Environmental Solutions.
Page 3 of 4
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC07442
Login Group: A0521G2
Sample Collection DatefTime: 5/14/01 12:45
Lab Submittal DatefTime: 5/14/01 13:15
The following analytical results have been obtained for the indicated sample which was submitted to this taboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ARSENIC Not detected mg/L 0.010 6010B 5/21/01 15:38 MSP
BARIUM 0.075 mg/L 0.010 6010B 5/21/01 1538 MSP
CADMIUM Not detected mg/L 0.001 60108 5/21/01 15;38 MSP
CHROMIUM 0.006 mg& 0.005 601013 5/21/01 15:38 MSP
LEAD Not detected mg/L 0.005 6010B 5/21/01 1538 MSP
SELENIUM Not detected mg/L 0,010 6010B 5/21/01 15:38 MSP
SILVER Not detected mg/L 0.005 60108 5121/01 15:38 MSP
MERCURY, TOTAL Less than mg/L 0.0002 EPA 245 1 5/17/01 13:45 PRF
MERCURY DIGESTION Completed EPA 245.1 5116/01 09:30 LC2
BROMODICHLOROMETHANE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
BROMOFORM Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
BROMOMETHANE Not detected ug/L 5 EPA 601/602 5/18/01 05:46 CMB
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
CHLOROBENZENE Not detected ug/L 1 EPA 6011602 5/18/01 05:46 CMB
CHLOROETHANE Not detected ug/L 5 EPA 601/602 5/18/01 05:46 CMB
CHLOROFORM Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
CHLOROMETHANE Not detected ug/L 5 EPA 6011602 5/18/01 05:46 CMB
DIBROMOCHLOROMETHANE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
1,2-DICHLOROBENZENE Not detected ugil.. 1 EPA 601/602 5/18/01 05:46 CMB
1,3-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
1,4-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601/602 5/18/01 05:46 CMB
1,1-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
1,1-01CHLOROETHENE Not detected ug/L 1 EPA 601/602 5/18/01 0546 CMB
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
TRANS-1,3-01CHLOROPROPENE Not detected ug/L 5 EPA 601/602 5/18/01 05:46 CMB
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road A. P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] AL 'roll Free Number: 1-800/529-6364 Fax: [phone]

Lab Report
5/21/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following anal
Full Service Analytcal & Environmental Solution
Page 4 of 4
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC07442
Login Group: A0521G2
Sample Collection Date/Time: 5/14/01 12:45
Lab Submittal Date/Time: 5/14/01 13:15
I results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED _ANALYST
EDB Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
METHYLENE CHLORIDE Not detected ug/L 5 EPA 601/602 5/18/01 05:46 CMB
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
TETRACHLOROETHENE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
1,1,1-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
1,1,2-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
TRICHLOROETHENE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMS
TRICHLOROFLUOROMETHANE Not detected ug/L 5 EPA 601/602 5/18/01 05:46 CMS
VINYL CHLORIDE Not detected ug/L 5 EPA 601/602 5/18/01 05:46 CMB
BENZENE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
ETHYLBENZENE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
IPE Not detected ug/L 5 EPA 601/602 5/18101 05:46 CMB
MTBE Not detected ug/L 5 EPA 601/602 5/18/01 05:46 CMB
TOLUENE Not detected ug/L 1 EPA 601/602 6/18/01 05:46 CMB
TOTAL XYLENES Not detected ug/L 3 EPA 601/602 5/18/01 05:46 CMB
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 5/18/01 05:46 CMB
METALS DIGEST-SURFACE/GROUNDW Completed SW846-3005 5/21/01 10:40 LC2
Sample Common
Angela D, 0vercash, V.P, Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No, 37735 - FL Certification No, E87519
449 Springbrook Road .iw P.O. Box 240543 .. Charlotte, NC 28224-0543
Phone: [phone] .. Toll Free Number: t-800/529-6364 AI. Fax: [phone]

Full Service Analytical
Client
Physical Address
Phone
P.O. /Billing Retere
Project Name
Environmental Solutions
CHAIN OF CUSTODY RECORD
PAGE,.. ^_ OF ___ QUOTE #1 e_ ---
449 Springbrook Road . Charlotte, NC 28217
P.O. Box 240543 .. Charlotte, NC 28224-0543
Phone: '704/529-6364. a. Fax: [phone]
REPORT TO: Name
Address
TO: Name
Address
e Date J 1 Day i] 2 Days LIB Days U 4 Days 5 Days
U 6-9 Days U Standard 10 days
Samples received after 15:00 will be processed the next business day,
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
Requested
LAB USE ONLY
&tmples INTACT open arrival
feceived ON WET ICE? Temp ;fir
PAt ER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES rec'd W/4UT HEADSPACE?
PROPER CONTAINERS used?
C
n
Requested FL NC SC Other
Water Chlorinated Yes No NA
Sample Iced Upon Collection
CMUD
NPDES
PRESS DOA
Yes No
OTHER
NO N(A
NA
CLIENT
DATE
SAMPLE DESCRIPTION COLLECTED
Sampler's Signature
"rir,rirh d By; qSi
NPDES:
E.J NC
sc
Shipment:
'11. UPS °_ Hand•-deRivered a Other:
TIME
COLLECTED
MILITARY
HOURS
UST:
NC
J SC
J OTHER
MATRIX
(SOIL,
ATER ORE 'TYPE
LUOGE) SEE BELOW i Na
ampled By (Prl
By: (Signolurey
GROUNDWATER: DRINKING WATER:
JNC JNC
C I' S.C. IJ SC
J OTHER Di OTHER
SAMPLE CONTAINER
SIZE
Name)
Pram Laboratories By:
SOLID WASTE:
J NC
J SC
J OTHER
ANALYSES REQUESTED
PRESERVA-
TIVES
RCRA: CERCLA LANDFILL
JNC JNC LJNC
rJ SC lJ SC iJ SC
L'.1 OTHER J OTHER CJ OTHER
Affiliation
OTHER:
J NC
IJ SC
J OTHER
SUB
1 LAB
REMARKS CERT,
ID NO.
Additional Cornments:
PRISM
LAB
ID NO.
Site Arrival Time
Site Departure Time:
Field Tech Fee:
SEE REVERSE FOR
TERMS 8r CONDITIONS
YPE CODES: A Amber C - Clear G = Glass P = Plastic Ti Tetin
ran A/rl4 1/nlnrire rlrnnninc amn14,.ric
�Inlhl O Dr1D7" V fV

6112/01
Law Eng & Env Services,
Attn: Matt Gustis
PG Box 11297
Charlotte, NC 28220
ISM
LABORATORIES, INC.
Fua Service Anaiyticai & Environmental 'Solutions
Page 1 of 4
Customer Project ID: Church St
Customer Semple 1D: EFFLUENT
Prism Sample ID: AC08214
Login Group: A0529G2 12:40
Sample Collection Date/Time: 5/21/01
Lab Submittal Date/Time: 5/22/01 07:45
ilowin analytical results have been obtained for the indicated sample which was submitted t�}�h� e or
The fo g DATE
REPORTING METHOD
AN
ALYST
TEST __._--_ -_. _ REFEREri10E _�TAR�.�.- __.. ._a, _._..-
TEST UNITSw _....... LIMIT ..
_RESl9LT ... _r_..
PARAMETER ..... ... 5123101 18.09 WAD
1 6Q
ED
Not detected ug/L 5723101 18'09 WAD
BROMOFICHLC)R'©METHANE 1 601
Not detected ug/L 5/23/01 tB=D9 WAD
BRQM©ORM 5 601
Not detected ug/L 5e23101 18.09 WAD
BROMOMETHANE 1 6Q 1
Not detected ug/L 5/231D118°.D9 WAD
CARBON TETRACR 6LGR9DE 1 601
Not detected. ug/L 5/23/01 18:09 WAD
CHLOROBENZENE 5 601
Not. detected ug/L 5/23/01 18.09 WAD
CHLOROETHANE 1 601
Not detected ugfL 5123°Q1 18:D9 WAD
CHLOROFORM 5 601
Not detected ug1L 5d23/p1 18:09 WAD
CHLOROMETHANE 1 601
Not detected ug/L 5/23/01 18'Q9 WAD
l2.Dt HL0R0)Rt?METHANE 1 6Q1
Not detected ug/L 5/23/01 18:Q9 WAD
1„2 utCHL©ROQENZENE 1 601
Not detected ugfL 5/23/01 18 Q9 WAD
1,3-DICNLC)RC)BENZENE 1 601
Not detected ugfL 5123°D1 113:D9 WAD
1,-DICHLGRC)BENZENE 5 601
Notdetected ug/L 5I23/011809 WAD
DICHLC)R©DIFWCJRC)METHANE 1 601
Notdetected ug/L 5123lD118:i19 WAD
1o1-DICHL©RC)ETD-LANE 1 601
Not detected ug/L 5/23/01 18:D9 WAD
1 „2 pICHLCJR©ETHANE 1 601
Not detected ug/L 5V31D1 18:09 WAD
1,1-DICHLC)RC)ETHENE 1 601
Not detected ug/L 5/23/01 18:D9 WAD
TRANS-1,2-DICHL©RCQETHENE 1 601
Not detected ug/L 5t23lDi 18:D9 WAD
1,2 DICHL©RC)PR'C?PANE 1 6p1.
Not detected ugfL 5/23/01 18;D9 WAD
CIS-1,3-D4CHLC)RiJJPRC)PENE 5 601
Not detected ug/L 5,°23,Q1 18:09 WAD
TRANS-1,3 DICHLC)RC)PRC)PENE 1 601
Not detected ug/L 5l23J'01 18.09 WAD
EDB 5 61
Notdetected ugfL 5t23lD118Q9 WAD
METHYLENE CHLORIDE 1 6D1
Not detected ug/L 5}23 01 18:09 WAD
1 „1 „2,2-TETRACHL+.?RCETHANE 1 601
Not detected ugiL bF2'31D1 18:09 WAD
TETRACHLOROETHENE 1 601
Not ug/L 5,i23ID118:Qg WAD
1 „1,1-TRICHLC)ROETHANE 1 601
Not detected ugfL 5�2'3lDi 18:Qg WAD
1,1,2-TRICHL©RdETHANE 1 601
Not detected ugfL 5/23/01 18aD9 WAD
TRICHLC)R©ETHENE � 601
Not detected ugfL 6123JD1 18:D9 WAD
TRtCHLORC)FLUGR )METHANE 5 601
Notdetected ug/L 5r231D118:€39 WAD
cIS l CHLORIDE 1 601
CIS-1,2-DICHL©RCETHEN'I°
Not detected ugfL
NC Certtficat'ion Na. 4© 2 - SC Cenifacation No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 5 pringbrooV°'-,,, .2 Fta Thli Fr e Number 1-8001 9-6364e.� Fax: [phone](19

IIIFli Report
6/12/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
Full Service Anelyticik 8. Erwironrnentel Sok items
Page 2 of 4
Customer Project [D: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC08214
Login Group:: A0529G2
Sample Collection Date/Time: 5/21/01 12:40
Lab Submittal Date/Time: 5/22/01 07:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
TEST
RESULT UNETS
ARSENIC Not detected mg/L
BARIUM 0.082 mg/L
CADMIUM Not detected mg/L
CHROMIUM Not detected mg/L
LEAD Not detected mg/L
SELENIUM Not detected mg/L
SILVER Not detected mg/L
REPORTING METHOD DATE/TIME
LIMIT REFERENCE STARTED ANALYST
0.010 60106 5/22/01 21:09 MSP
0.010 6010B 5/22/01 21:09 MSP
0.001 6010 B 5/22/01 21:09 MSP
0.005 60106 5/22/01 21:09 MSP
0.005 6010E 5/22/01 21:09 MSP
0.010 60106 5/22/01 21:09 MSP
0.005 60108 5/22101 21:09 MSP
MERCURY, TOTAL Less than mg/L 0.0002 EPA 245.1 6/11/01 12:02 PRE
MERCURY DIGESTION Completed EPA 245,1 5/22/01 14:45 LC2
METALS DIGEST-SURFACE/GROUNDW Completed SW846-3005 5/22/01 10:15 LC2
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 w- NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Spr°ingbrook Road Ah. P.C). Box 240543: a Charlotte, NC 28224-0543
Phone: [phone] AI, Toll Free Number: 1-800/529-6364 �. Fax: [phone]

Fr ab Report
6/12/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
PRISM
LABORATORIES, INC,
Full Seniine Ar yca & Environmental Solutions
Page 3 of 4
Church St
DW-2
AC08215
A0529G2
5/21/01 13:00
5/22/01 07:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST
PARAMETER RESULT
BROMODiCHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
DIBROMOCHLOROMETHANE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1.4-DICHLOROBENZE.NE
DICHLORODIFLUOROMETHANE
1,1-DICHLOROETH.ANE
,2-DICHLOROETHANE
1,1 -DICHLOROETHENE
TRANS-1,2-DICHLOROETHENE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRANS-1,3-DICHLOROPROPENE
EDB
METHYLENE CHLORIDE
1:1:2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
1:1,1-TRICHLOROETHANE
1.1.2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL. CHLORIDE
CIS-1,2-DICHLOROETHENE
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
REPORTING METHOD DATEMME
LIMIT REFERENCE STARTED ANALYST
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19;08
5/23/01 19:08
5/23/01 19:08
5/23/01 19;08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23101 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19;08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
5/23/01 19;08
5/23/01 19:08
5/23/01 19:08
5/23/01 19:08
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
NC Certification NoL 402 - SC Certification No. 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No, E87519
449 Springbrook Road P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Aik Toll Free Number: I-800/529-6364 Fax [phone]

!rif
b Report
6/12/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following analytic
TEST
PARAMETER
Sample Comments:
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Grout):
Sample Collection Date/Time:
Lab Submittal Date/Time:
PRISM
LABORATORIES, INC.
Roll Service AnalyticaR 8 Envkcinmenial Sclut4nri
Page 4 of 4
Church St
DW-2
AC08215
A0529G2
5/21/01 13:00
5/22/01 07:45
esults have been obtained for the indicated sample which was submitted to this laboratory:
TEST
RESULT UNITS
Angela D. Overcash, V,P. Laboratory Services
REPORTING METHOD DATE(TtME.
LIMIT REFERENCE STARTED
ANALYST
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No, 37735 - FL Certification No, E87519
449 Springbrook Road .r P.O. Box 240543 4 Charlotte, NC 28224-0543
Phone: 7041 29-t 364 Toil Free Number: 1-800/ 29.6364 Fax:[phone]

PRISM
LABORATORIES, INC..
ar
Full service Analytical Environmental Solutions
Client
Physical Address
Phone
P.O.#/Billing Reference
Project Name
Fax
CLIENT DATE
AMPLE DESCRIPTION l COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER 0
SLUDGE)
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Spritigbr-ook Road Charlotte, NC 28217
P.O. Box 240543 .. Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
REPORT TO:: Name
Address
BfLI TO: Name
Address
Requested Due Date J t Day J 2 Days 1 3 Days ,J 4 Days J s Days
J 6-9 Days ,a Standard 10 days
Samples received aher t5:00 will be processes the next busine-ss day.
Ttlmaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
SAMPLE CONTAINER:
*TYPE
SEE BELOW NO. SIZE
RESERVA.
TIVES
plus INTACT upon al'rival?
Received ON WET tCE'? hemp.-
PROPER PRESERVATIVES indicated`:'
Received WITHIN HOLDING TIMES?
CuSTOoN SEALS INTACT?
' VOL.ATftLES rec"d WdOUT HEADSPAGE7
PROPER. CONTAINERS used?
_
State Certification
Requested FL NC SC
Water Chlorinated Yes
Sample Iced Upon Collection
CMULJ NPDES
Other NA
No NA
Yes No
OTHER
PRESS DOWN FIR II.Y • 3 COPIES
ANALYSES REQUESTED
REMARKS
SUB
LAB
CERT„
ID NO.
PRISM
LAB
ID NO,
Sampler's Signature
Relinquished ©y (Signature,
Readnqussharf By: {y,lgsna,turo)
Relinqui
nature)
Method of Shipment,
Fed Ex'J UPS O k
PDES: UST:
IJ' NC
J SC
OTHER
rt
Sampled By (Print Narne)
Received: For Prism Laboratories By.,
Other;
GROUNDWATER: DRINKING WATER: SOLID WASTE:
IJNC iJNC: JNC
iJ SC J SC J SC
J OTHER J OTHER J OTHER
• A --- fl rnhetr T: — (:lace P — PlOir= -. Tr flnn
RCRA: CERCLA
NC J NC
`J SC Li SC
J OTHER U OTHER
enrt n Vt7A Volatile Om
Affiliation
Mdd
LANDFILL OTHER:
U NC J NC
J SC ;J SC
U OTHER .a OTHER
Additional Comments:
Anativsis (7ern Head Snace)
1
Slte AiYivali`ii1Yo:
Sites Dey e1ttre "0
Fi .Id 7e h Fee
SEE REVERSE FOR
TERMS & CONDITIONS
FINAL REPORT

Frab Report
6112/01
Law Eng & Env Services, inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
LABORATORIES, INC.
FuM Service Analylical & Envi.ranmentali Solutior6
Page 1 of 4
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC08756
Login Group: A065H2
Sample Collection Date/Time: 5/29/01 11 :45
Lab Submittal Date/Time: 5/29/01 16:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ARSENIC Not detected mglL 0,010 60106 6/4/01 22:44 MSC
BARIUM 0.072 Mg/ 0.010 6010B 6/4/01 22:44 MSC
CADMIUM Not detected mg/L 0.001 6010B 6/4/01 22:44 MSC
CHROMIUM Not detected mg/L 0,005 6010B 6/4/01 22:44 MSC
LEAD Not detected mg/L 0.005 60106 6/4/01 22:44 MSC
SELENIUM Not detected Mg/L 0,010 6010B 6/4/01 22:44 MSC
SILVER Not:detected mg/L 0.005 60106 6/4/01 22:44 MSC
MERCURY, TOTAL Less than mg/L 0.00 2 EPA 245,1 6/11/01 14:40 PRF
MERCURY DIGESTION Completed EPA 245.1 5/30/01 12:15 LC2
BROMODICHLOROMETHANE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
BROMOFORM Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
BROMOMETHANE Not detected ug/L 5 EPA 601/602 61/01 01:22 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
CHLOROBENZENE Not detected ug/L 1 EPA 601/602 6/1/01 01;22 WAD
CHLOROETHANE Not detected ugiL 5 EPA 601/602 6/1/01 01:22 WAD
CHLOROFORM Not detected ug/L 1 EPA 601/602 6/1/01 01;22 WAD
CHLOROMETHANE Not detected ug/L 5 EPA 601/602 6/1/01 01:22 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 611/01 01:22 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
1,4-D1CHLOROBENZENE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601/602 6/1/01 01:22 WAD
1,1-D1CHLOROETHANE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 6011602 6/1/01 01:22 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
CIS-1,3-DICHLOROPR0PENE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601/602 6/1/01 01:22 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ... P.O. Box 240543 ..h. Charlotte, NC 28224-0543
Phone: [phone] .... Toll Free Number: 1-800/529-6364 ..A. Fax: [phone]

rab Report
6/12/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
ISM
ABORATORIES, INC
Fut Service Analyticai. & Environmental Soititoris
Page 2 of 4
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC08756
Login Group: A065H2
Sample Collection Date/Time: 5/29/01 11:45
Lab Submittal Date/Time: 5/29/01 1600
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
EDB Not detected ug/l. 1 EPA 601/602 6/1/01 01.22 WAD
METHYLENE CHLORCE Not detected ug/L 5 EPA 601/602 6/1/01 01:22 WAD
1.1.2,2-TETRACHLOR0ETHANE Not detected ug/L 1 EPA 601/602 611/01 01:22 111AD
TETRACHLOROETHENE Not detected ug/L 1 EPA 601/602 6/1/01 0122 WAD
1,1 .1-TRICHLOROETHANE Not detected ugli_ 1 EPA 6011602 6/1/01 01:22 WAD
1.1,2-TRICHLORDETHANE Not detected ugIL 1 EPA 601/602 6/1/01 0122 WAD
TRICHLOROETHENE Not detected ug/L 1 EPA 601/602 6/1/01 01:22 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 EPA 601/602 6/1/01 01:22 WAD
VINYL CHLORIDE Not detected ug/L 5 EPA 601/602 6/1101 0122 WAD
BENZENE Not detected ug/L 1 EPA 601/602 6/1/01 01.22 WAD
ETHYLBENZENE Not detected ugl 1 EPA 601/602 6/1/01 0122 WAD
IPE Not detected ug/L 5 EPA 601/602 6/1101 01:22 WAD
MTBE Not detected ug/L 5 EPA 601/602 611/01 01'22 WAD
TOLUENE Not detected ug/L 1 EPA 601/602 6/1/01 0122 WAD
TOTAL XYLENES Not detected ug/L 3 EPA 601/602 6/1/01 01:22 WAD
CIS-12-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 60/01 0122 WAD
METALS DIGEST-SURFACE/GROUNDW Completed SW646-3005 6/4/01 0910 LC2
Sample Comments:
Angela D. 0vercash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012. - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springlyrook Road P.O. Box 240543 Charlotte, NC 28224-0543
Phone [phone] A.. Toll Free Number; 1-800/529-6364 Fax: '704/525-0409

ab Report
Fr
6/12/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The to
Customer Project ID:
Customer Sample ID:
Prism Sarnole ID:
Login Group:
Sample Co➢lection Date/Time:
Lab Submittal Date/Time:
PRISM
LABORATORIES, INC.
Felt Service Analyi cei & Environmental Soiutbri
Page 3of4
Church St
DW-2
AC08757
A©65H2
5/29/01 12:40
5/29/O1 16:00
owing analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
DIBROMOCHLOROMETHANE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
DICHLORODIFLUOROMETHANE
1,1 -DICHLOROETHANE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
TRANS-1,2-DICHL©R©ETHENE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRANS-1,3-DICHLOROPROPENE
EDB
METHYLENE CHLORIDE
1,1,2,2-TETRACHLOROETTHANE
TETRACHLOROETHENE
,1,1-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
BENZENE
TEST
RESULT
REPORTING METHOD DATE/TIME
UNITS LIMIT REFERENCE STARTED ANALYST
Not detected ug/L
Not detected ug/L
Not detected ugfL
Not detected ug/L
Not detected ug/L
Not detected ug/L
1,4 ug/L
Not detected ug,/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ugfL
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
4,6 ugfL.
Not detected ug/L
Not detected ug/L
Not detected ugfL.
Not detected ug/L
Not detected ug/L
Not detected ug/L
1 EPA 601/602.
1 EPA 601/602
5 EPA 601/602
1 EPA 601/602
1 EPA 601/602
5 EPA 601/602
1 EPA 601/602
5 EPA 601/602
1 EPA 601/602
1 EPA 601/602
1 EPA 601/602
1 EPA 601/602
5 EPA 601/602
1 EPA 601/602
EPA 601/602
1 EPA 601/602
1 EPA 601/602
1 EPA 601/602
1 EPA 601/602
5 EPA 601/602
1 EPA 601/602
5 EPA 601/602
1 EPA 601/602
1 EPA 601/602
1 EPA 601/602
1 EPA 601/602
1 EPA 601/602
5 EPA 601/602
5 EPA 601/602
1 EPA 601/602
6/1/01 02:19
6/1/01 02;19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02;19
611 /01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/'1 /C11 02:19
6/1/01 02;19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
6/1/01 02:19
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
WAD
NC Certification No. 402 - SC Certification No. 99012 - NC drinking Water Cert. No. 37735 - FL Certification N©. E87519
449 Springbrook Road r P.O, Box 22,40543 - Charlotte, NC 28224-0543
Phone: [phone] a Toil Free Number: t-800/529-6364 .. Fax [phone]

Fab Report
6/12/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
P© Box 11297
Charlotte, NC 28220
RISM
LA ORATORIES, INC.
Service Analyt/c & Ens#rc merval Scdunons
Page 4of4
Customer Project ID: Church St
Customer Sample ID: DW-2
Prism Sample ID: AC08757
Login Group: A065H2
Sample Collection Date/Time: 5/29/01 12:40
Lab Submittal date/Time: 5/29/01 16:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory;
TEST TEST
REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT ._._ REFERENCE STARTED ANALYST
ETHYLBENZENE Not detected ug/L 1 EPA 601/602 6/1/01 02:19 WAD
IPE
MTBE
TOLUENE
TOTAL XYLENES
CIS-1,2-©ICHLOROETHENE
Sample Comments:
Not detected ug/L 5 EPA 601/602 6/1/01 02:19 WAD
Not detected ug/L 5 EPA 601/602 6/1/01 02:19 WAD
Not detected ug/L 1 EPA 601/602 6/1101 02:19 WAD
Not detected ug/L 3 EPA 601/602 6/1/01 02:19 WAD
Not detected ug/L 1 EPA 601/602 611/01 02:19 WAD
Angela D. 0vercash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification Nn- E57 a19
449 Springbrooi+ Road A. P.O. Box 240543 r, Charlotte, NC 28224-0543
Phone: [phone] + 'Th.11 Free Number: t-8001529-6364 v fax [phone]

YsN
ATOMS, INC.
Full Service Analytical Environmental Solutions
Client
Physical Address
Phone
P.O.rt/Billing Reference
Project Name
Fax
CHAIN OF CUSTODY RECORD
PAGE OF _ QUOTE #
449 Springbrook Road A, Charlotte, NC 28217
P.O. Box 240543 A. Charlotte, NC 28224-0543
Phone: [phone] . Fax: [phone]
REPORT TO: Name
Address
BILL TO: Name
Address
Requested Due Dade ':J 1 Day Lk Days J 3 Days [J 4 Days °`Li 5 Days
LJ 6-9 Days J Standard 10 days
Samples received after 15:00 wi91 be processed the next business day.
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
pies INTACT upon arrival?
Received ON WET ICE? Temp t
PROPER PRESERVATIVES ind)cated?
d WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPAC€?
PROPER CONTAINERS used?
State Certification
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
SC Other
No NA
Yes No
OTHER
NA
PRESS Dt1NNN N FIR
Y COPIES
CLIENT DATE
AMPLE DESCRIPTION COLLECTED
TIME
OLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OI
SLUDGE)
Sampler's Signature
SAMPLE CONTAINER
*TYPE
SEE BELOW NO. SIZE
PRESERVA-
TIVES
ANALYSES REQUESTED
REMARKS
SUB
LAB
CERT,
ID NO.
PRISM
LAB
ID NO.
Sampled By (Print Name)
Affiliation
Relinquished By: (Signature)
F'1rdinquished By: (Signature)
Relinquished By: (Signatlure)
Method of Shipment:
D Fed Ex Li UPS 'J' Hand -delivered t..t Other:
Received By; (Signature)
Received By: (Signature)
aborat©ries E3y:
NPDES:
J NC
LSC
UST:
J NC
u SC
iJ OTHER
GROUNDWATER: DRINKING
dJ NC J NC
U SC lJ SC
IJ OTHER J OTHER
ATER: SOLID WASTE:
rJ NC
J SC
J OTHER
YPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Tell
RCRA: CERCLA LANDFILL OTHER:
'JNC -'Li NC JNC !...I NC
u SC J SC !J SC u SC
U OTHER (2.1 OTHER J OTHER L:I OTHER
n-Lined Cap VOA = Volatile Organics Analys
Additional Comments:
Zero Head Space)
FINA
Site -Arrival Time:
Site Departure Time:
REF
VERSE FOR
CONDITIONS
HI. COPY'

Fr—ab Report
6/12/01
Law Enq & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
Full Service Analytical 8, Environmental Solutions
Page 1 of 4
Customer Project ID: Church St
Customer Sample ID: DW-2
Prism Sample ID: AC09216
Loin Group: A0611H2A
Sample Collection Date/Time: 6/4/01 15:10
Lab Submittal Date/Time: 6/4/01 15:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Not detected ug/L 1 601 6/5/01 13:26 WAD
BROMOFORM Not detected ug/L 1 601 6/5/01 13:26 WAD
BROMOMETHANE Not detected ug/L 5 601 6(5/01 13:26 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 6/5/01 13:26 WAD
CHLOROBENZENE Not detected ug/L 1 601 6/5/01 13:26 WAD
CHLOROETHANE Not detected ug/L 5 601 6/5101 13:26 WAD
CHLOROFORM 4,7 ug/L 1 601 6/5/01 13;26 WAD
CHLOROMETHANE Not detected ug/L 5 601 6/5/01 13:26 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 6/5/01 13:26 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 601 6/5/01 13:26 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 601 6/5/01 13:26 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 6/5/01 13:26 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 6/5/01 13:26 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 6/5/01 13:26 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 601 6/5/01 13:26 WAD
1 „1-DICHLOROETHENE Not detected ug/1... 1 601 6/5/01 13:26 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 6/5101 13:26 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 601 6/5/01 13:26 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 6/5/01 13:26 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 6/5101 13:26 WAD
EDB Not detected ug/L 1 601 6/5/01 13:26 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 6/5/01 13:26 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 6/5/01 13:26 WAD
TETRACHLOROETHENE 61 ug/L 1 601 6/5/01 13:26 WAD
1,1,1-TRICHLOROETHANE Not detected ug/L 1 601 6/5/01 13:26 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L. 1 601 6/5/01 13:26 WAD
TR&CHLOROETHENE Not detected ug/L 1 601 6/5/01 13:26 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 6/5/01 13:26 WAD
VINYL CHLORIDE Not detected ug/L 5 601 6/5/01 13:26 WAD
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 601 6/5/01 13:26 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert, No, 37735 - FL Certification No, E87519
449 Spring,brook Road P.C), Box 240543 411. Charlotte, NC 28224-0543
Pholie 704/529-6364 Ai. 111 1ree Number: 1-800/529-6364 4., Fax: '704/525-4409

6/ 2/01
Eng & Env Services, Ind
Attn: Matt Gustis
PG Box 11297
Charlotte, NC 28220
The following an
mo
TEST
PARAMETER
Sample Corr relent
Customer Project ID Church St
Customer Sample ICE:
Prism Sample ID: AC09216
Login Group: A0611H2A
Sample Collection Date/Time: 6/4/ 1
Lab Submittal Date f in Ie 6/4/01
results have been obtained' for the indicated
TEST
RE UL T
Angela D. 0v rca h '.P. Laboratory Services
UNITS
c A a lyt olutron
Page 2 of 4
filch was submitted to this laboratory:
REPORTING METHOD
I ATE/TIME
LIMIT_ _REFERENCE TARTEPSTARTEDANALYST
n No. 402 - SC Certification No. 80012 - NC Brink€n Water Cerr. No, 37735 - FL Certification No, E87519
449 Spr
saes iO4
brsi��k Road ad P.O. Box 240543 Ch ar1
64`loll Free Number; t - +0(i3_ 9-t
Otte; C 2822 r-054
64 94. Fax, 704r" ' 5-0409

pr:Report
6/12/01
Law Eng & Env Services, Inc
Attn: Man Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC.
Full Service Analytical 8 Environmental Solutions
Page 3 of 4
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Same ID: AC09217
Login Group: A0611H2A
Sample Collection Date/Time: 6/4/01 15:00
Lab Submittal DaterTime: 6/4/01 15:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ARSENIC 0.035 mg/L 0.010 60106 6/11/01 13:20 MSP
BARIUM 0.087 mg/L 0.010 60106 6111/01 13:20 MSP
CADMIUM Not detected mg/L 0.001 60108 6/11/01 13:20 MSP
CHROMIUM 0.005 mg/L 0,005 6010E3 6/11/01 13:20 MSP
LEAD Not detected mg/L 0.005 6010B 6/11101 13;20 MSP
SELENIUM Not detected mg/L 0.010 60106 6/11/01 13:20 MSP
SILVER Not detected mg/L 0.005 6010B 6/11/01 13:20 MSP
MERCURY, TOTAL Less than mg/L 0.0002 EPA 245.1 6111/01 15:46 PRF
MERCURY DIGESTION Completed EPA 245,1 6/5/01 13.00 LC2
BROMODCHLOROMETHANE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
BROMOFORM Not detected ug/L 1 EPA 601/602 615/01 14:24 WAD
BROMOMETHANE Not detected ug/L 5 EPA 601/602 6/5/01 14:24 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 601/602 6/5/01 14;24 WAD
CHLOROBENZENE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
CHLOROETHANE Not detected ug/L 5 EPA 601/602 6/5/01 14:24 WAD
CHLOROFORM Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
CHLOROMETHANE Not detected ug/L 5 EPA 601/602 6/5/01 14:24 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 6/5/01 14;24 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601/602 6/5/01 14:24 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 EPA 601/602 6/5/01 14:24 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601/602 6/5/01 14:24 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No. E87519
449 Springbrook Road PC). Box 240543 A. Charlotte, NC 28224-0543
Phone [phone] Ab. Ton Free Number, 1-800.1529-6364 A.,. Fax: [phone]

6/12/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Login Group:
Sample Collection Date/Time:
Lab Submittal Date/Time:
PRISM
LABORATORIES, INC.
Furl Service Analytical & Environmental SDI 'Eons
Page 4 of 4
Church St
EFFLUENT
AC09217
AOS1 1 H2A
6/4/01 15:00
6/4/01 15:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
EDB
METHYLENE CHLORIDE
1,1 ,2,2-TET RACHLORO ETHANE
TETRACHLOROETHENE 4,0
1,1,'1-TR1CHLOROETHANE
1,1,2-TRlCHLOROETHANE
TRICHLOROETHENE.
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
BENZENE
ETHYLBENZENE
tPE
MTBE
TOLUENE
TOTAL XYLENES
CIS-1,2-DICHLOROETHENE
METALS DIGEST•SURFACE/GROUNDW Completed
TEST
RESULT
Sample Comments:
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Angela D. ©vercash, V.P. Laboratory Services
UNITS
ug/L
ugfL
ug/L
uglL
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
REPORTING METHOD
LIMIT REFERENCE
1
5
1
1
1
1
5
5
1
5
5
1
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
EPA 601/602
SW846-3005
DATE"TIME
STARTED ANALYST
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5/0114:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5101 14:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/5/01 14:24 WAD
6/8/0113:30 LC2
NC Certification No. 402 - SC Certific
No. 99012 - NC Drinking Water Cert. No, 37735 - FL Certification No, E87519
449 Springbrook Road t,O. Box 240543 .►. Charlotte, NC 28224-0543
Phone: [phone]. Toll Free Number: 1-800/529-6364 w Fax:[phone]

ABORATORIES, INC.
Full Service Analytical $. Environmental Solutions
Client
Physical Address
Phone
P.O.#/B
n
Project Name
ence
Fax
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE
449 Springbrook Road . Charlotte, NC 28217
P.O. Box 240543 Charlotte, NC 28224-0543
Phone:[phone] Fax:[phone]
REPORT TO; Name
Address
BILL TO: Name
Address ...
Requested Due Date Li 1 Day G 2 Days J 3 Days L1 4 Days ❑ S Days
0 6-9 Days :i Standard 10 days
Samples. received alter 1 ,f}(D vvdll Se processed the next business day.
Turnaround lime is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
NTACT upon arrival?
Received ON WET ICE? Temp
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
State Certification
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
CLIENT
AMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX.
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
'TYPE
SEE BELOW
NO.
SIZE
PRESERVA-
TIVES
NC N/A
SC Other NA ...
No NA
Yes No
OTHER
PRESS DOWN FIRMLY - 3 COPIES
ANALYSES REOUESTED
REMARKS
SUB
LAB
CERT:
ID NO.
PRISM
LAB
ID NO.
plee`s Signature
Sampled By (Print Name)
Affiliation
Se9ertqudshed By: (Sig ature
Beainquished By: (Signature)
aelinquiuhed By: (Signature)
kS )hod at Shipment:.
Fed Ex lJ UPS '-J Ha: d-devexed ;1 other:
ereaved By
Ived By (Sig are)
Received For Prism Labor4tone
UST: GROUNDWATER: DRINKING WATER: SOLID WASTE:
J NC :] NC Li NC J NC
J SC IJ SC J SC J SC
Li OTHER J OTHER J OTHER Li OTHER
RCRA:
CI NC
SC
J OTHER
Dale
Dale
Hours
CERCLA LANDFILL OTI-IER:
Li NC :1NC l,dNC
JSC JSC JSC
J OTHER. J OTHER ri OTHER
Additsonal Comments:
Field, Tech Fee:
SEE REVERSE, FOR
TERNS & CONDITIONS
FINAL REPORT COPY
A - — Toflnn..l Inw.d ran Vr1A `/nlafitp rlrnanir. Analysts (7.ero Head Space)

Fr—
ab Report
6/8/01
Law Eng & Env Services, Inc
Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC.
Fuft Service Analytic& 8 Environmental Sof Lions
Page 1 of 2
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC09570
Login Group: A068H1
Sample Collection Date/Time: 6/7/01 08:00
Lab Submittal DatefTime: 6/7/01 08:30
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Not detected ug/L 1 601 6/7/01 23:27 WAD
BROMOFORM Not detected ug/L 1 601 6/7/01 23:27 WAD
BROMOMETHANE Not detected uglL 5 601 6/7/01 23:27 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 6/7/01 23:27 WAD
CHLOROBENZENE Not detected ug/L 1 601 6/7/01 23:27 WAD
CHLOROETHANE Not detected ug/L 5 601 6/7101 23:27 WAD
CHLOROFORM Not detected uglL 1 601 6/7/01 23:27 WAD
CHLOROMETHANE Not detected ug/L 5 601 6/7/01 23:27 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 6/7/01 23:27 WAD
1,2-DLCHLOROBENZENE Not detected ug/L 1 601 6/7/01 23:27 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 601 6/7/01 23:27 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 6/7/01 23:27 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 6/7/01 23:27 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 6/7/01 23:27 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 601 6/7/01 23:27 WAD
1,1-DICHLOROETHENE Nat detected ug/L 1 601 6/7/01 23:27 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 6/7/01 23:27 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 6Ct1 6/7/01 23:27 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 6/7/01 23:27 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 6/7/01 23:27 WAD
EDB Not detected ug/L 1 601 6/7/01 23:27 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 6/7/01 23:27 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 6/7/01 23:27 WAD
TETRACHLOROETHENE Not detected ug/L 1 601 6/7/01 23:27 WAD
1,1,1-TRICHLOROETHANE Not detected ug/L 1 601 6/7/01 23:27 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L 1 601 6/7/0123:27 WAD
TRICHLOROETHENE Not detected ug/L 1 601 6/7/01 23:27 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 6/7/01 23:27 WAD
VINYL CHLORIDE Not detected ug/L 5 601 6/7/01 23:27 WAD
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 601 6/7/01 23:27 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road P.O. Box 240543 Charlotte, NC 28224-0543
Phorne: 704/529-6364 Toll Free Number: 1-800/524-6364 Faye: 704/525-0409

ces
618/01
Law Eng & Env ery
Matt Eustis
PO Box 11297
Charlotte, NC 8 0t
The folio in
TEST mm
PARAMETER
Sample ComComment
tic
AnCyh & ErvironrrentaI Saciutian
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC09570
Login Group: A068H1
ple Collection atelTime: 6/7/01
Lab Submittal Date/Time: 6/7/01
ag2 of2
08:00
08:30
btained for the indicated sample which was submitted to this'laboratcry.
22
TEST
RESULT UNITS
Angela D. Overcash, V.P, abora
NC Certification No, 402
SC Cerb cation No.
449Sprit) onk
Phone: 704/529
es
REPORTING METHOD
DATE/TIME
LIMIT REFERENCE E STARTED ANALYST
NC DrinkingOat
Cert. No. 37735 FL rkiflcation e. 875t9
P.O. Box 24 543 28224-0 43
e Number; 1- 00 529-6364 Ea : 704/525-0409

.Service Analytical & Envirwirneritail Solutions
Client .
Ptrysical Address
Fax
PAM/Billing Reference —
Prolect Name
CLIENT
SAMPLE DESCRIPTION
Sampler's Signature
Inqa
y. (Signature
Relinquished By {Signature).
Relinquished By: (Signature)
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE II
449 Springbrook Road Charlotte, NC 28217
P.O, Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
P DOWN FIRMLY - 3 COPiES
REPORT TO: Name
Address
BILL TO: Name
Address
Requested Due Dale —
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
SAMPLE CONTAINER
"TYPE
SEE BELOW
Sampled By (Print Name) _
RueMd By
ignaturet
Rcewed By: (Signature)
eceived For Prism Lahoratorles By:
Method of Shipment
NPDES NC UST NC ___ GROUNDWATEROTNER :
OTHERI.fTft
INER TYPE CODES: A 4,- Amber C = Clear G = Glass P Plastic:
PRESERVA-
TIVES
Date
Date
Samples INTACT upon anival?
Receivixl ON WET ICE? Temp
PROPER PRESEFTVATIVES inificated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed VOMIT HEADSPACE7
PROPER CONTAINERS use?
State Certification
Requested
YES A
NC SC Other NA
Water Chlorinated Yes , No NA
Sample Iced Upon Collection Yes No
YSES REOUESTED
/ ,/ /
/
Log -in Group No.
Affiliation
ryiNours
DRINKING WATER: NC
SC scoe
OTHER OTHER
TL Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
REMARKS
Additional Comments
SOLID WASTE:
NC
SC
SUB
LAB
CERT.
tD NO.
OTHER: NC
sc
OTHER
SEE REVERSE FOR
TERMS S CONDITIONS
PRISM
LAB
FINAL REPORT COPY

Full Service Analytical & Environmental Solutions
Ctient --
Physical Address
Phone _
P.O.M/Billing Re 1e n
Project Name
Fax
CHAIN OF CUSTODY RECORD
CLIENT DATE
AMPLE DESCRIPTION ! COLLECTED
PAGE OF® QUOTE
449 Springbrook Road .. Charlotte, NC 28217
P,O. Box 240543 :. Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
PRESS tM1i1NN FIRMLY - 3 COPIES
REPORT TO: Name
Address
BILL TO: Name _..
Address
Requested Due Date
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
LAB USE ONLY
Samples INTACT upon arrival?
Received ON WET ICE? Ternp
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES rec'd WIOUT HEADSPACE?
PROPER CONTAINERS used?
State Certification
Requested NC SC Others NA
Water Chlorinated Yes , No NA
Sample Iced Upon Collection Yes No
YES NO
TIME MATRIX
OLLECTED (SOIL
MILITARY WATER OR
HOURS SLUDGE)
SAMPLE CONTAINER
PRESERVA-
TIVES
REMARKS
SUB
LAB
CERT.
D NO.
PRISM
LAB
tD NO.
Sampler's Signature
Sampled By (Print Name)
idnquished By: {Signature)
eived By: ,Signature)
Rerrnquished By: (Signature)
Date
Affiliation ._ ._._._ __ .
/Ho
d' By: (Signature)
Relinquished By: (Signalu
hod of Slttpnaen
d For Prism Laboraton
up No.
NPDES NC
SC
OTHER
UST:
NC GROUNDWATER: NC . DRINKING WATER: NC
SC SC SC
OTHER OTHER OTHER.
Additional Comments
SOLID WASTE: NC . OTHER: NC
SC SC
OTHER OTHER
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (2
Head Space)

r .
ab Report
6/19/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC.
Full Service Ana lVtflr; . En rrtnSolutions
Page 1 of 4
Customer Project ID: Church St.
Customer Sample ID* EFFLUENT
Prism Sample ID: AC10061
Login Group: A0618H2A
Sample Collection Date/Time: 6/11/01 12:05
Lab Submittal Date/Time: 6/11/01 15:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE
BROMOFORM Not detected ug/L 1 601 6/16101 18:24 WAD
BROMOMETHANE Not detected ug/L 5 601 6/16/01 18:24 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 6/16/01 18:24 WAD
CHLOROBENZENE Not detected ug/L 1 601 6/16/01 18:24 WAD
CHLOROETHANE Not detected ug/L 5 601 6/16/01 18;24 WAD
CHLOROFORM Not detected ug/L 1 601 6/16/01 18:24 WAD
CHLOROMETHANE Not detected ug/L 5 601 6/16/01 '16:24 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 6/16/01 18:24 WAD
1,2-DICHLOR©BENZENE Not detected ug/L 1 601 6/16/01 18:24 WAD
1,3-DICHLOROBENZENE Not detected uglL 1 601 6/16/01 18:24 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 6/16/01 18:24 WAD
DICHLORODIFLUOROMETHANE Not detected uglL 5 601 6/16/01 18:24 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 6/16/01 18:24 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 601 6/16/01 18:24 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 601 6/16/01 18:24 WAD
TRANS-I,2-DICHLOROETHENE Not detected ug/L 1 601 6/16/01 18:24 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 601 6/16/01 18:24 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 6/16/01 18:24 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 6/16/01 18:24 WAD
EDB Not detected ug/L 1 601 6/16/01 18:24 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 6/16/01 18:24 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 6/16/01 18:24 WAD
TETRACHLOROETHENE Not detected ug/L 1 601 6/16/01 18:24 WAD
1,1,1-TRICHLOROETHANE Not detected ug/L 1 601 6/16/01 18:24 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L 1 601 6/16/01 18:24 WAD
TRICHLOROETHENE Not detected ug/L 1 601 6/16/01 18:24 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 6/16/01 18:24 WAD
VINYL CHLORIDE Not detected ug/L 5 601 6/16/01 18:24 WAD
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 601 6/16/01 18:24 WAD
Not detected ug/L 1 601 6/16/01 18:24 WAD
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No. E87519
449 SFringbro_uok Road ,a,. P.O. Box 240543 .. Charlotte, NC 2,8224-0543
Phetic. 704,/5294,364 Toll tree Number: 1-800/529-6364 Fax:',04/525-0409

ab Report
6/19/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC.
Full Service Analytical Environmental „Solutions
Page 2 of 4
Customer Project ID: Church St.
Customer Sample ID: EFFLUENT
Prism Sample ID: AC10061
Login Group: A0618H2A
Sample Collection Date/Time: 6/11/01 12:05
Lab Submittal Date/Time: 6/11/01 15:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
............„.
ARSENIC Not detected mg/L 0.010 60106 6/18/01 16:58 MSP
BARIUM 0 082 mg/L 0.010 60106 6/18/01 16:58 MSP
CADMIUM Not detected mg/L 0.001 60106 6/18/01 16:58 MSP
CHROMIUM Not detected mg/L 0.005 60106 6/18/01 16:58 MSP
LEAD Not detected mglL 0.005 6010B 6/18/01 16:58 MSP
SELENIUM Not detected mg/L 0.010 60106 6/18/01 16:58 MSP
SILVER Not detected mg/L 0.005 60106 6/18/01 16:58 MSP
MERCURY, TOTAL Less than rng/L 0.0002 EPA 245,1 6/19101 15:33 PRF
MERCURY DIGESTION Completed EPA 245.1 6/19/01 11:15 PRF
METALS DIGEST-SURFACE/GROUNDW Completed SW846-3005 6/18/01 10;20 LC2
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert., No. 37735 - FL Certification No. E87
449 Springbrook Road P:O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Toll Free Number: 1-8001529-6364 alh. Fax: [phone]

rab Report
6/19/01
Law Eng & Env Services, inc
Attn: Matt Gust's
PO Box 11297
Charlotte, NC 28220
PRISM
ABORATORIES, INC,
Full Service Analytical iS Environmental Soiutions
Page 3 of 4
Customer Project ID: Church St.
Customer Sample ID: DW.2
Prism Sample ID: AC10062
Login Group: A0618H2A
Sample Collection Date/Time: 6/11/01 12:30
Lab Submittal Date/Time: 6/11/01 15:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Not detected ug/L 1 601 6/16/01 19:20 WAD
BROMOFORM Not detected ug/L 1 601 6/16/01 19:20 WAD
BROMOMETHANE Not detected ug/L 5 601 6/16/01 19:20 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 6/16/01 19:20 WAD
CHLOROBENZENE Not detected ug/L 1 601 6/16/01 19:20 WAD
CHLOROETHANE Not detected ug/L 5 601 6/16/01 19:20 WAD
CHLOROFORM 2,1 ug/L 1 601 6/16/01 19:20 WAD
CHLOROMETHANE Not detected ug/L 5 601 6/16/01 19:20 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 6/16/01 19:20 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 601 6/16/01 19:20 WAD
1,3-DICHLORO6ENZENE Not detected ug/L 1 601 6/16/01 19:20 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 6/16/01 19:20 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 6/16/01 19.20 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 6/16/01 19:20 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 601 6/16/01 19:20 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 601 6/16/01 19:20 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 6/16/01 19:20 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 601 6/16/01 19:20 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 6/16/01 19:20 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 6/16/01 19:20 WAD
EDB Not detected ug/L 1 601 6/16/01 19:20 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 6/16/01 19:20 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 6/16/01 19:20 WAD
TETRACHLOROETHENE 24 ug/L 1 601 6/16/01 19:20 WAD
1,1,1-TRICHLOROETHANE Not detected ug/L 1 601 6/16/01 19:20 WAD
1,1,2-TRICHLOROETHANE Not detected ug/L 1 601 6/16/01 19:20 WAD
TRICHLOROETHENE Not detected ug/L 1 601 6/16/01 19:20 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 6/16/01 19:20 WAD
VINYL CHLORIDE Not detected ug/L 5 601 6/16/01 19:20 WAD
CIS-1,2-D1CHLOROETHENE Not detected ug/L 1 601 6/16/01 19:20 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No. E87519
449 Springbrook Road R.O. Box 240543 Charlotte, NC 28224-0.543
Phone: '704/529-6364 AI. Toll Free. Number: 1-8001529-6364 -a. Fax: [phone]

Frab Report
6/19/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
P© Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC,
Fut Serwl e Aaalo,cai & Envlrnrirrzrrr7Yai'Sclutians
Page 4 of 4
Customer Project ID: Church St.
Customer Sample ID: DW-2
Prism Sample ID: AC10062
Login Group: A©618H2A
Sample Collection Date/Time. 6/11/01 12:30
Lab Submittal Date/Time: 6/11/01 15:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
Sample Comments:
TEST
RESULT
Angela D. ©vercash, V.P, Laboratory Services
UNITS
REPORTING METHOD DATE/TIME
STARTED ANALYST
LIMIT REFERENCE
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert, No, 37735 - FL Certification No, E87519
449 Springhrrc ak. Road -,. P.O. Box 240543 Charlotte_, NC 28224-0543
I:r 7041329-636, IL Toll Free Number: 1-80077529-6364 Fax. [phone]

s
LABORATORIES,
Eull Brvlce Analytical Environmental Solutions
Client
Physical Address
Phone
P,O,tf/Billing Reference
Project Name
Fax
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Springbrook Road .. Charlotte, NC 28217
P.O. Box 240543 �. Charlotte, NC 28224-0543
Phone: [phone] ► Fax: [phone]
REPORT TO: Name
Address
BILL TO; Name
Address
Requested.Doe Date J 1 Day U 2 Days LI 3 Days •. 4 Days 't.J 5 Days
O 6-9 Days 1J Standard 10 days
Samples received alter 15:(70 will be processed the next business day.
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
Samples INTACT upon arrival?
Received ON WET ICE? Temp
PROPER PRESERVATIVES indicated?
lied WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEA[:'1'SPACE?
PROPER CONTAINERS used'?
State C
cation
Requested FL NC
Water Chlorinated Yes
Sample Iced Upon Collection
CMUD NPDES
CLIENT
SAMPLE DESCRIPTIO
DATE
COLLECTS
TIME
OLLECTED
MIMARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE) SEE BELOW
ANALYSE
SC Other
No NA
Yes No
OTHER
NO N?'A
NA
EOUESTED
SAMPLE CONTAINER
NO. ! SIZE
PRESEFIVA-
TIVES
REMARKS
SUB
LAB
CERT,
ID NO.
PRISM
LAB
ID NO,
Sampler's Signature
tied By; (Slgrralul'dp
By. (Signrrtur
By: (Signature)
hod of Shipment:
UPS J Pir3r
NPDES:
�JNC
SC
UST:
J NC
J SC
ER J OTHER
Sampled By (Print Name)
GROUNDWATER: DRINKING WATER:
INC INC
JSC CJSC
J OTHER J OTHER
SOLID WASTE::
'J NC
J SC
J OTHER
RCRA: CERCLA LANDFILL
JNC OJNC JNC
rJSC i_tSC JSC
J OTHER LJ ©THEM J OTHER
Affiliation
Additional Comments:
OTHER:
(1 NC
J SC
J OTHER
SEE REVERS
TERMS & CONII
FHNAL REP t HT.w COPY"
CODES: A = Amber C _ Clear
G = Glass P = Plastic; TL Teflon -Lined Cap VOA = Volatile Organics Anatysi
Zero Head Space)

pra.13 Report
6/26/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
RISM
ORATORIES, INC.
Full Service Anaiylical & Environmental Solutions
Page 1 of 4
Customer Project ID: Church St.
Customer Sample ID: EFFLUENT
Prism Sample ID: AC10836
Login Group: A0626H2
Sample Collection Date/Time: 6/19/01 11:40
Lab Submittal Date/Time: 6/19/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Not detected ug/L 1 601 6/27/01 12:01 WAD
BROMOFORM Not detected ug/L 1 601 6/27/01 12:01 WAD
BROMOMETHANE Not detected ug/L 5 601 6/27/01 12:01 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 6/27/01 12:01 WAD
CHLOROBENZENE Not detected ug/L 1 601 6/27/01 12:01 WAD
CHLOROETHANE Not detected ug/L 5 601 6/27/01 12:01 WAD
CHLOROFORM Not detected ug/L 1 601 6/27/01 12:01 WAD
CHLOROMETHANE Not detected ug/I_ 5 601 6/27/01 12:01 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 6/27/01 12:01 VVAD
1,2-DICHLOROBENZENE Not detected ug/L 1 601 6/27/01 12:01 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 601 6/27/01 12:01 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 6/27/01 12:01 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 6/27/01 12:01 WAD
1,1-DICHL0ROETHANE Not detected ugiL 1 601 6/27/01 12:01 WAD
1,2-DICHLOROETHANE Not detected ug/L 1 601 6/27/01 12:01 WAD
1,1-DICHLOROETHENE Not detected ugiL 1 601 6/27/01 12:01 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 6/27/01 12:01 WAD
1,2-DICHLOR0PROPANE Not detected ug/L 1 601 6/27/01 12:01 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 601 6/27/01 12:01 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 6/27/01 12:01 WAD
EDB Not detected ug/L 1 601 6/27/01 12:01 WAD
METHYLENE CHLORIDE Not detected ugiL 5 601 6/27/01 12:01 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 6/27/01 12:01 WAD
TETRACHLOROETHENE Not detected ug/L 1 601 6/27101 12:01 WAD
1,1,1-TRICHLOROETHANE Not detected ugIL 1 601 6/27/01 12:01 WAD
1,1,2-TRICHLOROETHANE Not detected ugit 1 601 6/27/01 12:01 WAD
TRICHLOROETHENE Not detected ug/L 1 601 6/27/01 12:01 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 6/27/01 12:01 WAD
VINYL CHLORIDE Not detected ug/L 5 601 6/27/01 12:01 WAD
CIS-1,2-DICHLOROETHENE Not detected ugit 1 601 6/27/01 12:01 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ..., P.O. Box 240543 .41.. Charlotte, NC 28224-0543
Phone: [phone] ... Toll Spree Nusnber: 1-800/529-6364 ..k. Fax: [phone]

Frab Report
6/28/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Loin Group:
Sample Collection Date/Time:
Lab Submittal DaterTime:
PRISM
LABORATORIES, INC
Full Service AnalytcW & En&onmenlel Solams
Page 2 of 4
Church St.
EFFLUENT
AC10836
A0626H2
6/19/01 11:40
6/19/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
MERCURY, TOTAL
MERCURY DIGESTION
METALS DIGEST-SURFACE/GROUNDW
Sample Comments:
TEST
RESULT
REPORTING METHOD DATE/TIME
UNITS LIMIT REFERENCE STARTED ANALYST
0,016 mg/L
0.051 mglL
Not detected mg/L
Not detected mg/L
Not detected mglL
Not detected mg/L
Not detected mglL
Less than mg,/
Completed
Completed
Angela D. Overcash, V.P, Laboratory Services
0,010 60108 6/26/01 15:07 MSC
0.010 6010B 6/26/01 15:07 MSC
0.001 6010B 6/26/01 15:07 MSC
0.005 6010B 6/26/01 15:07 MSC
0.005 6010B 6/26/01 15:07 MSC
0.010 6010B 6/26/01 15:07 MSC
0.005 60108 6/26/01 15:07 MSC
0 0002 EPA 245.1 6/22/01 13,37 PRF
EPA 245.1 6/21/01 13 50 LC2
SW846-3005 6/25/01 09:15 LC2
NC Certification No. 402 - SC Certific
No. 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No. E87519
449 Springbrook Road AL P.O. Box' 240543 AL. Charlotte, NC 28224-0543
Phone: [phone]. Ton Free N0mber: I-800/529-6364 Fax: [phone]

Frab Report
6/28/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC.
Fral Service Analytical Environmental Sdutionz
Page 3 of 4
Customer Project ID: Church St.
Customer Sample ID: DW-2
Prism Sample ID: AC10837
Login Group: A0626H2
Sample Collection Date/Time: 6/19/01 12:15
Lab Submittal Date/Time: 6/19/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ROMODICHLOROMETHANE Not detected ug/L 1 601 6/27(01 12:58 WAD
BROMOFORM Not detected ug/L 1 601 6/27/01 12:58 WAD
BROMOMETHANE Not detected ug/L 5 601 6/27/01 12:58 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 6/27/01 12:58 WAD
CHLOROBENZENE Not detected ug/L 1 601 6/27/01 12:58 WAD
CHLOROETHANE Not detected ug/L 5 601 6/27/01 12:58 WAD
CHLOROFORM 2,7 ug/L 1 601 6/27101 12:58 WAD
CHLOROMETHANE Not detected ug/L 5 601 6127/01 12:58 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 6/27i'01 12:58 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 601 6/27/01 12:58 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 601 6/27/01 12:58 WAD
1,4-D1CHLOROBENZENE Not detected ug/L 1 601 6127/01 12:58 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 6127/01 12:58 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 6/27/01 12:58 WAD
1,2-DICHLOROETHANE Not detected uglL 1 601 6127/01 12:58 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 601 6/27/01 12:58 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 6/27/01 12:58 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 601 6/27/01 12:58 WAD
CIS-1,3-DiCHLOROPROPENE Not detected ug/L 1 601 6/27/01 12:58 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 6/27/01 12:58 WAD
EDB Not detected uglL 1 601 6127/01 12:58 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 6/27/01 12:58 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 6/27/01 12:58 WAD
TETRACHLOROETHENE 19 ug/L 1 601 6/27/01 1256 WAD
1,1,1-TRICHLOROETHANE Not detected ug/L 1 601 6127/01 12:58 WAD
1,1,2-TR1CHLOROETHANE Not detected ugh. 1 601 6/27/01 12:58 WAD
TRICHLOROETHENE Not detected ug/L 1 601 6127/01 12:58 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 6/27/01 12:58 WAD
VINYL CHLORIDE Not detected uglL 5 601 6/27101 12:58 WAD
CI5-1,2-DICHLOROETHENE Not detected ug/L 1 601 6/27/01 12:58 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road 4., F.U. Box 240543 ..b. Charlotte, NC 28224-0543
Phone; 704;520 6364 ...... loll Free Number: 1-8001529-6364 Illa Fax [phone]

6/28/01
Law Eng & EnvServices, Inc
Attn: Matt Gust's
PO Box 1197
Charlotte, NC
F 6i 5ervrca An ytc t& Envir Wrier
Page 4 of
Customer Project ID: Church St.
Customer Sample ID:
Prism Sample ID: AC10837
Login Group: A0626H2
Sample Collection ate/T€me: 6/19/01 12:15
Lab,Submittal Date/Time. 6/19/01 14:45
The following nalytio rl results have been obtained for the indicated sample which was submitted to this labor a
TEST
PARAMETER
Samp)
Co
TEST
RESULT
REPORTING METHOD DATE/TIME
LIMIT REFERENCE .w.._ STARTED ANALYST
Angela D Overcash VP. L borateryServices
NC erttfl aton Na, 402 SC Certification Ne, 99012 Drinkino Water Cart. No. 37735 FL. Cellific tl n c E87519
449 Spun
R tt
2405ttarltt; ?ii 4
4
49

PRISM
LABORATORIES, INC.
Full Service Analytical & Envlronmofltal Solutions
Client
Physical Address
Phone
P.0,#/Billing Reference
Project Name
Fax
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Springhtook Road — Charlotte, NC 28217
P.O. Box 240543 Charlotte„ NC 28224-0543
Phone: [phone] Fax: [phone]
REPORT TO Name
Address
BILL TO.: Name
Address
Requested Due Date 1 '1. Day 12 Days 13 Day 1 4, Diy 1 5 Days
Li 6-9 Days :LJ Standard 10 days
Samples received alter 1600 wii.{ Oe processed the nexl..htisiness day,
Turnaround time is based on business Qiays, exciuding vveekencts and holidays:
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
LAB USE ONLY
NO N/A
Sampies INTACT upon arrivaI?
Received ON WET Co.? Temp
PROPER PRESERVATIVES indicated?
Received WI IHIN HOLDING TimES?
CUSTODY SEALS INT,ACT?
VOLATILES rin'd MOUT HEADSPACE?
PROPER CONTAflERE LNE3E:E?
State Certification
Requested FL NC SC Other NA
Water Chlorinated Yes No NA
Sample Iced Upon Collection Yes No
CMUD NPDES OTHER
PRESS DOWN FIRMLY - 3 COPIES
TIME MATRIX SAMPLE CONTAINER
CLIENT DATE COLLECTED (SOIL, PRESERVA-
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE TIVES
.
HOURS SLUDGE) SEE BELOW NOSIZE
ANALVSES REOUEST
REMARKS
SUB
LAB
CEFIL
ID NO.
PRISM
LAB
ID NO.
SamplePS Signature
Sampled By (Print Name)
HolinquiEAREci By: (Signamieu „,„
Holiiiquished By: 131.9tiaTiJiMi
r6nquseo Sy(SiEratutel
Moirtoo et Soipmertt
Ecu Ex 1 LIPS OIEKEE:
E eceiyed By: ESigiraium
Received By: (Sionaturel
Received For Prism Laboratories By:
bate
Affiliation
Ifitarylhours
Date ,
I .
Log -In Or NuL
NPDES:
1_1 NC
UST:
NG
j SC
j OTHER
GROUNDWATER: DRINKING WATER: SOLID WASTE:
Li NC INC LI NC
j SC tj SC j SC
ij OTHER Li OTHER j OTHER
RCRA:
L) NC
SC
OTHER
h — Amhrar G= (laP . Plastic,: TL Teflon -Lined Cap
CERCLA
ij NC
Li' SC
Li OTHER
LANDFILL OTHER:
NC INC
J SC i_J SC
Li OTHER ,J OTHER
Additional Conarnents
VOA = Volatile Oman cs Analysis (Zero Head Space)
Ari'iyai Time:
Silo DE:EN:ME:Ere Time:
Ersoki Fee:
Mil.iag
SEE REVERSE FOR
TERRIS CONDITIONS
FINAL REPORT COPY

ab Report
7/6/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC,
Ffi�ll ;per✓¢ce Analytica4 &
Page 1 of 4
Customer Project ID: Church St
Customer Sample ID: EFFLUENT
Prism Sample ID: AC11384
Login Group: A072H2
Sample Collection Date/Time: 6/25/01 14:20
Lab Submittal Date/Time: 6/25/01 15:55
n
ntal Solut'tuo.s
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
BROMODICHLOROMETHANE
BROMOFORM
BROMlOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHA.NE
DIBROMCCHLOROMETHANE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1„4-DICHLOR©BENZENE
D!CHLC)RODIFLUOROMETHANE
1,1-DICHLOROETHANE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
TRANS-1,2-DICHLOROETHENE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPR.OPENE
TRANS-1,3-DICHLOROPROPENE
EDB
METHYLENE CHLORIDE
1,1,2,2-TETRACHLOROETHANE
TE'TRACHLOROETHENE
1,1,1-TRICHI OROE'THANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLCRC FLUOROMETHANE
VINYL CHLORIDE
CIS-1,2-DICHLOROETHENE
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 5 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01.51 WAD
Net detected ug/L 5 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 5 601 7/6/01 01:51 WAD
No1 detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 5 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 5 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 5 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01;51 WAD
Not detected ug/L 5 601 7/6/01 01:51 WAD
Not detected ug/L 5 601 7/6/01 01:51 WAD
Not detected ug/L 1 601 7/6/01 01:51 WAD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No, E87519
449 SBringbrook Road A. P.O. Box 24415.#3 Charkttex NC 28224-0543
Phone:, 704 529-6364 ion Free Number: I-SOO/529-f 364 a, F.nr; 70- 52i 0409

7/6101
Law Erg & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
The following ana
TEST
PARAMETER
LABORATOR1E
t O Service Ana 'red Envrmri a to fu
Page2 of
Custo Project lids Church St
Customer mpl 1D: EFFLUENT
Prism Sample 1:: AC11384
LoginGroup: A072H2
Sample Collection Date/Time: 6/ 5/01 14:20
Lab Submittal Date/Time: 6/25/01 1 15:55
foal results have been obtained for the indicated sample which was submitted to this laboratory
ARSEMC
3AaR3M
CADMlUM
CRt OMI
LEAD
SELErveftM
StLEP
MERCURY, TOTAL
MERCURY DIGESTION
TEST
RESULT
METALS DIGEST—SURFACE/GROUND/
SampleComments:
Angel i;D. Over ash, V.P.
REP{RTiNG METHOD
UNITS LIMIT REFERENCE
0.019tg/L
0.080 mg/L
Not detected img/L
Not detected mg/L
Not detected mg/L
Not detected mg/I
Not detected mg/L
Less that mgiL
Completed
Completed
Co-ATE/TIME
STARTED ANALYST
0.010 6010E 7/3/0111;45 MSG
0,010 6010E 0 1:45 MSC
0.001 6010E 7l3/01 i 1:45 MSC
0.005 6010 7/ /01 11:45 MSG
0.005 6010S 7131 111:45 MSC
0.010 6010E 7/3/01 11.45 MSC
0 005 6010E 713/01 11:45 MSC
0.0002 EPA 245.1 6/29/01 12:41 PRF
EPA 245,1 6/28/01 09:15 LC2,
SW846-3005 7/210108:30 LC2
aborato Services
NC C rtitr at'sc n No. 402 - SC Cert
ation No, 99012 NC Drinking 'Water Dart. No, 37735 - FL Cortifc on No, 9875
44*/ Sprin rl ass
24ta
/to 240543 C,st art°tt , i (, 2 324-1t 4
Number. ! fttix52 -fa. r4 t'a :7041525-0409

lir ab Report
7/6/01
Law Eng & Env Services, Inc
Attn: Matt Gust's
PO Box 11297
Charlotte, NC 28220
R1SM
LABORATORIES, INC.
Flo Service Analytical Envircelmental Solutionz
Page 3 of 4
Customer Project ID: Church St
Customer Sample ID: DW-2
Prism Sample ID: AC11385
Login Group: A0721-12
Sample Collection Date/Time: 6/25/01 15:00
Lab Submittal Date/Time: 6/25/01 15:55
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Not detected ug/L 1 601 7/6/01 02:47 WAD
BROMOFORM Not detected ug/L 1 601 7/6/01 02:47 WAD
BROMOMETHANE Not detected ug/L 5 601 7/6/01 02:47 WAD
CARBON TETRACHLORIDE Not detected ug/L 1 601 7/6/01 02:47 WAD
CHLOROPENZENE Not detected ug/L 1 601 7/6/01 02:47 WAD
CHLCROETHANE Not detected ug/L 5 601 7/6/01 02:47 WAD
CHLOROFORM Not detected ug/L 1 601 7/6/01 02:47 WAD
CHLOROMETHANE Not detected ug/L 5 601 7/6/01 02:47 WAD
DIBROMOCHLOROMETHANE Not detected ug/L 1 601 7/6/01 02:47 WAD
1,2-DICHLOROBENZENE Not detected ug/L 1 601 7/6/01 02:47 WAD
1,3-DICHLOROBENZENE Not detected ug/L 1 601 7/6/01 02:47 WAD
1,4-DICHLOROBENZENE Not detected ug/L 1 601 7/6/01 02:47 WAD
DICHLORODIFLUOROMETHANE Not detected ug/L 5 601 7/6/01 02:47 WAD
1,1-DICHLOROETHANE Not detected ug/L 1 601 7/6/01 0247 WAD
1.2-DICHLOROETHANE Not detected ug/L 1 601 7/6/01 0247 WAD
1,1-DICHLOROETHENE Not detected ug/L 1 601 7/6/01 02:47 WAD
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 601 7/6/01 02:47 WAD
1,2-DICHLOROPROPANE Not detected ug/L 1 601 7/6/01 02:47 WAD
CIS-1,3-DICHLOROPROPENE Not detected ug/L, 1 601 7/6/01 02:47 WAD
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 601 7/6/01 02;47 WAD
EDB Not detected ug/L 1 601 7/6/01 02:47 WAD
METHYLENE CHLORIDE Not detected ug/L 5 601 7/6/01 02:47 WAD
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 601 7/6/01 02:47 WAD
TETRACHLOROETHENE 3.5 ug/L 1 601 7/6/01 02:47 WAD
1,1,1-TR7CHLOROETHANE Not detected ug/L 1 601 7/6/01 02:47 WAD
1.1.2-TR1CHLOROETHANE Not detected ug/L 1 601 7/6/01 02:47 WAD
TRICHLOFROETHENE Not detected ug/L 1 601 7/6/01 02:47 WAD
TRICHLOROFLUOROMETHANE Not detected ug/L 5 601 7/6/01 0247 WAD
VINYL CHLORIDE Not detected ug/L 5 601 7/6/01 02:47 WAD
CIS-1,2.-DICHLOROETHENE Not detected ug/L 1 601 716/01 02:47 WAD
NC Cerlificat n No, 402 - SC .Certification No, 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No, E87519
449 Springhrook Road At. P.0, Box 24054.3 Charlotte, NC 2S224-0543
Phone: 704,1529-636,4 JAI Free Nurnhc 1- 1i00/529-6364 „s, Fax: [phone]

7/6 01
Law Eng & Env Services, Ind
Attu: Matt Gusfis
PO Box 112977
Charlotte, NC 2220
Full settvi :Ga Ar,si
Customer Project ID: Church St
Customer Sarriple ID: DW4
Prism Sample ID: AC11385
Page4 of
Login Group; A072H2
Sample Collection at /Tim : /2 / 1 1 :00
Lab Submittal t/Tim. 6126101 1
The fcll Ling analyticaesul have been obtained for the indicated sample which was submitted to this laboratory
TEST
-Ar AM T
arnpio Com ents:
TEST
RESULT UNITS
Angola D. Overcash,'".P. LaboratoryServices
REPORTING METHOD DATETT1ME
LIMIT REFERENCE STARTED ANALYST
NC CAN flcation No, 402 - SC Certlfir stun No. 9901 T NC Drinking Water C rt, N . 37735 w FL Certification No, E87519
449 rriza r'cacrl C saa '.) 13a 24 !
I cr

PRISM
LABORATORIES, INC,
Full Service Anaytici & Environmental Solutions
Client
Physical Address
Phone
PA:Le/Billing Reference
Project Name
Fax
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE
449 Spritighrook Road Ai« Charlotte, NC 28217
P.O. Box 240543 4. Charlotte, NC 28221-0543
Phone l '704/529-6364 Fax: [phone]
REPORT TO: Name
Address
BILL TO: Name
Address
Requested Due Date 11 Day 2 fl/y 1 3 0ay 1 4 Days LI ays
LI 6-9 Days LI Standard 10 days
Samples received after 1500 will be processed the next business day
Turnaroundtime is based on business days, excluding weekends and holidays
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
Samples INTACT!' upon arrival?
Received ON WET I,CE? Tomo
PROPER PRE,SERVATI'VER indicrated?
Roc eive,r1 WITHIN HOLDING 'TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
State Certification
Requested FL NC SC Other NA
Water Chlorinated Yes No NA
Sample Iced t.lpon Collection Y'es No
CMUD NPDES OTHER
LY 3 COPIES
TIME MATRIX
CLIENT DATE COLLECTED (SOIL,
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR
HOURS SLUDGE)
Sampler's Signature
Relinquished By: tSiuceiterel
(Slur-rah:gel
Relinquished By liSignatur
klethod el Shipment,.;,
J Fed E, j UPS J Hanni,clelivernd J Olher
NPDES:
10 NC
10 SC
LA OTHER
UST:
J NC
J SC
I'D OTHER
GROUNDWATER:
NC
SC
rJ OTHER
SAMPLE CONTAINER
*TYPE
SEE BELOW
NO,
SIZE
Sampled By (Print Name)
Received By: (Signature)
Received By Signature)
FileeiyacI For,Erism Latdprmbdos
. ,
DRINKING WATER: SOLIDWASTE;
LI NC NC
SC L.-A SC
'LI OTHER 1 OTHER
PRESvEERsVA
TIVES
-
AGRA:
J NG
rU SC
21. OTHER
CERCLA
NC
0 SC
LI OTHER
Date
Date
Da
Loe-in Cirqui4 No, ,
ANALYSES REQUESTED
Affiliation
ivtiiitdryddm,rs
LANDFILL
NC
J Sc
OTHER
OTHER:
f•J NC
SC
OTHER
REMARKS
Additional Comments:
SUBI PRISM
LAB
LAB
CERT.
IDNO
ID NO.
PRfSM US
Site Arrival Time,
Silo Depart dre
I Tech Fee
Mileage
*CONTAINER TYPE CODES: A Amber 0 Clear G = Glass P Plastic; TL 'Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
FINAL REPORT COPY

7/11/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
PRIsm
LABORATORIES,
Full Service A:yca & E.rvironniental Solutions
Page 1 of 4
Customer Project ID: Church Street
Customer Sample ID: EFFLUENT
Prism Sample ID: AC11929
Login Group: A079H2
Sample Collection Date/Time: 7/2/01 10:15
Lab Submittal Date/Time: 7/2/01 11:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATETTIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ARSENIC Not detected mg/L 0.010 60106 7/9/01 1134 MSC
BARIUM 0,086 mglL 0.010 60106 7/9/01 11:34 MSC
CADMIUM Not detected mg/L 0.001 6010B 7/9/01 11:34 MSC
CHROMIUM Not detected mg/L 0.005 60106 7/9/01 11:34 MSC
LEAD Not detected mg/L 0,005 6010B 7/9/01 11:34 MSC
SELENIUM Not detected mg/L 0.010 60106 7/9/01 11:34 MSC
SILVER Not detected mg/L 0.005 6010B 7/9/01 11:34 MSC
MERCURY, TOTAL Less than mg/L 0.0002 EPA 245,1 7/10/01 15:30 PRF
MERCURY DIGESTION Completed EPA 245;1 7/9/01 10:10 LC2
BROMODICHLOROMETHANE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
BROMOFORM Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
BROMOMETHANE Not detected ug/L 5 EPA 601/602 7/10/01 20:07 CMB
CARBON TETRACHLORIDE Not detected ug/L 1 EPA 601/602 7/10/01 20;07 CMB
CHLOROBENZENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
CHLOROETHANE Not detected ug/L 5 EPA 601/602 7/10/01 20:07 CMB
CHLOROFORM Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
CHLOROMETHANE Not detected ug/L 5 EPA 601/602 7/10/01 20:07 CMB
DIBROMOCHLOROMETHANE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
1,2-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
1,3-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
1,4-DICHLOROBENZENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601/602 7110101 20:07 CMB
1,1-DICHLOROETHANE Not detected ug/L. 1 EPA 601/602 7/10/01 20:07 CMB
1,2-DICHLOROETHANE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
1,1-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
1,2-DICHLOROPROPANE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
CIS-1,3-DICHLOROPROPENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601/602 7/10101 20:07 CMB
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road .aix RO. Box 240543 Chadotte, NC 28224-05.43
Phone: [phone] ..txron 1ree Numbcr: 1-8(C529-6364 1 Lt 7"04/5.25-0409

Irr-
ab Report
7/11/01
Law Eng & Env Services, Inc
Attn: Matt Gust's
PO Box 11297
Charlotte, NC 28220
PRISM
LABORATORIES, INC,
FA Service. Analytical 8 EnviTcrunentai Solon,
Page 2 of 4
Customer Project ID: Church Street
Customer Sample ID: EFFLUENT
Prism Sample ID: AC11929
Login Grouo: A079H2
Sample Collection Date/Time: 7/2/01 10:15
Lab Submittal DaterTime: 7/2/01 11:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
EDB Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
METHYLENE CHLORIDE Not detected ug/L 5 EPA 601/602 7/10/01 20:07 CMB
1,1,2,2-TETRACHLOROETHANE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
TETRACHLOROETHENE Not detected ugh. 1 EPA 601/602 7/10/01 20:07 CMB
1,1,1-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
1,1,2-TRICHLOROETHANE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
TRICHLOROETHENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
TRICHLOROFLUOROMETHANE Not detected ug/L 5 EPA 601/602 7/10/01 20:07 CMB
VINYL CHLORIDE Not detected ug/L 5 EPA 601/602 7/10/01 20:07 CMB
BENZENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
ETHYLBENZENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
IPE Not detected ug/L 5 EPA 601/602 7/10/01 20:07 CMB
MTBE Not detected ug/L 5 EPA 601/602 7/10/01 20:07 CMB
TOLUENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
TOTAL XYLENES Not detected ug/L 3 EPA 601/602 7/10/01 20:07 CMS
CIS-1,2-DICHLOROETHENE Not detected ug/L 1 EPA 601/602 7/10/01 20:07 CMB
METALS DIGEST-SURFACE/GROUNDW Competed SW846-3005 7/6/01 09:20 LC2
Sample Comments:
Angela D Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No, E87519
449 Spriogbrook Road .%. RO. Box 240543 Charlotte, NC 28224.-0543
Phone: 704,629-6364 Toll Fr: Numbtr: I -800/529-6364 Fax: [phone]

Fr
ab Report
7/11/01
Law Eng & Env Services, Inc
Attn: Matt Gustis
PO Box 11297
Charlotte, NC 28220
RISM.
LABORATORIES, INC,
Page 3 of 4
Customer Project ID: Church Street
Customer Sample ID: DW-2
Prism Sample ID: AC11930
Login Group: A079H2
Sample Collection Date/Time: 7/2/01 10:30
Lab Submittal Date/Time: 7/2/01 11:20
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
REPORTING METHODDATEITIM
T
E
EST TEST
PARAMETER ....._ _RESULT_,. UNITS LIMIT ...�. REFERENCE STARTED ANALYST
BROMODICHLOROMETHANE Nat detected ug/L 1
BROMOFORM Not detected ug/L 1
BROMOMETHANE Not detected ug/L 5
CARBON TETRACHLORIDE Not detected ug/L 1
CHLOROBENZENE Not detected ug/L 1
CHLOROETH.ANE Not detected ug/L 5
CHLOROFORM 2.0 ug/L 1
CHLOROMETHANE Not detected ug/L 5
DIBROMOCHLOROMETHANE Not detected ug/L 1
1,2-DICHLOR.OBENZENE Not detected ug/L 1
1,3-DICHLOROBENZENE Not detected ug/L 1
1,4-DICHLOROBENZENE Not detected ug/L. 1
DICHLOROD/FLUOROMETHANE Not detected ug/L 5
1,1-DICHLOROETHANE Not detected ug/L 1
1,2-DICHLOROETHANE Not detected ug/L 1
1,1-DICHLOROETHE.NE Not detected ug/L 1
TRANS-1,2-DICHLOROETHENE Not detected ug/L 1
1 „2-DICHLOROPROPANE Not detected ug/L 1
CIS-1,3-DICHLOROPROPENE Not detected ugfL 1
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5
EDB Not detected ug/L 1
METHYLENE CHLORIDE Not detected ug/L 5
1,1;2,2-TETRACHLOR.OETHANE Not detected ug/L 1
TETRACHLOROETHENE 5.9 ug/L 1
1„1,1-TRICHLOROETHANE Not detected ug/L 1
1,1,2-•TRICHLOROETHANE Not detected ug/L 1
TRICHLOR,OETHENE Not detected ug/L 1
TRICHLOROFLUOROMETHANE Not detected ug/L 5
VINYL CHLORIDE Not detected ug/L 5
CIS-1,2-DICHLORCETHENE Not detected ug/L 1
601 7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7110/0119:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10/0119:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7110/01 19:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10101 19:11 CMB
7/10/01 19:11 CMB
7110/01 19:11 CMB
7/10/01 19:11 CMB
7/10/0119:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10/0119:11 CMB
7/10/01 19:11 CMB
7/10/01 '19:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
7/10/01 19:11 CMB
601
601
601
601
601
601
601
601.
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
601
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springhrook,Round .► P.O. Box 210543 _. Charlotte, NC, 264 034_
Phone [phone] Ton free Number: ➢-800 529-6364 r t5)X 04/5254)401

7/11/ 1
Law Bng & Env Eeryi es Iris
Attn: Matt C uSti
PO Brix 1129
Charlotte, NC 2322
Customer Project 1D: Church St
Customer er m l+ ID:
Prism Sample ID: AC11930
Login Group: A079H2
Bageaf
pie Collection Date/Time: 7/2/01 19:30
Lab Submittal Date/Time: 7/2101 11:29
The folio ng anal iedl results have been obtained f+ r the indicated sample which was ubrr4itted to this laboratory.
TEST
a._ARAt�fETER
pie Comments:
TEST
RESULT
REPORTING iETHO
UNITS LIMIT REFERENCE STARTED
An brash .. Labnratr Services
DATEfl ME
ANALYST
NC Certification too. 402 - C Certification No S 012
PO
NC
!inking Wa
rC
No, 3773E - EL Certifictlan No, E7

PRISM
LABORATORIES, INC.
Full Service AnalyticalEnvironmental Solutions
Client
Physical Address
Phone
P.0,rt/Billing Reference
Project Name
Fax
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE #
449 Springbrook Road Charlotte, NC 2821.7
P.O. Box 240543 Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
REPORT TO: Name
Address
BILL TO: Name
Address
Requested Due Date J Day J 2 Day 1 3 Dy J 4 DaytiJ Days
,;:t 6-9 Days 1 Standard 10 days
Samples received after 15:00 will be processed the next b„usiness day,
Turnaround time is based on business. days, excluding' weekends and holidays.
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
CMUD NPDES
LAB USE ONLY • • . -• • • •
Samples INTACT upon errivai?
I Received ON WET ICE? Temp
.OPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS iNTACT?
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
State Certilication
Requested FL NC
Water Chlorinated Yes
YLE'l NC) N1A
SC Other NA
No NA
Sample Iced Upon Collection Yes No
OTHER
PRESS WWII FIRMLY 3 COPIES
TIME MATRIX ' SAMPLE CONTAINER
CLIENT OLLECTED
DATE (SOIL,
SAMPLE DESCRIPTION COLLECTED ' MILITARY WATER OR 'TYPE
HOURS SLUDGE) SEE BELOW NO, I SIZE 1
Sampler's Signature
RoiloquisheriEt)r (Signor:Yet
Re1ingUi:ribed I ISicinatirro
PlinquishEid Ely Signattne)
Method c.it Shipment:,
Fed Ex J UPS Hanciiilelivered j Omer
Sampled By (Print Name)
PRESERVA-
TIVES
ANA
Received By. (Sign.ature Date
Rectiivriki ly SOnature)
Receive For Prism L:a )ratofll Ely
Date
Dale
YSES REQUEST
Legatn Group MI
- .
Attitiation
illtary/Hours
NPDES: UST: GROUN.0 ATER: DRINKING WATER:
'C ..,1 NC j_i NC ,J NC
I -I SC I'.a SC 7.-ii SC
' LI OTHER I...I OTHER ,J OTHER
SOLID WASTE:
NC
SC
ij OTHER
RCRA: CE.RCLA LANDFILL OTHER:
INC INC INC .....1 NC
...i SC Lii SC :_.1 SC J SC
IJ OTHER l'A OTHER I...I OTHER i'j OTHER
REMARKS
Additional Comments:
- U8 PRISM
LAB
CERLAB
T.' 10 NO,
ID NO,
PRISM ONE ONLY
Arnwii T roc„
ature Time:
Field Tech Fee'
Mileage
TERMS & CONDITIONS
FINAL REPORT' COPY
DF rrincq- A 7 Arnhor =
G Glass P = Pfastici TL = leflon Lined Cap VOA Volatile Organics Analysis (Zero Head Space)

Char
Full Servirbta Ana ns
Prism Laboratories, Inc,
Report Prepared for Law Eng & Env Services, In
Project, Church St,
The information contained in this Electronic Delivery for Analytical Results is privileged and confidential
intended only for the use of the individual or entity named on the E-Mail address, If the reader of this
you are hereby notified that any dissemination, distribution or copying of this communication is wrongfu
you to civil liability, If you have received this communication in error, please immediately notify us by to
at [phone],
Prism Client Date Time Submittal Submittal Method Analyte Results
Sample ID Sample ID Collected Collected Date Time Reference Name
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 BROMODJ Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 BROMOF Not detect
AC12365 EFFLUEN 7/9/01 12;40 7/9/01 15:25 601 BROMOM Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 CARBON Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 CHLORO Not detect
AC12365 EFFLUEN 7/9/01 12,40 7/9/01 15:25 601 CHLORO Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 CHLORO Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 CHLORO Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 DIBROMO Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,2-DICHL Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,3-DICHL Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,4-DICHL Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 DICHLOR Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,1-DICHL Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,2-DICHL Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,1-DICHL Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 TRANS-1, Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,2-DICHL Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 CIS-1,3-DI Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 TRANS-1, Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 EDB Not detect
AC12365 EFFLUEN 7/9/01 12;40 7/9/01 15:25 601 METHYLE Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,1,2,2-TE Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 TETRACH Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,1,1-TRI Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 1,1,2-TRI Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 TRICHLO Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 TRICHLO Not detect
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 601 VINYL CH Not detect

AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15',25 601
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 EPA 245.1
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 EPA 245.1
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 6010B
AC12365 EFFLUEN 7/9/01 12:40 7/9101 15,25 6010E
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 6010E
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 6010B
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 6010B
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 6010E
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 6010B
AC12365 EFFLUEN 7/9/01 12:40 7/9/01 15:25 SW846-30
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13;.40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15;25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13'40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
A012366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13,40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 1140 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9101 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 1525 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:25 601
AC12366 DW-2 7/9/01 13:40 7/9/01 15:2.5 601
CIS-1,2-DI Not detect
MERCUR Less than
MERCUR Completed
ARSENIC Not detect
BARIUM 0,085
CADMIUM Not detect
CHROMIU Not detect
LEAD Not detect
SELENIU Not detect
SILVER Not detect
METALS Completed
BROMODI Not detect
BROMOF Not detect
BROMOM Not detect
CARBON Not detect
CHLORO Not detect
CHLORO Not detect
CHLORO 2.4
CHLORO Not detect
DIBROMO Not detect
1,2-DICHL Not detect
1,3-DICHL Not detect
1,4-DICHL Not detect
DICHLOR Not detect
1,1-DICHL Not detect
1,2-DICHL Not detect
1,1-DICHL Not detect
TRANS-1, Not detect
1,2-DICHL Not detect
CIS-1,3-DI Not detect
TRANS-1, Not detect
EDB Not detect
METHYLE Not detect
1,1,2,2-TE Not detect
TETRACH 1.7
1,1,1-TRI Not detect
1,1,2-TRI Not detect
TRICHLO Not detect
TRICHLO Not detect
VINYL CH Not detect
CIS-1,2-DI Not detect

Main Office:
449 prvnghrrook Road
:0. Box 240543
Charlotte,; NC 8 4-0 4
Phone : 7 4t 29-9 64
11 00t 364
Fax: 704,525-0409
Prepared y: Robb' Jones
Delivered Via Email 7/1 /01
of rrn tiun
essage is not the intended redolent,
plent
and may subject
lephone
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugdL
ug/L
ug/L
ug/L
ug/L
ug/L
L Analysis Analysis
Date Time
1 7/14/01 3: 1
1 7/14/01 3:1
7/14/01 3 51
1 7/14/01 3: a1
1 7/14/01 3:1
5 7114/01 3: a 1
1 7/14/01 3 1
5 7/14/01
1' 7/14/01
1 7/14/01 3:5
1 7/14/01 3: .1
1' 7/14/01 3: 1
5 7/14/01 3: 1
1 7/14/01 3: 1
1 7/14/01 3:51
1 7/14/01 3:1'
1 7/14/01 3:1
1 7/14/01 3: 1
7/14/01 3:1
5 7/14/01 3 1
1 7/14/01 3. a1
5 7/14/01 3: 1
1 7/14/01 3: 1
7714/01 3: 1
1 7/14/01 3~1
1' 7/14/01 ;1:51
1 7/14/01
7/14/01
7/14/01 51

ug/L 1 7/14/01 3:51
rig/L 0,0002 7/13/01 11: 7
7/11/01 12:45
mg/L 0.01 7/16/01 12:26
rig/L 0,01 7/16/01 12:26
mg/L 0.001 7/16/01 112:26
rig/L 0,005 7/16/01 12:26
rig/L 0.00 7/16/01 12:26
mg/L 0,01 7/16/01 12:26
r ig/L 0,005 7/16/01 12:26
7/13/01 13:21
ug/L 1 7/14/01 4:48
ug/L. 1 7/14/01 4:48
ug/L 5 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 5 7/14/01 4:48
ug/L 1' 7/14/01 4:48
ug/L. 5 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14`01 4:48
ugh.. 1 7/14/01 4:48
ug/L 5 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7114/01 4:48
ug/L 1 7/14/01 4:48
ug/L 6 7/14/01 4:4
ug/L 1 7/14101 4:48
ug/L 5 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 1 7/14/01 4:48
ug/L 5 7/14/61 4:48
ug/L 5 7/14/01 4:48
ug/L 1 7/14/01 4:48